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Home My WebLink AboutNCG080839_2022 DMR_20220505 (2)aceAnalytical www.paealsbs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 March 31, 2022 Kaline Davis Covanta Environmental Solutions 2503 N. Fayetteville St. Asheboro, NC 27203 RE: Project: OUTFALL 1,2,3 3/24/22 Pace Project No.: 92595570 Dear Kaline Davis: Enclosed are the analytical results for sample(s) received by the laboratory on March 25, 2022. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, 4K- 4---- Tyler Forney tyler.forney@pacelabs.com (704)875-9092 Project Manager Enclosures cc: RANDY ATKINS, COVANTA ENV. SOL Vicki Zamudio REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: OUTFALL 1,2,3 3/24/22 Pace Project No.: 92595570 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 Ml aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 SAMPLE ANALYTE COUNT Project: OUTFALL 1,2,3 3124/22 Pace Project No.: 92595570 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92595570001 OUTFALL 3 EPA 1664B ICO 1 PASI-C SM 2540D-2015 MAB2 1 PASI-A EPA 9040C YEG 1 PASI-A 92595570002 OUTFALL 2 EPA 1664E ICO 1 PASI-C SM 2540D-2015 MAB2 1 PASI-A EPA 9040C YEG 1 PASI-A 92595570003 OUTFALL 1 EPA 1664B ICO 1 PASI-C SM 2540D-2015 MAB2 1 PASI-A EPA 9040C YEG 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 aceAnalytical www.pacolabs.corn Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 ANALYTICAL RESULTS Project: OUTFALL 1,2,3 3/24/22 Pace Project No.: 92595570 Sample: OUTFALL 3 Lab ID: 92595570001 Collected: 03/24/22 14:03 Received: 03/25/22 11:43 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 03/29/22 01:00 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Asheville Total Suspended Solids 6.7 mg/L 2.5 1 03/27/22 11:52 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 7.2 Std. Units 0.10 1 03/30/22 11:59 H3 Sample: OUTFALL 2 Parameters Lab ID: 92595570002 Collected: 03/24/22 14:10 Results Units Report Limit DF Received: 03/25/22 11:43 Matrix: Water Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 03/29/22 01:00 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids 11.4 mg/L 2.5 1 03/27/22 11:52 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 7.4 Std. Units 0.10 1 03/30/22 12:03 H3 Sample: OUTFALL 1 Lab ID: 92595570003 Collected: 03/24/22 14:20 Received: 03/25/22 11:43 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 03/29/22 01:00 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids 14.7 mg/L 2.5 1 03/27/22 11:53 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 7.2 Std. Units 0.10 1 03/30/22 12:14 H3 Date: 03/31/2022 01:17 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 ace Analytical www.pacolabs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Project: OUTFALL 1,2,3 3/24/22 Pace Project No.: 92595570 QC Batch: 687557 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92595570001, 92595570002, 92595570003 METHOD BLANK: 3593962 Matrix: Water Associated Lab Samples: 92595570001, 92595570002, 92595570003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 03/29/22 01:00 LABORATORY CONTROL SAMPLE: 3593963 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 14.3 72 64-132 MATRIX SPIKE SAMPLE: 3593964 92595540001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L <4.8 19.2 11.6 58 64-132 M1 SAMPLE DUPLICATE: 3593965 92595523001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03131 /2022 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 ,�aceAnalyfica( www.pacelabs.com QUALITY CONTROL DATA Project: OUTFALL 1,2,3, 3/24/22 Pace Project No.: 92595570 QC Batch: 687550 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92595570001, 92595570002, 92595570003 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 METHOD BLANK: 3593928 Matrix: Water Associated Lab Samples: 92595570001, 92595570002, 92595570003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/27/22 11:51 LABORATORY CONTROL SAMPLE: 3593929 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 260 248 95 90-110 SAMPLE DUPLICATE: 3593932 92595538002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 133 112 17 SAMPLE DUPLICATE: 3593933 92595543002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 58.3 63.3 8 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/31 /2022 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 aceAnalytical www.pacalablixont Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Project: OUTFALL 1,2,3 3/24122 Pace Project No.: 92595570 QC Batch: 688194 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92595570001, 92595570002, 92595570003 SAMPLE DUPLICATE: 3596612 92595145001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.2 7.6 0 H3 SAMPLE DUPLICATE: 3596613 92595570002 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.4 7.4 0 H3 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/31 /2022 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALIFIERS Project: OUTFALL 1,2,3 3/24/22 Pace Project No.: 92595570 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/31 /2022 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OUTFALL 1,2,3 3/24/22 Pace Project