WQ0018087_Monitoring - 12-2021_20220202

DAK Americas
January 19,2022
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
Subject: Permit No. WQ00.1.884- S'orr►
Cape Fear Manufacturing Facility
Surface Disposal of Class B Residuals (Dedicated)
Brunswick County
Dear Division of Water Resources:
Enclosed please find:
1. Two copies of Compliance and Monitoring Form (GW-59)for the 6 we
associated with the Sludge Disposal Unit. ',"1 fp:
2. Laboratory analysis for these same wells. F
3. Compliance Report Form GW-59a 2 2022
4. Summary of the Groundwater Monitoring Results
As shown in the summary, some of the results in the monitoring wells are above the ' "E'1h
permit limits. However,these results remain consistent with previous results and most
results show decreases in concentration. The regional office has received this data.
No additional actions are planned at this time.
If additional information is needed,please feel free to contact either myself on 910-371-
5232 or Larry Young on 910-264-2564.
Sincerely yours,
/4/7 0-Naii37
Penny C. Mahoney
Sustainability Director rn
DAK Americas LLC j' Cl)
rN
DAK Americas LLC • 1205 Culbreth Drive, Suite 100 •Wilmington, NC 28405
910-371-4863(Phone) • 910-371-4456(Fax)
www.dakamericas.com

GW-59A COMPLIAiNCE REPORT FORM Permit# W900/00117 "
(Submit one each monitoring period with GW-59 forms.)
1 Enter date monitoring results were due.(�/,//2�) Will this monitoring report(GW-59 and GW-59A) YES , NO •
be submitted after the established due date?
2 Was any required information missing on the GW-59 report forms? YES ley) -
IF the answer to question 1 or 2 is"YES", list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?If the answer is "Yes",contact the Regional Office for guidance.
4 Are any monitored constituents equal to or above the established standards? YE/VS
E� NO
If the answer to question 4 is"NO", skip to section 8.
If the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below: See 0E'7` TC,cl
5 For the constituents identified in question 4 above,have standards been exceeded previously for the YES,,NO
same constituent(s)in the same well(s)in the last two years? !!/
If the answer to question 5 is"NO", skip to section 8.
If the answer to question 5 is"YES';list in the space provided below, each well with constituent(s)exceeding
standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years).
.Sew Cy 7-a-e•/ 47
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YE - NO
If the answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is "NO",monitoring wells maybe improperly
located;contact the Regional Office.
OFclCe 4`.� 4...2e :,1 n ,,-/r-tc 7 e- ,,,
7 Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem?
If the answer to question 7 is"YES", describe those actions in the space provided below.
If the answer to question 7 is"NO", contact the Regional Office within 90 days;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation.
fines,and/or penalties.
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby ack owledge that the above information was evaluated and the information submitted in this
report(C lance e Thrt GW- A)is true and complete to the best of my knowledge.
CZ-" 4
Sign re f Permittee(or Authoriz d'A- nt) / / Date
GW-59A 12/8/2003

•
Permit MW-2A MW-2B MW-2C
Parameter Limit Units Dec-16 Dec-19 Dec-21 Dec-16 12/16 Rspl Jun-17 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21 Dec-16 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21
Ammonia Nitrogen 1.5 mg/I 12.0 82.5 83.5 47.9 84.3 37.9 53.5 32.9 18.0
Total Dissolved Solids 500 mg/I 827 509 632 673 727 800 692 753 588 597 568 504 744
Nitrate 10 mg/I 14.3 10.8 21.2 15.5
Arsenic 0.01 mg/I 0.017 0.02 0.02 0.02
Cobalt* 0.001 mg/I 0.002 0.022 0.021
pH 5.5 5.13
Permit MW-2D MW-2E
Parameter Limit Units Dec-16 12/16 Rspl Jun-17 Dec-17 Dec-18 Dec-19 Jun-21 Dec-16 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21 Dec-21
Ammonia Nitrogen 1.5 mg/I 157 12.8 96.4 142 80.5 45.8 57.3 9.5 11.0 8.5 5.5 3.3 8.4
Total Dissolved Solids 500 mg/I 678 846 532
Arsenic 0.01 mg/I 0.02
Cobalt* 0.001 mg/I 0.003 0.005 0.004
*New limit in 2020 permit
MW-2€ MW-02B
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Restricted Internal Use

