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HomeMy WebLinkAboutWQ0000889_Monitoring - 03-2022_20220510 • GW-59A COMPLIANCE REPORT FORM Permit# WQ0000889 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. (04/30/2022) Will this monitoring report(GW-59 and GW-59A)be YES NO submitted after the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO X IF the answer to question 1 or 2 is "YES",list in the space provided below the well identification number(s)and explain the problems encountered in obtaining the required information. DJ MAY 1 9 202 3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missiong cap, YES NO missing identification plate,area overgrown,etc.)? if the answer is "Yes,contact the Regional Office for X guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO X • If the answer to question 4 is "NO",skip to section 8. ! If the answer to question 4 is "YES', list the affected wells individually with costitueat(s)and concentrations(s) exceeding standards in the space provided below: r 3/8/2022 WWMW-1 TDS 400 Note: WWMW No. 1 is the established ground rr if king well. WWMW-2 TDS 340 WWMW-3 TDS 640 WWMW-4 TDS 690 5 For the constituents identified in question 4 above,have standards been exceeded previous for the same YES NO constituent(s) in the same well(s) X If the answer to question 5 is "NO",skip to section 8. If the answer to question 5 is "YES', list in the space provided below, each well with constituent(s)exceeding standards,concentration(s)reported, and sample collection date for each occurrence(for the last two years). 3/8/2022 11/4/2021 7/20/2021 3/23/2021 11/20/2020 7/16/2020 3/18/2020 WWMW-1 TDS 400 410 390 451 451 436 449 WWMW-2 TDS 340 410 390 440 630 695 695 WWMW-3 TDS 640 680 750 670 572 692 763 WWMW-4 TDS 690 680 660 660 673 690 685 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO X If the answer is"YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is"NO", monitoring wells may be improperly located;contact the Regional Office. *Only WWMW No. 1 is located beyond the review boundary. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO quality problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. if the answer to question 7 is "NO', contact the Regional Office within 90 days;an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,fines,and/or penalties. Contacted WaRO 04/27/2022. 8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with GW-59 forms for required wells to be address provided at the top of the current GW-59 form. I:hereby;acknowledgethat:the:above:utformation::was:evaluated and:the:information submitted:intfiisreport (Cornplca epo 91t):is a plete to the bestaf my:knovvledge .. • j 1-//77 /7cp22 Signature of Permittee(or Authorized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL GROUNDWATER QUALITY MONITORING: I WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:w00000889 Expiration Date: 04/30/2028 e X UIC PCS Phosphate Co./Nutrien, Inc Non-Discharge Facility Name: P 9 Permit Name(if different): NPDES Other Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora NC 28706 County Beaufort ❑ Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: Contact Person: Shelby Wiggins Telephone#: (252)-322-4111 ext.8573 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name:WWTP No.of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): WWMW-1 Date sample collected: 03/08/22 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400: 7.22 units Temp. °oelo 18.3 °C DRY at tMhos time of Depth to Water Level 82546:9.92 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec.Cond. 00094: 608 1. sampling, Measuring Point is 2.50 ft. above land surface Relative M.P. Elevation: 20.78 ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑YES ❑ NO ZN/A Field acidified:❑YES ❑NO Pi N/A LABORATORY INFORMATION y Date sample analyzed:03/08/2022 Laboratory Name: PCS Phosphate Co./Environment 1,Inc Certification No. #330/#10 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. ill AY COD 00335 N/A mg/L Nitrite(NO2)as N oo61s N/A mg/L Pb-Lead()lost N/A ug/L M,qY Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate(NO3)as N 00620 0.07 mg/L Zn-Zinc 01092 N/A mg/L v r',9. Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P o0665 0.043 mg/L NCO �? (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other(Specify Compounds and Concentration Units): �..re ) 9 ( P fY P8/ �r, Dissolved Solids:Total 70300 400 mg/L Al-Aluminum o11os N/A mg/L 0�Ct, pH (Lab)00403 7.22 units Ba-Barium 01007 N/A ug/L D l TOC o0680 3.11 mg/L Ca-Calcium o0916 N/A mg/L , Chloride 00940 <1.0 mg/L Cd-Cadmium 01027 N/A ug/L Arsenic 01o0z N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils oossz N/A mg/L Cu-Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 3273o N/A ug/L Fe-Iron°leas N/A ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg-Mercury 71900 N/A ug/L Lab Report Attached? ❑ Yes(1) El No(0) Specific Conductance 00095 N/A µMhos K-Potassium 00937 N/A mg/L VOC 7873 , method# N/A Total Ammonia o0610 0.16 mg/L Mg-Magnesium 00927 N/A mg/L , method# (Ammonia Nitrogen,NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 N/A ug/L , method# TKN as N oo6zs N/A mg/L Ni-Nickel 01067 N/A ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that.to the best of my knowledge and belief,the information submitted in this report is true.accurate,and complete.and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knew:ng violations. c� / William M.Penton,General Manager �' // / ( z �� ZFi 2-Z Permittee(or Authorized Agent)Name and Title-Please print or type -gnature of Permittee(or Authorized Agent) (Date) GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL GROUNDWATER QUALITY MONITORING: I WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:W00000889 Expiration Date: 04/30/2028 Facility Name: PCS Phosphate Co./Nutrien,Inc Non-Discharge X UIC Permit Name(if different): NPDES Other Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora NC 28706 County Beaufort ❑ Lagoon ❑ Remediation: Infiltration Gallery E Spray Field ❑ Remediation: Contact Person: Shelby Wiggins Telephone#: (252)-322-4111 ext.8573 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name:WWTP No.of wells to be sampled: 4 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): WI/MW-2 Date sample collected: 03/08/2022 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400: 7.45 units Temp.00010: 18.3 °C DRY at Mhos time of Depth to Water Level 82546:10.85 ft.below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec.Cond.00094: 533 µ sampling, Measuring Point is 2.50 ft.above land surface Relative M.P.Elevation: 20.84 ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑YES ❑ NO ®N/A Field acidified:❑YES ❑NO [1 N/A LABORATORY INFORMATION Date sample analyzed:03/08/2022 Laboratory Name: PCS Phosphate Co./Environment 1,Inc Certification No. #330/#10 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite(NO2)as N 00615 N/A mg/L Pb-Lead 01051 N/A ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate(NO3)as N 00620 <0.04 mg/L Zn-Zinc 01os2 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus:Total as P 00665 0.035 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 340 mg/L Al-Aluminum 01105 N/A mg/L pH(Lab)00403 7.61 units Ba-Barium 01007 N/A ug/L TOC 00680 2.75 mg/L Ca-Calcium 00916 N/A mg/L fJ 1 L Chloride 00940 6 mg/L Cd-Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium:Total 01034 N/A ug/L Grease and Oils 00552 N/A mg/L Cu-Copper 01042 N/A mg/L ORGANICS: (by GC,GC/MS, HPLC) Phenol 32730 N/A ug/L Fe-Iron 01045 N/A ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg-Mercury 71900 N/A ug/L Lab Report Attached? 