WQ0029653_Monitoring - 03-2022_20220504

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF EN WATER RESOURCES
GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and 1 Copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: —2%- ,. 2(o
Facility Name: Scotch Hall Preserve Non-Discharge wa0029653 UIC
Permit Name(if different): NPDES Other
Facility Address: merry hill TYPE OF PERMITTED OPERATION BEING MONITORED
merry hill i atreet) County Bertie ❑ Lagoon ❑ Remediation: Infiltration Gallery
(State; (Zip) © Spray Field ❑ Remediation:
Contact Person: Brian Jernigan Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:Scotch hall preserve No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): mW l Date sample collected: 3/2 1/2022 FIELD ANALYSES: WAS
Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 6.8 units Temp. 000lo: 12,2 °C DRY at
time of
Depth to Water Level szsas:7 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 00094: µMhos sampling,
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check
Volume of water pumped/bailed before sampling: 3.5 gallons Appearance tan here:
Samples for metals were collected unfiltered: CI YES ❑ NO and field acidified: ❑YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:./L I/LULL Laboratory Name: Environmental Chemists. Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 0.03 mg/L Pb-Lead 01os1 ug/L
Coliform: MF Fecal 31616 3 /100mL Nitrate(NO3)as N oos20 99 mg/L Zn-Zinc 01092
Coliform: MF Total 31504 /100mL Phosphorus:Total as P oosss 0.40 mg/L ;} i'Fr
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Cot�f enJatiora its)T
Dissolved Solids:Total 70300 53 mg/L Al-Aluminum o1105 mg/L (JJ
pH(Lab)00406.8 units Ba-Barium 01007 ug/L r
TOC oosao 2.2 mg/L Ca-Calcium o0916 MES mg/ -"^ f .r,s., ,,
Chloride 00940 <5 mg/L Cd-Cadmium 01027 ug/L
i_.!AV ri t; .
Arsenic 01002 ug/L Chromium:Total 01034 g/L
Grease and Oils oossz mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron o1oa5 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oo945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? El Yes(1) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method#
Total Ammonia oos10 <0,2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen,NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N Doses 1 ,02 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that.to the best of my knowledge and belief,the information submitted in this report is true,accurate and complete.and that the laboratory analytical data was produced u.n ig approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility r'f ranee a:w i',prisonment for knowing v,dations.
Mike Parah General manager lir `0" r'
Permittee(or Authorized Agent)Name and Title-Please print or type Signatur of Permittee(or Auth•'zed Agent) (Date)
GW-59 Rev.3-1-2016

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and 1 Copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699.1617 Phone:[phone]
FACILITY INFORMATION Please Pnflt Clearly or Type PERMIT Number: Expiration Date: a_aR_ 202(0
Facility Name: Scotch Hall Preserve Non-Discharge wa0029653 uic
Permit Name(if different): NPDES Other
Facility Address: merry hill TYPE OF PERMITTED OPERATION BEING MONITORED
merryhill street;
County Bertle ❑ Lagoon ❑ Remediation: Infiltration Gallery
Sties) (Zip) 0 Spray Field ❑Remediation:
Contact Person: Brian Jernigan Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Scotch hall preserve No.of wells to be sampled: 3 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): mw2 Date sample collected: 3/2 1/2022 FIELD ANALYSES: WAS
Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 6.5 units Temp. 00010: t .5 °C DRY at
Depth to Water Level 82546:12.3 ft. below measuringMhos time of
point Screened Interval: 5 ft. to 20 ft. Spec.Cond.00094: µ sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: none check
Volume of water pumped/bailed before sampling: 3.5 gallons Appearance brown here:
Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
Date sample analyzed:3/L I/LULL Laboratory Name: Environmental Chemists. Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N Doses 0.02 mg/L Pb-Lead o1051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N ooszo 0.09 mg/L Zn-Zinc o1o92 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 0.26 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 50 mg/L Al-Aluminum o11os mg/L
pH(Lab)00403 6.5 units Ba-Barium 01007 ug/L
TOC ooseo 1.3 mg/L Ca-Calcium oo916 mg/L
Chloride 00940 <5 mg/L Cd-Cadmium 01027 ug/L
Arsenic olooz ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oo945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance o0095 µMhos K-Potassium 00937 mg/L VOC 7873 , method#
Total Ammonia ooseo <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;Ntt3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 .11 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that.to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
EMIR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines dm-,imprisonment for i,rowing violations.
1 9,---.2--
Mike Parah General manager
Permittee(or Authorized Agent)Name and Title-Please print or type Signatu e of Permittee(•r Authoriz Agent) (Date)
GW-59 Rev.3-1-2016

