WQ0006101_Permit Application_20101220

SSYNAGRO
A Residuals Management Company
s
December 20, 2010
N.C. Department of Environment and Natural Resources
Division of Water Quality •
Land Application Permitting and Compliance Unit
Aquifer Protection Section
1636 Mail Service Center -
-Raleigh, NC 27699-1636
ATTENTION: Mr. Jon Risgaard -
VsECED
10.ER F11p EC 1 t01-1 SEC.
-I O: QEC 2.2 0«° 4 2 -
REFERENCE: APPLICATION FOR MODIFICATION OF PERMIT # WQ0006101:
CITY OF DUNN
Dear Mr. Risgaard:
On behalf of the City of Dunn, Synagro Central, LLC is submitting this application to modify the
referenced residuals land application permit. There is no check enclosed with this application. It
is my understanding, from an email written by Ed Hardy (copy follows this page), that no fee is
necessary for a modification of this sort.
This application for modification is limited to increasing the permitted dry tonnage of one of the
sources for this permit. No other changes are requested at this time.
This application package is believed to contain all of the information necessary to complete the
requested modification of the City of Dunn's permit. However, if you require additional
information or have further questions about the included information, please contact me at
"[e-mail]" or by phone at 336-971-9085. Thank you in advance for the timely
and efficient review of this application. -
Sincerely,
iEic N. Thompson
Soil Scientist/Technical Services Manager
cc: Ronald D. Autry, City Manager, City of Dunn
284 Boger Road • Mocksville, NC 27028-7619 • Ph: [phone] • Fax: [phone] • Toll Free: [phone]

Thompson, Eric
fit. ''m:
Cc:
Subject:
Hardee, Ed [[e-mail]]
Tuesday, December 14, 2010 08 27
Thompson, Eric
Barber, Jim
RE: Land application activities for Permit #WQ0OO61O1 (City of Dunn)
Eric,
We do not usually grant permission to exceed permit limits for dry tonnage except in
cases where a facility maybe closing out and only after a review of each -individual case.
Your option at this time is to submit a modification to increase the permitted dry tonnage
for this source. This should be a minor modification, with no fee, to adjust residual
volume without changing of treatment capacity or expansion•.
Ed Hardee
Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Phone (919j 715-6189
Fax [phone]
DISCLAIMER: Per Executive Order No. 150, all e-mails sent to and from
this account are subject to the North Carolina Public Records Law and
.may be disclosed to third -parties.
Original Message
From: Thompson, Eric [mailto:[e-mail]]
Sent: Monday, -December 13, 2010 2:27 PM
- Hardee, Ed
Puryear, Marshall
`-_.,^.Sject: Land application activities for Permit #WQ0006101 ,(City of Dunn)
Mr. -Hardee:
Based on early calculations of our most recent event, i.t appears that we
may have exceeded the permitted dry tonnage for the secbnd source (as
listed on the "Attachment A") for Permit #WQ0006101. Specifically, the
permit lists the permitted dry tonnage for the City of Dunn's WWTP as
206. From the data I have at this time (our monitoring section will
have more definitive numbers), it appears that we have land applied just
under 230 dry tons from that source in 2010.
This 'late in
increase the
modification
Or, is there
were able to
tonnage.
the year, we can still submit a permit modification to
permitted dry tonnage. However, it is not likely that the
would be approved before the end of the' year.
another procedure?, One of the guys in the office said you
write a letter for a project exceeding their permitted dry
Also, for your information: there is some construction going on at the
City of Dunn's WWTP. Also, if necessary, we can send a permit
modification in as soon as possible or early next year.
Thank you for any information,
Eric Thompson
. Soil Scientist/Technical Services Manager
`iagro Central, Mocksville, NC
971-9085
1

YNAGRQ.
A Residuals Management Company
APPLICATION FOR MODIFICATION OF
PERMIT NUMBER WQ0006101
RESIDUALS LAND APPLICATION PROGRAM
CITY OF DUNN
DUNN, NORTH CAROLINA
A better tomorrow for our Client Triangle: The GENERATOR, The LANDOWNER, and The ENVIRONMENT
Prepared by:
SYNAGRO CENTRAL, LLC
284 Boger Road
Mocksville, NC 27028
Toll Free: [phone]
Fax: [phone]
December 2010

Table of Contents
Section # - Title
Section 1 Attachment Order 1: Non -Dedicated Residuals Land Application Programs Form
Section 2 Attachment Order 2: Residuals Source Certification Attachment
Attachment Order 2: Residuals Source Certification Attachment
Attachment Order 2-a: Vicinity Map
Attachment Order 2=b: Process Flow Diagram
Attachment Order 2-c: Quantitative Justification for Residuals Production
Attachment Order 2-d: , Sampling Plan
Attachment Order 2-e: Laboratory Analytical Reports and Operational Data

Attachment Order 1:
Non -Dedicated Residuals Land Application Programs Form

State of North Carolina
Department of Environment and Natural Resou c S� irpO /trt'.PYR/(�.►t`10
P Division of Water Quality ` ` 'ROT'EC T i0p,a SEC.
NON -DEDICATED RESIDUALS LAND APPLICATION CCI MS 10; 42
(FORM: NDRLAP 070807)
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
Application Number: (to be completed by DWQ)
I. OWNERSHIP INFORMATION:
1. Specify whether the process facility is owned by:
❑ County; ❑ Federal; ® Municipal; ❑ State; ❑ Non -Government.
2. Owner's name (please specify the name of the municipality, corporation, individual, etc.)
City of Dunn
Mailing address: Post Office Box 1065
City: Dunn
State: North Carolina Zip: 28355
Physical address: 401 East Broad Street
City: Dunn
State: North Carolina Zip: _28355
Telephone number: ( 910_ ) _230-3500 Facsimile number: (_910) 230-3590
E-mail address:
3. Signing official's name and title: (See Instruction A)
Ronald D Autry, City Manager
Mailing address: _ Post Office Box 1065
City: Dunn State: North Carolina
Physical address: 401 East Broad Street
City: Dunn
Zip: _28355
State: North Carolina Zip: _28355
Telephone number: ( 910 ) _230-3500 Facsimile number: ( 910 ) _230-3590
E-mail address: rautry(a,dunn-nc.org
II. PERMIT INFORMATION:
1. Application is for: ❑ new,
2. Fee Submitted: $
® modified, ❑
renewed permit (check all that apply).
0.00 (See Instruction B)
3. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number WQ0006101
Most recent issuance date 10/10/07 , and the expiration date 9/30/12
Date of most -recently certified Attachment A: 10/10/07
Date of most -recently certified Attachment B: 10/24/07
FORM: NDRLAP 070807 Page 2 of 6 Attachment Order 1