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original 'EPARTMEN�'OP ENVIRON ENT INhTURAL REESOURCE$,
GROUNDWATER QUALITY MONITORING: �r. ISIO`N OF WAT�R�pU rIb �RMATION I:RCIC�SSING'UNIT
COMPLIANCE REPORT FORM and 1 copy to. L671MNLSERVICE�bIc7N'1E1 1 r,�1LEIGH,NC{27694677 ,`PFiane (-04)'733*2i
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington (,,,,„0) NC 28403 County Brunswick 0 Lagoon ❑Remediation: Infiltration Gallery
"diy) (
''`a"') i`J`'' ❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] El Rotary Distributor El Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2A No.of wells to be sampled: 6 ❑ Water Source Heat Pump N Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2A Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13.0 ft. Well Diameter: 2.0 in. pH 6.85 units Temp. 19.3 °C DRY at
Depth to Water Level: 7.6 ft.below measuring point Screened Interval: 3.0 ft. to 13.0 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 1.92 ft.above land surface Relative M.P. Elevation: 20.39 ft. Odor None check
Volume of water pumped/bailed before sampling: 10 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑NO and field acidified: ®YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: 12/03/21- 12/08/21 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N <0.02 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0.22 mg/I Zn-Zinc <0.01 mg/I
Coliform:MF Total /100m1 Phosphorus:Total as P <0.04 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 273 mg/I Al-Aluminum mg/I Cobalt-0.002mg/I
pH(when analyzed) 6.8 units Ba-Barium mg/I Selenium -<0.01 mg/I
TOC mg/I Ca-Calcium_ mg/I
Chloride 9 mg/I Cd-Cadmium <0.001 mg/I
Arsenic <0.01 mg/I Chromium:Total <0.01 mg/I
Grease and Oils ' mg/I Cu-Copper <0.01 mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 0.4 mg/I Mg-Magnesium 3.16 mg/I , method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese mg/I method#
TKN as N mg/I Ni-Nickel <0.01 mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility y'fines imprison"ten)for knowing violations
sa .
Penny C. Mahoney- Director of Sustainability and Operations Supp / /
- . /,
Permittee(or Authorized Agent)Name and Title-Please print or type gnat r- .'fermi esr(•r Authorized,Ag (Date)
GW-59 Rev.1/2007 /

