NCG030571_Monitoring Report_20220405

NICDEQ Division of Energy, (Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for N00030000
Metal Fabrication
Click here for instructions
N I7
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Uploa�tvithi
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate ce.
ropriate DEMLR iJffi
Certificate of Coverage No. NCG03 0571
ti
Person Collecting Samples: Bill Jacob
Facility Name: Norton
Laboratory Name: Pace Analytical services
Facility County: Union
Laboratory Cert. No.: 12 and 40
Discharge during this period: [D Yes 0 No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Yes No
If so, which Tier (I, II, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Yes U Na
Date Uploaded: 0313112020
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall soo-1
Outfall Soo-2
Outfall Soo-3
Outfall
Outfall
N/A
Receiving Stream Class
c
c
No discharge
N/A
Date Sample Collected MM/DD/YYYY
03/09/2022
0310912022
46529
24-Hour Rainfall in inches
0.55
0.55
C0530
TSS in mg/L (100 or 50*)
10
5
00400
pH in standard units (6.0 — 9.0 FW,
6.8-8.5 SW)
7.6
7.4
01119
Copper, total recoverable in mg/L
(0.010 FW, 0.0058 SW)
0.0064
o.007s
01051
Lead, total recoverable in mg/ L
(0.075 FW, 0.22 SW)
<o.005
<0.005
01094
Zinc, total recoverable in mg/ L (0.126
FW, 0.095 SW)
o-o7os
o.oa7
00340
Chemical Oxygen Demand (COD) in
mg/L (120)
31 I
28.8
00552
Non -Polar Oil & Grease in mg/L (15)
<4.8
<4.8
outralls to outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optiona 1): 5-DO-3 was not sampled hec a there was not a discharge A elea of coolant to 500-3 was discovered and the discharge PIP. was plugged Storm ware -s be ng collect d d Nppe d' `! t- f 1-spo I
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
fals information, including the possibility of fines and imprisonment for knowing violations."
5igna ure of Per ittee or Delegated Authorized Individual Date
unrer@assaabloy-com
Address
704-233-1556
Phone Number

aceAnalytical
www.pacelabs.com
March 25, 2022
Jeff Duke
Assa Abloy
3000 Highway 74 East
Monroe, NC 28112
RE: Project: STORMWATER
Pace Project No.: 92593091
Dear Jeff Duke:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
t704)875-9092
�1, n
,P�p�A
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di oh
0
Enclosed are the analytical results for sample(s) received by the laboratory on March 11, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Project: STORMWATER
Pace Project No.: 92593091
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICA-riONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 36

r a
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
STORMWATER
92593091
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92593091001
SDO-1
EPA 1664E
ICO
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
LMB
34
PASI-C
SM 2540D-2015
MA82
1
PASI-A
SM 4500-H+8-2011
YEG
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92593091002
SDO-2
EPA 1664E
ICO
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
LMB
34
PASI-C
SM 2540D-2015
MAB2
1
PASI-A
SM 4500-H+B-2011
YEG
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 36

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Project: STORMWATER
Pace Project No.: 92593091
Lab Sample ID
Method
92593091001
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 624.1
SM 2540D-2015
SM 4500-H+B-2011
SM 5220D-2011
92593091002
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
SM 254OD-2015
SM 4500-H+B-2011
SM 5220D-2011
Client Sample ID
Parameters
SDO-1
Performed by
Collected By
Collected Date
Collected Time
pH
Copper
Zinc
Trichloroethene
Total Suspended Solids
pH at 25 Degrees C
Chemical Oxygen Demand
SDO-2
Performed by
Collected By
Collected Date
Collected Time
pH
Copper
Zinc
Total Suspended Solids
pH at 25 Degrees C
Chemical Oxygen Demand
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
Assa Abloy
Jacob Bill
03/09/22
08:50
7.6
Std. Units
6.4
ug/L
70.9
ug/L
4.1
ug/L
10.0
mg/L
6.4
Std. Units
31 A
mg/L
Assa Abloy
Jacob Bill
03/09/22
09:00
7.4 Std. Units
7.9 ug/L
47.0 ug/L
5.0 mg/L
6.4 Std. Units
28.8 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/09/22 08:50
03/09/22 08:50
03/09/22 08:50
03/09/22 08:50
03/09/22 08:50
5.0
03/1512212:48
10.0
03/15/2212:48
2.0
03/14/2218:44
25
03/12/22 10:57
0.10
03/14/2212:52 H3
25.0
03/19/22 04:42 M1
03/09/22 09:00
03/09/22 09:00
03/09/22 09:00
03/09/22 09:00
03/09/22 09:00
5.0
03/15/2212:57
100
03/15/22 12:57
2.5
03112/2210:58
0.10
03/14/2212:55 H3
25.0
03/19/22 04:43
Page 4 of 36

f c7ceAnalVtic l
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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92593091
Method: EPA 1664B
Description: 1664 SGT-HEM, TPH
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for EPA 1664B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 684368
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 35702424001
M1. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3579312)
• Total Petroleum Hydrocarbons
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 36

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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92593091
Method: EPA 200.7 Rev 4.41994
Description: 200.7 MET ICP
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for EPA 200.7 Rev 4.4 1994 by Pace Analytical Services Asheville. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 Rev 4.4 1994 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC, Page 6 of 36

