NCG100023_2022 DMR_20220503

NCDEQ Division of (Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG100W
Used Motor Vehicles
Click here for instructions
Complete, sign, scan and submit the OMR via the Stormwater NPDE Permit Data Monit rin Report MR Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate EMLR Re ional Offrc .
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
outfall 001
OutfaO 002
Outfall 003
outfalf
I Outfall
Code
N/A
Receiving Stream Class
WS III
WS ill
WS III
N/A
Date Sample Collected MM/DD/YYYY
0311W2022
03/16/2022
03116/2022
46529
24-Hour Rainfall in inches
0.85
085
0.85
C0530
TS5 in mg/L (100 or 50•)
5.5
19.0
140
00400
pH in standard units (6.0— 9.0 FW,
7.31
7AS
7.26
64 — 5,5 S
00340
Chemical Oxygen Demand in mg/L
< 25.0
25.0
< 25.0
(120)
01051
Lead, total recoverable (as Pb) in
0.0104
0-0128
D 0105
m L 10.075 FW, 0.22 S
Ethylene Glycol in mg/ L (any amount
77023
detected Tier One, $,ODD mg/L Tier
<5.0
<5.0
<5.0
Two and Three)
00552
Non -Polar Oil & Grease in mg/L (15)
e5 2
< 5.1
K 5.1
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gallmorith
N/A
NIA
NIA
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nurwy Areas (PNA)
have a benchmark TSS limit of 50 mg/t. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater)SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submittmg
false YAinf rin sibili con, in tiding th osof fines and imprisonment for knowing violations."
z
Signature of Aermittee or Delegated Authorized Individual Date
`)CLrts�iVtC"yolyllOno 6 0 oM �36-49�-�792
Email Address Phone Number

aceAnal)ftal'
:� Mnlelscsa
March 29, 2022
Chuck Hoffman
Mid -Atlantic Associates, Inc
409 Rogers View Court
Raleigh, NC 27610
RE. Project: M&M MOTOR COMPANY R2045.b0
Pace Project No.: 92594257
Dear Chuck Hoffman_
Pace Analytical Swvtcn, LLC
arioo Ktstcey Are smote tat
Muniammille. NC 2a07P
(70447°r9ow
Enclosed are the analytical results for sample(s) received by the laboratory on March 18, 2022. The results relate o* to
the samples Included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's quality Manual, where applicable, unless otherwise noted In the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network-
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
i--
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Ron Davis, Mid. Atlantic Associalees, Inc.
REPORT OF LABORATORY ANALYSIS
Thin repo; 9h,a+ not tw reproduced excerl m fw.
wehout the written Consent of Pace Analytcal SeMCes.- LLC
Page 1 or 17

Paso Anayhoal S*rvtcea, LLC
1!2ce " ICBi "W A,m sw.,00
tarerrsnas roc Zwra
aw: I704 }07&4M
CERTIFICATIONS
PresleCl M1l,M MOTOR COMPANY P2005 00
Pace prtgw No 92SW257
Paco Analytical Services "onapolls
7726 Maker Dead Ind,anapo". IN 46268
I14nas Acomd•tat on N 200074
kitkana Dnnkrng Water Laboratory N C49-M
Kansas/TNl Cmufcauon N E-10177
Kariucky USTAgency int"vi N 80226
Kontuehy VM Laboratory ID 9 99019
Pau Analytical Services Charlotte
South Ca visna Laboratory ID 99006
98W K!r*cey Ave Ste 100, Huntersvi"o NC 28076
North Caroirta Dnnkrng Water Cert,fcahon N 37700
North Carolina Field Seorvtoes Certification N 5342
North Carolina Wastewater Certification N 12
South Caro>ina Laboratory ID 49W5
Pace Analytical Services Asheville
2225 Rvers,de Drove. Ash+v!Ne, NC 2880A
FloridarTlEL.AP Carufcabon N E0760
North Camkna Dnrl" Water CoMficatloe.. N 37712
North Caroiina Wastewater CoMficalron N 40
M! j*pn Dr:nk,n0 Water Labvnlory #W5O
Otwo VAP Cer4 and Laboratory N GL0065
Okinhoma LaboratoryN 9204
Tema Gertlrrcataon N T104704355
Ww.*rxrn Laboratory A 999788130
USDA Sol -Permit N P330-19-W257
South CaroNna c4mf cauon N 29006W1
South Cam" Dank" Water Cart N 9900Pi003
Flooda,'14EIAP Ced&catlon N EI17627
Kentucky UST Certiflcahon N 64
Louisiana DoN Drinking Water N LA029
V,rgxwaNELAP C*9Alca<6on # 460221
S&A Carmine Laboralory fA 9W30
South Carding Cerufpcation N 99030001
VirgimaiNELAP Cartf"kon N 4,60222
REPORT OF LABORATORY ANALYSIS

