WQ0002503_Monitoring - 03-2022_20220503

FORM: NDMR 07-13 NON-DISCHARGE MONITORING REPORT(NDMR) Page of
Sampling Person(s) Certified Laboratories
Name: Danny Hornbeck Name: Pace Analytical
Name: Name:
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? a Compliant ! .Non-Compliant
If the facility is non-compliant,please explain in the space below the reason(s)the facility was not in compliance. Provide in your explanation the date(s)of the non-compliance and describe the corrective
action(s)taken.Attach additional sheets if necessary.
MAY 0 3 027—
t“
Operator in Responsible Charge(ORC)Certification Permittee Certification
ORC: Danny Hornbeck Permittee: Frit Car, Inc.
Certification No.: 26718 Signing Official: Michael Newby
Grade: Phone Number: 252-638-2675 Signing Official's Title: Senior Vice President
Has the ORC changed since the previous NDMR? ❑Yes 11 No Phone Number: 251-867-7752 Permit Expiration: 6/30/2022
'2-
y'Z2 4/29/2022
Signature Date Sigrih r Date
By this signature,I certify that this report is accurrate and complete to the best of my knowledge. I certify,under penally of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for
gathering the information,the information submitted is,to the best of my knowledge and belief.true,accurate,and complete.I am
aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 2 76 99-1 61 7

FORM: NDAR-1 08-11 NON-DISCHARGE APPLICATION REPORT(NDAR-1) Page of
Permit No.: WQ0002503 Facility Name: Frit Car, Inc. County: Craven Month: March Year: 2022
Field Name: 1 Field Name: N/A Field Name: N/A Field Name: N/A
Did irrigation occur
Area(acres): 1.1 Area(acres): Area(acres): Area(acres):
at this facility? Cover Crop: Grass Cover Crop: Cover Crop:■� Cover Crop:
YES ,iNO
Hourly Rate(in): 0.014 Hourly Rate(in): Hourly Rate(in): Hourly Rate(in):-_
Annual Rate(in): 7.25 Annual Rate(in): Annual Rate(in): Annual Rate(in):
Weather Freeboard Field Irrigated? YES n NO Field Irrigated? ❑YES ❑NO Field Irrigated? ❑YEs F.NO Field Irrigated? ❑YES ❑NO
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12 Month Floating Total(in): }.' 0.00 ® _

FORM: NDAR-1 08-11 NON-DISCHARGE APPLICATION REPORT(NDAR-1) Page of
Did the application rates exceed the limits in Attachment B of your permit? 2 Compliant ❑Non-Compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Q Compliant ❑Non-Compliant
Was a suitable vegetative cover maintained on all sites as specified in your permit? ❑� Compliant Non-Compliant
Were all setbacks listed in your permit maintained for every application to each permitted site? m Compliant Non-Compliant
Were all freeboards maintained in accordance with the specified freeboard heights in your permit? ,2 Compliant E.Non-Compliant
If the facility is non-compliant,please explain in the space below the reason(s)the facility was not in compliance. Provide in your explanation the date(s)of the non-compliance and describe the corrective
action(s)taken.Attach additional sheets if necessary.
Operator in Responsible Charge(ORC)Certification Permittee Certification
ORC: Danny Hornbeck Permittee: Frit Car, Inc.
Certification No.: 26718 Signing Official: Michael Newby
Grade: Phone Number: 252-638-2675 Signing Official's Title: Senior Vice President
Has the ORC changed since the previous NDAR-1? E Yes ;J No Phone Number: 251-867-7752 Permit Exp.: 6/30/22
t2- IAA (r
4/29/22
Signature Date Signature Date
By this signature,I certify that this report is accurrate and complete to the best of my knowledge. I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervises in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted.Based on my
inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the
information submitted is.to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant
penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617

w
aceAnalytical® A \ ALYTICAL REPORT
April 07, 2022 1,,
Ss
Frit Car Inc.
4
Sample Delivery Group: L1473661 Cn
Samples Received: 03/22/2022 'Sr
Project Number:
Description: Bridgeton Facility Monthly QC
7
GI
Report To: Chris Barnes
2012 US Hwy 17N Al
New Bern, NC 28560
a
Sc
Entire Report Reviewed By: 4-
Heather J Wagner
4
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory.standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided,
and as the samples are received.
-. v
.
...
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 1 of 22