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original''EPARTMENTOF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 7 copy to 'VISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Dr, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation:Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2B No.of wells to be sampled: 6 ❑ Water Source Heat Pump ®Other:Surface Disposal Res.Sol
(from Permit) _
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2B Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH units Temp. °C DRY at
Depth to Water Level: 8.7 ft.below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 2.9 ft,above land surface Relative M.P.Elevation: 24 ft. Odor check
Volume of water pumped/bailed before sampling: gallons Appearance here: X
Samples for metals were collected unfiltered: EYES ❑NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: Laboratory Name: Certification No.
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/1
Coliform: MF Total /100m1 Phosphorus:Total as P mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/1 Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total mg/I Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/I
TOC mg/1 Ca-Calcium mg/I
Chloride mg/I Cd-Cadmium mg/I
Arsenic mg/I Chromium:Total mg/I
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/1 (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/1 Hg-Mercury mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC ,method#
Total Ammonia mg/1 Mg-Magnesium mg/I ,method#
(Ammonia Nitrogen:NH,as N:Ammonia Nitrogen,Total)
Mn-Manganese mg/I ,method#
TKN as N mg/I Ni-Nickel mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
(certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete.anr!Mat the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laborat• . I am aware that there are si.nificant penalties for submitting false information.indudin•the possibility of fines and impracnment for Knowin•vir'ations.
Penny C. Mahoney Director of Sustainability and Operations Supp / / _ / /% �L
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Per '•--(or Alit on ed Agent (Date)
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original"EPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy to: •IVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2C No. of wells to be sampled: 6 ❑ Water Source Heat Pump ®Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2C Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH units Temp. °C DRY at
Depth to Water Level: 8.1 ft.below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 3.05 ft.above land surface Relative M.P.Elevation: 25 ft. Odor check
Volume of water pumped/bailed before sampling: gallons Appearance here: A.
Samples for metals were collected unfiltered: OYES ❑NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: Laboratory Name: Certification No.
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/I
Coliform: MF Total /100ml Phosphorus:Total as P mg/I
(Note Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total _ mg/l Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/I
TOC mg/I Ca-Calcium mg/I
Chloride mg/I Cd-Cadmium mg/I
Arsenic mg/I Chromium:Total mg/I
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC ,method#
Total Ammonia mg/I Mg-Magnesium mg/I ,method#
(Ammonia Nitrogen;NN3as N;Ammonia Nitrogen,Total) Mn-Manganese mg/I ,method#
TKN as N mg/I Ni-Nickel mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical da:a was produced using approved methods of analysis by a
DWQ-certified laborato . I am aware that there are significant•enalties for submtten a false information,including the possibiti rif fines and imprisonment for knowip• violations.
Penny C. Mahoney- Director of Sustainability and Operations Supp .--1J 4/1-1---e",-7 �- //%Permittee(or Authorized Agent)Name and Title-Please print or type Signature 15f,P tttee(or Authorized A :Date)
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
ry((( s r4:14?� , a1IEPA[i71'.'!ENTOF.ENVIRONPIIENT&NATURAL RESOURCES
jiGROUNDWATERQUALITY ONITORING. k""� ° '+IVISIONOFWATER:QUALIY-INFORMATIONPROCESSINGUNIT
1COli3it�UANCE REPORT FORM •l�'"., t';. r t" 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1517 Phone:(919}733-3221
IFACIUTY INFORMATION Pfeese Print Clearlyy or Type (PERMIT Number.W(20018087 Expiration Date: Jan, 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
'Permit Name(if different): INPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick I, ❑ Lagoon ❑Remediation:Infiltration Gallery
II • ❑ Y
S ra Field ❑Remediation:
P
Contact Person: Larry Young Telephone#: [phone] ElRotary Distributor ElLand Application of Sludge
iWell Location/Site Name:Down gradient/Monitoring Well#2D No.of wells to be sampled: 6 ❑ Water Source Heat Pump t'Other:Surface Disposal Res.Sol
o- (L-om Penrvul I ..
SAMPLING INFORMATION( If WELL
WELL ID NUMBER(from Permit): MW#2D Date sample collected: 12/02/21 FIELD ANALYSES WAS
tWell Depth: 13 ft. Well Diameter: 2.0 in. pH units Temp. °C DRY at
time of
Depth to Water Level: 8.2 ft.below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. Mhos
sampling,
Measuring Point is 3-0 fL above land surface Relative M.P.Elevation: 22 ft. Odor check
.Volume of water pumped/bailed before sampling: gallons Appearance here:
Samples for metals were collected unfiltered: OYES ❑NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
liDate sample analyzed: Laboratory Name: Certification No.
1PARAIVIETERS NOTE:Values should reflect dissolved and colloidal concentrations.
ll COD ma/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
p Coliform:MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/I
i Coliform:ME Total /100m1 Phosphorus:Total as P mg/1
(Nolo: Use MPN methoe for highly toro:(1 samPres) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total mg/I Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/I
TOC mg/I Ca-Calcium mg/I
Chloride mg/I Cd-Cadmium mg/I
Arsenic mg/I Chromium:Total mg/1
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? ❑ Yes(1) R No(0)
Specific Conductance J.iMho5 K-Potassium mg/I VOC ,method#
Total Ammonia mg/I Mg-Magnesium mg/I ,method# pE+
Ammonia Nitrogen;NH,as N:Ammonia Nitrogen,Total) Mn-Manganese mg/I method#
TKN as N mg/I Ni-Nickel mg/l ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Y o ie rcif • o • rn +n i+s t qre a co e'a t 'et bore 'c ,,data j;.. aged'P(s gIa ved e(h" p' CK 1 s s,'t�a i' �tLL
lC k�" iti' t Y . .. c7 t. xl �: �% z et :'�R • M w s:
�o>ti�QeC.E11.�e. :.�^I.r -'r(L2.8Lettf12}fi1e7_ rij.�' r:?it.att+PS S G•° ..- o. .dtl.• 1u•11g. ea• - ba(1'•�ne.-� f7•Y M• S,41. tOr ., 1194 J. �tr01Y ��'�.�'�.y����.�• ... 'r.?.
Penny C. Mahoney-Director of Sustainability and Operations Supp / • �� • / •q O 2
Permittee(or Authorized Agent)Name and Title-Please print or type Signetu e 0 P ti ee(0 thonzed Agent t a•')
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original 'EPARTMENT OF ENVIRONMENT&NATURA,I.RE5QURCES
GROUNDWATER QUALITY MONITORING: ISIONOFWATERQUALIT1f NFORMA11ONPROGEBSINGUNIT
and 1 copy to: „, r ,
COMPLIANCE REPORT FORM 6I7 IAIL'SERVICE°CENTER RALEIGH;;NC 2T99=1617 'Phone..[phone] ,
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date:^Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington ° `'' NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
l;:Ii" vt5ic) `t"' ❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2E No.of wells to be sampled: 6 ❑ Water Source Heat Pump ®Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2E Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH 6.05 units Temp. 18.2 °C DRY at
Depth to Water Level: 7.9 ft.below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 3.0 ft.above land surface Relative M.P. Elevation: 23 ft. Odor None check
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑NO and field acidified: [RYES ❑NO
LABORATORY INFORMATION
Date sample analyzed: 12/03/21 - 12/08/21 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N 0.07 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0.24 mg/I Zn-Zinc <0.01 mg/I
Coliform:MF Total /100m1 Phosphorus:Total as P <0.04 mg/I
(Note. Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 92 mg/I Al-Aluminum mg/I Cobalt-0.004 mg/I
pH(when analyzed) 6.6 units Ba-Barium mg/I Selenium -<0.01 mg/1
TOC mg/I Ca-Calcium mg/I
Chloride 6 mg/I Cd-Cadmium <0.001 mg/1
Arsenic <0.01 mg/I Chromium:Total <0.01 mg/I
Grease and Oils mg/1 Cu-Copper <0.01 mg/I ORGANICS:(by GC,GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/1 Report Attached? 0 Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC ,method#
Total Ammonia 8.4 mg/I Mg-Magnesium 1.27 mg/I ,method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total)
Mn-Manganese mg/1 , method#
TKN as N mg/I Ni-Nickel <0.01 mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief the information submitted in this report is true,accurate,and complete and thy;the laboratory analytical dsra was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines mid imprisonment ror knowica diolations.
Penny C. Mahoney- Director of Sustainability and Operations Supp /71z7�
Permittee(or Authorized Agent)Name and Title-Please print or type Signature -e Mee.or tut orized Agen 'ate)
GW-59 Rev.1/2007 `!/