4. Check all that apply to the requested permit modification:
INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for existing residuals
source -generating facility(ies) certified.
❑ ADD ❑ DELETE residuals source -generating facility(ies) to/from those certified.
❑ INCREASE ❑ DECREASE the acreage associated with land applications site(s).
❑ ADD ❑ DELETE land application site(s) to/from those certified.
❑ OTHER. Explain:
III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. County where residual's land application program is headquartered: Harnett
2 County(ies) where residuals source -generating facilities are located: Harnett
3. County(ies) where land application sites are located: Harnett, Cumberland,
Sampson
4. Program contact person and/or consulting firm who prepared application: -
Eric Thompson_
Mailing address: 284 Boger Road
City: Mocksville State: NC Zip: 27028 -
Mailing address: 284 Boger Road
City: Mocksville State: NC Zip: 27028 _
Telephone number: ( 336 ) _998-7150 x 12 _ Facsimile number: ( 336 ) 998-8450
E-mailaddress:_ethompson(a�synagro. com
5. Who will be responsible for the day-to-day management of the residuals landapplication program:
❑ Permittee or ® residuals management firm. If a residuals management firm, complete the following:.
Firm contact person and title: Froncy Dail, Senior Operations Manager
Firm name: Synagro Central, LLC
Mailing address: 284 Boger Road
City: Mocksville ' State: NC
Zip: 27028
Telephone number: ( 910 ) _341-7542 Facsimile number: ( 336 ) 998-8450.
E-mail address: fdail(a,synagro.com

6. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application
program, their certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification
Number
ORC .
Rudolph Collins
Synagro
LA 19611
Back -Up ORC
Billy Addison
City of Dunn
LA 987525
Additional Back -Up ORCs
(if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this' residuals land application
program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's
completion of the required training school and certification test:
7. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated
by all residuals source -generating facilities as currently certified and proposed for certification with this
application and list the results in the following table:
Maximum amount of residuals to be certified: 650
dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
49.88
63.58
14,963
19,073
Five -Year Maximum Adjusted
73.36
87.06
22,009
26,119
b. Land Application Site Use Summary: Summarize information regarding the land application sites as
currently certified and proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
0
Row Crops`
206.1
Hay ,
204.8
Pasture
0
Total:
410.9
Methods
Surface
204.8
Incorporation or Injection
206.1
Total:
410.9
Restrictions
Year -Round
410.9
Seasonal
0
(2T permit)
Total:
410.9

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the
residuals as currently certified and proposed for certification assuming the scenarios listed in the
following table:
Assumed
Application Rate
(lbs PAN/ac-yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface. _
Incorporation or
Injection
50
299.3
381.5
440.2
522.4
100 .
149:6
190.7 .
220.1
261.2
150 .
99.8
127.2
. 146.7
174.1
200
74.8
95.4
110.0
130.6
8. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application
of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage,
not enough land, vector reduction practices not in place, etc.)
***FORM: NDRLAP CONTINUES ON NEXT PAGE***

12-20-'0;04:1ePN;City Manager
DEC-20-2010 12:20 From:
;910-230-3590
To:910 230 3590
# 2/
P.2/2
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime,
- facility without proper -closure; does not have an outstanding civil penalty,, where
abandoned, are compliant with any active compliance schedule, and do not have
2T .0105;
® Yes • ❑ No, Explain;
ARECEIVEO/OENR1D WO
QUIFER PROTECTION SFr.
10DEC22 ntit: 43
has not abandoned a wastcwater .
all appeals have been exhausted or
any overdue 'annual fees under Rule
Rnnald ll. Autry , attest that this application for modification o'fpcnnit number
W00006i01 has been
reviewed by me and is accurate and complete to the hest of my knowledge. 1 understand that the Division of Water
Qualify may not conduct a technical review of this program and approval does not constitute a variance to any rules
or statutes tulles speciBcally granted in the permit. Further, any discharge of residuals to surface waters or the land
will result it1 an immediate enforcen.teut action, which may include civil penalties, injunctive relief; and/or criminal
prosecution. I will make no claim against the Divisions of Water Quality should a condition of this permit be
violated. I also tmderstand that if all required parts of this application are not completed and that if all required
supporting information and attatlimcnt are not included, this applicatiun package will he returned to me as
incomplete: Note: in accordance with North Carolina General Statutes § I43-215.6A and §143-215.6B, any person
who knowingly snakes any false statement. represcntation, or certification in any application shall be guilty of a Class
2 misdemeanor, which may include a line not to exceed $10,000 as well as civil penalties up to $25,000 per
violation.
Signature:
Date: /..2- ` O —V D
THE' COMPLETED) APPLICATION PACKAGE,.
INCLUDING ALI..SUI'YORTING INFORMATION AND MATERIALS,
MOULD BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
AQUIFER PROTECTION SECTION
LAND APPLICATION UNIT
Fly U.S. Postal Service: By Courier/Special Delivery:
1636 MAIL SERVICE CENTER 2728 CAPITAL BOULEVARD
RAI.T;IGH, NORTH CAROLINA 27699-1636 RALEIGH, NORTH CAROLINA 27604
TELEPHONE NUMBER: [phone]

Attachment Order 2:
Residuals Source Certification Attachment

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 070807)
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
Applicant's name: City Of Dunn
Check all that apply: ❑ NEW RESIDUALS PROGRAM ❑ RENEWED RESIDUALS PROGRAM
® INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for this residuals source -
generating facility certified for this residuals program.
Current: 206 Dry Tons/yr. and proposed: 300 Dry Tons/yr.
❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for this
residuals program.
❑ OTHER Explain:
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Name of facility: Dunn WWTP
2. Facility permit holder: City of Dunn
Facility permit holder is (check one): ❑ federal, ❑ state, ® local government, or ❑ private.
Facility permit number: NC0043176
Facility permit issued by (check one): ® Div. of Water Quality, ❑ Div. of Environmental Health, or
❑ other (explain: ).
3. If the facility permit is not issued by the Div. of Water Quality, complete the following:
4. Facility contact person and title:
Facility complete mailing address:
City: State: Zip:
Telephone number: ( ) Facsimile number: (
E-mail address:
b. Facility complete location address:
City: State: Zip:
Latitude: and longitude:
County where facility is located: Harnett
6. Purpose of the facility (check one):
® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater, or
(approximate percentages: % industrial and % domestic)
❑ other (explain:
FORM: RSCA 070807
Page 2 of 8 Attachment Order 2

7. Does the facility have an approved pretreatment program: ® yes ❑ no
8. Facility permitted/design flow: 3.75 MGD and facility average daily flow: 2.0 MGD.
9. Averageamount of residuals being generated at this facility
210.4 dry tons per year.
10. Specify the following regarding treatment and storage volumes. available at the facility:
Type and volume of residuals treatment: aerobic digester: 600,000 gallons
Type and volume of residuals storage. (i.e., outside of residuals treatment units): two storage lagoons:
one 3.0 million gallons plus one 1.0 million gallons
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under (check one): ® 40 CFR Part503 or ❑ 40 CFR Part 257.
2. Specify if residuals are intended for (check one):
❑ Land Application/Distribution (Class A or Equivalent).
Complete all items EXCEPT Items II. 4b., 7b., and 7c.
Land Application (Class B or Equivalent).
Complete all items EXCEPT Items II. 4b., 7a., and 7c.
❑ Surface Disposal.
Complete all items EXCEPT Items II. 4a., 5., 7a., 7b., and 8.
***FORM: RSCA CONTINUES ON NEXT PAGE***
FORM: RSCA 070807
Page 3 of 8 Attachment Order 2