0 Yes(1) E No(0) Specific Conductance moss N/A µMhos K-Potassium 00937 N/A mg/L VOC 7873 , method# N/A Total Ammonia 00610 0.06 mg/L Mg-Magnesium 00927 N/A mg/L ,method# (Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 N/A ug/L , method# TKN as N 00625 N/A mg/L Ni-Nickel 01067 N/A ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that.to the best of my knowledge and belief.the information submitted in this report is true.accurate.and complete.and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. William M.Ponton,General Manager /ram\ i� i/ K/Z -7/2 Z 2-- Permittee(or Authorized Agent)Name and Title-Please print or type Sig ature of Permittee(or Authorized A.ent) (Date) GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:919 807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0000889 Expiration Date: Facility Name: PCS Phosphate Co./Nutrien,Inc Non-Discharge X UIC Permit Name(if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South Aurora, NC 27806 County Beaufort ❑ Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: Contact Person: Shelby Wiggins Telephone#: (252)-322-8573 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWTP No.of wells to be sampled:4 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): WWMW-3 Date sample collected: 03/08/22 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400: 7.13 units Temp.00010: 17.4 °C DRY at Mhos time of Depth to Water Level 82546:10.85 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec.Cond.00094: 1083 µ sampling, Measuring Point is 2.50 ft.above land surface Relative M.P. Elevation: 20.15 ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑YES ❑ NO ®N/A Field acidified:❑YES ❑NO Ll N/A LABORATORY INFORMATION Date sample analyzed:03/08/2022 Laboratory Name: PCS Phosphate Co./Environment 1,Inc Certification No. #330/#10 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite(NO2)as N o0s1s N/A mg/L Pb-Lead 01051 N/A ug/L Coliform: MF Fecal 31616< 1.0 /100mL Nitrate(NO3)as N ooszo <0.04 mg/L Zn-Zinc o1092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus:Total as P oosss 0.016 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other(Specify Cogo�oynds and Concentration Units): dissolved Solids:Total 70300 640 mg/L Al-Aluminum altos N/A mg/L U� pH(Lab)00403 7.39 units Ba-Barium 01007 N/A ug/L TOC oosso 2.55 mg/L Ca-Calcium owls N/A mg/L Chloride o0940 109 mg/L Cd-Cadmium 01027 N/A ug/L Arsenic olooz N/A ug/L Chromium:Total 01034 N/A ug/L Grease and Oils oossz N/A mg/L Cu-Copper 01042 N/A mg/L ORGANICS:(by GC,GC/MS,HPLC) Phenol 32730 N/A ug/L Fe-Iron o1045 N/A ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate o0945 N/A mg/L Hg-Mercury 71900 N/A uglL Lab Report Attached? ❑ Yes(1) ❑■ No(0) Specific Conductance 0009s N/A µMhos K-Potassium 00937 N/A mg/L VOC 7873 ,method# N/A Total Ammonia owl 0.11 mg/L Mg-Magnesium 00927 N/A mg/L , method# (Ammonia Nitrogen;NH3 as N:Ammonia Nitrogen,Total) Mn-Manganese moss N/A ug/L , method# TKN as N 00625 N/A mg/L Ni-Nickel 01067 N/A ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal%N/A I certify that.to the best of my knowledge and belief,the information submitted in this report is true.accurate.and complete.and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations William M. Ponton,General Manager �,-/72.