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HomeMy WebLinkAboutNC0021181_Renewal (Application)_20100630NPDES DOCIMENT SCANNING COVER SHEET NC0021181 Belmont WWTP NPDES Permit: Document Type: Permit Issuance Wasteload Allocation Authorization to Construct (AtC) Permit Modification Complete File - Historical Engineering Alternatives (EAA) . Renewal Application Instream Assessment (67b) Speculative Limits Environmental Assessment (EA) Document Date: June 30, 2010 This document is printed w . reuse paper - ignore arty content cwt.-the remzerse side �.� pust4C City of •Belmont Wastewater Treatment "CARD" June 30, 2010 Mr. Ron Berry 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Mr. Berry, PO Box 431 * Belmont, NC 28012 * www.cityolbclmont.org Telephone 704-825-3791 * Fax 704-825-0514 The enclosed information should contain everything you requested for the completion of the NPDES permit renewal for the City of Belmont #NC0021181. However this does not include any information that you need from Jerry Hatton. If you need any further information from me, please feel free to contact me at 704-825-3791. Sinc rely, Sandra M. Craft 1g6(1 City of Belmont Wastewater ORC POINT SOURCE BRANCH Enclosure Cc: File NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Coleen H. Sullins Dee Freeman Governor Director Secretary January 11, 2010 SANDRA M CRAFT ORC CITY OF BELMONT WWTP PO BOX 431 BELMONT NC 28212 Subject: Receipt of permit renewal application NPDES Permit NC0021181 Belmont WWTP Gaston County Dear Ms. Craft: The NPDES Unit received your permit renewal application on January 5, 2010. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. If you have any additional questions concerning renewal of the subject permit, please contact Ron Berry at (919) 807-6396. Sincerely, Suizu Dina Sprinkle Point Source Branch cc: CENTRAL FILES Isvlooresville Regional Office/Surface Water Protection NPDES Unit 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 Phone: 919-807-63001 FAX: 919.807-64921 Customer Service: 1-877-623-6748 Internet: www.ncwaterquality.org An Equal Opportunity 1 Affirmative Action Employer NorthCarolina 2atura!!j To: Western NPDES Unit Surface Water Protection Section Attention: Ron Berry SOC PRIORITY PROJECT: No Date: January 29, 2010 NPDES STAFF REPORT AND RECOMMENDATIONS County: Gaston NPDES Permit No.: NC0021181 PART I - GENERAL INFORMATION 1. Facility and address: City of Belmont WWTP Post Office Box 431 Belmont, N.C. 28212 Physical Location 298 Parkdale Drive Belmont, NC 28212 2. Date of investigation: January 28, 2010 3. Report prepared by: Michael L. Parker, Environmental Engineer II 4. Person contacted and telephone number: Chuck Flowers, Utilities Director; Sandra Craft, WWTP Superintendent (704) 825-0510 (WWTP). 5. Directions to site: From the intersection of Hwy. 273 and Catawba Street (Hwy. 7) in the City of Belmont, travel east on Catawba Street 0.7 mile and turn right on loth street. Travel 0.3 mile and turn left onto Parkdale Drive. Travel 0.2 mile and bear right into the entrance to the Belmont WWTP. 6. Discharge point(s), list for all discharge points: Latitude: 35° 13' 33" Longitude: 81° 00' 53" USGS Quad No.: G 14 NE 7. Receiving stream or affected surface waters: Catawba River (Lake Wylie). a. Classification: WS-IV, B b. River Basin and Subbasin No.: Catawba 030833 c. Describe receiving stream features and pertinent downstream uses: Lake Wylie is used for primary and secondary recreation and receives frequent bodily contact. There are no water intakes. for several miles below the point of discharge, however, there are other dischargers downstream of this facility. PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS 1. a. Volume of Wastewater: 5.0 MGD (Design Capacity) Page Two b. What is the current permitted capacity: 5.0 MGD c. Actual treatment capacity of current facility (current design capacity): 5.0 MGD d. Description of existing or substantially constructed WWT facilities: The existing WWT facilities consist of dual influent bar screens (one mechanical and one manual), caustic addition (if necessary), a parshall flume with flow meter, grit chamber with mechanical grit removal system (currently inoperable), dual aeration basins with mechanical aeration (only one in service), dual secondary clarifiers, chlorine gas disinfection with contact chamber, effluent parshall flume, effluent flow measurement with recorder, two aerobic sludge digesters, an aerated sludge holding tank, a stand-by power generator, and sludge drying beds (not used). e. Description of proposed WWT facilities: There are no proposed WWT facilities at this time. PART III - OTHER PERTINENT INFORMATION 1. Special monitoring or limitations (including toxicity) requests: None requested at this time .by the City nor are any recommended by this Office. 2. Compliance information: This facility consistently complied with all permit parameters in 2009. The most recent CEI performed at this facility did not find any issues with operations or maintenance that would warrant a NOV. PART IV - EVALUATION AND RECOMMENDATIONS The City of Belmont (the City) requests renewal of the subject permit. There have been no changes to the existing WWTP and/or the permit since the permit was last renewed nor are any proposed during the term of the new permit. In conversations with Mr. Flowers and Ms. Craft during the site visit, the possibility of including tiered effluent limits in the permit was discussed. The City has lost a number of industrial customers over the past several years, which has resulted in a significant reduction in hydraulic flow to the WWTP. Current wastewater flows over the past 12 months are averaging around 1.3 MGD, which is less than half the hydraulic capacity of the WWTP. Furthermore, the receiving waters have been found to be impacted by nutrients, which may eventually result in the City having to upgrade to meet future nutrient effluent limitations. The City hopes that by reducing the permitted flow, they would be able to postpone future nutrient removal upgrades. One possible scenario being considered by the City would be to establish effluent limits for 2.0 MGD and 5.0 MGD. If tiered limits are requested by the City and eventually incorporated into this NPDES permit, it is important that language also be included in the permit that specifically defines when the City must move from one permitted flow to the other. Without such written guidance, compliance becomes difficult to determine, especially when average flows are at or near the lowered tiered limit. Page Three Pending a review and approval of this request by the Western NPDES Unit, it is recommended that the subject permit be renewed. Signal of Report Preparer / et/ D e Water Quality Regional Supervisor h:\dsr\dsr 10\belmont doc Date Z0l9 ReveiJ FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 FORM 2A NPDES PERMIT ACTION REQUESTED: Renewal NPDES FORM 2A APPLICATION APPLICATION OVERVIEW RIVER BASIN: Catawba -Lake Wylie Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B Additional Application Information for Applicants with a Design Flow z 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to one or more of the following criteria must complete Part D (Expanded Effluent Te 1. Has a design flow rate greater than or equal to 1mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. �tIVE JAN - 5 2010 Toxicity Testing Data. A treatment works that meets one or more of the following t ATER Et( '�i i 'l}j l'ng Data): U C 1. Has a design flow rate greater than or equal to 1 mgd, POINT SOURCE BRANCH 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). Sills are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or c. Is designated as an SIU by the control authority. . Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie BASIC APPLICATION INFORMATION PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS: All treatment works must complete questions Al through A.8 of this Basic Application Information Packet. A.1. Facility Information. Facility Name City of Belmont, Wastewater Treatment Plant Mailing Address P.O. Box 431 Belmont, N.C. 28212 Contact Person Sandra M. Craft Title ORC Telephone Number j704) 825-3791 Facility Address 298 Parkdale Drive (not P.O. Box) Belmont, N.C. 28212 A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Mailing Address Contact Person Title Telephone Number i_L Is the applicant the owner or operator (or both) of the treatment works? X❑ owner X❑ operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. X❑ facility ❑ applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES NC 0021181 PSD UIC Other RCRA Other A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership Belmont 9500 Sanitary Sewer Municipal Total population served FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC 0021181 A.5. Indian Country. a. Is the treatment works located in Indian Country? PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie ❑ Yes X ❑ No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? ❑ Yes X ❑ No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of "this year" occurring no more than three months prior to this application submittal. a. Design flow rate 5.0 mgd b. Annual average daily flow rate c. Maximum daily flow rate Two Years Ago 1.304 Last Year This Year 1.441 1.373 2.233 2.740 2.688 A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. x❑ Separate sanitary sewer 100 ❑ Combined storm and sanitary sewer A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? X ❑ Yes 0 No If yes, list how many of each of the following types of discharge points the treatment works uses: Discharges of treated effluent ii. Discharges of untreated or partially treated effluent iii. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) v. Other 1 (one) None None None None b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? 0 Yes x❑ No If yes, provide the following for each surface impoundment: Location: N/A Annual average daily volume discharge to surface impoundment(s) N/A mgd Is discharge ❑ continuous or 0 intermittent? c. Does the treatment works land -apply treated wastewater? 0 Yes X 0 No If yes, provide the following for each land application site: Location: NIA Number of acres: NIA Annual average daily volume applied to site: Is land application N/A mgd ❑ continuous or ❑ intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? ❑ Yes X ❑ No FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC 0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie e. If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). N/A If transport is by a party other than the applicant, provide: Transporter Name Mailing Address Contact Person Title Telephone Number j ) For each treatment works that receives this discharge, provide the following: Name Mailing Address Contact Person Title Telephone Number j ) If known, provide the NPDES permit number of the treatment works Provide the average daily flow rate from the treatment works into Does the treatment works discharge or dispose of its wastewater in A.8. through A.8.d above (e.g., underground percolation, well If yes, provide the following for each disposal method: that receives this discharge the receiving facility. mgd in a manner not included injection): ❑ Yes x❑ No Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: Is disposal through this method ❑ continuous or ❑ intermittent? FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC 0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number 001 b. Location Belmont, N.C. (Lake Wylie) 28212 (City or town, if applicable) Gaston (Zip Code) North Carolina (County) (State) 35-13-37 81-00-52 (Latitude) (Longitude) c. Distance from shore (if applicable) 345 ft. d. Depth below surface (if applicable) 1223 ft. e. Average daily flow rate 1.560 mgd f. Does this outfall have either an intermittent or a periodic discharge? ❑ Yes x D No (go to A.9.g.) If yes, provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: mgd Months in which discharge occurs: g. Is outfall equipped with a diffuser? 0 Yes X ❑ No A.10. Description of Receiving Waters. a. Name of receiving water Catawba River b. Name of watershed (if known) Lake Wylie United States Soil Conservation Service 14-digit watershed code (if known): c. Name of State Management/River Basin (if known): United States Geological Survey 8-digit hydrologic cataloging unit code (if known): d. Critical low flow of receiving stream (if applicable) acute N/A cfs chronic N/A cfs e. Total hardness of receiving stream at critical low flow (if applicable): N/A mg/l of CaCO, FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catabwa-Lake Wylie A.11. Description of Treatment a. what level of treatment are provided? Check all that apply. ❑ Primary x❑ Secondary ❑ Advanced 0 Other. Describe: b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 85 % Design SS removal 85 Design P removal 0 % Design N removal 0 % Other N/A 04 c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe: Chlorine If disinfection is by chlorination is dechlorination used for this outfall? x ❑ Yes ❑ No Does the treatment plant have post aeration? 0 Yes x ❑ No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number. 001 PARAMETER MAXIMUM DAILY VALUE AVERAGE DAILY VALUE Value Units Value Units Number of Samples pH (Minimum) 7.07 s.u. pH (Maximum) 7.42 s.u. Flow Rate 1.906 mgd 1.373 mgd 3 Temperature (Winter) 14.0 c 14.0 c 3 Temperature (Summer) 28.0 c 22.9 c 3 * For pH please report a minimum and a maximum daily value POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLJMDL Conc. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN DEMAND (Report one) BOD5 16.0 mg/I 7.6 mgll 3 SM5210B 2.0 CBOD5 FECAL COLIFORM 55.0 col/100ml 6.0 com100 3 SM9222D 2.0 TOTAL SUSPENDED SOLIDS (TSS) 17.0 mgll 10.2 mg/I 3 SM2540D 1.0 END OF PART A. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE ' FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC002118 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie BASIC APPLICATION INFORMATION PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate >_ 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification). B.1. Inflow and Infiltration. Estimate the average number of gallons per day 20,000 gpd that flow into the treatment works from inflow and/or infiltration. Briefly explain any steps underway or planned to minimize inflow and infiltration. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within'/. mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ❑ Yes xD No If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). Name: Mailing Address: Telephone Number: j ) Responsibilities of Contractor: B.S. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. 0 Yes ❑ No FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). d. Provide dates imposed applicable. For improvements applicable. Indicate Implementation Stage - Begin Construction - End Construction - Begin Discharge - Attain Operational e. Have appropriate Describe briefly: by any compliance schedule planned independently dates as accurately as possible. Level permits/clearances concerning other or any actual dates of completion for the implementation steps listed of local, State, or Federal agencies, indicate planned or actual completion Schedule Actual Completion MM/DD/YYYY MM/DD/YYYY below, as dates, as Yes ❑ No / / / / / / / / / / / / / / 1 I Federal/State requirements been obtained? ❑ B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD Applicants that discharge to waters of the US must effluent testing required by the permitting authority on combine sewer overflows in this section. All information using 40 CFR Part 136 methods. In addition, this data QA/QC requirements for standard methods for analytes based on at least three pollutant scans and must be Outfall Number: 001 ONLY). provide effluent testing data for the following parameters. Provide for each outfall through which effluent is discharged. Do not include the indicated information conducted other appropriate data must be reported must be based on data collected through analysis must comply with QA/QC requirements of 40 CFR Part 136 and not addressed by 40 CFR Part 136. At a minimum effluent testing no more than four and on -half years old. POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MIJMDL Conc. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) .54 mgll .39 mg/l 3 350.1 0.10 CHLORINE (TOTAL RESIDUAL, TRC) .10 mgll .10 mgll 3 SM4500 CL G 0.10 DISSOLVED OXYGEN 8.82 mg/I 8.26 mgli 3 SM4500 OG 2.00 TOTAL KJELDAHL NITROGEN (TKN) 3.1 mg/1 1.5 mg/I 3 351.2 0.50 NITRATE PLUS NITRITE NITROGEN 21 mg/1 20 mg/I 3 353.2 0.20 OIL and GREASE 4.8 mg/1 4.6 mgll 3 1664 A 4.8 PHOSPHORUS (Total) 20.0 mg/I 9.3 mgll 3 365.1 0.50 TOTAL DISSOLVED SOLIDS (TDS) 630 mg/1 587 mgll 3 SM 2540 C 10 OTHER END OF PART B. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: c - ° Lake Wylie BASIC APPLICATION INFORMATION PART C. CERTIFICATION All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: x❑ Basic Application Information packet Supplemental Application Information packet: x❑ Part D (Expanded Effluent Testing Data) x❑ Part E (Toxicity Testing: Biomonitoring Data) x❑ Part F (Industrial User Discharges and RCRAICERCLA Wastes) ❑ Part G (Combined Sewer Systems) ALL APPUCANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title Barry L. Webb, City Manager� Signature 4 Telephone number 70 ,,4)JJ) 825- 86 Date signed Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENRI DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD ML MDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY .0058 mg/I .065 lbs .0047 mg/I .061 Ibs 3 200.8 .001 ARSENIC ND mg/I ND Ibs ND mg/I ND Ibs 3 200.8 .001 BERYLLIUM ND mg/I ND Ibs ND mg/I ND Ibs 3 200.8 .0004 CADMIUM .0013 mg/I .002 Ibs .0001 mg/I .0014 Ibs 3 200.8 .001 CHROMIUM ND mg/I ND Ibs ND mg/I ND Ibs 3 200.8 .005 COPPER .017 mgll .270 Ibs .016 mg/I .208 Ibs 3 200.8 .001 LEAD ND mg/1 ND lbs ND mgll ND Ibs 3 200.8 .001 MERCURY .0088 mg/I .099 lbs .0080 mg/I .104 Ibs 3 245.1 .0080 NICKEL ND mg/1 ND lbs ND mg/I ND Ibs 3 200.8 .005 SELENIUM ND mg/I ND lbs ND mg/I ND Ibs 3 200.8 .001 SILVER ND mg/I ND Ibs ND mg/I ND Ibs 3 200.8 .001 THALLIUM ND mg/I ND Ibs ND mg/I ND Ibs 3 200.8 .0005 ZINC .24 mg/I 3.82 lbs .16 mg/I 2.08 lbs 3 200.8 .01 CYANIDE ND mg/I ND Ibs ND mg/I ND lbs 3 SM 4500 CNE .010 TOTAL PHENOLIC COMPOUNDS .015 mg/I .168 Ibs .001 mg/I .143 lbs 3 420.4 .0050 HARDNESS (as CaCO3) 68 mgll 762 lbs 59 mg/I 768 Ibs 3 SM 2340 C 10 Use this space (or a separate sheet) to provide information on other metals requested by the permit write FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD ML/MDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples VOLATILE ORGANIC COMPOUNDS ACROLEIN ND mg/I ND Ibs ND mgll ND Ihs 3 8260 B .005 ACRYLONITRILE ND mgll ND Ibs ND mgll ND Ibs 3 8260 B .005 BENZENE ND mg/I ND Ibs ND mg/I ND Ibs 3 8260 B .001 BROMOFORM ND mg/I ND Ibs ND mg/I ND Ihs 3 8260 B .001 CARBON TETRACHLORIDE ND mg/I ND Ibs ND mg/I ND Ibs 3 8260 B .001 CHLOROBENZENE ND mg/I ND Ibs ND mg/I ND Ibs 3 8260 B .001 CHLORODIBROMO- METHANE ND mgll ND Ibs ND mg/I NO Ibs 3 8260 B .001 CHLOROETHANE .0035 mg/I .080 Ibs .005 mg/I .065 Ibs 3 8260 B .005 2-CHLOROETHYLVINYL ETHER ND mg/I ND Ibs ND rng/I ND Ibs 3 8260 B .001 CHLOROFORM .0062 mg/I .074 Ibs .0035 mg/I .046 Ibs 3 8260 B .001 DICHLOROBROMO- METHANE .0036 mg/I .043 Ibs .0024 mgll .031 Ibs 3 8260 B .001 1,1-DICHLOROETHANE ND mgll ND Ibs ND mg/I ND Ibs 3 8260 B .001 1,2-DICHLOROETHANE ND mg/I ND Ibs ND mgll ND Ibs 3 8260 B .001 TRANS-I,2-DICHLORO- ETHYLENE ND mg/I ND Ibs ND mg/I ND Ibs 3 8260 B .001 1,1-DICHLORO- ETHYLENE ND mgll ND Ibs ND mg/I ND Ibs 3 8260 B .001 1,2-DICHLOROPROPANE ND mgll ND Ibs ND mg/I ND lbs .. 