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-
hazardous under RCRA:
a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
§261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity
characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and
reactivity: laboratory: Summit Environmental Tech. Inc and date of analysis: 01/21/10
Passed corrosivity test: ® yes ❑ no. pH: 5.98 s.u. (2 < pH < 12.5).
Passed ignitability test: ® yes ❑ no. Flashpoint: >140 °F (> 140°F).
Passed reactivity test: ® yes ❑ no. HCN: <0.5_ mg/kg (<250) & H2S: _<25.0 nig/kg (<500).
TCLP Parameter
Limit
(mg/L)
Result
(mg/L)
TCLP Parameter
Limit
(mg/L)
Result
(mg/L)
Arsenic
5.0
<0.5
Hexachlorobenzerie
0.13
<0.1
Barium
100.0
<5.0
Hexachloro-1,3-Butadiene
0.5
<0.1
Benzene
0.5
<0.1 .
Hexachloroethane
3.0
<0.1
Cadmium
1.0 '
<0.1 ,
Lead
5.0
• <0.5 -
Carbon Tetrachloride
0.5
<0.1
Lindane
0.4
<0.002
Chlordane .
0.03
.. <0.01
Mercury
0.2 -
<0.002
Chlorobenzene
100.0
<0.1
Methoxychlor
10.0
<0.002
Chloroform
6.0
<0.1
Methyl Ethyl Ketone
200.0
<2.0
Chromium
5.0
<0.2
Nitrobenzene
2.0
<0.1
m-Cresol
200.0 .
<5.0
Pentachlorophenol
100:0
<0.25
o-Cresol
200.0
<5.0
Pyridine
5.0
- <0.25
p-Cresol
200.0
<5.0.
Selenium
1.0
<0.5
Cresol
200.0
. <5.0
Silver
5.0
<0.5
2,4-D
10.0
<5.0
Tetrachloroethylene
0.7
<0.1
1,4-Dichlorobenzene
7.5
<0.1-
.Toxaphene _
0.5
' <0.1
1,2-Dichloroethane
0.5
<0.1
Trichloroethylene
0.5
- <0.1
1,1-Dichloroethylene
0.7
<0.1
2,4,5-Trichlorophenol
400.0
<0.25
2,4-Dinitrotoluene
0.13
<0.1
2,4,6-Trichlorophenol
2.0.
<0.25
Endrin
0.02
<0.002
2,4,5-TP (Silvex)
1.0
<0.25
Heptachlor and its Hydroxide
0.008 '
<0.002
• Vinyl Chloride
0.2
<0.2
FORM: RSCA 070807
Page 4 of 8
Attachment Order 2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the
residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Class A or Class B: Fill in the following table with the results of the latest analyses (i.e., on a dry
weight basis) for the following metal parameters:
Laboratory: _A&L Eastern Labs
and date of analysis: _O1/18/10
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg).
Monthly Average
Concentration Limits
.. (For Class A Only)
(mg/kg)
Result
•
(mg/kg)
Arsenic
75
41
5.7
Cadmium
85
. 39
1.2
Copper .
4,300.
1,500
220
Lead
840
300
30
Mercury
57
17
1.4
Molybdenum
75
n/a
10
Nickel
420
420
24
Selenium
100
100
1.3
Zinc
7,500
2,800
357
b. For Surface Disposal: Fill in the following table with the results of the latest analyses (i.e., ona dry
weight basis) for the following metal parameters:
Laboratory: and date of analysis:
Closest Distance
to Property Lines
(meters)
Arsenic
(mg/1(g)
Chromium ' .
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
>25but <50
'. 34
220
240
> 50 but < 75
39
260
270 .
> 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125 but < 150
62
450
420
> 150
73
600
420
FORM: RSCA 070807
Page 5 of 8
Attachment Order 2

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 2.84 %.
b. Fill in the following table' with the results of the latest analyses (i.e., on a dry weight basis) for the
following nutrient and micronutrient parameters: laboratory: A&L Eastern Labs
and date of analysis: 01/18/10
Parameter
Result
(mg/kg, dry weight)
Aluminum
17400
Ammonia -Nitrogen
13700
Calcium
8100
Magnesium
3200
Nitrate -Nitrite Nitrogen
28.2
pH (Standard Unit)
6.53
. Phosphorus
20100
Potassium
6000
Sodium
1950
Total Kjeldahl Nitrogen
73900
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.78 .
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the
residuals: 30 %. This rate is a ® default value or D actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or
provide technical justification as to why the selected default value is appropriate to be applied to these
residuals:
Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following table:
Application Method
First Year
. PAN
(mg/kg)
Five -Year
Maximum Adjusted
PAN
(mg/kg)
Surface
24,938
36,682
Injection/Incorporation
31,788
43,532
e. Are the residuals a registered fertilizer with the NC Department of Agriculture and Consumer Services:
❑ yes ® no. If yes, provide date of registration approval:
the current registration number:
and the fertilizer equivalent: %, %, and %.
FORM: RSCA 070807 Page 6 of 8
Attachment Order 2

3
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the
residuals and list the results of the latest analyses:
7. Pathogen Reduction Determination: Specify which alternative(s) will be used to meet the pathogen reduction
requirements:
a. For Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids.
OR
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed):
❑ Alternative 1 [40 CFR §503.32 (a)(3)] - Time/Temperature Compliance.
❑ Alternative 2 [40 CFR §50332.(a)(4)] - Alkaline Treatment.
❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [40 CFR §50332 (a)(6)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation.
❑ Alternative 6 [40 CFR §50332-(a)(8)] - PFRP-Equivalent Process.
Explain:
b. For Class B or Equivalent:
❑ Alternative 1 [40 CFR §503.32 (b)(2)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [40 CFR §50332 (b)(3)] - Process to Significantly Reduce Pathogens (PFRP)
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
❑ Alternative 3 [40 CFR §50332 (b)(4)] - PSRP-Equivalent Process.
Explain:
❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
c. For Surface Disposal:
❑ Alternative for Surface Disposal Units Only [40 CFR §50333 (b)(11)] - Soil/Other Material Cover.
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
FORM: RSCA 070807
Page 7 of 8 Attachment Order 2

8: Vector Attraction Reduction Determination: Specify which alternative(s) will be used to meet the vector attraction
reduction requirements:
El Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ _Alternative 2 [40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
® Alternative 3 [40 CFR §503.33. (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
® Alternative 4 [40 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [40 CFR. §503.33 (b)(5)] - 14-Day Aerobic Processes.
• Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization.
❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals.
El Alternative 8 [40 CFR §503.33 (b)(8)] - Drying of Unstabilized Residuals.
® Alternative 9 [40.-CFR §503.33 (b)(9)] - Injection.
® Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
El Alternatives for Animal Processing Residuals Only:
Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10.
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
FORM: RSCA 070807
Page 8 of 8 Attachment Order 2

Attachment Order 2-a:
Vicinity Map

SYNAGRO
VICINITY MAP
COUNTY Qrneff—
A Residuals Management Company
OWNER 61-‘,/4 U WIT