-- - / /2 7l'7� Z Z Permittee(or Authorized Agent)Name and Title-Please print or type Si. ature of Pe ittee(or Authonzed Agent) /' (Date) GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES and 1 copy t0: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:W00000889 Expiration Date: 04/30/2028 Facility Name: PCS Phosphate Co./Nutrien,Inc Non-Discharge X UIC Permit Name(if different): NPDES Other Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora NC 28706 County Beaufort ❑ Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: Contact Person: Shelby Wiggins Telephone#: (252)-322-4111 ext.8573 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name:WWTP No.of wells to be sampled: 4 ❑ Water Source Heat Pump ❑Other (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): WWMW-4 Date sample collected: 03/08/22 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400. 7.24 units Temp. 00o10: 19.9 °C DRY at time of Depth to Water Level 82546:13.75 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec. Cond. 00094: 1126 µMhos sampling, Measuring Point is 2.50 ft. above land surface Relative M.P. Elevation: 20.81 ft. Odor 00085 None check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑YES ❑ NO ®N/A Field acidified:❑YES ❑ NO IA N/A LABORATORY INFORMATION Date sample analyzed:03/08/2022 Laboratory Name: PCS Phosphate Co./Environment 1,Inc Certification No. #330/#10 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite(NO2)as N 00615 N/A mg/L Pb-Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate(NO3)as N 00620 <0.04 mg/L Zn-Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus:Total as P 00665 0.077 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other(Specify Compounds and Concentration Units): dissolved Solids:Total 70300 690 mg/L Al-Aluminum 01105 N/A mg/L pH(Lab)00403 7.60 units Ba-Barium 01007 N/A ug/L DJ TOC 0068o 2.33 mg/L Ca-Calcium 00916 N/A mg/L Chloride 00940 124 mg/L Cd-Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils 00552 N/A mg/L Cu-Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 N/A ug/L Fe-Iron 01045 N/A ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg-Mercury 71900 N/A ug/L Lab Report Attached? ❑ Yes(1) 0 No(0) Specific Conductance o0o9s N/A µMhos K-Potassium 00937 N/A mg/L VOC 7873 , method# N/A Total Ammonia 00610 0.33 mg/L Mg-Magnesium 00927 N/A mg/L , method# (Ammonia Nitrogen;Nhi3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 N/A ug/L , method# TKN as N 00625 N/A mg/L Ni-Nickel 01067 N/A ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that,to the best of my knowledge and belief.the information submitted in this report is true.accurate,and complete.and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment/ for knowing violations. William M.Ponton,General Manager ^/ 1/Z 7 �(DZ? Permittee(or Authorized Agent)Name and Title-Please print or type Signa ure of Permittee(or Authorized Agent) (Date) GW-59 Rev.05-02-2017 En/ITO:MEI °" - •' ^ - Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE PHONE (252) /56-6208 GREENVILLE. N.C. 27858 FAX (252) 756-0633 ID#: 1605 NUTRIEN (WELLS 1-4) MR. BRYAN MILLS 1530 NC HWY. 306 SOUTH DATE COLLECTED: 03/08/22 AURORA, NC 27806 DATE REPORTED : 03/18/22 REVIEWED BY: ✓ \ Domestic Domestic Domestic Domestic Analysis Method PARAMETERS Mwell #1 Mwell #2 Mwell #3 Mwell #4 Date Analyst Code Fecal Coliform (MF), /100 Nils <1 <1 <1 <1 03/08/22 HCE 9222D-15 Ammonia Nitrogen as N, mg/I 0.16 0.06 0.11 0.33 03/10/22 TRJ 350.1 R2-93 Nitrate Nitrogen as N, mg/1 0.07 <0.04 <0.04 <0.04 03/09/22 KES 353.2 R2-93 Total Organic Carbon, mg/I 3.11 2.75 2.55 2.33 03/15/22 HMM 5310C-14 Chloride, mg/I <1 6 109 124 03/14/22 DIJ 4500CLB-11 Total Dissolved Residue, mg/1 400 340 640 690 03/10/22 DNS D5907-13 ---f7)T17 011- %/IA Author:Bryan Mills Date:3/30/2022 Original Run Filename: OM_3-30-2022_03-32-54PM.OMN Created:3/30/2022 3:32:54 PM Original Run Author's Signature: [aurlenv] Current Run Filename: OM_3-30-2022_03-32-54PM.OMN Last Modified:3/30/2022 3:54:20 PM Current Run Author's