8260 B .001 1,3-DICHLORO- PROPYLENE ND mgll ND Ibs ND mg/I NO Ibs 3 8260 B .001 ETHYLBENZENE ND mg/I ND Ibs ND mg/I ND lbs 3 8260 B .001 METHYL BROMIDE ND mg/I ND Ibs ND mg/I ND Ibs 3 8260 B .002 METHYL CHLORIDE ND mg/I ND Ibs ND mgll ND Ibs 3 8260 B .002 METHYLENE CHLORIDE ND mgll ND Ibs ND mg/l ND Ibs 3 8260 B .001 1,1,2,2-TETRA CHLOROETHANE ND mg/I ND Ibs ND mg/I ND lbs 3 8260 B .001 TETRACHLORO- ETHYLENE ND mgll ND Ibs ND mgll ND Ibs 3 8260 B .001 TOLUENE ND mg/I ND Ibs ND mg/I ND Ibs 3 8260 B .001 FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MUMDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples 1,1,1- TRICHLOROETHANE ND ug/I ND Ibs ND ug/I ND Ibs 3 8260 B 1.0 1,1,2 TRICHLOROETHANE ND ug/I ND Ibs ND ug/I ND Ibs 3 8260 B 1.0 TRICHLOROETHYLENE ND ugll ND Ibs ND ugll ND Ibs 3 8260 B 1.0 VINYL CHLORIDE ND ug/I ND Ibs ND ugll ND Ibs 3 8260 B 2.0 Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL 2-CHLOROPHENOL ND ug/I ND Ibs ND ug/1 ND Ibs 3 8270 C 1.0 2,4-DICHLOROPHENOL ND ug/1 ND Ibs ND ugll ND Ibs 3 8270 C 1.0 2,4-DIMETHYLPHENOL ND ug/1 ND Ibs ND ugll ND Ibs 3 8270 C 1.0 4,6-DINITRO-O-CRESOL 2,4-DINITROPHENOL ND ug/I ND Ibs ND ugll ND Ibs 3 8270 C 1.0 2-NITROPHENOL ND ugA ND Ibs ND ug/1 ND Ibs 3 8270 C 2.0 4-NITROPHENOL ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 5.1 PENTACHLOROPHENOL ND ug/1 ND lbs ND ug/I ND lbs 3 8270 C 5.1 PHENOL ND ug/I ND Ibs ND ug/l ND Ibs 3 8270 C 1.0 2,4,6- TRICHLOROPHENOL ND ug/I ND Ibs ND ugll ND Ibs 3 8270 C 1.0 Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 ACENAPHTHYLENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 ANTHRACENE ND ug/I ND Ibs ND ug/1 ND Ibs 3 8270 C 1.0 BENZIDINE ND ugA ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 BENZO(A)ANTHRACENE ND ugA ND Ibs ND ugll ND Ibs 3 8270 C 1.0 BENZO(A)PYRENE ND ugA ND Ibs ND ug/l ND Ibs 3 8270 C 1.0 FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLIMDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples 3,4 BENZO- FLUORANTHENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 BENZO(GHI)PERYLENE ND ug/I ND lbs ND ugll ND Ibs 3 8270 C 1.0 BENZO(K) FLUORANTHENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 BIS (2-CHLOROETHOXY) METHANE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 BIS (2-CHLOROETHYL)- ETHER ND ug/1 ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 BIS (2-CHLOROISO- PROPYL) ETHER ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 BIS (2-ETHYLHEXYL) PHTHALATE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 4-BROMOPHENYL PHENYL ETHER ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 BUTYL BENZYL PHTHALATE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 2-CHLORO- NAPHTHALENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 4-CHLORPHENYL PHENYL ETHER ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 CHRYSENE ND ugll ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 DI-N-BUTYL PHTHALATE ND ug/I ND Ibs ND ug/I ND lbs 3 8270 C 5.0 DI-N-OCTYL PHTHALATE ND ug/I ND lbs ND ug/I ND Ibs 3 8270 C 5.0 DIBENZO(A,H) ANTHRACENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 1,2-DICHLOROBENZENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8260 B 1.0 1,3-DICHLOROBENZENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8260 B 1.0 1,4-DICHLOROBENZENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8260 B 1.0 3,3-DICHLORO- BENZIDINE ND ugll ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 DIETHYL PHTHALATE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 DIMETHYL PHTHALATE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 5.0 2,4-DINITROTOLUENE ND ug/I ND Ibs ND ug/1 ND Ibs 3 8270 C 2.0 2,6-DINITROTOLUENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8270 C 2.0 1,2-DIPHNYL- HYDRAZINE ND ug/I ND Ibs ND ug/I ND lbs 3 8270 C 1.0 FACIUTY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD ML/MDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples FLUORANTHENE ND ug/l ND Ibs ND ug/I ND lbs 3 8270 C 1.0 FLUORENE ND ug/I ND lbs ND ugll ND lbs 3 8270 C 1.0 HEXACHLOROBENZENE ND ugll ND lbs ND ugll ND lbs 3 8270 C 1.0 HEXACHLORO- BUTADIENE ND ugh ND Ibs ND ugh ND lbs 3 8270 C 1.0 HEXACHLOROCYCLO- PENTADIENE ND ug/1 ND Ibs ND ugll ND Ibs 3 8270 C 5.0 HEXACHLOROETHANE ND ug/l ND Ibs ND ug/l ND Ibs 3 8270 C 1.0 INDENO(1,2,3-CD) PYRENE ND ugll ND Ibs ND ugil ND Ibs 3 8270 C 1.0 ISOPHORONE ND ugll ND Ibs ND ugll ND Ibs 3 8270 C 1.0 NAPHTHALENE ND ugh ND Ibs ND ugll ND Ibs 3 8270 C 1.0 NITROBENZENE ND ug/I ND lbs ND ugll ND Ibs 3 8270 C 1.0 N-NITROSODI-N- PROPYLAMINE ND ugh ND Ibs ND ug/I ND lbs 3 8270 C 1.0 N-NITROSODI- METHYLAMINE ND ug!I ND lbs ND ugll ND Ibs 3 8270 C 1-0 N-NITROSODI- PHENYLAMINE ND ugll ND Ibs ND ug/I ND Ibs 3 8270 C 1.0 PHENANTHRENE ND ug/I ND Ibs ND ugll ND lbs 3 8270 C 1.0 PYRENE ND ug/I ND lbs ND ug/I ND lbs 3 8270 C 1.0 1,2,4 TRICHLOROBENZENE ND ug/I ND Ibs ND ug/I ND Ibs 3 8260 B 1.0 Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g , pesticides) requested by the permit writer END OF PART D. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using altemate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent x❑ chronic ❑ acute E.2. Individual Test Data. Complete the column per test (where each species toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one constitutes a test). Copy this page if more than three tests are being reported. Test number: 1 Test number. 2 Test number. 3 a. Test information. Test Species & test method number Ceriodaphnia Ceriodaphnia Ceriodaphnia Age at initiation of test <24 hrs <24 hrs <24 hrs Outfall number 001 001 001 Dates sample collected 11/15/09,11/17/09,11/19/09 5/17/09,5/19/09,5/21/09 2/15/09,2/17/09,2/19/09 Date test started 11/17/09 5/19/09 2/17/09 Duration 24 hrs 24 hrs 24 hrs b. Give toxicity test methods followed. Manual title Chronic Manual Chronic Manual Chronic Manual Edition number and year of publication EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 Page number(s) 144-189 144-189 144-189 c. Give the sample collection me hod(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination X X X FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC00121181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Test number: 1 Test number: 2 Test number. 3 e_ Describe the point in the treatment process at which the sample was collected. Sample was collected: Before River Before Rive Before River f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity x x x Acute toxicity g. Provide the type of test performed. Static Static -renewal x x x Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water x x x Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water x x x Salt water j. Give the percentage effluent used for all concentrations in the test serves. 2,4,8,16,32 % 2,4,8,16,32 % 2,4,8,16,32 % k. Parameters measured during he test. (State whether parameter meets test method specifications) pH yes yes yes Salinity Temperature yes yes yes Ammonia Dissolved oxygen yes yes yes I. Test Results. Acute: Percent survival in 100% effluent 97.5 % 100 % 92.5 % LC50 95% C.I. Control percent survival 97.5 % 100 % 92.5 % FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Chronic: NOEC PASS % PASS PASS IC25 PASS % PASS % PASS % Control percent survival 97.5 % 100 % 92.5 % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? YES YES YES Was reference toxicant test within acceptable bounds? YES YES YES What date was reference toxicant test run (MM/DD/YYYY)? 11/17/2009 5119/2009 2/17/2009 Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes X❑ No Is the treatment works involved in a Tox city Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results. Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, or information regarding the the information was submitted to the permitting authority and a summary Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal Rl..(ER BA: ("°� �SINake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent IX chronic ❑ acute E.2. Individual Test Data. Complete the column per test (where each species toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one constitutes a test). Copy this page if more than three tests are being reported. Test number. 4 Test number: 5 Test number. 6 a. Test information. Test Species & test method number Ceriodaphnia Ceriodaphnia Ceriodaphnia Age at initiation of test <24 hrs <24 hrs <24 hrs Outfall number 001 001 001 Dates sample collected 11/12/08, 11/17/08 8/13/08, 8/18/08 5/14/08, 5/20/08 Date test started 11/13/08 8/15/08 5/16/08 Duration 24 hrs 24 hrs 24 hrs b. Give toxicity test methods followed. Manual title Chronic Manual Chronic Manual Chronic Manual Edition number and year of publication EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 Page number(s) 144-189 144-189 144-189 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination X X X FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC00121181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: flake Wylie Test number. 4 Test number: 5 Test number. 6 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Before River Before Rive Before River f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity x x x Acute toxicity g. Provide the type of test performed. Static Static -renewal x x x Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water x x x Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water x x x Salt water j. Give the percentage effluent used for all concentrations in the test series. 8 % 8 % 8 % k. Parameters measured during the test. (State whether parameter meets test method specifications) pH yes yes yes Salinity Temperature yes yes yes Ammonia Dissolved oxygen yes yes yes I. Test Results. Acute: Percent survival in 100% effluent 100 % 100 % 100 % LCso 95% C.I. % % % Control percent survival 100 % 100 % 100 % Other (describe) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal Colo. RIVER B IN: ake Wylie Chronic: NOEC PASS % PASS % PASS IC25 PASS % PASS % PASS % Control percent survival 100 % 91 % 100 % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? YES YES YES Was reference toxicant test within acceptable bounds? YES YES YES What date was reference toxicant test run (MM/DD/YYYY)? 11/13/08 8/15/08 5/16/08 Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes K No Is the treatment works involved in a Tox city Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results. Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, or information regarding the the information was submitted to the permitting authority and a summary Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: it (..t°``"')Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using altemate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent XI chronic ❑ acute E.2. Individual Test Data. Complete the column per test (where each species toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one constitutes a test). Copy this page if more than three tests are being reported. Test number: 7 Test number. 8 Test number. 9 a. Test information. Test Species & test method number Ceriodaphnia Ceriodaphnia Ceriodaphnia Age at initiation of test <24 hrs <24 hrs <24 hrs Outfall number 001 001 001 Dates sample collected 2/13/08, 2/18/08 11/07/07, 11/12/07 8/15/07, 8/20/07 Date test started 2/15/08 11/09/07 8/16/07 Duration 24 hrs 24 hrs 24 hrs b. Give toxicity test methods followed. Manual title Chronic Manual Chronic Manual Chronic Manual Edition number and year of publication EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 Page number(s) 144-189 144-189 144-189 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination X X X FACILITY NAME AND PERMIT NUMBER: City of Belmont, NCOO121181 PERMIT ACTION REQUESTED: Renewal RIVER BA IN: r24040,40 ake Wylie Test number: 7 Test number: 8 Test number. 9 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Before River Before Rive Before River f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity x x x Acute toxicity g. Provide the type of test performed. Static Static -renewal x x x Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water x x x Receiving water i. Type of dilution water. If salt water, specify "natural' or type of artificial sea salts or brine used. Fresh water x x x Salt water j. Give the percentage effluent used for all concentrations in the test senes. 8 % 8 % 8 % k. Parameters measured during the test. (State whether parameter meets test method specifications) pH yes yes yes Salinity Temperature yes yes yes Ammonia Dissolved oxygen yes yes yes I. Test Results. Acute: Percent survival in 100°% effluent 100 % 83 % 92 % LC50 95°% C.I. % % % Control percent survival 100 % 91 % 100 % Other (describe) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal R VER B N: ake Wylie Chronic: NOEC PASS % PASS % PASS IC25 PASS % PASS % PASS % Control percent survival 100 % 91 % 100 % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? YES YES YES Was reference toxicant test within acceptable bounds? YES YES YES What date was reference toxicant test run (MM/DD/YYYY)? 2/15/08 11/09/07 8/16/07 Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes .rxf No Is the treatment works involved in a Toxicity Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitortng Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results. Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, or information regarding the the information was submitted to the permitting authority and a summary Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal nRIVER B` SIN: �'0" ?Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • if you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using altemate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent k chronic ❑ acute E.2. Individual Test Data. Complete the column per test (where each species toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one constitutes a test). Copy this page if more than three tests are being reported. Test number. 10 Test number. 11 Test number. 12 a. Test information. Test Species & test method number Ceriodaphnia Ceriodaphnia Ceriodaphnia Age at initiation of test <24 hrs <24 hrs <24 hrs Outfall number 001 001 001 Dates sample collected 5/16/07, 5/17/07 2/14/07, 2/19/07 11/13/06, 11/16/06 Date test started 5/17/07 2/16/07 11/15/06 Duration 24 hrs 24 hrs 24 hrs b. Give toxicity test methods followed. Manual title Chronic Manual Chronic Manual Chronic Manual Edition number and year of publication EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 Page number(s) 144-189 144-189 144-189 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination X X X FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC00121181 PERMIT ACTION REQUESTED: Renewal°"' RIyER ASIN// ake Wylie Test number: 10 Test number: 11 Test number: 12 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Before River Before Rive Before River f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity x x x Acute toxicity g. Provide the type of test performed. Static Static -renewal x x x Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water x x x Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water x x x Salt water j. Give the percentage effluent used for all concentrations in the test serves. 8% 8% 8% k. Parameters measured during the test. (State whether parameter meets test method specifications) pH yes yes yes Salinity Temperature yes yes yes Ammonia Dissolved oxygen yes yes yes I. Test Resits. Acute: Percent survival in 100% effluent 100 % 100 % 100 % LC50 95% C.I. % % % Control percent survival 100 % 100 % 100 % Other (describe) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN) bbLa//ke Wylie Chronic: NOEC PASS % PASS % PASS IC25 PASS % PASS % PASS % Control percent survival 100 % 91 % 100 % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? YES YES YES Was reference toxicant test within acceptable bounds? YES YES YES What date was reference toxicant test run (MWDD/YYYY)? 5/17l07 2/16/07 11115/06 Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes :rit No Is the treatment works involved in a Tox city Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results. Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, or information regarding the the information was submitted to the permitting authority and a summary Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program? x❑ Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non -categorical Sills. 0 b. Number of CIUs. 1 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Spartan Dyers Inc. Mailing Address: P.O. Box 790 Belmont, N.C. 28012 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Commission Yam Dyeing F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Dyed Yam. Raw material(s): Yam, Electrolytes, (NaCI, Na2, SO4) Weak Organic Acids, Soda Ash, Sodium Hydro Sulfite, Softners, Detergent F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 175.400 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 15,500 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits X ❑ Yes ❑ No b. Categorical pretreatment standards ❑ Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? N/A FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must indude quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using altemate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent © chronic ❑ acute E.2. Individual Test Data. Complete the column per test (where each species toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one constitutes a test). Copy this page if more than three tests are being reported. Test number: 1 Test number: 2 Test number. 3 a. Test information. Test Species & test method number Chronic Fathead -Minnow Multi -Concentration Chronic Fathead -Minnow Multi -Concentration Chronic Fathead -Minnow Multi -Concentration Age at initiation of test <24 hrs <24 hrs <24 hrs Outfall number 001 001 001 Dates sample collected 2/15/09,2/17/06,2/19/09 5/17/09,5/19/09,5/21/09 8/16/09,8/18/09,8/20/09 Date test started 2/17/09 5/19/09 8/18/09 Duration 24 hrs 24 hrs 24 hrs b. Give toxicity test methods followed. Manual title Chronic Manual Chronic Manual Chronic Manual Edition number and year of publication EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 EPA-600-4-91-002 July 94 Page number(s) 58-139 58-139 58-139 c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X X X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination X X X 'FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC00121181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Test number: 1 Test number: 2 Test number: 3 e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Before River Before River Before River f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X X X Acute toxicity g. Provide the type of test performed. Static Static -renewal X X X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water X X X Receiving water i. Type of dilution water. If salt water, specify `natural" or type of artificial sea salts or brine used. Fresh water X X X Salt water j. Give the percentage effluent used for all concentrations in the test series. 2,4,8,16,32 % 2,4,8,16,32 % 2,4,8,16,32 k. Parameters measured during the test. (State whether parameter meets test method specifications) pH yes yes yes Salinity Temperature yes yes yes Ammonia Dissolved oxygen yes yes yes I. Test Results. Acute: Percent survival in 100% effluent LC50 95% C.I. Control percent survival Other (describe) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Chronic: NOEC >32% >32% >32% IC25 >32% >32% >32% Control percent survival 90 % 100 % 97.5 % Other (describe) ChV >32% >32% >32% m. Quality Control/Quality Assurance. Is reference toxicant data available? YES YES YES Was reference toxicant test within acceptable bounds? YES YES YES What date was reference toxicant test run (MM/DD/YYYY)? 2/10/2009 5/9/2009 8/1/2009 Other (describe) E.1. Required Tests. Indicate the number of whole effluent ® chronic 0 acute E.2. Individual Test Data. Complete the column per test (when: each species toxicity tests conducted in the past four and one-half years. following chart for each whole effluent toxicity test conducted in the last four and one-half vears. Allow one constitutes a test). Copy this page if more than three tests are being reported. Test number: 4 Test number. Test number: a. Test information. Test Species & test method number Chronic Fathead -Minnow Multi -Concentration Age at initiation of test <24 hrs Outfall number 001 Dates sample collected 11/15/09.11/17/09.11119/09 Date test started 11/17/09 Duration 24 hrs b. Give toxicity test methods followed. Manual title Chronic Manual Edition number and year of publication EPA-600-4-91-002 July 94 Page number(s) 58-139 c_ Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite X Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination X FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC00121181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Test number: 4 Test number: Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected: Before River f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity X Acute toxicity g. Provide the type of test performed. Static Static -renewal X Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water X Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water X Salt water j. Give the percentage effluent used for all concentrations in the test series. 