Attachment Order 2-b:
Process Flow Diagram

To:9108928871
-
LAB.
AOMINITRATION
BUILDING
GRIT
REMOVAL!
BLOViER
BUILDING .
•
BLOWER
9UILO ING
U
J.
AER*T1
BASIN
AEROBI C
DIGESTER
TH I C14QJ EF
BUI LONG
CITY OF DUNN
BLACK RIVER WASTEWATER TREATMENT PLANT
is:e',.+•!-114tt i 744.'
FFL`JEt
PUMP S'
CHLORW£•• ' I 1
CHLCR':NE 1
CO1NTACT.'
BASIN
FUTURE
C_ARIFIE R
NO. 4

Attachment Order 2-c:
Quantitative Justification for Residuals Production

Quantitative Justification for Residuals Production Rate
Facility:
City of Dunn WWTP and City of Dunn WTP
Requested Permitted Rate:
300 dt/yr WWTP 350 dt/yr WTP
Justification:
The City of Dunn currently produces roughly 300 dry tons of biosolids, based on the
calculations below and an assumption of2,84% solids at its WWTP. The City of Dunn
also produces roughly 292 dt/yr of alum residuals, based on the calculations below and an
assumption of 3.5% solids at its WTP
Calculations:
Based on the concept that average daily flow is approximate to annual volume of
residuals produced:
City of Dunn WWTP
(2,450,000ga1/yr)•x (2.84% solids) x (8.5 lbs/gal) = 296 dt/yr
(2,0001bs/ton)
City of Dunn WTP
(1,964,000 gal/yr) x (3.5 % solids) x (8.5 lbs/gal) = 292dt/yr
(2,000 lbs/ton)

Attachment Order 2-d:
Sampling Plan

Residuals Sampling Plan
City of Dunn Land Application Program
Wastewater Treatment Plant
Nutrients and Metals Analysis
Sampling Point: Digester
Sampling Frequency: Yearly
Sample Type: Composite
Lab: A&L Eastern Laboratories, Inc.
Pathogen Reduction
Sampling Point: Digester
Sampling Frequency: Yearly
r Sample Type: Grab
Lab: Cameron Testing Services, Inc.
Vector. Attraction Reduction
Sampling Point: Digester
Sampling Frequency: Yearly.
Sample Type: Composite
Lab: Cameron Testing Services, Inc..
TCLP
Sampling 'Point: Digester
Sampling Frequency: Annually
Sample Type: Composite
Lab: Summit Environmental Technologies, Inc

Attachment Order 2-e:
Laboratory Analytical Reports and Operational Data

Report Number:
Account Number:
Submitted By:
Page: 1 of 2
10-015-0206
46789
JAMES R BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DUNN
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number : 74445
Sample Id : DUNN WWTP
Total Solids *
Moisture *
Total Kjeldahl Nitrogen
Total Phosphorus
Total Potassium
Total Sulfur
Total Calcium
Total Magnesium
Total Sodium
Total Iron
Total Aluminum
Total Manganese
Total Copper
Total Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
Total Cadmium
2.84
97.16
7.39
2.01
0.60
0.74
0.81
0.32
0
v w.al-labs-easterh,corn
L astern Laboratories, Inc.
7821 Whitepine Road Rictiinond, ltirginia'23237 :[phone] fax [phone]
Project : PO#50-2188
NC CERT#257
REPORT OF ANALYSIS
28400
73900
20100
6000
7400
8100
3200
0.20 1950
16100
17400
170
220 _
357
1.37 13700
6.02 60200
28.2'
1.2
Date Sampled: 1 /13/2010 14:00:00
Date Received: 01/15/2010 00:00
Date Reported: 01/21/2010
ANALYSIS'
DATEIT,tME;;°°
100.0 MW 01/18/2010 07:59
100.0 MW 01/18/2010 07:59
0 MW 01/18/2010 08:24
100 KM 01/18/2010 08:30
100 KM 01/18/2010 08:30
100 KM 01/18/2010 08:30
100 KM 01/18/2010 08:30
100 KM 01/18/2010 08:30
100 KM 01/18/2010 08:30
1 KM 01/18/2010 08:30
10 KM 01/18/2010 08:30
1 KM 01/18/2010 08:30
1 KM 01/18/2010 08:30
1 KM 01/18/2010 08:30
10.0 MW • 01/18/2010 08:24
10.0 01/18/2010 08:24
1.00 TMW 01/18/2010 08:25
1.0 KM 01/18/2010 08:30
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports_and totters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
SM-2540G
81b1-2540G
SM-4500-N H 3C-TKN
SW-6010B
SW-6010B
SW-6010B
S W-6010B
SW-6010B
SW-6010B
SW-6010B
S W-6010 B
SW-6010B
SW-6010B
SW-601 OB
SM-4500-NH3C
CALCULATION
SM-4500NO3F
SW-6010B
Oscar Ruiz

Page: 2 of 2
Report Number: 10-015-0206
Account Number: 46789
Submitted By: JAMES R BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DUNN
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number : 74445
Sample Id : DUNN WWTP
Total Chromium
Total Nickel
Total Lead
Total Arsenic
Total Mercury
Total Selenium
pH (as received) *
Total Volatile Solids
Total Molybdenum
.0 iY.al.laps-eastern,cbiri
A&L Eastern Laboratories, Inc.
741 §V6it'epirid Road Rteli'mond, '0'gi8Ta 23237 :(B04) 743-9401 Fail (804) 271-64446
Project : PO#50-2188
NC CERT#257
REPORT OF ANALYSIS.
33 5
24 5
30 5
5.7 1.0
1.4 0.4
1.3 1.0
6.53 1.00
75.85 758500 100.0
10 5
KM
KM
KM
KM
km
KM
MW
MW
Date Sampled: 1/13/2010 14:00:00
Date Received: 01/15/2010 00:00
Date Reported: 01/21/2010
01/18/2010 08:30 SW-6010B
01/18/2010 08:30 SW-60108
01/18/2010 08:30 SW-6010B
01/18/2010 08:30 SW-60108
01/18/2010 10:20 SW-7471A
01/18/2010 08:30 SW-6010B
01/18/2010 08:25 SW-9045D
01/18/2010 07:59 SM-2540G
KM 01/18/2010 08:30 SW-6010B
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
• Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor rnay any reference be made "
to the work, the results, or the company in any advertising, news release, .or other public announcements without obtaining our prior written authorization.
Oscar Ruiz

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ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Approved By :
LABORATORY REPORT
Client
Synagro Southeast
284 Boger Rd.
Mocksville, NC 27028
Order Number
1000660
Project Number
Dunn VVTP WWTP
Issued
Friday, January 22, 2010
Total Number of Pages
7 (excluding C.O.C. and cooler receipt form)
QA Manager
NEAP Accreditation #E87688
"Analytical Integrity" • EPA Certified • NEAP Certified
. -.3310 Win Street • Cuyahoga Fails, Ohio 44223 -Phone:,330-•253-8211 • Fax: [phone]
Web Site: www.seitek.com

