HomeMy WebLinkAboutNCG030027_Q2 Sampling Results_20220621ur +
aceAnalytical ® ANALYTICAL REPORT
June 21, 2021
Eaton Corporation
Sample Delivery Group: L1362234
Samples Recelved: 06/05/2021
Project Number: 28091-R
Description: Eaton Corp Monthly Stormwater
Site: ROXBORO, NC
Report To: Edmara Bloomer
2564 Durham Road
Roxboro, NC 27573
Entire Report Reviewed By:
Heather J Wagner
Project Manager
Results relate only to the Items tested or calibrated and are reported as rouMed values. This test report shall not be
reproduced, except In full, without written approydl of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance pr#Med In laboratory standard operating procedures ENV-S0P-M1JL4067 and
ENV-SOP.MTJL-0068. Where samplingtonducted by the customer, results relate to the accuracy of the information provided.
and as the Samples are received.
Li
all
Pace Analytical •
e :ss
ACCOUNT: PROJECT: SD6'. DATEn IME'
Eaton Corporabon 28091E L131,2234 06/21/21 09'.45
PAGE:
1of23
TABLE OF CONTENTS
Cp: Cover Page
1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
SS
NE ENTRY L1362234-01
5
aCr1
Qc: Quality Control Summary
9
Gravimetric Analysis by Method 2540 D-2011
9
Sl
Wet Chemistry by Method 16648
10
Metals (ICP) by Method 200.7
11
FC
Volatile Organic Compounds (GC/MS) by Method 624.1
12
GI
Pesticides (GC) by Method EPA 608.3
14
Polychlorinated Biphenyls (GC) by Method EPA-608.3
16
[Al
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
17
GI: Glossary of Terms
21
BSc
Al: Accreditations & Locations
22
Sc: Sample Chain of Custody
23
ACCOUNT: PROJECT: SDG: DATE[TIME: PAGE:
Eaton Corporation 28091-R L1362234 0621/2109 45 2 of 23
SAMPLE
SUMMARY
Collected by
Collected date/time
Received date/time
NE ENTRY L1362234-01 WW
Chris Fuller
06/03/2117:50
06/05/2109:30
Method
Batch
Dilution
Preparation
Analysis
Analyst
Locatlon
datelhme
date/time
Gravlmetric Analysis by Method 2540 D-2011
WG1686421
1
06/1012115:23
06/10/2117:45
MMF
Mt. Juliet, IN
Wet Chemistry by Method 1664E
WG1686563
1
0611012109:16
06/10/2120:11
ERK
Mt. Juliet, IN
Metals(ICP) by Method 200.7
WG1690234
1
0611712109:54
06/17/2120:56
CCE
Mt. Juliet, IN
Volatile Organic Compounds(GC/MS) by Method 624.1
WGI683600
1
06105/2122:36
06/05/2122:36
JHH
Mt. Julie[, IN
Pesticides (GC) by Method EPA 608.3
WG7684259
1.05
06108/2109:48
06/08/2119:25
HMH
Mt. Jul let, IN
Polychlorinated Biphenyls(GC) by Method EPA-608.3
WG1684259
1.05
06108/2109.48
06/08/2118:08
JMB
Mt. Jullet. IN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WGI684262
1
06/0812117:52
06/0912108:21
AMG
Mt. Jullet, IN
ACCOUNT: PROJECT: SDG: DATE/tIME: PAGE:
Eaton Corporation 28091-R L1362234 0621/2109:45 3of 23
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
Rp
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been Identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
■
asr
• ' 41
rGl
Heather J Wagner
a _
Project Manager
9Sc
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Eaton Corporation 28091-R L1362234 06121/2109:45 4 of 23
NE ENTRY SAMPLE RESULTS - 01
Collected date/time: 06/03/21 17:50 L1362234
Additional Information - Results for field analyses are not accredited to ISO 17025
Result Units
Analyte
pH (On Site) 7.09 su
Temperature (on -site) 21.6 deg. C
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mgA mg/l date l time
Suspended Solids 132 16,7 1 06/10/202117.45 WGI686421
Wet Chemistry by Method 1664B
Result
Qualifier MDL
RDL Dilution
Analysis Batch
Analyte
mgA
mg/I
mg/1
date/time
TPH - Oil & Grease
U
1.04
714 1
06=202120:11 WG1686563
Sample Narrative:
L1362234-01 WG1686563: Total Oil&Grease is non -detect. Extract was not processed through silica gel.
Metals (ICP) by Method 200.7
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
mgA
mg/I
mgA
date/time
Copper
0.0145
0.00226
0.0100
1 06117/202120*56
WG1690234
Lead
0.00438
J 0.00227
0.00500
1 06/17/202120:56
WGI690234
Zinc
0,0480
J 0,00578
0.0500
1 06P7/202120:56
WG1690234
Volatile Organic Compounds (GC/MS) by Method 624.1
Result
Qualifier MDL
RDL
Dilution
Analysis
Batch
Analyte
mgA
mg/I
mgA
date/time
Acrolein
U
0.00254
0.0500
1
06/05202122:36
WG1683600
Acrylonimle
U
0.000671
0.0100
1
06105002122:36
WG1683600
Benzene
U
OA000941
0.00100
1
06105/20212236
WG1683600
Bromodichioromethane
U
0.000136
0.00100
1
06105/202122:36
WG1683600
Bromoform
U
0.000129
0.00100
1
06/05/202122:36
WG1683600
Bromomethane
U
0.000605
0.00500
1
06105/202122:36
WG1683600
Carbon tetrachloride
U
0.000128
0.00100
1
06/05/2021 22:36
WG1683600
Chlorobenzene
U
0.000116
0.00100
1
06105/202122:36
WG1683600
Chlorodibromomelhane
U
0.000140
0.00100
1
061051202122:36
WG1683600
Chloroethane
U
0.000192
0.00500
1
06/05/202122:36
WG1683600
2-Chloroethyl vinyl ether
U
0.000575
0.0500
1
06105/202122:36
WG1683600
Chloroform
U
0,000111
0.00500
1
06/051202122:36
WG1683600
Chloromethane
U
0.000960
0.00250
1
061051202122.36
WC1683600
1,2-Dichlorobenzene
U
0.000107
0.00100
1
06/05202122:36
W1683600
1,3-Dichlorobenzene
U
0.000110
0.00100
1
06/0520212236
WG1683600
1,4-Dichlorobenzene
u
0.000120
0.00100
1
06/05/2021 22:36
WG1683600
DichlorodiFluoromethane
U
0.000374
0.00500
1
06/051202122:36
WG1683600
1,1-Dichloroethane
U
0.000100
0.00100
1
06/05/202122:36
WG1683600
1,2-Dichloroethane
U
0.0000819
0.00100
1
06/05/202122:36
WG1683600
1,1-Dichloroethene
U
0.000188
0.00100
1
06105/202122:36
WG1683600
trans-1,2-Dichloroethene
U
0000149
0,00100
1
06105/20212236
WG1683600
1,2-Dichloropropane
u
0.000149
0.00100
1
06/05/202122:36
WG1683600
cls-1,3-Dlchloropropene
U
0.000111
0.00100
1
06/05/202122:36
W61693600
trans-1,3-Dichloropropene
U
0.000118
0.00100
1
06/05/202122:36
WG1683600
Elhylbenzene
U
0.000137
0.00100
1
06/05/2021 22:36
WG1693600
Methylene Chloride
U
0.000430
0.00500
1
06/05/202122:36
WG1683600
T1,42-Telrachloroethane
U
0,000133
0.00100
1
06/05/202122:36
WG1683600
Tetrachloroethene
U
0.000300
0.00100
1
06/05/202122:36
WG1683600
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Eaton Corporation 28091-R L1362234 06/21/21 09:45 5 of 23
NE ENTRY
SAMPLE
RESULTS - 01
Collected date/time: 0610
3/2117:50
L1362234
Volatile Organic Compounds
(GC/MS) by Method 624.1
Result
Qualifier MDL RDL
Dilution Analysis
Batch
Cp
Analyze
mgA
mg4 mgA
date/time
Toluene
U
0.000278 0.00100
1 06/05/202122:36
WG1683600
�Tc
1,1,1-Trichloroethane
U
0.000149 0.00100
1 06/05/202122:36
WGI683600
1,1,2-Trichloroethane
U
M00158 0.00100
1 06/051202122:36
WG1683600
Trichloroethene
U
0.000190 0.00100
1 06/05/202122:36
WG1683600
PSITrichiorofluoromethane
U
0,000160 0.00500
1 06I05/202122:36
WGI683600
Vinyl chloride
U
0.000234 0.00100
1 06/06/2021 22:36
WGI683600
Ql
(5)Toluene-d8
102
80.0.120
06105/101122:35
WG1683600
(3)4-BromoBuorobenrene
90.4
80.0-120
061051202122.36
WG1683600
(S)1.2-Dlchloroethane-d4
111
70.0-130
061051202122.36
WGI683600
Pesticides (GC) by Method
EPA 608.3
aQc
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyze
mg4
mgll
mgA
date/time
7GI
Aldrin
U
0.0000208
0.0000525
1.05
06108/202119:25
WG1684259
Alpha BHC
U
0.0000181
0.0000525
1,05
06/08/202119:25
WG1684259
a
Beta BHC
U
0.0000218
0.0000525
1.05
06/09/202119:25
WG1684259
AI
Delta BHC
U
0.0000158
0.0000525
1.05
06/08/202119:25
WGI684259
Gamma BHC
U
0.0000219
0.0000525
1.05
06/08/202119:25
WG1684259
aSC
Chlordane
U
0.0000208
0.00525
1.05
06/081202119:25
WG1684259
4,4-DDD
U
0.0000186
0.0000525
1,05
06/08/202119:25
WG1684259
4,4-DDE
U
0.0000162
0.0000525
1.05
06108/202119:25
WGI684259
4,4-DDT
U
0.0000208
0.0000525
1.05
06108/202119:25
WG1684259
Dieldrin
U
0.0000170
0.0000525
1-05
06/081202119:25
WG1684259
EndosulfanI
U
0.0000168
0,0000525
1.05
06108/202119:25
WG1684259
Endosuffan II
U
0.0000172
0.0000525
1.05
06/08/202119:25
WG1684259
Endosulfan sulfate
U
0.0000228
0.0000525
1.05
06/0W202119:25
WG1684259
Endrin
U
0.0000169
0.0000525
1.05
061081202119:25
WG1684259
Endrin aldehyde
U
J4
0.0000249
0.0000525
1.05
06/08/202119:25
WG1684259
Endrin ketone
U
0,0000230
0.0000525
1.05
06/08/202119:25
WGI684259
Heptachlor
U
0,0000155
0.0000525
1.05
06/08/202119:25
WG1694259
Heptachlor epoxide
U
0.0000192
0.0000525
1.05
06/08/202119:25
WG16B4259
Hexachlorobenzene
U
0.0000185
0.0000525
1.05
06108/202119:25
WG1684259
Methoxychior
U
0.0000203
0.0000525
1.05
06/08/202119;25
WG1684259
Toxaphene
U
0.000176
0.000525
1.05
06108/202119:25
WG1684259
(S) Decochlorobiphenyl
44.4
'10.0.144
owa,1202119.,25
WG7684259
(5) Tetrochloro-m-xylene
52.1
10.0.135
06708/202119:25
WGI684259
Polychlorinated Biphenyls
(GC) by Method EPA-608.3
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyze
mgA
mgA
mgA
date/time
PC81016
U
J4
0.000294
0.000525
1.05
06/08/202118:08
WG1684259
PC61221
U
0.000284
0.0G0525
1.05
06/08/202118%
WGI684259
PCB 1232
U
0.000284
0,000525
1.05
06/08/202118:08
WGI684259
PCB 1242
U
0.000294
0,000525
1.05
06/08/202118:08
WG1684259
PCB 1248
U
0.000181
0.000525
1.05
06/08/202118:08
WGI684259
PCB 1254
U
0,000181
0,000525
1.05
06108/202118:08
WGI684259
PCB 1260
U
0.000181
0.000525
1.05
06108/202118:08
WGI684259
(S) Decochlorobiphenyl
43.0
10.0-144
06/08202118..*08
WG1684259
(s) Telrachloro-m-xy/ene
58.6
10.O 135
061081202118.08
WG1684259
ACCOUNT:
PROJECT:
SDG:
DATEMME:
PAGE:
Eaton Corporation
28091-R
L1362234
06/2121 09:45
6 of 23
NE ENTRY SAMPLE RESULTS - 01
Collected date/time: 06/03/21 17:50 1.7362234
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution
Analysis
Batch
Analyte
mgA
mgA
mgA
date l time
Acenaphthene
U
0.0000886
0.00100
1
06109/202108:21
WG1684262
Acenaphthylene
U
0.0000921
0.00100
1
06/09/202108:21
WGI684262
Anthracene
U
0.0000804
0.00100
1
06/09/202108:21
WG1684262
Benzidine
U
J3 0,00374
0.0100
1
06/09/2021013:21
WGI684262
Benzo(a)anthracene
U
0.000199
0,00100
1
06/09/202108:21
WG1684262
Ben2o(b)8uoranthene
U
0.000130
0,00100
1
06109/202108:21
WG1684262
Senzoikl8uoranthene
U
0.000120
0.00100
1
06/09/202108:21
WG1684262
Benzo(g,h,pperylene
U
0.000121
0.00100
1
06/09/202108:21
WG1684262
Benzoialpyrene
U
0.0000381
0.00100
1
06/091202108:21
WG1684262
Bis(2-chlorethoxylmethane
U.