2,4,8,16,32 % k. Parameters measured during the test. (State whether parameter meets test method specifications) pH yes Salinity Temperature yes Ammonia Dissolved oxygen yes I. Test Results. Acute: Percent survival in 100% effluent 97.5 LC50 95% C.I. ye Control percent survival 97.5 % Other (describe) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie Chronic: NOEC >32% IC25 >32% Control percent survival 97.5 % Other (describe) ChV >32% m. Quality Control/Quality Assurance. Is reference toxicant data available? YES Was reference toxicant test within acceptable bounds? YES What date was reference toxicant test run (MM/DD/YYYY)? 11103/09 Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes © No Is the treatment works involved in a Toxicity Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results_ Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, the information was submitted to the permitting or information regarding the authority and a summary Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes X ❑ No if yes, describe each episode. RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? 0 Yes X ❑ No (go to F.12) F.10. Waste transport Method by which RCRA waste is received (check all that apply): ❑ Truck 0 Rail 0 Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number Amount Units CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? 0 Yes (complete F.13 through F.15.) x❑ No F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the next five years). F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) F.15. Waste Treatment. a. Is this waste treated (or will be treated) prior to entering the treatment works? ❑ Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? 0 Continuous ❑ Intermittent If intermittent, describe discharge schedule. END OF PART F. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie SUPPLEMENTAL APPLICATION INFORMATION PART G. COMBINED SEWER SYSTEMS If the treatment works has a combined sewer system, complete Part G. G.1. System Map. Provide a a. All CSO discharge b_ Sensitive use areas outstanding natural c. Waters that support G.2. System Diagram. Provide includes the following information. a. Location of major sewer b. Locations of points c. Locations of in -line d. Locations of flow -regulating e. Locations of pump CSO OUTFALLS: map indicating the following: (may be included with Basic Application Information) points. potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and resource waters). threatened and endangered species potentially affected by CSOs. a diagram, either in the map provided in G.1 or on a separate drawing, of the combined sewer collection system that trunk lines, both combined and separate sanitary. where separate sanitary sewers feed into the combined sewer system. and off-line storage structures. devices. stations. Complete questions G.3 through G.6 once for each CSO discharge point. G.3. Description of Outfall. a. Outfall number b. Location (City or town, if applicable) (Zip Code) (County) (State) (Latitude) c. Distance from shore d. Depth below surface e. Which of the following ❑ Rainfall 0 CSO flow f. Flow many storm events G.4. CSO Events. a. Give the number of (Longitude) (if applicable) ft. (if applicable) ft. were monitored during the last year for this ❑ CSO pollutant concentrations volume 0 Receiving water quality were monitored during the last year? CSO events in the last year. events (❑ actual or ❑ approx.) CSO? 0 CSO frequency b. Give the average duration per CSO event. hours (0 actual or 0 approx.) FACILITY NAME AND PERMIT NUMBER: City of Belmont, NC0021181 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba -Lake Wylie G.5. G.6. c. Give the average volume per CSO event. million gallons (❑ actual or 0 approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall Description of Receiving Waters. a. Name of receiving water: b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code c. Name of State Management/River Basin: (if known): United States Geological Survey 8-digit hydrologic cataloging unit CSO Operations. Describe any known water quality impacts on the receiving water caused intermittent shell fish bed closings, fish kills, fish advisories, other recreational code (if known): by this CSO (e.g., permanent or intermittent beach closings, permanent or loss, or violation of any applicable State water quality standard). END OF PART G. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. ----- - 1 .. . - . - N' -; •-• • PM ,.,:.,„. •... .i.,)!,..,,,,,s,:.,..1,,...:.......,.:_•-•,„i:,, ii„,,„---.-11,,.. --,...'./..--..;`:1-‹: --; i....C.I.',...---••• 1•:.:. . . , 'II,: s,-„1-:-..- . ,. ',•,.. \ 7•-.:....t:..• -).---- :. ...,,t.,. - - .,. ..:-.,, 6" ,e. .-.1(i'V. 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Ch F ; • • II t • 1 City of Belmont WWTP Gaston County NC0021181 DIGESTER NO. 2 (EAST) DIGESTER NO. 1 (WEST) 0, Z-6 Z M 6- 8-S LEGEND PUMP AERATOR MIXER PLUG VALVE & GATE VALVE CHECK VALVE SLUICE LATE FLOW METER STRUCTURE WASTEWATER (Ww) RETURN ACTIVATED SLUDGE (RAS) WASTE ACTIVATED SLUDGE (WAS) DIGESTED SLVDGE (DS) SUPERNATANT (S) FLOW ARROW DIGESTER BUILDING Z a WW-2 DS-8 HTM-3 DIGESTER SLUDGE PUMPS 8-WAS • 12" WAS-14 THRU WAS-23 SLUDGE HOLDINM TANK r../ B'S 5-7 30" W W PARSHALL FLUME INFLUENT METER GRIT REMOVAL MECHANICAL BAR SCREEN PRETREATMENT (HEADWORKS) PLANT INFLUENT 05-10 DS49 TM-2 HOLDING TANK PUMP STATION 8"OS 6"WAS 4-Ds SLUDGE TO LAND DISPOSAL T SLUDGE PUMPS e_ 8-WAS AERATION BASIN NO. 2 (EAST) O EA-1 EA-2 EA-5 WW-12 a N WW-3 0 WA-3 WA-2 RAS-11 RAS-8 (6) EA-3 EA-4 RAS-12 RAS-13 ry Wt4-14 WW-SN RAS-9 RAS-10 WA-4 O 5 0_1 wA-•7 AERATION BASIN 3, 9 /116 NO. 1 (WEST) 0 WA-6 0 WA-8 20-RAS 8 WAS WAS-10 WAS FLOW METER— RAS FLOW METER FIGURE 11.1 V/ASTERWATER AND SLUDGE HANDLING SCHEMATIC SLUDGE PUMP STATION WAS-11 WAS-9 WAS-8 11 WAS-7 WAS-6 -- �Z � I RAS-6 �2 RAS-4 I L RAS-5 I I 20-RAS J f — — — JI WW-9 30"ww WW-8 WW-7 30-WW ri WW-6 14, RAS--3 WAS-4 'tip L SCUM PIT RAS-2 `WAS iti 34 p r 6 BPS 0/ CHLORINE CONTACT WAS-5 RAS-7 CLARIFIER NO. 2 (EAST) \�. r WAS-2 WAS-1 �/ CLARIFIER ND. 1 (WEST) 24-RAS RAS-1 Pr- WAS PUMPS RAS PUMPS SCUM PUMP WAS-3 24"Ww 3O"WW CHLORINE FEED SYSTEM TANK r),/O%MG 0.376 M6 3" DIFFUSER , "M'-1D 30" BYPASS EFFLUENT METER W.W.T.P. EFFLUENT 30"Ww WW-11 ee,t wwr ' wtA) 1 ! _ Ziv 5Pi--Gi ��- Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Facility: Belmont Laboratory: ETT Environmental, Inc. NPDES # NC0021181 Pi Signature of Operator in Responsible Charge Signature of Laboratory Supervisor pe #: 001 County: Gaston Comments! MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 8-Dec-15 % Eff. Control Repl. Surviving # Original # Wt/original (mg) 2 Surviving # Original # Wt/original (mg) 4 Surviving # Original # Wt/original (mg) 8 Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 16 32 Water Quality Data Control pH (SU) Init/Fin DO (mg/L) tnit/Fin Temp (C) Init/Fin High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp at Receipt ( C) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 1 / 1530 2 3 4 Avg Wt/Surv. Control 10 10 10 9 10 10 10 9 0.6160 0.6450 0.6130 0.7378 10 10 10 10 10 10 10 10 0.5150 0.6600 0.6660 0.5970 9 10 9 9 10 10 9 10 0.5700 0.6090 0.7578 0.5390 10 10 9 9 10 10 10 9 0.6930 0.6260 0.6260 0.8078 10 10 10 10 10 10 10 10 0.6060 0.7010 0.6610 0.7550 10 9 8 10 10 9 8 10 0.8330 0.7022 0.7163 0.8810 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.6530 100.0% 0.6530 100.0% 0.6095 94.9% 0.6190 97.4% 0.6882 100.0% 0.6808 100.0% 0.7831 0 1 2 3 4 5 8.2 / 7.6 7.8 / 7.7 7.9 / 7.5 8.0 / 7.5 8.1 / 7.2 7.8 / 7.6 7.8 / 7.8 7.7 / 6.6 7.1 / 5.7 7.7 / 5.3 7.8 / 6.3 7.9 / 4.3 7.4 / 5.4 7.6 / 6.1 25.0 / 24.9 24.9 1 25.4 24.7 / 25.4 24.6 / 24.8 24.6 1 25.3 24.8 / 24.7 24.5 / 25.4 0 1 2 3 4 5 7.7 / 7.6 7.6 / 7.4 7.7 / 7.4 7.8 / 7.3 8.0 / 7.2 7.6 / 7.3 7.7 / 7.6 8.1 / 6.9 7.4 / 5.0 8.3 / 4.9 7.9 / 4.7 8.0 / 4.3 7.5 / 4.8 7.7 / 5.8 25.0 1 24.9 24.5 / 25.4 25.0 / 25.4 24.7 1 24.8 24.4 / 25.3 24.8 / 24.7 24.3 / 25.4 1 2 3 12-7-15 12-09-15 12-10-15 24 hr 24 hr 24 hr 40.0 47.0 47.0 21.4 31.1 36.0 572 1057 1266 <0.05 _ <0.05 0.06 0.6 1.4 2.4 50.0 46.80 211 Test Organisms PlCultured In -House u X Outside Supplier Hatch Date: < 48 hrs Hatch Time: 1000-1000 Survival Growth Overall Result Normal III no I I yes ChV Hom. Var. no ❑ yes NOEC 32.0% 32.0% LOEC >32.0% >32.0% ChV >32.0% >32.0% Method Steels Dunnetts >32% Stats Survival Growth Conc. Critical Calculated Critical Calculated 2 10 18 2.41 0.70 4 10 14 2.41 0.61 8 10 16 2.41 -0.64 16 10 18 2.41 -0.50 32 10 18 2.41 -2.35 DWQ Form AT-5 (1/04) Page 2 of 6 Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Facility: Belmont Laboratory: ETT Environmental, Inc. NPDES # NC00 21181 Pi x Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor pe #: 001 County: Gaston Comments! MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 12-May-15 / 1628 % Eff. Control Repi. Surviving # Original # Wt/original (mg) Surviving # Original # Wtloriginal (mg) Surviving # Original # Wtloriginal (mg) 2 4 8 Surviving # Original # Wtloriginal (mg) 16 Surviving # Original # Wt/original (mg) 32 Surviving # Original # Wt/original (mg) Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp at Receipt ( C) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhoslcm) 1 2 3 Avg Wt/Surv. Control 10 9 10 10 10 9 10 10 0.7530 0.7811 0.7590 0.7440 9 10 10 10 10 10 10 10 0.7790 0.8990 0.8030 0.6700 9 10 10 10 9 10 10 10 0.7700 0.6260 0.7470 0.7000 10 9 8 6 - 10 9 8 8 0.7340 0.8111 0.7450 _ 0.9200 10 9 5 10 10 9 7 10 0.7120 0.7633 0.5843 0.7800 8 9 9 10 9 10 9 10 0.6467 0.5300 0.8156 0.8680 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) Survival Avg Wt (mg) 0.759 100.0% 0.7593 97.5% 0.7878 100.0% 0.7108 96.4% 0.8025 92.9% 0.7099 94.7% 0.7151 1 2 3 4 5 6 7.8 / 7.6 8.2 / 7.8 7.9 / 7.4 7.9 / 7.5 8.0 / 8.4 8.2 / 7.8 7.8 / 7.5 7.4 / 6.3 7.9 / 6.4 8.1 / 5.6 8.1 / 6.3 8.0 / 6.5 8.3 / 5.6 7.6 / 6.7 25.0 1 25.1 25.1 / 25.2 24.7 1 25.2 24.8 / 24.9 24.8 / 25.2 25.0 I 25.4 24.8 / 24.9 0 1 2 3 4 5 6 7.6 / 7.7 7.7 / 7.7 7.8 / 7.5 7.7 / 7.5 7.8 / 7.8 8.0 / 7.4 7.9 / 7.6 7.8 / 7.2 7.9 / 6.6 8.6 / 6.4 8.1 / 5.6 8.0 / 6.4 8.5 / 5.3 7.9 / 6.2 25.0 / 25.1 24.9 / 25.2 24.5 / 25.2 24.7 / 24.9 24.5 1 25.2 24.7 / 24.4 24.8 / 24.9 1 2 3 5-11-15 5-13-15 24 hr 24 hr 38.0 0.8 61.5 45.1 808 1145 _ <0.05 <0.05 0.6 _ 1.7 50.0 39.10 248 Survival Growth Normal 7 no [] yes Horn. Var. ❑ no yes NOEC 32.0% 32.0% LOEC >32.0% >32.0% ChV >32.0% >32.0% Method Steels Dunnetts Test Organisms )Cultured In -House U X Outside Supplier Hatch Date: 5-12-15 Hatch Time: 0730-0900 Overall Result ChV >32% Stats Survival Growth Conc. Critical Calculated Critical Calculated 2 10 17.5 2.41 -0.43 4 10 18 2.41 0.73 8 10 13 2.41 -0.65 16 10 15.5 2.41 0.75 32 10 13 2.41 0.67 t% DWQ Form AT-5 (1/04) Page 2 of 5 Ncov2�IsSl Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test x Facility: Belmont Laboratory: ETT Environmental, Inc. NPDES # NC00 21181 Pi Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor pe #: 001 County: Gaston Comments! MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 10-Nov-15 % Eff. Control Repl. Surviving # Original # Wt/original (mg) 2 Surviving # Original # Wt/original (mg) 4 Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 8 16 Surviving # Original # Wt/original (mg) 32 Surviving # Original # Wt/original (mg) Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) init/Fin High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp at Receipt ( C) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 1 / 1650 2 3 4 Avg Wt/Surv. Control 10 10 9 10 10 10 9 10 0.8260 0.9100 0.8920 0.9610 10 10 8 9 10 10 10 9 0.8640 0.8870 0.8660 0.9311 10 10 10 10 10 10 10 10 0.7770 0.9590 0.7900 1.0070 8 9 9 10 10 10 10 10 0.6840 0.8290 0.8960 0.9200 10 10 10 6 10 10 10 10 1.0000 1.1400 0.9860 0.6620 9 9 10 9 9 10 10 10 1.0078 0.9100 1.0220 0.8510 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.8973 100.0% 0.8973 94.9% 0.8870 100.0% 0.8833 90.0% 0.8323 90.0% 0.9470 94.9% 1 0.9477 0 1 2 3 4 5 6 8.3 / 7.3 7.4 / 6.5 7.8 / 7.3 7.8 / 7.3 7.8 / 7.2 7.8 / 7.5 7.9 / 7.4 8.1 / 5.5 6.2 / 7.7 7.7 / 6.0 7.4 / 5.3 7.2 / 5.8 7.3 / 6.3 8.1 / 6.1 24.7 1 24.6 24.5 / 24.9 24.6 / 24.9 24.9 / 24.7 24.5 1 24.7 24.6 / 24.8 24.4 / 24.5 0 1 2 3 4 5 6 7.9 / 7.3 8.0 / 7.3 7.7 / 7.3 7.7 / 7.3 7.6 / 7.4 7.6 / 7.4 7.8 / 7.4 7.9 / 5.9 7.8 / 5.4 7.7 / 5.6 8.1 / 5.4 7.8 / 5.7 7.1 / 6.1 8.1 / 5.6 25.0 1 24.6 24.3 / 24.9 _ 24.4 / 24.9 25.1 / 24.7 25.2 / 24.7 24.3 / 24.8 24.5 / 24.5 1 2 3 11-9-15 11-11-15 11-12-15 24 hr 24 hr 24 hr 46.0 48.0 48.0 26.9 72.0 52.0 517 869 960 <0.05 <0.05 <0.05 0.8 0.0 0.2 50.0 46.80 211 Normal Horn. Var. NOEC LOEC ChV Survival 11 Test Organisms I Cultured In -House u X Outside Supplier Hatch Date: 11/9-11/10 Hatch Time: 1500-1000 Growth Overall Result no ❑ yes ChV yes 1 I yes 32.0% 32.0% >32.0% >32.0% >32.0% >32.0% Method Rank Sum t Test >32% Stats Survival Growth Conc. Critical Calculated Critical Calculated 2 10 18.0 2.41 0.13 4 10 20.0 2.41 0.18 8 10 20.0 2.41 0.81 16 10 18.0 2.41 -0.62 32 10 14.0 2.41 -0.63 DWQ Form AT-5 (1/04) Page 2 of 6 Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Facility: Belmont Laboratory: ETT Environmental, Inc. NPDES # NC00 21181 Pi x Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor pe #: 001 County: Gaston Comments' MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 10-Feb-15 % Eff. Control Repl. Surviving # Original # Wt/original (mg) 2 Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 4 8 16 Surviving # Original # Wt/original (mg) 32 Surviving # Original # Wt/original (mg) Water Quality Data Control pH (SU) Init/Fin DO (mg/L) !nit/Fin Temp (C) 'nit/Fin High Concentration pH (SU) Init/Fin DO (mg/L) !nit/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp at Receipt ( C) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 1 / 1658 2 3 4 Avg Wt/Surv. Control 9 10 10 10 9 10 10 10 0.9256 0.9420 0.7420 0.7330 10 10 10 9 10 10 10 9 0.7120 0.8520 0.8610 0.8989 10 10 10 9 10 10 10 10 0.8680 0.9200 0.8760 0.7250 10 9 10 10 10 10 10 10 0.7670 0.6840 0.8960 0.8610 9 10 9 10 10 10 10 10 0.7020 0.8100 _ 0.9530 0.9900 10 10 9 10 10 10 9 10 1.0480 0.8820 0.8656 0.8490 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.8357 100.0% 0.8357 100.0% 0.8310 97.5% 0.8473 L 97.5% 0.8020 95.0% 0.8638 100.0% 0.9112 0 1 2 3 4 5 6 8.0 / 7.8 8.2 / 7.6 7.8 / 8.3 8.2 / 8.1 8.1 / 7.7 8.3 / 7.4 8.3 / 8.2 7.9 / 6.8 8.2 / 5.7 7.7 / 5.6 7.7 / 6.6 7.6 / 7.1 8.1 / 6.0 8.0 / 6.2 24.6 / 25.0 25.0 / 25.1 25.1 I 25.0 24.7 1 25.1 24.5 1 24.7 24.7 1 24.9 24.6 / 25.1 0 1 2 3 4 5 6 7.6 / 7.6 7.6 / 7.3 7.6 / 7.6 7.7 / 7.5 7.6 / 7.5 7.7 / 7.3 7.8 / 7.5 7.8 / 6.7 8.0 / 6.0 8.0 / 6.1 7.9 / 6.2 8.4 / 6.3 8.0 / 5.4 8.1 / 5.3 25.0 / 25.0 25.0 / 25.1 24.6 1 25.0 24.4 / 25.1 24.7 1 24.7 24.7 1 24.9 24.5 / 25.1 1 2 3 2-9-15 2-11-15 2-12-15 24 hr 24 hr 24 hr 40.0 42.0 38.0 24.2 47.0 50.2 607 937 1089 0.17 0.07 0.19 0.8 1.7 2.0 50.0 53.80 213 Survival Test Organisms I 1Cultured In -House U X Outside Supplier Hatch Date: 2-9-15 Hatch Time: 0730-0900 Growth Overall Result Normal f no 0 yes ChV I >32% Hom. Var. E no I I yes NOEC 32.0% 32.0% LOEC >32% >32% ChV >32% >32% Method Steels Dunnetts Stats Survival Growth Conc. Critical Calculated Critical Calculated 2 10 18 2.41 0.07 4 10 17.5 2.41 -0.16 8 10 17.5 2.41 0.47 16 10 15 2.41 -0.39 32 10 18 2.41 -1.05 Page 2 of 7 DWQ Form AT-5 (1/04) 06/30/2010 11:33 8648776936 ETT ENVIRONMENTAL PAGE 02 Effluent Toxicity Report Form -Chronic Fathad Minnow MuhlConeentralbn T1tta:05/29/09 Facility: Belmont NPDES M NC00 21181 Pi pea: 001 County: Gaston Laboratory: ETT Environmental Signature of Operator in RespaneiblZjI yi� ! it Signature of Laboratory Supervisor Comments' MAIL ORIGINAL TO: Environmental Sciences Rreaeh Division of Water Quality N(: DF.NR 1621 Mall Service Cantor Ratdgh,TIC 278194621 .dcLA€_, .2(4� InCi- �X 1 CCuv4 z fl c�Yr 01!IO(OC 1 Teat initiation Date/Time 17-Feb-09 % Eft. Control Reps. Surviving* Original 0 Wt/original (mg) Surviving N Original R WUorlglnal (mg) 2 Surviving N Original WUDriginal (mg) Surviving Original* IA!/original (mg) 41 8 10 Surviving x Original e WUoriglnal (mg) 32 Surviving* Original 4 WI/original (mg) Water Quality Data Control pH (SU) Ini /Fin DO (mg/L) IniuFin Temp (C) InIUFIn High Concentration pH (SU) IniUFin DO (mg/L) IniUFin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Conductivity (umhoahxn) Alkalinity (mg/L) Hardness (mg/I.) CP lorino(mg/L) Tamp at Receipt ('C) Test Organisms Cultured In -House Outside Supplier Hatch Oete/TIrnp / 1530 2 3 Avg Wt/Surv. Control 8 10 9 9 10 10 10 10 0 310 0.329 0.389 0.379 10 10 10 9 10 10 10 10 0,290 0.249 0,314 0.394 9 10 9 10 10 10 10 10 0.274 0.302 0.383 0.333 9 10 9 9 10 10 10 10 0.333 0.328 0.298 0.316 6 9 10 9 10 10 t0 10 0.329 0.262 0.310 0.294 10 9 9 10 10 10 10 10 0.322 0.339 0.342 0.356 Day % Survival Avg WI(mg) % Survival Avg Wt (rng) % Survival Avg WI (mg) °h Survival Avg WI (mg) % Survival Avg WI (mg) % Survival Avg Wt (mg) 0.387 0.347 97,5 0.312 L 95.0 0.323 92.5 0.319 90.0 0.304 95,0 0.340 0 2 3 4 5 8 7 8.2 / na 7.2 / 7.6 7.6 1 7.a 7.8 / 7.7 7.9 1 7.e 7.8 / 7.9 7.8 / 7.8 no / 7.7 8.5 / na 9.2 1 9.0 8.0 I 7.2 8.3 1 7.4 8.8 1 7.5 8.2 / 7.2 8.1 / 7.4 na / 8.3 25.1 / no 25.3 / 25.0 25.2 / 24,7 25.3 / 24.9 25.4 / 24.3 25.2 / 25,0 24.9 / 24.4 no / 24.0 D 2 3 4 5 8 7 7.9 / no 7.10 1 7.20 7.10 1 7.20 7.20 / 7.30 7.30 / 7.20 7.20 / 7.40 7.10 / 7.50 na / 7.30 8.3 / na 9.2 / 8.3 8.1 / 7.1 8 0 1 7.6 8.2 / 7.8 8.3 / 7.7 8.3 1 7.1 NI 1 7.8 25.2 1 na 25.4 1 25.0 25.5 / 24.7 25.3 / 24.9 25.2 1 24.3 24.7 / 25.0 25.2 / 24.4 na 1 24.8 2 3 02/15/09 02/17/09 02/19/09 24hr5 24hrs 24nrS 787 728 1014 50.0 52.0 81.4 60 54 58 <0.05 <0 05 <0.05 2.7 3.0 3.0 ,11111, X 02-1A-09 a Control Hardness 48 mg/L Alka9ntty 38.8 mg/L ConductMty 191 wnneuee / 11AM-2:30PM Survival Growth Normal We 0,95 yes 0.9e yes Hom. Var. 8= 1.o yea 0.97 yes NOEC > 32.0% > 320% LOEC > 32.0% > 32.0% ChV > 32.0% > 32.0% Method Dunn, I TOSI Dunn. t Teti CM Urtmm 2.55 2.55 Cone. 2.0% -1.63 1.37 4.0% -1,06 0.93 8.0% -00.49 1.08 16.0% 0 00 1,66 32.0% -1.06 0.27 DWG Form AT-5 (WON TT nvironmentai. inc. Mailing Address: P.O. Box 16414, Greenville, SC 28606-7414 Shipping Address: 4 Craftsman Court, Greer, SC 29660 Phone: (664) 077-6942 Fax: (984) 0774988 Toll ROW (8OO) 88142335 Email: maUUGsttanvironmsntal.com Facility:C N C &ir 1 HAS Site Description: gsf 1 t.�ff4 emirs; f Sa ff'yJ"e state: 14,c County: ei Gi.5 Y1 NI* DES d4W 1 I RI Pipe 114lbi CHAIN OF C...STODY FORM GRAB SAMPLES Collected By (print): Signatuue: Datemme: Pro COMPOSITE SAMPLES set By (print): 6. «oSCnbeeg Collected Signature: £ . fiaiosaloc L Signature: LA Date/fcne: z,z oa1 Sdt{R+m Dawn. 114}09 1)1/'t'k Frequancyilis.davraitAtkeittegtateple Chiiled7 Yea 1 No C-\Z 2cs1 dtk&t— -0H 09 Page et - m • ..,. .VL-q iilA0:fm .. .:CYTGT�•Ql. ;JO t JYY `'fl3m _ Y#AYiWY{WA7 AAY' AO r c a(82 e ikt �YMA�Vfi .c1i ___ !•�w• tlefnte�it' w.�. a=... ..{•; 7...•t••:.•;VS:••�w.. :�.'i:ce. .....-_.. .._..:�+.'.]....-, ca r -rs . 2. 'c-'. 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Transport Metlactildd Received By (Signature): RECEIPT AT LABORATORY • -.III0/114,( Relinquished By• - ' '1 • d By: • ,:• nzalion: 4— Organization:Datefrrme: 1t DalelTime: Z, /f . a r %�.if Unsealed By: k �'� Arrival Temp: .3O 'C Sample Disposed/Returned By: Date: pases.vaHww wea....nadasfinna aim Irinur if bT MwpanlwaHnn limas .«...w.►wa•.a-••• ww• ••.a 0IOL/0£/90 8£69LL8098 101N3WNO8IAN3 LL TT nvironmental. Inc. Mailing Address: P.O. Box 16414, Gresnvilte, SC 26606-7414 Shipping Addrs= 4 Crastsrnan Court. Greer. SC 29660 Phone: (864) 677-6942 Fax: (6S4) BT7-6938 Toll Free: (900) 891.2325 Email: mailOettenvirorrmentaLcom FacitrtyCt4% j IMAM 4- ti i Silo Oescrlplion: Calfirf rbinfleIS i t 5 ,pl L State: 11 count,: C1Cu5itn NPOES 0: L ) I RI Pipe * CO •a•tOil` tyathr 2i QF! 2. CHAIN OF C.