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Home My WebLink AboutNCG060407_Monitoring Report_20220729NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG060000 Food and Kindred Ih Click harp fnr inctrurtinnc - W - - -- - - i, C v' "c7 Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DM bjjjj twit in 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR RSR Office. ^- Certificate of Coverage No. NCG060407 Person Collecting Samples: Amanda Farr Facility Name: Amazon.com Services LLC - RDU1 Laboratory Name: Eurofins Test America Savannah Facility County: Wake Laboratory Cert. No.: 269 Discharge during this period: ❑✓ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes 0 No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ✓❑ Yes ❑ No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Code Parameter Outfall001 Outfall002 Outfalf Outfall Outfall N/A Receiving Stream Class C;NSW C;NSW N/A Date Sample Collected MM/DD/YYYY 6/27/2022 6/27/2022 46529 24-Hour Rainfall in inches 0.2 0.2 C0530 TSS in mg/L (100 or 50*) 79 7.7 00400 pH in standard units (6.0 — 9.0 FW, 6.8-8.5SW) 8.69 8.38 Fecal Coliform per 100 ml of 31616 freshwater (if required) (1000) N/A N/A 61211 Enterococci per 100 ml of saltwater " N/A N/A (if required) ( Chemical Oxygen Demand in mg/L 00340 44 17 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A N/A 00552 Non -Polar Oil & Grease in mg/L ; N/A N/A Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of All other water classifications have a benchmark of (Freshwater) (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Zd2/4�1__ , Signature of Permittee or Delegated Authorized Individual cedrob@amazon.com Email Address 'x ?'ltc� Date (214) 534-7676 Phone Number urofins Environment Testing America ANALYTICAL REPORT Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-217493-1 Client Project/Site: Storm Water - Amazon Warehouses RDU1 For. ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Ig"a.AAA- lla"f ns Authorized for release by: 711212022 12:22:30 PM Roxanne Cisneros, Senior Project Manager (615)301-5761 rxanne.cisneros@et.eurofinsus.com Alt 2,9 �a JEJV& E ooresvr/Q �g.s al coon The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU 1 Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. ❑ Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative/Absent POS Positive / Present PQL Practical Quantitation Limit FIRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-217493-1 Eurofins Savannah Page 2 of 12 7/12/2022 Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU1 Lab Sample ID Client Sample ID Matrix Collected Received 680-217493-1 RDU1_Sample_Point_01_062722 Water 06/27/2217:00 06/28/2210:30 680-217493-2 RDU1_Sample_Point_02_062722 Water 06/27/2217:30 06/28/2210:30 Job ID: 680-217493-1 Page 3 of 12 Eurofins Sa'dWW2 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU1 Job ID: 680-217493-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-217493-1 Comments No additional comments. Job ID: 680-217493-1 Receipt The samples were received on 6/28/2022 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 5.90 C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Eurofins Savannah Page 4 of 12 7/12/2022 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU1 Job ID: 680-217493-1 Client Sample ID: RDU1_Sample_Point_01_062722 Lab Sample ID: 680-217493-1 Date Collected: 06/27/22 17:00 Matrix: Water Date Received: 06/28/22 10:30 General Chemistry Analyte Result Qualifier RL MDL Unit Total Suspended Solids 79 10 10 mg/L Chemical Oxygen Demand 44 10 5.0 mg/L Client Sample ID: RDU1_Sample_Point_02_062722 Date Collected: 06/27/22 17:30 Date Received: 06/28/22 10:30 General Chemistry Analyte Result Qualifier RL MDL Unit Total Suspended Solids 7.7 2.5 2.5 mg/L —Chemical Oxygen Demand 17 10 5.0 mg/L Page 5 of 12 D Prepared Analyzed Dil Fac 06/30/22 14:19 1 07111/2213:03 1 Lab Sample ID: 680-217493-2 Matrix: Water D Prepared Analyzed Dil Fac 06/30/22 14:19 1 07/11 /22 13:03 1 Eurofins Savannah 7/12/2022 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU1 Method: 254OD-2015 - Total Suspended Solids (Dried at 103-1050 Lab Sample ID: MB 680-728593/1 Matrix: Water Analysis Batch: 728593 MB MB Analyte Result Qualifier RL MDL Unit LTotal Suspended Solids <2.5 2.5 2.5 mg/L Lab Sample ID: LCS 680-72859312 Matrix: Water Analysis Batch: 728593 Analyte LTotal Suspended Solids Lab Sample ID: LCSD 680-728593/3 Matrix: Water Analysis Batch: 728593 Analyte Total Suspended Solids Job ID: 680-217493-1 Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 06/30/22 14:19 