0.000116
0.0100
1
06/09202108:21
WG1684262
Bis(2-chloroethyl)ether
U
0.000137
0.0100
1
06/09/202108:21
WG1684262
2,2-Oxybis(1-Chloropropane)
U
0.000210
0.0100
1
06/09202108:21
WG1684262
4-Bromophenyl-phenyiether
U
0.0000877
0.0100
1
06/09/202108:21
WG1684262
2-Chloronaphthalene
U
0.0000648
0.00100
1
06109/202108:21
WG1684262
4.Chlorophenyl-phenylether
U
0.0000926
0.0100
1
06109/202108:21
WG1684262
Chrysene
U
0.000130
0.00100
1
061091202108:21
WG1684262
Dibenz(a,h)anthracene
U
0.0000644
0.00100
1
06/09/202108:21
WG1684262
3,3-Dichlorobenzidine
U
0.000212
0.0100
1
06109/202108:21
WG1694262
2,4-Dinitrotoluene
U
0.0000983
0.0100
1
06/09/202108:21
WGI684262
2,6-Dinitrotoluene
U
0,000250
0.0100
1
061091202108:21
WGI684262
1,2-Diphenylhydrazine
U
0.000105
0.0100
1
06/091202108:21
WG1684262
Fluoranthene
U
0,000102
0.00100
1
06/091202108:21
WGI694262
Fluorene
U
0,0000844
0.00100
1
06/09/20210821
WGI684262
Hexachlorobenzene
U
0.0000755
0.00100
1
06109202108:21
WGI684262
Hexachloro-1,3-buladiene
U
0.0000968
0,0100
1
06/09/202108:21
WG1684262
Hexachlorocyclopentadiene
U
0.0000598
0.0100
1
06/09/20210821
WG1694262
Hexachloroethane
U
0.000127
0.0100
1
06/09/20210821
WG1684262
Indenoil,,2,3-cd)pyrene
U
0.000279
0.00100
1
O6/09202108:21
WG1684262
Isophorone
U
0.000143
0.0100
1
06/09/202108:21
WGI684262
Naphthalene
U
0.000159
0.00100
1
061091202108:21
WG1684262
Nitrobenzene
U
0.000297
0,0100
1
06/09/202108:21
WGI684262
n-Nitrosodlmethylamine
U
0.000998
0,0100
1
06/09202108:21
WGI684262
n-Nitrosodiphenylamine
U
0.00237
0,0100
1
06/091202108:21
WG1684262
n-Nitrosodi-n-propylamine
U
0.000261
0.0100
1
06/09/202108:21
WGI684262
Phenanthrene
U
0.000112
0.00100
1
06/09/202108:21
WG1684262
Senzyibutyl phthalate
U
0.000765
0.00300
1
060202108:21
WG1684262
Bis(2-elhylhexyl)phthalate
U
0.000895
0,00300
1
06109202108:21
WG1684262
DI-n-butyl phthalate
U
0,000453
0,00300
1
06109202108:21
WG1684262
Diethyl phthalate
U
0.000287
0,00300
1
0610M02108:21
WG1684262
Dimethyl phthalate
U
0.000260
0.00300
1
06109202108:21
WG1684262
Di-n-Wyl phthalate
U
0.000932
0.00300
1
061091202108:21
WG1684262
Pyrene
U
0.000107
0.00100
1
061091202108:21
WG1684262
1,2,4-Trichlorobenzene
U
0.0000698
0.0100
1
06/09/202108:21
WG1684262
4-Chloro-3-methylphenol
U
0.000131
0,0100
1
061091202108:21
WG1684262
2-Chlorophenol
U
0.000133
0.0100
1
06/09/202108:21
WG1684262
2.4-Dichlorophenol
U
0.000102
0,0100
1
06109/202108:21
WG1684262
2,4-Dimethylphenol
U
0.0000636
0.0100
1
06/09/202108:21
WG1684262
4,6-Dinitro-2-melhylphenol
U
0.00112
aoloo
1
06/09/202108:21
WGI684262
2,4-Dinilrophenol
U
0.00593
00100
1
06/091202108:21
WG1684262
2-Nitrophenol
U
0.000117
0.0100
1
06/09202108:21
WGI684262
4-Nitrophenol
U
0.000143
0.0100
1
06/092021 08:21
WG1684262
Pentachlorophenol
U
0.000313
0.0100
1
061091202108:21
WG1684262
Phenol
U
0.00433
0.0100
1
06/09202108,21
WG1684262
2,4,6-Trichlorophenol
U
0.000100
0.0100
1
06/091202108:21
WG1684262
(5)2-Fluorophenol
55.1
10.0.120
061091202108.21
WG1694262
(5) Phenol-d5
38.6
800424
06109/202108:21
WG1684262
ACCOUNT:
PROJECT:
SDG:
DATEMME:
Eaton Corporation
28091-R
L1362234
061212109:45
PAGE:
7 of 23
NE ENTRY
Collected date/time: 06/03/21 17:50
SAMPLE RESULTS - 01
L1362234
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
mg4 mg/I
mgA
date/time
tS) Nitrobenzene-6
88.5
15.0-314
061091202108.21
WG1684262
(S)2-Fluorobiphenyl
73.7
22.0-127
061091202108.21
WGI684262
(S) 2,4,6 Tribromophenol
102
10.0453
061091202108.21
WGI684262
(S)p-Terphenyd14
73.7
29.0-141.
067091202108:21
WGt684262
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Eaton Corporation 28091-R L1362234 06012109:45 8 o123.
WG1686421
QUALITY CONTROL SUMMARY
Gravimetrlc Analysla by Method 2540 D-2011
L1362234-01
Method Blank (MB)
Cr/
IMBIR3666326-1 06MO/2117:45
MR R.ft M8 G.K. MR MDL MR RDL
Analyle mgA mgA mgA
C
Suspended Mies U 2.50 250
'S$
L1362087-01 Original Sample (OS) • Duplicate (DUP)
(OS) Lf362067-01 06O00 nR45 -(DUP) R36663263 061100 0:45
n
Or1ynM Result DUP RewX Mutton DUPRPD
P.M.W
DUP RPO
LWM
6$f
Anayb mgA mgA %
%
Suspended blMs 188 21.0 1 15.7
PI
5
L1362208-01 Original Sample (OS) • Duplicate (DUP)
'GI
(OS) 1136220841 06AO/2117:45 • (DUP) R36663264 O6a0/21 p:45
Orfglnel Rewll DUPRewX OMW DLIPRPD
DUP04,41ft
LDuPRPO
0AI
AwLyU mgA NA %
%
Suspe^detl blNS 106 IL] I 5.50
PI
5
eSC
Laboratory Control Sample (LCS)
(LCS)R3666326-2 O6/10/2117:45
Splet Am0u1A UZResuR LCS R.. R.. LMitf LCS 0w110er
A.M. MA mgA % %
_......_.___—_._._.-_.—-- —___ _—
SuspelMedSolks ]]3 836 108 89-ttd
ACCOUNT: PROJECr: MG. DATE/TIME PAGE:
E.b Corp0ra0m 21Ntli" L13622N 06RWI()9:45 9of 23
WG1686563 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 16648 1,1363134-6t
Method Blank
(Mail R3665847-1 06nO1212011
NO Result ME Qualifier MO MOL ME ROL
AeeMe mgA mgA mgA
TPH -Oil&Grease D 0.725 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 1?366584b2 06/10/2120.11 • (LC50) R366584
SPlke Amdu t LCSRMK
An4Me mgA mgA
TPH-Oil& Grease 400 35.O
LCSO Residt LCS Rec LCSO Rec Rec, Limps LCS O_almer LOSDOIulIRe1 RPO
mgA It % % %
389 92.5 973 640-132 10.6
ACCOUNT: PROJECT: SOG:
Eirt n Cortwlallan 1809411 L1362234
RPD Limits
34
DATE/TIME:
O6120109:45
PAGE:
10 or23
WG1690234
QUALITY CONTROL SUMMARY
Metals (ICPI 6y Method 200.7
L136223401
Method Blank (MB)
_
C
(MB1R3668908&1 0"7/2120:09
)I
MR Result M6 O_all0er MR MOL
MRRDL
AR61/te mgA m9A
m9ATC
Copper U 0.00216
0.0100
Lead U 0.00227
000500
355
21nc U 000578
00500
Cn
Laboratory Control Sample (LCS)
{LCS) R3668908-2 O6I17/2120:I2
$f
Spite Amount LCS ResuR LCS Red.
R.. LRniN LCS DuMli%r
Atw," mQA mgA %
%
a
Copper 100 0961 961
05.0415
Lead. 100 0965 96.5
850-.115
0
Zlod 1.00 0953 953
85.0-115
(jl
L1360805-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
aAl
(OS) 11360805 ti MA7i2120:M • (MS) R36689084 06RA212019 • (MSD) R3668908-5 06A7/2120:22
s
Span Arndi OrlgRlal R.A MSR.A
MM ResuR MS Red. MSD Rec. 1)1l
Red. UinRs ME OuaMln
MSD OuaIMMr RPO
RM t1mRs
$C
Malyte mgA mgA mgA
Rtv % %
%
%
%
Copper 100 000116 0981
0974 976 969 I
]0.0-130
0314
20
Lead 1.00 U 0982
09M 98.2 976 1
70.0-130
0567
20
Inc 1.00 000948 0.958
0952 94.8 94.3 1
70.0-130
0558
20
L1362251-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS7 L1362251-02 06A7]212o25 • (MS) R3668908-6 06A712120 27 • (MSD) R366890&7 (XiMnl 2029
SpiteftwAt
Otglnal Restif MSResuR
MSD R.ft
MS Red.
MSD R..
DliMon Red. L9nM
MS OuallOer MSD Qualifier RPD
RPD LimRe
AR*W
m9A
m,A m9A
mgA
%
%
%
%
Copper
1.00
U 098]
0981
98]
98.1
1 700-130
0.614
20
Lead
1.00
U 0.987
0.981
98.7
98A
1 70,0430
0.296
20
21na
100
U 0.959
0956
959
95.6
1 MO-130
0.352
20
ACCOUNT: PROJECT: 60G: DATE/TIME: PAGE:
Earon Carporanon 26091.R 11361234 06/21009M5 11a123
WG1683600 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GCIMS) by Method 624A 0362234-01
Method Blank (MB)
(MB)R3664179-3 0610512120:34
Cp
MBReault
AnaMe mgA
... ___...
MB OoMdler MB MOI
mQA
MB RDL
mgA
Aaokm U
.__..
00015d
___..
00500
AcryWnhrik U
0.000671
0,0100
3$5
Benzene U
0.0000941
0.00100
Bromodl<hlofomethane U
0.000136
000100
Bmmotorm U
0,000129
0.00106
Cn
Bromamethene U
0.000605
0.00500
Carbon tetrachloride U
0000128
0,00100
a
$f
Chbrobenlene U
0.000116
0.00100
Chlcumiromemethane U
0.000140
0.00100
Onameme s - U
0.000192
0.00500
2-01oraelhylmrMether U
0000575
0.0500
Chwmrorm U
0oo0111
000500
TGI
Chloromethane U
0000960
000250
1.2-0Icbbrobenzene U
0000102
0.00100
aAl
1,3-Obhbrobenxne U
0000110
000100
1,4-0bhbmbenfine U
0.000120
0.00100
01<hblooffluoromethene U
0,000374
000500
e$C
M-0Ichlomebane U
0,000100
0,00100
1,2-0lcbbroethane U
00000819
0.00100
1,14tolometherm U
0.000188
0,00100
trans-1,24)Ichbmethene U
0,000149
0,00100
1,2-Dichloapropane U
0.000149
000100
ds-t3-0Inhbropnopeoe U
0.000111
0,00100
transs1,3-0Ichbm res, ne U
0.000118
0.00100
Ethyloemene U
0,000137
0,00100
Medrylerre Chloride U
0.000430
0.00500
1,1.2, 2 TetrinnIomethana U
0000133
0,00100
Tetmchbroethene U
0.000300
0.00100
Toluene U
0.000278
0,00100
1,1,18rkhbmethanc U
0.000149
0.00100
11,24rchloroetrane U
0.000158
0,00100
TrlMbroethene U
0.000190
0.00100
Tdrnbroflumomethane U
0.000160
0,00500
VN tllbride U
0.000234
0.00100
(5/2oAxne4 03
800120
RI FBromoRumheneena 9a0
WO120
f5) E2-UkhbmehahuneE 10
M.."30
ACCOUNT:
PROJECT:
MG: GATE2TWE PAGE
Eaton C...... Oon
2809LR
L1362234 M21I2109:45 12 of 23
WG1683600
QUALITY CONTROL SUMMARY
Volatile Organic Compounds
(OWNS)
by Method 524A
J4362234.01
Laboratory Control
Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
CP
ILCS)R3664179-1 06/05/211912 •(LCSD)
R3664179-2
06/05al 1933
Spll,Amount
LCS Real
LCSD Result
LCS Rec. LCSD Rec.