-STODY FORM GRAB SAMPLES 0 z Residua i • QI p — • JAI 3 Page t of 1 Collected By (print): Signature: Date/Tine: s•C�ar^♦ ,asitax . e t4 _ i COMPOSITE SAMPLES Set By (printrr Stig,eCollected by::7 f7 S�gnaiurf Signaturec"1 ,,AL., Daterrims:71. q VW, �w�Dna�te me 212af a 0� Frequency: WL i��{►nr, t" ' 63Ii� ie Chiliad? Yes 1 No Program Area _aa. r• aa..a♦ •.i. yx: :g: ♦ •<♦ — a1J }?;:?: ... var :•:: c. Yt:I C i (MIL —MXiCc4,f ETI IIiTi ISAMPLECUSTODY TRANSFER RECORD (Please sign) Sample Seared By: Relinqurshed By: Received By: Relinquished By: Received Br "4‹ Kr -- Relinquished By: Received By: Relinquished By: Received By: ntzation:G. o � nization: BC rn Organization: Organization: i\ Stew to.f+' t CtSX 1i lam. Organization: Organization: Organization: Organization: Preservativa concentrations are below DOTooncentration Wale. DatelTime: zJ,Ojacr l't)PO Data/Time: ,V4i ideali‘f Date/Time: Date/Time: Date/Time: Date/Time: Date/Time: Datellhne: SAMPLE TRANSPORT Carder: 6 e Transport Metho Received By (Signature): RECEIPT AT LABORATORY Relinquished By �.111rOr — � 12aB , . • . �T OrganRation r: Date/Time: 2 DatefTime: . ar% ed Atrial Temp: 3.1 'C Sample Disposed/Returned By: Date: 010Z/0E/90 8£69LL8098 Z N+ Inorganic non-metals Client: City of Belmont Description: Effluent Date Sampled:01125/2017 0850 Date Received:01/25/2017 Laboratory ID: SA25079-001 Matrix: Aqueous Run Prep Method 1 350.1 1 1 2 1 1 351.4 Analytical Method (Ammonia - N ) 350.1 (Hardness (to) SM 2340C-2011 (Nitrate-Nitr) 353.2 (Phosphorus) 365.1 (TDS) SM 2540C-2011 (TKN) 351.2 Dilution 1 1 10 5 1 1 Analysis Date Analyst 02/02/20171548 MSG 01/30/20171841 DMA 02/01/20171545 MSG 02/02/20171045 KWP 01/26/20171140 CLM 02/01/20171157 KWP Batch 33383 32967 33237 02/01/2017 1656 33202 32654 01 /31 /2017 1535 33096 Prep Date Parameter Ammonia - N (gas diffusion) Hardness (total) Nitrate -Nitrite - N Phosphorus TDS TKN CAS Number 7723-14-0 Analytical Method Result Q 350.1 0.36 SM 2340C-20 38 353.2 8.9 365.1 0.98 SM 2540C-20 420 351.2 2.3 PQL 0.10 10 0.20 0.050 10 0.10 Units Run mglL 1 mg!L 1 mg1L 1 mg/L 2 mg1L 1 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% No Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W Shealy Environmental Services, Inc. Page: 4 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Semivolatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:01/25/2017 0850 Date Received:01/25/2017 Laboratory ID: SA25079-001 Matrix: Aqueous Run Prep Method 1 625 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625 1 01/30/2017 1546 RBH 01/27/2017 1140 32766 Parameter Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene 4-Bromophenyl phenyl ether Butyl benzyl phthalate bis (2-Chloro-1-methylethyl) ether 4-Chloro-3-methyl phenol bis(2-Chloroethoxy)methane bis(2-Chloroethyl)ether 2-Chloronaphthalene 2-Chiorophenol 4-Chlorophenyl phenyl ether Chrysene Dibenzo(a,h)anthracene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Diethylphthalate Dimethyl phthalate 2,4-Dimethylphenol Dl-n-butyl phthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate 1,2-Diphenylhydrazine(as azobenzene) bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachiorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d )pyrene Isophorone CAS Analytical Number Method Result Q PQL Units Run 83-32-9 625 ND 1.6 ug/L 1 208-96-8 625 ND 1.6 ug/L 1 120-12-7 625 ND 1.6 ug/L 1 92-87-5 625 ND ' 8.0 ug/L 1 56-55-3 625 ND 1.6 ug/L 1 50-32-8 625 ND 1.6 ug/L 1 205-99-2 625 ND 1.6 ug/L 1 191-24-2 625 ND 1.6 ug/L 1 207-08-9 625 ND 1.6 ug/L 1 101-55-3 625 ND 1.6 ug/L 1 85-68-7 625 ND 1.6 ug/L 1 108-60-1 625 ND 1.6 ug/L 1 59-50-7 625 ND 1.6 ug/L 1 111-91-1 625 ND 1.6 ug/L 1 111-44-4 625 ND 1.6 ug/L 1 91-58-7 625 ND 1.6 ug/L 1 95-57-8 625 ND 1.6 ug/L 1 7005-72-3 625 ND 1.6 ug/L 1 218-01-9 625 ND 1.6 ug/L 1 53-70-3 625 ND 1.6 ug/L 1 95-50-1 625 ND 1.6 ug/L 1 541-73-1 625 ND 1.6 ug/L 1 106-46-7 625 ND 1.6 ug/L 1 91-94-1 625 ND 8.0 ug/L 1 120-83-2 625 ND 1.6 ug/L 1 84-66-2 625 ND 1.6 ug/L 1 131-11-3 625 ND 1.6 ug/L 1 105-67-9 625 ND 1.6 ug/L 1 84-74-2 625 ND 1.6 ug/L 1 534-52-1 625 ND 8.0 ug/L 1 51-28-5 625 ND 8.0 ug/L 1 121-14-2 625 ND 3.2 ug/L 1 606-20-2 625 ND 3.2 ug/L 1 117-84-0 625 ND 1.6 ug/L 1 103-33-3 625 ND 1.6 ug/L 1 117-81-7 625 ND 1.6 ug/L 1 206-44-0 625 ND 1.6 ug/L 1 86-73-7 625 ND 1.6 ug/L 1 118-74-1 625 ND 1.6 ug/L 1 87-68-3 625 ND 1.6 ug/L 1 77-47-4 625 ND 8.0 ug/L 1 67-72-1 625 ND 1.6 ug/L 1 193-39-5 625 ND 1.6 ug/L 1 78-59-1 625 ND 1.6 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC cotumns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a W Shealy Environmental Services, Inc. Page: 5 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Semivolatile Organic Compounds by GC/MS Client: City of Belmont Description: Effluent Date Sampled:01/2512017 0850 Date Received:01125/2017 Laboratory ID: SA25079-001 Matrix: Aqueous Run Prep Method 1 625 Analytical Method Dilution Analysis Date Analyst Prep Date Batch ' 625 1 01/30/2017 1546 RBH 01/27/2017 1140 32766 Parameter Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine (Diphenylamine) Pentachlorophenol Phenanthrene Phenol Pyrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol CAS Analytical Number Method Result Q PQL 91-20-3 625 ND 1.6 98-95-3 625 ND 1.6 88-75-5 625 ND 3.2 100-02-7 625 ND 8.0 62-75-9 625 ND 1.6 621-64-7 625 ND 1.6 86-30-6 625 ND 1.6 87-86-5 625 ND 8.0 85-01-8 625 ND 1.6 108-95-2 625 ND 1.6 129-00-0 625 ND 1.6 120-82-1 625 ND 1.6 88-06-2 625 ND 1.6 Run 1 Acceptance Surrogate Q % Recovery Limits Units Run ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 2-Fluorobiphenyl 63 37-129 2-Fluorophenol 35 24-127 Nitrobenzene-d5 65 38-127 Phenol-d5 47 28-128 Terphenyl-d14 48 10-148 2,4,6-Tribromophenol 66 41-144 POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery 1s out of criteria Where applicable. all sot sample analysis are reported on a dry weight basis unless flagged with a "W" Shealy Environmental Services, Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com ICP-MS Client: City of Belmont Description: Effluent Date Sampled:01/2512017 0850 Date Received:01/2512017 Laboratory ID: SA25079-001 Matrix: Aqueous Run Prep Method 1 200.2 2 200.2 3 200.2 Analytical Method Dilution Analysis Date Analyst 200.8 1 01/28/2017 0117 BNW 200.8 1 01/30/2017 1322 BNW 200.8 1 01/30/2017 1753 BNW Prep Date Batch 01/26/2017 1925 32681 01/26/2017 1925 32681 01/26/2017 1925 32681 Parameter Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Nickel Selenium Silver Thallium Zinc CAS Analytical Number Method Result Q 7440-36-0 200.8 23 7440-38-2 200.8 ND 7440-41-7 200.8 ND 7440-43-9 200.8 ND 7440-47-3 200.8 ND 7440-50-8 200.8 11 7439-92-1 200.8 ND 7440-02-0 200.8 ND 7782-49-2 200.8 3.7 7440-22-4 200.8 ND 7440-28-0 200.8 ND 7440-66-6 200.8 60 PQL 1.0 1.0 0.40 0.10 5.0 1.0 1.0 5.0 1.0 1.0 0.50 10 Units Run uglL 3 ug/L 1 ug/L 1 ug/L 1 ug/L 1 uglL 1 ug/L 1 ug/L 1 ug/L 2 ug/L 1 ug/L 1 ug/L 1 POL = Practical guantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N s Recovery is out of criteria Where applicable, ail soil sample analysis are reported on a dry weight basis unless flagged with a -W- Shealy Environmental Services, Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client: City of Belmont Description: Effluent Date Sampled:01/2512017 0831 Date Received:0112512017 Laboratory ID: SA25079-002 Matrix: Aqueous Run Prep Method Analytical Method 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- (Phenolics) 420.4 1 (HEM (oil and) 1664B 1 Dilution 1 1 1 Analysis Date Analyst 02/02/20171638 KWP 01/27/2017 2207 MSG 01/31/20171134 JMM Prep Date Batch 02/02/2017 1120 33353 01/26/2017 1441 32698 33049 Parameter Cyanide - Total Phenolics HEM (oil and grease) CAS Number 57-12-5 Analytical Method Result Q SM 4500-CN 0.013 420.4 ND 1664E ND PQL 0.010 0.020 4.4 Units Run mg/L 1 mg/L 1 mg/L 1 POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < POL and MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, an soil sample analysis are reported on a dry weight basis unless flagged with a W. Shealy Environmental Services, Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Volatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:01/25/2017 0831 Date Received:01/25/2017 Laboratory ID: SA25079-002 Matrix: Aqueous Run Prep Method 1 5030B Analytical Method Dilution Analysis Date Analyst Prep Date Batch 624 1 01/26/2017 2353 JJG 32727 Parameter Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane (Methyl bromide) Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane (Methyl chloride) Dibromochloromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Vinyl chloride Surrogate CAS Analytical Number Method Result Q PQL 107-02-8 624 ND 50 107-13-1 624 ND 50 71-43-2 624 ND 5.0 75-27-4 624 ND 5.0 75-25-2 624 ND 5.0 74-83-9 624 ND 5.0 56-23-5 624 ND 5.0 108-90-7 624 ND 5.0 75-00-3 624 ND 5.0 110-75-8 624 ND 10 67-66-3 624 ND 5.0 74-87-3 624 ND 5.0 124-48-1 624 ND 5.0 75-34-3 624 ND 5.0 107-06-2 624 ND 5.0 75-35-4 624 ND 5.0 156-60-5 624 ND 5.0 78-87-5 624 ND 5.0 10061-01-5 624 ND 5.0 10061-02-6 624 ND 5.0 100-41-4 624 ND 5.0 75-09-2 624 ND 5.0 79-34-5 624 ND 5.0 127-18-4 624 ND 5.0 108-88-3 624 ND 5.0 71-55-6 624 ND 5.0 79-00-5 624 ND 5.0 79-01-6 624 ND 5.0 75-01-4 624 ND 5.0 Run 1 Acceptance Q % Recovery Limits Units Run ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 1,2-Dichloroethane-d4 120 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 107 70-130 POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W- Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Sample Summary City of Belmont Lot Number: SC17044 Sample Number Sample ID 001 Effluent Comp 002 Upstream 003 Effluent Cornp 004 Upstream 005 Effluent Comp 006 Effluent Comp 007 Upstream 008 Effluent Comp 009 Upstream 010 Upstream Matrix Date Sampled Date Received Aqueous 03/13/2017 0858 03/17/2017 Aqueous 03/13/20171128 03/17/2017 Aqueous 03/142017 0851 03/17/2017 Aqueous 03/1420171044 03/17/2017 Aqueous 03/152017 0848 03/17/2017 Aqueous 03/162017 0853 03/17/2017 Aqueous 03/1620171117 03/17/2017 Aqueous 03/17/2017 0840 03/17/2017 Aqueous 03/17/2017 0847 03/17/2017 Aqueous 03/p/20171115 03/17/2017 (10 samples) tS C0entCity of Belmont Description: Effluent Comp Date Sampled:03/13/2017 0858 Date Received:03117/2017 Laboratory ID: SC17044-001 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result Q 37 PQL Units Run 10 mg/L 1 Client City of Belmont Description: Upstream Date Sampled:03/13/20171128 Date Received:03/172017 Laboratory ID: SC17044-002 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03/242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result Q 20 PQL 10 Units Run mglL 1 CiientCity of Belmont Description: Effluent Comp Date Sampled:03/142017 0851 Date Received:03/172017 Laboratory ID: SC17044-003 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03/242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result Q PQL Units Run 33 10 mglL 1 Client City of Belmont Description: Upstream Date Sampled:03/1420171044 Date Received:03/17/2017 Laboratory ID:SC17044-004 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03/24/2017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result 0 22 PQL 10 Units Run mglL 1 Client City of Belmont Description: Effluent Comp Date Sampled:03/15/2017 0848 Date Received:03/17/2017 Laboratory ID: SC17044-005 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03/242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result Q PQL 33 10 Units Run mglL 1 ..._.a......_ ........__..._ Client City of Belmont Description: Effluent Comp Date Sampled:031162017 0853 Date Received:03/17/2017 Laboratory ID: SC17044-006 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result 0 33 PQL 10 Units Run mglL 1 ClientCity of Belmont Description: Upstream Date Sampled:03/16/20171117 Date Received:03/17/2017 Laboratory ID: SC17044-007 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 031242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number fettg SM 2340C-20 Result 0 20 PQL 10 Units Run mg/L 1 ClientCity of Belmont Description: Effluent Comp Date Sampled:03/17/2017 0840 Date Received:03/17/2017 Laboratory ID:SC17044-008 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03/242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result 0 33 PQL Units Run 10 mg/L 1 CfientCity of Belmont Description: Upstream Date Sampled:03/172017 0847 Date Received:03/17/2017 Laboratory ID: SC17044-009 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number Method SM 2340C-20 Result Q 20 PQL 10 Units Run mgfL 1 CbentCity of Belmont Description: Upstrea1 Date Sampled:03 m171115 Date Received:03/17/2017 Laboratory ID: SC17044-010 Matrix: Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 (Hardness (to) SM 2340C-2011 1 03242017 0955 BWS Batch 37971 Parameter Hardness (total) CAS Analytical Number JWlejjeod Result Q PQL SM 2340C-20 20 10 Units Run mg/L 1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number: PE07095 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 05/07/2014 0915 05/07/2014 002 Effluent Aqueous 05/07/2014 0922 05/07/2014 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client: City of Belmont Description: Effluent Date Sampled:06/07/2014 0915 Date Received:06/07/2014 Laboratory ID: PE07095-001 Matrix: Aqueous Run Prep Method 1 350.1 1 1 1 1 1 351.4 Analytical Method (Ammonia - N ) 350.1 (Hardness (to) SM 2340C-2011 (Nitrate-Nitr) 353.2 (Phosphorus) 365.1 (TDS) SM 2540C-2011 (TKN) 351.2 Dilution 1 5 20 10 1 1 Analysis Date 05/16/2014 1257 05/19/2014 1920 05/08/2014 1753 05/24/2014 1500 05/12/2014 1608 05/15/2014 1423 Analyst Prep Date Batch BLB 05/14/20141558 46767 TAF 47249 AKW 46460 NCM 05/23/20141628 47416 AKG 46588 NCM 05/13/20141500 46666 Parameter Ammonia - N (phonate) Hardness (total) Nitrate -Nitrite - N Phosphorus TDS TKN CAS Number 7723-14-0 Analytical Method 350.1 SM 2340C-20 353.2 365.1 SM 2540C-20 351.2 Result Q 0.35 52 32 4.7 680 1.9 PQL 0.10 50 0.40 0.10 10 0.10 Units Run mg/L 1 mg/L 1 mg/L 1 mg1L 1 mg/L 1 mg/L 1 PQL = Practical quantitation limit ND = Not detected at or above the PQL B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, ail soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 4 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Semivolatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:05/07/2014 0915 Date Received:05/07/2014 Laboratory ID: PE07095-001 Matrix: Aqueous Run Prep Method 1 625 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625 1 05/13/2014 1828 DRB1 05/09/2014 1212 46479 Parameter CAS Analytical Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug/L 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug/L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 ug/L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 ug/L 1 2-Chlorophenol 95-57-8 625 ND 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug/L 1 Chrysene 218-01-9 625 ND 2.0 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 ug/L 1 Diethylphthalate 84-66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug/L 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug/L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 ug/L 1 Fluoranthene 206-44-0 625 ND 2.0 ug/L 1 Fluorene 86-73-7 625 ND 2.0 ug/L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug/L 1 Hexachiorobutadiene 87-68-3 625 ND 2.0 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug/L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug/L 1 lsophorone 78-59-1 625 ND 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < P0L and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W' Shealy Environmental Services, Inc. Page: 5 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Semivolatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:05/07/2014 0915 Date Received:05/07/2014 Laboratory ID: PE07095-001 Matrix: Aqueous Run Prep Method 1 625 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625 1 05/13/2014 1828 DRB1 05/09/2014 1212 46479 Parameter CAS Analytical Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug/L 1 Pentachlorophenol 87-86-5 625 ND 10 ug/L 1 Phenanthrene 85-01-8 625 ND 2.0 ug/L 1 Phenol 108-95-2 625 ND 2.0 ug/L 1 Pyrene 129-00-0 625 ND 2.0 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 2.0 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 78 37-129 2-Fluorophenol 70 24-127 Nitrobenzene-d5 70 38-127 Phenol-d5 71 28-128 Terphenyl-d14 57 10-148 2,4,6-Tribromophenol 90 41-144 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and> MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a NT Shealy Environmental Services, Inc. Page: 6 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com ICP-MS Client: City of Belmont Description: Effluent Date Sampled:05107/2014 0915 Date Received:05/07/2014 Laboratory ID: PE07095-001 Matrix: Aqueous Run Prep Method 1 200.2 2 200.2 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 200.8 1 05/08/2014 2014 CDF 05/08/2014 0957 46363 200.8 1 05/09/2014 1925 CDF 05/08/2014 0957 46363 Parameter Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Nickel Selenium Silver Thallium Zinc CAS Analytical Number Method Result Q PQL Units Run 7440-36-0 200.8 8.8 1.0 ug/L 1 7440-38-2 200.8 12 1.0 ug/L 1 7440-41-7 200.8 ND 0.40 ug/L 1 7440-43-9 200.8 ND 0.10 ug/L 1 7440-47-3 200.8 ND 5.0 ug/L 1 7440-50-8 200.8 20 1.0 ug/L 2 7439-92-1 200.8 ND 1.0 ug/L 1 7440-02-0 200.8 ND 5.0 ug/L 1 7782-49-2 200.8 1.5 1.0 ug/L 1 7440-22-4 200.8 ND 1.0 ug/L 1 7440-28-0 200.8 ND 0.50 ug/L 2 7440-66-6 200.8 130 10 ug/L 1 POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 7 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:City of Belmont Description: Effluent Date Sampled:05/07/2014 0922 Date Received:05/07/2014 Laboratory ID: PE07095-002 Matrix: Aqueous Run Prep Method Analytical Method 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- (Phenolics) 420.4 1 (HEM (oil and) 1664E 1 Dilution Analysis Date Analyst 1 05/17/20141800 NCM 1 05/19/2014 2107 TAF 1 05/15/2014 0025 TDT Prep Date Batch 05/17/20141340 46817 05/14/20141505 46761 46783 Parameter Cyanide - Total Phenolics HEM (oil and grease) CAS Number 57-12-5 Analytical Method SM 4500-CN 420.4 1664B Result Q PQL 0.011 ND 6.4 0.010 0.020 4.7 Units Run mg/L 1 mg/L 1 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 8 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Volatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:05/07/2014 0922 Date Received:05/07/2014 Laboratory ID: PE07095-002 Matrix: Aqueous Run Prep Method 1 5030B Analytical Method Dilution Analysis Date Analyst Prep Date Batch 624 1 05/13/2014 2129 PMM2 46702 Parameter Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane (Methyl bromide) Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane (Methyl chloride) Dibromochloromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetra chloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Vinyl chloride CAS Analytical Number Method Result Q PQL Units Run 107-02-8 624 ND 50 ug/L 1 107-13-1 624 ND 50 ug/L 1 71-43-2 624 ND 5.0 ug/L 1 75-27-4 624 ND 5.0 ug/L 1 75-25-2 624 ND 5.0 ug/L 1 74-83-9 624 ND 5.0 ug/L 1 56-23-5 624 ND 5.0 ug/L 1 108-90-7 624 ND 5.0 ug/L 1 75-00-3 624 ND 5.0 uglL 1 110-75-8 624 ND 10 ug/L 1 67-66-3 624 5.7 5.0 ug/L 1 74-87-3 624 ND 5.0 ug/L 1 124-48-1 624 ND 5.0 ug/L 1 75-34-3 624 ND 5.0 ug/L 1 107-06-2 624 ND 5.0 ug/L 1 75-35-4 624 ND 5.0 ug/L 1 156-60-5 624 ND 5.0 ug/L 1 78-87-5 624 ND 5.0 ug/L 1 10061-01-5 624 ND 5.0 ug/L 1 10061-02-6 624 ND 5.0 ug/L 1 100-41-4 624 ND 5.0 ug/L 1 75-09-2 624 ND 5.0 ug/L 1 79-34-5 624 ND 5.0 ug/L 1 127-18-4 624 ND 5.0 ug/L 1 108-88-3 624 ND 5.0 ug/L 1 71-55-6 624 ND 5.0 ug/L 1 79-00-5 624 ND 5.0 ug/L 1 79-01-6 624 ND 5.0 ug/L 1 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 105 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 112 70-130 PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 9 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Zo 13 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number: 0B07109 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 02/07/2013 0930 02/07/2013 002 Effluent Aqueous 02/07/2013 0935 02/07/2013 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 Level 1 Report v2 1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Inorganic