CeAnaocalg
l
SAMPLE ANALYTE COUNT
fate An•Iylteal a*rv,eae, LLC
9fl00 r'J"f Avg ravte 100
HurterwilN. NC 2a018
(7P41875.9092
Prolecl,
MdM MOTOR COMPANY R2W5 00
Parrs Project No
92SM257
Analytts
Lab 10
Sample 10
Method
Analysts
Reported
Laboratory
92594257001
OUTFALL NO 1
EPA 1664E
lCO
1
PASI-C
EPA tot5Alcohol-Glycot
CPH
1
PASI-1
EPA 200 7 Rev 4.4 1994
KH
5
PASI-A
EPA 60100
CRW
1
PASI-A
SM 254OD-2015
MAE2
1
PASI-A
SM 522OD-2011
JP1
1
PASI-A
92594257002
OUTFALL NO 2
EPA 1664E
IGO
1
PASI-G
EPA 6015 Alo"-Glycol
CPH
1
PASI-1
EPA 200.7 Rev 4 4 1994
KH
5
PASI-A
EPA 60100
CRW
1
PASI-A
SM 254OD-2015
MA132
1
PASi-A
SM 522OD-2011
JP1
1
PASI-A
92594257003
OUTFALL NO 3
EPA 16646
1CO
1
PASI-C
EPA 80 15 Alcohol- Glycol
CPH
1
PASI-1
EPA 200 7 Rev 4.4 1994
KH
5
PAS$ -A
EPA60100
CRW
1
PAS"
SM 2590D-2015
MA82
1
PA& -A
SM 522OD-2011
JP1
i
PAS"
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-1 = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
This sh,V rkN be 'eplud--el e.,�evl in toil
w:i4n,S Hv c—se�.l e7 Pace Anat�", ral Services LLC

Cel4i7��f�;a! e
+ wa�lssieiawr
ANALYTICAL RESULTS
Racy Analyteal Servfcee, LLC
9e00 +WCy Ave SU*@ 100
HarswwAe. MC 20D79
(704)IM2092
Protect M&M MOTOR COMPANY R2005 00
Pact Prmect No 925MZ57
Sample COUTFALL NO 1
Lab ID 92594257001 Cw`.lected 0311t3122 17 18
Recowed 03118122 1100 Mallu Walla
Parameters
Resulls Ur.its Repots Lunn
DF
Prepared Anatped CAS No Dual
Field Data
Analy>aeel Mellhod
Pad Analytical Services - Cnarlolle
Performed by
Mld
1
03128172 15 00
Atlantic
Collected By
Heath
1
03I28122 15 00
McCaskill
Collected Data
0311=2
1
0312&22 15 00
Collected Time
17:13
1
03r21122 15 00
pH
7.31 Slid Units
1
03 W22 15:00
Rainfall
0.85" Indies
i
03128r2215:00
1664 SGT-HEM, TPH
Analytical Meltwd.. EPA 1664E
Pace Analytical Sermes • Charlotte
Total Petroleum Hydrocarbons
ND mg'- 52
1
03r21M 10.00
e015M Glycols In water
Aralyt" Method EPA 8015AkAhol-Glytol
Pace Analytical Services - Indianapolis
Ethylene ytycoi
ND mp1L 5 0
1
0312522 18 00 107.21-1
200 7 MET ICP
Analytical Method EPA 200 7 Rev 4 4 1994 Preparation M0010d EPA 200 7 Rev 4 4 1994
Pace Analytical Services -Asheville
Cadmium
ND 119"t f:0
1
03119/22 18 47 03121/22 22 58 7440A3-9
Copper
39.3 u91- 5.0
1
03119122 1847 0312i122 22 58 7440-50-8
Iron
1630 UVL Soo
1
03119122 18 47 03121122 22 58 7439-89-6
Lead
10.7 uW1. 5 0
1
=19W 18 47 03121122 22 58 7439-92-1
Zinc
33.9 uglL 100
1
03J19122 18 47 03121#22 22 58 74.40-6"
6010 MET ICP
Analytical Method EPA 6010D Preparation Method EPA3010A
Pace Analyl<cat Services -Asheville
Lean
10A ugrL 50
1
03123122 00 35 03123/22 12 16 7439-92-1
2S40D Total Suspended Solids
Analytical Method SM 25400-2015
Pace Analytical Services -Asheville
Total Suspended Solids
5.5 mg.L 29
1
03119r22 1100
5220D COD
Anayical L4ethod SM 52200-2011 Preparation Method SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg.+L 250
1
03125122 01 28 03125122 04 33 M1:R1
Date v3%2%2022 04 10 PM
REPORT OF LABORATORY ANALYSIS
This report snail rwil be reproduced, except n fi:
wrtnoul The written cnnxerrl or Pace Ana#yl�cal Services. Lc G
Page 4 of 17