SUBMIT FORM ON YFLLOW PAPER ONLY
Mail original °EPARTMENTOFI<NVIRONMENT4 NATURAL RESOVRCES
GROUNDWATER QUALITY MONITORING: 10NPF WA'I"ERQt1AXf7YYat1FOR#lIAT10 NPRQGE3sING.UNIT
COMPLIANCE REPORT FORM and 1 copy to !'617\MAILsiojAcECENTER RALI_IGH;.MC27699-16�17, Phone,"(919)`733-3221
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington "'"°"0 NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
"0 `a`',' ❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Background/Monitoring Well#3A No.of wells to be sampled: 6 ❑ Water Source Heat Pump lR Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#3A Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13.25 ft. Well Diameter: 2.0 in. pH 5.95 units Temp. 17.9 °C DRY at
Depth to Water Level: 5.7 ft. below measuring point Screened Interval: 3.25 ft. to 13.3 ft. Spec.Cond. µMhos time of
1.76 sampling,
Measuring Point is ft.above land surface Relative M.P. Elevation: 24.78 ft. Odor None check
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑NO and field acidified: ®YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: 12/03/21 - 12/08/21 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N 0.03 mg/I Pb-Lead <0.01 mg/I
Coliform:MF Fecal /100m1 Nitrate(NO3)as N 0.04 mg/I Zn-Zinc 0.015 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P <0.04 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 107 mg/I Al-Aluminum mg/I Cobalt-<0.001 mg/I
pH(when analyzed) 6.2 units Ba-Barium mg/I Selenium-<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride 7 mg/I Cd-Cadmium <0.001 mg/I
Arsenic <0.01 mg/I Chromium:Total <0.01 mg/I
Grease and Oils mg/I Cu-Copper 0.010 mg/I ORGANICS:(by GC, GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 0.2 mg/I Mg-Magnesium 1.00 mg/I ,method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese mg/I method#
TKN as N mg/I Ni-Nickel <0.01 mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility or fines and imprisonment for Knowing violations.
Penny C. Mahoney- Director of Sustainability and Operations Supp < J l
Permittee(or Authorized Agent)Name and Title-Please print or type . Signature o>f 'rmittee(or A 'orized Agent / Date)
GW-59 Rev.1/2007

