NCG060396_Monitoring Report_20220125

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCGO60000
Food and Kindred
Click here for instructions
RECEIVED
JAN 25 2022
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard cow of the DMR to the appropriate DE MLR Regional Office.
Certificate of Coverage No. NCG06 0396
Person Collecting Samples: Darrin Paine
Facility Name: Amazon.com Services LLC - CLT2
Laboratory Name: Eurafias TestAmerica, Savannah
Facility County: Mecklenburg
Laboratory Cert. No.: 269
Discharge during this period:
Q
Yes
❑ No rifno, skip to signature and date)
Has your facility implemented mandatoryTier response actions this sample period for any benchmark exceedances? ❑ Yes 0 No
If so, which Tier (I, Il, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR x❑ Yes ❑ No
Date Uploaded: 0 111 q I UZY
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
outfa8 OD1
OutfaB
oul fall
Outfall
outfall
Code
N/A
Receiving Stream Class
B, CA
N/A
Date Sample Collected MM/DD/YYYY
12/30/2021
46529
24-Hour Rainfall in inches
0.16
C0530
TSSin mg/L (100 or 50*)
4.8
00400
pH in standard units (6.0 — 9.0 FW,
7.68
6.8—B.SSW)
31616
Fecal Coliform per 100 ml of
freshwater (if required) (1000)
N/A
61211
Enterococci per 100 ml of saltwater
N/A
(if required) (500)
Chemical Oxygen Demand in mg/L
00340
(120)
6.3
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
NCOIL
Estimated New Motor/Hydraulic Oil
N/A
Usage in gal/month
00552
Nan -Polar Oil & Grease in mg/L(15)
N/A
* Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmatkTSSUmit of 50 mg/L-AU other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Basedon my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false Information, including the possibility of fines and imprisonment for knowing violations."
Signature of
Authorized Individual
01 1 2� 2Z
Date
[e-mail] [phone]
Email Address Phone Number

eurofins
Environment
America
..iestin�
�9 ��F
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ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-209608-1
Laboratory SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
Client Project/Site: Storm Water - Amazon Warehouses CLT2
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Ro%&h*u. ez"rvs
Authorized for release by:
111312022 3:05:11 PM
Roxanne Cisneros, Senior Project Manager
[phone]
roxanne.cisneros@ Eurofinsetcorn
The test resultsin thisreport meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the semple(s) as received by the laboratory.

Definitions/Glossary
Client: ERM-West Job ID: 680-209608-1 Project/Site: Storm Water - Amazon Warehouses CLT2 SDG: 10240 Old Dowd Rd, Charlotte, NC 28214 in
94
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greaterthan or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present In this report.
a Listed underthe "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Funning Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis ofthe sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MCL Method Quantitation Limit
NC Not Calculated
NO Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative/Absent
POS Positive / Present
POL Practical Quarditat ion Lint
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 2 of 12 1/13/2022

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Case !narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT2
Job ID: 680-209608-1
Laboratory: Eurofins Savannah
Narrative
Job ID:680-209608-1
SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
a
Job Narrative
680409608-1
Comments
No additional comments.
Receipt
The sample was received on 1/4/202210:50 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 4.00 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Savannah
Page 4 of 12 1/13/2022

Client Sample Results
Client: ERM-West Job ID: 680-209608-1
Project/Site: Storm Water - Amazon Warehouses CLT2 SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
Client Sample ID: CLT2_Sample_Point_01_20211230 Lab Sample ID: 680-209608-1
Date Collected: 12/30/21 12:50 Matrix: Water
Date Received: 01/04122 10:50
General Chemistry
Aaatyta Result Qualifier RL MOL Unit D Prepared Analyzed Qa Far
Total Suspended Solids 4.8 2.5 2.5 mg/L 01/05P2210:52 1
Chemical Oxygen Demand 6.3 J 10 50 mg/L 01/1=1127 i
Eurofins Savannah
Page 5 of 12 1/13/2022

QC Sample Results
Client: ERM-West
Project/Site: Storm Water -Amazon Warehouses CLT2
Job ID:680-209608-1
SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-1050C)
Lab Sample ID: MB 680-701940/1
Matrix: Water
Analysis Batch: 701940
Client Sample ID: Method Blank
Prep Type: Total/NA
ate me
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dill Fee
Total Suspended Solids <2.S 2.S 2.5 mg/L G1105M 10:52 1
Lab Sample ID: LCS 680-70194012
Matrix: Water
Analysis Batch: 701940
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-70194013
Matrix: Water
Analysis Batch: 701940
Analyte
Total Suspended Solids
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
951 852 mg/L 90 80-120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rao Limits RPD LtmR
951 888 mg/L 91 80-120 2 25
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-702898/3
Matrix: Water
Analysis Batch: 702898
Client Sample ID: Method Blank
Prep Type: Total/NA
MB Me
Analyte Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dill Fac
Chemical Oxygen Demand <5.0
10 5.0 mg/L
01/13/22 11:27 1
Lab Sample ID: LCS 680-702898/4
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 702898
Spike
LCS LCS
%Rec.
Analyte Added
Result Qualifier
Unit D %Rec
Limits
Chemical Oxygen Demand 50.0
45.7
mg/L 91
90-110
Eurofins Savannah
Page 6 of 12
1/13/2022

QC AssooiaVon Summary
Client: ERM-West
Project/Site: Stone Water - Amazon Warehouses CLT2
General Chemistry
Analysis Batch: 701940
Job ID: 680-209608-1
SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
F Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-209608-1
CLT2_Sample_Point_01_20211230
TotaVNA
Water
2540 D-2011
MB 680-701940M
Method Blank
TotaVNA
Water
2540 D-2011
LCS 680-701940/2
Lab Control Sample
TotaVNA
Water
2540 D-2011
LCSD 680-70194W3
Lab Control Sample Dup
TotaVNA
Water
2540 D-2011
Analysis SU.t\ch: 1I nV20.98
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-209608-1
CLT2 Sampfe_Point 01_20211230
TotaYNA
Water
5220D-2011
Me 680-702898/3
Method Blank
TotaVNA
Water
5220D-2011
LCS 6a0-702898/4
Lab Control Sample
TotaVNA
Water
5220D-2011
Eurofins Savannah
Page 7 of 12 1/13/2022

Lab Chronicle
Client: ERM-West Job ID: 680-209608-1
ProjecUSite: Storm Water - Amazon Warehouses CLT2 SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
Client Sample ID: CLT2_Sample_Point_01_20211230 Lab Sample ID: 680-209608-1
Date Collected: 12130/21 12:50 Matrix: Water
Date Received: 01/04/22 10:50
Batch Batch
DII
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis 2540 D-2011
1
1000 mL
1000 mL
701940
01/05/22 10:52
PG TAL SAV
Instrument 10: NQEQUIP
TotaVNA Analysis 5220D-2011
1
2 mL
2 mL
702898
01113/22 11:27
ALG TAL SAV
Instrument ID: SPC7
Laboratory Reterenees:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue,
Savannah, GA 31404, TEL[phone]
Eurofins Savannah
Page 8 of 12 1/13/2022

Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT2
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Job ID:680-209608-1
SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
FkUthority Program MentlReatto Number Expirefien r%te
North Carolina (W W/SN) State 269 12-31-22
H
Eurofins Savannah
Page 9 of 12 1/13/2022

Method Summary
Client: ERM-West Job ID: 680-209608-1
Project/Site: Storm Water - Amazon Warehouses CLT2 SDG: 10240 Old Dowd Rd, Charlotte, NC 28214
Method Method Description Protocol Laboratory
2540 D-2011 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV
5220D-2011 Chemical Oxygen Demand SM TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of water And Wastewater"
Laboratory References:
TAL SAV'= Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (g?2)354-7858
711
Eurofins Savannah
Page 10 of 12 1/13/2022

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Eurofins TestArmerica, Savannah
5 102 LaRoche Avenue
Savannah GA 31404
Phone [phone] Fax [phone]
Chain of Custody Record
N,W*-I..!I*Jve;MEMO ��
Client Information
Sampler
Ilroxannq
Lab PM
Cisnerc5,Roxarne
CamerTra No(si
COC No
240-87327-333401
Chem Contact
Dena Haverldnd
Phone
E-MaO
asne•Os@EurgfinseLcorn
Stele of Origen
Page
Page 1 of 1
Company PwSto
ERM-Southeast, Inc,
Analysis Requested
! #'
Address.
The Towerp a• `bilIm)od Plaza 3200 Windy Hill Road Sune i 50
Due Date Requested
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Preservatrcn Codes
A HCL M Kexaoe
6 NaOH N None
C Zn Acetate O AsNapr,
0 Nitric Add P Na204S
E NaHSO4 0 Na2SA3
F McOt : R Na2SA03
H Ascor s H2SO4
AcortxsAcid T TSPDodecahyQrate
i Ice U Acetone
J DI Water V MCAA
K EDTA W pH 4,5
L EDA Z other (specify)
Other
UT
Atlanta
•—
TAT Requested(days)
State Zip
GA, ;.0339
Comp Ance Project: .1 Yes 4 No
Phone
443-812-0046 R el)
Email
dens haverlandgerm Cam
PO ft
CLT2
WO t
Project Name.
Storm Water - Amazon' Warehouses
Projeap
24024260
Site
SSOVO
Sample Identification
Sample Date
Sample
Time
Sample
Type
(C--comp,
rab)
Matrix
(vw. —
saau�re.
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special tristructiorislNote
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reservation Code:
S
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waterid
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2 pg Chain of Custody --�
Possrble Hazard ldarrtificadon
© Non -Hazard Flammable �Skrn Irritant M Poison B Q Unknown PRadrological
Sample DlspoSal (A fee may be ass. sed ' samples are rletalrt longer than i month)
�Retum Tq Client �Disppsal By Lab �Anchrve For Months
Deliverable Requested'I II III IV Other (specify)
Specta lnstn Ri`ons/Q Requirements
Empty Kit Reli fished by n jData jTirtte
me" of Shcpnlent
Refinquished by
DateiTi a
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Co any
ReclHved by
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ReUngmthed Y�
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Comps
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Relinquished by-
0atelt' me
Company
Recelved
Datdnme
C o S''d
Cotttparry
Custody Seats Intact
5 Yes , No
Custody Seal NO P
Coeir Temperaturets} 6C anq r RemarRs.
. � 16
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Login Sample Receipt Checklist
Client: E€tM-West
Login Number: 209608
List Number. 1
Creator: Hartley, Tyler
Question
Job Number: 680-209fi08r 4
SDG Number. 10240 Old Dowd Rd, Charlotte, NC 28214
List Source: Eurofins Savannah
Ans` w Comment
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
NIA
The cooler's custody seal, if present, is intact.
True
Sample custody, seats, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered wish.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Samplers name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Samples PRwervatlm Verified..
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4').
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
'12
Eurofins Savannah
Page 12 of 12 1/13/2022