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL I PRALITY-DIV.OF OCESSING UNIT
RESOURCES
INFORMATION OCE SING UNIT
COMPLIANCE REPORT FORM and 1 Copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: Expiration Date: , -a$_ aO.Z(o
Facility Name: Scotch Hall Preserve Non-Discharge wa0029653 uic
Permit Name(if different): NPDES Other
Facility Address: merry hill TYPE OF PERMITTED OPERATION BEING MONITORED
merryhill street)
County Bertie ❑ Lagoon El Remediation: Infiltration Gallery
(Zip) 0 Spray Field ❑Remediation:
Contact Person: Brian Jernigan Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:Scotch hall preserve No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
ail
WELL ID NUMBER(from Permit): a ►'M 1u 3 Date sample collected: 3/21/2022 FIELD ANALYSES: WAS
p 2 pH 00400: 7.0 units Temp.00o10:('3, \ °C DRY at
Well Depth: 20 ft. Well Diameter: in.
time of
Depth to Water Level 82546:15,6 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec.Cond. 00094: µMhos sampling,
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check
Volume of water pumped/bailed before sampling: 2.5 gallons Appearance brown here:
Samples for metals were collected unfiltered: •YES ❑ NO and field acidified: 0 YES 0 NO
LABORATORY INFORMATION
Date sample analyzed:i/L I/LULL Laboratory Name: Environmental Chemists. Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N oo61s 0.02 mg/L Pb-Lead omos1 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.50 mg/L Zn-Zinc o1092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 0.53 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 73 mg/L Al-Aluminum o1105 mg/L
pH(Lab)00403 7.0 units Ba-Barium 01007 ug/L
TOC 00680 0.6 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 6 mg/L Cd-Cadmium 01027 ug/L
Arsenic atooz ug/L Chromium:Total 01034 ug/L
Grease and Oils oossz mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron oloas ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? 0 Yes(1) 0 No(0)
Specific Conductance woes µMhos K-Potassium 00937 mg/L VOC 7873 , method#
Total Ammonia o0610 <0,2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N,Ammonia Nitrogen,Total)
Mn-Manganese o1055 ug/L , method#
TKN as N 00625 0.52 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate and complete.and that the laboratory analytical data was produced ding approved methods of analysis by a
D'NR-certified laboratory. lam aware that there are significant penalties for submitting false information,including the possibild'/ Kid fincs ,d imprisonment for knowing violations.
Mike Parah General manager ff�®' / r-; 9...)--�
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.3-1-2016

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4124 Fax
710 Bowsertown Road,Martteo, NC 27954 • 252.473.5702 Lab/Fax
''.
i.d 255-A Wilmington Highway,Jaccson�ille,NC 28540e 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(i)enl,ironmentalchemists.com
Scotch Hall Preserve Date of Report: Mar 30, 2022
105 Scotch Hall Court Customer PO#:
Merry Hill NC 27957 Customer ID: 17050011
Attention: Brian Jernigan Report#: 2022-05090
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-12187 Site: MW-1 3/21/2022 8:20 AM Water Tom Beasley
Test Method Results Date Analyzed
Color Color Tan 03/21/2022
Depth to water, ft. Depth to Water,Ft 7.0 feet 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 < 0.2 mg/L 03/24/2022
Gallons bailed before sampling Gallons Bailed before sampling 3.5 gallons 03/21/2022
Odor Qualitative None 03/21/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 53 mg/L 03/21/2022
Temperature SM 2550 8-2010 12.2 C 03/21/2022
pH SM 4500 H B-2011 6.8 units 03/21/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.40 mg/L 03/29/2022
Total Organic Carbon (TOC) SM 5310 B-2014 2.2 mg/L 03/24/2022
Fecal Coliform SM 9222 D-2015 MF 3 Colon ies/100mL 03/21/2022
Chloride SM4500 CI E-2011 < 5 mg/L 03/22/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.03 mg/L 03/21/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 1.02 mg/L 03/23/2022
Nitrate Nitrogen Subtraction Method 0.99 mg/L 03/30/2022
Report# 2022-05090 Page 1 of 3

M
Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
environmentalchemists.com
Scotch Hall Preserve Date of Report: Mar 30, 2022
105 Scotch Hall Court Customer PO#:
Merry Hill NC 27957 Customer ID: 17050011
Attention: Brian Jernigan Report#: 2022-05090
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-12192 Site:MW-2 3/21/2022 8:06 AM Water Tom Beasley
Test Method Results Date Analyzed
Color Color Brown 03/21/2022
Depth to water, ft. Depth to Water,Ft 12.3 feet 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.20.1993 <0.2 mg/L 03/24/2022
Gallons bailed before sampling Gallons Bailed berore sampling 3.5 gallons 03/21/2022
Odor Qualitative None 03/21/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 50 mg/L 03/21/2022
Temperature SM 2550 B-2010 12.5 C 03/21/2022
pH SM 4500 t1 8-2011 6.5 units 03/21/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.26 mg/L 03/29/2022
Total Organic Carbon (TGC) SM 5310 8-2014 1.3 mg/L 03/24/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/21/2022
Chloride SM4500 CI E-2011 < 5 mg/L 03/22/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.20,1993 0.02 mg/L 03/21/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev 2.0,1993 0.11 mg/L 03/23/2022
Nitrate Nitrogen Subtraction Method 0.09 mg/L 03/30/2022
Report IL 2022-05090 Page 2 of 3

!" l'
Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 4 910.392.0223 Lab e 910.392.4424 Fax
sM 710 Bowsertown Road,Manteo,NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 = 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Scotch Hall Preserve Date of Report: Mar 30, 2022
105 Scotch Hall Court Customer PO#:
Merry Hill NC 27957 Customer ID: 17050011
Attention: Brian Jernigan Report#: 2022-05090
Project ID: Monitoring Wells
Lab ID Sample ID: _._.. Collect Date/Time Matrix Sampled by
22-12193 Site: MW-3 3/21/2022 7:42 AM Water Tom Beasley
Test Method Results Date Analyzed
Color Color Rust 03/21/2022
Depth to water, ft. Depth to water,Ft. 15.6 feet 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 < 0.2 mg/L 03/24/2022
Gallons bailed before sampling Gallons Bailed before sampling 2.5 gallons 03/21/2022
Odor Qualitative None 03/21/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 73 mg/L 03/21/2022
Temperature SM 2550 B-2010 13.1 C 03/21/2022
pH SM 4500 H B-2011 7.0 units 03/21/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.53 mg/L 03/29/2022
Total Organic Carbon (TOC) SM 5310 B-2014 0.6 mg/L 03/24/2022
Fecal Coliform SM 9222 D-2015 ME <1 Colonies/100mL 03/21/2022
Chloride SM4500 CI E-2011 6 mg/L 03/22/2022
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 03/21/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.52 mglL 03/23/2022
Nitrate Nitrogen Subtraction Method 0.50 mg/L 03/30/2022
Comment: � t
Reviewed by: ,Q, �
• Report#. 2022-05090 Page 3 of 3