Environmental Chemists, Inc.
envirochem"'<< 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.47 3.5702 Lab/Fax .
av 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info,menvironmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53379 Site:2A 12/2/2021 11:46 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Magnesium EPA 200.7,Rev4.4,1994 3.16 mg/L 12/10/2021
Nickel EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Zinc EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Arsenic EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Cadmium EPA 200.8,Rev.5.4,1994 <0.001 mg/L 12/08/2021
Mercury EPA 245.1,Rev.3.0,1994 <0.0002 mg/L 12/10/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.4 mg/L 12/08/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 273 mg/L 12/03/2021
pH SM 4500 H B-2011 6.8 units 12/07/2021
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 12/09/2021
1,'1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,1-Trichloroethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichioroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichloroethene Stv18200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dich loropropene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
., ...- a t._z_ _ . . .b4L.._c_,... �. �_ �. _.,_ r.a�._� ......�u-,.. ,.m�
n_--.+u.. nnn, n•an-, Paola 1 ni 1n

Environmental Chemists, Inc.
envirocheni 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax .
eM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info a environmentalchemists.com
DAK Americas Revised Report: Jan 03. 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer 10: 08100044
Project ID: LLC-Cape Fear Manufacturing
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Benzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromobenzene sM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromochioromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromodichioromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chlorobenzene sM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroethane sM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,3-Dichloropropene sM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dichlorodifluoromethane SM 6200 0-2011 <0.5 pg/L 12/03/2021
Ethylbenzene SM 6200 B-2011 <0.5 pglL 12/03/2021
Pans.9 of 10

Environmental Chemists, Inc. .
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sM •
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infosa environmentalchemists.com
OAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 12/03/2021
lsopropylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 12/03/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Propyibenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 12/03/2021
p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
sec-Butylbenzene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Styrene SM 6200 B-2011 <0.5 pg/L 12/03/2021
tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Tetrachloroethene SM 6200 8.2011 <0.5 pg/L 12/03/2021
Toluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,3-dichloropropene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trichlorofluoromethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloride SM4500 CI E-2011 9 mg/L 12/03/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 12/02/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.22 mg/L 12/07/2021
Nitrate Nitrogen Subtraction Method 0.22 mg/L 12/13/2021
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
21-53379A Site: 2A 12/2/2021 11:46 AMNI Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5.4,1994 0.002 mg/L 12/08/2021_