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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92593091
Method: EPA 625.1
Description: 625 RVE
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for EPA 625.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 684999
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 35703096001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3582050)
2,4-Dinitrophenol
4, 6- D i n itro-2-meth yl phen of
R1: RPD value was outside control limits.
MSD (Lab ID: 3582051)
• 3,3'-Dichlorobenzidine
• 4-Nitrophenol
• Pentachlorophenol
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 7 of 36

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Project: STORMWATER
Pace Project No.: 92593091
Method: EPA 625.1
Description: 625 RVE
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Additional Comments:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRA"f'IVE
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 8 of 36

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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.. 92593091
Method: EPA 624.1
Description: 624 Volatile Organics
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for EPA 624.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 684527
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92592830002
M1: Matrix spike recovery exceeded QC limits.
MS (Lab ID: 3579935)
Chloroethane
• Chloroform
Chloromethane
MSD (Lab ID: 3579936)
• Chloroethane
• Chloromethane
Additional Comments:
Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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PROJI~(I- NARRATIVE
Project: STORMWATER
Pace Project No.: 92593091
Method: SM 2540D-2015
Description: 2540D Total Suspended Solids
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for SM 2540D-2015 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92593091
Method: SM 4500-H+B-2011
Description: 4500H+ pH, Electrometric
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for SM 4500-H+B-2011 by Pace Analytical Services Asheville. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H3: Sample was received or analysis requested beyond the recognized method holding time.
• SDO-1 (Lab ID: 92593091001)
• SDO-2 (Lab ID: 92593091002)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 36

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PROJECTNARRATIVE
Project: STORMWATER
Pace Project No.: 92593091
Method: SM 5220D-2011
Description: 5220D COD
Client: Norton Door Controls (Assa Abloy)
Date: March 25, 2022
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for SM 5220D-2011 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with SM 5220D-2011 with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 685913
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92593091001,92593358003
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS (Lab ID: 3586686)
• Chemical Oxygen Demand
• MSD (Lab ID: 3586687)
• Chemical Oxygen Demand
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 36

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Project: STORMWATER
Pace Project No.: 92593091
Sample: 5DO-1
Parameters
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92593091001 Collected: 03/09/22 08:50 Received: 03/11/22 12:51 Matrix: Water
Results Units Report Limit DF
Field Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Assa Abloy 1
Collected By
Jacob Bill 1
Collected Date
03/09/22 1
Collected Time
08:50 1
pH
7.6 Std. Units 1
Prepared Analyzed CAS No. Qual
03/09/22 08:50
03/09/22 08:50
03/09/22 08:50
03/09/22 08:50
03/09/22 08:50
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND
mg/L
4.8
1
03/14/22 10:09
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
6.4
ug/L
5.0
1
03/15/22 03:29 03/15/22 12:48 7440-50-8
Lead
ND
ug/L
5.0
1
03/15/22 03:29 03/15/22 12:48 7439-92-1
Zinc
70.9
ug/L
10.0
1
03/15/22 03:29 03/15/22 12:48 7440-66-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 83-32-9
Acenaphthylene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 208-96-8
Anthracene
ND
ug/L
45
1
03/16/22 05:50 03/17/22 03:19 120-12-7
Benzo(a)anthracene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 56-55-3
Benzo(a)pyrene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 191-24-2
Benzo(k)fluoranthene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 101-55-3
Butylbenzylphthalate
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 85-68-7
4-Chloro-3-methylphenol
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 59-50-7
bis(2-Chlorcethoxy)methane
ND
ug/L
9.1
1
03/16/22 05:50 03/17/22 03:19 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 111-44-4
2-Chloronaphthalene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 91-58-7
2-Chlorophenol
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 7005-72-3
Chrysene
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 218-01-9
Dibenz(a,h)anthracene
ND
Gg/L
4.5
1
03/16/22 05:50 03/17/22 03:19 53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
91
1
03/16/22 05:50 03/17/22 03:19 91-94-1
2,4-Dichlorophenol
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 120-83-2
Diethylphthalate
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 84-66-2
2,4-Dimethylphenol
ND
ug/L
9.1
1
03/16/22 05:50 03/17/22 03:19 105-67-9
Dimethylphthalate
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 131-11-3
Di-n-butylphthalate
ND
ug/L
4.5
1
03/16/22 05:50 03/17/22 03:19 84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
9.1
1
03/16/22 05:50 03/17/22 03:19 534-52-1
2,4-Dinitrophenol
ND
ug/L
45.5
1
03/16/22 05:50 03/17/22 03:19 51-28-5
2.4-Dinitrotoluene
ND
ug/L
4-5
1
03/16/22 05:50 03/17/22 03:19 121-14-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC,
Page 13 of 36