non-metals Client:City of Belmont Description: Effluent Date Sampled:02/07/2013 0930 Date Received:02/07/2013 Laboratory ID: 0B07109-001 Matrix: Aqueous Run Prep Method 1 SM4500-NH3 1 1 1 1 1 351.4 Analytical Method (Ammonia - N) 350.1 (Hardness (to) SM 2340C- (Nitrate-Nitr) 353.2 (Phosphorus) 365.1 (TDS) SM 2540C-2011 (TKN) 351.2 Dilution 1 1 50 10 1 1 Analysis Date 02/20/2013 1029 02/08/2013 1015 02/19/2013 1706 02/14/2013 1644 02/14/2013 0814 02/19/2013 1614 Analyst MML KMB HBB MML KES MML Batch 02/19/2013 0900 14382 13636 14478 02/13/2013 1630 14085 14051 02/18/2013 1319 14334 Prep Date Parameter Ammonia - N (phenate) Hardness (total) Nitrate -Nitrite - N Phosphorus TDS TKN CAS Number 7723-14-0 Analytical Method 350.1 SM 2340C-20 353.2 365.1 SM 2540C-20 351.2 Result Q 0.37 50 18 3.0 640 0.68 PQL 0.10 10 1.0 0.10 10 0.10 Units Run mg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L 1 mglL 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure Shealy Environmental Services, Inc. Page: 4 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com Semivolatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:02/07/2013 0930 Date Received:02/07/2013 Laboratory ID: 0B07109-001 Matrix: Aqueous Run Prep Method 1 625 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625 2 02/14/20131730 RBH 02/11/20131013 13738 Parameter CAS Analytical Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug/L 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug/L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 ug/L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 ug/L 1 2-Chlorophenol 95-57-8 625 ND 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug/L 1 Chrysene 218-01-9 625 ND 2.0 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 ug/L 1 Diethylphthalate 84-66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug/L 1 2,4-Dimethylphenol 105-67-9 625 ND L 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug/L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.1 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.1 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 ug/L 1 Fluoranthene 206-44-0 625 ND 2.0 ug/L 1 Fluorene 86-73-7 625 ND 2.0 ug/L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug/L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug/L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug/L 1 lsophorone 78-59-1 625 ND 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL E = Quantitation of compound exceeded the calibration range H = Out of holding time 0 = Surrogate failure P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W- S = MS/MSD failure Shealy Environmental Services, Inc. Page: 5 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Semivolatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:02/07/2013 0930 Date Received:02/07/2013 Laboratory ID: OB07109-001 Matrix: Aqueous Run Prep Method 1 625 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625 2 02/14/20131730 RBH 02/11/20131013 13738 Parameter CAS Analytical Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.1 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug/L 1 Pentachlorophenol 87-86-5 625 ND 10 ug/L 1 Phenanthrene 85-01-8 625 ND 2.0 ug/L 1 Phenol 108-95-2 625 ND 2.0 ug/L 1 Pyrene 129-00-0 625 ND 2.0 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 2.0 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,4,6-Tribromophenol 52 41-144 Phenol-d5 51 28-128 Nitrobenzene-d5 51 38-127 2-Fluorobiphenyl 47 37-129 2-Fluorophenol 44 24-127 Terphenyl-d14 39 10-148 POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time 0 = Surrogate failure ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS1LCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a ' W' S = MS/MSD failure Shealy Environmental Services, Inc. Page: 6 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com ICP-MS Client: City of Belmont Description: Effluent Date Sampled:02/0712013 0930 Date Received:02107/2013 Laboratory ID: OB07109-001 Matrix: Aqueous Run Prep Method 1 200.2 2 200.2 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 200.8 1 02/08/2013 2126 CDF 02/08/2013 1048 13601 200.8 1 02/12/2013 1040 CDF 02/08/2013 1048 13601 Parameter Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Nickel Selenium Silver Thallium Zinc CAS Analytical Number Method Result Q PQL Units Run 7440-36-0 200.8 9.4 1.0 ug/L 2 7440-38-2 200.8 ND 1.0 ug/L 1 7440-41-7 200.8 ND 0.40 ug/L 1 7440-43-9 200.8 ND 0.10 ug/L 1 7440-47-3 200.8 ND 5.0 ug/L 1 7440-50-8 200.8 22 1.0 ug/L 1 7439-92-1 200.8 ND 1.0 ug/L 1 7440-02-0 200.8 ND 5.0 ug/L 1 7782-49-2 200.8 ND 1.0 ug/L 1 7440-22-4 200.8 ND 1.0 ug/L 1 7440-28-0 200.8 ND 0.50 ug/L 1 7440-66-6 200.8 160 10 ug1L 1 PQL = Practical quantization limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time 0 = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure Shealy Environmental Services, Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client: City of Belmont Description: Effluent Date Sampled:02/07/2013 0935 Date Received:02/07/2013 Laboratory ID: OB07109-002 Matrix: Aqueous Run Prep Method Analytical Method 1 10-204-00-1-X (Cyanide - To) SM 4500-CN 1 (Phenolics) 420.4 1 (HEM (oil and) 1664E Dilution 1 1 1 Analysis Date 02/14/2013 0059 02/19/2013 2348 02/18/2013 0953 Analyst Prep Date Batch M M L 02/13/2013 1205 13908 HBB 02/19/2013 1100 14383 AJK 14258 Parameter Cyanide - Total Phenolics HEM (oil and grease) CAS Number 57-12-5 Analytical Method SM 4500-CN 420.4 1664B Result Q PQL ND 0.025 ND 0.010 0.020 4.5 Units Run mg/L 1 mg/L 1 mg/L 1 POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a' W' S = MSIMSD failure Shealy Environmental Services, Inc. Page: 8 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Volatile Organic Compounds by GC/MS Client:City of Belmont Description: Effluent Date Sampled:02/07/2013 0935 Date Received:02/07/2013 Laboratory ID: OB07109-002 Matrix: Aqueous Run Prep Method 1 5030B Analytical Method Dilution Analysis Date Analyst Prep Date 624 1 02/11 /2013 2251 JAC Batch 13826 Parameter Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane (Methyl bromide) Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane (Methyl chloride) Dibromochloromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Vinyl chloride CAS Analytical Number Method Result Q PQL Units Run 107-02-8 624 ND 50 ug/L 1 107-13-1 624 ND 50 ug/L 1 71-43-2 624 ND 5.0 ug/L 1 75-27-4 624 ND 5.0 ug/L 1 75-25-2 624 ND 5.0 ug/L 1 74-83-9 624 ND 5.0 ug/L 1 56-23-5 624 ND 5.0 ug/L 1 108-90-7 624 ND 5.0 ug/L 1 75-00-3 624 ND 5.0 ug/L 1 110-75-8 624 ND 10 ug/L 1 67-66-3 624 ND 5.0 ug/L 1 74-87-3 624 ND 5.0 ug/L 1 124-48-1 624 ND 5.0 ug/L 1 75-34-3 624 ND 5.0 ug/L 1 107-06-2 624 ND 5.0 ug/L 1 75-35-4 624 ND 5.0 ug/L 1 156-60-5 624 ND 5.0 ug/L 1 78-87-5 624 ND 5.0 ug/L 1 10061-01-5 624 ND 5.0 ug/L 1 10061-02-6 624 ND 5.0 ug/L 1 100-41-4 624 ND 5.0 ug/L 1 75-09-2 624 ND 5.0 ug/L 1 79-34-5 624 ND 5.0 ug/L 1 127-18-4 624 ND 5.0 ug/L 1 108-88-3 624 ND 5.0 ug/L 1 71-55-6 624 ND 5.0 ug/L 1 79-00-5 624 ND 5.0 ug/L 1 79-01-6 624 ND 5.0 ug/L 1 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 102 52-138 Bromofluorobenzene 96 70-147 Toluene-d8 92 76-125 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 2 or SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Sandra Edwards Project Name: NPDES 2A Renewal Lot Number:KE21057 Date Completed:06/02/2009 itisbie- akin R. Brooke Montgomery Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report Chain of Custody Record and Sample Receipt Checklist. • • • • • • • • • Shealy Environmental Services, Inc. Page: 1 of 9 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Levert Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DEHNR No: 329 Case Narrative City of Belmont Lot Number: KE21057 This Report of Analysis contains the analytical results) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. Page: 2 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number: KE21057 Sample Number Sample ID Matrix Date Sampled Date Received 001 Pipe 001 Eff Aqueous 05/21/20091130 05/21/2009 002 Pipe 001 Eff Aqueous 05/21/2009 1200 05/21/2009 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Belmont Lot Number: KE21057 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 Pipe 001 Eff Aqueous Ammonia - N (phenate) 350.1 0.33 mg/L 5 001 Pipe 001 Eff Aqueous BOD, 5 day SM 5210B 4.8 mg/L 5 001 Pipe 001 Eff Aqueous Hardness (total) SM 2340C 68 mg/L 5 001 Pipe 001 Eff Aqueous Nitrate -Nitrite - N 353.2 20 mg/L 5 001 Pipe 001 Eff Aqueous Phosphorus 365.1 3.4 mg/L 5 001 Pipe 001 Eff Aqueous TDS SM 2540C 630 mg/L 5 001 Pipe 001 Eff Aqueous TKN 351.2 0.98 mg/L 5 001 Pipe 001 Eff Aqueous TSS SM 2540D 9.5 mg/L 5 001 Pipe 001 Eff Aqueous Antimony 200.8 5.8 ug/L 7 001 Pipe 001 Eff Aqueous Cadmium 200.8 0.13 ug/L 7 001 Pipe 001 Eff Aqueous Copper 200.8 16 ug/L 7 001 Pipe 001 Eff Aqueous Zinc 200.8 140 ug/L 7 001 Pipe 001 Eff Aqueous Mercury 245.1 0.0088 mg/L 7 002 Pipe 001 Eff Aqueous Phenolics 420.4 0.015 mg/L 8 002 Pipe 001 Eff Aqueous Fecal Coliform-MF SM 9222D 64 col/100 8 002 Pipe 001 Eff Aqueous Bromodichloromethane 8260B 2.4 uglL 8 002 Pipe 001 Eff Aqueous Chloroform 8260E 3.4 ug/L 8 (17 detections) Shealy Environmental Services, Inc. Page: 4 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Ciient:City of Belmont Description: Pipe 001 Eff Date Sampled:05/21/2009 1130 Date Received:05/21/2009 Laboratory ID: KE21057-001 Matrix: Aqueous Inorganic non-metals Run Prep Method 1 SM4500-NH3 1 1 1 1 1 1 351.4 Analytical Method (Ammonia - N ) 350.1 (BOD, 5 day) SM 5210B (Hardness (to) SM (Nitrate-Nitr) 353.2 (Phosphorus) 365.1 (TDS) SM 2540C (TKN) 351.2 (TSS) SM 2540D Dilution 1 1 1 10 10 1 1 1 Analysis Date 05/29/2009 2223 05/27/2009 0936 05/27/2009 2134 06/01/20091911 06/02/20091317 05/28/2009 0925 05/29/20091121 05/25/20091005 Analyst MML SAM SLH WD MML HBB MML HBB Prep Date Batch 05/29/20091450 11532 05/22/2009 0826 5031 11436 11661 05/27/2009 1916 11412 11447 05/28/2009 1100 11446 11219 Parameter Ammonia - N (phonate) BOD, 5 day Hardness (total) Nitrate -Nitrite - N Phosphorus TDS TKN TSS Run 1 Prep Method 3520C CAS Number 7723-14-0 Analytical Method 350.1 SM 5210B SM 2340C 353.2 365.1 SM 2540C 351.2 SM 2540D Result Q 0.33 4.8 68 20 3A 630 0.98 9.5 PQL 0.10 2.0 10 0.20 0.10 10 0.50 5.0 Semivolatile Organic Compounds by GC/MS Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8270C 1 05/29/20091656 DC 05/26/20091430 11321 Units Run mglL 1 mglL 1 mglL 1 mglL 1 mg/L 1 mglL 1 mglL 1 mglL 1 Parameter Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perytene Benzo(k)fluoranthene 4-Bromophenyl phenyl ether Butyl benzyl phthalate 4-Chloro-3-methyl phenol ., bis(2-Chloroethoxy)methane bis(2-Chloroethyl)ether bls(2-Chioroisopropyl)ether 2 roronaphthalene 4-Chiorophenyl phenyl ether CAS Number 83-32-9 208-96-8 120-12-7 92-87-5 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 101-55-3 85-68-7 59-50-7 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 Analytical Method 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C Result Q ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND PQL 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Units Run ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 POL = Practical quantitation limit B = Detected In the method blank ND - Not detected at or above the POL J = Estimated result < PQL and > MDL Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "V E = Quantitation of compound exceeded the aeration range P = The RPD between two GC columns exceeds 4096 N = Recovery is out of criteria H - Out of holding time Shealy Environmental Services, Inc. 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page: 5 of 9 Level 1 Report v2.1 C ient:City of Belmont Uescnption: Pipe 001 Eff Date Sampled:05/21/20091130 Date Received:05/21/2009 Laboratory ID: KE21057-001 Matrix: Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3520C 8270C 1 05/29/20091656 DC 05/26/20091430 11321 Parameter Chrysene Dian -butyl phthalate Di-n-octylphthalate Dibenzo(a,h)anthracene 3.3'-Dichtorobenzidine CAS Analytical Number Method Result Q PQL Units Run 218-01-9 8270C ND 1.0 ug/L 1 84-74-2 8270C ND 5.0 ug/L 1 117-84-0 8270C ND 5.0 ug/L 1 53-70-3 8270C ND 1.0 ug/L 1 91-94-1 8270C ND 5.0 ug/L 1 120-83-2 8270C ND 1.0 ug/L 1 Dieth rpnmaIa e 84-66-2 8270C ND 5.0 ug/L 1 Dimetbyln thalatR 131-11-3 8270C ND 5.0 ug/L 1 2,4-Di_rylohenol 105-67-9 8270C ND 1.0 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 8270C ND 5.0 ug/L 1 no - 51-28-5 8270C ND 5.0 ug/L 1 2,4-Dinitrotoluene 121-14-2 8270C ND 2.0 uglL 1 2,6-Dinitrotoluene 606-20-2 8270C ND 2.0 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 8270C ND 1.0 uglL 1 bis(2-Ethylhexyl)phthalate 117-81-7 8270C ND 5.0 uglL 1 Fluoranthene 206-44-0 8270C ND 1.0 ug/L 1 Fluorene 86-73-7 8270C ND 1.0 ug/L 1 Hexachlorobenzene 118-74-1 8270C ND 1.0 ug/L 1 Hexachlorobutadiene 87-68-3 8270C ND 1.0 ug/L 1 Hexachlorocyctopentadiene 77-47-4 8270C ND 5.0 ug/L 1 Hexachloroethane 67-72-1 8270C ND 1.0 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 8270C ND 1.0 ug/L 1 Isophorone 78-59-1 8270C ND 1.0 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 8270C ND 1.0 ug/L 1 N-Nitrosodimethylamine 62-75-9 8270C ND 1.0 ug/L 1 N-Nitrosodlphenylamine (Diphenylamtne) 86-30-6 8270C ND 1.0 ug/L 1 Naphthalene 91-20-3 8270C ND 1.0 uglL 1 Nitrobenzene 98-95-3 8270C ND 1.0 ugiL 1 2-Nitrophenol 88-75-5 8270C ND 2.0 ug/L 1 4-Nitrophenol 100-02-7 8270C ND 5.0 ug/L 1 Pentachlorophenol 87-86-5 8270C ND 5.0 ug/L 1 Phenanthrene 85-01-8 8270C ND 1.0 ug/L 1 Phenol 108-95-2 8270C ND 1.0 ug/L 1 fence 129-00-0 8270C ND 1.0 ug/L 1 2,4,6-Trichlorophenol 88-06-2 8270C ND 1.0 ug/L 1 PQL = Practical quentitatlon limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 4096 Where applicable, all son sample analysis are reported on a dry weight basis unless flagged with a NV N = Recovery is out of criteria H = Out of holding time Shealy Environmental Semces, Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 C[ient:City of Belmont Description: Pipe 001 Eff Date Sampled:05/21/20091130 Date Received:06/21/2009 Laboratory ID: KE21057-001 Matrix: Aqueous Surrogate Run 1 Acceptance Q % Recovery Limits 2,4,6-Tribromo_ohenol 2-Ffuorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 78 41-144 41 37-129 43 24-127 43 38-127 48 28-128 68 10-148 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 05/28/2009 0009 FTS 05/25/2009 2030 11270 2 200.2 200.8 10 08/02/2009 0228 KJC 05/25/2009 2030 11270 CAS Analytical Parameter Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 5.8 1.0 uglL 1 Arsenic 7440-38-2 200.8 ND 1.0 ug/L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1 Cadmium 7440-43-9 200.8 0.13 0.10 uglL 1 Chromium 7440-47-3 200.8 ND 5.0 ug/L 1 Copper 7440-50-8 200.8 16 1.0 uglL 1 Lead 7439-92-1 200.8 ND 10 ug/L 2 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 ND 1.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-66-6 200.8 140 10 uglL 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 245.1 1 05282009 0058 BNW 0527/20091700 11394 CAS Analytical Parameter Number Method Result Q PQL Units Run Mercury 7439-97-6 245.1 0.0088 0.0080 mglL 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitatlon of compound exceeded the calibration range ND = Not detected at or above the PQL J = Estimated result < PQL and = MDL P = The RPD between two GC columns exceeds 40% Where applicable, all sot sample analysis are reported on a dry weight basis unless Bagged with a "W' N = Recovery is out of criteria H = Out of holding time Shealy Environmental Services, inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client:City of Belmont Description: Pipe 001 Eff Date Sampled:05/21/2009 1200 Date Received:05/21/2009 Laboratory ID: KE21057-002 Matrix: Aqueous Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Dissolved Ox) SM 1 05/21/2009 1200 SFM 1 (Flow) Flow 1 05/21/2009 1200 SFM 1 (pH - Field) SM 4500-H 1 05/21/2009 1200 SFM 1 (Temperature ) SM 1 05/21/2009 1200 SFM 1 (TRC - Field) SM 4500- 1 05/21/2009 1200 SFM 1 (Cyanide) SM 4500-CN 1 05/27/2009 0939 WD 05/26/2009 1130 11294 1 (Phenolics) 420.4 1 05/29/2009 1305 WD 05/27/2009 0900 11385 1 (Fecal Colifo) SM 1 05/22/2009 1717 WD 05/21/2009 1633 1 (HEM (oil and) 1664A 1 05/22/2009 0931 JBK 11158 CAS Analytical Parameter Number Method Result Q PQL Units Run Dissolved Oxygen - Field SM 4500-0 G 8.56 2.00 mg/L 1 Flow Flow 1343800 gal/day 1 pH - Field SM 4500-H B Field 7.42 su 1 Temperature - Field SM 2550B 20.0 ° C 1 TRC - Field SM 4500-CL G ND 0.10 mg/L 1 Cyanide 57-12-5 SM 4500-CN E ND 0.010 mg/L 1 Phenolics 420.4 0.015 0.0050 mg/L 1 Fecal Coliform-MF SM 9222D 64 2 col/100mL 1 HEM (oil and grease) 1664A ND 4.8 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 82608 1 05/26/2009 0432 DLB 11282 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 8260B ND 5.0 ug/L 1 Acrylonitrile 107-13-1 8260B ND 5.0 ug/L 1 Benzene 71-43-2 8260B ND 1.0 ug/L 1 Bromodichloromethane 75-27-4 8260E 2.4 1.0 ug/L 1 Bromoform 75-25-2 8260B ND 1.0 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260B ND 2.0 ug/L 1 Carbon tetrachloride 56-23-5 8260B ND 1.0 ug/L 1 Chlorobenzene 108-90-7 8260E ND 1.0 ug/L 1 Chloroethane 75-00-3 8260B ND 2.0 ug/L 1 2-Chloroethylvinylether 110-75-8 82608 ND 5.0 ug/L 1 Chloroform 67-66-3 82608 3.4 1.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260B ND 2.0 ug/L 1 Dibromochloromethane 124-48-1 8260E ND 1.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260E ND 1.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260E ND 1.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260E ND 1.0 ug/L 1 PQL = Practical quantitatton limit 8 = Detected in the method blank ND = Not detected al or above the PQL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' E = Quantitation of compound exceeded the calibration range P = The RPO between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time Shealy Environmental Services, Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client:City of Belmont Description: Pipe 001 Eff Date Sampled:05/21/20091200 Date Received:05/2112009 Laboratory ID: KE21057-002 Matrix: Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260E 1 05/26/2009 0432 DLB 11282 Parameter 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2 Tetrachloroethane Tetrachloroethene Toluene 1,2,4-Tr ichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trlchloroethene Vinyl chloride CAS Analytical Number Methgtl Result Q PQL Units Run 75-34-3 8260B ND 1.0 ug/L 1 107-06-2 8260B ND 1.0 ug/L 1 75-35-4 8260B ND 1.0 ug/L 1 156-60-5 8260E ND 1.0 ug/L 1 78-87-5 8260B ND 1.0 ug/L 1 10061-01-5 8260B ND 1.0 ug/L 1 10061-02-6 8260B ND 1.0 ug/L 1 100-41-4 8260E ND 1.0 ug/L 1 75-09-2 8260B ND 1.0 ug/L 1 79-34-5 82608 ND 1.0 ug/L 1 127-18-4 8260E ND 1.0 ug/L 1 108-88-3 8260B ND 1.0 ug/L 1 120-82-1 8260E ND 1.0 ug/L 1 71-55-6 8260E ND 1.0 ug/L 1 79-00-5 8260B ND 1.0 ug/L 1 79-01-6 8260B ND 1.0 ug/L 1 75-01-4 8260E ND 2.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 81 70-130 Bromottuorobenzene 81 70-130 Toluene-d8 85 70-130 PQL = Practical quantitation limit B = Detected In the method blank E _ Quantitation of compound exceeded the calibration range ND = Not detected at or above the PQL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery Is out of criteria H = Out of holding time Shealy Environmental Services. Inc. Page: 9 of 9 106 Vantage Pant Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 CWA / NPDES SHEALY Chain of Custody Record Cue,it CAN n � ` • SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive • Wct Columbia, SC 291/2 Tela:shone No. (8031 7 91.9700 Fax No. (803) 791-9111 www.sPieelylab.com Aop:wt i (a7n'.3cf ` , 1'ro,'Ac1,`.ii tiaok, I ,'r, Code ill •5 J,j�:ItUr2 _ �•jtl P,.rur••! Mrrv:. S3tr;ie i:.' Oes:r,:ban fi n iags•3. i fd:i 2.70 , :81'te COT ILVX, 0'1 Cre Ce:t I 17719 • fro:h Start Hnjh Fr•rah ,)4t •\\.1r d 'ova 1.4 roa 0,1 4 Ttn .t iK Number 17532 16(@xtow f.'.7, ' r3! N * ' c-n..J It t:ii '1tiG. Ovals. 1'10 '_aye C'9 Anatysis (A 1ftic1 Ns( it m:.r. s�xa ,F ;a,.daA F'aA F6.11710161 (1.e , (Oa .rvrT: , .':.i, ri' he ►eocrCN c?:ocs r9,es4 .4e,„ Los 'Or 2- I� s� q:m•r:ukr:. • ^(IIC, r.7. T.uv Ant nur Tine .4fnv.irni jP.*.r t,4 •u.etu'•+ •:-.;'w, r: J.