NCG060396_Monitoring Report_20220719

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG060000
Food and Kindred
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) I forw��ithir��
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEML a0nal Bt�yce.
Certificate of Coverage No. NCG060396
Person Collecting Samples: Parker Cliatt
Facility Name: Amazon.com Services LLC - CLT3
Laboratory Name: Eurofins Test America Savannah
Facility County: Cabarrus
Laboratory Cert. No.: 269
Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes Q No
If so, which Tier (I, II, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ✓❑ Yes ❑ No
Date Uploaded: eo --
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall001
Outfall002
Outfall003
Outfall004
Outfall
N/A
Receiving Stream Class
C
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
6/14/2022
6/14/2022
6/14/2022
6/14/2022
46529
24-Hour Rainfall in inches
0.5
0.5
0.5
0.5
C0530
TSS in mg/L (100 or 50*)
11
59
14
4.3
pH in standard units (6.0-9.0 FW,
00400
6.8 — 8.5 SW)
7.84
7.36
7.86
6.86
Fecal Coliform per 100 ml of
31616
freshwater (if required) (1000)
N/A
N/A
N/A
N/A
Enter cocci per 100 ml of saltwater
61211
(if required) (500)
N/A
N/A
N/A
N/A
Chemical Oxygen Demand in mg/L
00340
9.9
5.5
<5.0
<5.0
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
N/A
N/A
N/A
00552
Non -Polar Oil & Grease in mg/L ,1�: i
N/A
I N/A
I N/A
I N/A
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of SC,r;r,%i. All other water classifications have a benchmark of
Fv,v (Freshwater) v (saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to th best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false informatiok, it cluding the possibility of fines and imprisonment for knowing violations."
or Delegated Authorized Individual
[e-mail]
Email Address
0-0 2�-z �-
Date
484-252-1748
Phone Number

LINKS .....
eurofins
Environment Testin'
America i
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-217004-2
Client Project/Site: Storm Water - Amazon Warehouses CLT3
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
iRoxa.�u. Cc�,u-ng
Authorized for release by:
6/24/2022 8:17:59 AM
Roxanne Cisneros, Senior Project Manage
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
� 11
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Qualifiers
Job ID: 680-217004-2 0
General Chemistry
Qualifier Qualifier Description
F5 Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL, and the absolute difference between results is <
the upper reporting limits for both.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Abbreviation These commonly used abbreviations may or may not be present in this report.
n Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 2 of 13 6/24/2022

Sample Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Lab Sample ID
Client Sample ID
Matrix
680-217004-2
CLT3 Sample_Point 01_20220614
Water
680-217004-3
CLT3 Sample —Point 02 20220614
Water
680-217004-4
CLT3 Sample_Point 03 20220614
Water
680-217004-5
CLT3 Sample Point 04 20220614
Water
Collected
Received
06/14/2210:14
06/15/2219:00
06/14/2210:27
06/15/2219:00
06/14/2210:34
06/15/2219:00
06/14/2211:03
06/15/2219:00
Job ID: 680-217004-2
Page 3 of 13
Eurofins SOWW2

Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Job ID: 680-217004-2
Laboratory: Eurofins Savannah
Narrative
Job ID: 680-217004-2
V 45
Job Narrative
680-217004-2
Comments
No additional comments.
Receipt
The samples were received on 6/15/2022 7:00 PM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 2.80 C and 3.30 C.
General Chemistry
Method SM 2540D: The sample duplicate precision for the following sample associated with analytical batch 680-726189 was outside
control limits: (680-217004-A-3 DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD)
precision met acceptance criteria.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Savannah
Page 4 of 13 6/24/2022