R. Lando LCS Qualifier LCSD Ouallhar
RPO
RPD Limits
a6_/le-
gA
p_oi
gA
%
%
%
%
T
_An.
0250
.
0.05800157
.% ...-.-
63.
0635
20A<mlem
Acrytanlblle
00250
0.0209
0,0205
836
820
60,0440
1.93
20
3$5
Benzene
000500
0.00464
0.0046S
We
930
650-135
0,215
20
Bromodichbromethahe
0.00500
0.00496
0.00502
99.2
100
650-135
1.20
20
4
Bromoform
0.00500
0.00402
0.00400
80.4
Roo
700-130
0499
20
Cn
Bromome0lane
0.00500
0.00572
0.00564
114
113
150-185
1.41
20
Carbon tetrachloride
0.00500
0.00449
0.00440
Ke
88.0
70013D
2.02
20
65T
Chbrobenzene
000500
000Am
0,00465
92.5
93o
mo-135
OA31
20
Chbrockmarrmmethane
000500
0.00484
0.00484
96.8
96.8
700-135
0.000
20
ChbmeMane
0.00500
000682
0.00685
136
137
400-160
OA39
20
2{ loomdl,yl ali ether
00250
0.0227
0.0720
90.8
88.0
0.100-225
3,13
20
Chloroform
000500
000497
0,00513
WA
103
700435
3.17
20
[GI]
Chloromelbane
000500
000622
0.00638
124
12B
0.100-205
2,54
20
12-0bhbrabenzene
000500
000454
0.ON71
908
94.2
650-135
3.68
20
a
1.3-Dlcbbrobenzene
0.00500
0.00469
000505
938
101
70.0130
7.39
20
AI
1,4Dlchbfobanzene
0.00500
0.004M
0.00505
95.6
bi
650435
549
20
DidllomdlRuoromebane
0.00500
0.00445
0.ON72
no
94A
49.0-155
5.89
20
S$C
13-0ichm "immersing
0,00500
0.00524
0.00531
105
106
70.0-130
1.33
20
1.2 Dichlomethane
000500
0.00486
000507
972
101
700-130
4,23
20
1,1DRhlofcethene
0.00500
0,00487
000508
97.4
102
Wo450
/22
20
bans-1,2-0khbrcemene
0.00500
000508
000529
102
106
70.0-130
405
20
1.2-Dichbrcpropane
0.00500
0.00535
0.0051I
107
102
350-165
4.59
20
cis-1.3-0ichbropropene
000500
0.00484
0,00473
969
94.6
250-175
2,30
20
trans1,3-0ichbropropene
0.00500
000M3
000458
me
91.6
50.0-150
3.33
20
6thylbenzene
0.00500
000477
000463
954
92,6
60.0-140
2,98
20
Methylene Chloride
0.00500
0.00485
Doomfi
97.0
101
600440
4.24
20
1.1,2,2-Tebechromethxne
000500
0.00476
0.00507
95.2
101
600-140
6.31
20
Tebachbmethene
0.00500
0.00459
0.00467
918
93.4
70.0-130
03
20
Toluene
000500
000441
Dome
88.2
898
700-130
1.80
20
t,t,t➢IchbrceNane
0,00500
0,00500
000516
100
103
70.0-130
3.15
20
11.2-Trl<hbroelhane
000500
000489
0.00471
97.8
94.2
700430
3.75
20
Trlchbroetherle
0.00500
0.00462
0o*481
92A
96.2
65.0436
4.03
20
Tr blblorodromethane
0.00500
000458
0.00501
99.6
100
50.0-150
0601
20
Mini chloride
0.00500
Dome
0.Dome
lie
Ito
5.00-195
3.46
20
/5) TONene-d8
103
02
80.0120
IS) 44Bmmoibwpberue.
97.8
no
80.0420
l5)t2-DkAbroemdne44
108
w
700130
ACCOUNT: PROJECT: SOG: DATE/TBAE: PAGE
Eaton Corporation 38091-R LI362234 06121M 09:45 13 of 33
WG1684259
Pesrlciees (GC) by Method EPA 608.3
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1362234,01
C47
(M8) R3665513-1 06108M 16A5
MB Resuh MB Walther
MB MOL
M8 ROL
,
_A_a_lyse mgA
mgA .
TC
Atkin U
_00s
_gA
0,0_0.s0oo0t
Alpha BHC U
0,0000172
00000500
a$S
BeW BHC U
0M00208
0,0000500
Delta BHC U
010000150
0,0000500
4
Gamma00 BHC U
000209
00000500
Cn
4,142DD U
0.0000m
00000500
4,44)DE U
0.0000154
00000500
a
Sr
4,4-0DT u
0,0000198
0.0000500
OlekM U
0.0000162
0.0000500
ErkomBenI U
00000160
00000500
■
Erdosulwn 11 U
0.0000164
0.0000500
EnaoSuBxn SuMale U
00000217
0.00005()0
7G1
Enerin U
00000161
00000500
EntrinaWehytle U
O-OM237
0.0000500
y
EntlM ketone U
0,0000219
0.0000500
AI
Hepladrbr U
0.00(flam
00000500
Heptatlrbr epodoe U
00000183
00000500
eSC
Heachlorobervere U
OA000176
0.0000500
Methoeychlor U
0.0000193
0.0000500
ChbrEana U
00000198
000500
To apherm U
o 000168
0000500
137De -hb1-dp7)el 1 56.o
U.0-144
(5) wtro hbo maylene 68.5
706t35
Laboratory Control Sample (LCS)
(LCS)R366551}2 06/08/2110.57
Sp)ke Amount
LCS Resuh
LCS Rec.
R.. Lkeha LCS Gualft.
Anelyte
mgA
mgA
%
%
Akan
0.00100
0000838
83.B
42.0-140
Alpha BHC
000100
0000948
94.8
37,0440
flew BHC
000100
0.00103
103
17.0-147
OeAa BHC
000100
0,000940
94.0
19,0440
Gamma BHC
000100
0.000971
97.7
320-140
4,4a0D
0.00100
0.00104
1N
310.141
4,4-DDE
000100
0000899
B9,9
300-145
4,4-DDT
O.00WO
0.000B70
87.0
25.0-160
Okkrin
000100
000101
101
36.0-146
EnOoeuBanl
0.00100
0.000949
94.9
45.0-153
ACCOUNT:
PROJECT: SOO. DATE(TIME: PAGE:
Eaton Corporation
26094R L1362234 06Rlnl 0945 14 o123
WG1684259 QUALITY CONTROL SUMMARY
Pesticides IGCI by Method EPA 608.3 L1362234-01
Laboratory Control Sample (LCS)
C
(LCS) R3666513-2 O6/0822116.57
P
Splits Amours
LCS Result
LCS Rec.
Rec.Llmlts
LCS OuallOer
AnaMe nFl
mgA
%
%
TC
Endosulfen ll 000100
0.00104
fOd
100-201
EnOosuBan Wide 000100
0.00105
105
2&0-144
s$5
Endrin 000100
000101
101
300-10
Endrin Mehyde 000100
0.00197
197
560428
J4
4
Enddn ketone 000100
0000996
99.6
54.0142
Cn
Heptachlor 0,00100
0000875
875
34.0-140
Heptachlor epoxide 000100
0.000957
957
37.0-142
Syr
Hexachloroben2ene 000100
0.000760
76.0
35.0-120
Metiwxychkb 0.00100
000106
106
440460
A)DecachbroOlPAenyl
707
V..0-144
■
(S)r.occhbro-rn 4*ee
7J0
"..a 735
GI
Original Sample (OS) • Matrix
Spike (MS) • Matrix Spike Duplicate (MSD)
aAl
(OS) •(MS) R3665513-3 06/082119:01•(MSD)
R36655134 06/OSM 1913
Spike Atmunt
OrglnalRrnM MS Result
MSD R.ft
MS Rec
MSD R..
Dimon
Rec. Limtts
MS Oualiher
MSD Qualifier
RFD
RPD❑mm
Ansloe mgA
mgA
mgA
%
Is
%
%
Agrb 0.00100
OOOOA3
0000195
71.3
195
1
/2.0440
P
J3 JSP
119
35
Alpha BHC 0,00100
0.000898
0.000676
83A
60.9
1
37.0.140
P
28.2
36
Beta BHC 0,00100
0000676
0.000620
67.6
62.0
1
170-147
P
8.64
A
Deha BHC 0.00100
0.000875
0.000728
87.5
728
1
19.0-140
P
P
18.3
52
Gamma BHC 0,00100
0.000877
0,000675
877
ET5
1
320-140
P
P
260
39
4,4-0DD 0.00100
0.000709
0.000232
70.9
231
1
31.0441
P
73 J6 P
101
39
4A-00E 000100
0.000638
0,000131
63.8
131
1
300445
P
J316
132
35
4,4-007 ODOM
0.000606
0.000140
60.6
1A.0
1
15.0.160
P
JJJ6
s25
42
Ddddrm a 00100
0.000762
0.000320
76.1
32.0
1
36.0-146
P
J3 J6
817
49
Endosug.b 1 0.0000
0.000581
0.00218
58.1
218
1
4S0453
P
J3 J6 P
116
28
EndosuBen ll O W
0000858
0000484
85.8
48.4
1
1.00-202
P
J3
55.7
53
EnclosuRen su8ate 0.00100
0.000874
0.000542
0.4
54.2
1
26.0-td4
P
A P
46.9
38
Endrin OOOM
0000853
0,000387
85.3
387
1
30,0447
P
J3P
75.2
48
EnorinaMehyde 0.00f00
0,00160
0,00109
160
109
1
56.0-128
&P
73P
37.9
20
EnUhn ketone 0.00100
0.000971
0.000651
97.1
65.1
1
54.0-142
P
J3P
39.5
20
Heptachlor 0.00100
0.003715
0.000208
n.5
208
1
34.0d40
P
J3 A P
110
43
Heplachbr epoxide OOOTO
0.00186
0.0005A
186
579
1
370-142
35P
J3P
M5
26
Hexachlorobebsene 0.00100
0.000782
0,0000803
78,2
8.03
1
35.0420
P
73 J6
163
25
Methoxycblor 000100
0.000751
0,000280
75.1
28.0
I
44.0-I60
P
J3 J6 P
91A
22
rS)D4eachbro&,PW d
483
103
10.0144
/S)Tendchbro m-xyleae
52.1
103
100135
ACCOUNT: PROJECT: SOG: DATE,'TIME:
Eeton Corporative 2a091.R L1362234 OWnt 09:4S
PAGE:
150123
WG1684259
QUALITY CONTROL SUMMARY
Polychlorinated Biphenyl¢ (GC) by Method EPA-608.3
L1362234-01
Method Blank (MB)
(Mal R3665296-1 06/081211649
1
Me ResuR ME Quall0er
Analyte mg4
ME MOL
mgA
MR ROL
mgATC
PCB 1260 U
0.000173
0.0005o0
PCB 1016 U
0.000270
0.000500
$5
PCB 1221 U
0.000220
0.000500
PCB 1232 U
0.000270
0.000500
aCn
PC81242 U
0.000270
0,000500
P081248 U
0,000173
0.000SOO
PCB 1254 U
0.000173
0.000500
IS/Oecahbmblpheryl 60.5
now
r
IS]
(5) rehochbro m-ryle. 26.1
100-135
Laboratory Control Sample (LCS)
GI
(LCS) R3665296-2 06/08/2116.58
Spike AmoulR LCSRd.ft
LCS Rec,
Rec. Llmlis LCS 0udtlfler
AnaMe mgA m9A
%
%
Al
PCB 1260 0.00250 000128
512
800-140
PCB 1016 0,00250 0.00363
145
500-140 AP
SC
(S) Ve hbmbiphenyl
491
10.0144
p'J Tetrxhbro-mOkrle
I13
10.0 U5
ACCOUNT: PROJECT: SOG: DATE/TIME PAGE:
EeWn COryare0. 2809M L1362234 OW21/2109A5 16 or 23
WG1684262 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounde (GCIM51 by Method 625.1 0362334.01
Method Blank (MB)
(MB)R3664843-3 OM96nO0:38
MB R.ft
MBOualRler MB MOL
MB ROL
Mayta
Aura-
mgA _-_
NA
___ _...__._._.
"A
Acenaphthene
a
0.0000886
000100
Acenaphthyle.