•,: eta. .j ij TAT) Prr • j ti',.n 11•;1 �� •e 1 Ut ir:i ri.ircr/L. •1 `' Z ° ..n,,nsr*s i �f wSi11%1OICP31J G: .1 1.4., n.1,rcr4,1 t•.y X •� Ir r• SRnrr,A C..9t1C-511 OC rteptdferl,r1(s (5,.lec'y) (_� Nl;f�.',- •D i�':Y.0 thcmszi :'i Lai ram: Po x•cr:ad ht• xX r os. uc i irlr d 11.1:nhn.csnc.1 t(J per-Ila:ard I_'nr 3CIe = Skh It Ilan! O F.: ;on 1 Urkr :.•rnV L1.,!to Trr:,:: i 4a,:cvtic.' for .1::'ic,s.'::y Pao. i 11nA rkne, �,(c Tirna Note. Ail samples are rammed for six weeks frcrn receipt unless other arrangements are made OwSTAHaul)on: WH,TL S •/ELiCt'.'-flctr.'01046 .*ahoy n.f/ Sarwt.'disl. r'JNK-FstAV, „r'.'Cuuy Lite uSE ONLY A'a Ice r^aN I Pt err TA'rp_ `____ ... 1 'rrrK• 15 M Do,:.rvr :1 Nur,iL a i• .A_') s)?LX .,..1 cn 1 m m z 0 Z rn z r co m 0 rn r SHEALY ENVIRONMENTAL SERVICES, INC. 1).:•;un:nt Nun-')cr F-A121-1..1t. Nurr xr•.. Rrrlair.5 Daic: Lf7rc...:tv: Date: Sample Receipt Checklist (SR() civil:: AA. ')'""g‘ el4 Cooler 11:4.1ec:ed byidate. f-jil .f) 1?-1 fe 1 Lot ° IMcalli tti 7".:t......::pt.: SESI • Client LJ UPS TT FedEx 0 Airborne Ex: E Other No -NA 0 ; 1 Were custody seals present en the cooler? Ye1-71.._ No it. NA F1'i 2. If com-or- seals were prescn:. wcrr thc-, intact an. unhrc!ken" Cooler ID.':ernperature •,ipon receipt 1- ±_,..- `C N-lethotf.: 7-emperatu.rc Method of coelant: Blank .• Against &Ages ja-NVet lee E Blue lee D Dry lee 0 None ; :7-response is No 1.07 - Ycs for 14. 15. 16i. an nationiresoAltier. MUM be PrOVidtd. 1 Ye5 . LI \ A Er .1%. If tempt:ratan: of any :..:ole:- exceeded 6.0'C. was Projet.1 Mart:ger notified'? PN-1 notified by SRC. phone. note (circle :Art :. other . . 1,'F...ir co, ler-s- re...cel\-eil via ciiintnrcai zc-roier. PM.; are to he ii.otif7ed ittiliediAlt:!, . Ye Lil NioEi NA •:-. IS the commercial courier's packing. slip anazhed to this form? Yec I No NA :) We- c rproper crmody TrocedureA ;:-clinquishedireeevce..) followed? Ye7, 2 N.' \A 6 We-e sample 1Ds listed? '125 a No D INA ' Was collection date & time listed' Yes No NA D . Were tests le be perforrnze listed on the ('.:_).:.: or wr.s :ruck: •orcyided? ).: Y:...---,7-4 YeD I-- Nlo El N,'.., ! No JD NA • .\ A f1 7 '. I )id all sa:nnles arr've in the prriper z.ontainers 7or each test'' 10. Did all eontLiner label :rifor ;nal ion (11). da:e. time' at -tree with CO.. NA D 1 1. Did all containers arr7ve in t.'od condition 1 unbroken. lids on. et:.). Pi N.., 17 \ A I -I .. - I 2. \Va.': :;deritsatesarrinle volirrne available'? . .._ Y es D No NA 13. Wcre all samples :e.:•ei% et: within :.•': the holding :rine cl- 4S haus. •.-%liielicx er conies first? . • cs No 2' NA 1 14. Wzrc an' sz:.7n_plzs eontainers rrissiic? 'es IJ No •NA -1 15. \V:rc there any excess san-.71cs not listed on COC? Noak N.r., 1 .- - 11. Were bAbbles present >-pea-size- i',',.for 6mri ir ciieteri ir any '‘, t.)A l vrals? \ cs -4-''Ni:..) 0 I NA ; 17. Were all nietal0)&.G;HEN-1/nutrient .artipl,'...s reee%.t.:: al ii pi-1 oC<2.' Ycs i,2( No 0 NA 18. Wcre all cyanid: ardicr sultithc samples received at a p1-1 >12. : Yes j„..---No 0 --, I 19. Were all applicable NR3.7kNicyanide.:pher.o.2.1.3NA;pest;K:Blierb NA _f (.-f-C2.211-1.2..11_J an. tk-ly.ictv (*•::(1. l mei.) samples free :if rcsidez...1 ch:orine? '1 cs .J No D N.A„23" 20. Were eoLec:ion temperatures dozwrented on the COC for NC samples? Sample Preservation rNtrist *De completed for any sarne,le(s i incon-t-ci: ereser.'ed :_)r with headspace.) Sample( .0 receive:1 ineorree:iy preserved and were adjustee 11-.vordiril) in sample recer..irg v.. tit (1-1,SO4J-1N0,1-1CI.Nt..01 ri with the SR r.' (number! Sainplet Sample; si were reeeivezi with bubbles :net. in diameter. we received with TRC >0.2 m.Lfi:r NIL. Alpe,t:PC1ilierb (oNien) stmiplett.) Yr-ere teeer‘ed itil 1 K(>0_ 1 m2/1_ and yen.: I anal‘.7ecl method Corrective Action taken, II necessary: Was client no:ifie: 1 es N E SLSI employee: Cerninerits:_ Die: client respond- Y- E Ni..El L>ate. of response: Shealy Environmental Services, Inc. 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 ,446 - 2ai ? SHEALY ENVIRONMENTAL SERVICES, INC. . !Yr. ft.L Y TCS Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Sandra Edwards Project Name:NPDES 2A Renewal Lot Number:KH20039 Date Completed:09/02/2009 Sabrina E Boles Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DEHNR No: 329 Case Narrative City of Belmont Lot Number: KH20039 This Report of Analysis contains the analytical resutt(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. Page: 2 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number: KH20039 Sample Number Sample ID Matrix Date Sampled Date Received 001 Pipe 001 Aqueous 08/20/20091105 08/20/2009 002 Pipe 001 Aqueous 08/20/20091110 08/20/2009 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 Level 1 Report 4.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Belmont Lot Number: KH2O039 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 Pipe 001 Aqueous Ammonia - N (phenate) 350.1 0.30 mg/L 5 001 Pipe 001 Aqueous Hardness (total) SM 2340C 55 mg/L 5 001 Pipe 001 Aqueous Nitrate -Nitrite - N 353.2 21 mg/L 5 001 Pipe 001 Aqueous Phosphorus 365.1 4.4 mg/L 5 001 Pipe 001 Aqueous TDS SM 2540C 590 mg/L 5 001 Pipe 001 Aqueous TSS SM 2540D 4.0 B mg/L 5 001 Pipe 001 Aqueous Antimony 200.8 5.6 ug/L 7 001 Pipe 001 Aqueous Copper 200.8 16 ug/L 7 001 Pipe 001 Aqueous Zinc 200.8 110 ug/L 7 002 Pipe 001 Aqueous Phenolics 420.4 0.0064 mglL 8 002 Pipe 001 Aqueous Bromodichloromethane 8260E 3.6 ug/L 8 002 Pipe 001 Aqueous Chloroform 8260E 6.2 ug/L 8 (12 detections) Shealy Environmental Services, Inc. Page:4 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client:City of Belmont Description: Pipe 001 Date Sampled:08/20/2009 1105 Date Received:08120/2009 Laboratory ID: KH20039-001 Matrix: Aqueous Run Prep Method 1 SM4500-NH3 1 1 1 1 1 1 351.4 1 Analytical Method (Ammonia - N ) 350.1 (BOD, 5 day) SM 5210B (Hardness (to) SM (Nitrate-Nitr) 353.2 (Phosphorus) 365.1 (TDS) SM 2540C (TKN) 351.2 (TSS) SM 2540D Inorganic non-metals Dilution 1 Analysis Date 09/01/2009 2250 1 08/26/2009 1510 1 08/28/2009 1859 20 09/01/20091830 10 08/31/20091027 1 08/27/2009 0841 1 09/02/2009 1221 1 08/27/2009 0839 Analyst WD HBB MML BM DAS SLH WD SLH Prep Date Batch 09/01/2009 0910 17108 08/21/20091255 5180 17052 17176 08/28/2009 1400 16959 16828 09/01/2009 1018 17117 16827 Parameter Ammonia - N (phenate) BOD, 5 day Hardness (total) Nitrate -Nitrite - N Phosphorus TDS TKN TSS CAS Number 7723-14-0 Analytical Method 350.1 SM 5210B SM 2340C 363.2 365.1 SM 2540C 351.2 SM 2540D Result Q 0.30 ND 55 21 4.4 590 ND 4.0 B Semivolatile Organic Compounds by GC/MS PQL 0.10 2.0 10 0.40 0.10 10 0.50 2.0 Units Run mg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L 1 Run Prep Method Analytical Method 1 3520C 8270C 1 08/27/2009 1230 DC 08/24/2009 2005 16631 Dilution Analysis Date Analyst Prep Date Batch Parameter CAS Analytical Number Method Result Q PQL Units Run Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene 4-Bromophenyl phenyl ether Butyl benzyl phthalate 4-Chlore-3-methql-phertar bis(2-Chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-C h loroisopropyl)ether 2-Chloronaphthalene Chloropheno 4-Chlorophenyl phenyl ether 83-32-9 208-96-8 120-12-7 92-87-5 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 101-55-3 85-68-7 59-50-7 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0 1.0 1.0 5.1 1.0 1.0 1.0 1.0 1.0 1.0 5.1 1.0 1.0 1.0 1.0 1.0 1.0 1.0 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time Shealy Environmental Services, Inc. Page: 5 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Belmont Description: Pipe 001 Date Sampled:08/20/2009 1105 Date Received:08/20/2009 Laboratory ID: KH20039-001 Matrix: Aqueous Run Prep Method 1 3520C Semivolatile Organic Compounds by GC/MS Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8270C 1 08/27/20091230 DC 08/24/2009 2005 16631 Parameter Chrysene Di-n-butyl phthalate Di-n-octylphthalate Dibenzo(a,h)anthracene 3,3'-Dichlorobenzidine Dietphthalate Dimthyi phthalate 4,6-Dinitro-2-methylphenol . 2,4-Dinitrotofuene 2,6-Dinitrotoluene 1,2-Diphenylhydrazine(as azobenzene) bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane tndeno(1,2,3-c,d)pyrene Isophorone N-Nitrosodi-n-propylamine N-Nttrosodimethylamine N-Nitrosodlphenylamine (Diphenylamine) Naphthalene Nitrobenzene ophenel--. �entachlorophenol Phenanthrene Phenol Pyrene richlorophenol CAS Number 218-01-9 84-74-2 117-84-0 53-70-3 91-94-1 120-83-2 84-66-2 131-11-3 105-67-9 534-52-1 51-28-5 121-14-2 606-20-2 103-33-3 117-81-7 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 621-64-7 62-75-9 86-30-6 91-20-3 98-95-3 88-75-5 100-02-7 87-8(i-5 85-01-8 108-95-2 129-00-0 88-06-2 Analytical Method 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C Result Q PQL Units Run ND 1.0 ug/L 1 ND 5.1 ug/L 1 ND 5.1 ug/L 1 ND 1.0 ug/L 1 ND 5.1 ug/L 1 ND 1.0 ug/L 1 ND 5.1 ug/L 1 ND 5.1 ug/L 1 ND 1.0 ug/L 1 ND 5.1 ug/L 1 ND 5.1 ug/L 1 ND 2.0 ug/L 1 ND 2.0 ug/L 1 ND 1.0 ug/L 1 ND 5.1 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 5.1 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 ND 2.0 ug/L 1 ND 5.1 ug/L 1 ND 5.1 ug/L 1 ND 1.0 ug/L 1 ND 1.0 uga. 1 ND 1.0 ug/L 1 ND 1.0 ug/L 1 PQL = Practical quantitation emit B = Detected in the method blank NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless Ragged with a "W" E Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria H = Out of hotding time Shealy Environmental Services, Inc. 106 Vantage Polnt Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vwrw.shealytab.com Page: 6 of 9 Level 1 Report v2.1 Client:City of Belmont Description: Pipe 001 Date Sampled:08120/2009 1105 Date Received:08/20/2009 Laboratory ID: KH20039-001 Matrix: Aqueous Surrogate Run 1 Acceptance Q % Recovery Limits 2,4,6-Tribromophenol 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 59 41-144 45 37-129 43 24-127 45 38-127 43 28-128 64 10-148 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 08/26/2009 2201 FTS 08/24/2009 1720 16616 CAS Analytical Parameter Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 5.6 1.0 ug/L 1 Arsenic 7440-38-2 200.8 ND 1.0 ug/L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1 Cadmium 7440-43-9 200.8 ND 0.10 ug/L 1 Chromium 7440-47-3 200.8 ND 5.0 ug/L 1 Copper 7440-50-8 200.8 16 1.0 uglL 1 Lead 7439-92-1 200.6 ND 1.0 ug/L 1 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 ND 1.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-66-6 200.8 110 10 ug/L 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 245.1 1 08/24/2009 2116 BNW 08/24/2009 1645 16607 CAS Analytical Parameter Number Method Result Q PQL Units Run Mercury 7439-97-6 245.1 ND 0.00010 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the POL J = Estimated result < PQL and > MDL Where applicable, al soil sample analysis are reported on a dry weight basis unless flagged with a -W' E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time Shealy Environmental Services, Inc. Page: 7 of 9 106 vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client:City of Belmont Description: Pipe 001 Date Sampled:08/20/2009 1110 Date Received:08/20/2009 Laboratory ID: KH20039-002 Matrix: Aqueous Run Prep Method 1 1 1 1 1 1 1 1 1 Analytical Method (Dissolved Ox) SM (Flow) Flow (pH - Field) SM 4500-H (Temperature ) SM (TRC - Field) SM 4500- (Cyanide) SM 4500-CN (Phenolics) 420.4 (Fecal Colifo) SM (HEM (oil and) 1664A Inorganic non-metals Dilution 1 1 1 1 1 1 1 1 1 Analysis Date 08/20/2009 1110 08/20/2009 1110 08/20/2009 1110 08/20/2009 1110 08/31/2009 1747 09/01/2009 1501 08/21/2009 1550 08/27/2009 1633 Analyst GMC GMC GMC GMC BM BM SLH JKP Prep Date Batch 08/31/2009 1400 17070 08/28/2009 1621 16987 08/20/2009 1626 16877 Parameter Dissolved Oxygen - Field Flow pH - Field Temperature - Field TRC - Field Cyanide Phenolics Fecal Coliform-MF HEM (oil and grease) CAS Analytical Number Method SM 4500-0 G Flow SM 4500-H B Field SM 2550B SM 4500-CL G 57-12-5 SM 4500-CN E 420.4 SM 9222D 1664A Result Q PQL Units Run 7.41 1429000 7.38 28.0 ND ND 0.0064 ND ND Volatile Organic Compounds by GC/MS 2.00 mg/L 1 0.000 gaUday 1 0.000 su 1 0.000 ° C 1 0.10 mg/L 1 0.010 mg/L 1 0.0050 mglL 1 2 col/100mL 1 4.1 mg/L 1 Run 1 Prep Method 5030E Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8260E 1 08/24/20091601 DLB 16649 Parameter Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane (Methyl bromide) Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane (Methyl chloride) Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene CAS Number 107-02-8 107-13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 Analytical Method 8260B 8260B 8260E 8260E 8260E 8260B 8260E 8260E 8260E 8260E 8260B 8260E 8260E 8260B 8260B 8260B Result ND ND ND 3.6 ND ND ND ND ND ND 6.2 ND ND ND ND ND Q PQL Units Run 5.0 ug/L 1 5.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 2.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 2.0 ug/L 1 5.0 ug/L 1 1.0 ug/L 1 2.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 POL = Practical quantitation Ilmd ND = Not detected at or above the POL B = Detected in the method blank J = Estimated result < POL and > MIX Where applicable, at soil sample analysis are reported on a dry weight basis unless flagged with a "W E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time Shealy Environmental Services, Inc. Page: 8 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client:City of Belmont 'Description: Pipe 001 Date Sampled:08/20/20091110 Date Received:08/2012009 Laboratory ID: KH20039-002 Matrix: Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 08/24/20091601 DLB 16649 Parameter 1,1-Dichloroethane 12-Dichloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichtoropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2 Trichloroethane Trichloroethene Vinyl chloride CAS Analytical Number Method Result Q PQL Units Run 75-34-3 8260B ND 1.0 ug/L 1 107-06-2 8260B ND 1.0 uglL 1 75-35-4 8260B ND 1.0 ug/L 1 156-60-5 8260E ND 1.0 uglL 1 78-87-5 8260B ND 1.0 ug/L 1 10061-01-5 8260B ND 1.0 ug/L 1 10061-02-6 8260E ND 1.0 ug/L 1 100-41-4 8260B ND 1.0 ug/L 1 75-09-2 8260B ND 1.0 uglL 1 79-34-0 8260B ND 1.0 uglL 1 127-18-4 8260B ND 1.0 ug/L 1 108-88-3 8260B ND 1.0 uglL 1 120-82-1 8260E ND 1.0 ug/L 1 71-55-6 8260B ND 1.0 ug/L 1 79-00-5 8260E ND 1.0 uglL 1 79-01-6 8260E ND 1.0 ug/L 1 75-01-4 8260B ND 2.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichtoroethane-d4 87 70-130 Bromofluorobenzene 90 70-130 Toluene-d8 88 70-130 PQL = Practical quantltation limit 8 = Detected In the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% Where applicable, all soli sample analysis are reported on a dry weight basis unless Ragged with a'W N = Recovery Is out of criteria H = Out of holding time Shealy Environmental Services, Inc. Page: 9 of 9 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.00m Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. O CO z 8 2 -17 X k .77 • A • S 7. CT r 3-/S7`?ry4A rt,1G0 1 ri cc 7 Aro. ma1..- u�rtc 3 cS _ L. L 0 !h:c u7Kolt NivrL r F-A 1-031 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com Level 1 Report v2•1 SHEALY ENVIRONMENTAL SERVICES, INC. =n'.'ir;nn:ri7! `•CT.'ic . Inc r:licnt:_ trYt of Pa c ' ,t Rcni.'rs Dal: fl: Sample Receipt ('llt cklls. (S1 C, . Cooler ir:spaneci b,•' :�'te ����� .16 Poi, i:.t 4 k-i 2oo3' 'vi_.ins D1 --_ :p: SESi f ' (-jell': E 1 PS I 1•ecil=.x ❑ Airh:vrr:c Exp 111 Jt'ncr i 1 '- T \., i I 11. Were cusi'cr. >:-fti1 present on the cuuler" L. N _' I s r ec wen.- br:nker':' ;'; �• - _J ��f ra�u>u; et:.� ;;.r::~r cn:. r they :m�;.' ;-,,tic: un. 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C ,rrectiN a -iciicin Taken. if reccNiar' : Was c:lent aatitieli: :� NI_' irnr,•11c112; L'.d ci'cn' r•_a��nJ 1 e _ tie J Daly : f res vns : Shealy Environmental Services, Inc. 106 Vantage Pant Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 F 2OdT SHEALY ENVIRONMENTAL SERVICES, INC. (maQ ,z1,e Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Sandra Edwards Project Name: NPDES 2A Renewal Lot Number.KB19033 Date Completed:03/09/2009 &t5a-e_ dAkAisir R. Brooke Montgomery Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report Chain of Custody Record and Sample Receipt Checklist. • • • • • • • • • Shealy Environmental Services, Inc. Page: 1 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DEHNR No: 329 Case Narrative City of Belmont Lot Number: KB19033 This Report of Analysis contains the analytical result(s) for the samples) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Semivolatile Organic Analysis Sample -001 had two surrogates recovered outside of the acceptance limits due to confirmed matrix interference for the analysis of semivolatile organic compounds. Shealy Environmental Services, Inc. Page: 2 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number KB19033 Sample Number Sample ID Matrix Date Sampled Date Received 001 Pipe 001 Aqueous 02/19/20091030 02/19/2009 002 Pipe 001 Aqueous 02/19/20091055 02/19/2009 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Belmont Lot Number: KB19033 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 Pipe 001 Aqueous Ammonia - N (phenate) 350.1 0.54 mg/L 5 001 Pipe 001 Aqueous BOD, 5 day SM 5210B 16 mg/L 5 001 Pipe 001 Aqueous Hardness (total) SM 2340C 54 mg/L 5 001 Pipe 001 Aqueous Nitrate -Nitrite - N 353.2 20 mg/L 5 001 Pipe 001 Aqueous Phosphorus 365.1 20 mg/L 5 001 Pipe 001 Aqueous TDS SM 2540C 540 mg/L 5 001 Pipe 001 Aqueous TKN 351.2 3.1 mg/L 5 001 Pipe 001 Aqueous TSS SM 2540D 17 mg/L 5 001 Pipe 001 Aqueous Antimony 200.8 2.8 ug/L 7 001 Pipe 001 Aqueous Copper 200.8 17 ug/L 7 001 Pipe 001 Aqueous Zinc 200.8 240 ug/L 7 002 Pipe 001 Aqueous Phenolics 420.4 0.012 mg/L 8 002 Pipe 001 Aqueous Fecal Coliform-MF SM 9222D 55 co1/100mL 8 002 Pipe 001 Aqueous Bromodichloromethane 8260E 1.3 ug/L 8 (14 detections) Shealy Environmental Services, Inc. Page: 4 of 9 Level 1 Report v2.1 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com ClientCity of Belmont Description: Pipe 001 Date Sampled:02119/20091030 Date Received:02/19/2009 Laboratory ID: KB19033-001 Matrix: Aqueous Inorganic non-metals Run Prep Method 1 SM4500-NH3 1 1 1 1 1 351.4 1 Analytical Method (Ammonia - N ) 350.1 (BOD, 5 day) SM 5210B (Hardness (to) SM (Nitrate-Nitr) 353.2 (Phosphorus) 365.1 (TDS) SM 2540C (TKN) 351.2 (TSS) SM 2540D Dilution 1 1 1 10 50 1 1 1 Analysis Date 02/27/20091546 02/25/20091011 02/27/2009 1629 02/25/20091348 02/24/2009 2037 02/24/20091715 02/25/2009 1338 02/25/2009 0908 Analyst SLH MML MML RLM SLH WD SLH WD Prep Date Batch 02/25/20091254 95828 02/20/2009 0918 4879 96117 95852 02/23/20091248 95638 95779 02/24/20091800 95757 95799 Parameter Ammonia - N (phonate) BOD, 6 day Hardness (total) Nitrate -Nitrite - N Phosphorus TDS TKN TSS CAS Number 7723-14-0 Analytical Method Result 360.1 0.64 SM 6210B 16 SM 2340C 64 353.2 20 365.1 20 SM 2540C 540 361.2 3.1 SM 2640D 17 Semivolatile Organic Compounds by GC/MS PQL 0.10 2.0 10 0.20 0.50 10 0.60 1.0 Units Run mglL 1 mglL 1 mg1L 1 mglL 1 mglL 1 mg/L 1 mglL 1 mglL 1 Run Prep Method 1 3520C Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8270C 1 03/06/20091816 GLR 02/26/2009 2328 95980 Parameter Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene 4-Bromophenyl phenyl ether Butyl benzyl phthalate roro-3-methyl phen bi: . _ • methane bis(2-Chroroethyl)ether bis(2-Chloroisopropyl)ether 2- oronaphtharene 4-Chlorophenyl phenyl ether CAS Number 83-32-9 208-96-8 120-12-7 92-87-5 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 101-55-3 85-68-7 59-50-7 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 Analytical Method 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Q PQL Units Run 1.0 uglL 1 1.0 ug/L 1 1.0 ug/L 1 5.0 uglL 1 1.0 ug/L 1 1.0 uglL 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 5.0 uglL 1 1.0 ug/L 1 1.0 ug/L 1 1.0 uglL 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 PQL = Practical quantttatlon limit B = Detected In the method blank ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL Where applicable, ail soil sample analysis am reported on a dry weight basis unless flagged with a W E = Quentitation of compound exceeded the caitbratlon range P - The RPD between two GC columns exceeds 4096 N = Recovery is out of criteria Shealy Environmental Services, Inc. 