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Home My WebLink AboutNCG060407_Monitoring Report_20211101NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG060000 �� ! Food and Kindred o �✓ Click here for instructions °,dam o� p 0 2 Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DU%qoIo@0Aprm\ in 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate NP&Rei'Okal Nce. Certificate of Coverage No. NCG06 0407 Person Collecting Samples: Bing Bai Facility Name: Amazon.com Services LLC - RDUt Laboratory Name: Eurofins TestAmerica Facility County: Wake Laboratory Cent. No.: 269 Discharge during this period: +I Yes No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? 17 Yes + No If so, which Tier (1, 11, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Q Yes [—]No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall001 Outfall002 Outfall Outfall Outfall Code N/A Receiving Stream Class C, NSW C, NSW N/A Date Sample Collected MM/DD/YYYY 9/22/2021 9/22/2021 46529 24-Hour Rainfall in inches 0.4 0.4 C0530 TSSin mg/L(100 or SO*) 39 26 00400 pH in standard units (6.0-9.0 FW, 7.04 7.13 6.8-8.5SW) 00556 Oil & Grease in mg/L (30) N/A N/A Fecal Coliform per 100 ml of 31616 freshwater (if required) 1000) N/A N/A 61211 Enterococci per 100 ml of saltwater N/A N/A (if required) (SOO Chemical Oxygen Demand in mg/L 00340 (120) 13 12 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A N/A 00552 1 Non -Polar Oil & Grease in mg/L (15) N/A IN/A • Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of SO mg/L. All other water classifications have a benchmark of 100 mg/L FW (Freshwater) SW (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best 4my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, includip(gkhe possibility of fines and imprisonment for knowing violations." of Permittee or Delegated Authorized Individual boese@zmazon.com Email Address 4 Date (214)326-3468 Phone Number .............. LINKS eurofins Environment Testing America ANALYTICAL REPORT Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-204895-1 Laboratory SDG: 4851 Jones Sausage Rd, Garner NC 27529 Client Project/Site: Storm Water - Amazon Warehouses (RDU1) For: ERM-Northeast One Beacon Steet 5th Floor Boston, Massachusetts 02108 Attn: Ms. Melissa Pierce Rna-%. Caftevurns Authorized for release by: 101412021 3:32:27 PM Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros@Eurofinset.com The test results in this report meet all 2003 NELAC. 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. C Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-Northeast Job ID: 680-204895-1 Project/Site: Storm Water- Amazon Warehouses (RDW) SDG: 4851 Jones Sausage Rd, Garner NC 27529 L Glossary Abbreviation These commonly used abbreviations may or may not be present In this report o Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoDlDOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) - MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated NO Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit FIRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 2 of 13 10/4/2021 Sample Summary Client: ERM-Northeast Job ID: 680-204895-1 Project/Site: Storm Water - Amazon Warehouses (RDU1) SDG: 4851 Jones Sausage Rd, Garner NC 27529 Lab Sample ID Client Sample ID Matrix Collected Received 680-204895-1 RDU1-OF01-20210922 Water 09122/2113:50 09/23/2110:30 680-204895-2 RDU1-OF02-20210922 Water 09/22/2113:25 09/23/2110:30 Page 3 of 13 Eurofins TestAmerica, SaIMMWIl Case Narrative Client: ERM-Northeast Job ID: 680-204895-1 Project/Site: Storm Water -Amazon Warehouses (RDU1) SDG: 4851 Jones Sausage Rd, Gamer NC 27529 Job ID: 680-204895-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job Narrative 680-204896-1 Comments No additional comments. Receipt The samples were received on 