�.. aceArlatytical'
e�r+tlacr/a4sa
r
ANALYTICAL RESULTS
Face Analytical Servicaa, LLC
9" ttxuay Ave SuAm 100
Hunreraviae NC M?s
1704 WS-W92
Protect. MdM MOTOR COMPANY R2005 00
Pace Prated No 92594261
Sample OUTFALL NO 2
Lab ID 92594257002 Collected 0306122 17 29
Received 0311 b122 11 OD Matrix Water
Parameters
Results Una& Report L mK
DF
Prepared Analyzed GAS No, Qttal
Field Data
AnalyLcal Me01ad
Paco Arialytmal Serices - Charlotte
Performed by
Mid
1
03P2W22 15 i6
Atlantic
Collected By
Heath
1
03121122 15 18
MCCasklll
CotlWed Date
03/16122
1
03t W2 15 t8
Coilerted Ttme
17:29
7
03tZOW 15-18
PH
7.48 Std Units
1
0328221518
1664 SGT-HEM, TPH
Analytical Method EPA 16849
Pace Anilytical Services - Charlotta
Total Petroleum Hydrocarbons
NO mg.11- 5.1
1
01r2V22 1000
8015M Glycols In water
Analytical Mew EPA 8015 Alcohol -Glycol
Pace Analyt cal Services - Ind,anapohs
Ethylene glycol
NO mg'L 50
1
03125M 16 09 107-21-1
200 7 MET ICP
AnaMical Method EPA 200 7 Rev 4.4 1994 Preparstm Malhod: EPA 200.7 Rev 4.4 1904
Pace Analytical Services-Ashawlle
Cadrruum
ND u9V1 1.0
1
03119,/22 1847 0312t122 23 01 7440-439
Copper
68.4 U91L 5.0
1
03AW2 18 47 03R1122 23 01 74404M
Iron
2050 UW1 So 0
1
03/19/22 16 47 03t21122 23 01 7439- "
Lead
13.5 U9111- 5.0
1
0311922 11147 0321122 23 01 7439-92.1
Z.nc
38.4 UA too
1
03/19/22 18 47 03121/22 23 01 7440-66-6
601D MET ICP
Ana lytica I Method EPA 601OD PreparaWn Method EPA 3010A
Paoe Analybral Services -Asheville
s e'xcl
12.9 uglL 5 0
1
03123122 00 35 0312322 12.37 7439-92-1
2540D Total Suspended Solids
Analytical Method SP.4 254OD-2015
Pace Analytical Services -Asheville
Total Suspended Solids
19.0 mgll 27
1
03119122 1100
52200 COD
Analytical Method SM 52200-2011 Preparation Method SM 52200-20It
Pace Analytical Services-Ashev4e
CherrecW Oxygen Demand
NO mVL 25 0
1
03125M 01.28 03/25122 04 34
REPORT OF LABORATORY ANALYSIS
Date. 0W912022 04 10 PM

