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Home My WebLink AboutNCG100036_2022 DMR_20220509NCDEQ Division of Energy, Mineral and Land Resources 5tormawater Discharge Monitoring Report (DMR) Forma for NCG100000 Used Motor Vehicles Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG10 0036 Person Collecting Samples: Keith Schronce Facility Name: Schronce Used Parts & Cars Inc. Laboratory Name: Pace Analytical Facility County: Catawba Laboratory Cert. No.: 12 Discharge during this period: E' Yes No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Yes nNo If so, which Tier (I, 11, or III)? 1 A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Byes 1:1 No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities - Benchmarks in (Red) Parameter Code Parameter Outfall 001 Outfall Outfall Outfall Outfall N/A Receiving Stream Class WS-IV N/A Date Sample Collected MM/DD/YYYY 04/05/2022 46529 24-Hour Rainfall in inches 0.75 C0530 TSS in mg/L (100 or 50*) 18.3 00400 pH in standard units (6.0 - 9.0 VFW, 6.8 - 8.5 SW) 00340 Chemical Oxygen Demand in mg/L (220) N/A Lead, total recoverable (as Pb) in 01051 mg/ L (0.075 FW, 0.22 SW) 0.0060 Ethylene Glycol in mg/ L (any amount 77023 detected Tier One; 8,000 mg/L Tier <5.0 Two and Three) 00552 Non -Polar Oil & Grease in mg/L (15) <4.9 NCOIL Estimated New Motor/Hydraulic Oil Usage in gal/month N/A Outtalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L EW (freshwater) SW (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee or Delegated Authorized Individual Date ariltia.@ ow nciftg foals, cow, a28- Email Address Phone Number aceAnaljftal www.paeslobs.com April 15, 2022 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 Dear Chuck Hoffman: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 06, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Indianapolis If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 at eAnaljftal wrw.pacelabs.eam Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 Pace Analytical Services Indianapolis 7726 Moller Road, Indianapolis, IN 46268 Illinois Accreditation #: 200074 Indiana Drinking Water Laboratory #: C49-06 Kansas/TNI Certification #: E-10177 Kentucky UST Agency Interest #: 80226 Kentucky WW Laboratory ID #: 98019 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS Michigan Drinking Water Laboratory #9050 Ohio VAP Certified Laboratory #: CL0065 Oklahoma Laboratory #: 9204 Texas Certification #: T104704355 Wisconsin Laboratory #: 999788130 USDA Soil Permit #: P330-19-00257 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnaljftal www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: SCHRONCE USED AUTO & CARS 92597592 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92597592001 OUTFALL NO. 1 EPA 1664B ICO 1 PASI-C EPA 8015 Alcohol -Glycol CPH 1 PASI-I EPA 601 OD CBV 1 PASI-A SM 2540D-2015 ZMC 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-I = Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 acmnalytical www.pacelabs.eom ANALYTICAL RESULTS Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL NO. 1 Lab ID: 92597592001 Collected: 03/31/22 13:00 Received: 04/06/22 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 16648 Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 04/11/22 04:00 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Pace Analytical Services - Indianapolis Ethylene glycol ND mg/L 5.0 1 04/12/22 15:57 107-21-1 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services - Asheville Lead 6.0 ug/L 5.0 1 04/08/22 02:19 04/11/22 23:43 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids 18.3 mg/L 2.5 1 04/07/22 16:33 Date: 04/15/2022 02:01 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnaljftal www.pacelabs eom QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 QC Batch: 690508 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92597592001 METHOD BLANK: 3608458 Matrix: Water Associated Lab Samples: 92597592001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 04/11/22 04:00 LABORATORY CONTROL SAMPLE: 3608459 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.5 78 64-132 MATRIX SPIKE SAMPLE: 3608460 92597737002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.5 19.0 74 64-132 SAMPLE DUPLICATE: 3608461 92597701002 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L <5.0 ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/15/2022 02:01 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 acemaIxicat www.pecelabs.com Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 QC Batch: 670810 QC Batch Method: EPA 8015 Alcohol -Glycol Associated Lab Samples: 92597592001 METHOD BLANK: 3089050 Associated Lab Samples: 92597592001 Parameter Units Ethylene glycol mg/L QUALITY CONTROL DATA Analysis Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Laboratory: Pace Analytical Services - Indianapolis Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04/12/2215:48 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3089051 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 31.0 124 39-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3089052 3089053 MS MSD 50313028001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 40.3 37.8 161 151 36-158 6 MO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/15/2022 02:01 PM without the written consent of Pace Analytical Services, LLC, Page 6 of 13 aceAnalXical trwle.pacelabs.tom QUALITY CONTROL DATA Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 QC Batch: 690140 Analysis Method: EPA6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92597592001 METHOD BLANK: 3606497 Matrix: Water Associated Lab Samples: 92597592001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 04/11/22 