No.: 92595570 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92595570001 OUTFALL 3 EPA 1664B 687557 92595570002 OUTFALL 2 EPA 1664B 687557 92595570003 OUTFALL1 EPA 1664B 687557 92595570001 OUTFALL 3 SM 254OD-2015 687550 92595570002 OUTFALL 2 SM 2540D-2015 687550 92595570003 OUTFALL 1 SM 254OD-2015 687550 92595570001 OUTFALL 3 EPA 9040C 688194 92595570002 OUTFALL 2 EPA 9040C 688194 92595570003 OUTFALL 1 EPA 9040C 688194 Date: 03/31/2022 01:17 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 9 of 12 Document Name: Document Revised: November 15, 2021 aceAnalyiieal Sample Condition Upon Receipt (SCUR Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.08 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville E] t Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville7l Sample Condition Client Name: WO1t • 92'3595570 Upon Receipt Project # � I III Courier: Fed Ex ❑UPS ❑USPS []Client II I II' I Ilil III I II I ❑ Commercial .]Pace ❑Other: 92595570 1 Custody Seal Present? []Yes 'QNo Seals Intact? ❑yes �o % z Date/Initials Person Examining Contents: �'� �` ✓14l ZZ Packing Material: , %ubble Wrap 186ubble Bags ❑None ❑ Other Thermometer. {Vet ❑Blue IR Gun ID: Type of ice: f Correction Factor: / Cooler Temp: (L t Add/Subtract (°C) l .` - Cooler -Temp Corrected ('C): 1, J USDA Regulated Soll ('0 N/A, water sample) Did samples originate in'a quarantine zone within the United States: CA, NY, or SC (check maps)? nva. nti. Biological ,Tissue Frozen? ❑ 4' DY-es— aryu-�/A Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process Did samples originate from a foreign source (internationally, Comments/Discrepancy: Chain of Custody Present? Yes No N/A 1. Samples Arrived within Hold Time? es []No N/A 2. Short Hold Time Analysis (02 hr.)? Yes No N/A 3. Rush Turn Around Time Requested? []Yes 1:]-No N/A 4. Sufficient Volume? s QNo N/A S. Correct Containers Used? -Pace Containers Used? 'aes thes (:]No ❑No [-]N/A ❑N/A 6. Containers Intact? 4es ONO N/A 7. Dissolved analysis: Samples Field Filtered? Yes []No HlajA 8. Sample Labels Match COC? Includes Date/Time/ID/Analysis Matrix: '-,O'es iA, ❑No [)N/A 9. Headspace in VCIA Vials (>5.6mm)? Yes No N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes LJYes 'oh c, LJNo ❑N/A []K/A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time. Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date: Date: Field Data Required? ❑Yes ❑No Page 10 of 12 Document Name: Sample Condition Upon Recell Analytical Document No.: f •-CA R-CS-033-Rev.08 *Check mark top half of box If pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of pax is to list number of bottles Document Revised: November 15, 2021 Page 2 of 2 Issuing Authority: Project WOI* : 92595570 PM: A'rF Due Date: 04/01/22 CLIEN'r: 91-COVANTA V W y U U Z Q _ OM V a Q 2 ? Z Z Z \ N Z C Z ^ N Q 4 Z M M 13 Z y r N 2 a C a M u a 2 A W v p q ` \ Z M a �f Y rn a \ Z Y 2 U N N —�_ C --_ _ C U_ M Q N Vf 2 -Q ? _- S — �� L Z c c O —C C 2 N Z M 2 N u N 6 e 1 .%� y_. 'w a w a V a M, y _A .Y =° a Y ',Y„ 3 L o C y a E `y a E E ¢ a E E a E N N i Q O Z ¢ O Z Q O S ¢ O Y y a 61 �, 0! y m M D E Q = c N M E J E J E J d v d E J E a E d E E a Q a Q J Q a„` J E M % E > E > E > E N ° u+ u7 E J E V1 E Q E Na N pE g N N �N/� N ry of N If .1 4 4 _— Q If ry of N $ 0 90 E a m M m N m 14 m Q m M O m g 3 e+ 0 .r O M 0 rl l7 M M 0 01 � a Ot t7 01 IM t7 O O G \ > M a N a 0 Co m a a a a a a > > > &A v, m a > o 1 i � Z 2 3 4 5 6 7 8 9 10 11 12 I _J pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot li Note: Whenever there is a discrepancy affecting North Carolina compllance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (I.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 O Q J z 0 uj m 5 c N Ea u O a v - a � a Q d n E U u z m c u Q o 0 w J H 1O L O V LL � C? u o z Q m V u c 0 m V) W V C C a E u° �zzzzzzz�.�zz z z ' zzzzzzzzzz z z � u u ti �'- 2 N U H N a a ro a s N N a a w u u E N ~ N u �. N _j u C a. w a N N W a •• A c o v E u N N 4 0 u 4 r. c ° w L A a E cu c E v m° d a c ro N a v a b a u u u° N 01 U N O •ti ro a 0 0 Q' .� C •N ro u 7 a a v 2- u u a m a •• L E� u C z m Qt V1 L u U N m L 4 a u aa• c0Lav cu.. wro �za p ON = O E >. >• O N u.ai N x a N ro� -•+ a U �0 'O 'O U a U u a ix a 7 w a H 'O 4 •O W E (''�� 4 m\ ", 5 N t/ d v$ 0. to O O a .-� a -•� r+ •-� u .+ u .+ u u.+ u ww a Q a-•+w av)w'O A m N, u w w E 4 0 E N E N A A ti f0 r0 77 0 0 0 7 m CA ro a '+ m S 7 U u m u vl (n a En PL V N a th -^ u y 0 c A W L 0 V n O V 4 v' — -- -- - --- - -- — O a - h M0 c N � a` E n I VT ° — 0 10 c 0 U > f0 T � m Y a c L E a w I a m U a N u 6 N CT cc �o 0 O n G E u 0 O 0 010 E t1 a Or'i o u o _ ly 0 u z ro°o •f a z 14 i a 2 o N a m a }l 0 m ° 4 E a as 0 v —. v �.� H 'O > .. C w °a U u x y u 7 U O u u Ev^; a N K Y A Z a E a w wstaFu° c E \ aroO.+ r m a a= c w E E a a a a c E -pp O E O ..0 7Hi 88 z _7 E. F u u u U r/ z '�\\ j\z c n a j 0 0 d a o L u 110 Q_IT n. d N n w �o /V f^ w ut o " ,o v = E E E o Y " tro t M ) ¢ F a 0 OM 0 rrN 0 N N J fE0 V1 a m m m i f n x �n E E E 8 V1 D -D > > C V V V `3 � z N N ) M � M � E E E• O M Io O v1 a 9 >' c c m m m in in in c c c N L C K K G _ 0 a10- ---