u
0,0000921
0.00100
Anthracene
u
00000804
0.00100
hobeniene
u
0000105
0,0100 -
Beneldlne
u
0,00374
0.0100
Benio(a)anlhracene
0
0000199
0,00100
Ben7o(b1fluoranthene
u
0000130
000100
BentoMfidaranNerw
u
0.000120
0 00100
Benm(g.RgpeMe^e
u
0000121
0.00100
Senio(a)pyrene
u
C 0000381
000100
Bls(2-cAbrettoxomehame
a
0.000116
0.0100
Brsl2thlomethy0etner
u
0,000137
0.0100
22-0aybla(1-Chloropropane)
U
0000210
00100
44komaphilir"henyleNer
U
0.0000877
0.0100
2-ChbronaphNalene
U
00000648
0.00100
HTbraphgmy,henyktner
U
0.0000926
0.010)
Chry d
u
0000130
000100
Obemlle,hbnthiacene
U
0.0000644
0.00100
3.3-0IchbrobemMine
a
0.000212
0.0100
2.4-01ndrotobene
U
0.0000983
0.0100
2,6-Dinnrntoluene
a
0000250
00100
Fbpranffiw
u
0.000102
0 00100
Fluorine
U
0.0000844
0.00100
14mchlorobentare
u
00000755
0,0010
Hexarhl0ro-1,34outadiene
a
0.0000968
0 0100
Hettachlordcyclownsedlere
U
0.0000598
0.0100
Nexachloroelhane
a
0,000127
0,0100
lndeyy1,23tdlpyene
u
0.000279
0.00100
Isoplmrone
a
0,000143
0,0100
Naphthalene
u
0.000159
0.00100
Nllraben7ene
a
0000297
0.0100
nNmosodlmethybmrte
u
0.000998
0,0100
nNhrosodiphenylamme
a
0,00237
0.0100
nNArosodlonyaopYMmine
a
0.000261
0.0100
Phenan0lrene
u
0 000112
0.00100
Ben3y4buM phthalate
u
0.000765
0.00300
Bis(22thythexyAphihalale
a
0.000E95
0.00300
DM43uMph0alate
u
0.000453
0.00300
Diethyl phthalate
a
0000287
0.00300
Dlmet00 phthabte
u
0 000260
0,00300
ACCOUNT:
PROJECT:
Eaton
Corporation
29091-R
6DG
L1362234
DATEITNE:
06I2V21SPAS
PAGE:
17 or 23
WG1684262 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1362234-01
Method Blank (MB)
(MB)R3664S43.3 06/09/2100:3a
ME Result
AnaMe m9A
ME OualRier ME MU
m9A
ME RDL
mgA
-I(
U�-naclyl phthalate U
0.00093]
0.00300
Pyrene u
0.000107
0 00ro0
Ss
1,2/-irlcMoropenierre U
00000698
0.0100
4-CAbra3meNyiphenal u
0.000131
0.0100
1�brophenal U
0.000133
0.0100
CO
2.40chbrophenai u
0.000102
0.0100
244Amemylymrol U
00000536
0.0100
s$f
4,6-0InBrt-2-me"Insnol U
0.00112
0,0100
2.4 Ineiophenoi a
000593
0.0100
N4Nophenol u
0.000tn
0.0100
4-NRmphe.1 J
0,000143
0.0100
PanMchbrophenol U
0,000313
0.0100
TGI
Phepol U
0.00433
0.0100
2A.6-TAchlomphenol a
C.000100
0,0100
aQl
(S)NttrbGenlened5 673
150-314
(S) 2-FNomhlpheny, 738
22.0127
fs/PTamhogy m SZ3
290141
S$C
!S)PAandd 28.9
8.00424
IS) 2 FArompherol 446
100120
IS) 2.4.6.7ribromophenol 710
10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3664843-1 06/OMI 23-50 • (LCSD) R366484}2 06109/210014
Spike Amount
LCSRes Jt
LCSD Result
LCS Roc
LCSD R..
Rec Lash
LCS OuallRer LCSD OueliRar RPD
PRO Lands
Mayle
mgA
mgA
mgA
%
%
%
%
It
%
_...__
A<enaphNeite
__. - -
00500
0_
0370.0310
_._.--'-.
0.0365
74.0
__ _-- - __-_-_
13.0
47.0-145
_.
1.36
-
48
Acendiddrykrle
0.0500
0,0395
00387
79.0
77.4
33.0-145
2.05
74
Anthracene
00500
00408
0,0403
$1.6
80.6
27.0-133
1.23
66
Aeobensene
0.0500
0.0360
0.0365
73.6
73.0
37.0425
0.819
20
Benabine
0100
0.0129
0.00561
12.9
561
1.00120
J3 ME
36
Benage)anthmcene
0.0500
0.0464
0.0449
92.8
$9.0
33.0-143
3.29
53
Benao(b)Ouorantheoe
0.0500
0.0429
0,0421
858
84.2
24.0-159
1.88
71
Beao(k1ftMorinthene
00500
0.043
0.0437
88.6
87.4
11.0-162
136
63
Mitiolg,h.lipeMene
0.0500
00395
0.0379
79.0
ME
1 00-219
4,13
97
Banro(a)pyrene
0.0500
0.0426
0.0411
85,2
82.2
17.0463
3.58
72
81s12<bbremox,imethera
0,0500
0.0309
0.0310
618
610
1.00.219
0.323
54
Blsl2,chbmear,"m
0.0$00
0.0345
0.0342
6910
68.4
33.0485
0.873
108
22-0,gohr{Tbropropene)
00500
00360
00357
72,0
A
360-166
0837
76
ACCOUNT:
PROJECT:
SDG;
DATEITIME: PAGE
Eaton Corpweaan
28091
L1362234
064Hnl 09.45 18 of 23
WG1684262
QUALITY CONTROL SUMMARY
Saint Volatile Organic
CarnpoundS
(GC/MS) by Method 625.1
t1362234�01
Laboratory Control
Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
Cp
(LCS)R3664843-1 0620822123:50•(LCSD) R3664843.2 06A091210014
Sputa Amount
lCS Rewb
LCSD Rewb
LCS Rec. LCSD R.,
A. LIm86 1C50ualtller LCSD Oualft
RPD
RPO Levity
2
Analyte
mgA
mgA
mgA
%
%
%
%
%TCl
4-8romophenyl-pllenylelher
00500
00410
0,0410
82.0
82.0
53043]
0,000
43
HhWronaphthaWre
005DO
00371
0.0364
74.2
728
60.0-120
190
24
a$a
4{hlorapheriN4llenNelher
00500
0.0438
0.0434
87.6
86.8
25.0-158
0.917
61
Chrysene
00500
0.0443
0.0423
88.6
84.6
17.0-168
4.62
87
DOeni(a,h)anlhracene
00500
0.0402
0,0386
80.4
77.2
1.00-227
4.06
126
Cn
3.30chloroben2idme
0100
0.0059
0.0819
859
819
100-262
4D
108
2,4-OlnttroloWene
00500
0.0488
0.0507
97.6
101
39.0-139
382
42
- S$(
]6Llnitrotoluene
0.0500
0.0458
0.0450
916
900
500-158
176
48
FWoranthene
00500
00461
0.0451
927
90.2
26.0-137
2.19
66
Morena
00500
0.0425
0.0416
850
83.2
59.0-121
2,14
38
■
Hevadibrobenzene
0.0500
0,0392
0.0383
78A
76.6
1.00452
2,32
55
HeucntoroA.3-0 tedmw
00500
0.0373
0.0381
74.6
76.2
24.0-120
212
62
TGI
Nerechlorocycbpentediene
0.0500
00231
0,0230
462
46.0
10.0-120
0.4N
31
Heaachicroethane
00500
00349
0,0349
699
698
40.0-120
0000
52
e
Indeno0,2.3uypyrene
0.0500
0.0376
00353
75,2
70-6
1.00-171
6.31
99
%AI
6ophorone
00500
00311
00314
62,2
629
21.0-196
0.960
93
Naphthalene
00500
00328
0.0331
65.6
66.2
2LU133
0910
65
e$C
lRobemene
0.0500
00304
0.0304
60.8
608
35.0-180
0000
62
nAttromtlimethylamIne
00500
0.0210
0.0218
42.0
43.6
104120
3.74
34
nNhrowb0ha,brMre
00500
003➢
0.0370
754
740
440420
1.87
21
"DowdM-0ropylamine
0.0500
0.0339
0.0345
67.8
69.0
100-230
1.5
87 -
Phenanmrene
00500
0.0410
0.0402
820
BOA
54.0-120
1.97
39
Scraylbuto"alate
0.0500
0.0436
0.N32
87.2
06A
100452
0,922
60
81s(2eNNheayiphthalate
00500
00402
00385
80A
720
8.00-158
4.32
82
OPodutyl phlbelate
00500
0.0445
0.0441
Wit
8131
1.00.120
0.903
47
,
Dlemyi phthalate
0.0500
0.0438
00443
8t6
886
1.00-120
114
100
DlmeNyl phhalate
00500
0.0420
0.0416
84.0
83.2
1.00420
0.957
183 -
Dlocctylphthalate
0.0500
0.0383
0.0365
76.6
73.0
4.00-146
4,81
69
Pyrene
0.0500
0041
0.0446
88.2
89.2
52.0-120
L13
49
1,2,-Trrhlorobeneene
00600
00362
0.0368
72.4
73.6
440-142
L64
50
4{ 1,00-lmethylpheral
0.0500
0,0312
0,0314
62.4
62.6
22.0447
0.639
73
2Chlorophenol
0.05M
00337
0.0339
674
628
230134
0.592
61
2,401rhlorophenol
0.0500
0.0347
0.0350
69A
70A
39.0435
0.861
50
24-01methbphenol
0.0500
0.0299
0.0298
59.8
576
32.0420
3.75
58
4.6-0mtlro�2m thylpheool
0.0500
0,0538
0,0546
108
109
1.00.181
1.48
203
2,4LIn8rophenol
0.0500
0,0485
0.0509
97.0
102
100491
4.83
132
2N11rophen0l
0,0500
0.0362
0.0378
72.4
75.6
29.0482
4.32
55
4Nitropheml
0.0500
0,0139
00156
27,8
31.2
100-132
11.5
131
Pentachlorophend
00500
0.0409
0,0430
81.6
$6.0
14.0-176
6.25
86
Phenol
0.0500
0.0154
0.0162
30.8
32.4
5.00.120
5.06
64
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Eaton Corporation 28091-R L1362234 06221RI 09:45 19 or 23
WG1684262 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1362234-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
/.
(LCS) R36648434 06108¢123.50 • (LCSD) R3664843-2 06/091210014
P
Spike Amount LCS ResuR LCSD Result LCS Rec.
LCSD Rec.
R. Large LCS OualMor LCSD Warier RPC RPO Umtts
Anatyte mgA mgA mgA %
%
% % %
TC
2,4.6-TSICAbrophenol 0.0500 0.0395 0.0397 79.0
79.4
V,O-W 0.505 58
(S)NArobemened5 510
624
15.O N
3$S
(SJI FA.nroblPbenyl 80.4
77..2
220-121
(5) ag0anywAr 810
78.8
29,091
(3)PAero7d6 30.3
323
8.00<24
Cfl
I5)2-fuhmpherol 472
4Z3
0..0-120
tS) 24.67nbromoPAeno1 800
82.5
W.P153
SSf
ACCOUNT: PROJECT: SDG.
Eaton Corporation 28091-R 1.1361134
DATE(TIME:
061211210945
PAGE
20 o(23
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below Is designed to better explain the various terms used in your report of analytical results from the Laboratory. This Is not
Intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer- Information that may be provided by the customer, and contained within this report, Include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Datesrrlmes, and
Sampling Location. Results relate to the accuracy of this Information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit
RDL
Reported Detectioniimit
Rec.
Recovery.
RPD
RelafvePercent Difference
.that__ ._
SDG
Sample Delivery Group.
h-�
Surrogate (Surrogate Standard) - Analytes added. to every blank sample, Laboratory Control Sample/Duplicateand
;(S)
Matrix Spike/Duplicate, used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be.
detected in all environmental media
U
Not detected at the Reporting Limit (or MDL where applicable).
al
Abalyte
The name ofe pa thrticular compound or analysis performed: Some Analyses and Methods well have multiplearialytes 1
,
If the sample matrix contains an intedering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analyzes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
�
These are the target %recovery ranges or %difference value. that the laboratory has historically determined as normal
!Limits
for the method and analyze being reported. Successful QC Sampleanalysis will target all analytes recovered or
�..
duplicated within these ranges..
Original Sample
The non -spiked sample in the prep hatch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be Included within the reported SDG.
l
___.._ _. and/or.
This column piovioes a letter and/or number designation that corresponds to additional Information concerning the result
,Qualifier
reported. If a Qualifier is present a definition per Qualifier is provided within the Glossary and Definitions page and !
I
potentially a discussion of possible Implications of the Qualifier in the Case Narrative If applicable.
_ .__._ that._ _.._....._. _
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND' (Not Detected) or "BDL"
Result
(Below Detectable Levels). The Information in the results column should always he accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
(Uncertainty.
,(Radiochemistry)
Confidencelevel,of 251gma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report
i. __ _____._..tclud_�
This section of the report includes the results ofihe laboratory quality control analyses required by procedure or
Quali-t Control
SSummary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verity the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
_.. _ _ .-_. __ __ _ ___ that __._ _ __. .. _..-.. . _.. _ y . _ ... _ _ _ ..