aceAna0cal,
ANALYTICAL RESULTS
Pace Analyttcel SoovIces, LLC
"M t(tnaey Ave Suft 100
HurmtrAw. NC ZW79
dtD4her�9oe2
Proiecl.. MSM MOTOR COMPANY R2005 00
Paea Project No 92594257
Sample QUTFALL NO 3
Lab ID° 92524257003 Cotlecled 0311W2 1742
Rrceved 03M0)22 11 00 MatrixWater
Parameters
Results Units Report Limit
OF
Prepared Anatyzed CAS No. Qual
Field Data
Analyt,cal Method
Pace Analytcal Services - Charlotte
Performed by
Mid
1
0312&22 15 18
Atlantic
Collected By
Heath
1
OWN22 15.18
McCaskill
Collected Dale
0311V22
1
03128122 1S 18
Collected Tme
17.42
1
0312812215.1IS
PH
7.25 SW Units
1
03T2812215 18
1664 SGT HEM, TPH
Analytical Method EPA 16648
Pace Analytical Servtees - Charlotte,
Total Petroleum Hydrocarbons
ND rngil- 5.1
1
0312N22 10 00
4015M Glycols In water
Analytical Method EPA 8015 Alcohol -Glycol
Pace Analyl�cal Services - Indianapolis
Ethylene glycol
ND mgiL 5.0
1
0325122 16.18 107-21-1
2D0.7 MET ICP
Analytical Method EPA 200 7 Rev 4.4 1994 Preparation
Method_ EPA 200 7 Rev 4A 1994
Pace Analytical Services -Asheville
Cadmium
ND ugL 10
1
03119,122 18 47 03121122 23 04 744"3-9
Copper
940 ug;L 5.0
1
0311922 18 47 03/21122 23 04 7440.50-9
Iron
1530 ugtl 50 0
1
03119122 1847 0321122 23 04 7439419.6
Lead
6.8 u91 50
1
03/19/22 18 47 03121122 23 04 7439-92-1
Zinc
71.5 i gfL 100
1
03/19/22 18.47 03f21P22 23 04 7440-6"
6010 MET ICP
Analytical Method EPA 6010D Preparation Method EPA 3010A
Pace Analytical Services -Asheville
Lead
10.5 ugfL 60
1
03123/22 00 35 03123/22 12 41 7439-92.1
2540D Total Suspended Solids
Analytical Method SM 2540D-2015
Pace AnalylEcal Services -Asheville
Total Suspended Solids
14,0 mg;L 2 6
1
03119r22 11.01
52200 COD
Analytical Method 5M 5220D-2011 Preparation Method SM 5220E -2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND w'L 25.0
1
031292201,28 03i25d2204;34
REPORT OF LABORATORY ANALYSIS
1n,s report 4MN no[ be reproduced, except An full,
Date 03129i2022 04 10 PM w u but"written wnseri as pace Anayn-cal Seroces, UC Page 6 of 17

Pace ArMlpYcal SwWres, LLE
9800 Kur[ay Aye Soo 100
HUPUWWAW l+C 2807e
1701)875-coe2
QUALITY CONTROL DATA
Project MGM MOTOR COMPANY R2005 00
Pace Protect No 925W257
OC Balch 645593
Ana€ysis Method
EPA 1664E
QG Batch Method EPA 1664B
Analysis Oescnphon
1664 SGT•HEM, TPH
Laboratory
Pap Anadyircal Serviaas - Chado to
Assoaatvd Lab Samples 92594257001 92594257002, 92594257003
METHOD BLANK. 359M23
Matrix Water
Issouated Lab Samples 92594257001 92594257002, 925964257003
Blank RepoMn
Parameter
Units
Resu" Lmi
Analyzed Ouallfrers
Total Petroleum Hydrocarbons
mglL
NO
$ 0 03/21/22 10 00
LABORATORY CONTROL SAMPLE
3SM24
Spike LCS
LCS % Rec
Parameter
Untts
Conc. Result.
% Rec Loft QuWV*s
Total Peuokurn Hydrocarbons
MWL
20 137
68 64-132
MATRIX SPIKE SAMPLE:
3$96625
92593916003 Spfke
MS MS % Rec
Parameter
huts
Result Carl[..
Resun % Rec Lxnds Oualzers
Total Pebnleum Hydrocarbons
myL
ND 20 129 62 64-132 M1
SAMPLE DUPLICATE 3SW26
92594058001 Oup
Parameter Una$ Result Result RPD QUsa6ers
Total Petroleum Hydrocarbons mg1L NO ND
Resuhe c+a+emed an 1hi. PRO err in"un11. fndkateM by the'UAJ1 ' relu— —Pi rf— an ea.rwl. Unrt :. rresenm M a.+" of" et "dL
REPORT OF LABORATORY ANALYSIS
. I . -•J axcepl n tUl,
.;ate. 03129 O22 04 10 PM wittmul to wntlea consern or Pate Mary?CW Sennua_ LLC Page 7 of 17

