NCG090034_2022 DMR_20220504

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PaceAnalyfical
Report of Analysis
INOLEX
12345 Steele Creek Rd
Charlotte, NC 28273
Attention: Alanna Smith
Project Name: Stormwater
Project Number: INOLEX, Inc.
Lot Number:XD06073
Date Completed:04/21/2022
04/29/2022 4:13 PM
Approved and released by:
Manager: Michael L. Kilpatrick
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
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PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
INOLEX
Lot Number: XD06073
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Non -Metals
Sample XD06073-001 Hexavalent Chromium - The laboratory control sample (LCS) and contiuning
calibration verification (CCV) for analytical batch 37554 exceeded acceptance method criteria. The result
was biased high and were not detected in the sample. The continuing calibration verification (CCV)
associated with sample was outside of method criteria. Hexavalent Chromium was not detected at or
above the LOQ, data has been qualified with a U accordingly.
Inorganic Metals
Sample XD06073-001 ICP-MS Metal sample had turbidity present, the sample was diluted at 5X to
protect the integrity of the instrument. The LOQ has been elevated to reflect the dilution. The ICP-MS
Metals for Cd, Cr, Pb were not detected at or above the LOQ, data has been qualified with a U
accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvww.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
INOLEX
Lot Number: XD06073
Sample Number Sample ID Matrix Date Sampled Date Received
001 SW1 Aqueous 04/05/20221800 04/06/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES, LLC
Detection Summary
INOLEX
Lot Number: XD06073
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SW1 Aqueous TSS SM 2540D- 120 mg/L 5
(1 detection)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Inorganic non-metals
Client:INOLEX Laboratory ID:XD06073-001
Description: SW1 Matrix: Aqueous
Date Sampled:04/05/2022 1800
Date Received:04/06/2022
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
3
(Hexavalent C) 218.6
1 04/19/2022 1635 YCB
04/06/2022 1747 37384
1
(pH) SM 4500-H B-2011
1 04/17/2022 1909 NBW
38414
1
(TSS) SM 254OD-2011
1 04/12/2022 1916 CVR
37912
Parameter
Hexavalent Chromium
pH@15.4°C
TSS
CAS Analytical
Number Method Result Q LOQ Units Run
18540-29-9 218.6 0.30 U
SM 4500-H B-20 5.7
SM 254OD-2011 120
1.0 ug/L 3
su 1
17 mg/L 1
LOQ = Limit of Quantitation V = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % 1 = Estimated result < LOQ and > DL L = LCS/LCSD failure
Q = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

ICP-MS
Client:INOLEX Laboratory ID:XD06073-001
Description: SW1 Matrix: Aqueous
Date Sampled:04/05/2022 1800
Date Received:04/06/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 04/12/2022 1631 BPK 04/09/2022 0609 37421
Parameter
Cadmium
Chromium
Lead
CAS Analytical
Number Method Result Q LOQ Units Run
7440-43-9 200.8 0.63 U
7440-47-3 200.8 6.3 U
7439-92-1 200.8 1.3 U
2.5 ug/L 1
25 ug/L 1
5.0 ug/L 1
LOQ = Limit of Quantitation V = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % 1 = Estimated result < LOQ and > DL L = LCS/LCSD failure
Q = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Cdecldkst (MCI �MIOOUC-15) Ravi ed:s,1V2e.lan
Isyuirrg Authority; Pace ENV - WCOL P�3 16f 1
Sample Reedpt Cbeckiist ( RQ
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mmtls armcdip[; J pacco Client �] llldS Fed�ai Cldter
Y-1 Jl K(J I, iVvre custody scats presonccn the coo16r'!
F-jYo5j'No � NA4 2. If custud� seals were prescilt, wem the IILIUGL U10 LLbruk�;n?