This section of your reportwill provide the results of all testing performedon your samples. These results are provided
Sample Results (Sr)
by sample ID and. are separated by the analyses_ performed on each sample. The header line of each analysis section for:
each sample will provide the name and method number for the analysisreported. _
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
_ _. _. _._..._ __ .___ _ _._. ___ __...._. -b_...-..___.__ __.._ _._ __._.... —__ -_._._ _. _._
The associated_batch QC was outside the es_ta611shed qualitycon_Vol_range_for_precisio_n. _
J4
The associated batch QC was outside the established quality control range for accuracy.
_._____-_ _._.____f. _____________.—make---___ ---___that
_uc.—_. ---
'The sample_maViz i_nt_ertered witfi the ability to make any accurate determination _spike value is high:
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
jP
_ RPD between the primary and confirmatory analysis exceeded 40%. !
.._.______ _ _._________
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT. SDGDATE/rIME:
Eaton Corporation 28091-R L1362234 06/212109:45
PAGE:
21 of 23 '
ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
A20612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
Newyork
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohl.—VAP
CLOO69
Illinois
200008
Oklahoma
9915
Indiana
C4N-01
Oregon
TN200002
Iowa
364
Pennsylvania
6802979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' °
KY90010
South Carolina
84004002
Kentucky'
16
South Dakota
Na
Louisiana
A130792
Tennessee"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
Wert Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21A
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
QLA— ISO 17025°
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15.00234
EPA—Crypto
TN00003
'Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity 'Chemical/Microbiological "Mold "Wastewater are Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported In the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE7TIME:
Eaton Corporation 28091-R L1362234 06/21/21 09:45
PAGE:
22 of 23
f � -
M. amrmdAddmanY-e,s;'
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Eaton
NA Finandal SenfVeS Ceniir I'M
1009
2564 Durham Road'
PO Box 818024
Ftoxhoro,NC27573
Cleveland, OR 44181-802
Edmara Bloomer
afty/staw
can.*:
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336 541 11,41
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qFr
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6-3-.21
$!Log
'S'
X-
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Slqnd/Mcmc..:
ww-wat Water
FWw Othn,
mY'lulakInSWater
Sanmks.urnM�Ia:
r
suffiqiatnt val� ents 1/ L-N
W - OtIr
_Courier -S
T raWns ii si (r3 cl i
If Al,,Iie.hl,
WA ft�. N
Pfcaervation �rwt/Ctmnk.d: I N
PuO Sateen 20.5 "Ihrt 2v —N
AeH,�hedby:jS1gnvtLm.) Pat
TAPIMankmannd! Y.,W,
I'nm:
pN
TIR
v Data:
Re-I,nnd W. INF-tamal
Timfllw Ic Blr L�
lf"e,emti.n�frelky�gtn:Date/Nme
eels wished by: Mgmatural Date,
Time:
Rnwp?bbbr.(SJp.t.m) v
Data,
H
CamflIA
KA P
A 'I ,
aceAnalytical e ANALYTICAL REPORT
June 18, 2021
Eaton Corporation
Sample Delivery Group:
Samples Received:
Project Number:
Description:
Site:
Report To:
L1362288
06/05/2021
28091-R
Eaton Corp Monthly Stormwater
ROXBORO,NC
Edmara Bloomer
2564 Durham Road
Roxboro, INC 27573
Entire Report Reviewed By: 4l
Heather J Wagner
.._, Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shalt not be
reproduced. except In full. without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV -SOP MTJL*67 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
0 4
4
ACCOUNT: PROJECT: SDG: DATE/TIM E. PAGE.
Eaton Corporation 28091-R L1362288 0618.2116.35 1 of 23
TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
SS
OUTFALL 005 L1362288-01
5
aCn
Oc: Quality Control Summary
9
Gravimetric Analysis by Method 2540 D-2011
9
SSr
Wet Chemistry by Method 1664E
10
Metals (ICP) by Method 200.7
11
QC
Volatile Organic Compounds (GC/MS) by Method 624.1
12
,
GI
Pesticides (GC) by Method EPA 608.3
14
Polychlorinated Biphenyls (GC) by Method EPA-608.3
16AI
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
17
GI: Glossary of Terms
21
9SC
Al: Accreditations & Locations
22
Sc: Sample Chain of Custody
23
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE'
Eaton Corporation 28091-R L1362288 06/182116:35 2 of 23
SAMPLE SUMMARY
OUTFALL 005 L1362288-01 M
Collected by
Chris Fuller
Collected date/time
06/03/2117:30
Received datehime
0610512109:30
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
datehime
Gravimetric Analysis by Method 2540 D-2011
WG1686147
1 06AO/2113:08
06AO12113:11
MMF
Mt. Juliet, TN
Wet Chemistry by Method 1664E
WG1686563
1 06/10/2109:16
06/10/2120:11
ERK
ML Juliet, TN
Metals (ICP) by Method 200.7
WG1690706
1 06/17/2116:55
06/17/2123:36
CCE
Mt. Juliet, TN
Volatile Organic Compounds(GC/MS) by Method 624.1
WG1683600
1 06/05/2122:56
06/05/2122:56
JHH
Mt. Juliet, TN
Pesticides (GC) by Method EPA 608.3
WG1684259
1 06/08/2109:48
06/08/2119:38
HMH
Mt. Juliet, TN
Polychlorinated Biphenyis (GC) by Method EPA-608.3
WG1684259
1 06/08/2109AB
06108/2118:17
JMB
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG1684262
1 0610812117:52
06/09/2108:42
AMG
MC Juliet, TN
I
) ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
I Eaton Corporation 28091-R L1362288 06/18/2116:35 3 of 23
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
cp
I
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
aSs
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been Identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
■
5sr
,� /
//'hlVil
aQC
11/Y•e`OtG/ v
l�L��/"� `
�GI
Heather J Wagner
aAl
Project Manager
9Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1362288 06n8R116:35 4of 23
OUTFALL 005 SAMPLE RESULTS - 01
Collected date/time: 06/03/21 17:30 L1362288
Additional Information - Results for field analyses are not accredited to ISO 17025
Result Units
Analyte
pH (On Site) 6,87 so
Temperature (on -site) 23 Deg
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier RDL Dilution Analysis
Analyte mg/I mgA date/time
Suspended Solids 142 10D 1 06f10/202113:11
Wet Chemistry by Method 1664E
Result Qualifier MDL RDL Dilution Analysis
Analyte mgA mgA mgA date/time
TPH -Oil&Grease U 1.12 7.69 1 06/10/202120:11
Sample Narrative:
L1362288-01 WG1686563: Total 011&Grease Is non -detect. Extract was not processed through silica gel.
Metals (ICP) by Method 200.7
Result
Qualifier MOIL
RDL
Analyte
mgA
mg/1
mgA
Copper
Alli
0.00226
0.0100
Lead
U
0.00227
0.00500
Zinc
0.0496
J 0.00578
0.0500
Volatile Organic Compounds (GC/MS) by Method 624.1
Dilution Analysis
date / time
Batch
WG1686147
FCp
FTC]
aS$
4Cn
6Q0
WG1686563 7GI
aAl
9
Sc
RaMh
Batch
1 06117/202123:36 WGI690706
1 06/17/202123:36 'Al
1 06/17/202123:36 WGI690706
Result
Qualifier MDL
RDL
Dilution
Analysis
Batch
Anayte
mgA
mgA
mgA
date/time
Acrolein
U
0.00254
0.0500
1
O6I0550212256
WG1683600
Acrylonitrile
U
0.000671
0.0100
1
06/05202122:56
WGI683600
Benzene
U
0.0000941
0.00100
1
06/05/202122*56
WG1683600
Bromodichloromethane
U
0.000136
0.00100
1
06/05202122:56
WG1683600
Bromoform
U
0.000129
0.00100
1
06/05/202122:56
WG1683600
Bromomethane
U
0.000605
0.00500
1
061051202122:56
WGI683600
Carbon tetrachloride
U
0.000128
0.00100
1
06/05/202122:56
WG1683600
Chlorobenzene
U
0.000116
0.00100
1
06/05/202122:56
WG1683600
Chlorodibromomethane
U
0.000140
0.00100
1
06/05/202122:56
WG1683600
Chloroethane
U
0.000192
0.00500
1
06/05/202122:56
WGI683600
2-Chloroethyl vinyl ether
U
0.000575
0.0500
1
06/0512021 22:56
WG1683600
Chloroform
U
0.000111
0.00500
1
06/05202122:56
WGI683600
Chloromethane
U
0.000960
0,00250
1
06105/202122:56
WG1683600
1,2-Dichlorobenzene
U
0.000107
0.00100
1
06/05/2021 22:56
WGI683600
1,3-Dichlorobenzene
U
0.000110
0.00100
1
06/OS/2021 22:56
WG1683600
1,4-Dichlorobenzene
U
0.000120
0,00100
1
06105202122:56
WGI683600
Dichlorodi8uoromethane
U
0.000374
0.00500
1
06I05/2021 22:56
WGI683600
1,1-Dichloroethane
U
0.000100
0.00100
1
06/05/2021 22:56
WG1683600
1,2-0ichioroethane
U
0.0000819
0.00100
1
06/05/2021 22:56
W01683600
1,1-Dichlorcethene
U
0.000188
0.00100
1
06/05/202122:56
WGI683600
trans-1,2-Dichloroethene
U
0.000149
0.00100
1
06/05/2021 22:56
WG1683600
1,2-Dichloropropane
U
0.000149
0.00100
1
0610520212256
WG1683600
cis-1,3-Dichlompropene
U
0.000111
0.00100
1
06/051202122:56
WGI683600
trans-1,3-Dichloropropene
U
0.000118
0.00100
1
06/05/202122:56
WGI683600
Ethylbenzene
U
0,000137
0,00100
1
06/05/2021 22:56
WGI683600
Methylene Chloride
U
0.000430
0.00500
1
06105202122:56
WGI683600
1,1,2,2-Tetrachloroethane
U
0.000133
0.00100
1
06/05/202122:56
WG1683600
Tetrachloroethene
U
0.000300
0.00100
1
06/05202122:56
WG1683600
ACCOUNT:
PROJECT:
SDG:
DATEMME:
Eaton Corporation
28091-R
L1362288
06/182116:35
PAGE:
5 of 23
OUTFALL 005
SAMPLE
RESULTS - 01
Collected dateltime; 0610312117:30
L1362288
Volatile Organic Compounds (GOMS)
by Method 624.1
RP
Result Qualifier
MDL RDL
Dilution
Analysis
Batch
mgA
mg/I mgA
date/time
Toluene U
0.000278 0.00100
1
M05/202122:56
WGI683600
1Te
1.1,1-Trichloroethane U
0.000149 0.00100
1
06/05/202122:56
WG1683600
1.12-Trichloroethane U
0.000158 0.00100
1
06/05/2021 22:56
WGI683600
a
Trichloroethene U
0.000190 0.00100
1
06/051202122:56
WG1683600
$S
TrichloroAuoromethane U
0.000160 0.00500
1
06/05/202122:56
WG1683600
Vinyl chloride U
0.000234 0.00100
1
06/05/202122:56
WG1683600
°
Cn
(SJToluene-d8 104
80.0-20
06/05/102122:56
WG1683600
(SJ4-BromoBuorobenzene 92.4
80.0420
061051102122:56
WG1683600
(S) 1.1-Dichloroethone-0 115
70.0-130
061051202122,56
WG1683600
Pesticides (GC) by Method EPA 608.3
a0C
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
mg4
mg/l
mg/I
date/lime
Aldrin
U
0.0000198
0.0000500
1 06/081202119:38
WG1684259
Alpha BHC
U
0.0000172
0.0000500
1 06/08/202119:38
WGI684259
a
Beta BHC
U
0.0000208
0,0000500
1 06/08/202119:38
WG1684259
AI
Delta BHC
U
0.0000150
0.0000500
1 06108/202119:38
WGI684259
Gamma BHC
U
0.0000209
0.0000500
1 06108/202119:38
WG1684259
9SC
Chlordane
U
0.0000198
0.00500
1 06108/202119:38
WGI684259
4,4-DDD
U
0.0000177
0.0000500
1
06/081202119:38
WGI684259
4,4-DDE
U
0.0000154
0.0000500
1
06/08/202119:38
WG1684259
4,4-DDT
U
0.0000198
0.0000500
1
06108/202119:38
WG1684259
Dieldrin
U
0.0000162
0.0000500
1
06/081202119:38
WGI684259
Endosulfan I
U
0.0000160
0,0000500
1
06/08/202119:38
WG1684259
Endosulfan It
U
0.0000164
0.0000500
1
06108/202119:38
WG1684259
Endosulfan sulfate
U
0.0000217
0.0000500
1
06/0W202119:38
WG1684259
Endrin
U
0.0000161
0.0000500
1
06/081202119:38
WG1694259
Endrin aldehyde
U
J4 00000237
0,0000500
1
06/08/202119:38
WG1684259
Endrin ketone
U
0.0000219
0.0000500
1
06108/202119:38
WG1684259
Heptachlor
U
0.0000148
0.0000500
1
06108/202119:38
WG1684259
Heptachlor epoxide
U
0.0000183
0.0000500.