ENVIRONMENTALTECHNOLOGIES, INC.
Analytical Laboratories
Sample Summary
Client: Svnaoro Southeast
Order Number: 1000660
2
Laboratory ID
Client ID Matrix Sampling Date
1000660-01 Dunn WTP Sludge 1/13/2010
10.00660-02 Dunn WWTP Sludge 1/13/2010
• "Analytical Integrity" • EPA Certified • NELAP Certified • •
3310 Win Street • Cuyahoga Fells, Ohio 44223 Phone: [phone] • Fax: [phone]
Web Site: wvvw.settek.corn

ENVIRONMENTAL TECHNOLOGIES, INC.
naiyticai Laboratories
Report Narrative
Client: Svnagro Southeast
Order Number: 1000660
3
No problems were encountered during analysis of this order number, except as noted.
•
Data Qualifiers:
B = Analyte found in: the method blank
,J:= Estimated concentration of analyte,between MDL (LOD) and Reporting Limit (LOQ)
•0 Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract'was analyzed at a higher dilution
X.= User defined data qualifier.
S::= Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request.
The test results meet the requirements, of the NELAC standard; except where Noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. 'It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc or the client for which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different -sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data included herein.
Matrices;
A = Air
C=Cream
DW = Drinking Water
L =. Liquid
O'.=-Oil
$L: ,Sludge
SO = Soil
S = Solid
T = Tablet
TC = TCLP Extract
WW =Waste Water
W'= Wipe .
"Analytical Integrity" • EPA Certified • NELAP Certified
i+!in Street • Cuyahoga Falls, Ohio 44223 a Phone: [phone] Fax: 330-25
Web Site: www.settek.com

Client ID#
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
DunnWTP
Dunn WTP
Dunn WTP
. Client IN
Dunn WTP
Dunn:WCP
Dunn WTP.
Dunn WTP
Dunn WTP
Dunn.Wi'P
' ! `1•WTP
• WTP
Dunn WTP
Dunn WTP
J
Client.lD#
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
Dunn WTP
NVIRONMENTAL TECHNOLOGIES, INC.
inafytiCaf LY boi'4it.or es
Lab ID#
1000660:01
1000660-01
-1000660-01
1000660.01
1000660-01
1000660=01
1000660-01
1000660'-01
Lab 1D#
1000660-01
1000660-01
100066 ,01
1000660-01
1000660-01
1000660=01
1000660-01
1000660-01
1000660;01
1000660'-01
Lab. ID#.
1000660-01
1000660-01,
1000660;01
1000660-01
1000660401
100066.0-01
1000660,01
1000660-01
1000660-01
1000660-01
1000660-01
Collected Analyse
13-Jan-10 Cadmium
13-Jan-1O Chromium
13-Jan-10. Selenium
13-Jan-10 Arsenic
13-Jan-10 Lead
13-Jan-10 Silver
13-1an710 Barium.
13-Jan-10 Mercury
Collected Analyte.
13-Jan-10 Trichioroethene
13-Jan-10 2=Butanone (MEK)
13 Jan-10 Vinyl -Chloride
13-Jan-10 Chlorobenzene,
13 )an-10 ttiloroforrn
13-Jan-10 1,1-Dictiloroethene
13-Jan-10;Carbon tetrachloride
13 Jan-10:Benzene
13 Jan-10 1,2.Dichloroethane
13-Jan-10 Tetrachloroethene
TCLP Metals
Rep Lmt
0.1
0.2
0.5
0.5
0.5
0.5
5
0.002
TCLP Volatiles
Rep Lmt
0.1
2
0.2
0.1
0.1
0.1.
0.1
0.1
0.1
0.1
TCLP BNA
Collected Analyte
13-)an-10,2,4,6;. Trichlorophenol
13-Jan-10 Nitrobenzene
13-Jan-10 Cresols
13-Jan iO 2,4,5 Trichlorophenol
13-Jan-10'.Pentach lorophenol
13-Jan-10 Pyridine
13-Jan-10 2,4-Dinitrotoluene
13-Jan-10 Hexachloroethane
-13-Jan-10 Hexachlorobenzene
13-Jan-10 1,4-Dichlorobenzene
13-)an-10.Hexachloro 1,3-butadiene
Rep Lmt
0.25
0.1
5
0.25
0.25
0.25
0.1
0.1
0.1
0.1
0.1
January 22, 2010
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville, NIC 27028
Received: l/15/2010
Project #: Dunn WTP, 'WWTP
Result Units Mattis Method
<0.1 mg/I SL 1311
<0.2 mg/I SL 1311
<0.5 mg/l SL 1311
<0.5 mg/I SL 1311
<0.5 mg/I SL 1311
<0.5 mg/l SL 1311
<5.0 mg%I, SL . 1311
<0.002 mg/I SL 1311
DF ReqLvl Rut. Analyst'
1 1 - 20-Jan-1O WK
1 5 20-Jan-10 VVK
1 . '1 20-Jan-10 VVK
1 5 20-Jan-10 VVK
1 5 , 20-Jan-10'VVK
1 5. 20-Jan-10 WK
1 100 20-Jan-10-VVK
1 0.2 20-Jan-10.VVK'
Result Units Matrix Method Dr'
<0.1 mg/L SL 1311 1
<2.0 mg/L SL 1311 1
<0.2 - . mg/L SL 1311 1
<0.1 rng/L SL 1311 1
<0.1 mg/L SL 1311 1
<0.1 mg/L SL. 1311 1
<0.1 mg/L SL 1311 1
<0.1 mg/L SL 1311 1
<0.1 mg/L 'SL 1311 1
<0.1 rng/L SL 1311 1
Result Units Matrix Method DF
<0.25 mg/I SL 1311 1
<0.1 mg/I SL 1311 1
<5.0 mg/I SL 1311 1
<0.25 mg/I. SL 1311 1
<0.25 mg/1 SL 1311 1
<0,25 mg/1 SL 1311 , '1
<0.1 mg/I SL 1311 1
<0.1 mg/I SL 1311 1
<0.1 mg/I SL 1311 1
<.0.1 mg/I SL 1311 1
<0.1 mg/1 SL 1311 1
'Analytical Integrity" • EPA Certified • NELAP Certified
3310 Win Street • Cuyahoga Pails, Ohio 44223 Phone: [phone] • Fax: 330-
Web Site: www. settek.cam
ReqLvl . Run Analyst
0.5. 19-Jan-10 MS
200 19 Jan-10 MS
0:2 19-Jan-10 MS
100 19-Jan-i9 MS
6.* 19-Jan710 MS
0.7 19-Jan-10 MS
0.5 19-Jan-:10 MS
0.5 19 Jan-10 MS
0.5 19Jan-1O MS
0.7 '19=Jan-1.O MS
ReqLvl ;Run Analyst
2 , 21 Jan-10 AE
2 21-Jan-10 AE
200 21 Jan-10 AE
400 21.Jan 10 AE
100 21-Jan-10 AE
5 21-Jan-l.O.AE
0.13 21-Jan-10 AE
3 21-Jan-10 AE
0.13 .21 Jan-10 AE
7.5 21-Jan-10.AE
0.5 21 Jan-10 AE
-4489
Page 4

ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
TCLP Pesticides
Client ID# Lah ID# Collected Analvte Rep Lmt Result
Dunn WTP 1000660-01 13-Jan-10 Methoxychlor 0.002 <0.002
Dunn WTP 1000660-01 13-Jan-10 Toxaphene 0.1 <0:1-
Dunn WTP 1000660-01 13-Jan-10' Endrin 0.002 <0.002
Dunn WTP 100066Q-01 13-Jan-10 Gamma-BHC 0.002 <0.002
Dunn WTP 1000660-01 13-Jan-10 Heptachlor Epoxide 0.002 <0.002
Dunn WTP 100066Q-01 13-Jan-10 Heptachlor 0 002 <0.002
Dunn WTP 1000660-01 13-Jan-10 Chlordane 0.01 <0.01
TCLP Herbicides
Cliint'ID# Lab ID# Collected An_ alvte Rep'Lmt Result
Dunn WTP 1000660-01 13-Jan-10 2,4,5-TP(Silvex) 0.5 <0.5
Dunn WTP 1000660-01 13-Jan-10 2,4,1) 5 <5.0
C:liental)#
Dunn- WTp `
•
tlD#
I� r.S1 WTP
Client ID#
Dunn: WTP
Client 11)#
Dunn WTP
Lah ID# Collected Analytc
1000660-01 13-Jan-10 Flath Point
Lah ID# Collectczi Analvte
1000660-01 13-Jan-10 pH
Lab ID# Collected Analvte
1000660-pi 13-Jan-10 Reactive Cyanide
Lab. ID# Collected Analvte
1000660-01 13-Jan-10 Reactive Sulfide
Client ID# Lab•ID# Collected Analyte
Dunn.WWTP 1.000660.-02 13 Jan-10 Cadmium
Dunn WWTP 1000660-02 13-Jan710 Chromium
bunn WWTP 1000660=02 13-Jan-10 Selenium
Dunn WWTP 1000660,-02 '13-Jan-10 Arsenic
Dunn-WWTP 1000660-02 13-Jan-10 Lead
Dunn WWTP 100066Q-02 13-Jan-10 Silver
•Dunn WWTP 1000660-02 13-Jan-.10 Barium
Dunn WWTP 1000660-02 13-Jan-10 Mercury
TCLP Metals
Rep Lmt
0.1
0.2
0.5
0.5
0.5
0.5
5
0.002
Result
>140F
January 22, 2010
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville, NC 27028
Received: 1/15/2010
Project #: Dunn WTP, WWTP
Units Matrix
mg/I SL
mg/I SL
mg/I SL
mg/I SL
mg/I SL
mg/I SL
mg/I SL
Method
1311
1311
1311
1311
1311
1311
1311
DF
1
1
.1
1
1
1
1
ReaLvl Run Analyst
10' 21-Jan-10 KMG
• 0'5 21-Jan-1Q KMG
• 0.02 21-Jan-10 'KMG
0.4•. 21-Jan-10 KMG
0.008 21-Jan-10 KMG
0.008 21-Jan-10 KMG
0.03 21-Jan-10 KMG
Units Matrix Method DF RegLvII Run' Analyst
mg/l SL 1311 1 1 20-Jan-10 KMG
ntg/I SL 1311 1 10 20-Jan-1Q .KMG
Units Matrix Method DF LOQ Run Analyst
SL .1010 1 18-Jan-10 DVW
Result .tltiits Matrix Method Di' LOQ Run Analyst
6.46 su©19.4C -SL 9040 1 - 0.01 18-Jan-10 RJM
Result
<0.5
Result
<25.0
Result
<0.1
<0.2
<0.5
<0.5
<0.5
<0.5
<5.0
<0.002
Units Matiix Method DF LOQ Run Analvst
mg/kg SL 7,3.3.2 1 0.5 19-Jan-1Q TRB
Units Matrix Method DF LOQ Run Analvst.
rng/kg .SL 7.3.4.2 1 25 19-Jan-10 TRB
Units Matrix
mg/I SL.
mg/1 SL
mg/I SL
mg/I. SL
mg/I SL
mg/I SL
mg/I SC
mg/1 SL
Method
1311
1311
1311
1311
1311
1311
•1311
1311
DF
1
1
1
1
1
1
1
1
ReciLvl Run Analyst
1 20-Jan-10 VVK
5 20-Jan-10 WK
. 1 20-Jan-10 VVK
5 20-Jan 10 WK
5 20-Jan-10 VVK
5 20-Jan-10 VVK
100 20-Jan-10 VVK
0.2 20-Jan-10 VVK
Page 5
"Analytical Integrity" • EPA Certified • - NELAP-Certified
3310 Win Street • Cuyahoga Fails, Ohio 44223.• a Phone: 3$0.253-8211 • Fax: [phone]
Web Site: Www.settek.com