l ceAnalytical
' rre:pceWe.a�
QUALITY CONTROL DATA
Pace Ann"W Urvicn, Li.0
Kir?erfwae rrC 20079
Protect M&M MOTOR COMPANY R?005 00
Pace Project No 92594257
OG Batch 66d245
Antlers Method
EPAa0I5A1c&v dycal
QC 841ch McT*d EPA $015 Alc W C ml
Analysts Do4cApwn
EPA 8015 Mcd+fied
LAW-t-y
Pace Ana yt cal Seances - ind-wFc z
Associated Lab Samples 92594257001 92594257002, 92594267003
METKOD BLANK 3077001
Matrix Water
Assocated Lab Samples 92594257001. 925W257002, 92SU257003
Btenx Rajlorlrng
PRrarneler Untls
Result L"A
Analyzed Ouaftliers
Ethylene oc4N moll
ND
5 0 Q3 92Y 12 15
LABORATORY CONTROL SAMPLE. 3077002
Sp" LCS Lc$ % Rec
Parameter Urals Cunt A*" % Rec Lln o Ouamiers
Ethylene glycol mplL 25 318 127 39-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE 3077547 3077548
MS MSD
5291827003 Sp" Sp4te MS MSD MS MSD % Rac
Parameter Un4s Result Cone Cone. Resax Result % Rec % Rec Lars RPD Quill
Ethylene glyw "VL ND 25 25 310 285 123 114 36.15E 11
Itfau It. pnf MI\d M nti. p". m M 1he w ft Wed by aM Untb' CYt4mA o1 tW •rhfn M kh 1 &M SHIM In pF6t6M1bd $* Oft mgfK Of W n"
REPORT OF LABORATORY ANALYSIS
pate 034241202204 1Q Pkr n
Page 8 01 17

18�2
aCeAnao.
QUALITY CONTROL DATA
Protect M8M MOTOR COMPANY R2005 00
Pace Project No 92594257
CPC Baich 685960 Anatysn Metnad EPA 200 7 Rey 4,4 1994
OC Balch Method EPA200 7 Rev 4.4 19M Analyses Dounpitipn 200 7 MET
Lobvviory PaceAnaPyl" Servroes-A.hevft
Assmalod Lab Samples 92594257D01, 92594257D02. 92594257003
METHOD BLANK 3596865
Matax WSW
Associated Lab Samples
92594257001. 92594257002, 92594257003
Blank
Repo"
Parameter
Units
Result
LW A
Anayied 4uatflers
Cadmum
u91L
ND
i.0
0312112221 18
Copper
1JA
NO
50
03I2l122 21 18
Iron
AIL
NO
50 0
03/21122 21 18
Lead
ugdL
ND
5.0
03/21122 21 18
Mnc
ugfL
NO
100
03121122 21 18
Foos "yl tlawlwa, LLC
NM Kr"y Ane huh 100
HunionvfM. NC 2807d
17041675 W§2
LABORATORY CONTROL SAMPLE
3588866
Splka
LCS
LCS
% Rec
Parameter
Units
Cone
Result
% Rec
Limits Ouaii ws
Cadmium
ugfL
500
485
97
85-115
Copper
ug,'L
SI)D
505
101
05-115
Iran
ugrL
5000
4910
98
85115
Lead
ug1L
500
485
97
85-115
21nc
LVL
500
476
95
85.115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE
3586867
MS
92593976001
Spike
Parameter
Units
Result
Canc
Cadmium
ug!L
51.5
500
Capper
ugrL
698
500
Iron
u9,1
NO
5000
Lead
ugrL
NO
500
Zinc
uglL
238
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE,
3586869
MS
92594264001
Spike
Parameter
units
Result
Conc.
Cadmium
LKA
NO
500
Copper
ug/L
NO
500
Iron
ug'L
388
5000
Lead
uglL
NO
Soo
Zinc
u911
114
500
3586998
MSD
Spike
M5
MSD
MS
MSD
% Rec
Cone,
Result
Result
% Ret
% Rec
Lurwis
RPD
500
543
548
98
99
70.130
1
5D0
586
585
103
103
70-130
0
5000
4920
4890
98
97
70-130
1
500
444
447
88
89
70-130
1
500
T08
714
94
95
70-130
1
3586870
MSD
Spike
MS
MSD
MS
MSD
%Ret
Conc
Result
Result
% Rec
% Rec
Limits RPD
500
487
462
97
96
70-130 1
500
494
491
99
98
70-130 1
5000
5400
5300
100
98
70-130 2
500
482
479
96
96
70.130 1
500
588
584
95
94
7N130 1
R...11, pr.... Wd P this p.ge n. in th. -In- Wlh-1.4 by Ih*'v.0' C.k— —pl wMr* M svitrml. wM 4 pfrs-v" ra th. rlpht f 1k. rMul.
REPORT OF LABORATORY ANALYSIS
This report shall not De reprti .o*1_ ea, ept n 150.
Data, 0312912022 04:10 PM rilhovt the wr4uen consanf of Pau Amk"caj Serwcas, LLC
Qual
Pago9of17

aceAnaoical'
limicalthim
QUALITY CONTROL DATA
Project: MSM MOTOR COMPANY R2005.00
Pace Project No . 92594257
OC Batch 686745
Ariatysts Method
EPA 60100
CiC Ba" Method EPA3010A
Analysis 0*scnpUon
6010 MET
Laboratory
Pace Analyc tServices- Asheville
Asaocialed Lab Samples 92594257D01, 92594257D02, 92594257D03
METHOD BLANK 3WO72
Matrix Water
Assoc-,ated Lab Samples 92594257D01, 92594257002, 92594257003
Bu ink Reperttng
Parameter Units
Result Limit
Analyzed QualNrs
Lead ug/L
NO
5 0 O 23M 12 00
Pace Anatytical Sarvpcaa, LLC
96M Kmcsy Ave Suts 100
"'intorw". NC WW16
{7001175-9092
LABORATORY CONTROL SAMPLE 35ND73
Spike LCS LCS :4 Rep
Pararneter Units Conc. Result % Rec Limits OuahlSers
Lead y91L 500 503 101 W120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 35a8074 3SOM75
MS MSD
92594257001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone, Conc. Result Result %Rex %Refc Limits RPO Qua!
Lead ugiL 10.4 500 500 483 485 95 95 75-125 0
RRtult0 pracan lad on thla yaps are in She units lnd—ird by tlta'Umhl column aaupl wfwre an a%a mata unit is p+rasartiad to Uw right of tit wwlL
REPORT OF LABORATORY ANALYSIS
'hs, rep.od sh a:v nct he mpfoduced, except in rut.
Date 03l29i2022 04:10 PM wtnaft the wMien consent of Pau Analytical Services, LLC
Page 1 D of 17

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QUALITY CONTROL DATA
Project. MAM MOTOR COMPANY R2005 00
Pip Protect No 92594257
QC Batch W946
Analysis line"
SM 254OD-2015
OC Botch Method SM 254p0-2015
Analysis De€mptrae
2540D Total Suspended SMds
Labaalory
Pace Analytwal S4fV"% e Ashevtlb
A4so"ted Lab Samples 92594257001. 92594257002, 92594257003
METHOD BLANK 35867"
Mom Wator
Assoctaled Lab Samples 92594257001. 92594257002, 92594257003
Blank Repo"
Parameter Units
Result LKnit
Analyzed Quakfiars
Total Suspended Solids MA
NO
25 OW19M 10.5E
Pace Aimlytice17ervicee, LLC
9WO Amoy Ave Suft 100
Hurxenvie. NC 28078
(704)ers-w92
LABORATORY CCN+1TRCX SAMPLE 3SH745
Spike LCS LC3 % Roc
Parameter Units cone Result % Rac Limits Quawws
Total Suspended Sohds mglL 2m 236 95 90-110
SAMPLE DUPLICATE 3W?60
92594327001 pup
Parameter Units Resuh Result RPO Quakfaars
Total Suspended Sotlda nv& $52 910E B
SAMPLE DUPLICATE 3585761
92594316004 Dup
Parameter Units Result Result RPD Cwalif>ats
Total Suspended Solids ntylt 448 43.2 4
Resuhi Presented— aus ptye ve R.0 0.1s ind.tmed by the'Uoft' cMl .. except .hear e. ar[►meN unit is preeenH9 to We gbvm n✓ the _.ji,
REPORT OF LABORATORY ANALYSIS
TIVS f*PW shell not be reproduted. excMA in full.
Date. O3f2912022 04 10 PM Ai1r*ui ft written tunsent Of Pew AmNlcmi Serwcea, LLG
P,

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QUALITY CONTROL DATA
Prolect MdM MOTOR COMPANY R2005 00
Pace P"d No 92SS4257
OC Batts+ W905 An*sis Method SM 62200-2011
QC Batch Method SM 52ND-2011 Analysis Descnpt*n 52200 COD
Laboratory Pace Analytwal Sarvices - Asheville
Assarated Lab Samples 92594257001 92594257002, 92594257003
METHOD BLANK 3590d93 Matrix Water
AssoaaSad Lab Samples 92594257001 92594257002, 92594257003
Blank Reportkrp
Parameter Units Rest 11 Lunt Analyzed Qualifiers
Chemical Oxygen Demand MWL ND 25 0 03125M 04 32
lose Ana"M s+rricee, LLC
9MrO Kw"y Are Su" 100
NWtferlvNe NC ZW75
t70401'S-W92
LABORATORY CONTROL SAMPLE 3590894
Spike LCS LCS % Rec
Parameter Units Conc. ResuR % Roe L»tks QtrelifiMs
Chemical Oxygen Demand rv&L 150 795 106 90-110
MATRIX SPIKE S MATRIX SPIKE DUPLICATE. 3590895 3590698
NIS MSD
92594257001 Spike Sp*e MS MSD MS MSD No Rec
Parameter Units Result Cont. Conc Result Result %Rat %Rat Umits RPD Qual
Chemual Oxygen Demand Mgt NO 100 100 107 116 103 it2 0-110 S M1.R1
MATRIX SPIKE & MATRIX SPIKE DUPL ICATE 3590897 3590098
MS MSD
92594664003 Spike Spike MS MSD MS MSD % Ric
Parameter Units Result Conc. Cone Result ResuR No Rat % Rat Loma RPO Quat
chemical Oxygen Demand mg'L 52.9 100 100 156 163 103 110 96.110 4 R1
fiasuni pnientad on this par are to the units inilicai.d by the'Un€is• column esc*p1 w%tm w sitar Able eaa la pesrbW M eH"N Ilia rbeUt
REPORT OF LABORATORY ANALYSIS
Thu report snail not be reproduced. axupt in full
Date. 03/29/2022 04 10 PM without the vmr,*n consent of Pace AnaN It cal Serncas LLC
Page 12 of 17