1
06/08/202119:38
WG1684259
Hexachlorobenzene
U
0.0000176
0.0000500
1
06/08/202119:38
WG1684259
Methoxychlor
U
0.0000193
0.0000500
1
06109/202119:38
WGI694259
Toxaphene
U
0.000168
0.000500
1
061081202119:38
WGI684259
(S) Decochloroblpheny/
34.7
10.0-144
06/08/202119:38
WGI694259
(S) Tetrachloro-m-xylene
570
10.0-135
061081202119:38
WG1684259
Polychlorinated Blphenyls (GC) by Method EPA-608.3
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
All
mgA
mgA
mg4
date/time
PCB 1016
U
J4 0,000270
0.000500
1 06/08/202118:17
WG1684259
PCB 1221
U
0.000270
0.000500
1 06/08M2118:17
WGIM259
PCB 1232
U
0,000270
0.000500
1 06/081202118:17
WG1684259
PCB 1242
U
0.000270
0.000500
1 061081202118:17
WGI684259
PCB 1248
U
0.000173
0.000500
1 061081202118:17
WG1684259
PC81254
U
0.000173
0.000500
1 06M202118:17
WGI694259
PCB 1260
U
0.000173
0.000500
1 06108/202118:17
WGI684259
(S) Demchlorobiphenyl
35.3
10.0/44
0& W102I Pt f7
WGI684259
(S) Tetrochbro-m-xylene
63.6
10.0-135
067081201118.17
WG1684259
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1362288 06A8/2116:35 6 of 23
OUTFALL 005 SAMPLE RESULTS - 01
Collected date/time: 06/03/21 17:30 L1362288
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MOIL
ROL
Dilution
Analysis
Batch
Analyte
mg/1
mg/I
mg4
date/time
Acenaphthene
U
0.0000886
0.00100
1
06/09/202108.42
WG1684262
Acenaphlhylene
U
0,0000921
0.00100
1
06/091202108:42
WG1684262
Anthracene
U
0,0000804
0.00100
1
06/091202108:42
WG1684262
Benzidine
U
J3 0.00374
0.0100
1
06/091202108:42
WG1684262
Benzo(a)anthracene
U
0.000199
0.00100
1
06/091202108:42
WGI684262
Benzo(b)8uoranthene
U
0.000130
0.00100
1
06/09/202108:42
WG1684262
Benzo(k)fluoranthene
U
0.000120
0.00100
1
06109/202108:42
WGI684262
Benzo(g.1h,i)perylene
U
0.000121
0.00100
1
06109/202108:42
WG1684262
Benzo(a)pyrene
U
0.0000381
0.00100
1
06109/202108:42
WG1684262
Bls(2-chloretho)Mmethane
U
0.000116
0.0100
1
06/09/202108:42
WG1694262
BIs(2-chloroethyl)ether
U
0.000137
0.0100
1
06/09/202108:42
WG1684262
2,2-Oxybis(1-Chloropropane)
U
0.000210
0.0100
1
06109/202108:42
WG1694262
4-Bromophenyl-phenylether
U
0.0000877
0.0100
1
06/09/202108:42
WG1684262
2-Chloronaphthalene
U
0,0000648
0.00100
1
06/09/202108:42
WG1684262
4-Chlorophenyl-phenylether
U
0.0000926
0,0100
1
061091202108:42
WG1694262
Chrysene
U
0.000130
0.00100
1
06/09/202108:42
WG1684262
Dibenz)a,h)anthracene
U
0.0000644
0.00100
1
O6/09/2021 08:42
WG1684262
3,3-Dlchlorobenzidine
U
0,000212
0.0100
1
06109/202108:42
WGI694262
2,4-Dinitrotoluene
U
0.0000983
0,0100
1
06109/202108:42
WG1684262
2,6-Dinitrotoluene
U
0.000250
0.0100
1
061091202108:42
WG1684262
1,2-01pheny1hydrazine
U
0.000105
0.0100
1
06109/202108:42
WG1684262
Fluoranthene
U
0.000102
0.00100
1
06/09/202108:42
WG1684262
Fluorene
U
0,0000844
0,00100
1
06/09/202108:42
WG1684262
Hezachlorobenzene
U
0.0000755
0,00100
1
06109/202108:42
WG1684262
Hexachloro-1,3-butadiene
U
0.0000968
0.0100
1
06/09/202108:42
WG1684262
Hexachlorocyclopentadiene
U
0.0000598
0.0100
1
06/091202108:42
WG7684262
Hexachloroethane
U
0.000127
0.0100
1
06109/202108:42
WG1684262
Indeno(1,2,3-cd)pyrene
U
0.000279
0.00100
1
061091202108:42
WG1684262
Isophorone
U
0.000143
0.0100
1
06/091202108:42
WG1684262
Naphthalene
U
0.000159
0.00100
1
06/09/202108.42
WG1684262
Nitrobenzene
U
0.000297
0.0100
1
06109/202108:42
WGI684262
n-Nitrosodimethylamme
U
0.000998
0.0100
1
06/092021 OBA2
WGI684262
n-Nitrosodiphenylamine
U
0.00237
0.0100
1
06/09/202108:42
WG1684262
n-Nitrosodi-n-propylamine
U
0.000261
0,0100
1
06109/202108:42
WG1684262
Phenanthrene
U
0.000112
0.00100
1
06/09/202108:42
WG1684262
Benzylbutyl phthalate
U
0.000765
0.00300
1
06109202108:42
WG1684262
B1s(2-ethy1hexyI)phthalate
U
0.000895
0.00300
1
06/09/202108:42
WG1684262
DI-n-butyl phthalate
U
0.000453
0.00300
1
06/09/202108:42
WG1684262
Diethyl phthalate
U
0.000287
0.00300
1
06/09/202108:42
WG1684262
Dimethyl phthalate
U
0.000260
0.00300
1
06/09/202108:42
WG1684262
Dl-n-octyl phthalate
U
0.000932
0.00300
1
06/09/202108:42
WG1684262
Pyrene
U
0.000107
0.00100
1
06/09/202108:42
WG1684262
1,2,4-Trichlorobenzene
U
0.0000698
0.0100
1
06/09/202108:42
WG1684262
4-Chloro-3-methylphenol
U
0.000131
0.0100
1
06/09/202108:42
WG7684262
2-Chlorophenol
U
0.000133
0,0100
1
06/09/202108:42
WG7684262
2,4-Dichlorophenol
U
0.000102
0.0100
1
06109202108:42
WG1694262
2,4-Dimethylphenol
U
0.0000636
0.0100
1
06/091202108:42
WG7684262
4,6-Dlnitro-2-methylphenol
U
0.00112
0,0100
1
061091202108:42
WG1684262
2,4-Dinitrophenol
U
0.00593
0.0100
1
06109/202108:42
WG7684262
2-Nhrophenol
U
0.000117
0.0100
1
06/09/202108:42
WG1694262
4-Nitrophenoi
U
0,000143
0.0100
1
06/09/202108:42
WG1684262
Pentachlorophenol
U
0.000313
0.0100
1
OW09/202108:42
WG1684262
Phenol
U
0.00433
0.0100
1
W09/202108:42
WG1684262
2,4,6-Trichlorophenol
U
0.000100
0.0100
1
06Po9202108:42
WG7684262
(S)2-Fluorophenol
449
10.0-120
061091202108.42
WG1684262
(S) Phenohd5
29.8
8.00-424
06M9/202108:42
WG1684262
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1362288 06d8/2116:35 7of23
OUTFALL 005 SAMPLE RESULTS - 01
Collected date/time: 06/03/21 17:30 L1362288
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL
RDL
Dilution Analysis
Analyte
mg/I mg/I
mg/1
date/time
(S)Nitrobenzene-d5
78,2
15,0-314
061091202108.42
(S) 2-Fluorobiphenyl
73.2
220-127
061091202108.42
(S)2,4,6-fabromophenol
99.5
10.0-153
06109120210842
(S)p-7erphenyFdM
88.2
29.0-141
061091202108.42
Batch
WGI684262
WGI684262
WG1684262
WG1684262
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Eaton Corporation 28091-R L1362288 06/18/2116:35 8 of 23
WG1686147
QUALITY CONTROL SUMMARY
GravimeVlc Analysis by Method 2540 D-2011
0362288 01
Method Blank (MB)
(MB) R3666209-1 06A0/2113:11
(J
❑
MB R.ft MB Qualifier MB MOL MB RDL
Meyta mgA mgA NA
-TC
Suspender SORES U 1.50 250
.5$
L1361645-01 Original Sample (OS) • Duplicate (OUP)
aCn
(OS) 1136164501 06AW2113:11 • (DUP) R366620g 3 O6A0/2113:11
0,"Result DUPR.ft [hital DUPRPD
DUP Odulger DUPRPD
U'aft
sf
Are m nelygA mqA %
SuspcMeU So1Ms 41.1 41.1 I 0.000
__.._._%.
5
1-1361645.02 Original Sample (OS) • Duplicate (DUP)
TGi
(OS) 11361646-02 06MOQ11311- (DUP) 1?3666209 01011
OrlgBwl ResuX DUPRNdA Distion 011.1i
DUPQuaMer WPMURds,
sQl
anew mgA mgA %
%
Suspended Solids 300 322 1 2L1
J3 5
pSC
Laboratory Control Sample (LCS)
(LCS) R366620G-2 O6A0/2113:11
Spike AmourE LCSR,l LCS Rae. Rac. Unit LCSQualBbr
Anayte mgA mgA % %
Suspended Solids A3 830 114 85.2-114
ACCOUNT: PROJECT: SOG: DATMIME PAGE:
EeWn Coma...n 28094R L1362288 06ntinl6'.35 90f 23
WG1686563
QUALITY CONTROL SUMMARY
Wet Chemist, by Method 16648
0362213-01
Method Blank (MB)
C
(MS) R3665S47-1 06A02120:11
P
MB Remit MBO=aiHbr MB MOL
Analyte mgA mgA
MBRDL
ogA
,TC
IDH - 0116 Grease B 0 ]25
5.00
f
S
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3665847-2 06A0121 20.11 • (LCSD) R3665847-3 06A012120:11
Ca
Spine Amount LCSR.ft LCSD ResuR
M.M. mgA .0 N
LCS Re UND R.. Rec Limits LCS OuallRer LUD-Outtift RPD RPD L"M
% % % % %
SSf
TM -0116 Grease 40.0 35.0 38.9
875 97.3 W.0-132 10,6 31
TGI
aAl
FSC
ACCOUNT: P oJEC. SDG: DATGfnME PAGE
Eaten Corporaeon 28o91J2 L1362288 06A81211635 100123
WG1690706
QUALITY CONTROL SUMMARY
Metels ([CPI by Method 200J
U862288.01
Method Blank (MB)
Cp
(ME)R3668910-5 Waal 0156
❑
MG Rautl M13 Oua181er M8 MDL
AWA. mgA mgA
MORDL
MgAl
C
Copper D 0.00226
0.0100
Lead U 0.00727
000500
aSS;
Inc J 0.005M
00500
aCn
Laboratory Control Sample (LCS)
(LCS)R3668910-1 G6A7/2t23:17
a$f
Spft Amount -CS Rmft LCS Rea.
Rec. L8na6 LCS 0.11k
Aaalyte mg0 m9A %
%
Copper 100 0914 914
85.0115
Lead 1.00 0926 92.6
85.0-D5
A. 1.00 0.912 91.2
85.0-115
L1362290-03 Original Sample (OS) • Matrix Spike
(MS) • Matrix Spike Duplicate (MSD)
aAl
(OS) L136229a43 06A7/212120 • (MS) R3668910-3 W72123:25 • (MSD) R366111M -0 06A7/212328
9$C
Sp" Amaud Original Rauh MS Pew*
MSD Res MS Rea, MSD R.. D6u1bn
R.Llmtta MSOualNer
MSD Oualfler RP0
RPM Lkaft
Analyte mgA mgA mgA
m9A % %
%
%
%
-_ __ - -___-
Copper UN 0.00585 0.939
0958 933 95.2 1
]0.0.130
1.99
10
Leaf 1.00 U 0.951
0.961 951 96.3 '1
70.0-130
Ln
20
Zinc 100 0.00156 0.922
0.9dd 91.5 93.6 1
70.0-130
2.31
20
ACCOUNT: PROJECT: SOG: DATEAME: PAGE:
Eaton CoWratlon 28W5 L1362288 06dMi 16:35 110123
WG1683600 QUALITY CONTROL SUMMARY
Volatile Organic Compounds IGCIMSI by Method 624A 41363288.01
Method Blank (MB)
MB RemB
MB Oualilkr MBMDL
MB RDL
Anar)4e
mgn
mgn
di
Aaolein
U
0.00254
0.0500
Acrybnnrlle
U
0.00m6
0,0100
Benzene
U
00000941
0.00100
&omodohmomajane
U
0.000136
000100
Bromoform
U
0000129
a0010a
Bromomethane
U
0.000605
0.00500
Carbon tetrachloride
U
0000128
000100
Chlambanzece
U
0.0001%
0.00100
CLbrodbromamethane
b
MOO
0.00100
ChbioeNarie
U
0,000*2
0.00500
2{hbrodi vbyt ether
U
0.000575
0.0500
Dibrofarm
U
0000111
0.00500
Chlomme0ane
U
0.000960
0.00250
12-Diolosebendame
U
0.000107
000100
1.3-Di<hbrobenzene
U
0000110
0.00100
ts-Dichlorobed.