• TABLE OF CONTENTS
Cp:Cover Page 1
Tc:Table of Contents 2
Ss:Sample Summary 3
Cn:Case Narrative 4
Sr:Sample Results 5 Ss
EFFLUENT L1473661-01 5 4
Cn
Qc:Quality Control Summary 7
Gravimetric Analysis by Method 2540 C-2011 7 "Sr
Gravimetric Analysis by Method 2540 D-2015 8
Wet Chemistry by Method 300.0 9 Qc
Wet Chemistry by Method 350.1 11
GI
Wet Chemistry by Method 365.4 12
Wet Chemistry by Method 420.4 13 Al
Wet Chemistry by Method 4500H+ B-2011 14
y
Wet Chemistry by Method 4500P E-2011 15 Sc
Wet Chemistry by Method 5210 B-2016 16
Wet Chemistry by Method 5310 B-2014 17
Metals(ICP) by Method 200.7 18
GI:Glossary of Terms 20
Al:Accreditations& Locations 21
Sc:Sample Chain of Custody 22
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 2 of 22

•
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
EFFLUENT L1473661-01 WW C.Barnes 03/21/2214:15 03/22/22 09.00
Method Batch Dilution Preparation Analysis Analyst Location --
date/time date/time
Tr.
Gravimetric Analysis by Method 2540 C-2011 WG1836555 1 03/22/22 17:18 03/22/22 19:29 MMF Mt.Juliet,TN
Gravimetric Analysis by Method 2540 D-2015 WG1837996 1 03/24/22 19:10 03/24/22 21:13 BRG Mt.Juliet,TN
Wet Chemistry by Method 300.0 WG1836300 100 03/22/22 20:45 03/22/22 20:45 KEG Mt.Juliet,TN Ss
Wet Chemistry by Method 300.0 WG1837980 10 03/24/22 21:28 03/24/22 21:28 LBR Mt.Juliet,TN
Wet Chemistry by Method 350.1 WG1837876 10 03/25/22 15:44 03/25/22 15:44 SL Mt.Juliet,TN °
Cn
Wet Chemistry by Method 365.4 WG1841250 100 03/30/22 07:16 03/31/22 14:39 LDT Mt.Juliet,TN
Wet Chemistry by Method 420.4 WG1839168 1 03/28/22 03:32 03/30/22 12:12 CAT Mt.Juliet,TN s
Wet Chemistry by Method 4500H+8-2011 WG1838206 1 03/25/22 13:15 03/25/22 13:15 EPW Mt.Juliet,TN Sr
Wet Chemistry by Method 4500P E-2011 WG1836684 400 03/23/22 00:24 03/23/22 00:24 TWF Mt.Juliet,TN
Wet Chemistry by Method 5210 B-2016 WG1836304 10 03/22/22 14:41 03/27/22 10:41 ABA Mt.Juliet,TN r:
Cc
Wet Chemistry by Method 5310 B-2014 WG1838693 1 03/26/22 13:21 03/26/22 13:21 GJA Mt.Juliet,TN
Metals(ICP)by Method 200.7 WG1837408 1 03/24/22 19:07 03/25/22 14:24 KMG Mt.Juliet,TN 7
Metals(ICP)by Method 200.7 WG1837408 1 03/24/22 19:07 03/26/22 12:33 KMG Mt.Juliet,TN GI
Metals(ICP)by Method 200.7 WG1837408 5 03/24/22 19:07 03/25/22 18:21 KMG Mt.Juliet,TN
Al
9
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 3 of 22

• • CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers,with the
Cp
appropriate preservatives,and within method specified holding times, unless qualified or notated within
the report. Where applicable,all MDL(LOD)and RDL(LOQ)values reported for environmental samples ?Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative,a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge,all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory,and no information or data have been 4
knowingly withheld that would affect the quality of the data. Cn
s
Sr
Qc
7GI
Heather J Wagner R
Project Manager Al
ScC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/2211:41 4 of 22