Pace Analytical Services, LLC
1��aceklalyiicdl
9800 Kincey Ave, Suite 100
WmI.pacelabs.com Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92593091
Sample: SDO-1
Lab ID: 92593091001
Collected: 03/09/2208:50 Received: 03/11/2212:51 Matrix: Water
Parameters
Results
Units
Report Limit
DF Prepared Analyzed CAS No. Qua[
625 RVE
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 606-20-2
Di-n-octylphthalate
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 117-81-7
Fluoranthene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 206-44-0
Fluorene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 87-68-3
Hexachlorobenzene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.1
1 03/16/22 05:50 03/17/22 03:19 77-47-4
Hexachloroethane
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 193-39-5
Isophorone
ND
ug/L
9.1
1 03/16/22 05:50 03/17/22 03:19 78-59-1
Naphthalene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 91-20-3
Nitrobenzene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 98-95-3
2-Nitrophenol
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 88-75-5
4-Nitrophenol
ND
ug/L
9.1
1 03/16/22 05:50 03/17/22 03:19 100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 621-64-7
N-Nitrosodiphenylamine
ND
ug/L
9.1
1 03/16/22 05:50 03/17/22 03:19 86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 108-60-1
Pentachlorophenol
ND
ug/L
9.1
1 03/16/22 05:50 03/17/22 03:19 87-86-5
Phenanthrene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 85-01-8
Phenol
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 108-95-2
Pyrene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
4.5
1 03/16/22 05:50 03/17/22 03:19 120-82-1
2,4,6-Trichlorophenol
ND
ug/L
9.1
1 03/16/22 05:50 03/17/22 03:19 88-06-2
Surrogates
Nitrobenzene-d5 (S)
77
%
10-120
1 03/16/22 05:50 03/17/22 03:19 4165-60-0
2-Fluorobiphenyl (S)
69
%
15-120
1 03/16/22 05:50 03/17/22 03:19 321-60-8
Terphenyl-d14 (S)
81
%
11-131
1 03/16/22 05:50 03/17/22 03:19 1718-51-0
Phenol-d6 (S)
51
%
10-120
1 03/16/22 05:50 03/17/22 03:19 13127-88-3
2-Fluorophenol (S)
61
%
10-120
1 03/16/22 05:50 03/17/22 03:19 367-12-4
2,4,6-Tribromophenol (S)
92
%
10-137
1 03/16/22 05:50 03/17/22 03:19 118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Pace Analytical Services - Charlotte
Benzene
ND
ug/L
1.0
1 03/14/2218:44 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1 03/14/2218:44 75-27-4
Bromoform
ND
ug/L
2.0
1 03/14/2218:44 75-25-2
Bromomethane
ND
ug/L
2.0
1 03/14/2218:44 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1 03/14/22 18:44 56-23-5
Chlorobenzene
ND
ug/L
2.0
1 03/14/2218:44 108-90-7
Chloroethane
ND
ug/L
2.0
1 03/14/2218:44 75-00-3
Chloroform
ND
ug/L
2.0
1 03/14/2218:44 67-66-3
Chloromethane
ND
ug/L
2.0
1 03/14/2218:44 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1 03/14/2218:44 124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1 03/14/2218:44 95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not
be reproduced, except in full,
Date: 03/25/2022 02:12 PM
without the written consent of Pace Analytical
Services, LLC. Page 14 of 36

aceAnalXical
w riv.pacelabs.corn
Project. STORMWATER
Pace Project No.: 92593091
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SDO-1
Lab ID: 92593091001 Collected: 03/09/22 08:50 Received:
03/11/22 12:51 Matrix: Water
Parameters
Results Units Report Limit
DF Prepared
Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA624.1
Pace Analytical Services - Charlotte
1,3-Dichlorobenzene
ND ug/L
2.0
1
03/1412218:44
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
03/14/22 18:44
106-46-7
1, 1 -Dichloroethane
ND ug/L
2.0
1
03/14/22 18:44
75-34-3
1,2-Dichloroethane
ND ug/L
2.0
1
0311412218:44
107-06-2
1, 1 -Dichloroethene
ND ug/L
2.0
1
03/14/22 18:44
75-35-4
cis- 1, 2-Dichloroethene
ND ug/L
2.0
1
03/14/22 18:44
156-59-2
tra ns- 1, 2-Dichloroethene
NO ug/L
2 0
1
03/14/22 18:44
156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1
03/14/22 18:44
78-87-5
cis- 1, 3-Dichloropropene
ND ug/L
2.0
1
03/14/22 18:44
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
2.0
1
03114/2218:44
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
03/14/22 18:44
100-41-4
Methylene Chloride
ND ug/L
2.0
1
03/14/22 18:44
75-09-2
1,1,2,2-Tetrachloroethane
NO ug/L
2.0
1
03/14/22 18:44
79-34-5
Tetrachloroethene
ND ug/L
2.0
1
03/14/22 18:44
127-18-4
Toluene
ND ug/L
1.0
1
03/14/22 18:44
108-88-3
1, 1, 1 -Trichloroethane
ND ug/L
20
1
03/14/22 18:44
71-55-6
1.1,2-Trichloroethane
ND ug/L
2.0
1
03/14/22 18:44
79-00-5
Trichloroethene
4.1 ug/L
2.0
1
03/14/22 18:44
79-01-6
Trichlorofluoromethane
NO ug/L
2.0
1
03/14/22 18:44
75-69-4
Vinyl chloride
ND ug/L
2.0
1
03/14/22 18:44
75-01-4
Surrogates
4-Bromofluorobenzene (S)
101 %
70-130
1
03/14/22 18:44
460-00-4
Toluene-d8 (S)
107 %
70-130
1
03/14/22 18:44
2037-26-5
1,2-Dichloroethane-d4 (S)
87 %
70-130
1
03/14/22 18:44
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services -Asheville
Total Suspended Solids
10.0 mg/L
2.5
1
03/12/22 10:57
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.4 Std. Units
0.10
1
03/14/22 12:52
H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
31.1 mg/L
25.0
1 03/19/22 00:51
03/19/22 04:42
M1
Date: 03/25/2022 02:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 36