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 951 806 mg/L 85 80 - 120 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 951 798 mg/L 84 80 - 120 1 25 Method: 5220D-2011 - Chemical Oxygen Demand Lab Sample ID: MB 680-730044/3 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 730044 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac LChemical Oxygen Demand <5.0 10 5.0 mg/L 07/11/22 13:03 1 Lab Sample ID: LCS 680-730044/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 730044 Analyte Chemical Oxygen Demand Lab Sample ID: 680-217493-2 MS Matrix: Water Analysis Batch: 730044 Analyte Sample Sample Result Qualifier (Chemical Oxygen Demand 17 Lab Sample ID: 680-217493-2 MSD Matrix: Water Analysis Batch: 730044 Sample Sample Analyte Result Qualifier Chemical Oxygen Demand 17 Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 50.0 48.2 mg/L 96 90 -110 Client Sample ID: RDU1_Sample_Point_02 062722 Prep Type: TotalINA Spike MS MS %Rec Added Result Qualifier Unit D %Rec Limits 50.0 72.2 mg/L 109 90 -110 Client Sample ID: RDU1_Sample_Point_02_062722 Prep Type: Total/NA Spike MSD MSD %Rec RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 50.0 71.5 mg/L 108 90 - 110 1 30 Eurofins Savannah Page 6 of 12 7/12/2022 QC Association Summary Client: ERM-West Job ID: 680-217493-1 Project/Site: Storm Water - Amazon Warehouses RDU1 General Ch Analysis Batch: 728593 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217493-1 RDU1_Sample_Point_01_062722 Total/NA Water 2540D-2015 680-217493-2 RDU1_Sample_Point_02_062722 Total/NA Water 2540D-2015 MB 680-728593/1 Method Blank Total/NA Water 2540D-2015 680-728593/2 Lab Control Sample Total/NA Water 2540D-2015 �LCS LCSD 680-728593/3 Lab Control Sample Dup Total/NA Water 2540D-2015 Analysis Batch: 730044 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217493-1 RDU1_Sample_Point_01_062722 Total/NA Water 5220D-2011 680-217493-2 RDU1_Sample_Point_02_062722 Total/NA Water 5220D-2011 MB 680-730044/3 Method Blank Total/NA Water 5220D-2011 LCS 680-730044/4 Lab Control Sample Total/NA Water 5220D-2011 680-217493-2 MS RDU1_Sample_Point_02_062722 Total/NA Water 5220D-2011 680-217493-2 MSD RDU1_Sample_Point_02_062722 Total/NA Water 5220D-2011 Eurofins Savannah Page 7 of 12 7/12/2022 Lab Chronicle Client: ERM-West Job ID: 680-217493-1 Project/Site: Storm Water - Amazon Warehouses RDU 1 Client Sample ID: RDU1_Sample_Point_01_062722 Lab Sample ID: 680-217493-1 Date Collected: 06/27/22 17:00 Matrix: Water Date Received: 06/28/22 10:30 Batch Batch [Prep Dil Initial Final Batch Prepared Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 2540D-2015 1 250 mL 1000 mL 728593 06/30/22 14:19 PG TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL 2 mL 730044 07/11/22 13:03 ALG TAL SAV IL Instrument ID: SPC7 Client Sample ID: RDU1_Sam ple_Point_02_062722 Date Collected: 06/27/22 17:30 Date Received: 06/28/22 10:30 Lab Sample ID: 680-217493-2 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 2540D-2015 1 1000 mL 1000 mL 728593 06/30/22 14:19 PG TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL 2 mL L Instrument ID: SPC7 Laboratory References: TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 730044 07/11/22 13:03 ALG TAL SAV Eurofins Savannah Page 8 of 12 7/12/2022 Accreditation/Certification Summary Client: ERM-West Job ID: 680-217493-1 Project/Site: Storm Water - Amazon Warehouses RDU1 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW) State 269 12-31-22 Eurofins Savannah Page 9 of 12 7/12/2022 Method Summary Client: ERM-West ProjecUSite: Storm Water -Amazon Warehouses RDU1 Method Method Description 254OD-2015 Total Suspended Solids (Dried at 103-105°C) 5220D-2011 Chemical Oxygen Demand Protocol References: SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Job ID: 680-217493-1 Protocol Laboratory SM TAL SAV SM TAL SAV Eurofins Savannah Page 10 of 12 7/12/2022 t-n: /Qnian -MA ! 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The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Job Number: 680-217493-1 List Source: Eurofins Savannah Eurofins Savannah Page 12 of 12 7/12/2022 "+-+..1 .r ir'...� i'!^ • L._'l: •j is .. •t `�; �i . ..t}+ •:t 1 , 1 _ ' -;. - - `.r-t! •-.p•n � iti _:f�i.�r Alt. ': 'lt,�y ��;}� S'r} �1.� ,• lYS ,�I~ L' I.r= rl ` :�itl _.. +-. .fr �.-. .••�' � ��'-. .:`. .+, in, t' •�1 is- t :•,t'.tl �- �. -:1-� _i •. II --- ,•. - r,- • slizi4i • 'y; ._..i ( � - !'• ! �.` 1. �-:.r :r. �{,Y.. � I- r.._ I 'r _ . i. rr -, _. :, it t r.':•-. �_ .. jj t 1• Vvzr +.♦ �' ._ �.r�_'� �'..:r S:If'fl ..+:. .I- �J• -- �• y - �.. 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