Client ID# •
Dunn WWTP
Dunn WWTP
Dunn WWTP'
Dunn'WWTP
'Dunn WWTP
Dunh WWTP
Dunn WWTP
Dunn WWTP
Dunn WWTP
Dunn WWTP
Client ID#
Dunn WWTP-
Dunn WWTP
Dunn WWTP
Dunn WWTP
WWTP
a WWTP
Dunn WWTP
,Dunn WWTP
DunnW,WTP
„ Dunn WWTP
• Dunn, WWTP
Clicnt.lD#:
Dunn: W WTP
Dunn WWTP
Dunn WWTP
Dunn WWTP
Dunn WWTP
Dunn WWTP
Dunn WWTP
Client ID#
Dunn WWTP
Dunn WWTP
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Labor teries
Lab ID#
1000660-02
1000660-02
1000660-02
1000660-02
1000660-02'•
1000660-02
1000660-02
1000660-02
1000660=02
1000660-02
Lib 11)#
1000660-02
1000660-02
1000660-02
1000660-02
1000660-02
1000660-02
1000660-02
1000660-02
1000660-02
10.00660-02
1000660-02
Lab ll)#
1000660.02
1000660=02
1000660-.02
1000660=02
1000660-02
1000660-02
1000660-02
TCLP Volatiles
Collected Analyte
13-Jan-10 Trichloroethene
13-Jan-I0 2-Butanone (MEK)
13-Jan-10 Vinyl Chloride.
13-Jan-10 Chlorobenzene
13-Jan-10; Chloroform .
13-Jan-10 1,1-Dichloroethene
13-Jan-10 Carbon tetrachloride
13-Jan-10 Benzene
13-Jan-10 1,2-Dichloroethane
13-Jan-10 Tetrachloroethene
January 22, 2010
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville, NC 27028
Received: 1/15/2010
Project #: Dunn WTP, WWTP
Rep Lmt Result Units Matrix Method DI' ReqLvl
0.1 <0.1 mg/L SL 1311 1 0.5
2 <2.0 mg/L SL 1311 1 200.
0.2 . <0.2 . mg/L SL 1311 . 1 0.2
0.1. <0.1 nig/L SL 1311 1 100
0.1. <0.1, mg/L . SL. 1311 1 6
0.1 <0.1 mg/L SL 1311 1 0.7
0.1 <0.1 mg/L SL 1311 1 0.5
0.1, <0.1 mg/L SL 1311 1 0.5
0.1 <0.1 mg/L SL 1311 1 0.5
0.1 <0.1 mg/L SL 1311 1 0.7
TCLP BNA
Collected Analyte
13 Jan-10 2,4,6--Trichlprophenol
13 Jan-10 Nitrobenzene
13-Jan-10 Cresols
13 Jan=10 2,4,5-Trichlorophenol
13 Jan-10 Pentachlorophenoi
13 Jan-10 Pyridine
13-Jan-1014=D ich lorobenzene
13-Jan-104Hexachloro 1,3-butadiene
13=Jan-10 2,4-Dinitrotoluene
13-Jan-10 Hexachlorobenzene
:13-Jan-10 Hexactiloroethane
Rep Lmt Result Units Matrix Method DI' ReqLvl
0.25• <0.25 mg/I SL 1311 1 2
0.1 <0.1 mg/I SL 1311 1 2
5 <5.0 mg/I SL 1311 1 200
0.25 <0.25 mg/i SL 1311 1 400
0.25 <0.25 mg/I SI_ 1311 1 100
0.25 <0.25 mg/I SL 1311 1 ' 5
0.1 <0.1 mg/I SL 1311 1 75
0,1 <0.1 mg/I SL 1311 1 0.5
0.1 <0.1 mg/I SL 1311 ' 1 0.13
0.1 <0.1 mg/I SL 1311 1 0.13
0.1 <0.1 mg/I SL 1311 1 3
TCLP Pesticides
Collected Analyze
13-Jan-10 Gamma-BHC
13-Jan-10 Toxaphene
13-Jan-10 Methoxychit r
13: Jan-10 Endrin
13-Jan-10 Heptachlor Epoxide
13-Jan-10 Heptachlor
13-Jan-10 Chlordane
Lab ID# Collected Analyte
1000660-02 13-Jan-10 2,4,5-TP(Silvex)
1000660-02 13-Jan-10 2,4,D
Rep Lmt Result
0.002 <0.002
0.1 <0.1
0.002 <0.002
0.002 <0.002
0.002 <0.002
0.002 <0.002
0.01 <0.01
TCLP Herbicides
Rep Lmt Result
0.5 <0.5
5 <5.0
Units Matrix Method [)I RegLvl
mg/I SL 1311 1 0.4
mg/1 SL 1311 1 0.5
mg/I SL. 1311 1 10
mg/I SL 1311 1 0.62
nig/I Si_ 1311 1 0.008'
mg/I SL. 1311 1 0.008
m0/I ' SL 1311 ' 1 0.03
. Units Matrix Metliod
mg/I SL . 1311
mg/I SL 1311
"Analytical Integrity" • EPA Certified •. NELAP Certified
331E Win Street • Cuyahoga Palls, Ohio 44223 Phone: [phone] • Fax:
Web Site: yt=ivw.seitek.corn,
Run Analyst
19-Jan-I0 MS
19-Jan40 .MS
19-Jan-10 MS
19-Jan-10 MS
19-Jan-10 MS
19-Jan-10 MS
19-Jan-10 MS
19=Jan-10 MS
19 Jan-10 MS
19 Jan-10 MS
Run Analyst
21-Jan-.10 AE
21-Jan-10 AE
21-3an-10 AE
21-Jan-10 AE
21-Jan-10 AE
21-Jan-10 AE.
21-Jan-10 AE
21-Jan-10 AE
21-Jan-10 AE
21,Jan-10 AE
21-Jan-10 AE
Run ' Analyst
21-Jan-10 KMG
21: Jan-10. KMG.
21-Jan710 ;KMG
21-Jan-10 KMG
21-Jan-10 KMG
21-Jan-10 KMG
21-Jan-10: KMG
DE ReqLvl Run Analyst
1 1 20-Jan-10 KMG
1 10 20-Jan-10 KMG
2
4489
Page 6

client 1D#
Dunn WWTP.
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Lab ID# Collected Analvte
1000660-02 13-jan-10 Flash Point •
January 22, 2010
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville, NC 27028
Received: 1/15/2010
Project ti: Dunn WTP, WWTP
Result Units Matrix Method DF LOQ Run Analyst
>140F SL 1010 1 187.1an-10 DVW
. Client ID# Lab IDN Colleett‘i Analvte Result Units Matrix 'Method DF LOQ Run' Analyst
Dunn WWTP 1000660-02 5.98 su@1911c SL 9040 1 0.01. 18-lan-10 RJM
Client ID# Lab ID# Colleted 'Analvte
DUrin WWTP 1000660-02 13-Jan-10 Reactive Cyanide
Result. . Units Matrix Method DF LOQ Rtin Analyst
<0.5 mg/kg SL 7,3.3.2 .1 0:5 19-Jai-10 TRB
„ Lab ID# Collected •Analyte ResultUnits .Matrix Method DE LOQ Run Analyst
bunn WVVTP 1000660-02 13-Jan-10 ReaCtive Sulfide <25..0 • Mg/kg SL 7.3.4.2 1 25 19-Jan-10 TRB
Page 7
"Analytical integrity" • EPA Certified • NELAP Certified
3310 Win Street • Cuyahoga Falls, Ohio 44223 a Phone: [phone] • Fax: [phone]
Web Site: www.settek.com

Summit Environmental Technologies, Inc.
Cooler Receipt Form
Client' Order Number: 1 000g&)
Date Received: //' / 5 Time Received: �V Gb `
Number 'f Co.: su&axes: 1 N/A
Shippe . FED UPS DHL Airborne US Postal Walk-in Pickup . Other:
Packaging:
Tape on cooler/box:
Custody Seals intact
C-O-C in plastic
Peanuts ,Nubble 'rap Paper Foam None Other:
N N/A
.N
•N N/A
Ice?{ Blue. ice N/A
N/A
N/A
present / absent / melted
Sample Temperatureoc
C-O-C. filled out properly t Y N
Samples in separate bags Y N
Sample containers intact* N
*lino, list broken sample(s).
N/A
N/A
Sample label(s) complete (ID, date, etc.)
Label(s) agree with C-O-C
Correct containers used
Sufficient sample received
Bubbles absent -.from 40 mL vials**
Y
**Samples with bubbles less than the size of.a pea are acceptable.
Was client contacted about samples
Will client send new samples Y N
Client contact:
N N/A
N N/A
N N/A
N N/A
Y
Date/Time:.
Logged in by:
Comments:
Rev. 6

min VII,011111entai lecnnologtes, Inc.
sEl WILL
__;"thogrPalrOtrier-6142-23' Tel: [phone] Fax: [phone]o9
Client Name
•
•ql 14 A
Client Address
*a=g4. A/ O4Lr' e..1-
1A04.1c.01 b D.1
Client Phone No.
VCA- 1119, /1 (.0
Client Fax No. Please Fax Results
Project Name
01).-N4 Nie 60-T e
nalysis equ.estiChain of Custoof
For Summit Environmental Technologies, Inc. use only
Page
-ofSET No.
Project AddreSs
Report'to
Po#
Client Email
Quote No.,
Contact erson r, •
samPkt4,,
Sample Identification
cx...)4psi LAYT
Otkr4*.. LiL.Tp
Check if Ohio VAP samples
•Date
CollreCted
Time
'C011ected •
3 0 pivk
•
'64
•
• a-
• E
)k.
Number of Containers
$‹.
AirmlyticaI Parameters and Methods
•
2
d b :
..ti)
Date
1-7•14.+10
Time
Received by:
Date
rime
Received in lab by:
/(.5 7Ci /01 .24
Date
Tune
Rush Requested: Days
Must be.approved by lab manager
Notes/Comments:
•
White and yellow pagesshould accompanysamples to the laboratory The client retains the pink page.
22F2fl