15,-:ate=,a-o, ENVIRONMENTAL CHEMISTS, INC 910.392.0223 252.473.5702
Analytical&Consulting Chemists
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: DAK Americas PROJECT NAME: LLC -Cape Fear Manufacturing REPORT NO:c,/i— aj,30
ADDRESS: 1 L/3c./ (.,.x ii ii r,,J-ea I Hu Dr. CONTACT NAME:
.,awry �.Gu_�:,i Work Order NO:
5�-f � 3 a5 REPORT TO: / ` �..f �
.
(� PHONE/FAX: ��/D�,, ��fS ,f
�/iYle`/1 +�- ��� a?89 � COPY TO: ern ail•
Sampled By:+ r ,.4i eAs fi/H /,, c; snq.;n.1? , SAMPLE TYPE:I=influent, E=Effluent,W=Well,ST=Stream,SO=Soil, SL=Sludge, Other:
ollection
PRESERVATION
1 . o .c, . e = FJ W
Sample Identification E o I ANALYSIS REQUESTED
- i "5 p a. E W 5- g J Q I g z 2 w
Dat Time Temp Cl) ~ v v 0. u E z z = 2 = z ~ o
Mw# " A 1 / l //•5. C� C � _
`'. _ 19 $ `l G `d, DJ X �] -f Chloride, Nitrite, TDS
e
,r li, `-6 4 1 C ;�) <.k •:i u
Depth to Water: . :;,o G X Ammonia, Nitrate, TP
! //; v )
C (-) I
Gallons Bailed: I [- _ G X As,Cd,Cr,Co,Cu,Pb,Mg,Ni,Se,Zn,Hg
c !!! C P I
pH (field): /p . `v I
! G G
i C P •
Lc? :�
Color: e)eQ // uG, 9 ;LG' IG," ! X VDUs (December Only)
ft/ _ C P
Odor: J'Y O G G
C P
G G
C P
G G
.
C P
G G i
Transfer Relinquished By: Date/Time Received By: Date/Time
2.
Temperature when Received °C: e, 'ted -' !-- R9iected: Resample eq ested:
Delivered By: '-I.9• Received By: i A-0--1
� Date: Time:
Comments: pti- petli 1: :jO p , to , c5,j -/- 11.'53 /-mp /9/. TURNAROUND:

Environmental Chemists, Inc. .
envirochem 6602 Windmill Way,Wilmington,NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sin 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info aenvironmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53389 Site:2E 12/2/2021 12:26 PM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Magnesium EPA 200.7,Rev 4.4,1994 1.27 mg/L 12/10/2021
Nickel EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Zinc EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Arsenic EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Cadmium EPA 200.8,Rev.5.4,1994 <0.001 mg/L 12/08/2021
Mercury EPA 245.1,Rev.3.0,1994 <0.0002 mg/L 12/10/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 8.4 mg/L 12/08/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 92 mg/L 12/03/2021
pH SM 4500 H B-2011 6.6 units 12/07/2021
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 12/09/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,1-Trichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichioroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trimethylbenzene Srvi 6200 B-2011 <0.5 pg/L 12/03/2021

Environmental Chemists, Inc.
envirocheni. 6602 Windmill Way,Wilmington,NC 28405 it 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sM •
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info aenvironmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroethane SM 5200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pglL 12/03/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Benzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromobenzene SM 6200 0-2011 <0.5 pg/L 12/03/2021
Bromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromodichloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chioromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dichlorodifluoromethane St i 6200 B-2011 <0.5 pg/L 12/03/2021
Ethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021