N SIrip ID: *I' .. - Chlorine SI:'ip ID-. w,} 'I'eslad--
'ij'intJ ttmpsrimra upon receipt r Derived (Corrected) icmpuratun: lipvn mcoipt %Solid Snap -Cup ID: {`
3.3 13.3 cG NA j HA cC NA f NA a NA { VA uC
h'ic#hod; FJ]TemMml1:n-a lllank Q4&airlst Bottles fit Gwl ED: 5 IR Fw jur: 0 °C
Method of -oolam, 0 Wd Ivc ❑ luu Packs ❑ Dry Ice ❑ Nor e
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3. Ifttemperature of any U-bl-Or exccedcd 6.0"C, was Pl-aject Manager Noiifed?
1'M was Notifled bV= ph rlel email l face ro-face fcircla one}.
Yes
No
IZJ.NA
4. Is the cominerc.ial o0ur_er'F; pnekin T"slip xrt,r.had to this form?
21 Yes
No
5. Were pmperopstvp procedure (-cI:r:t:uishcdlm--civcd, fol+owed7
5. Were -sample If}s li�ltM nn the COO?
7. Weresa,nple IDs Iistedun al umplccontpincrs7 -
V Ycs
Nn
+ Yes
[IN01
/ Yes
El `Jo;
3, Was rallec:ion da,e & litrw listed Ou rho COC?
YLS
NO!l
;�. 1'dBScol ICC-imi-dwe&Iinie1ig1edarialI9ample:ufmviiTiers?
110. Did alJ container label infbTwation %'ID, dnir, timr) agree with thq- IXIC 7 --
Ves
❑�Ja
. Yrs
NO
1 I . U+-rc tc:t9 to be perform6d lis,.ed on tho COC?
0 Y�s
❑ No
12. Did ail samples arrive In fte pmner Con Laincrs frw each tw andlor i,l good co;rci_=on
u39133-nkan, li;lu can, r.tc.)?
Y25
No
13_ Was aftivAto sample volume available?
Yes
�ltf
I4_ Ware A11 " n-jIFL%received wMidn'A the hoEdino time or 48 hot:M. whirheveT comes firs'
Yes
U No
15. Ware 2131 uimteiruars missineclnecss (curcla one) ssm-nles Na listed txi COC?
❑Y r
❑Ntl
l hiA
....
16. For VOA anc RSK-175 samples, were bubbles prCSCnt>'pca-size" ('la:'or6nun in diarnete_)
in any cr ttte VOA viaL�.'
4 'esLl
No
LJNA
17. Were rill D R(Vmei a l slnanierrt .sam pies received at a pH oC < 2?
'LJ
No
kITEA
19- WeM Al oyani& earn Plus TEMived at a pH', 12 aad sul fide sarnpl es received di L pH
❑ Yac
❑ No
DNA
• Were g3E3I1=IJJc N14y7KNIL!ymni,i.:lpheno r .3, .!6 8.3 (< 0.SmVL) samples free of
rosidual Chlorine:
Yes
El -No
ENA
20. 'Werc cli-rtt rcmQrksl'rcqucsrs (F-e_ INIIe�ted diI1Elinnc, 1riZWSf] drsigtritions, Ctr....)
correcl# mucri had tmnt the CDC in In fie: rnm,,rmt maim in 11Fr1S
❑ `!e5 I
L!fNDI21.
l�k'ag the U076 ttUrnber listc�l on i`hc :oinaiuc: lobe]? IFyc�, �uatc #
*ampJe i'rewervaf n n (Mimi be cnmpl n.W for uny satnplels) ial �urectl}• presen�ed ar �a ii]1 lseadSp�e 1
wem receiver'_ i7corteetly and wgrc 8djusted aecordingJy
I Sample mueivilig wit}t NA tnL of c[rcle Dne: H2SO4, HNO3, I IC1, NaO14 using SR # NA
ime pf prqserval oa NA --- I €;Wore than o u przzwrudya is needed, please tt,ow in Cho commonts bciow_
arnp]a(5) ] A - WU-15Teceived with huhHes>5 Inln in diarneitr.
amples(s) ' were relxived with TRC> 0,5 ina (If 919 b ATV) and were:
3jusicd accordingly in sample immiving with seditun tltiosuI%W (N32S3O3) with Sticaly 1D; I`A
19R 1h n.0rJr Ixbals appked 0y; 15INK _ Datc. OU0fialaz III
C;onur.ents:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9