Signature: [aurlenv] Description: Default New Run Channel 3 Sample Rep. Cup No. Total Phosphorou Detection Time ADF MDF Description s(ma P/L)1 CalStd A 1 S1 0.500 3/30/2022@3:34:38 PM CalStd B 1 S2 0.250 3/30/2022@3:35:46 PM CalStd C 1 S3 0.100 3/30/2022@3:36:55 PM CalStd D 1 S4 0.0500 3/30/2022@3:38:04 PM CslStd E 1 S5 0.0200 3/30/2022@3:39:13 PM Blank 1 S6 -1.58e-4 3/30/2022@3:40:22 PM Known Conc: 0.00 Calibration: Table/Fig. :1 mid range 1 1 ( S2 0.248 3/30/2022@3:41:30 PM Known Conc: 0.250 QA 1 1 0.350 3/30/2022@3:42:39 PM V' WWTP#1 1 2 0.0427 3/30/2022@3:43:49 PM WWTP#2 1 , 3 0.0292 3/30/2022@3:44:58 PM WWTP#3 1 4 9.24e-3 3/30/2022@3:46:07 PM v/ WWTP#4 1 5 0.0768 3/30/2022@3:47:16 PM WWTP#4 dup_ 1 6 0.0791 3/30/2022@3:48:25 PM WWTP#4 spike 1 7 0.174 3/30/2022@3:49:34 PM I WWTP#4 spike dup 1 8 0.191 3/30/2022@3:50:43 PM Blank 1 S6 0.0136 3/30/2022@3:51:51 PM Known Conc: 0.00 mid range 1 1 I S2 0.246 3/30/2022@3:52:59 PM Known Conc: 0.250 Table: 1 (Total Phosphorous) Known Conc. Rep Peak Area Peak Height %RSD %Residual Det.Conc Detection Date Detection Time (mg P/L) (V.$) (V) (mg P/L) 1 0.500 1 5.51 0.607 0.0 -0.1 0.500 3/30/2022 3:34:38 PM 2 0.250 1 2.54 0.275 0.0 0.9 0.248 3/30/2022 3:35:46 PM 3 0.100 1 1.05 0.109 0.0 -2.8 0.102 3/30/2022 3:36:55 PM 4 0.0500 1 0.575 0.0562 0.0 -5.0 0.0528 3/30/2022 3:38:04 PM 5 0.0200 1 0.234 0.0203 0.0 13.8 0.0166 3/30/2022 3:39:13 PM Figure: 1 (Total Phosphorous) 5.51, Area=3.74*ConcA2+8.96*Conc+0.0905 Conc=-2.91 a-3*AreaA2+0.108*Area-8.58e-3 h Correlation C:::0eh1t i (r)=0.99991 m Weighting: Y N 0. 0.00 Concentration mg P/L 0.500 ctrrIn)I�T�S i �� �A l U 1. �-+�' 1V�' Igo 1�71�t- 10Y1e21h7 I 1�ls -1 - Author:Bryan Mills Date: 3/30/2022 Original Run Filename: OM_3-30-2022_01-42-13PM.OMN Created: 3/30/2022 1:42:13 PM Original Run Author's Signature: [aurlenv] Current Run Filename: OM_3-30-2022_01-42-13PM.OMN Last Modified:3/30/2022 2:13:56 PM Current Run Author's Signature: [aurlenv] Description: Default New Run _._ Channel 3 Sample Rep. Cup No. Total Detection Time ADF MDF Description Phosphorou s(mg P/L) CalStd A 1 S1 0.500 3/30/2022@1:45:06 PM CalStd B 1 S2 0.250 3/30/2022@1:46:14 PM CalStd C 1 S3 0.100 3/30/2022@1:47:23 PM CalStd D 1 S4 0.0500 3/30/2022@1:48:32 PM CalStd E 1 S5 0.0200 3/30/2022@1:49:41 PM Blank 1 S6 -4.54e-3 3/30/2022@1:50:49 PM Known Conc: 0.00 Calibration: Table/Fig. :1 mid range I 1 I S2 0.249 3/30/2022@1:51:58 PM Known Conc: 0.250 ' QA 1 1 0.327 3/30/2022@1:53:07 PM 005 1 2 0.0505 3/30/2022@1:54:16 PM 007 1 3 0.143 3/30/2022@1:55:26 PM 009 1 4 0.267 3/30/2022@1:56:35 PM 009dup 1 5 0.263 3/30/2022@1:57:44 PM 009spike 1 6 0.344 3/30/2022@1:58:52 PM 009 dup spk 1 7 0.344 3/30/2022@2:00:01 PM Blank 1 S6 -3.79e-3 3/30/2022@2:01:09 PM Known Conc: 0.00 mid range I 1 I S2 0.252 3/30/2022@2:02:18 PM Known Conc: 0.250 JWWTP#1 1 8 0.0233 3/30/2022@2:03:26 PM WWTP#2 1 9 0.0348 3/30/2022@2:04:35 PM WWTP#3 1 _ 10 0.0159 3/30/2022@2_05:44 PM WWTP#4 1 i 1 u.0464 3/30/2022@2:06:52 PM WWTP#4 dup 1 12 0.0617 3/30/2022@2:08:00 PM WWTP#4 spike 0.1482 1 13 3/30R022@2:09:08 PM WVVTP#4 spike dup 1 14 - 0.169 3/30/2022@2:10:17 PM Blank 1 S6 -3.84e-3 3/30/2022@2:11:25 PM Known Conc: 0.00 mid range j 1 I S2 0.247 3/30/2022@2:12:33 PM Known Conc: 0.250 Table: 1 (Total Phosphorous) Known Conc. Rep Peak Area Peak Height %RSD %Residual Det.Conc Detection Date Detection Time (mg P/L) (V.$) (V) (mg P/L) 1 0.500 1 6.48 0.597 0.0 0.0 0.500 3/30/2022 1:45:06 PM 2 0.250 1 3.00 0.271 0.0 0.3 0.250 3/30/2022 1:46:14 PM 3 0.100 1 1.16 0.100 0.0 -1.6 0.101 3/30/2022 1:47:23 PM 4 0.0500 1 0.546 0.0450 0.0 1.4 0.0493 3/30/2022 1:48:32 PM 5 0.0200 1 0.206 0.0151 0.0 1.8 0.0200 3/30/2022 1:49:41 PM l'� 1,,� ii tL�B 164 -6IV 4,-R 1V1 e, evn a w a f I Glts I. j cugc5 -1 -