Environmental Chemists, Inc. -
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
:sn+ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info:a environmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 12/03/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Naphthalene SM 6200 8-2011 <0.5 pg/L 12/03/2021
n-Butylbenzene SM 6200 8-2011 <0.5 pg/L 12/03/2021
n-Propylbenzene SM 6200 8-2011 <0.5 pg/L 12/03/2021
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 12/03/2021
p-lsopropyltoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
sec-Butylbenzene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Styrene SM 6200 B-2011 <0.5 pg/L 12/03/2021
tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Tetrachioroethene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Toluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,3-dichloropropene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Trichloroethene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Trichlorofluoromethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloride sM4500 CI E-2011 6 mg/L 12/03/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.07 mg/L 12/02/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.31 mg/L 12/07/2021
Nitrate Nitrogen Subtraction Method 0.24 mg/L 12/13/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53389A Site: 2E 12/2/2021 12:26 PM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5.4,1994 0.004 mg/L 12/08/2021
,- , .. ..... ,....,.- Pon R of 11

' " pox,,,, ENVIRONMENTAL CHEMISTS, INC
910.392.0223 252.473.5702
Analytical&Consulting Chemists
NCDENR:DWQ CERTIFICATION#94;!CORNS:DLS CERTIFICATION#37729
[e-mail]
COLLECTION AND CHAIN OF CUSTODY
PROJECTCLIENT: DAK Americas REPORT NO:. / - c�{,3O"�
• • .Sampled By.1111111111111111
S SAMPLE TYPE: 1 =Influent, E=Effluent,W=Weil,ST=Stream, SO=Soil,SL=Sludge,Other:
ction 2
N PRESERVATION
Sample Identification E F a'8 a o �, m n
Q (. o o a o W ANALYSIS REQUESTED
Date Time Temp (n U U a v J z z I i = = Z M o
MW# E is-1 pia, G f°'''• -` �3
e X �}-¢� Chloride, Nitrite, TDS
/ 'A C (_P" ,4A.,(1
Depth to Water: 7 f Cc fG M. X Ammonia, Nitrate, TP
/41 /3? C 1 .6,L)
Gallons Bailed: G
+ (, .� i _ a X As,Cd,Cr,Co,Cu,Pb,Mg,Ni,Se,Zn,Hg
�- t C P t
pH (field): u� , t�'� d
+ G G J !�
Color: �e;;! r 1 , G) l`! ''"-•�..+'
X VOC's (December Only)
C P —
Odor. A",J G G
-
C G - 1
_ C P
G G
C P
G G
Transfer Relinquished By: __ Date/Time Received By: Date/Time
1. �^ �'" 4) /33V 1
2.
Temperature whe 'tar.ived °C: .ccepted: ,--' •ected: Resarnr le Requested:
Delivered a , Received By: Date: f %1-1 Time: _
Comments: . �' ate_ Jt.... ■e (1 , O.�"' • , ? 0 /:� ..- TURNAROUND:

Environmental Chemists, Inc. .
envirocheni 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
'M •
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53390 Site: 3A 12/2/2021 11:11 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 0.010 mg/L 12/10/2021
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Magnesium EPA 200.7,Rev 4.4,1994 1.000 mg/L 12/10/2021
Nickel EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Zinc EPA 200.7,Rev 4.4,1994 0.015 mg/L '12/10/2021
Arsenic EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Cadmium EPA 200.8,Rev.5.4,1994 <0.001 mg/L 12/08/2021
Mercury EPA 245.1,Rev.3.0,1994 <0.0002 mg/L 12/10/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.2 mg/L 12/08/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 107 mg/L 12/03/2021
pH SM 4500 H B-2011 6.2 units 12/07/2021
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 < 0.04 mg/L 12/09/2021
1,1,1,2-Tetrachloroethane SM 8200 B-2011 <0.5 pg/L 12/03/2021
1,1,1-Trichloroethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,2-Trichloroethane SM 6200 0-2011 <0.5 pg/L 12/03/2021
1,1-Dichioroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichlorobenzene SM 6200 8-2011 <0.51.ig/L 12/03/2021
1,2,3-Trichloropropane SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,2,4-Trichlorobenzene SMi 6200 8-2011 <0.5 pg/L 12/03/2021
1,2,4-Trimethylbenzene SM 6200 8-2011 <0.5 lJg/L 12/03/2021