Analytical Results
Synagro Central
284 Boger Rd.
Mocksville
Entered 2/23/2010
Reported: 3/1/2010
Sample Remark
NC 27028
Sample ID Parameter Cust ID
For: Dunn
Result Units Method Date Analyzed Analyst
100223-7.1
100223-7:1
100223-7.1
100223-7.2
100223-7.2
3-7.3
100223-7.3
100223-7.4
100223-7.4
100223-7.5
100223-7.5
100223-7.6
100223-7.6
100223-7.7
100223-7.7
% Solids 1
Fecal Coliform MTF 1 •
Geometric Mean
% Solids
2
Fecal Coliform MTF 2
% Solids 3
Fecal Coliform MTF 3
% Solids
4
Fecal Coliform MTF 4
% Solids 5
Fecal Coliform MTF 5
% Solids
6
Fecal Coliform MTF 6
% Solids • 7
Fecal Coliform MTF 7
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
NC00909
2.62
343,511
85,394
2.62
114,504
2.50
68,000
2.51
31,873
2.66
30,075
2.57
66,148
2.58
193,798
MPN/g
MPN/g
MPN/g
%
MPN/g
%
MPNIg
MPN/g
MPN/g
%
MPN/g
SM2540B
SM92210E
dry wt. basis
SM2540B
SM92210E
SM2540B
SM9221 CE
SM2540B
SM92210E
SM2540B
'SM92210E
SM2540B
SM92210E
SM2540B
SM9221 CE
2/23/10
2/23/10
2/25/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
2/23/10
CL
CL
CL
CL
CL
CL
CL
CL
CL
CL
CL
CL
CL
CL
CL
P.O. Box 228 • Statesville, North Carolina 28687.704/872/4697

Client: � 7�
, 0
STATESVI aNALYTICAL
122 Court Street • P.O. Box 228
Statesville, NC 28687 "
[phone]
Chain of
Custody Record
_" I
Address: � s j / ��
M o Les`Vi t.,i, i l ►Q C.- 2 70 2.a
e "
Contact Person: E-4 c !, j,,,, „�l<O . ) Phone # �?� _ -71 ,4 s' FAX# �?.�._a58 .8156
' `4'
—
ANALYTIC LE
AL
PO # Requisitioned by: (Time Date)
Customer
Sample ID#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled
(Grab nlv)
08
E
Matnx �.
Parameters requested for analysis
sludge
w
yew
D /•-li VC l
1,(- (0 0l -1- ). /t
L S•
6 13/ 0
: --
rCCAr_ ev z- - .0 N>' /
Z
5
q
S
1
.
)
i 1
Relinquished by:
/ Time Z ' /2- arr m Date a?/ 2- ?/ id Sampled by: c/ee /i-r<<--4er<n!
7•••
Received by: Time am, pm Date /_/_ Transported by:
-%
Relinquished by: • Time am, pm Date / /
Holding times met:
Received by: `i�
cam'
��— ��Time am,�ate- [ U
Compliance work:
Composite Sampling #1:
Time begin am, Date / / Non-compliance work:
pm
Time end am, Date / /
pm
Composite Sampling #2•
Lab Comments:
Time begin am, Date /•
_ pm
Time end am, Date / /
pm

Condition of Receipt
Sample ID 100223-7
Client Synagro Central
Temp on Arrival I.
pH upon Arrival
pH upon Arrival
Parameter Schedule
% Solids
HNO3
HCI
NaOH
H2SO
Na2S2O
❑ - Dechlorinated
Parameter Schedule:
Fecal Coliform MTF
❑ HNO3
❑ HCI
❑ NaOH
• H2so
Na2S2O
❑ Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
0 Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
• Received on Ice
❑ Samples chilled upon receipt
O Chemicals in containers, lab
Page 1,of 1

Decernber2008/ January 2009 Vector Attraction
Rec. 77%
Holding 1 ank C7q(
.77-.67
.77-(.77x.f 7)
11-CA--NA1�

May 09 Vector nllractian
Itec.-82%
Holding Tank— 74°,
.82-.74 - 39%
.82-(.82x.74)
August 2008 Vector Attraction
Rcc. 809G
HoldingTank-69.5%,
.80 69.5 T-43°%
.80-(.80x.695)

Sejilelnber 09 vector Attraction
liec.-79'%
Holding Iank
.79.69 41%
.79-(.79x.69)
August 2008 Vector Attraction
Rec: —80%
Holding Tank-695%
.80-69..5 -43%
.801.80x 695)

NCDENSZ
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
January 12, 2011
Ronald D. Autry
City of Dunn
PO Box 1065
Dunn. NC 28355
Subject: Acknowledgement of Application No. WQ0006101
City of Dunn Residuals Land Application Program
Land Application of Residual Solids (503)
Harnett
RECEIVED
JAN 1 4 2011
DENR-FAYETTEVILLE REGIONAL OFFICE
Dear Mr. Autry:
The Aquifer Protection Section of the Division of Water Quality (Division) acknowledges receipt of your permit application and
supporting materials on January 11, 2011. This application package has been assigned the number listed above and will be reviewed
by Alice Wessner.
The reviewer will perform a detailed review and contact you with a request for additional information if necessary. To ensure the
maximum efficiency in processing permit applications, theDivisionrequests your assistance in providing a timely and complete
response to any additional information requests.
Please be aware that the Division's Regional Office, copied below, must provide recommendations prior to final action by the
Division. Please also note at this time, processing permit applications can take as long as 60 - 90 days after receipt of a complete
application.
If you have any questions, please contact Alice Wessner at 919-715-5208, or via e-mail at [e-mail]. If the reviewer
is unavailable, you may leave a message, and they will respond promptly.
PLEASE REFER TO THE ABOVE APPLICATION NUMBER WHEN MAKING INQUIRIES ON THIS PROJECT.
Sincerely,
M2c4DIA
for Jon Risgaard
LAU Supervisor
cc:c.F—rote��
ayettevill Regional -Off ce,—Aquifer Pction_SectibiCi
Synagro (Eric N. Thompson - 284 Boger Road, Mocksville, NC 27028)
Permit Application File WQ0006101
AQUIFER PROTECTION SECTION
1636 Mail Service Center, Raleigh, North Carolina 27699-1636
Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604
Phone: [phone] FAX 1: 919-715-0588; FAX 2: 919-715-6048 \ Customer Service: 1-877-623-6748
Internet: www.ncwaterauality.orq
An Equal Opportunity 1 Affirmative Acton Employer
One
N©r.thCaroiina
dtura 2y