NCG060398_Monitoring Report_20220121

NCDEQ Division of Energy, Mineral and Land Resources
7—
m°
Stormwater Discharge Monitoring Report (DMR) Form for NCGO60000
am,
Food and Kindred
m@zrO�f
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload I'm vt"in
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR ReMonal Office.
Certificate of Coverage No. NCG06 0398
Person Collecting Samples: Madison Shoemaker
Facility Name:ServicesLaboratory
Name: EuTofins TestAmerica Savannah
Facility County: M klenbur
Laboratory Cert. No.: 269
Discharge during this period: Yes
❑
No rfno, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes E]No
If so, which Tier (I,11, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Q Yes [—]No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
parameter
OutfaB
Outfau
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
001
002
N/A
Date Sample Collected MM/DD/YYYY
10/28/2021
10/28/2021
46529
24-Hour Rainfall in inches
0.1
0.1
C0530
TSSin mg/L (100or50')
38
1
00400
pH in standard units (6.0-9.0 FW,
7.34
7.54
6.8-8.5SW)
31616
Fecal Coliform per 100 mlof
freshwater (if required) (1000)
N/A
N/A
61211
Enterococci per 100 ml of saltwater
N/A
N/A
(if required) (S00)
00340
Chemical Oxygen Demand in mg/L
5.3
<5.0
(120)
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
NCOIC
Estimated New Motor/Hydraulic Oil
N/A
N/A
Usage in gal/month
00552
1 Non -Polar Oil & Grease in mg/L (15)
1 1.71
1<0.74
" Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. Ali other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible forgathering the information, the Information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false infokmation,lncludingthe possibility of fines and Imprisonment for knowing violations."
Signature of Permittee or Delegated Authorized Individual
[e-mail]
Email Address
Date
[phone]
Phone Number

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-206738-1
Laboratory SDG: 3830 Parrott Drive, Charlotte, NC 28214
Client Project/Site: Storm Water - Amazon Warehouses (DLT1)
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Rn&^*U Cc'"Ivs
Authorized for release by.
1111012021 4:37:43 PM
aPr O
0
Roxanne Cisneros, Senior Project Manager °
[phone]
roxanne.cisnerosgEurofinset.com
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
❑1

Definitions/Glossary
Client: ERM-West Job ID: 680-206738-1
Project/Site: Storm Water - Amazon Warehouses (DLT1) SDG: 3830 Parrott Drive, Charlotte, NC 28214
Qualifiers - -- - - - -
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present In this report.
a Listed under the"0" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative/Absent
PCs Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Savannah
Page 2 of 14 11/10/2021

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Case Narrative
Client: ERM-West
ProjecttSite: Storm Water -Amazon Warehouses (DLT1)
Job ID: 680-206738-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
Job ID: 680-206738-1
SDG: 3830 Parrott Drive, Charlotte, NC 28214
a
680-2067384
Comments
No additional comments.
Receipt
The samples were received on 11/1/2021 9:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 0.50 C.
General Chemistry
Methods 1664A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 680-692593.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerica, Savannah
Page 4 of 14 11/10/2021

Client Sample Results
Client: ERM-West Job ID: 680-206738-1
Project/Site: Storm Water -Amazon Warehouses (DLT1) SDG: 3830 Parrott Drive, Charlotte, NC 28214
Client Sample ID: DLT1_Sample_Point 01 20211028 Lab Sample ID: 680-206738-1
Date Collected: 10/28/21 16:10 Matrix: Water
Date Received: 11/01/21 09:30
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
D8 Fac
Oil B Grease (HEM)
1.7 J
2.6
0.74
mg/L
11/0321 08:31 11/0321 11:05
1
Total Suspended Solids
38
5.0
5.0
mg/L
11/0221 19:43
1
Chemical Oxygen Demand
5.3 J
10
5.0
mg/L
11/1021 10:36
1
Eurofins TestAmerica, Savannah
Page 5 of 14 11/10/2021

Client Sample Results
Client: ERM-West Job ID: 680-206738-1
Project/Site: Stone Water -Amazon Warehouses (DLT1) SDG: 3830 Parrott Drive, Charlotte, NC 28214
Client Sample ID: DLT2_Sam ple_Point_02_20211028 Lab Sample ID: 680-206738-2
Date Collected: 10/28/21 16:30 Matrix: Water
Date Received: 11101/21 09:30
General Chemistry
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed DO Fac
Oil & Grease (HEM)
<0.74
2.6
0.74 mg/L
11/0321 08:31 11/0321 11:05 1
Total Suspended Solids
15
2.5
25 mg/L
1110221 19:43 1
Chemical Oxygen Demand
<5.0
10
5.0 mg/L
11/1021 10:36 1
Eurofins TestAmenca, Savannah
Page 6 of 14 11/10/2021

QC Sample Results
Client: ERM-West
Project/Site: Stone Water - Amazon Warehouses (DLT1)
Method: 1664A - HEM and SGT-HEM
Lab Sample ID: MB 680-69259311-A
Matrix: Water
Analysis Batch: 692671
MB. MB.
Analyte Result Qualifier
Oil & Grease (HEM) 11..4
Lab Sample ID: LCS 680-69259312-A
Matrix: Water
Analysis Batch: 692671
Analyte
Oil & Grease (HEM)
Lab Sample ID: LCSD 680-692693/3-A
Matrix: Water
Analysis Batch: 692671
Analyte
Oil & Grease (HEM)
Job ID: 680-206738-1
SDG: 3830 Parrott Drive, Charlotte, NC 28214
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 692593
RL MDL Unit D Prepared Analyzed DII Fac
5.0 1..4 mg/L 11/03/2108:31 11/032111.:05. 1,
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 692593
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
40.0 34.00 mg/L 85 78-114
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 692593
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
40.0 32.40 mg/L 81 78-114 5 18
Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C)
Lab Sample ID: MB 680-69255911 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 692559
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac
Total Suspended Solids <2.5 2.5 2.5 mg/L 1110221 19:43 1
Lab Sample ID: LCS 680-69256912 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 692559
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 951 824 mg/L 87 80 - 220
Lab Sample ID: LCSD 680-692559/3 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: TotallNA
Analysis Batch: 692559
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Total Suspended Solids 951 824 mg/L 87 80-120 0 25
Method: 410.4-1993 R2.0 - COD
Lab Sample ID: MB 680-69376213 Client Sample ID: Method Blank
Matrix: Water Prep Type: TotalINA
Analysis Batch:693762
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Chemical Oxygen Demand <5.0 10 5.0 mg/L 1111021 10:36 1
Eurofins TestAmerica, Savannah
Page 7 of 14
11/10/2021

QC Sample Results
Client: ERM-West
Project/Site: Storm Water -Amazon Warehouses (DLT1)
Method: 410.4-1993 R2.0 - COD (Continued)
Lab Sample ID: LCS 680-693762/4
Matrix: Water
Analysis Batch: 693762
Analyte
Chenucal. Oxygen. Demand
Job ID:680-206738-1
SDG: 3830 Parrott Drive, Charlotte, NC 28214
spike LCS LCS
Added Result Qualifier
50.0 51..5
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit D %Rec Limits
mg/L 11(13 9D.,110
Eurofins TestAmerica, Savannah
Page 8 of 14 11/10/2021

QC Association Summary
Client: ERM-West Job ID: 680-206738-1
Project/Site: Storm Water - Amazon Warehouses (DLT1) SDG: 3830 Parrott Drive, Charlotte, NC 28214
General Chemistry
Analysis Batch: 692559
Lab Sample ID
Client Sample 1D
Prep Type
Matrix
Method Prep Batch
680-206738-1
DLT1_Sample_Point 01_20211028
Total/NA
Water
2540 D-2011
680-206738-2
DLT2 Sampte_Point 02 20211026
TbtaVNA
Water
26400-2011
MB 680-692559/1
Method Blank
TotalINA
Water
2540 D-2011
LCS 680-692559/2
Lab Control Sample
Total/NA
Water
2640 D-2011
LCSD 680-69255913
Lab Control Sample Dup
Total/NA
Water
2540 D-2011
Prep Batch: 692593
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-206738-1 -
DLT1_Sample_Point_01_20211028
TotaVNA
Water
1664A
680-206738-2
DLT2_Sample_Point02_20211028
Total/NA
Water
1664A
MB 680-69259311-A
Method Blank
Total/NA
Water
1664A
LCS 68"92593/2-A
Lab Control Sample
TotaVNA
Water
1664A
LCSD 680�692593/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
Analysis Batch: 692671
Lab Sample ID
Client Sample b
Prep Type
Matrix
Method
Prep Batch
680-206738-1
DLT1_Sample_Pcint_01_20211028
TotayNA
Water
1664A
692593
680-206738-2
DLT2_Sample_Point _02_20211029
Total/NA
Water
1€64A
692593
MB 680-692593/1-A
Method Blank
TotaVNA
Water
1664A
692593
LCS680B92593/2-A
Lab Control Sample
Total/NA
Water
1664A
692593
LCSD 680-692593/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
692593
Analysis Batch: 693762
Lab SamplelD
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-206738-1
DLT1_Sample_Point_01_20211028
Total/NA
Water
410.4-1993 R2.0
680-206738-2
DLT2_Sampie_Point 02_2021t028.
TotaVNA
Water
41.0.4-1993R2.0
MB 680-69376213
Method Blank
Total/NA
Water
410.4-1993 R2.0
LCS 6W-693.7WN
Lab. Control. Sample
Total/NA
Water
410.4-1993R20
Eurofins TestAmerica, Savannah
Page 9 of 14 11/10/2021