Environmental Chemists, Inc. -
envirocheni 6602 Windmill Way,Wilmington,NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax •
sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910 347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info:i=environmentalchemists.com
OAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichioropropane SM 6200 B-2011 <0.5 pg/L 12/03/202'1
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dich loropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
2,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 12/03/2021
2-Chiorotoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
4-Chlorotoluene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Benzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 12/03/202'1
Bromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromodichloromethane SM 6200 B-2011 <0.5 pg/L '12/03/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroform Sivl 6200 B-2011 <0.5 pg/L 12/03/2021
Chioromethane SM 6200 B-2011 <0.5 pg/L '12/03/2021
cis-1,2-Dichioroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,3-Dich loropropene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromochloromethane sM6200 B-2011 <0.5 pg/L 12/03/2021
Dibromomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dichlorodifluoromethane SM 6200 8-2011 <0.5 pg/L 12/03/202'1
Ethylbenzene sM6200 8-2011 <0.5 pg/L 12/03/2021

Environmental Chemists, Inc. •
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
stir 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(i environmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 12/03/2021
lsopropylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 12/03/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg1L 12/03/2021
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 12/03/2021
p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Styrene SM 6200 B-2011 <0.5 pg/L 12/03/2021
tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Toluene SM 8200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,3-dichioropropene S1416200 B-2011 <0.5 pg/L 12/03/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloride SM4500 CI E-2011 7 mg/L 12/03/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev 2 0,1993 0.03 mg/L 12/02/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.07 mg/L 12/07/2021
Nitrate Nitrogen Subtraction Method 0.04 mg/L 12/13/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53390A Site: 3A 12/2/2021 11:11 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5.4,1994 <0.001 mg/L 12/08/2021

Environmental Chemists, Inc.
envirochem l 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax •
sr+ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info'a environmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
Comment: Amended 01/03/2022 to amend Cobalt results
.Reviewed by:

(71...._,L7.-fr_2„-T,.4"70-;-.1 ENVIRONMENTAL CHEMISTS, INC 910.392.0223 252.473.5702
Analytical&Consulting Chemists
NCDENR:DWQ CERTIFICATION#94 NCDHF{S:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: DAK Americas PROJECT NAME: LLC-Cape Fear Manufacturing REPORT NO: l^a/30
7
ADDRESS: ')3(,) Z.,ofyvyj0,i bo 1lij1 i ;' CONTACT NAME: gr.‘4
;J, / �2. r �'� ,�.r7y Work Order NO:
SR., f e- -5 c REPORT TO: '� L; > s C.1 r
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Sampled By: z ./, 5,,,0,E ,;s SAMPLE TYPE: I=Influent, E Effluent,W=Well, ST=Stream,SO=Soil,SL=Sludge,Other:
i y
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PRESERVATION
Sample Identification a s o - " ` = o m ii
ro ti (Ti c ° ° °i �'0 •g z -. I 'o 0 0 o uT,, ANALYSIS REQUESTED
Date Time Temp in
0 0. o e g D 0 = • _ = i o
fi G ,1A,53317) X '-Pi Chloride, Nitrite, TDS
!/;Q ;r!_ ,J I
Depth to Water: 5• 7 / ,{� ° '
5. � G X I Ammonia, Nitrate, TP
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Gallons Bailed: s
�'� _ / . J G \ X As,Cd,Cr,Co,Cu,Pb,Mg,Ni,Se,Zn,Hg
pH (field): 5, I s t +�d G G
,� i I/'( 1 C P I , .� _
Color: L•1et r I /L1 ��•
I . , L� �G� _ ' _ X VOC's (December Only)
C P
Odor: ,f\/ G G
C P
G G
C P
G G
C P
G G I
Transfer Relinquished By: Date/Time Received By: Date/Time
I. fay— — /Ai '
2. / �, .-/
Temperature whe eceived °C: �', epted: Rejected: Resam le 1 p_ Pfteq ested:
Delivered By:---�' -" ., Received By: _ Date: I d-(`1`1est Time:
Comments: • C• - T LI i ?,_• TURNAROUND: