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NCG030669_Monitoring Report_20220329
NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG030000 -N- Metal Fabrication Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DM'0} Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate Dt<'tVil�.R,Regional Office. Certificate of Coverage No. NCG03 06 Person Collecting Samples: AV1_?1"/e j WFAIS-L Cl Facility Name: /{ C % L / 'T Y Laboratory Name: 1PACC is /1,eyTr G/1 L Facility County: R V W4 Laboratory Cert. No.: D . ' %OG� Discharge during this period: Yes E]No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Yes ONo If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Yes No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Code Parameter Outfall % Q Outfall Outfall Outfall Outfall N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 03 /fo e&.? 46529 24-Hour Rainfall in inches Qa <-+ C0530 TSS in mg/L (100 or 50*) C' 2 S �.��L 2. 5-'" 2 00400 pH in standard units (6.0-9.0 FW, T �� 6.8-8.5SW) 01119 al le in mg/L (0.010 FWt0.0058 SW) +GG'�t� 01051 Lead, total recoverable in mg/ L rn �s < 003-0 m� (0.075 FW, 0.22 SW) / 01094 Zinc, total recoverable in mg/ L (0.126 �° FW, 0.095 SW) .v/Cyr➢ 00340 Chemical Oxygen Demand (COD) in <,/n� m'/ 00552 Non -Polar Oil & Grease in mg/L (15) < 9 %V11 < 5- U ir�z * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L FW (Freshwater) SW (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee or Delegated Authorized Individual 1 �t «� f 1'✓��CC1? - Y ti'�^QC �1f'�r�' Ce ail Address Z �C) L, Date I/ fI_S /1 Phone Number aceAnalytical www.pacelabs.cem March 24, 2022 Robert Hensley Agility Fuel Systems 1010 Corporate Center Drive Salisbury, NC 28146 RE: Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 Dear Robert Hensley: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RECEIVED MAR 29 M22 UENK-DEMLR Land Quality Section Mooresville Regional Office Enclosed are the analytical results for sample(s) received by the laboratory on March 18, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek. hooks@pace labs. com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification M 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: 1ST QUARTER STORMWATER 92594346 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92594346001 OUTFALL 2 GRAB EPA 1664E ICO 1 PASI-C EPA 200.7 Rev 4.4 1994 KH 3 PASI-A SM 2540D-2015 MA62 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92594346002 OUTFALL 1B GRAB EPA 1664B ICO 1 PASI-C EPA 200.7 Rev 4.4 1994 KH 3 PASI-A SM 254OD-2015 MAB2 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 2 GRAB Lab ID: 92594346001 Collected: 03/16/22 17:00 Received: 03/18/22 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 03/21/22 23:53 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper ND ug/L 5.0 1 03/19/22 18:47 03/21/22 22:35 7440-50-8 Lead ND ug/L 5.0 1 03/19/22 18:47 03/21/22 22:35 7439-92-1 Zinc ND ug/L 10.0 1 03/19/22 18:47 03/21/22 22:35 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids ND mg/L 2.5 1 03/21/22 13:06 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services - Asheville Chemical Oxygen Demand ND mg/L 25.0 1 03/24/22 01:42 03/24/22 04:46 Date: 03/24/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 1B GRAB Lab ID: 92594346002 Collected: 03/16/22 18:00 Received: 03/18/22 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 03/21/22 23:53 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper ND ug/L 5.0 1 03/19/22 18:47 03/21/22 22:38 7440-50-8 Lead ND ug/L 5.0 1 03/19/22 18:47 03/21/22 22:38 7439-92-1 Zinc ND ug/L 10.0 1 03/19/22 18:47 03/21/22 22:38 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids ND mg/L 2.5 1 03/21/22 13:06 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services - Asheville Chemical Oxygen Demand ND mg/L 25.0 1 03/24/22 01:42 03/24/22 04:46 Date: 03/24/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 QC Batch: 686269 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92594346001, 92594346002 METHOD BLANK: 3588125 Matrix: Water Associated Lab Samples: 92594346001, 92594346002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 03/21/22 23:53 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3588126 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 17.8 89 64-132 MATRIX SPIKE SAMPLE: 3588127 92594214001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 14.4 66 64-132 SAMPLE DUPLICATE: 3588128 35704294001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L 5.OU ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/24/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aceAnaIXical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 1 ST QUARTER STORMWATER Pace Project No.: 92594346 QC Batch: 685960 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92594346001, 92594346002 METHOD BLANK: 3586865 Matrix: Water Associated Lab Samples: 92594346001, 92594346002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 03/21/22 21:18 Lead ug/L ND 5.0 03/21/22 21:18 Zinc ug/L ND 10.0 03/21/22 21:18 LABORATORY CONTROL SAMPLE: 3586866 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 505 101 85-115 Lead ug/L 500 485 97 85-115 Zinc ug/L 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3586867 3586868 MS MSD 92593976001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 69.8 500 500 586 585 103 103 70-130 0 Lead ug/L ND 500 500 444 447 88 89 70-130 1 Zinc ug/L 238 500 500 708 714 94 95 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3586869 3586870 MS MSD 92594264001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 494 491 99 98 70-130 1 Lead ug/L ND 500 500 482 479 96 96 70-130 1 Zinc ug/L 114 500 500 588 584 95 94 70-130 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/24/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 QC Batch: 686030 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92594346001, 92594346002 METHOD BLANK: 3587064 Matrix: Water Associated Lab Samples: 92594346001, 92594346002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/21/22 13:05 LABORATORY CONTROL SAMPLE: 3587065 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 3587261 92594270001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 251 266 6 SAMPLE DUPLICATE: 3587262 92594330001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 126 107 16 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/24/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalj cal www.pacelabs.com QUALITY CONTROL DATA Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 QC Batch: 686575 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92594346001, 92594346002 METHOD BLANK: 3589466 Matrix: Water Associated Lab Samples: 92594346001, 92594346002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 03/24/22 04:40 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3589467 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 766 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3589468 3589469 MS MSD 92593813003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mg/L 26.5 100 100 130 125 103 99 90-110 4 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3589470 3589471 MS MSD 92593813006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 121 121 112 112 90-110 0 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/24/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 aceAnalXical www.pacelabs.com QUALIFIERS Project: 1 ST QUARTER STORMWATER Pace Project No.: 92594346 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/24/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 FaceAnalytical www.pacelabs.com , QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: 1ST QUARTER STORMWATER Pace Project No.: 92594346 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92594346001 OUTFALL 2 GRAB EPA 1664B 686269 92594346002 OUTFALL I GRAB EPA 1664B 686269 92594346001 OUTFALL 2 GRAB EPA 200.7 Rev 4.4 1994 685960 EPA 200.7 Rev 4.4 1994 685977 92594346002 OUTFALL 1 B GRAB EPA 200.7 Rev 4.4 1994 685960 EPA 200.7 Rev 4.4 1994 685977 92594346001 OUTFALL 2 GRAB SM 2540D-2015 686030 92594346002 OUTFALL 1B GRAB SM 2540D-2015 686030 92594346001 OUTFALL 2 GRAB SM 5220D-2011 686575 SM 5220D-2011 686901 92594346002 OUTFALL I GRAB SM 5220D-2011 686575 SM 5220D-2011 686901 Date: 03/24/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Documeht.Nanie: Document Revised: November 15,2021 hd Sample Condition Upon Recefpt(SCU(i), pa e,1 of 2 aCeAr lye c(C�l Documet No;; Issuing Authority; ^�_ F•CAR•t 5•t)33•Rev:OB Pace Caro)ima QualitYOHlce t.ebora ory receiving samples: Asheville (1 Eden❑ Greenwood n Huntersville C] Raleigh[] Mechanlesville❑ Atlanta❑' KernersyilleF� Client Nastte; Project#:WO# : 92;594346 9�L�t� F`,P% St,s�r.� s courier: ed Esc$ �1 ❑Client II' II" IIII'I' II (I I'I) ©:Cortim. eroal El Pace 92594:346 Custody Seat Present? Dyes ®No Seals,itttact? ❑Yes MNo - Packing Materiel; ❑Bub.bie Wrap. VIBUbbie Bags ❑None ❑ Pther Thermorfieter: � IR run xv, 93 / 0% / ®4Vet ❑glue Type.uf ice: ^CQUection Factor: COON?TerMpt © Atid/Subtract ('C) CbalerIemp Corrected ('C): USt)A Regul@ted Soll Q N/A, water sample) Did samples originate to a quarantine tone within the United States: CA, NY, or SC (cheek mops)? d'iVnc rANn Dale/IrilUalsPerson:ExarriiningCaritent9;.1 �(/-�.z-/�/{ Biological Tissue Prozon? ❑ye's (lNo MNJA nNonr, Temp should be above freezing to 6°C []5emplos Out of lemp criteria. 5bm ples on kq, coaling pmcess hat begun Did sainpiei ollglnutefrdm a lorefgn source pnternatlanaliy, CPiTurn /Dls repancy_ -- Chalri of6ustod .Present? ONa. ❑4/A 1 Sa nip fasArOvedwithin HoicITlme710yes . No .... ❑N'q 2, shpit bold Ttme Anal sis <72 hr.)? (QYes .EbNo Qq1A 3: ttuiliTutn.ArooOdThneRogtlested7 Yes. No tIN/A 4. SuffoentVnluRm7,_ `_ Yes_❑No N A _5, _ CorrdatC.opcainers Used? Pace t ontainers Used?.. Myos; ❑Na Qti/A Yes .: (]No.. .. (JN/A S _.. Dissolved analysis; Sample's field Filtered? _ Yes No N A 8, Santpita Labels Match Cbe? irteludes gate/time/ID/Analysis Matrix:. ( (7-�- Yes QNo W ! DN/A 9. Plead$ pace In VUA VWs (>S-6mm)? Yes rJNo N/A 10. 11, Trip 61ankPresent? ❑yes [INo [ jN/A Trip Blanktgstody5palsPresent? QYes ❑Na N/A COMMENTS/SAMPLE DISGREDANCY Field Data Required? ❑*s (].No Lot ID of spliteofltaifters CLIENT NOTIFICATION/RESOLUTION — — Person contacted: Project Manager.SCURF Review; Project Manager SRF Review: Date/Tfine: Date: Date. Page 12 of 14 ant Naive: No,: "Check mark top half of box. if pH and/or dechiorination is verified and.within the'acceptance range for preservation samples, Extepglorts;VOA; Coliform;_:TOC, Oil ddd Grease, DRO/8025 (wktfr) 00C,. LLHg *'Bottohrhalf of, box ls,to list number of Bottles Document Revised: November Pake2 of 2 ParF.[arollnas Oualliv Office Project # W01t : 92594346 PM: T:iH Due Dale: 03/25/22 CLIENT: 92-Agility F u p T 1 V x �^ G [L7.'i, N •. a x § u C .� e � ;w •n � d v ` � ci a E. x � � � a� :yc � � w a �. Z: a, a ..'a 0. E 2 d . Q 4 ry � : O .O� 0. �' N' A CL Z. cy i o ��+ a`. E. E P k E E £ In N i� ri ra�r i cE iJ' e c6� iJ "� a r�� Y g E �E Y`� yYp, 0.. MJN 4 :o . — P3 pH Adjustment Log for PreservedSamples _ Semple to. Type of Preservative pH upon receipt Qate,preservatlon adtufted Tinte.preservatim, adjusted Amount of Preservative Added Lot p Note: Whenever there Is a dhcrepancy affecting North Carolina compliance samples, a Copy of this form will be sentto the North_Coolina QEtINR Certifination Office(i.e. Out of'hold, Incorrect.preseivative, out of temp., incorrect containers, Page 13 of 14 ITEM # a P , i A o 0 (n IN V Sr 0 :E 'R MATRO(COM SAMPE TYPE (GaGRAB C=CO,%!P) 0 > cn 0 SAMPI If -L'PATCCLILECTION A FV 112SO4 z HNO3 iF 8' I IW Moll Na2,1320 (D CA PIZ,, hialhanol Ed 1 0:1101 7 _j --F-1- Ti N F 3. F-1 TSS tp 1664 OJ rml G!9m mstsis by 203.7 'U z t CD Rouidtful Cli'cdno (YIN) y flac&vud on (YIN) cuslody Sunled co ter .Y/N) A samrifig n1act __A_LL__L i 1 .1-1 1 Page 14 of 14