Client Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Job ID: 680-217004-2
Client Sample ID: CLT3_Sample_Point 01_20220614 Lab Sample ID: 680-217004-2
Date Collected: 06/14/22 10:14 Matrix: Water
Date Received: 06/15/22 19:00
General Chemistry
Analyte Result Qualifier
RL
Total Suspended Solids
11
2.5
LChemical Oxygen Demand
9.9 J
10
Client Sample ID: CLT3_Sample_Point
02_20220614
Date Collected: 06/14/22 10:27
Date Received: 06/15/22 19:00
General Chemistry
Analyte Result Qualifier
RL
Total Suspended Solids
59
13
LChemical Oxygen Demand
5.5 J
10
Client Sample ID: CLT3_ Sam ple_Point_03_20220614
Date Collected: 06/14/22 10:34
Date Received: 06/15/22 19:00
MDL Unit D Prepared Analyzed Dil Fac
2.5 mg/L 06/16/2215:50 1
5.0 mg/L 06/23/22 10:50 1
Lab Sample ID: 680-217004-3
Matrix: Water
MDL Unit D Prepared Analyzed Dil Fac
13 mg/L 06/16/2215:50 1
5.0 mg/L 06/23/22 10:50 1
Lab Sample ID: 680-217004-4
Matrix: Water
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Total Suspended Solids
14
2.5
2.5
mg/L
06/16/22 15:56 1
Chemical Oxygen Demand
<5.0
10
5.0
mg/L
06/23/22 10:50 1
Client Sample ID: CLT3_ Sam pie —Poi nt 04
20220614
Lab Sample ID: 680-217004-5
Date Collected: 06/14/22 11:03
Matrix: Water
Date Received: 06/15/22 19:00
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Total Suspended Solids
4.3
2.5
2.5
mg/L
06/16/22 15:50 1
Chemical Oxygen Demand
<5.0
10
5.0
mg/L
06/23/22 10:50 1
Eurofins Savannah
Page 5 of 13 6/24/2022

QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Method: 254OD-2015 - Total Suspended Solids
FLab Sample ID: MB 680-726189/1
Matrix: Water
Analysis Batch: 726189
MB MB
Analyte Result Qualifier
LTotal Suspended Solids <2.5
r
Lab Sample ID: LCS 680-72618912
Matrix: Water
Analysis Batch: 726189
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-726189/3
Matrix: Water
Analysis Batch: 726189
Analyte
Total Suspended Solids
LLab Sample ID: 680-217004-3 DU
Matrix: Water
Analysis Batch: 726189
Sample Sample
Analyte Result Qualifier
LTotal Suspended Solids 59
at 103-105°C
Job ID: 680-217004-2
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
2.5 2.5 mg/L 06/16/22 15:50 1 i ; I
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
951 852 mg/L 90 80 _ 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
951 826 mg/L 87 80 _ 120 3 25
Client Sample ID: CLT3_Sample_Point_02_20220614
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
55.5 F5 mg/L 6 5
Method: 5220D-2011 - Chemical Oxygen Demand
'Lab Sample ID: MB 680-727303/3 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 727303
MB MB
Analyte Result Qualifier
LChemical Oxygen Demand <5.0
r
Lab Sample ID: LCS 680-72730314
Matrix: Water
Analysis Batch: 727303
i
Analyte
I Chemical Oxygen Demand
L
LLab Sample ID: 680-217004-2 MS
Matrix: Water
Analysis Batch: 727303
Sample Sample
Analyte Result Qualifier
Chemical Oxygen Demand 9.9 J
RL MDL Unit D Prepared Analyzed Dil Fac
10 5.0 mg/L 06/23/2210:50 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
50.0 45.9 mg/L 92 --CO _ 110
Client Sample ID: CLT3_Sample_Point_01_20220614
Prep Type: Total/NA
Spike MS MS %Rec
Added Result Qualifier Unit D %Rec Limits
50.0 60.5 mg/L 101 90 -110
Eurofins Savannah
Page 6 of 13 6/24/2022

QC Sample Results
Client: ERM-West Job ID: 680-217004-2
Project/Site: Storm Water - Amazon Warehouses CLT3
Method: 6220D-2011 - Chemical Oxygen Demand (Continued)
FLab Sample ID: 680-217004-2 MSD Client Sample ID: CLT3_Sample_Point_01_20220614
Matrix: Water Prep Type: Total/NA
Analysis Batch: 727303
Sample Sample Spike MSD MSD %Rec RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
L Chemical Oxygen Demand 9.9 J 50.0 60.5 mglL 101 90 _ 110 0 30
Eurofins Savannah
Page 7 of 13 6/24/2022

QC Association Summary
Client: ERM-West
Job ID: 680-217004-2
Project/Site: Storm Water
- Amazon Warehouses CLT3
General Chemistry
Analysis Batch: 726189
r
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217004-2
CLT3_Sample_Point _01_20220614
Total/NA
Water
2540D-2015
680-217004-3
CLT3 Sample_Point_02_20220614
Total/NA
Water
2540D-2015
680-217004-4
CLT3_ Sample_ Point _03_20220614
Total/NA
Water
254OD-2015
680-217004-5
CLT3_Sample_Point_04_20220614
Total/NA
Water
254OD-2015
MB 680-726189/1
Method Blank
Total/NA
Water
254OD-2015
LCS 680-726189/2
Lab Control Sample
Total/NA
Water
254OD-2015
LCSD 680-726189/3
Lab Control Sample Dup
Total/NA
Water
2540D-2015
L680-217004-3 DU
CLT3_Sample_Point_02_20220614
Total/NA
Water
2540D-2015
Analysis Batch: 727303
FLab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217004-2
CLT3_Sample_Point_01_20220614
Total/NA
Water
5220D-2011
680-217004-3
CLT3_ Sample_ Point _02_20220614
Total/NA
Water
5220D-2011
680-217004-4
CLT3_Sample_Point_03_20220614
Total/NA
Water
5220D-2011
680-217004-5
CLT3_Sample_Point_04_20220614
Total/NA
Water
5220D-2011
MB 680-727303/3
Method Blank
Total/NA
Water
5220D-2011
LCS 680-727303/4
Lab Control Sample
Total/NA
Water
5220D-2011
680-217004-2 MS
CLT3_Sample_Point_01_20220614
Total/NA
Water
5220D-2011
680-217004-2 MSD
CLT3_Sample_Point_01_20220614
Total/NA
Water
5220D-2011
Eurofins Savannah
Page 8 of 13 6/24/2022

Lab Chronicle
Client: ERM-West
Job ID: 680-217004-2
Project/Site: Storm Water - Amazon Warehouses
CLT3
Client Sample ID: CLT3_Sample_Point
01_20220614
Lab Sample ID: 680-217004-2
Date Collected: 06/14/22 10:14
Matrix: Water
Date Received: 06/15/22 19:00
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method
Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 2540D-2015
1 1000 mL
1000 mL
726189 06/16/22 15:50 PG TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis 5220D-2011
1 2 mL
2 mL
727303 06/23/22 10:50 ALG TAL SAV
L Instrument ID: SPC7
Client Sample ID: CLT3_Sample_Point
02_20220614
Lab Sample ID: 680-217004-3 iili�
U
Date Collected: 06/14/22 10:27
Matrix: Water
Date Received: 06/15/22 19:00
i—
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method
Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 2540D-2015
1 200 mL
1000 mL
726189 06/16/22 15:50 PG TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis 5220D-2011
1 2 mL
2 mL
727303 06/23/22 10:50 ALG TAL SAV
Instrument ID: SPC7
Client Sample ID: CLT3_ Sam pie —Poi
nt_03_20220614
Lab Sample ID: 680-217004-4
Date Collected: 06/14122 10:34
Matrix: Water
Date Received: 06/15/22 19:00
r Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method
Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 254OD-2015
1 1000 mL
1000 mL
726189 06/16/22 15:50 PG TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis 5220D-2011
1 2 mL
2 mL
727303 06/23/22 10:50 ALG TAL SAV
i Instrument ID: SPC7
Client Sample ID: CLT3_ Sam ple_Point
04_20220614
Lab Sample ID: 680-217004-5
Date Collected: 06/14/22 11:03
Matrix: Water
Date Received: 06/15/22 19:00
L Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method
Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
TotaUNA Analysis 254OD-2015
1 1000 mL
1000 mL
726189 06/16/22 15:50 PG TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis 5220D-2011
1 2 mL
2 mL
727303 06/23/22 10:50 ALG TAL SAV
Instrument ID: SPC7
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah,
GA 31404, TEL [phone]
Page 9 of 13
Eurofins Savannah
6/24/2022

Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT3
Laboratory: Eurofins Savannah
The accredRation s/certifications listed below are applicable to this report.
Authority Program
North Carolina (WW/SW) State
Job ID: 680-217004-2
Identification Number Expiration Date
269 12-31-22
Eurofins Savannah
Page 10 of 13 6/24/2022

Method Summary
Client: ERM-West Job ID: 680-217004-2
Project/Site: Storm Water - Amazon Warehouses CLT3
Method Method Description Protocol Laboratory
2540D 2015 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV
522OD-2011 Chemical Oxygen Demand Sm TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 11 of 13 6/24/2022

sv
CD
N
0
w
�.z
N
0
N
N
Eurofins Savannah
5102 LaRoche Avenue
Savannah GA 31404
Phone [phone] Fax:[phone]
Chain of Custody Record
eurofins En "onmew "*eat ng
r.-e"Ca
SamplerRAA-r l f
tab PM
Carrier Tracking No(s)
COC No:
Client Information
utd
Cisneros Roxanne
Iroxanne
]Page
240-96101-33331
1
Ghent Contact:
Doug Wade _
Phone:
7o(c- S-71 S-3611
E- A State of Origin.
cisneroso=t rornsus com
Page:
1 of 1
., oany
PWStD
Job !t
EFIA-west
Analysis Requested
Preservation Codes
u i
1 c c •- '400 I
,�
City
�AT rt a (oays)
A HCL
8 NaOH
M Hex: n
N None
Iry ne
C - Zn Acetate
0. AsNa02
v
O Nitric Acid
p Na2SO3
Phone
443-a12-0046(Tel)
r O IF
1 I�,,,,
mooO+
H As hoc Ado
S Hta(j4
T - TSP Dodecahydrate
Email
doug wade oQerm com
WO #:
Z . ,
.0 '�'
i-ice
J - Dr Water
U Acetone
CAA
w a
Project Name
Storm Water Amazon Warehouses
Project #�
24024260
W
=
K - EDTA
»A
Y - Triama
-
Z - over (spedfy)
Site:
wL ri, -),.o c,.w ev... J�r v L4 C CL 77J
SSOWJt:
v
Other
v,
o
0
Sample Matrix a
P m o,
Type
(W-MWram-
.
Sample (C=ccmp,
com. m m
Sam a Identification
Sample Date Time G=rab
o n.sn.AaAk T V H
i"
S vial InstructionslNot�e
'Presetvahon
Code:
g
y
jT
water
L P-P' e4 ... OZ +' 2.o L* (a ��
6 1 t.Z-
f t Z7
Water
Ii
t
Y u.
t6 ,.5q 4
G
1
Z
tr'3-3. . t ..fo.vj- 6y-�zz.o4,q
�,� z
:d3,,
6
,
,
.
I
TJJ
Possible Hazard Identification
Sample Disposal (A fee may be assessed ff samples areretained longer than T month)
0 Non =1 Im ED ED
IM M
ED
-Hazard Flammable Skin Irritant Poison
B Unknown Radio-1-0-VC-0
Retum. To Client Disposal Py Lab
Archive For
Months
Deliverable Requested I It III IV Other (specify)
Special Instnicbons/oC Requirements.
Empty Kit Relinquished by-
Date.
Tithe McOwd of shipment
Rer= Lby
Datemme
Date/fi
Company
Company
Received by' 1 L�►
Received by
Datemm
DatelTime.
Company
Company
Rertn4uished ''
Relinquished by
Da
Company
Received by
DateM le
Company
l
(� /
Custody Seals Intact:
o Yes No
Custody Seal No
Cooler Tempembze(s) OC and Other Remarks.
a
ver 0610$n?02 t

Login Sample Receipt Checklist
Client: ERM-West
Login Number: 217004
List Number: 1
Creator: Bissonnette, Ian
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4').
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Job Number: 680-217004-2
List Source: Eurofins Savannah
J
Eurofins Savannah
Page 13 of 13 6/24/2022