Lab Chronicle
Client: ERM-West
Project/Site: Storm Water -Amazon Warehouses (DLT1)
Client Sample ID: DLT1_Sample_Point_01_20211028
Date Collected: 10/28121 16:10
Date Received: 11/01/21 09:30
Job ID: 680-206738-1
SDG: 3830 Parrott Drive, Charlotte, NC 28214
Lab Sample ID: 680-206738-1
Matrix: Water
Batch
Batch
Dil Initial Final Batch
Prepared
Prep Type
Type
Method
Run Factor Amount Amount Number
or Analyzed
Analyst Lab
TotaVNA
Prep
1664A
950 mL 500 ­mL 692593
11/0321 08:31
JAB TAL SAV
TctaVNA
Analysis
11
1. 692671
11/032111:05
JAS TAL SAV
Instrument ID: NoEquip
TotaVNA Analysis 2640-D-2011 1 500 mL
Instrument ID: NOEQUIP
TotaVNA Analysis 410.4-1993 R2.0 1 2 mL
Instrument ID: SPC7
Client Sample ID: DLT2_Sample_Point 02_20211028
Date Collected: 10/28/21 16:30
Date Received:11/01121 09:30
1000 mL 692559 11 /0221 19:43 PG TAL SAV
2 mL 693762 11/1021 10:36 ALG TAL SAV
Lab Sample ID: 680-206738-2
Matrix: Water
Batch Batch
oil
Initial
Final
Batch
Prepared
Prep Type
Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
TotaVNA
Prep 1664A
950 mL
500 mL
692593
11/0321 08:31
JAS
TAL SAV
TotaVNA
Analysis 1664A
1
692671
11/032111:05
JAS
TAL SAV
Instrument ID: NoEquip
TotaVNA
Analysis 2540 D-2011
1
1000 mL
1000 mL
692559
11/0221 19:43
PG
TAL SAV
Instrument ID: NOEQUIP
TotaVNA
Analysis 410.4-1993 R2.0
1
2 mL
2 mL
693762
11/1021 10:36
ALG
TAL SAV
Instrument ID: SPC7
Laboratory References:
TAL SAV= Euroflns TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 10 of 14 11/10/2021

Accreditation/Certification Summary
Client: ERM-West Job ID: 680-206738-1
Project/Site: Storm Water -Amazon Warehouses (DLT1) SDG: 3830 Parrott Drive, Charlotte, NC 28214
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
�Authanty Program Identification Number Expil"M rate
North Carolina (WW/Sv) State 269 12-31-21
0
Eurofins TestAmerica, Savannah
Page 11 of 14 11/10/2021

Method Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses (DLT1)
•a_a�_r ■��at��r
1664A HEM and SGT-HEM
2540 D-2011 Total Suspended Solids (Dried at 103-105°C)
410.4-1993 R2.0 COD
1664A HEM and SGT-HEM (Aqueous)
Job ID: 680-206738-1
SDG: 3830 Parrott Drive, Charlotte, NC 28214
Protocol
Laboratory
1664A
TAL SAV
SM
TAL SAV
MCAWW
TAL SAV
1664A
TAL SAV
Protocol References:
1664A = EPA-821-98-002
MCAWW'= "Methods For Chemical Analysis Of WaterAnd' Wastes", EPA-600/4-79-020, March 1`983 And' Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV*= Eurofins TestAmerica, Savannah, 51'02 LaRoche Avenue, Savannah, GA 31404, TEL [phone]a
Eurofins TestAmerica, Savannah
Page 12 of 14 11 /10/2021

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Client Information
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Cisneros Rosanne
24087324-333311
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Doug Wade
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Sample Identification
Sample Date
Sample
Time
Sample Matrix
Type h..�
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G• rab .,�
Preservation Code
Special lnsWctionslNple:
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Chain of Custody
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Possible Na:artl Identification
L"NOn-Ra4ard =Flammable �Skmlrritanl GPOROns UUnkrtown LiRadolognai
Sa_,le Disposal ( A fee may be assessed if samples are retained longer Man 1 month)
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Login Sample Receipt Checklist
Client: ERMrlillest
Login Number: 206738
List Number..1
Creator: Hartley, Tyler
Questien
Job Number: 680-206738-1
SDG Number: 3830 Parrott Drive, Charlotte, NC 28214
List Source: Eurofins TestAmerica, Savannah
Aus` u Cammenit
Radioactivity wasn't checked or is </= background as measured by a survey
NIA
Meter -
The cooler's custody seal, if present, is intact.
True
Sample custodr seals-, if present, are intact..
True.
The cooler or samples do not appear to have been compromised or
True
tarnpered• with:
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
QQQ is filled. Qut.in. ink- and legible..
True
COC is filled out with all pertinent information.
True
Is the Field Sampler`s name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection datettimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sampla Rreservation. Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4').
Muliiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
Eurofins TestAmerica, Savannah
Page 14 of 14 11/10/2021