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92593091
Sample: SDO-2
Lab ID: 92593091002 Collected:
03/09/22 09:00 Received: 03/11/22 12:51 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Assa Abloy
1
03/09/22 09:00
Collected By
Jacob Bill
1
03/09/22 09:00
Collected Date
03/09/22
1
03/09/22 09:00
Collected Time
09:00
1
03/09/22 09:00
pH
7.4
Std. Units
1
03/09/22 09:00
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND
mg/L
4.8
1
03/14/22 10:09
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
7.9
ug/L
5.0
1
03/15/22 0129 03/15/22 12:57 7440-50-8
Lead
ND
ug/L
5.0
1
03/15/22 03:29 03/15/22 12:57 7439-92-1
Zinc
47.0
ug/L
10.0
1
03/15/22 03:29 03/15/22 12:57 7440-66-6
625 RVE
Analytical Method:
EPA 625.1 Preparation
Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 83-32-9
Acenaphthylene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 208-96-8
Anthracene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 120-12-7
Benzo(a)anthracene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 56-55-3
Benzo(a)pyrene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 191-24-2
Benzo(k)fluoranthene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 101-55-3
Butylbenzylphthalate
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 85-68-7
4-Chloro-3-methylphenol
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 111-44-4
2-Chloronaphthalene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 91-58-7
2-Chlorophenol
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 7005-72-3
Chrysene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 218-01-9
Dibenz(a,h)anthracene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 91-94-1
2,4-Dichlorophenol
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 120-83-2
Diethylphthalate
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 105-67-9
Dimethylphthalate
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 131-11-3
Di-n-butylphthalate
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
1
03/16/22 05:50 03/17/22 03:48 51-28-5
2,4-Dinitrotoluene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 121-14-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 36

it
PaceAnalytical
wwa.pacelabsxom
ANALWICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92593091
Sample: SDO-2
Lab ID: 92593091002 Collected: 03/09/22 09:00 Received: 03/11/22 12:51 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 606-20-2
Di-n-octylphthalate
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 117-81-7
Fluoranthene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 206-44-0
Fluorene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 87-68-3
Hexachlorobenzene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 77-47-4
Hexachloroethane
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.2
1
03116/2205:50 03/17/22 03:48 193-39-5
Isophorone
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 78-59-1
Naphthalene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 91-20-3
Nitrobenzene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 98-95-3
2-Nitrophenol
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 88-75-5
4-Nitrophenol
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 621-64-7
N-Nitrosodiphenylamine
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 108-60-1
Pentachlorophenol
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 87-86-5
Phenanthrene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 85-01-8
Phenol
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 108-95-2
Pyrene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
4.2
1
03/16/22 05:50 03/17/22 03:48 120-82-1
2,4,6-Trichlorophenol
ND
ug/L
8.3
1
03/16/22 05:50 03/17/22 03:48 88-06-2
Surrogates
Nitrobenzene-d5 (S)
31
%
10-120
1
03/16/22 05:50 03/17/22 03:48 4165-60-0
2-Fluorobiphenyl (S)
27
%
15-120
1
03/16/22 05:50 03/17/22 03:48 321-60-8
Terphenyl-d14 (S)
59
%
11-131
1
03/16/22 05:50 03/17/22 03:48 1718-51-0
Phenol-d6 (S)
19
%
10-120
1
03/16/22 05:50 03/17/22 03:48 13127-88-3
2-Fluorophenol (S)
24
%
10-120
1
03/16/22 05:50 03/17/22 03:48 367-12-4
2,4,6-Tribromophenol (S)
53
%
10-137
1
03/16/22 05:50 03/17/22 03:48 118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
1.0
1
03/14/22 19:02 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
03/14/22 19:02 75-27-4
Bromoform
ND
ug/L
2.0
1
03/14/22 19:02 75-25-2
Bromomethane
ND
ug/L
2.0
1
03/14/22 19:02 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
03/14/22 19:02 56-23-5
Chforobenzene
ND
ug/L
2.0
1
03114/2219:02 108-90-7
Chloroethane
ND
ug/L
2.0
1
03/14/22 19:02 75-00-3
Chloroform
ND
ug/L
2.0
1
03/14/22 19:02 67-66-3
Chloromethane
ND
ug/L
2.0
1
03/14/22 19:02 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
03/14/22 19:02 124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
03/14/22 19:02 95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 36

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92593091
Sample: SDO-2
Lab ID: 92593091002 Collected: 03109/22 09:00 Received:
03/11/22 12:51 Matrix: Water
Parameters
Results Units Report Limit
DF Prepared
Analyzed CAS No. Qua]
624 Volatile Organics
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
1,3-Dichlorobenzene
ND ug/L
2.0
1
03/14/22 19:02 541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
03/14/22 19:02 106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
03/14/22 19:02 75-34-3
1.2-Dichloroethane
ND ug/L
2.0
1
03/14/22 19:02 107-06-2
1, 1 -Dichloroethene
ND ug/L
2.0
1
03/14/22 19:02 75-35-4
cis- 1, 2-Dichloroethene
ND ug/L
2.0
1
03114/2219:02 156-59-2
trans-1,2-Dichloroethene
ND ug/L
2.0
1
03/14/22 19:02 156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1
03/14/22 19:02 78-87-5
cis-1,3-Dichloropropene
ND ug/L
2.0
1
03/14/22 19:02 10061-01-5
trans- 1, 3-Dichloropropene
ND ug/L
2.0
1
03/14/22 19:02 10061-02-6
Ethylbenzene
ND ug/L
1.0
1
03/14/22 19:02 100.41-4
Methylene Chloride
ND ug/L
2.0
1
03/14/22 19:02 75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
2.0
1
03/14/22 19:02 79-34-5
Tetrachloroethene
ND ug/L
2.0
1
03/14/22 19:02 127-18-4
Toluene
ND ug/L
1.0
1
03/14/22 19:02 108-88-3
1. 1. 1 -Trichloroethane
ND ug/L
2.0
1
03/14/22 19:02 71-55-6
1,1,2-Trichloroethane
ND ug/L
2.0
1
03/14/22 19:02 79-00-5
Trichloroethene
ND ug/L
2.0
1
03/14/22 19:02 79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1
03/14/22 19:02 75-69-4
Vinyl chloride
ND ug/L
2.0
1
03/14/22 19:02 75-01-4
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
03/14/22 19:02 460-00-4
Toluene-d8 (S)
103 %
70-130
1
03/14/22 19:02 2037-26-5
1,2-Dichloroethane-d4 (S)
86 %
70-130
1
03/14/22 19:02 17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D-2015
Pace Analytical Services -Asheville
Total Suspended Solids
5.0 mg/L
2.5
1
03/12/22 10:58
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.4 Std. Units
0.10
1
03/14/22 12:55 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2611
Pace Analytical Services -Asheville
Chemical Oxygen Demand
28.8 mg/L
25.0
1 03/19/22 00:51
03/19/22 04:43
Date: 03/25/2022 02:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 36

leAnalytical
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QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
QC Batch: 684368 Analysis Method- EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593091001, 92593091002
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
METHOD BLANK: 3579310
Matrix: Water
Associated Lab Samples: 92593091001, 92593091002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 5.0
03/14/22 10:09
LABORATORY CONTROL SAMPLE:
3579311
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 13.6
68
64-132
MATRIX SPIKE SAMPLE:
3579312
35702424001 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
4.8U 19.2
10.7
40 64-132 M1
SAMPLE DUPLICATE: 3579313
35702306002 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Total Petroleum Hydrocarbons
mg/L
4.9U ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 0212 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 36

/JceAna/j6ca1'
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I
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92593091
QC Batch: 684672
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92593091001, 92593091002
METHOD BLANK: 3580573
Matrix: Water
Associated Lab Samples: 92593091001, 92593091002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Copper ug/L
ND 5.0
03/15/2212:41
Lead ug/L
ND 5.0
03/15/2212:41
Zinc ug/L
ND 10.0
03/15/2212:41
LABORATORY CONTROL SAMPLE: 3580574
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Copper ug/L
500 493
99 85-115
Lead ug/L
500 462
92 85-115
Zinc ug/L
500 471
94 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3580575 3580576
MS MSD
92593091001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc Result
Result % Rec % Rec
Limits RPD Qual
Copper ug/L 6.4
500 500 492
493 97 97
70-130 0
Lead ug/L ND
500 500 467
461 93 92
70-130 1
Zinc ug/L 709
500 500 552
546 96 95
70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 36

l aced ialyfical
werv.pacelabs,com
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
UU batch: 684527 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593091001, 92593091002
METHOD BLANK: 3579933
Associated Lab Samples: 92593091001, 92593091002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
03/14/22 14:50
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
03/1412214:50
1,1,2-Trichloroethane
ug/L
ND
2.0
03/1412214:50
1, 1 -Dichloroethane
ug/L
ND
2.0
03/14/22 14:50
1, 1 -Dichloroethene
ug/L
ND
2.0
03/14/22 14:50
1,2-Dichlorobenzene
ug/L
ND
2.0
03/1412214:50
1,2-Dichloroethane
ug/L
ND
2.0
03/14/22 14:50
1,2-Dichloropropane
ug/L
ND
2.0
03/14/22 14:50
1,3-Dichlorobenzene
ug/L
ND
2.0
03/14/22 14:50
1,4-Dichlorobenzene
ug/L
ND
2.0
03/14/22 14:50
Benzene
ug/L
ND
1.0
03/14/22 14:50
Bromodichloromethane
ug/L
ND
2.0
03/14/22 14:50
Bromoform
ug/L
ND
2.0
03/14/22 14:50
Bromomethane
ug/L
ND
2.0
03/14/22 14:50
Carbon tetrachloride
ug/L
ND
2.0
03/14/22 14:50
Chlorobenzene
ug/L
ND
2.0
03/14/22 14:50
Chloroethane
ug/L
ND
2.0
03/14/22 14:50
Chloroform
ug/L
ND
2.0
03/14/22 14:50
Chloromethane
ug/L
ND
2.0
03/14/22 14:50
cis- 1, 2-Dichloroethene
ug/L
ND
2.0
03/14/22 14:50
cis-1,3-Dichloropropene
ug/L
ND
2.0
03/14/22 14:50
Dibromochloromethane
ug/L
ND
2.0
03/14/22 14:50
Ethylbenzene
ug/L
ND
1.0
03114/2214:50
Methylene Chloride
ug/L
ND
2.0
03/14/22 14:50
Tetrachloroethene
ug/L
ND
2.0
03/14/22 14:50
Toluene
ug/L
ND
1.0
03/14/22 14:50
trans-1,2-Dichloroethene
ug/L
ND
2.0
03/14/22 14:50
trans-1,3-Dichloropropene
ug/L
ND
2.0
03/14/22 14:50
Trichloroethene
ug/L
ND
2.0
03/14/2214,50
Trichlorofiuoromethane
ug/L
ND
2.0
03/14/22 14:50
Vinyl chloride
ug/L
ND
2.0
03/14/22 14:50
1,2-Dichloroethane-d4 (S)
%
88
70-130
03/14/22 14:50
4-Bromofluorobenzene (S)
%
100
70-130
03/14/22 14:50
Toluene-d8 (S)
%
105
70-130
03/14/22 14:50
LABORATORY CONTROL SAMPLE: 3579934
Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1. 1, 1 -Trichloroethane ug/L 20 20.8 104 70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC-
Page 21 of 36

Vt+jjli. yl l�
aCeAnal tical
vnw.pacelabs.coln
Project: STORMWATER
Pace Project No.: 92593091
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
3579934
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits
Qualifiers
1,1,2,2-Tetrachloroethane
ug/L
20
20.0
100
70-130
1,1,2-Trichloroethane
ug/L
20
18.8
94
70-130
1, 1 -Dichloroethane
ug/L
20
21.6
108
70-130
1, 1 -Dichloroethene
ug/L
20
20.3
102
70-132
1,2-Dichlorobenzene
ug/L
20
21.0
105
70-130
1,2-Dichloroethane
ug/L
20
21.7
108
70-130
1,2-Dichloropropane
ug/L
20
21.2
106
70-130
1,3-Dichlorobenzene
ug/L
20
21.2
106
70-130
1,4-Dichlorobenzene
ug/L
20
20.9
104
70-130
Benzene
ug/L
20
20.4
102
70-130
Bromodichloromethane
ug/L
20
19.7
99
70-130
Bromoform
ug/L
20
19.0
95
70-130
Bromomethane
ug/L
20
29.1
146
30-177
Carbon tetrachloride
ug/L
20
21.2
106
70-130
Chlorobenzene
ug/L
20
20.3
101
70-130
Chloroethane
ug/L
20
21.0
105
46-131
Chloroform
ug/L
20
20.6
103
70-130
Chloromethane
ug/L
20
21.9
110
49-130
cis- 1, 2-Dichloroethene
ug/L
20
20.9
105
70-130
cis-1,3-Dichloropropene
ug/L
20
21.1
105
70-130
Dibromochloromethane
ug/L
20
18.1
90
70-130
Ethylbenzene
ug/L
20
19.2
96
70-130
Methylene Chloride
ug/L
20
20.7
104
68-130
Tetrachloroethene
ug/L
20
19.5
97
70-130
Toluene
ug/L
20
20.5
102
70-130
trans-1,2-Dichloroethene
ug/L
20
21.4
107
70-130
trans-1,3-Dichloropropene
ug/L
20
19.8
99
70-130
Trichloroethene
ug/L
20
20.3
102
70-130
Trichlorofluoromethane
ug/L
20
19.2
96
61-130
Vinyl chloride
ug/L
20
211
106
59-142
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
95
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE
3579935
3579936
MS
MSD
92592830002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1, 1, 1 -Trichloroethane
ug/L
ND
20
20
24.5
23.5
123
117
70-148
4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.3
22.0
111
110
70-131
1
1,1,2-Trichloroethane
ug/L
ND
20
20
219
20.3
110
101
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
25.6
24.2
128
121
71-143
5
1,1-Dichloroethene
ug/L
ND
20
20
23.4
22.0
117
110
70-158
6
1,2-Dichlorobenzene
ug/L
ND
20
20
23.6
22.1
118
110
70-133
7
1,2-Dichloroethane
ug/L
ND
20
20
24.0
23.0
120
115
72-137
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02 12 PM without the written consent of Pace Analytical Services, LLC, Page 22 of 36

11
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
aceAnalj cal Huntersville, NC 28078
wvnv.pacelabs.com [phone]
QUALITY CON`mol_ DATA
Project: STORMWATER
Pace Project No.: 92593091
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3579935
3579936
MS
MSD
92592830002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2-Dichloropropane
ug/L
ND
20
20
24.3
23.6
122
118
70-138
3
1,3-Dichlorobenzene
ug/L
ND
20
20
23.3
22.7
117
113
75-133
3
IA-Dichlorobenzene
ug/L
ND
20
20
22.7
21.7
113
109
70-133
4
Benzene
ug/L
ND
20
20
23.6
21.3
118
107
75-125
10
Bromodichloromethane
ug/L
ND
20
20
24.0
22.3
116
108
70-138
7
Bromoform
ug/L
ND
20
20
20.9
21.1
104
106
57-138
1
Bromomethane
ug/L
4.0
20
20
34.5
31.5
152
137
10-200
9
Carbon tetrachloride
ug/L
ND
20
20
24.5
22.8
123
114
70-125
7
Chlorobenzene
ug/L
ND
20
20
22.8
22.8
111
111
82-137
0
Chloroethane
ug/L
ND
20
20
ND
ND
0
0
51-166
M1
Chloroform
ug/L
4.1
20
20
28.5
27.7
122
118
70-121
3 M1
Chloromethane
ug/L
ND
20
20
ND
ND
0
0
24-161
M1
cis- 1,2-Dichloroethene
ug/L
ND
20
20
25.2
23.4
126
117
67-148
7
cis- 1, 3-Dichloropropene
ug/L
ND
20
20
24.0
22.1
120
111
70-142
8
Dibromochloromethane
ug/L
ND
20
20
19.8
19.0
99
95
69-133
4
Ethylbenzene
ug/L
ND
20
20
21.4
21.5
107
107
75-134
0
Methylene Chloride
ug/L
ND
20
20
24.3
22.8
121
114
64-148
6
Tetrachloroethene
ug/L
ND
20
20
21.1
213
105
106
70-133
1
Toluene
ug/L
ND
20
20
22.9
21.9
114
109
75-134
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.5
24.0
122
120
70-143
2
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.9
21.3
115
107
70-138
7
Trichloroethene
ug/L
ND
20
20
23.0
20.9
115
105
75-138
10
Trichlorofluoromethane
ug/L
ND
20
20
21.4
20.6
107
103
61-154
4
Vinyl chloride
ug/L
ND
20
20
14.0
15.6
70
78
55-172
11
1,2-Dichloroethane-d4 (S)
%
99
103
70-130
4-Bromofluorobenzene (S)
%
97
101
70-130
Toluene-d8 (S)
%
105
104
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 36