- EFFLUENT SAMPLE RESULTS - 01
Collected date/time: 03/21/22 14:15 L1473661
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch Cp
Analyte ug/I ug/I date/time
Dissolved Solids 10400000 200000 1 03/22/2022 19:29 WG1836555 Tc
Gravimetric Analysis by Method 2540 D-2015 35s
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4
Cn
Suspended Solids 990000 50000 1 03/24/2022 21:13 WG1837996
5
Wet Chemistry by Method 300.0 Sr
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time Qc
Chloride 4770000 100000 100 03/22/2022 20:45 WG1836300
Sulfate 204000 50000 10 03/24/2022 21:28 WG1837980 7 GI
Wet Chemistry by Method 350.1
Al
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time
a
Ammonia Nitrogen 36400 2500 10 03/25/2022 15:44 WG1837876 Sc
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time
Phosphorus,Total 142000 10000 100 03/31/202214.39 WG1841250
Sample Narrative:
L1473661-01 WG1841250:Results confirmed by re-analysis
Wet Chemistry by Method 420.4 .
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time
Total Phenol by 4AAP ND 40.0 1 03/30/202212:12 WG1839168
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier Dilution Analysis Batch
Analyte su date/time
pH 5.01 T8 1 03/25/2022 13:15 WG1838206
Sample Narrative:
L1473661-01 WG1838206:5.01 at 17.8C
Wet Chemistry by Method 4500P E-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time
Phosphate,Ortho 393000 12000 400 03/23/2022 00:24 WG1836684
Sample Narrative:
L1473661-01 WG1836684:Result confirmed by re-analysis
Wet Chemistry by Method 5210 B-2016
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time
BOD 27500 K1 K6 20000 10 03/27/202210:41 WG1836304
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 5 of 22

• EFFLUENT SAMPLE RESULTS - 01
Collected date/time: 03/21/22 14:15 L1473661
Wet Chemistry by Method 5310 B-2014
Result Qualifier RDL Dilution Analysis Batch CP
Analyte ug/I ug/I date/time
TOC(Total Organic Carbon) 6870 1000 1 03/26/2022 13:21 WG1838693 TC
Metals (ICP) by Method 200.7
Ss
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4
Cadmium 6.77 2.00 1 03/25/202214.24 WG1837408 Cn
Chromium 16.8 10.0 1 03/25/2022 14:24 WG1837408
Copper 403 10.0 1 03/25/202214.24 WG1837408
Iron 10000 100 1 03/26/2022 12:33 WG1837408 11111
Lead ND 5.00 1 03/25/2022 14:24 WG1837408
Nickel 172 10.0 1 03/25/2022 14:24 WG1837408 QO
Sodium 1020000 5000 5 03/25/2022 18:21 WG1837408
Zinc 322 50.0 1 03/25/2022 14:24 WG1837408 7GI
s
Al
9
SC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 6 of 22

WG1836555 QUALITY CONTROL SUMMARY
Gravlmetric Analysis by Method 2540 C-2011 L1473661-01
Method Blank (MB)
(MB)R3773683-1 03/22/22 19:29 CiJ
MB Result MB Qualifier MB MDL MB RDL 2
Analyte ug/I ug/I ugh Tc
Dissolved Solids U 10000 10000 —_._
Ss
L1472030-03 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1472030-03 03/22/22 19:29•(DUP)R3773683-3 03/22/22 19:29 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Sr
Analyte ug/I ug/I % %
Dissolved Solids 789000 831000 1 5.10 J' 5 6
QC
L1472030-04 Original Sample (OS) • Duplicate (DUP) 7G1
(OS)L1472030-04 03/22/22 19:29•(DUP)R3773683-4 03/22/22 19:29
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits Al
Analyte ug/I ug/I %
Dissolved Solids 768000 767000 1 0.173 5 JSC
Laboratory Control Sample (LCS)
(LCS)R3773683-2 03/22/22 19:29
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
Dissolved Solids 8800000 8580000 97.5 77.4-123
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 7 of 22

WG1837996 QUALITY CONTROL SUMMARY •
Gravimetric Analysis by Method 2540 D-2015 L1473661-01
Method Blank (MB)
(MB)R3774212-1 03/24/22 21:13 Cp
MB Result MB Qualifier MB MDL MB RDL
z
Analyte ugh ugh' ugh' Tc
Suspended Solids U 2500 2500
Ss
L1474333-01 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1474333-01 03/24/22 21:13•(DUP)R3774212-3 03/24/22 21:13 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPLimits RPDF.Sr
Analyte ug/I ug/I % %
Suspended Solids 129000 158000 1 20.2 J' 5
Qc
L1474336-02 Original Sample (OS) • Duplicate (DUP) 7GI
(OS)L1474336-02 03/24/22 21:13•(DUP)R3774212-4 03/24/22 21:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPts RPD
Limi Al
Analyte ugh ug/I % %
Suspended Solids 58000 61600 1 6.02 I.' 5 Sc
Laboratory Control Sample (LCS)
(LCS)R3774212-2 03/24/22 21:13
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ugh ugh % %
Suspended Solids 773000 880000 114 85.7-114
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 8 of 22