9/23/2021 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 4.7° C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 13 10/4/2021 Client Sample Results Client: ERM-Northeast Project/Site: Storm Water - Amazon Warehouses (RDU1) Client Sample ID: RDU1-OF01-20210922 Date Collected: 09/22/21 13:50 Date Received: 09/23/21 10:30 Job ID: 680-204895-1 SDG: 4851 Jones Sausage Rd, Garner NC 27529 Lab Sample ID: 680-204895-1 Matrix: Water General Chemistry — Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Chemical Oxygen Demand 13 10 5.0 mg/L 10/04/21 12:52 1 Total Suspended Solids 39 2.5 2.5 mg/L 09/28/21 18:14 1 Eurofins TestAmerica, Savannah Page 5 of 13 10/4/2021 Client Sample Results Client: ERM-Northeast Job ID: 680-204895-1 Project/Site: Storm Water- Amazon Warehouses (RDU1) SDG: 4851 Jones Sausage Rd, Garner NC 27529 Client Sample ID: RDU1-OF02-20210922 Lab Sample ID: 680-204895-2 Date Collected: 09/22/21 13:25 Matrix: Water Date Received: 09/23/21 10:30 General Chemistry Analyte Result qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand 12 10 5.0 mg/L 10/04/21 12:52 1 Total Suspended Solids 26 2.5 2.5 mg/L 09/28/21 18:14 1 Eurofins TestAmerica, Savannah Page 6 of 13 10/4/2021 QC Sample Results`'"; Client: ERM-Northeast Job ID: 680-204895-1 - Project/Site: Storm Water - Amazon Warehouses (RDU1) SDG: 4851 Jones Sausage Rd, Garner NC 27529 Method: 5220D-2011 - Chemical Oxvaen Demand Lab Sample ID: MB 680-68784813 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 687848 - Me MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 10/04/21 12:52 1 Lab Sample ID: LCS 680-687848/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 687848 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 50.0 44.8 mg/L 90 90-110 Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 680-687021/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 687021 MB Ma Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac Total Suspended Solids <2.5 2.5 2.5 mg/L 09/28/21 18:14 1 Lab Sample ID: LCS 680-687021/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 687021 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 834 mg/L 88 80-120 Lab Sample ID: LCSD 680-68702113 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 687021 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 830 mg/L 87 80-120 0 25 Eurofins TestAmerica, Savannah Page 7 of 13 10/4/2021 QC Association Summary Client: ERM-Northeast Project/Site: Storm Water - Amazon Warehouses (RDU1) General Analysis Batch: 687021 Job ID:680-204895-1 SDG: 4851 Jones Sausage Rd, Garner NC 27529 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-204895-1 RDU1-OF01-20210922 TbtaVNA Water SM 2540D 680-204895-2 RDUl-OF02-20210922 Total/NA Water SM 2540D MB 680-687021/1 Method Blank TotaUNA Water SM 2540D LCS 680-687021/2 Lab Control Sample TotaUNA Water SM 2540D LCSD 680-687021/3 Lab Control Sample Dup TotaVNA Water SM 2540D Analysis Batch: 687848 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-204895-1 RDU1-OF01-20210922 TotaUNA Water 5220D-2011 680-204895-2 RDUl-OF02-20210922 TotaUNA Water 5220D-2011 MB 680-68784813 Method Blank TotaUNA Water 5220D-2011 LCS 680-687848/4 Lab Control Sample TotaUNA Water 5220D-2011 Eurofins TestAmerica, Savannah RNI Page 8 of 13 10/4/2021 Lab Chronicle Client: ERM-Northeast Job ID: 680-204895-1 Project/Site: Storm Water - Amazon Warehouses (RDU 1) SDG: 4851 Jones Sausage Rd, Garner NC 27529 Client Sample ID: RDU1 -OFO1 -20210922 Lab Sample ID: 680-204895-1 Date Collected: 09/22/21 13:50 Matrix: Water Date Received: 09/23/21 10:30 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 52201)-2011 1 2mL 2 mL 687848 10I04/21 12:52 ALG TAL SAV Instrument ID: SPC7 Total/NA Analysis SM 25400 1 1000 mL 1000 mL 687021 09/28/21 18:14 PG TAL SAV Instrument ID: NOEQUIP Client