aceAnalytical
www.pacelabs.com
Project:
Pace Project No.:
QC Batch:
QC Batch Method:
STORMWATER
92593091
684999
EPA 625.1
Associated Lab Samples: 92593091001, 92593091002
QUALITY CONTROL DATA
Analysis Method EPA 625.1
Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 3582048
Associated Lab Samples: 92593091001, 92593091002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
03116/2215:47
2,2'-Oxybis(1-chloropropane)
ug/L
NO
5.0
03/16/22 15:47
2,4,6-Trichlorophenol
ug/L
NO
10.0
03/16/22 15:47
2,4-Dichlorophenol
ug/L
NO
5.0
03/16/22 15:47
2,4-Dimethylphenol
ug/L
NO
10.0
03/16/22 15:47
2,4-Dinitrophenol
ug/L
NO
%0
03/16/22 15:47
2,4-Dinitrotoluene
ug/L
NO
5.0
03/16/22 15:47
2,6-Dinitrotoluene
ug/L
NO
5.0
03/16/22 15:47
2-Chloronaphthalene
ug/L
NO
5.0
03/16/22 15:47
2-Chlorophenol
ug/L
ND
5.0
03/16/22 15:47
2-Nitrophenol
ug/L
NO
5.0
03/16/22 15:47
3,3'-Dichlorobenzidine
ug/L
NO
10.0
03/16/22 15:47
4,6-Dinitro-2-methylphenol
ug/L
NO
10.0
03/16/22 15:47
4-Bromophenylphenyl ether
ug/L
NO
5.0
03/16/22 15:47
4-Chloro-3-methylphenol
ug/L
NO
5.0
03/16/22 15:47
4-Chlorophenylphenyl ether
ug/L
NO
5.0
03/16/22 15:47
4-Nitrophenol
ug/L
NO
10.0
03/16/22 15:47
Acenaphthene
ug/L
ND
5.0
03/16/22 15:47
Acenaphthylene
ug/L
NO
5.0
03/16/22 15:47
Anthracene
ug/L
NO
5.0
03/16/22 15:47
Benzo(a)anthracene
ug/L
NO
5.0
03/16/22 15:47
Benzo(a)pyrene
ug/L
NO
5.0
03/16/22 15:47
Benzo(b)fluoranthene
ug/L
ND
5.0
03/1612215:47
Benzo(g,h,i)perylene
ug/L
NO
5.0
03/16/22 15:47
Benzo(k)fluoranthene
ug/L
NO
5.0
03/16/22 15:47
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
03/16/22 15:47
bis(2-Chloroethyl) ether
ug/L
NO
5.0
03/16/22 15:47
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
03/16/22 15:47
Butylbenzylphthalate
ug/L
ND
5.0
03/16/2215:47
Chrysene
ug/L
NO
5.0
03/16/22 15:47
Di- n-butylphthalate
ug/L
ND
5.0
03/16/22 15:47
Di-n-octylphthalate
ug/L
NO
5.0
03/16/22 15:47
Dibenz(a,h)anthracene
ug/L
ND
5.0
03/16/22 15:47
Diethylphthalate
ug/L
NO
5.0
03/16/22 15:47
Dimethylphthalate
ug/L
NO
5.0
03/16/22 15:47
Fluoranthene
ug/L
ND
5.0
03/16/22 15:47
Fluorene
ug/L
NO
5.0
03/16/22 15:47
Hexachloro-1,3-butadiene
ug/L
NO
5.0
03/16/22 15:47
Hexachlorobenzene
ug/L
NO
5.0
03/16/22 15:47
Hexachlorocyclopentadiene
ug/L
NO
10.0
03/16/22 15:47
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02A2 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 36