WG1836300 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 300.0 L1473661-01
Method Blank (MB) ,
Cp.
(MB)R3773597-1 03/22/22 09:31
MB Result MB Qualifier MB MDL MB RDL 1
Analyte ug/I ug/I ug/I Tc
Chloride U 379 1000
'SS
L1473729-01 Original Sample (OS) • Duplicate (DUP) 4Cn
(OS)L1473729-01 03/22/22 14:01•(DUP)R3773597-3 03/22/22 14:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits Sr
Analyte ug/I ug/I % %
Chloride 4610 4450 1 3.49 20 5
Qc
L1473751-14 Original Sample (OS) • Duplicate (DUP) 7GI
(OS)L1473751-14 03/22/22 19:51•(DUP)R3773597-7 03/22/22 20:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Al
Limits
Analyte ug/I ug/I % %
Chloride 13200 12800 1 2.83 20 Sc
Laboratory Control Sample (LCS)
(LCS)R3773597-2 03/22/22 09:44
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
Chloride 40000 38400 96.0 90.0-110
L1473729-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1473729-01 03/22/22 14:01•(MS)R3773597-5 03/22/22 14:55•(MSD)R3773597-6 03/22/22 15:08
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
Chloride 50000 4610 56300 56500 103 104 1 80.0-120 0.347 20
L1473751-14 Original Sample (OS) • Matrix Spike (MS)
(OS)L1473751-14 03/22/22 19:51•(MS)R3773597-8 03/22/22 20:18
Spike Amount Original Result MS Result MS Rec. Dilution Rec.Limits MS Qualifier
Analyte ug/I ugh' ug/I % %
Chloride 50000 13200 62100 97.8 1 80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 9 of 22

WG1837980 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 300.0 L1473661-01
Method Blank (MB)
(MB)R3774104-1 03/24/22 21:02 Ci
MB Result MB Qualifier MB MDL MB RDL 2
Analyte ugh' ug/I ug/I TC
Sulfate U 594 5000
3
SS
1_1474616-09 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1474616-09 03/24/22 22:19•(DUP)R3774104-3 03/24/22 22:32 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPLimits RPD
Sr
Analyte ugh ugh % %
Sulfate ND ND 1 0.000 20 6
QC
L1474827-05 Original Sample (OS) • Duplicate (DUP) 7Gl
(OS)L1474827-05 03/25/22 03:14•(DUP)R3774104-6 03/25/22 03:27
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits "Al
Analyte ugh ug/I % %
Sulfate 9860 10100 1 2.56 20 `'Sc
Laboratory Control Sample (LCS)
(LCS)R3774104-2 03/24/22 21:15
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
Sulfate 40000 39600 98.9 90.0-110
L1474616-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1474616-09 03/24/22 22:19•(MS)R3774104-4 03/24/22 22:45•(MSD)R3774104-5 03/24/22 22:58
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % %
Sulfate 50000 ND 50600 52400 101 105 1 80.0-120 3.58 20
L1474827-05 Original Sample (OS) • Matrix Spike (MS)
(OS)L1474827-05 03/25/22 03:14•(MS)R3774104-7 03/25/22 03:40
Spike Amount Original Result MS Result MS Rec. Dilution Rec.Limits MS Qualifier
Analyte ug/I ugh ugh % %
Sulfate 50000 9860 58700 97.7 1 80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 10 of 22