22:57 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3606498 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug/L 500 538 108 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3606499 3606500 MS MSD 92596637001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 489 492 97 98 75-125 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/15/2022 02:01 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnaIXical wrw.paeel�bs.eom QUALITY CONTROL DATA Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 QC Batch: 689941 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92597592001 METHOD BLANK: 3605282 Associated Lab Samples: 92597592001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 3605283 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 3606557 Parameter Total Suspended Solids SAMPLE DUPLICATE: 3606558 Parameter Total Suspended Solids Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 04/07/2215:21 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 248 99 90-110 92597433001 Dup Units Result Result mg/L 15.7 22.2 92597384001 Dup Units Result Result mg/L 307 253 RPD Qualifiers 34 D6 RPD Qualifiers 19 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/15/2022 02:01 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceftljftal www.pacolabs.com QUALIFIERS Project: SCHRONCE USED AUTO & CARS Pace Project No.: 92597592 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. Date: 04/15/2022 02:01 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 13 IaceAnaljftal" (�www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: SCHRONCE USED AUTO & CARS 92597592 Lab ID Sample ID QC Batch Method Analytical QC Batch Analytical Method Batch 92597592001 OUTFALL NO. 1 EPA 1664B 690508 92597592001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol 670810 92597592001 OUTFALL NO. 1 EPA 3010A 690140 EPA 601 OD 690272 92597592001 OUTFALL NO. 1 SM 2540D-2015 689941 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/15/2022 02:01 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 aC AnalOiCal Document Name: Sample Condition Upon Receipt SCUR Document Revised: November 15, 2021 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.08 Issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville aleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑ Upon pt Clien//t�I Name: Project tt: WO# : 92597592 Courier: ed Ex ❑UPS ❑USPS ❑Client II I II" III I III' ('I I'll ❑ Commercial ❑Pace ❑Other: Custody Seal Present? � ❑Yes L_.INo Seats Intact? ❑Yes -' ►o 92597592 Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap Bubble Bags ❑None ❑ Other Biological Tissue Fro n? Thermometer ❑rfR Gun ID: �-��, et ❑Blue ❑Yes ❑No N/A ❑None Type of Ice: Correction Factor: Cooler Temp: Add/Subtract (°Cj t� Temp should be above freezing to 6°C n ❑Samples out of temp criteria. Samples on ice, coolin¢ aracess USDA Regulated Soil ( N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, r1YPS nNa •••8 •••••o•• rvawmwpUrt:S UFVO Comments Discrepan Chain of Custody Present? Yes ONo N A 1. Samples Arrived within Hold Time? ides [:]No N/A 2. Short Hold Time Analysis c72 hr.)? Oyes E< ONIA 3. Rush Turn Around Time Requested? Yes o N A 4. Sufficient Volume? es ONO ' N/A S. Correct Containers Used? -Pace Containers Used? EYq es ON. ON. ❑N/A N/A 6. Containers Intact? Yes No ONIA 7. Dissolved analysis: Samples Fleld Filtered? OYes ONo /A B. Sample Labels Match COC7 -includes Date/Time/ID/Analysis Matrik: L� es ❑No ❑N/A 9. Headspace in V0A Vials >5.6mm►? Yes ONO PEA 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes OYes QUO.— ONo N/A A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? []Yes []No Page 11 of 13 Document Name: Document Revised: November 15, 2021 n Sample Condition Upon Receipt ISCUR) Pape 2 of 2 Document No.: Issuing Authority: r3CBAll3ij/ttCc7� . F-CAR-CS-033-Rev.09 Pace Carolinas Quality Office *Check mark top half of box If pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottles WO#:92597592 PM: TIH Due Date: 04/20/22 CLIENT: 92-MID ATLAN ? v u a d vaJ yi DW N v d v .a. ca M1 C N _ ~ V 8i 2 i = S V _ Z 1 Z Z v Y! Z 1✓ 1 1 �. y 9 CL n C > r n S m i U N 20 Z 1y(d W ZCL U CV11 C ij e� S y Q ¢ ? O N %A 2 do z \ > U U ^ z -I AD N n a 9 d d ay A I3 S n J a d q a E g E a E E ¢ Z E E Q E < O Z ¢ O x D .c c :: Q d E Ln E ppE Y J E N E J E :N J vNE1 N 3 , QE N pE Y1 '' O J E J O E .�B i _A E in '1 E O 1 29 E O pE O N O 6 6 6 6 DD Q. m d m G to 6 m 3 �— t i Q M Q a a > 01 > 1 > > & V1 m a Q 1 d X" J121 31 1 4 1 N-\\\ .1 5 6 . 7 8 I \\N\ 9 I \J\N\ -.L N\\ I 10 \\N\ N\ 11 \\[\\d 12 N N\NT�---�s--LLN pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot A Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy or this form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 12 of 13 30 am N N Received on 0 @ Ice (Y/N) 0 w N Custody Seale( b Cooler (YIN) N r 0 I Samples Intact (YIN) RIMFEM i 0 a r 0 3 z N '4 - I- IA I- I- I- IITEM # C n m O a 3 n � m (n 00 oDD 3 N p m'm m� v O z m ° 1 p m P O A j y A Iiy d S N ti F I� 6 x yma� X a � M m 0 MATRIXCODE I--11dwd.totee) 0 SAMPLE TYPE (G=GRAB C=COMP) u o a S, m N 1� `.� m H n O M W n poTy� rn rn gZZZ U } m m SAMPLE TEMP AT COLLECTION ti # OF CONTAINERS HCl NaOH NazSZO, Methanol (Method 1664) ene Glycol , Total Recoverable Residual Chlorine (Y/N) D v 2 N � d m iu m v O O y O 0 z v Dn c M Cn m 0 B o A A ED a o CD 93 G Pr �, 0 z fD H 0 N 0 a o n' O (7 N N K <. o. o g i� C 10 M a) O C 01 o dnt 3 1D 0 N 0 3 � L �z S 5O 3 8 n n m 01 C m� v 3 v z -0< s a 3 aa'O a a o a - z 60 p 0 i _Z 1 $ D o c ,= z D N 0 G O i 0 m 1O m D < fy < < d N _ O b C n 0 EL TT N N ? ni 3 CD NN 3 U 0 CD n n 0 M C m C a y a ti v S m �c M mW m a M z n..D.._.O A O Z v ... 13 of 13