U
0 000120
0,00100
DinlaradmuoromeNane
U
0A00374
000500
1WbAbroethane
U
0.000100
0.00100
1b01chbroettene
U
0.0000819
0,00100
11-0IchWroathene
U
0.000188
0.001)o
4an5-1,2-0ichlamethene
U
0000149
0,00100
1,1-01ctibropropane
U
0.01
0.00100
cis-1.3-01cbbropropene
U
0.000111
0,00100
Bar'a-1.3-0Iifibropcipene
U
0.000118
0,00100
Ethyll,amene
U
0.000137
000100
McNyleme Chbdde
U
OMN30
0.00500
112,2-TetracnbtceNale
U
0000133
000100
Tetrachbrcethene
U
0.000300 .
0.00100
toluene
U
0000228
0.00100
1,1,1-Ttldl1dmenane
U
0.00099
0.00100
1.1,2-Trirhlorcethane
U
0.000158
0 00100
TUrhbrcethene
U
0.000190
0.00100
TCNbrofluoromethane
U
0000160
0.00500
Vmyl ilibrbe
U
0.000234
000100
IS)Tdsuzda 8
103
80, -120
)S14-BrombhroroDen2ere
900
80.6120
(112-Dkhb/aefnamW4
IV
200 U0
ACCOUNT: PROJECT: SDG:
EMon Cmponstbn 28MI-R L1362288
DATEenlAe
06M18211635
PAGE
12 of 23
WG1683600
QUALITY CONTROL SUMMARY
Volatile Organic Compounds
(GC/MS)
by Method 624A
L1362238.01
Laboratory Control
Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
Cp
(LCS) R36641731 O6/052119.12 • (LCSD)
R3664179-2
067052119:33
Spite AmaurB
LCS Result
LCSO Result
LCS R. LCSO R.
Rec Lhnits LCS OuaIRMr LCMQualgkr
RRO
RPO Limtts
AnaMe
WA
m94
m08
%
%
%
%
%
Tc
A<rolem
00250
0.0158
00157
63.2
628
60.0-140
0.835
20
Acrylontris
00250
0.0209
0.0205
83.6
82.0
60.0-140
1.93
20
3$5
Benzene
0.00500
0.00464
0.00465
928
93.0
65,0-135
0,215
20
BromodldBorometbane
0.00500
000496
0.00502
99.2
100
65.0-135
1,20
20
•Cii
Rromororm
0.00500
0.00402
0.00400
804
800
700-130
0499
20
Bromcmethane
TOOM0
0.00572
000564
1M
113
15.0485
1,41
20
Carbon tetrachtonde
000500
000449
000440
HE
B8.0
70.0-130
202
20
a$r
UErobenxene
0.00500
000463
000465
92.6
93.0
65.0-135
0431
20
-
CinnMdibmmomethene
000500
000484
0,00484
968
968
70.0-135
0000
20
chb.11h.he
0.00500
000682
000685
136
137
40.0460
0.439
20
2iicroethyl Nnyl ether
0.0750
00727
00220
90.8
880
0.100-225
3,13
20
chloroform
0005M
000497
0.00513
99A
103
]0.0-135
In
20
7GI
chioromethane
0,00500
000622
000638
124
128
0100-205
254
20
1,2-0kh1hm1xmvme
000500
0.00454
0.004]i
908
84.2
65.0-135
3.68
20
u
1,3-0ichbrobenxene
000500
000469
0.005(35
93.8
101
70.0.130
7.39
20
1.4Dktrbmbenxene
0.00500
0.00470
0.00505
966
101
65.0435
549
20
pidilonA luoromelhane
0,00500
000445
0.00472
89)
94A
49.0-155
5.89
20
°$C
1,1-0ichl.hathane
0.00500
0.00524
0.00531
TS
106
70.0130
L33
20
1.2-prchbroettmns
0.00500
000486
0.00507
97.2
101
70.0-130
423
20
1.10kMoroetnene
0.00500
0.00487
000508
97.4
102
50.0150
4.22
20
bens-1.2-0k brcemene
0.00%0
0.00508
0.00529
102
106
700-130
405
20
1.20bhbmprapane
0.00500
0.00535
0.00511
107
102
350-165
4b9
20
t1,1.3-0kh1oropmperte
000500
000484
000473
96.8
94.6
250-M
2.30
20
Vara4.3-0khlomprcpehe
O.Oo500
0.00443
0.00458
8&6
91.6
50u450
3.33
20
Btlrytbemene
0.00500
0.00472
0.00463
954
926
600-140
2AB
20
Madaithechbrbe
0.00500
0.00485
0.005M
920
101
600-MO
4.24
20
1.1.2,24dachlomelhane
000500
0.00476
0.00507
952
101
600-140
6.T
20
Talachiumethene
0.00500
0.00459
0.00467
918
93.4
70.0-130
1.73
20
Tobene
0.00500
000441
000449
88.2
89.8
700130
1.80
20
1,tLTrlchbroethane
0.00500
0.00500
0.00516
100
103
700430
3.15
20
1.1.2-Trkhichelhene
000500
000489
0004T
97.8
94.2
70.0-130
375
20
Tndrbroetbene
0,00500
0.00462
0.00481
92A
962
65,0135
4.03
20
T6chbro0uoromethane
0.0050C
0.00498
000501
998
100
500-150
0.601
20
vinyl chbOde
0.00500
006588
0.00568
118
114
5.00-15
3,46
20
IS)TorLened
8U
*2
800-fx
(3)4 Moanroberuerre
978
k70
80.0-120
(S tT-0khbroefMmd4
108
108
700-130
ACCOUNT: PROJECT: MG. OATE/fR4E PAGE:
Eaton Corporarbn 28091A L1362268 Waal 16.35 13 or23
WG1684259
Pefticides (GC) by Method EPA 608.3
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1362288 01
(MB)R3665513-1 06ffl Ql 16:45
P
MD Result
Anal,e mgA
._.._._-
ME OVelifler
ME MDL
mgA
--`____m`_N-
ME EEL
mgA
TC
AMrin U
0.0000198
00000500
Alpha BHC u
0.0000172
0.0000500
a
SS
Beta BHC U
OOW0206
00000500
Delta SHE U
0.0000150
00000500
4
Gamma BHC u
0.0000209
0.0000500
Cn
4.4-ODD U
0.0000177
OE000500
4.4-0DE U
0,0000154
00000500
sS!
4¢DDT U
0.0000f98
00000500
DleldrIn u
0.0000162
0.0000500
Ergosulfanl a
0.00WIW
0.000500
Enilosulfan ll U
00000164
0,0000500
Endoanttan su8ate U
00000217
0,0000500
G
Entlrin a
00000161
00000500
Entlrin aldehyde U
0.0000237
0.0000500
aAl
Enann ketone a
0.00002N
0.0000500
Hetpach X u
o 0000148
0,0000500
HepMchlorewAme a
00000183
0.0000500
eSC
Herachtyrobenzane U
0.W00176
0.0000500
McVhcocychbr U
0.0000193
0.0000500
Chlordane U
0.0000198
0,00500
TOBapbene U
0000168
0000500
(5)DecochkobbipAesy7 560
10.0-M4
6)7ehachld a-.ykne 685
VnO 135
Laboratory Control Sample (LCS)
(LEE) R3665513-2 OW0812116:57
Sp*.Amount
LCS ResvA
LCS Rec,
Rec, Li.b LC50_aMler
An.w mgA
mgA
%
%
AMrin 0.00100
0.000838
838
420-040
Alpha BHC 0.00100
0.000948
94.8
37.0-MO
Beu BHC 0.00100
0,00103
103
17.6147
Delta BHC 000100
&000940
94.0
11.0-140
Gamma SHE 0.00100
00009D
973
32.0-MO
4.40DD 0.00100
0.00104
104
31.0441
4.4-0DE 0.00100
0000899
89.9
M0O.M5
0,10DT 000100
0.000970
87.0
25.0-160
DieMrin 000100
000101
101
360-146
Enddsulfan1 000100
0000949
94.9
45.0-153
ACCOUNT:
PROJECT: EEG: DATE/TWE:
PAGE
Eaton Corporation
28G9tR L1362288 0618n11635
14 of 23
WG1684259 QUALITY CONTROL SUMMARY
Pesticldes IGC) by Method EPA 608.3 L1362288 D1
Laboratory Control Sample (LCS)
71
(LCS)R3665513-2 061082116,57
Sp*o Amourd LCS RewR
LCS Rec.
Rec. ❑loft LCS Ooallfe,
AnaMe mgA mgA
%
%
TC
EndoedMn II 0.06100 000104
164
1.00-202
Endos.Han suRate 000100 0.00105
105
260-144
3$s
Endrin 000100 000101
101
300147
Endrn akehyde 000100 000197
W
56.0-128 J4
Endrin Rel00e 000100 0000996
996
540-142
n
Heptar111or 000100 0000875
875
340-140
Heptachlor epoxtlh 0.00100 0000957
953
37,0442
Fri
0.00100 0.000760
260
350-120
Melhowychlor 000100 000106
106
410-160
RJ DeCOCDbroDiplcerryl
703
vow
(S) Tdt,.hbm mxykne
210
200135
ACCOUNT: PROJECT: SOO.
Eeton Comorabon 28091-R L1362288
DATE?IME:
064012116:35
PAGE:
15 of 23
WG1684259
Polychlorinated Blphenyls (GC) by Method EPA-608.3
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1262228-01
(MB)R3665296-1 06AGSaI1649
Cp
M9 R.ft M80_alrtrer
MB MOL
MB RDL
AnaMe mgA
NA
mgA
TC
PCB R60 U
00 00173
0.000500
PC81016 U
0.000210
0.000500
3$5
PC81221 U
0.000270
0.000500
PC81232 U
0000270
0,000500
PCB 1242 U
0000210
0000500
Fin
1248 U
0.000173
0000500
PCB 1254 U
0.000173
0.000500
6Sr
(S)DemJb-WR, 1 605
V..0.Ml
1S1 Tet.1sU R-,h,. At
81.6135
■
Laboratory Control Sample (LCS)
2GI
(LCS) R3665296-2 060W211658
SPere A..M LCSR.K
LCS R..
Rec LIm88 LCS O.1M.r
eAl
A tyte MgA 1r5A
%
%
PCB Rfi0 000250 0.00120
PCB 1016 0.00250 000363
SL2
145
8.00-140
50..0-140 ju
e$C
(S) D.hbroblpheM1
49.1
130 M4
(51 TetrdrhbA"Ra eRe
n3
As&M
ACCOUNT: PROJECT: SDG'
Eaton CorpdraTion 20001-R L1362288
DATERIME.
06b0R116:35
PAGE
16 of 23
WG1684262 QUALITY CONTROL SUMMARY
Semi Volatile organic Compounds (GC/MS) by Method 625.1 L1362289-01
Method Blank (MB)
(MBRR3664843-3 06109/210038
MR Result
MR Qualifier MR MEL
MR RDL
Analyte
mgA
mg4
mgA
Acenaphthene
U
0,6000886
0.0010)
Acenaphthykne
U
0,0000921
0.00100
Anmramne
U
0.DONS04
0,00100
AnOenzene
U
0000105
0,0100
REOZidlae
U
0,00374
0,0100
Benzp(alanthracene
U
0,000199
0,00100
Benzo(b(Omranthene
U
0000130
0.00100
Benzo(p0uoranthene
U
0.000120
O0o100
Benzo(gh,q,, ene
U
0,000121
0,0000
Benzo(apyrene
U
0.0000381
0.00100
Bis(2e bremoxytmetbane
U
0.000116
00100
Bis(2dloreeNygefler
U
0000137
00100
2, 2-0xybis(1Lmpmpropanel
U
0,000210
00100
4-13romophenyl henNether
U
0.00000P
0.0100
2-0ilomnaphthalene
U
00000648
000100
4.Chidrophen"henyhNer
U
0.0000926
00100
Ch,ene
U
0.000130
0,00100
Dlbenz(a.h(anthracene
U
0,00006"
000100
3.3-01mlorobenzidlne
U
0,000212
0,0100
2,01nnrotoluehe
U
D.0000983
0,0100
2.6-01nitretoluene
U
0,000250
0.0100
Fluoian8iene
U
O.W0102
000100
Fluaene
U
0000084
000100
Hexealerobenzene
U
(10000256
000100
Herachloro-1,3butadiene
U
0,0000968
O Oloo
HaPiMmi,dppentadlene
U
00000598
00100
Haxarhl... URPOa
U
O oD012]
00100
Indeno0.2,3cd)pyrene
U
0.0002M
0.00100
Isophprone
U
0000143
00100
Naphthalene
U
0.000159
0.00100
Wmideniene
U
0.000297
0.0100
"itroyedlmethyhm4ie
U
0000998
00100
n*Kbdadiphenylamhe
U
000237
00100
n-film 0in9repylamine
U
0.000261
0,0100
phenanthrene
U
0.000112
0,00100
BenzylbuM pli111ahte
U
0.000765
0,00300
Bis(2ePylherygphthalate
U
0.000895
0,00300
DMLulyl phtralabe
U
0 W0453
0.00300
Dialhy pinhabte
U
0000287
000300
DlrnethA phNalate
U
0.000260
0.00300
ACCOUNT:
PROJECT:
Ea. Corparaeon
2909M
50G:
L1362288
DATE/THE
US1812116'.35
PAGE:
17 of 23
WG1684262 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1362289.01
Method Blank (MB)
.