WG1837876 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1473661-Ot
Method Blank (MB) •
(MB)R3774177-1 03/25/22 15:04 ._. I Cp I•
MB Result MB Qualifier MB MDL MB RDL 2
Analyte ug/I ug/I ug/1 Tc
Ammonia Nitrogen U 117 250
3
Ss
L1472727-01 Original Sample (OS) • Duplicate (DUP)
_-- 4Cn
(OS)L1472727-01 03/25/22 15:13•(DUP)R3774177-5 03/25/22 15:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Sr
Analyte ug/I ug/I %
Ammonia Nitrogen ND ND 1 5 65 10
L1473607-02 Original Sample (OS) • Duplicate (DUP) 'GI
(OS)L1473607-02 03/25/22 15:34•(DUP)R3774177-7 03/25/22 15:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits JAI
Analyte ug/I ug/I % %
Ammonia Nitrogen 298 321 1 7.43 10 9
Sc
Laboratory Control Sample (LCS)
(LCS)R3774177-2 03/25/22 15:05
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
Ammonia Nitrogen 7500 7220 96.2 90.0-110
L1473502-01 Original Sample (OS) • Matrix Spike(MS)
(OS)L1473502-01 03/25/22 15:31•(MS)R3774177-6 03/25/22 15:32
Spike Amount Original Result MS Result MS Rec. Dilution Rec.Limits MS Qualifier
Analyte ug/I ug/I ug/I % %
~__
Ammonia Nitrogen 5000 2560 7180 92.4 1 90.0-110
L1472411-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1472411-01 03/25/22 16:03•(MS)R3774177-8 03/25/22 16:05•(MSD)R3774177-9 03/25/22 16:06
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/1 ug/1 ugh ug/I % % % % %
Ammonia Nitrogen 5000 ND 4970 5140 99.4 103 1 90.0-110 3.32 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 11 of 22

WG1841250 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4 L1473661-01
Method Blank (MB) •
(MB)R3776174-1 03/31/22 12:44
MB Result MB Qualifier MB MDL MB RDL , -
---Analyte ug/I ug/I ug/I f c
Phosphorus,Total 66.4 35.0 100
Ss
L1472727-01 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1472727-01 03/31/22 12:47•(DUP)R3776174-3 03/31/22 12:48 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
5Sr
Analyte ug/I ug/I % %
Phosphorus,Total 7240 6900 2 4.81 20 5
Qc
Laboratory Control Sample (LCS) 7GI
(LCS)R3776174-2 03/31/22 12:46
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ugh' % % Al
Phosphorus,Total 7560 7130 94.3 83.2-116
Sc
L1472727-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1472727-01 03/31/22 12:47•(MS)R3776174-4 03/31/22 12:49•(MSD)R3776174-5 03/31/22 12:51
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
Phosphorus,Total 2500 7240 8320 8820 43.2 63.2 2 90.0-110 _ 1_: 5.83 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 12 of 22

WG1839168 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 420.4 L1473661-01
Method Blank (MB)
(MB)R3775689-1 03/30/22 12:07 1
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/1 ug/I ug/1 Tc
Total Phenol by 4AAP U 8.30 40.0
Ss
L1473729-05 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1473729-05 03/30/22 12:18•(DUP)R3775689-5 03/30/22 12:19 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPits RPD5
Lim
Sr
Analyte ug/1 ug/I % %
Total Phenol by 4AAP 46.6 ND 1 55.7 P" 20
Qc
L1474149-02 Original Sample (OS) • Duplicate (DUP) 7GI
(OS)L1474149-02 03/30/22 12:22•(DUP)R3775689-7 03/30/22 12:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits Al
Analyte ug/1 ugh % %
Total Phenol by 4AAP ND ND 1 0.000 20 `'SC
Laboratory Control Sample (LCS)
(LCS)R3775689-2 03/30/22 12:08
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/1 ug/1 % %
Total Phenol by 4AAP 500 502 100 90.0-110
L1472888-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1472888-02 03/30/22 12:10•(MS)R3775689-3 03/30/22 12:11•(MSD)R3775689-4 03/30/22 12:12
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ugh ugh % % % % %
Total Phenol by 4AAP 500 ND 892 895 178 179 1 90.0-110 lb 0.369 20
L1473729-06 Original Sample (OS) • Matrix Spike (MS)
(OS)L1473729-06 03/30/22 12:19•(MS)R3775689-6 03/30/22 12:20
Spike Amount Original Result MS Result MS Rec. Dilution Rec.Limits MS Qualifier
Analyte ugh ugh' ugh % %
Total Phenol by 4AAP 500 ND 895 178 1 90.0-110 ib
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 13 of 22

WG1838206 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500H+ B-2011 L1473661-01
L1473269-01 Original Sample (OS) • Duplicate (DUP)
(OS)L1473269-01 03/25/22 13:15•(DUP)R3774080-2 03/25/22 13:15 Cp
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits `Ic
Analyte su su
pH 8.59 8.59 1 0.000 1
SS
Sample Narrative:
OS:8.59 at 16.7C 4Cn
Cn
DUP:8.59 at 16.7C
Sr
L1473441-01 Original Sample (OS) • Duplicate (DUP)
(OS)L1473441-01 03/25/22 13:15•(DUP)R3774080-3 03/25/22 13:15 _ QC
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Llmits
Analyte su su % % GI
pH 7.41 7.80 1 5.13 1
Al
Sample Narrative:
OS:7.41 at 16.5C 9
DUP:7.8 at 17.3C SC
Laboratory Control Sample (LCS)
(LCS)R3774080-1 03/25/22 13:15
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte su su
pH 10.0 9.94 99.4 99.0-101
Sample Narrative:
LCS:9.94 at 19.5C
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 14 of 22

WG1836684 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500P E-2011 L1473661-01
Method Blank (MB)
Cp •
(MB)R3772802-1 03/22/22 23:48
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I Tc
Phosphate,Ortho U 14.0 30.0
3Ss
L1473605-01 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1473605-01 03/22/22 23:53•(DUP)R3772802-5 03/22/22 23:54 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Sr
Analyte ug/I ug/I % %
Phosphate,Ortho ND ND 20 0.000 20 •
Qc
Laboratory Control Sample (LCS)
GI
(LCS)R3772802-2 03/22/22 23:48
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Al
Analyte ug/I ug/I % %
Phosphate,Ortho 245 257 105 85.0-115
Sc
L1473604-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1473604-01 03/22/22 23:49•(MS)R3772802-3 03/22/22 23:50•(MSD)R3772802-4 03/22/22 23:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ugh' % % % % %
Phosphate,Ortho 500 64.0 513 510 89.8 89.2 1 80.0-120 0.587 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 15 of 22

WG1836304 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 5210 B-2016 L1473661-01
Method Blank (MB)
(MB)R3774447-1 03/27/22 12:47
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
BOD U 200 200
'Ss
L1473684-02 Original Sample (OS) • Duplicate (DUP) 4
(OS)L1473684-02 03/27/22 10:47•(DUP)R3774447-3 03/27/22 10:49 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPLimits RPD
Sr
Analyte ug/I ug/I % %
BOD 3740 3440 1 8.36 30
QC
L1473714-01 Original Sample (OS) . Duplicate (DUP) 7GI
(OS)L1473714-01 03/27/22 11:16•(DUP)R3774447-4 03/27/22 11:18
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits Al
Analyte ug/I ug/I % %
BOD 3470 4670 1 29.5 30 Sc`'
Laboratory Control Sample (LCS)
(LCS)R3774447-2 03/27/22 09:12
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
BOD 198000 160000 80.7 84.6-115
.j-
LilI.)oratory Control San-iple (LCS)
(LCS)R3774447-5 03/27/22 12:22
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
BOD 198000 U 0 84.6-115
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 16 of 22

•
WG1838693 QUALITY CONTROL SUMMARY .
Wet Chemistry by Method 5310 B-2014 L1473661-01
Method Blank (MB) •
(MB)R3774762-2 03/26/22 10:02
MB Result MB Qualifier MB MDL MB RDL I
Analyte ug/I ug/I ug/I ?C
TOC(Total Organic Carbon) 590 102 1000
3
Ss
L1473661-01 Original Sample (OS) • Duplicate (DUP)
4
(OS)L1473661-01 03/26/22 13:21•(DUP)R3774762-5 03/26/22 13:38 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Sr
Analyte ugh! ug/I % %
TOC(Total Organic Carbon) 6870 6970 1 1.49 20
Qc
Laboratory Control Sample (LCS) 7G1
(LCS)R3774762-1 03/26/22 09:47
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Al
Analyte ug/I ug/I % %
TOC(Total Organic Carbon) 75000 74100 98.8 85.0-115 9
Sc
L1472777-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1472777-01 03/26/22 11:54•(MS)R3774762-3 03/26/22 12:16•(MSD)R3774762-4 03/26/22 12:37
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
TOC(Total Organic Carbon) 50000 6950 57400 57000 101 100 1 80.0-120 0.787 20
L1473675-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1473675-03 03/26/22 15:20•(MS)R3774762-6 03/26/22 15:43•(MSD)R3774762-7 03/26/22 16:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
TOC(Total Organic Carbon) 50000 4110 53500 53800 98.7 99.4 1 80.0-120 0.653 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 17 of 22

WG1837408 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 200.7 L1473661-01
Method Blank (MB)
l2,
(MB)R3774220-1 03/25/22 14:07 1
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/1 ug/I ugh' .TC
Cadmium U 0.552 2.00
Chromium U 1.63 10.0 3 SS
Copper U 2.26 10.0
Lead U 2.27 5.00 4
Nickel U 1.82 10.0 Cn
Sodium U 444 1000
Zinc U 5.78 50.0 5Sr
6
Method Blank (MB) Qc
(MB)R3774323-1 03/26/22 12:16
7
MB Result MB Qualifier MB MDL MB RDL GI
Analyte ug/I ugh ug/I
Iron U 20.5 100 sAi
Laboratory Control Sample (LCS) 9Sc
(LCS)R3774220-2 03/25/22 14:10
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
Cadmium 1000 987 98.7 85.0-115
Chromium 1000 945 94.5 85.0-115
Copper 1000 959 95.9 85.0-115
Lead 1000 971 97.1 85.0-115
Nickel 1000 968 96.8 85.0-115
Sodium 10000 9720 97.2 85.0-115
Zinc 1000 933 93.3 85.0-115
Laboratory Control Sample (LCS)
(LCS)R3774323-2 03/26/22 12:19
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte ug/I ug/I % %
Iron 10000 9530 95.3 85.0-115
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 18 of 22

•
WG1837408 QUALITY CONTROL SUMMARY .
Metals (ICP) by Method 200.7 L1473661-01
L1473652-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1473652-01 03/25/22 14:13•(MS)R3774220-4 03/25/22 14:19•(MSD)R3774220-5 03/25/22 14:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits -- --
Analyte ug/I ug/I ug/I ug/I % % % % %
Cadmium 1000 ND 1020 1010 102 101 1 70.0-130 0.848 20 ._.---u
Chromium 1000 ND 977 956 97.7 95.6 1 70.0-130 2.14 20 SS
Copper 1000 ND 964 967 96.4 96.7 1 70.0-130 0.321 20
Lead 1000 ND 992 982 99.2 98.2 1 70.0-130 1.02 20 4
Nickel 1000 ND 994 981 99.4 98.1 1 70.0-130 1.38 20 Cn
Sodium 10000 28600 37500 37500 89.4 89.8 1 70.0-130 0.0962 20
Zinc 1000 ND 954 944 95.4 94.4 1 70.0-130 1.10 20 cSr
6
L1473661-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) Qc
(OS)L1473661-01 03/25/22 14:24•(MS)R3774220-6 03/25/22 14:27•(MSD)R3774220-7 03/25/22 14:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Gl
Analyte ugh' ug/1 ug/I ug/1 % % % % %
Cadmium 1000 6.77 1130 1130 112 113 1 70.0-130 0.0611 20 I
Al
Chromium 1000 16.8 944 945 92.8 92.8 1 70.0-130 0.0600 20
Copper 1000 403 1460 1460 106 106 1 70.0-130 0.109 20
Lead 1000 ND 990 995 99.0 99.5 1 70.0-130 0.446 20 SC
Nickel 1000 172 1190 1200 102 103 1 70.0-130 0.351 20
Sodium 10000 1050000 1040000 1060000 0.000 36.4 1 70.0-130 E V E V 1.15 20
Zinc 1000 322 1200 1200 87.8 88.0 1 70.0-130 0.196 20
L1473652-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1473652-01 03/26/22 12:21•(MS)R3774323-4 03/26/22 12:27•(MSD)R3774323-5 03/26/22 12:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ugh' ug/I ug/I ug/I % % % % %
Iron 10000 ND 9760 9600 97.6 96.0 1 70.0-130 1.60 20
L1473661-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1473661-01 03/26/22 12:33•(MS)R3774323-6 03/26/22 12:36•(MSD)R3774323-7 03/26/22 12:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/1 ug/I ug/I ug/I % % % % %
Iron 10000 10000 19200 19200 91.5 91.8 1 70.0-130 0.164 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 19 of 22

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The Information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
Cp
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, Tc
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
3
Abbreviations and Definitions Ss
MDL Method Detection Limit.
4
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery. 5 Sr
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit(or MDL where applicable). Qc
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the GI
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the
result reported has already been corrected for this factor. 8Ai
These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges. ScC
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The Information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary(Qc) analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration(ICAL).
J The identification of the analyte is acceptable;the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination;spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is low.
J- The associated batch QC was outside the lower control limits;associated data has a potential negative bias.
K1 The sample dilutions set-up for the BOD/CBOD analysis did not meet the oxygen depletion criteria of at least 2 mg/L.
Reported result is an estimated value.
K6 Glucose/glutamic acid BOD/CBOD was below method acceptance criteria.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8 Sample(s)received past/too close to holding time expiration.
V The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc L1473661 04/07/2211:41 20 of 22

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05 L- -
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975 l `
Arkansas 88-0469 New Jersey—NELAP TN002
California 2932 New Mexico' TN00003
Colorado TN00003 New York 11742 Ss
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina' DW21704 4
Georgia NELAP North Carolina' 41 C n
Georgia' 923 North Dakota R-140
Idaho TN00003 Ohio—VAP CL0069
Illinois 200008 Oklahoma 9915 Sr
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356 0C
Kentucky 15 KY90010 South Carolina 84004002
Kentucky I 16 South Dakota n/a 7
Louisiana 4130792 Tennessee'° 2006 GI
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas 5 LAB0152 8A'
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033 9
Minnesota 047-999-395 Washington C847 SC
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA—ISO 17025 5 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
'Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity °ChemicaVMicrobiological 5 Mold 'Wastewater n/a Accreditation not applicable
'Not all certifications held by the laboratory are applicable to the results reported in the attached report.
'Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. L1473661 04/07/22 11:41 21 of 22

Company Name/Address: Billing Information: I An,jvcic/rnntA,npr/Drpcervatl,u )Chain of Custody Page_of
Frit Car Inc. Accounts Payable Pres ; C6
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PO Box 1340 ace ,.
2012 US Hwy 17N Brewton,AL 36427 KONA ADVANC NG SCIENCE
New Bern,NC 28560 ,n
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Report to Ema l To [e-mail] O.
0 12055 le W reth Rd Mont 4041.TN 17122
Subnunn,A,Rmpe.o,tr.'th0=n of 4000
Chris Barnes 40040E40i aclno*eedVnoen,*Ad otter..Of the
City/State Please Circe a Path Term.wcondno f+««p„
Project Description: 2t.� r�^ Ce nut,Term and Cee mn,/hpb+uws,urdud-
Bridgeton Facility Monthly Collected l7 )✓L PT MT CT rd,
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g Rush? (Lab MUST Be Notified) a vt a w a a Same Day _Five Day = = o E o _ = w Preloain:P902034
Next Day 5 Day(Rad Duty) Date Results Needed C a.m.'
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Immediately Two Day 10 Day(Rad Only) No. t� 0 s1S al C7 0 i O p = PB:"J''+i, �` t✓ ,.)2.:j 2
Three Day of r"'s ti. rrt S cl C _2
Packed on Ice N Y u1 0 N cn N N .-r Shipped
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Sample ID Comp/Grab Matrix Depth Date Ti c 0 -� _ rp I 0 I i— o 0 hemafts `Am ,t
m u Z z a a. a f— f- 1—
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•Matrix Remarks: ! en rt,yrs Lc>J p� Lead N to 1 Sample Receipt Checklist/
d AIR-Air F-Filter Lo�tM1�U� G�!}CO 1 j rL pH Temp CCC Seal Present/Intact: NB (Y
Z;�` 1���t (60 d;,J M y�'rol f5ro 1/ieedi2d COL Signed/Accurate: _
55-So N
Gw-Groundwater B-Bioassay i
Flow Other Bottles arrive intact: _N
WW-Waste Water Correct bottles used: _ _N
Sufficient volume sent: N
DW-Dunking Water Samples returned via:
OT-Other Tracking# If Applicable
UPS FedEx _Courier VOA Zero Peadapace: Y N
> ?reservation Correct/Checked: N
Relf uu d b •(Signature) Date: Time Received by.(Signature) Trip Blank Received: Yes/ `�d RAD Screen c0.5 mR/hr: _Y _N
✓L J - /� 4cz) /D HCL/Meofi
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Time: Received b Si Bottles Received: If preservation required by Login:Date/Time
Relinquished by:(Signature) Date. y (Signature)nature) Tem }4p9-C
Relinquished by (Signature) Date: Time: Re
eived or lab by:(Signature) Da,le: Time: Hold: Conditio
J/�,G '� 3P-. -�' C NCF / �/