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QUALIFIERS
P,. i•ct M&M MOTOR COMPANY R2005.00
Pan Prated No 92524257
DEFINITIONS
OF - f.7dutron Factor it roomed represents the factor appaed to Use reported data due to dAilion of tie salripia dpuot
ND - Not Domaod at or above ad)usted repwowg writ
TNTC = Too Numt,+ou9 To Courm
J - Estmatod concentration above the adusted n*Uwd detection Hrfut and hetaw tie adfustsd rapor" irni.
L*L-Adtusled MathOd Deiecbon Lime!
Pats AnOyti[et Ssrwep, LLC
9RIC, Kreuy Ave Sum 100
H"W&MV+e. NC M78
1704fa79ds *1
PQL - PraclKal 4uanlitatron L4rat.
RL - ReporWq Lrmrt - The lowesf conc.tntratron value that meets protect foci t*anuol3 for rlusr*t&Wo data with known procWm and
brae for a speuht anWe m a spook matrix_
S - Sur*opte
1.2-Dipherryjhydraarne decmposeu to end Cannot be separated from Arobenzene umV Me1Fwd 5270. The resalf for aulr aneyle n
a cOmbrned concenUat ran
Conerstant wrth EPA Quodehnes, unrounded data are disptayed vd have been used to calpffalie % recovery and RPD values,
LCSIDI - Laboratory Conlrot Sample (Dupitcole)
M5(0) - Matrix Sprke 0upieeate)
DUP - Sample Duplcate
RPD - Relafive Percent O Eerenoo
NC - Not Calcutablo
SG - Silica Gel - Ciean-Up
U - Indrralts the compound was anayz*d for but nol detected
Acid preservation may not be oppropnatt for 2 Crdoroethylvinyl eter
A separate waI preserved to a pH of 4-5 is recommended in SVVW Chapter 4 for tle anallm of AcroPem andA4rylonr4rae by EPA
Method 8760
N-Nitrosodiphanytismwie decomposes and cannut ho separstad from Dephenylamne u" Method 5270 The wsuv reported for
each analyte is a combined concentrawn
Reported results are not rounded unhl Me final slap prior to rpoeWg Therefore, caicutrod parameters let are typ may rvp~ as
'Polar may vary sightly fmm the sum of Ike reported component parameter
Pace Anatocal es TNI atu&'Itled Contact yoarr Pace PM for the current hat of actredoad anatyt"
TNI - The NELAC InsmAe
ANALYTE QUALIFIERS
Mt Matrix sprkt retwveryexceeded QC hrnila. Belch accepted based on laboratory convvif sample ILCSI revery
R1 RPD vakre was outsrde control Knits
REPORT OF LABORATORY ANALYSIS
rtre ret ori" not be reprodveed. sxeW in fug,
Data 03d39,2022 D4 10 PM snout fM wnftn rant of paw Arutyt" Sermes. Li G

Cmnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
raw AmhosM Zee. LLC
9KO 14nea} Aw Sw 100
N,Wun vile. NC "07'e
1704 d 11-�
Promd kMAM MOTOR COMPAAY R2045 00
Pate Projed Na 92594257
Anidy tiul
Lab ID Sample ID t30 Batch Method ❑C &atr h Analybc4l Method Bitch
92594257001
OUTFALL NO 1
92594257002
OUTFALL NO 2
92594257003
QUTFALL NO 3
92594257001
OUTFALL NO 1
EPA 16648
68559]
92594257002
OUTFALL NO 2
EPA 166AB
655443
92594257003
OUTFALL NO 3
EPA 1664E
685893
92594257001
OUTFALL NO 1
EPA 8015 Fk *ho *W
668245
22594257002
OUTFALL NO2
EPA 8015AWOho1-G"
6"245
92594257003
OUTFALL NO 3
EPA 5015 A1cWt01-GIyKo
668245
92SS4257001
OUTFALL NO 1
EPA 200 7 Rev 4 4 1994
6859W
EPA 200 7 Rev 4 4 19W
685977
92594257002
OUTFALL NO 2
EPA 20Q 7 Rev 4 4 1994
685960
EPA 7% 7 Rev 4 4 19W
6a"77
92594257003
OLFTFALL NO 3
EPA 200 7 Rev 4 4 1994
685960
EPA 200 7 Rev 4 4 1994
ft"7'7
92594257001
OUTFALL NO 1
EPA 3010A
SM245
EPA 60100
686584
92594257002
OUTFALL NO 2
EPA 3010A
686245
EPA 6O100
586584
92594257003
OUTFALL NO 3
EPA 3010A
686245
EPA 6010O►
666W
92594257001
OUTFALL NO 1
SM 25400-2015
665W
92594257002
OUTFALL NO 2
SM 25400-2015
685946
92594257003
OUTFALL NO 3
SM 2540D-2015
685948
92594257001
OUTFALL NO 1
SM 5MD-2011
686905
SM 5220D-2Q11
687212
02594257002
OUTFALL NO 2
SM 522CO.2011
6&905
sm 5220D-2011
607212
92594257003
OUTFALL NO 3
SM 5220D-2011
06905
5M 52200.24111
687212
Date OlrN2022 04 10 PM
REPORT OF LABORATORY ANALYSIS
7lre epw ulkal ro tw rep W except in km
wo?ktwt vv wroon corrxaenl & Pan Anal Somas LLC
Page 14 01 17

DKvmgnt Name.
Dwtonen! Revaed M"mber 15, 2aZI
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SeTee Callon Upon Reee t SL1kR4
pilaf 1 of 2
ODCL"ent Ne .
Isswsi Au[Itdr1ty-
F-CAA-0-033-Ray.01
Pau CaroitnasQAM otfrse
Laboratory rueiving samplers:
Ashevflle ❑ Eden❑ Greenwood ❑ Huntersville Ralelgh❑ Mechanicsville[] Atlsnta❑ ic.ernersv.11e—
CiientNarne: PrDle<t R: WO # ! 92594257
IIII II 11 II ii II ll
41, - Wj t kis
Courlar: LIFed £a uups USPS ent
❑ Cammtl[lai Due {other
9�5g�4257
CuWndySraf Presenl7 Oyes PFea Seals [Asact7 ❑lfrs M�N, —
! DWllpAlak Peroes Lrandwesy Cantenta: f L'
Padiin j Material- 'iffjubble wrap n&bh lays ❑Npne ❑ Other llolojital nuue Froern?
Tharratgmrtlr, Dyes ON* JD%A
-E3?01 Gun W. C. TG n � e arK
TV" N k!:
Etsrrectlon Factor:
Cooler Temp- AddlSubtrut j'Cl i TW1 Orw16IFe >0r Free6ngto VC
❑f.a!{fk%our i raA "00A. Shy n Yn, ON&M POEM
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USDA Rojulated Sind (L-�Ai9A, mar sample)
otd san+R+es ars�haite i4 a qua+antine tone within fhr Urdlyd Saks CA, NY, tar St IchrdE A+apsl? tasd sae�pes arrtirny srenr a saresja aeKce f�tp+�xivr+r✓tt,
Chain al Cuilody Present?
nwas
Dion
Colo
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Stmri A•rved MOM Hold Time?
CING
CkA
2.
Shirt Hlld Tfm! Ane K72 hr. 7
Yu
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3.
Rt1hT4rA Ars+rnd alma uv1tld2
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Cal" Containers Used?
•PaceCoctiir•ersUsedl
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CcntainerslAtaM22YO
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Sample labels Match COC7
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Trip Blank Present?
Trsp stank [.study Seals Presets?
[]Yes
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JaWA
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CCAAMIMSISAMPU O-SCREeANCV
Ir" OM SwAr M? Qt n [>4
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Per -San Conu ted:
Project Manajer SCURF Review,
Prefect Minim SAF Revlew:
DatelTme
Cole.
Cale:

Cocumcnt Name: j Document Revlted, November 15, 2U21
Condition Upon Recef t (SLUR) Page 2 of 2
Document No.: (swing Authority,
j F-G4R-fS•OSS•Rev.D� I o"'r a/�%
'Check mark top half of box if pH and/or dechlorination IS Project wo# ; 9+ 259a"F��__��—�'��
verified and within the acceptance range for preservation yN�d--� Dye Date: 03/29�ZZ