Sample ID: RDU1-OF02-20210922 Date Collected: 09/22/21 13:25 Date Received: 09/23/21 10:30 Lab Sample ID: 680-204895-2 Matrix: Water Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 5220D-2011 1 2 mL 2 mL 687848 10/04/21 12:52 ALG TAL SAV Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 1000 mL 1000 mL 687021 09/28/21 18:14 PG TAL SAV Instrument ID: NOEQUIP Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 9 of 13 10/4/2021 Accreditation/Certification Summary Client: ERM-Northeast Job ID: 680-204895-1 Project/Site: Storm Water- Amazon Warehouses (RDU1) SDG: 4851 Jones Sausage Rd, Gamer NC 27529 Laboratory: Eurofins TestAmerica, Savannah The accreditation/certifications listed below are applicable to this report, Authority Program Identification Number Expiration Date North Carolina (WW/SW) State 269 12-31-21 0 Eurofins TestAmerica, Savannah Page 10 of 13 10/4/2021 Method Summary Client: ERM-Northeast Project/Site: Storm Water - Amazon Warehouses (RDU 1) Job ID: 680-204895-1 SDG: 4851 Jones Sausage Rd, Garner NC 27529 Method Method Description Protocol 5220D-2011 Chemical Oxygen Demand SM SM 2540D Solids, Total Suspended (TSS) SM Protocol References: SM = "Standard Methods For The Examination Of WaterAnd Wastewater" Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Laboratory TAL SAV TAL SAV Eurofins TestAmerica, Savannah Page 11 of 13 10/4/2021 Eurofns TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Phone: 912.354.785E Fax: 912-352-0165 Chain of Custody Record �[+eurofins Envbo eel raeuex America Client Information SNnper N Brt I Lae PM Cisneros. Roxanne Gmar Tocanq NN.) CM N. 240-86684-33172 1 CM1we CPnwa Doug Wade /y `7 o - q-1 i Z EJAaY roxanm.asneros@Euro6nseLcom sm. dpgn Pape Page 1 of 1 epmpenx ERM-west PWsit) Analysis Requested Add,... 1920 Main Street Sude 300 pW pre R-,. hid: — S o j Z `P L G N Z a o :. ^ C p O Z � r Pm..rvatbn CodaC A-HCL M-He. E`NROH N-None C-Zn Acetate 0-MM02 D - Nick And P-Na204S E-111aHs04 G-WS03 F-10i R-Ne25203 G - A Phor s.H2s04H-Aumeicaee T � TSP Guded."ti, I.b G-Anbne i - IN WMI yVY-MCAA L-EOA Z-dear (ePedhl Doer. GN lfVlm TAT aeyuested(di s): sNb. Z.p CA. 92614 CanPNr Preledb d Yea A No Prom, 443-812-0046(Tel) Po/ Purchase Order Requested EmM1 doug.Wade@erm.com wo. Props Name Raleigh. NC prgect/ 24024260 sne lri r i 1' SSGw/ E ya O � 6 9 G; Sample Identification Sample Date Sample Time Sample TyM (Cacpmp, G= rab Matrix 1. O+xw.A n.re.,..Am S bl ImlrudionsMote: Preservation Code: S N I IX 0L1►' —202 J 2 ss D (3� O dj Water til k J j :2 - is7 water k k V ✓ Ib -A" — — wsr.r tlla101 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII 680-204895 Chain of Cu r IIIIIIIIIIIIIIIIIIIIIIIII Brody Possible Hazard Idendlica0on IX Non -Hamel =Flammable Skin Irritant CD Poison a Ej Unknown C--1 RadologCal - -- Sample Disposal (A fee may be sssassed if samples arc retained longer than 1 month) 0 Return To Client DQDis sal By Leb Archwe For Months Deliverable Requested, 1. It, III. IV, Other (specify) Special Instructiowi Requirements. Empty Kit Relinquished by: Irma,: Meibod a she . Re.rr),.WyM B- r t 0al.rr %�2 i Comparq R.p,aed br (nwhim 5_z 3 z r /o10 coin P Rexr9sdras company Refined by DaM/TYne Canpan Relenr by Didarina en,w), Pori try DaYRna 'Cmrony Custody Seals Intact A Yes A No Custody Seal Na Coaw T.mp.r...(,)'C aW Dins R., .� .31t Ver. 86408/2021 Client: ERM-Northeast Login Number: 204896 List Number: 1 Creator: Sims, Robert D Question Login Sample Receipt Checklist Job Number: 680-204895-1 SDG Number: 4851 Jones Sausage Rd, Gamer NC 27529 List Source: Eurofins TestAmerica, Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey NIA meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1 /4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins TestAmerica, Savannah Page 13 of 13 10/4/2021