(MB)R36648433 MM9/210038
Cp
MB Result
AnaMe mgA
_.
-"CIA
MBOwIBier MB MOL
mgA
MB ROL
m9A
2TC
Diawdyl phAalale U
0.000932
_.
0.00300
Pyrene U
0000107
0.00100
7$5
1,2,44dThlorohrriene U
0.0000699
0.0100
A{Moro-3-meNylphenol U
0000131
00100
aCn
2-0Mprophenol U
0000133
00100
ZSDichtcrophenol U
0 i00102
00100
2,4-Dimegiylphnmoi U
0.0000636
00100
5$f
4,6-Dirb.2-msthApNa,c1 U
Hong
0.0100.
24-D1narophenol U
0W593
0.0100
2Nmophenol U
0.000117
0.0%)o
4-Nbrophenal U
0,000143
0.0100
Pentachiomphenol U
0.000313
0.0100 TGI
Phenol U
0.00433
00100
2.4. -Trichbrophewi U
0,000100
00100
e(AI
(S) MRm5en2eneCS 623
15039
(S) 2-FW.Nphed,1 78.8
22.0-127
(S)P7eryheryLdl4 873
29.0-141 0$C
(5)pwyxdd5 28.9
ItOO424
(5) 2-FAmroGhenol 44.6
100 720
MZ.e,6-FrPommopheno1 7l0
10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(-CS) R36648431 015MB 12360 • (LCSD) R3664843-2 06/09210014
Spike Aemurd
La Result
LM Resit
LCS Rec.
LOW R.,
Red, Lanl6
LCS OualHier LCSOOttaffer RPD
RM Lan16
Malyte
mgA
NA
mgn
%
%
%
%
%
Acenaphthene
00500
00370
00365
74.0
73.0
06145
136
4
Acenaph0y .
0,0500
0.0395
0.0387
79.0
77A
33.0-145
2.05
74
AnUacene
00500
00408
0.0403
816
800
27.0-133
1,23
66
Mobeniene
00500
0,0368
0.0365
73.6
73.0
37.0425
0.919
20
Remidirie
0.100
0.0129
0.00561
12.9
5,61
1.00-120
J3 78.8
36
Servok)anthacens
0.0500
0.0464
0.0449
92.9
89.8
330-143
IN
53
Serp.iblAUorenthere
00500
0.0429
00421
85.8
842
240159
188
71
BentoNfluoraNhene
00500
0.043
0.0431
M86
87.A
11.0-162
1.36
63
Benio(g.h.rperylene
a0500
00395
0.0379
79-0
75.8
1.00-219
413
97
Beneo(apyrene
0.0500
00426
0.0411
85.2
82.2
17,0-163
3.58
72
Bis(2-chbreNce,imethane
0.0500
00309
0.0310
61'8
62.0
1.00-219
0.323
54
BIS(2Chomed,fAttier
0.0500
0.0345
0.0342
69.0
684
33.0485
0.B73
108
2.2-OxyUso-Chloropropanel
0.0500
0.0360
00357
72.0
714
360166
0.837
%
ACCOUNT:
PROJECT:
SDG:
DATERME: PAGE
Eaton
Corporabon
28091-R
L1362288
O6/IBR11635 18 or 23
WG1684262
QUALITY CONTROL SUMMARY
Semi Volatile Organic
Compaunds
IGCIMSI by
Method 625.1
L1362216-01
Laboratory Control
Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
Cp
(LCS) R36648434 06709/21233.50 • (LCSD) R3664843-2 0670912100:14
Spike Amount
LCS Result
LCSD ResuN
LCS Rey. LCSD Re
Ra,,Urrils LCS Qualifier LCSOOuallller
RPD
RPO Llmlts
,
A.M.
m,A
NA
mgA
%
A
A
%
%
TC
d41rom0p6enyl-phenNether
00500
00410
0.04I0
82.0
81.0
530427
0.000
43
213timonaphMalene
00500
003T
0.0364
74.2
72.8
600-120
ISO
24
3$5
4alarophanybpheriylelher
00500
00438
0.0434
87.6
86.8
25.0-158
0,917
61
Cbrysepe
0,0500
00443
00423
886
84.6
17.0-168
4.62
87
4
Dkiam(a,h1an01racene
005M
0.0402
0.0386
80.4
71.2
1.00-227
4.06
126
Cn
3,3-Dirlllmobenzidme
0,100
0.0859
OOBN
859
81.9
1.00-262
4.A
108
2,4-0iNtmta ene
0,0500
0.0488
D.0507
97.6
101
39.0-139
382
42
S$f
2,6-0lnhrololuene
00500
0.0458
0.0450
91S
90.0
S0.0458
L76
48
FWoranzhene
0,0500
0.0461
C.0451
922
90.2
260137
2.19
66
Fluorene
0.0500
00425
00416
35.0
83.2
59,0121
214
38
HeAift.benzene
00500
00392
0.0383
78.4
766
100152
2.32
55
HeiaWOro-1,3-buladiene
0,0500
0.0373
0.0381
74.6
762
24.0-120
212
62
7�
Heow6lo i,lopentadiane
00500
0,0231
00230
41.2
46.0
10.0420
0,434
31
Hexactilom.m.mi
0.0500
0.0349
0.0349
698
698
40.0-120
0000
52
e
Inamio(1,2.3- clay ene
0,0500
0.0376
0.0353
75.2
70.6
1,00171
6.31
99
AI
Isophomne
0.0500
0.0311
0.0314
62.2
628
21,0-196
0960
93
Naphilliakoe
0.0500
0.0328
0.0331
65.6
116.2
21,M33
0,910
65
R$C
Nitrobenzene
0.0500
0.0304
OSXM
608
60.8
350480
0600
62
n4lRmsodimemykmMe
0.0500
0.02R1
00218
42.0
43.6
100120
3,74
u
n-Nhaeodiphenyamioe
00500
00377
0,0370
75.4
74.0
44,0420
187
21
n-Nxrm di,l pmo,a*mine
0.0500
0.0339
0.0345
67.8
69.0
100230
I.M
0
Phenan0lrene
00500
0.0410
0.0402
820
WA
54.0-120
197
39
BentybutylphttlaWle
00500
0.0436
0.0432
97.2
66.4
1.00452
0.922
60
B1s(2elh,hey1)phNalme
(0500
00402
0.0385
804
77.0
800-158
432
82
Dt Ito phthalate
0.0500
0.0145
0.0441
89.0
88.2
100110
0.903
47
DkNylptimalate
00500
OIM38
0,0443
BZ6
886
100120
114
100
Dm1e6rylplWaWle
00500
OOQO
C0416
840
83.2
T0,T120
0.957
183
Dladctyl plMalale
0.0500
0.0383
0.0365
766
73.0
4.00-46
481
0
Pyrelte
0.0500
0.041
0.0446
88.2
0.2
52.0420
113
49
1.2kPichlooibeniene
0,0500
0.0362
00368
72.4
73.6
4/.0442
1.64
50
UOdbro-3-maittii enol
0,0500
0.0312
00314
62.4
62.8
22.V47
0.639
73
24 1,yo,:Nmd
C0500
00337
0.0339
674
67.8
23.041
0.592
61
2,44)1ch1mophenol
0,0500
0,0347
0.0350
69A
70.0
39.0435
0.861
50
1.LDIme0rylpM1enol
0.0500
0.02%
0.0288
59S
576
320420
3,75
58
4,6 hlbo2-r,a#Wbed0l
0.0500
0.0538
0.0546
to
T9
100181
148
203
2.14linitrophenol
0,0500
00485
0.0509
970
102
1.00191
4.83
132
2-1,11trophenol
0.0500
0.0362
0.03R
72.4
75.6
29.0182
4.32
55
4 NIVaphenol
0.0500
OXUS
00156
278
31.2
1,00432
11,5
131
Penlechkomplalol
0,0500
0.0409
0.0430
816
86.0
14.0-176
5.25
86
Phenol
0.0500
0,0154
0,0162
308
32.4
5.00-120
506
64
ACCOUNT PROJECT: SDG: DATEMME PAGE
Eaton Cammadon 28091-R L1361288 06A8/211635 19.123
WG1684262 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GCIMS) by Method 625.1 L1342298-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3664843-1 MMW212350 • (LCSD) R366C843-2 rhi 0014
p
Spike Amount LCSR.k LCSD Result LCS Red.
LCSD Rec.
Red. LImIK LCS Oualifer LCSD OuaIIRm RPD
RPD Limns
Analyze mye mgA mgA %
%
% %
%
TC
M,�._ 6PkkbmpAenal 0.0500 00395 0:039] ]90
79.1
370-144 0.505
58
(S)Nd dd,pd/ S 610
624
15.03M
3SS
(S) 2 F8rbrobichiviJ 80.4
R2
22PI22
P,n,TegmNanAd14 810
289
290-91
is)ppmoms 303
323
8:.00d21
C31
(5)2-FArompAeegl 472
473
100-120
(9) 24,6Tribmempbenpl 80.0
82.5
N..0-153
3$f
ACCOUNT: PROJECT: Sini
Eason Corporation 28091-R L1362288
DATE?IME:
0GA812T1635
PAGE
30M13
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
Cp
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer- Information that may be provided by the customer, and contained within this report, Include Permit Limits, Project Name,
ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
TC
Sample
Sampling Location. Results relate to the accuracy of this Information provided, and as the samples are received.
Abbreviations and Definitions
S
MDL
�RDL
Method Detection Limit
Reported Detection Limit. _
dCn
Rec.^
Recovery.
RPD
Relative Percent Difference
SDG
Sample Delivery Group.Sr
.. _ _ _
I(S)
__. _._. . __ __ ._ ,_ _ _ . _
Surrogate (Surrogate Standard) Analytes added to everyblank sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate used to evaluate analytical efficiency by measuring recovery, Surrogates are not expected to be
aQC
detected in all environmental media
U
lAnalyte
Not detected at the Reporting Limit (or MDL where applicable).
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
a
AI
laboratory.can accurately report, the sample maybe diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
iLimits
These are the target% recovery ranges or%difference value that the laboratoryhas historicallydeter-mined as normal
for the method and analyte being,reported.'Successful OC Sample analysis will target all analytes recovered or
SC
L
duplicated within these ranges.. I
Original Sample
The non -spiked sample In the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
i
This columnprovldes aletter and/or number designation that corresponds to additional Information concerning the result
lQualifier
reported If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
_
potentially a discussion of possible Implications of the Qualifier In the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported foryour sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The Information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowestvalue that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma
A brief discussion about the Included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report
iQuality Control
This section of report includes the results of the laboratory quality control analyses required by procedure or '
:Summary, (Glc)
analytical methods to assist in evaluating the validity of the results reported for your samples..These analyses are not
being performed on your samples typically, but on laboratory generated material.
This Is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perforr This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section ofycur report will provide the results of all testing performed on your samples. These results are provided
,Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for;
I
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
limes of preparation and/or analysis.
Qualifier Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
_
__.___.__..__.-__.__tch, __..._...._.._,_.__. __ .._.___ _ ___ __._.__
The associated batch OC was outside the established quality control range for precision.
J4
The associated batch OC was outside the established quality control range for accuracy.
iP
_____.. __ _._.._-__. --- .._ .__
RPD between theprimary and confirmatory analysis exceeded 40%.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1362288 06A9/2116:35 21 cf 23
ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15.05
Alaska
17-026
Nevada
TN000032021-1
Arlmna
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey-NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
Newyork
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
OW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-110
Idaho _
TN00003
_
Ohio-VAP
CL0069
Illinois
200008
Oklahoma _
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68.02979
Kansas _
_ E-10277 _ _
Rhode Island
L1000356
Kentucky '°
KV90010
South Carolina
84004002
Kentucky °
16 _ _
South Dakota
We
Louisiana
A130792 _ _
_
Tennessee "
2006
Louisiana_ _ __.. __._
_ LAO/8
Texas
71047042.45-20-18
Maine
TN00003
_Texas'
LA80152
Maryland
324 _ _
_ Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
_ 9958
Virginia
110033
Minnesota
047.999-39.5
—
Washington
C847
Mississippi
TN00003
West Virginia
-__
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A2LA-ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21LA-150170253
1461.02
DOD
_
1461.01
Canada
1461.01
USDA _
_
P330.15-00234
EPA-Ciypto
TN00003
'Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 'ChemicalRAKrobldlogical 'Mold °Wastewater n/a Accreditation not applicable
' Not all certifications held bythe Laboratory are applicable to the results reported In the attached report.
• Accreditation is only applicable to the test methods speciiletl on each scope of accreditation held by Pace AnaMical.
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Eaton Corporation 28091-R L1362288 06/18/2116:35 22 of 23
6 6 .
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