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com Page: 6 of 9 Level 1 Report v2.1 Client: City of Belmont Description: Pipe 001 Date Sampled:02119/20091030 Date Received:02/19/2009 Laboratory ID: KB19033-001 Matrix: Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method 1 3520C Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8270C 1 03/06/20091816 GLR 02/26/2009 2328 95960 Parameter Chrysene Dian -butyl phthalate Di-n-octylphthalate Dibenzo(a,h)anthracene 3,3'-D azdine ,4-Dichlorophenol Diethy iithelate Di late 274-Dimethyiphenoll 4,6-Dinitro-2 methylphenol 2,4-Dinitrophenol l 2,4-Dinitrotoluene 2,6-Dinitrotoluene 1,2-Diphenyihydrazlne(as azobenzene) bis(2-Ethylhexyl)phthalate Fluoranthene Moreno Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadlene Hexachloroethane lndeno(1,2,3-c,d)pyrene Isophorone N-Nitrosodl-n-propylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine (Diphenylamine) Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,6-Trichlorophenol CAS Number 218-01-9 84-74-2 117-84-0 53-70-3 91-94-1 120-83-2 84-66-2 131-11-3 105-67-9 534-52-1 51-28-5 121-14-2 606-20-2 103-33-3 117-81-7 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 621-64-7 62-75-9 86-30-6 91-20-3 98-95-3 88-75-5 100-02-7 87-86-5 85-01-8 108-95-2 129-00-0 88-06-2 Analytical Mettjod 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C Result Q ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND PQL 1.0 5.0 5.0 1.0 5.0 1.0 5.0 5.0 1.0 5.0 5.0 2.0 2.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0 5.0 5.0 1.0 1.0 1.0 1.0 Units Run ug/L 1 uglL 1 uglL 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 uglL 1 ug/L 1 ug/L 1 uglL 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 uglL 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 uglL 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 ug/L 1 uglL 1 ug/L 1 ug/L 1 PQL = Practical quantltatloon limit B = Detected to the method blank ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with WIN' E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 4096 N = Recovery Is out of criteria Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page: 6 of 9 Level 1 Report v2.1 CiientCity of Belmont Description: Pipe 001 Date Sampled:02/19/2009 1030 Date Received:02/19/2009 Laboratory ID: KB19033-001 Matrix: Aqueous Surrogate Run 1 Acceptance Q % Recovery Limits 2,4,6-Tribromophenol 2-Ftuoroblphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 52 41-144 N 28 37-129 27 24-127 N 32 38-127 32 28-128 47 10-148 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 02/23/20091921 FTS 02/20/20091355 95533 CAS Analytical Parameter Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 2.8 1.0 ug/L 1 Arsenic 7440-38-2 200.8 ND 1.0 ug/L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1 Cadmium 7440-43-9 200.8 ND 0.10 ug/L 1 Chromium 7440-47-3 200.8 ND 5.0 ug/L 1 Copper 7440-50-8 200.8 17 1.0 ug/L 1 Lead 7439-92-1 200.8 ND 1.0 ug/L 1 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 ND 1.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-68-6 200.8 240 10 ug/L 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 245.1 1 02/26/20091651 KJC 02/25/2009 2046 95862 Parameter Mercury CAS Analytical Number Method Result Q PQL Units Run 7439-97-6 245.1 ND 0.00010 mg/L 1 PQL = Practical quantitatlon limit B = Detected in the method blank ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a "W" E = Quantitatlon of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of crttcna Shealy Environmental Services, inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com Level 1 Report v2.1 Client:City of Belmont Description: Pipe 001 Date Sampled:02/19/2009 1055 Date Received:02/19/2009 Laboratory ID: KB19033-002 Matrix: Aqueous Run Prep Method 1 1 1 1 1 1 1 1 Analytical Method (Dissolved Ox) SM (pH - Field) SM 4500-H (Temperature ) SM (TRC - Field) SM 4500- (Cyanide) SM 4500-CN (Phenolics) 420.4 (Fecal Colifo) SM (HEM (oil and) 1664A Inorganic non-metals Dilution 1 1 1 1 1 1 1 1 Analysis Date 02/19/2009 1055 02/19/2009 1055 02/19/2009 1055 02/19/2009 1055 02/27/2009 1036 02/23/2009 1423 02/20/2009 1516 03/02/2009 1430 Analyst SFM SFM SFM SFM RLM RLM SLH JKP Prep Date Batch 02/26/20091038 95924 02/20/20091309 95532 02/19/2009 1651 96136 Parameter Dissolved Oxygen - Field pH - Field Temperature - Field TRC - Field Cyanide Phenolics Fecal Coliform-MF HEM (oil and grease) CAS Analytical Number Method SM 4500-0 G SM 4500-H B Field SM 2550B SM 4500-CL G 57-12-5 SM 4500-CN E 420.4 SM 9222D 1664A Result Q 8.82 7.07 14.0 ND ND 0.012 55 ND Volatile Organic Compounds by GC/MS PQL 2.00 0.10 0.010 0.0050 2 4.8 Units Run mg/L 1 su 1 "C 1 mg/L 1 mg/L 1 mg/L 1 co1/100mL 1 mg/L 1 Run Prep Method 1 5030B Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8260E 1 02/25/2009 0311 DLB 95810 Parameter Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane (Methyl bromide) Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane (Methyl chloride) Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane CAS Number 107-02-8 107-13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-34-3 107-06-2 Analytical Method 8260B 8260B 8260B 8260E 8260B 8260E 8260E 8260B 8260B 8260E 8260B 8260E 8260E 82608 8260E 8260B 8260B 8260E Result ND ND ND 1.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND Q POL Units Run 5.0 ug/L 1 5.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 2.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 2.0 ug/L 1 5.0 ug/L 1 1.0 ug/L 1 2.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 1.0 ug/L 1 POL = Practical quantitation limit 8 = Detected in the method blank ND - Not detected at or above the PQL J = Estimated result < POL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" E = Ouantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page: 8 of 9 Level 1 Report v2.1 Client City of Belmont Description: Pipe 001 Date Sampled:02119/20091055 Date Received:02/19/2009 Laboratory ID: KB19033-002 Matrix: Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030E 8260B 1 02/25/2009 0311 DLB 95810 Parameter 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dlchloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,4-Trichlorobenzene 1,1,1-Trtchloroethane 1,1,2-Trichtoroethane Trichloroethene Vinyl chloride CAS Analytical Number Method Result Q PQL Units Run 75-35-4 8260B ND 1.0 ug/L 1 156-60-5 8260E ND 1.0 ug/L 1 78-87-5 8260B ND 1.0 ug/L 1 10061-01-5 8260B ND 1.0 ug/L 1 10061-02-6 8260B ND 1.0 ug/L 1 100-41-4 8260E ND 1.0 ug/L 1 75-09-2 8260B ND 1.0 ug/L 1 79-34-5 8260B ND 1.0 ug/L 1 127-18-4 8260E ND 1.0 ug/L 1 108-88-3 8260E ND 1.0 ug/L 1 120-82-1 8260B ND 1.0 ug/L 1 71-55-6 8260E ND 1.0 ug/L 1 79-00-5 8260B ND 1.0 ug/L 1 79-01-6 8260E ND 1.0 ug/L 1 75-01-4 8260B ND 2.0 ug/L 1 Run 1 Surrogate Q % Recovery Ac Lim i ts 1,2-Dtchloroethane-d4 108 70-130 Bromofuorobenzene 109 70-130 Toluene-d8 109 70-130 PQL Practical quantttation limit 8 z Detected in the method blank ND Not detected at or above the PQL J Estimated result < PQL and > MDL Whore appEicabte, an son sample analysis are reported on a dry weight basis unless Slagged with a "W' E v Quantitation of compound exceeded the catibradon range P = The RPD between two GC columns exceeds 40% N n Recovery is out of crtterta Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com Level 1 Report v2.1 • SHEALY ENVIRONMENTAL SERVICES, INC. • •••..••s (2, • 2! 75 Z cn CI) ILI 0 (.) Ci) .11 2 cn Z E Qo r— o -s, Z 0 • 2 9 z 0 C CC E 0. --- Z UJ g >'• B > LU ot X CA 1— >4 c n a rr- 1-1'1,2 if- ••, 4-1 LC .47 PIVT.S.' 4C-I1J. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sh:al;, :;:wtrunu,r,t .l Scrvic;!. Inc ,rm•ent l.ur tka F-.�J-•11G \u,atici ti Cher:: ,.;r C a: 1 •,f I r'cplsc:s Date Ettc_t_.'c rgat: t: 5:29 Sample Receipt Checklist (SRC) Cooler inspected bv!datc: ,�� t� 2 i / `J/6 Lot k ,3 `( & > ; 57.44/1 Means of revein ['SESI [ Client ❑ UPS C FedEx. Airtxxne Exp ❑ Other ves ] ND d I SA ❑ 1 Were eutitc�dv seals =resent on the cooler? Yes ❑ �;p \A 12. If custody seals were present. •�'e-c tiiev intact and un' rckcn" Cooler :D1:crni erasure upon receipt 1. 2 _ `C N•lethod: '-e:naeranrr' Blank ] Actainst Bottles Method o co o;ant: W et ice vC ❑ 31ue Ice E L)r ice None 1f response :s No ..,r Ycs for 14.: `. ar exnlanatior.: re.suli :iOrr trust be provided. 3. I temper�rire .of any cooler exceeded 6.:):C, was Project Manager notified'.:' Yes ❑ No 0N - PM notified by SRC_', pione, note (circle one), other: rFor crrriler; received via :o-nmercial courier. PNIs are to be notified immedia:elv. 4. 15 :he comrner:al cot.rier's paci:ir.e slip attached to this form'' 5. Were proper cuitodz Sri 2 lures treiiaouishecl/received l followed' b. We:e sarnole IDs listed? No ❑ N. L, 7. Was collectior. J:i.c . time listed' R. Were tests to be pr;fonned listed on the CK. ;It- was euate provide:? NA 0 9. Did al: samples arrive in the proper containers for each t:5t? SA [ : Q. Did all eorit&ir er label ir.tcrmation i ID, date. tine) introit: with COC? C ..�'t:o:: ••rfpr ker i-dr� a .' ��rt . I. Diu .ill ��tri►:.ii►��S::ai:�C iG �'ti:za C:.•• � {--.._••.•e.•,••. _. .. lC.i. _ S C : _. was volume available' 3. Were eta samples received wtrhin ! :he holding time or 4S hCL S. r�.t.chever Yes ❑ vo NA [ - carte; first`' Ycs . Yes Ycs g Yc (1r Y• e; C/ Yes 'r Ci i' e s No 7 NA NA No NA No ❑ .\ o ❑ •U Yc_: [l N- 7 , NA L I :.1. Were any samples containers missing.' 1 r. Were there ar.• cz:CS. samples not listed on ("7OC? 1 6. Were bubbles present >` pcz.-size ' t::/4"or 5rnrn :n diameter) in any VOA vials? Yc� N N a L Yes ❑ N,_ NA Y i No ❑ NA Q : 7. Were al: mcthis.O& r''HF.M, i atri:nt samples-ezeived a: a pH of •=2'.'_ Y . .Nc '❑ NA I : , S. Wcrc al. :cyanide an for su:f di sam-ii_; receive:: at a pH >:=.1 ‘:C5 No❑ N. F. 9. Were all applicable N71.TKNrevanide:pl►enol;BNA`pcs:2C!:herh (--0.2mg:-) and :oxrcln• (r-Y1. l ni.:`L) samples free of resioual chlocine'.' e, 7 No ❑ NA 120. Were collection 'ern leratares docum: r on r1 e CC)C for NC samples? Sample Preservation (ivkist be completed for any sam7:1e(s) incorrectly p:esc:.cd or witI• headspa;:.) Sample t s) _:Fero received iuciareedy preserved and were adjusted i 1 accoruin..Iy in sample rc'cei ins: wir.h t I,SO..HNO .F'C1.NaOH) with the SR (number) Samplci s) Samples:s ) were received with Dibbles men in diameter. wer::__eired with TRC >0.2 :n ._ for NH Tk.Nicvanide:BN 1pcsIPCRlierh. j Toxicity. sarhp'c(s) were received with TRC 1 soul. and were anaivze:' by method 330.5. Corrective Action taken. if necessary: Was client uotif:ed: Yes n No ❑ IFS' ernal. a e: i 'rnrnen:s: Did client respond: Yes ❑ No ❑ Date cf respons:: Shealy Environmental Services, Inc. 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheaiylab.com Level 1 Report v2.1 ' Peiznit No. i t Oa I I g Outfall 0C...0 Annual Monitoring and Pollutant Scan Zdo g`' Month Year Apri' P.; o r'8 Facility Name: City of Belmont, WWTP Date of sampling: April Analytical Laboratory: Shealy Environmental ORC Sandra S. Edwards Phone 704-825-3791 AMEND Ammonia (as N) Composite 350.1 0.1 0.41 mg/L 1 Dissolved oxygen Nitrate/Nitrite Grab Composite 4500.0 G 353.2 0.4 8.08 25 mg/L mg/L 1 1 Total Kjeldahl nitrogen Total Phosphorus Composite Composite 351.2 365.1 0.5 0.2 2.2 9 mg/L mg/L 2 1 Total dissolved solids Composite SM 2540C 10 460 mg/L 1 Hardness Composite SM 2340C 10 67 mg/L 1 Chlorine (total residual, TRC) Grab 8370 2-500 15 ug/L 1 Oil and grease Metals (total recoverab%), Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Thallium Zinc Cyanide Total phenolic compounds Volatile organic iiiiii eai. Grab 1664 A _ fide Midtotal:phezioliktiff;taig,, Composite Composite Composite 200.8 200.8 200.8 Composite 200.8 Composite 200.8 Composite Composite Composite Composite Composite Composite Composite Composite Grab Grab 200.8 200.8 245.1 200.8 200.8 200.8 200.8 200.8 SM 4500-CNE 420.4 4.6 1 1 0.4 0.1 5 1 1, 0 .000 10 5 1 1 0.5 10 0.01 0.02 ND 3.9 ND ND ND ND 15 ND ND ND ND ND ND 120 0.015 0.033 r,f mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L mg/L ug/L ug/L ug/L ug/L ug/ L mg/L mg/L 1 1 1 1 2 1 1 1 1 1 1 1 1 1 1 2 Acrolein Acrylonitrile Benzene Bromoform Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromomethane Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab 624 624 624 624 624 624 624 624 624 624 50 50 5.0 5.0 5.0 5.0 5.0 5.0 10 5.0 ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1 1 1 1 1 1 1 1 1 1 1,1-dichloroethane 1,2-dichloroethane Trans-1,2-dichloroethylene . Y s Parameter ; _ ' y Volatile organic compounds (Con 1,1-dichloroethylene 1,2-dichloropropane 1,3-dichloropropylene Grab Grab Grab Grab Grab Grab 624 624 624 5.0 5.0 5.0 uantitation rlevel> ND ND ND �le> ug/L ug/L ug/L Units Measurement 1 1 1 lumber of samples);. Ethylbenzene Methyl bromide Grab Grab 624 5.0 ND ug/L Form - DMR- PPA-1 Page 1 Annual Monitoring and Pollutant Scan Permit No. /I 00:4i f Outfall 00 Month Apr, I e • - Year Methyl chloride Grab 624 5.0 ND ug/L 1 Methylene chloride Grab 624 5.0 ND ug/L 1 1,1,2,2-tetrachloroethane Grab 624 5.0 ND ug/L 1 Tetrachloroethylene Grab 624 5.0 ND ug/L 1 Toluene Grab 624 5.0 ND ug/L 1 1,1,1-trichloroethane Grab 624 5.0 ND ug/L 1 1,1,2-trichloroethane Grab 624 5.0 ND ug/L 1 Trichloroethylene Grab Vinyl chloride Grab 624 5.0 ND ug/L 1 Acid -extractable comimunds:-,,,,N--•;.:,,,,..:T.jj„i,,,i1,,',,i4";:'-''''-'S7:1.;10.1..-40,:"-i.-,,.:°iri47',--='],,::-.4ii-t-CA:i4,,---:•ii;•'; '",-;;.,i-''*:--.--;:-- P-chloro-m-creso Grab 2-chlorophenol X Grab 625 _ ND ug/L 2,4-dichlorophenol1 Grab 625 ND ug/L 1 2,4-dimethylphenol )( Grab 625 C5:-.5 1 ND ug/L 1 4,6-dinitro-o-cresol Grab 2,4-dinitrophenol Grab 625 26 ND ug/L 1 2-nitrophenol Grab 625 10 ND ug/L - 1 4-nitrophenol Grab 625 26 ND ug/L 1 Pentachlorophenol 7( Grab 625 A ND ug/L 1 Phenol Grab 625 5.1 ND ug/L 1 2,4,6-trichlorophenol Grab 625 4. ND uz/L 1 B'As'e*eiitiiiraiiiiijoei".thkdoi%ISVA!V,:12-tWrd)ttt: '' --..,0 :.i..e. : . , :.1.)-2:4,. ' -44,CVZOA ,,siwe ortVjgCtiaVingi Acenaphthene Grab 625 5.1 ND ug/L 1 Acenaphthylene Grab 625 5.1 ND ug/L 1 Anthracene Grab 625 5.1 ND ug/L 1 Benzidine Grab 625 . 26 ND ug/L 1 Benzo(a)anthracene Grab 625 5.1 ND ug/L 1 Benzo(a)pyrene Grab 625 5.1 ND ug/L 1 3,4 benzofluoranthene Grab 625 5.1 ND ug/L 1 Benzo(ghi)perylene Grab 625 5.1 ND ug/L 1 Benzo(k)fluoranthene Grab 625 5.1 ND ug/L 1 Bis (2-chloroethoxy) methane Grab 625 5.1 ND ug/L 1 Bis (2-chloroethyl) ether Grab 625 5.1 ND ug/L 1 Bis (2-chloroisopropyl) ether Grab 625 5.1 ND ug/L 1 Bis (2-ethylhexyl) phthalate Grab • . 4-bromophenyl phenyl ether Grab 625 5.1 ND ug/L 1 Butyl benzyl phthalate Grab 625 10 ND ug/L 1 2-chloronaphthalene Grab 625 5.1 ND ug/L 1 4-chlorophenyl phenyl ether Grab 625 5.1 ND ug/L 1 Para,,,,..:mo.,..;1 ^ '''' ='-'4 -,•- ,-1- .• --- ' - : ,', e . - -' ; ''-: !. - 7 ' ..., .. - ,-,- - -.-4- -,...--z, 6 ii:,', 4 ._ .. , . •,' r,,-....,-„%-„, __,--.4,,,N47- .n):17 i --11j9701,4-i,-- 4 ,,,. iiii,., - * .'- - ,ia,t,f ... ti::-, 1,14.ir riv..,,,,; A:1.t,6',6147-.4, ' ,,, %--.-- - ----- - ..,:._..eas Men* ' ,. . Number: of : •,,. ,,-;., • ,,,,,, ' - ,, ...--, . ." .' ,Base'.ife,a :ablikiii -;:: -- 1#,!'.? -Iga4,- ,--71::+:21i-375-11'„'W:,),:- 'TA,Re.-7-iAtolA.,- Chrysene Grab 625 5.1 ND ug/L 1 Di-n-butyl phthalate Grab 625 5.1 ND ug/L _ 1 Di-n-octyl phthalate Grab 625 5.1 ND ug/L 1 Dibenzo(a,h)anthracene Grab 625 5.1 ND ug/L 1 1,2-dichlorobenzene Grab 625 5.1 ND ug/L 1 1,3-dichlorobenzene Grab 625 5.1 ND ug/L 1 1,4-dichlorobenzene Grab 625 5.1 ND ug/L 1 3,3-dichlorobenzidine Grab 625 5.1 ND ug/L 1 Diethyl phthalate Grab 625 5.1 ND ug/L - 1 Dimethyl phthalate Grab 625 5.1 ND ug/L 1 2,4-dinitrotoluene Grab 625 10 ND ug/L 1 ' 2,6-dinitrotoluene Grab 625 10 ND - ug/L 1 1,2-diphenylhydrazine . Grab . 625 5.1 . ND ug/L 1 Form - DMR- PPA-1 Page 2 Pefmit No. A/C oo l I S Outfall uc Annual Monitoring and Pollutant Scan Month R*rI Year e?0°S Fluoranthene k Grab 625 5.1 ND ug/L 1 Fluorene Grab 625 5.1 ND ug/L 1 Hexachlorobenzene _ Grab 625 5.1 ND ug/L 1 Hexachlorobutadiene Grab 625 5.1 ND ug/L 1 Hexachlorocyclo-pentadiene Grab 625 26 ND ug/L 1 Hexachloroethane Grab 625 5.1 ND ug/L 1 Indeno(1,2,3-cd)pyrene Grab 625 5.1 ND ug/L 1 Isophorone _ Grab 625 - 5.1 ND ug/L 1 Naphthalene Grab 625 5.1 ND ug/L 1 Nitrobenzene Grab 625 5.1 ND ug/L 1 N-nitrosodi-n-propylamine Grab 625 5.1 ND ug/L 1 N-nitrosodimethylamine Grab 625 5.1 ND ug/L 1 N-nitrosodiphenylamine _ Grab 625 1 5.1 ND ug/L 1 Phenanthrene Grab 625 5.1 ND ug/L 1 Pyrene Grab 625 5.1 ND ug/L 1 1,2,4,-trichlorobenzene Grab 625 5.1 ND ug/L 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibel for gathering the information, the information submitted is , to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. fl T rCk Ed (,Jo (ofS 'Authorized Representative name S Lc,c-(-06}Jo.LcA, Signature /61.73/0g Date Form - DMR- PPA-1 Page 3 06/30/2010 11:33 8648776938 ETT ENVIRONMENTAL -ffluent Toitkity Report Form•Chronie Fathead Minnow Multi -Concentration T *te:08131109 PAGE 10 1 81 Control x Faciliy Delmont Laboratory; ETT Environmental NPOES 0 NCO0 21181 Pipes: 001 County Gaston 5ignatur,!of Operator In Responsible Charge Sig attire o(Lalwratory Supervisor ommonta MAIL, ORIGINA1. TO: Environment") Sciences *ranch Division of Water Qualkv NC DENR 1621 Mall Service Center Raleigh, NC 27699-1621 ttcd JIL r �()(1ac( Test Inllletion Onto/Time 18-Aug-09 % Eff. Repl. Surviving a Orlglner Wt/original (mg) 2 ) Surviving # Original 0 WI/original (mg) Surviving # Original # WI/origin/II (mg) Surviving # Original # Wt/0rugirtel (mg) 4 16 Surviving # Original* Wt/original (mg) Surviving # Original* Wt/originat (mg) Water Quality Data 321 Control pH (SU) InIUFin 00 (mg1L) Init/FIn Temp (C) !nit/Fin High Concentration PH (SU) Inh/Fin D0 (mg/L) INUFin Temp (C) Init/Fin Smolt Ceeection Start Date Grab Cornposlto (Duration) Conductivity (umhos/cm) Alkalinity (ntg/L) Hardness (mg/L) Chlorine(men-) Temp at Receipt ("C) Test Organisms Cultured In -House Outside Supplier Hatch Date/Time' 08"17.09 ( 1300 2 4 Avg Wt/Surv. Control 10 10 9 10 10 10 10 10 0.389 0.400 0.339 0,447 10 10 10 10 10 10 10 10 0.402 0.397 0.408 0.391 10 10 10 9 10 10 10 10 0.383 0.384 0.489 0.342 10 10 10 9 10 10 10 10 0 443 0.431 0.444 0,405 10 10 8 10 10 10 10 10 0.395 0.425 0.371 0,398 9 10 9 10 10 10 10 10 0.435 0.483 0.418 0.390 Day 96 Su/Nivel Avg WI (mg) % Survival Avg WI (mg) % Survival Avg WI (mg) 1 Survival Avg Wt(mg) % Survival Avg Wt (mg) 1 Survival Avg Wt (mg) 0.4031 ) 0.3941 100.0 0.400 97.5 0.4061 97.5 L 0.4311 95.01 0.397 95.0 0,4321 0 2 7.80 1 no 7.90 / 7.80 7.60 / 7.40 7.80 / 7.30 7.70 / 7.00 7.80 / 7.70 7.70 / 7,70 no 1 7,00 8.3 1 na 8.1 1 7,3 8.0 / 7.1 8.3 I 7.4 8.4 / 7.2 8.8 / 7.1 7.8 1 7.0 na 1 7.8 24.7 I na 249 / 24.9 25.1 / 24.9 25.3 / 24.4 20.2 / Z5.1 24.8 / 24.8 26.1 / 24a iv / 24.3 2 7,40 1 na 7.40 / 7.40 7.40 / 7.30 7,40 / 7.60 7,00 / 7.80 7,70 / 7.80 7.50 t 7.90 no I 7.40 8,7 / no 0.0 / 7.8 8,3 / 7.4 8.1 ( 7.0 8,2 / 7.2 8.4 1 7.2 7.8 / 7.0 na / 7.5 25.1 / na 24.7 / 24.9 25.3 / 24.9 24,5 1 24.4 24,8 1 25.1 25.1 / 24.8 24.9 1 24.4 na / 24.1 08/16/09 08/18/09 08/20/09 24 hrs 24 hrs 24 his 1010 1073 11t16 -I 88.8 64,8 67,3 46 50 44 0.05 '0.05 <0.05 4.7 2.7 4.6 OWO Form AT-5 (&03) Control Hardness 48 mg/L Alkalinity 45.1 mgll Conductivity 182 umnowon 1 0830 - 1000 MDT Survival Growth Normal W= n,81 no 0.93 yes Hom. Var. Sr- -13.2 yes 11.3 yes NOEC > 32.0% > 32,0% LOEC - 32 0% > 32.0% > 32.0% > 32.0% Rank &um Dvm.1 Teat 11 2.55 ChV Method Crit Ursum Conc. 2.0% 4.0% 8.016 16.0% 32.0% 18.00 20.00 20.00 18.00 14.00 -0.22 -0.22 -1.41 "0.11 -1.44 BILLED SEP - 5 2009 Sliv7T! 9 SEP r 5 2ME EflVkonmeinIld. inc. TT Liaittng Address: RO. Box 16414, Greenville, SC 29805-7414 ShippingAddress:4 Craftsman Court, Grey, SC 28650 Phone: (814) B774942 Fax: (864) 877-6938 Too Free: (800) a91.2325 Email: maileettenviinonmentaLcom Facility: 641i of (JjVJr 1, klui I r site Description:: E flQ(fl] CCOVINSi k cS t State: f4C , County: NPDES 9: (t}Zl, Pipe It obi CHAIN OF L ..STO DY FORM GRAB SAMPLES Collected By (Print): Signature: Datetflme: Sump iDot�tgi :� Titn B:tis>lliOuiii "PtG tff Gumpp t4 ii��.�as "`!� ' ram{- l ,. i i SAMPLE CUSTODY TRANSFER RECORD (Please sign) Sample Sealed By: Relinquished By - Received 8y: 'Relinquished By: JReceived By: Relinquished By: Received By: Relinquished By: Received By: i i COMPOSITE SAMPLES CIzflesictial- r -rf-t13m rla.3� Page of __1_ Set By (print): N San Brien deck Collected bry: 5CFiCir Signatum ,tv,^ Roc x signature: DaterTime: 811640PI � $'•�8f�r� 1Jate/Time:2J11/0? ti17oWYN Frequeacy: ALA 6rwmic- Y 1 No 1 f dt DatotTlme: t�i en7:},n ff DatefTime: f • /o Organization: Date/Tme: Organization: Datefflme: tLE4t• 0511 fi 1 /03a Organization: Date/Time: Organization: Date/Time: Organization: Organaa9on: Preservation concentrations am below DOT concentratton Wks. Date/Time: Date/Time: SAMPLE T IIISP T Carrier. Transport Method:S Received By (Slgrra RECEIPT AT LABORAT • Y Relinquiahe d By �"— v � '_ ceived anization:Ein Organization: Date/Time: I•f7-� /a`� Date/rime: e. /'' , p9 /zap unsealed By: Arrival Temp: Y. 7 •C Semple Unposed/Returned By: Date: 8E69LL8b98 virenmentdl, Inc. Mailing Address: RO. Box 16414, Grecnvflle, SC 22868-7414 Shipping Address: 4 Craftsmen Court, Greer, SC 29650 Phone: (814) sn-6942 Fax: (884) 8774993 Ton Free: (SOO) 8912325 Email: mail®ettsmrfronmentsl.com FaciSty:C111 BQT mbr M StEe Desaipiion: iuen4 Corripily i5ample Stale: K.ii County: Ga.s4th NPDES P: lr 14 81 Pipe 2: OIN I [t2 ..��v •,.'. t..:T{, �:: :r •. .�. �- •-";i :x:zvh �eyvv`hr ry r • •� I •t Jl t' • �i1.lt$�11trS �fi CHAIN OF LJSTODY FORM GRAB SAMPLES C; I Z twit - 04 .p I.44f. `Tcm9'10-re Page Canocted By (print): Signature: Date/Time: COMPOSITE SAMPLES Set By (print):1&+ 7.0 P' Signature: Coiected by:TSC e' Signature:.-^ 1DaeIrunj 935 1 �atuRtme: 41 0t)1 ? 2.4 j .Wt# Frequency: rA PrsForl'M J ample Chilled? d I No Z PAS A{Vj nkloox isrogram Area' •rRi' yii........ .. .. .:�. {..`:X:: i :•�hr .... � rw•w{ j : : •.[ aI•ys;-.Z'1, kv:.•s. .... r. ::..1 ..t tt:t. v 'i. t.... C%tnic f»t73 JSAMPLE CUSTODY TRANSFER RECORD (Please sign) Sample Seated By: Reinquished 8y: Received By: 4Ce 2t 4". lees-1 -%. 40-- o`14 t �+ ! la35. Rerinqutahed By: Organization: Received By: Orgafiza6on: Relinquished By: Organization: 'Received BY Organization: Preservation concentrations are below DOT concerdratlon »mils. v. SAMPLE TRANSPORT Canter: Date/Time: M)1 ,1 I Z ilk" Transport Mclhod: v . !ration: �Z tY Dategime.lepireAgerReceived 8y (Signature) - Organization: Date/Tirne: Organisation: Date/Time: Date/Time: Date/Time: Date/Time: Date/Time: RECEIPT AT LABORATO Relinquished ived By. Organization:LT Organization: f a/Time: t? i 'aj Oet.frane: ��� / LQUnseaIed By: Airtval Temp: a? -C Sample Disposed/Returned By: Date: 0t0Z/0£/90 8£69LL8b98 TT nvirenmentalt, inc. Mailing Address: P.O. Box 16414, Greenville, SC 29980S-7414 Shipping Address: 4 Craftsmen Court, Greer, SC 29830 CHAIN OF LoSTODY FORM Page Cltllu&t- •cv3 9S 'l•S; oft • ••••••••• �••••••, v.•-•••••••• •-w•. �a�ai.com +j fr. •-vwv 'Wig r.w: ta441J ow11-sos� Email: naileetterwircnmcrd Facility: C (AN Q If IYhA4 W u1.r II' RAB SAMPLES Collected By Wirt): Signature: Date/Time: COMPOSITE SAMPLES Set By (Pitti • Collected by• . - , 2CJr Signatu S' nalw.: To Dale/Time: St2titicA 17--1 1 DaterTime: eiz~ic/q VOW" f Sr1. Sample Chilled? / No Site Description: gr kill Cianzsi 143 State: NC County: C1of4tri Pipe it: (b ( , NPDES a: CO2,) MI .. - �� �:���:. ..- m Area .. a.• .... � � _Frequency .. r.... .. .. ♦ r . .. Sainplaln ::= •: - - - . .: r.., • . cc .., - ....... a r.vv r• =' . iffatd.' ---....... -. Y. . TiniiQ°. • _ >¥ orltei fir. Twr,.Wolvmro ..... .. :?v . , �� r ♦, .-�-�r. . Vi: vti a -r r_r.v.. . a k`_ .'' .... • ... ... ....... . , ; -.: i::. . ... �.; 3'aa • : Eiarjztars :.. _ . �'j•.'�: Iti>Rl- . . cf C01 - 6 S4 2 1z NO L/ ejnnar� c Tot fi �a vie: C- ,Pk pt4.7.3g .` • _ T 5 A1 1 i SAMPLE CUSTODY TRANSFER Sample Sealed By: Relinquished = . �+ �� 40010 Received B� : ''r .� / , RECORD (Please sign) • �j t Organization: 0�N•�Datefrme: 'i2 �� �� 'lianapattllAatho:i' �/ 0 f Organization: Oateffims:�.� �� Organization: Date/ lime: Organization: Date/Time: SCcvr4 lock•'... �r+17 �•'� rolJ Organization. Date/Time: Organization: Dale/Time: Organization: Date/Time: Organization: Date/Time: SAMPLE TRANSPORT Cater: Received By (Signature): Relinquished By: Received By: �pt- �i+pk 1 Relinquished By. 1 Received By: Relinquished By: Received 8y RECEIPT AT LABORATORY J, � ' 14 Relinquished By- need By: rganzaiion:67/�� Organization: n: Date/Time: r'.0-0 g Date/Time: S %� 47 / OOUrrseaied By: ` ✓` Arrival Temp: T. f� $- 'C Sample Disposed/Returned By: Date: • reservation concernlrations arebelow DOT ooncentratbn limilo. m N m w w 8E69LL81'98 D m 06/30/2010 11:33 8648776938 ETT ENVIRONMENTAL Effhpant Toi.±city Report Form -Chronic Fat/road Minnow Multi-ConcentratIon TMtr.11130109., PAGE 14 Patiity: Belmont Laboratory: ETT Environmental NPDE$>MNC00 21181 Signsturo of Operator In Responsible Charge nature of a • . - tory Supervisor Pipe tt: 001 County Gaston MAIL OR1f71NAI. TO: environments, Seiencen Branch Division of Writer Quality NC DOIR 1.621 Mill Servioc Center Raleigh. NC 17499-1621 Test Initiation Dant/Time 17-Nov.09 Control S EK. Rep!. Sunriving it Original Wt/orignal (mg) 2 Surviving X Original4 Wt/nnginal (mg) 4 Surviving 4 Original 0 Wt/original (mg) 8 Surviving 0 Original* Wt/original (mg) 10 ( Surviving 4 Original X Wfloriginal (mg) Surviving* Original 0 WI/original (mg) Wetor Duality Data Control pH (SU) InWirin DO (mg/L) Snit/Fin Temp (C) Init/Fln 321 High Concentration pH (SU) Init/Fin DO (mg/L) Intt/Fin Temp (C) Init/Fln Sample Collection Start Date Grob Composite (Duration) Conductivity (umnos/cm) Akalinity (mg/14 Hardness (mg/L) Chiorine(mg/L) Temp al Roosipt ('C) 1 / 1300 2 3 Avg Wt/Surv. Control 10 10 10 9 10 tO 10 10 0.4.10 0.364 0.405 0.426 10 10 10 10 10 10 10 10 0 403 0.449 0.411 0.432 9 9 10 10 10 10 10 10 0.404 0.373 0.434 0.490 10 10 10 9 10 10 10 10 0.437 _ 0 473 0.465 D.397 10 10 10 10 10 10 10 10 0,551 0,427 0.575 0.443 8 g 10 8 )o )0 1 10 10 0.483 0.442 0.518 0.494 Day % Survival Avg Wt (mg) 4 Survival Avg WI (mg) % Survival Avg Wt (mg) % Survival Avg Wt(mg) % Survival Avg W1(mg) 9 Survival Avg Wt (mg) 0 2 0,423 l 0.4111 100.01 0.4241 es,01 0.425 97,5 0.443 100.0 0.499 07.51 0.479 IIIIMY 7.7 1 1 na 7,8 / 7.6 7,8 / 7.4 7.7 / 7.5 7.8 / 7.6 7,7 / 7.7 7.8 / 7.8 na r 1 8.1 8.9 / ne 8.0 / 7.5 7.6 / 8.2 8.1 / 8.2 8,2 / 7.1 8,3 / 6.7 8.2 / 6.5 na / 6.5 24.8 / na 23.1 1 25.4 24.7 1 25.2 25.1 / 25.1 25,5 / 24.9 25,3 / 25.1 25,7 / 25.8 na / 25.3 0 7,5 / na 8,1 / ne 25,2 / no 7.8 / 7.5 7,8 / 8.7 25.2 1 25.4 2 7.5 / 7.4 8.1 / 8.5 28.0 / 25.2 1 2 11/15/09 11 /17/09 11 /19/09 24 hrs 24 hrs 24 hra 783 888 1278 32.8 55.7 62.5 60 54 46 =0 05 c0 05 0.07 1.2 2.1 2.$ Teat Orgenlsms Cultured In -House Outside Supplier )( Hatch DatefinlP.ilw..i•1D.0B.. Control Hardnoan 48 mg/L Alkalinity 57.8 mg/L Conductivity 183 um4oelcm / 0830 - 1000 MST 3 7.5 / 7,7 4 7.8 / 7,8 8.1 1 6.7 8,2 / 7 2 24.8 / 25.t 25.1 / 24,9 5 6 7.8 / 7.8 7.7 / 7.8 8.1 / 7.0 25.2 / 25.1 Survival Normal W= 0.90 yes Hom. Var. 9= -29.2 yes NOEC > 32,0% LOEC > 32.0% ChV > 32.0% Method Dunn. 1 T94l Cri1 t/rsum 2.55 Conc. 2.0% -0,68 4.0% 0,98 5.0% 16.1" 32.0% 0.00 -0.88 2.54 8,2 1 6.7 25.3 1 25.5 Growth 0.97 yes 5.01 yes > 32,0% 32.0% > 32.0% Dunn. t Tool 2.55 -0.41 -0,46 -1.02 -2.78 •2.16 7 na / 7.7 na / 6.6 no / 26.3 DWQ Form AT-5 (8/03) BILLED DEC - 8 2009 SHIPPED DEC - 2 2009 TOXICITY CHAIN OF CUSTODY Facility: ciboSfInikits4IQ INt21k ETT ASSIGNED LABm# 3 0f! SAMPLE ID I TT eDvuonMental, inc. l'gsrsnonroaale! Test Container Paean Sample Pro .m (Indicate%&Containers -dire T 1 3 5 k 0 g oc • • • O -mt w 0 V Liz tweeetaf ..U1 Idailing Address: PO Elea 16414. Geemdlls, 9C 29605.7414 Shipping Ad st 4 Csnitzetan Ct, Greer. SC 29650 Phew (I164) 977.6942 or (BOO) 891-2325 V 0 oN, Acute 1 Testpanantaer Maele neon To:dcity t• 0 11 a . da: EPA 1002 J Chronic o°a 8 a •a Special Sediment O O 0 O O 1f: 33 Temp-5. ,,- Pogo J of E FAX: (164)877 - 6938_ ermsail:ziaiglationoinomonialcomo Testpariometer Aoudafsd Cbseebt*y 0 .a ICOMPOSHIt SAMPLING PROCZDURRS Composite sample, muss to c,!!armed over a 34 haw polio& Tina Proportional: l maple each hour far 24 hots. Bqualwabanes. or et nitrite= t tamp!* envy 4 hours over 24 haws. Flow Proportional: As par instructions in NPDESpenrlil. Spacid fristerctiaas: ThMPHRRIilRB bMCWIIORWOPROCtTBURHS Somp!e tetaprtaturo dazing collection eui In mipost oust lea between 0.0 and 6.0 •C. Serapler crust nal be Goren. Us* avatar ice is sealed begs. *mum tamp none upon receift arid meat Nati& client to temple Map endure is out change. HOLD 77MitPROCSDl/R&S For taxyCosting the sample must Got bI used within36boon of sample coUactina(cosephtian of coop Doke sample). Semple may not be used altar 72 harsh from sample collection Sample Custody Transfer Date Time Record R - Willy l Orgtaizetiaa Receipt Temp •C Receive 1 etim Secure e 1tiktuo Sdsecrd :.. _ / _..., Arg/C Sampling Coraposde 1 Q Start Oale/Time:11,109 itlaA 1it.Date(rima: sedBy: ,Law." K ,odh Conectedfy rn4Dm1dFim. t \i Yr1 Ended Ur aS, ITemO. siCotleetir . 8E69 rrl m p� r to uz Ke etaid- t - 5.4' TOXICITY CHAIN OF CUSTODY Fe\ kf lP o e: ii1i1'DS b02,11511 E1T ASSIGNED LAB ID 34[4eo3 SAMPLE ID Davisooraaatd Pit 0 0, { z Efenvironmental, inc. Ted Container TT Indicate * ofCoalainess t1 1 $I g 9 0 -Presjerrf .ative • Semple Type 8 0. M a. • 0 O Mailing Adams: PO Rex 16414, Cremes, s, SC 29606.7414 kg" Slrfppd g Addeo=4 Craftsman C . Meer, SC 29650 Pleas (1164)877.6942ar (800)891--2325 co FAX: (864)877 - 6938 � w • m esaaiL• 4 Acute Ttstp+ramater Whole Effluent Tea kIIy 0 �4 W A 4 4 0 cal a Special e� moo. 2q arr f 04 Sediment 8 Teslptsanseter m Associated Chtasista7 co ta)tat .1 V • h et f COMPOSfli mamma PRUC OWLTS Composite samples cast bs collected over a24hour period Time Progortioaat-1 sample each hour fbr24h urn Equd volumes. or etrobi nuo L sample every 4haws over 3Aboars Flow Proportional: A s per instructions in NPDFS permit. • Special Inslmatioas: i 116. • f I 1 i TTJ,IPBRITURS MOJ4IIVR WG PROCEDURES Ssmple temperatura dining collection and transport must be b:Owen 00 and60°C. Samples must not ba frozen. Use wales ice is sealed bags. Mearuse temperature uponsaceipt and :scent. Ned/ client to crumple Jtemperature is out of wage. Sample Castody Transfer Record Date Time ReiragniabedilylOrmaaatiom Received Byr/Organaatioan Secure • a Receipt Teenp°+C ivAtct 4,;g .4t _ti- —.1.ilV.itfr7:1:11-;Al ...r''-';_ 1 i HOLD TU/S PROCEDURES For toxicity lasting the sample most first be used mill i:136 W= escalate colleelaion(corapletion al:eompasite sample) Sample may not be weed after 73 haunt front sample calls ctiom. i Sampling C .. Orb StartData/Ti:es: ,' :'' . ` v, gtgAli t Datcflima: HetB>J 4 r' Collected By V End Dalsffisam ��` ► • gear Fused _ 11Tearp dConecliionc 8£69LL8b98 tr TOXIdi i Y CHAIN OF CUSTODY Fact iy: OCtad Lkile e: Witt tl Eminences i' ASSIGNE ETD LAB104 SAMPLED 3 oc ' r-Sc Comp ?torso eavronmenfal, Inc. 7'estCanteiner 1Preserr buicers S otContaiaers 1-dive 2 Sample T7tu Maim Address: PO Box 16414, Grcenvila,SC 29406.7414 SkIpplag Address:4 Craftsman Ct. Greer, SC 29Q68 Plrorse:0164)677-6942 or (0 )691 Tcstparaa:sdar Wlrsls1211aantToadrity Acute I E1 0� V � ��!i fQV f� esati7 `� 4 ii2:1 ao Qom] .2 a A ti A H v rl co a. i `AL tcestdua i - .010 r" -' I.4v imp FAX tf64)877.119311; snsaii: maiieeitonebrounsntalmta Test wanner Associated. Chemistry et CI w Chromic M 0 O. U fa iv Fathead: EPA 1000 0 0 a. p poi gig Sstttm4211 11 YV 1 oz f COMPOSER SAWPL1NG PROCItDURt4 Comp asks samples snot be collected ores a 24 hoot puke!. Time Propotianot 1 simple etch hour Par21 hours. Equal voles. as at minimum 1 surge every 4 hours over 24 hours. Flow Prop oatioaaat As per instructions in NPOES pemnt. Special Instructions: r-- 1f 1 • i 7701dPSRAIT/RSMON1117Ra 1t PROCBDURSS Semple temperature duaogcoasttiors artd trumped must b s between 0.0 and 60'C. Samples must nab* &rain Use water ice in seeded bags. Measure temperadme upon receipt and record Nosily d ent to rumple Utarn esatasro is out of ramp. i i 1 l 1 HOLD 7102 PROCEDURES For toxicity totting the sample must first be used within 36 bons of sample collectioa(eoorprelion of composite sample). Sample may not be used after 72 hours from semp*c collection. Sample Custody Transfer Record Oats Receipt Tamp'C a4. Sang Composite Grab Sla:tDelo/rime: ll,t411,4 �� Da1 fires: Sot Collected Br Enid Detarruae: % of 55Z? t&+� Temp. alCOteeetiarr et6Z/0£/9e 8£69LL8098 ETT ENVIRONMENTAL PAGE 06 06/30/2010 11:33 8648776938 EfflWrit Toxicity Report Farm -Chronic Fathead Minnow Multi•Conantration TQate:08102J09 Facility: Belmont Laboratory: ETT Environmental Signature of Operator In Responsible Charge SI• ature of La••ra • Supervisor NPDES A N000 21181 Pipe 0: 001 County; Gaston Comments I MAR ORIGINAL TO: Gnvirnnnteetil Se:e.cee branch Dlvi+inn nr Water Qui I ity NC DENR 1621 Mail Scrvico Center Raleigh, NC 27699-1621 I od oc( Test Initiation Date/Time 19-May-09 / 1800 % Eft. Control Repl, Surviving X Original N WI/original (mg) Surviving % Original 0 Wtloriginal (mg) Surviving # Original Y WI/original (mg) 2 4 8 Surviving Original* WI/Original (mg) Surviving # Original 8 WI/original (mg) Surviving # Original $ Wt/original (mg) 18I 32 Water Quality Data Control pH (SU) Ink/Fin DO (mg/L) Init/Fin Tamp (C) Init/Fin High Conc,ntratlon pH (SU) Init/Fin DO (mg/L) InitlFin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Conductivity (unlhoe!cm) Alkalinity (mg/L) Hardness (mg1L) Chlonne(mg!L) Tamp at Receipt (•C) Test Organisms Cultured In -louse Outside Supplier Hatch Date/Time 2 3 4 Avg WI/Su/v. ControlI 0.3701 10 10 1D 1D 10 10 10 10 0.326 0.392 0.369 0.394 10 10 10 9 10 10 10 10 0.429 0.383 0,356 0.313 10 10 10 8 10 10 1D 10 0.375 0.403 0.321 0.327 9 9 10 10 10 10 10 10 0.369 0401 0.396 0.380 9 9 9 10 10 10 10 10 0.383 0.345 0.377 0.388 6 9 10 10 10 iD 10 10 D.380 0.383 0.357 0.385 Day % Survival Avg Wt (mg) % Survival Avg Wt (Mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % 3trrvlval Avg Wt (mg) % Survival Avg Wt (mg) 97.5 t 0.3701 95.0 0.357 95.0 0.387 92.51 0.388 92.5 0,378 0 2 4 6 7.90 / na 7.60 1 7.60 7,70 / 7.50, 7.80 / 7.70 7.70 / 7,60 7.00 / 7.70 7.90 / 7.60 na 1 6.00 8.3 / na 8.2 1 7.8 8.3 1 7.4 8.3 / 7.2 8.4 / 7,1 8.8 / 7.1 8.3 1 7.7 no / 7.7 24.3 / 111 25.0 1 24.2 25.0 / 25.2 25.2 1 25.0 25,4 / 26.7 25.4 / 25.5 20.3 1 24.7 na 1 25.3 2 3 5 a 7 7.50 / no 7.10 1 7 30 7A0 1 7.40 7.50 / 7.00 7.60 / 7 70 7.70 / 7.7D 7.70 1 7.50 no / 7.60 8.2 / 1 na 8.2 1 7.3 8.4 / 7.5 8.4 / 7.3 8.4 / 7,2 8.5 / 7.0 8.3 / 7.9 na / 7.7 25.1 / na 25.1 / 24.2 25.1 / 25.2 25.2 / 25.0 25.2 / 25.7 25.5 1 25.5 25.3 / 24.7 na / 25,3 2 3 05/17109 05/19/09 05/21/09 24 hrs 24 hrs 24 hrs 885 993 t104 30.4 59.9 63.7 50 88 52 0.07 0.06 <0.05 1.1 _ 2.3 3.5 X 08.18.0E Control Hardness 40.0 mg/L Alkalinity 59.4 mg/L Conductivity 211 urho,/em 1 11AM•ZPM Survtvel Growth Normal W= 0.92 yes 0.07 yes Horn. Ver. B^ -12.3 yes 7.57 yae NOEC > 32.0% > 32.0% LOEC > 32.0% > 32,0% ChV > 32.0% > 32.0% Method Oven. I Toil Cam. t Teat Crlt tlrsvm 2.55 2.55 Cone, 2,0% 0.55 D.00 4.0% 1.02 0.64 8.0% 1.09 -0.75 18.0% 1.64 0.09 32.0% 1.57 -0.28 ResuIt Pass Ch=32,0% ) BILLED JIJN 1 5 2009 0140 form A7-6 (8 03) SHIPPED JUN 1 3 2009 TT nvironmental, inc, Mailing Address: P.O. Box 16414, Greenville, SC 29606.7414 Shipping Address: 4 Craftsman Court, Greer, SC 296S0 CHAIN OF ATODY FORM c,1_IS e 1r1ua l o1y� P Page 1_ of - ---.. . —• .-•••r..•. ,=... , -. r-vwv .w. r.w. MOW oa.-aaca MaileetterwlronmargaLcorr► FacilityCl\-ki nk 1' d rnDA4 14.1 1& GRAB SAMPLES Collected 8y (print)- Signature: Dataf lne: COMPOSITE SAMPLES Set By (prbt)� by: - ell ir �• St �� collected Signature: Signature: � r Datefe: S M G 1Lo v, Date/Time: �410q � / 3 Mr Frequency: fita Weip(4s'ae1Lt.IChilled? (Yet I N. rr11 l _ G Site aescription:� •till ef{ C.Cri cSt N &n1pk State: l y e- Count)Jph Pipe d: obi Q Af NPDES A: O i t gi Y. ♦.:: I i i � Yr .. : ., i:••:.. : • , • _ $artlgfA Ili I .. ., ....'!•1:.: .i, �Q!>ss�r,,: _ Y�:: � .E?ai� .: v -.. lh::t : iTitne:- : ♦\/. � • �<Kai�a :1YYFKY ,�(A� : i �� V' .••O•f ::; "t t• >,l3t�rrv�t • `• ,p.rsIstworea L•tha,.:wY ;• g<Y 7}VS: V•. :::V•fV.lYY\'P.:]'•� 1. 1.2..•t�i•IY VJl:ri•�:•:.:•-Y .. , y�y,.<y- � : _ }:: w i s ' • • r w•a : • t • • ,...,:,;:„:v.. .:. Zti.rY•i�.. i:WY: ..: .• .: •YY (•♦ ..$ inY - �+��J (� -+h5 , -�1 t--WConie r\ NbtIcts. .• .... -//..�_1.`/_�■e/. t: \:/� SAMPLE CUSTODY Sample Sealed By: Relinquished B : Received By: �� Relinquished Ely: Received By: tt Relinquished By: Received Br. Relinquished By: Received By-. TRANSFER RECORD (Please sign) - --.40- ganizadonOt 0 C OatelTime: 4 r" Organization: Date/Time• /ioe Organization: DatetTime: Organization: Datsl4e: &N , 01J3 +0 i°3". Organization: Dale/Time: •Organization: DateRlme; Oration: DatelTmre: Orgai atien: Date/Time: SAMPLE TRANSPORT Carrier: k7P--- TlaImport Method" /� ' eceivad 8y (Signature): .� i' 1` frill h, Steam RECEIPT AT LABORATORY -I'Trm Relinquished By .--...s• :'III! �"� ived 9 : Organization:er Organization- Date/Tirne• S /)j i DateRtme Z�" %,aq Unseated By: 'r�-� Annual Temp:, \ S • C sea* DisposedIRetumed By: Date: an bemW DOT concentrafbn tmila. r Ot0Z/0£/90 co COen 426 .en CO w m Eilvhronmen,aI. inc. 7T Mailing Address: P.O. Box 18414, Greenville. 5C 29808•7414 Shipping Address: 4 Craftsman Court, Greer, SC 29650 CHAIN OF LJSTODY FORM 1rsid- ti - • 03 ' cnip -l1.5 page L of L ir.+..,... twerp or r-va7S r.w: WWI, yr r-wwv ■ ul4 riw: %OW/ 121,711.41111.4, Email: matlOenenvironmental.com Facifty: CA-4 Q tieleflar14 VI kA-1TP GRAB SAMPLES Collected By (Pdnt): Signature: Date/The: ICO MROSlTE SAMPLE'S Set By (print):Su►ssn It 0 Ski KKCaliected by. . SeV Z {✓ S ture:1m.•. eo 1tn.. Signatu • 5tbArn1 IfY1 Daterme:r� �1t DatelTrme: S tt S lcq `23 3 1A Pr+equency rood aA triarztra$4le Chilled? 8 I No Site Description: l'?1�t� keno Cr%11 t SQrY14€. State: MC- , County: --tA.S NPOES ttoPik %t Pipe it:NN 1 EE�iT=: 3amplerif3 . , _• `, Gv- Q4to�I; :. ,t'.: 4a�8: `; .:ii�Iis';• A'�>:r � �+1!� .,;,���eSA?� , 7QItl� ` � '.: •v; . •, .., ::.. • is. '.: - �2rrarn . • � -- =, . . a ` .: � : �..: �_ • t' �? �;�: ;: CA 4 Gnmp 5)%101 NM NiS i.tscd i`Vont 04 4/, 33gofr avran t t. —Tati c t SAMPLE CUSTODY TRANSFER RECORD (Please sign) Sample Sealed By: Rehnqulobad Organization 1 ?C Date/Ti:ne: 511 e1M 83811YY% Received By: ;.A. Organization: %2 Datof irn :ffir firt 0/4-?SrReceived . Relinquished 8y: ' Organization: Date/Time: Received By: • Organiza!l'en: Date Time: mC 6 vot. txcii� Ra,, o 3 -44 1133 . Relinquished By: Organization: Data/The:0 Received By: Organization: OatelTime: Relinquished By: Organization: Datemrne: Received Sy: Organization: Date/Tfrne: SAMPLE TRANSPORT Cartier Tampon Method. By (Signahne): RECEIPT AT LABORATORY GOA Relinquished By: ��� •• ived By: . = ninth:in:LT Organization: / Date/Time: die�/ ,Da�/Tisne:=7- 'f y /y® Unseated By: fV.tia m �AMval Temp: 1.1 •C Semple (Reposed/Returned By: Cate: Noma concentrations are below DOT crn mth lion Iimih. OIOZ/0E/90 8E69LL8098 7a1N3WNO8 U1N3 113 TT nvironmentel, Inc. Melling Address: RO. Box 18414, Greenville. SC 29606-7414 Shipping Address: 4 Craftsman Court, Greer, SC 29850 Phone: (884) 977.6942 Fast O884) 877.6938 Toll Free: (800) 991-2325 EmaA: mail@ettenvireementaLcom W ' t Feciity: C1 � t �CY C,L441P Site Descriptions Eccitalikk COPIlfthiV State: Courtly: elf f NPoES *: etat l gi Pipe ii: bb • • •C4 r:: 5040 i tics CHAIN OF L.,STODY FORM Cla'Res Lt1-,\ 1.Qq —RA%) - L2•11-. • S Page 1 of GRAB SAMPLES Collected By (print): Signature: Datelilme: Program Area COMPOSITE SAMPLES Collected by:.�. S 5i.ef Signature Signature: (....).Adir DablTirr3e:511q WI 921 rim Date1Time: 5i21a" Q f4 Frequency: No c tmialCb hitlsd? / No Set By (print) : ..3'�' :rvtr• L rxx■/�yCy dS r^'r-i. rr NI tat -to, or Cirutwic . ldox.icL ag. SAMPLE CUSTODY TRANSFER RECORD (Please sign) Semple Sealed By: ethrgedshed B Received By: Relinquished By: Received By: Relinquished By: Received By: Relinquished By: Received By: a bition:C A.4 D Dale/Vine:S��D oc{ 1�0 ' ( l 15c ,nntAir- organization: atelTime:v�♦/ /AS Organization: Date/Tune: Organisation: Datefllme: Organization: Date/Time: Organization: Date/TIme: Organization: Organization: Preservation concentrations are berms DOT concentration 6rnits. Date1Time: Datefilme: SAMPLE TRA Carrier: import Method: i Received By (Signature RECEIPT AT LABORATORY Relinquished By: eceived B Organization: Or Oroar:Italian: 6 Degernme:.�.»° 4 v0 r--- IDateJTime:,,�i►Q' /4..b- Unseated By: Fa'e-' Andval Temp: a 3 •G Sample Disposed/Returned By: Days: • 8E69LL8P98