t t.
aceAnalytical
wmv.imcelahs.com
(QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
METHOD BLANK: 3582048 Matrix: Water
Associated Lab Samples: 92593091001, 92593091002
Parameter
Units
Hexachloroethane
ug/L
Indeno(1,2,3-cd)pyrene
ug/L
Isophorone
ug/L
N-Nitroso-di-n-propylamine
ug/L
N-Nitrosodimethylamine
ug/L
N-Nitrosodiphenylamine
ug/L
Naphthalene
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Phenanthrene
ug/L
Phenol
ug/L
Pyrene
ug/L
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Blank
Result
Reporting
Limit
Analyzed
ND
5.0
03/16/2215:47
ND
5.0
03/16/2215:47
ND
10.0
03/16/2215:47
ND
5.0
03/16/2215:47
ND
5.0
03/16/2215:47
ND
10.0
03116/2215:47
ND
5.0
03/1612215:47
ND
5.0
03/1612215:47
ND
10.0
03/16/2215:47
ND
5.0
03/16/2215:47
ND
5.0
03/16/2215:47
ND
5.0
03/16/2215:47
104
10-137
03/16/2215:47
83
15-120
03/16/2215:47
74
10-120
03/16/2215:47
94
10-120
03/16/2215:47
56
10-120
03/16/2215:47
108
11-131
03/ 16/22 15:47
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3582049
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
29.3
59
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
44.5
89
36-166
2,4,6-Trichlorophenol
ug/L
50
46.9
94
37-144
2,4-Dichlorophenol
ug/L
50
45.4
91
1-191
2,4-Dimethylphenol
ug/L
50
51.8
104
32-119
2,4-Dinitrophenol
ug/L
250
82.8
33
1-181
2,4-Dinitrotoluene
ug/L
50
49.0
98
39-139
2,6-Dinitrotoluene
ug/L
50
47.6
95
50-158
2-Chloronaphthalene
ug/L
50
35.2
70
60-118
2-Chlorophenol
ug/L
50
45.7
91
23-134
2-Nitrophenol
ug/L
50
53.6
107
29-182
3,3'-Dichlorobenzidine
ug/L
100
82.6
83
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
114
114
1-181
4-Bromophenylphenyl ether
ug/L
50
42.0
84
53-127
4-Chloro-3-methylphenol
ug/L
100
101
101
22-147
4-Chlorophenylphenyl ether
ug/L
50
40.5
81
25-158
4-Nitrophenol
ug/L
250
147
59
1-132
Acenaphthene
ug/L
50
40.7
81
47-145
Acenaphthylene
ug/L
50
404
81
33-145
Anthracene
ug/L
50
43.5
87
1-166
Benzo(a)anthracene
ug/L
50
46.3
93
33-143
Benzo(a)pyrene
ug/L
50
45.3
91
17-163
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 36

aceAnalj6cal9
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
LABORATORY CONTROL SAMPLE:
Parameter
3582049
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(b)fluoranthene
ug/L
50
45.3
91
24-159
Benzo(g,h,i)perylene
ug/L
50
36.7
73
1-219
Benzo(k)fluoranthene
ug/L
50
45.7
91
11-162
bis(2-Chloroethoxy)methane
ug/L
50
46.4
93
33-184
bis(2-Chloroethyl) ether
ug/L
50
47.2
94
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
54.6
109
8-158
Butylbenzylphthalate
ug/L
50
57.3
115
1-152
Chrysene
ug/L
50
46.0
92
17-168
Di-n-butylphthalate
ug/L
50
48.2
96
1-118
Di-n-octylphthalate
ug/L
50
54.2
108
4-146
Dibenz(a,h)anthracene
ug/L
50
37.9
76
1-227
Diethylphthalate
ug/L
50
46.8
94
1-114
Dimethylphthalate
ug/L
50
44.1
88
1-112
Fluoranthene
ug/L
50
42.7
85
26-137
Fluorene
ug/L
50
43.3
87
59-121
Hexachloro-1,3-butadiene
ug/L
50
25.7
51
24-116
Hexachlorobenzene
ug/L
50
39.9
80
1-152
Hexachlorocyclopentadiene
ug/L
50
25.8
52
25-150
Hexachloroethane
ug/L
50
30.6
61
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
36.5
73
1-171
Isophorone
ug/L
50
46.5
93
21-196
N-Nitroso-di-n-propylamine
ug/L
50
49.1
98
1-230
N-Nitrosodimethylamine
ug/L
50
42.1
84
25-150
N-Nitrosodiphenylamine
ug/L
50
45.0
90
25-150
Naphthalene
ug/L
50
35.2
70
21-133
Nitrobenzene
ug/L
50
43.7
87
35-180
Pentachlorophenol
ug/L
100
107
107
14-176
Phenanthrene
ug/L
50
44.5
89
54-120
Phenol
ug/L
50
36.9
74
5-112
Pyrene
ug/L
50
49.6
99
52-115
2,4,6-Tribromophenol (S)
%
119
10-137
2-Fluorobiphenyl (S)
%
89
15-120
2-Fluorophenol(S)
%
92
10-120
Nitrobenzene-d5 (S)
%
107
10-120
Phenol-d6 (S)
%
77
10-120
Terphenyl-d14 (S)
%
107
11-131
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3582050
3582051
MS
MSD
35703096001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
1.7U 50
50
29.1
35.1
58
70
44-142
19
2,2'-Oxybis(1-chloropropane)
ug/L
1.2U 50
50
32.5
37.4
65
75
36-166
14
2,4,6-Trichlorophenol
ug/L
1.61.1 50
50
41.4
52.1
83
104
37-144
23
2,4-Dichlorophenol
ug/L
1AU 50
50
43.8
52.2
88
104
1-191
18
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 36

aceAnalytical
w:,rw.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92593091
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3582050
3582051
MS
MSD
35703096001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
2,4-Dimethylphenol
ug/L
1.7U
50
50
41.7
49.5
83
99
32-119
17
2,4-Dinitrophenol
ug/L
26.OU
250
250
ND
41.8J
0
17
1-181
M1
2,4-Dinitrotoluene
ug/L
1.61.1
50
50
32.9
41.0
66
82
39-139
22
2,6-Dinitrotoluene
ug/L
1.7U
50
50
36.2
46.0
72
92
50-158
24
2-Chloronaphthalene
ug/L
1.7U
50
50
31.2
39.3
62
79
60-118
23
2-Chlorophenol
ug/L
1.2U
50
50
36.1
42.1
72
84
23-134
15
2-Nitrophenol
ug/L
1.4U
50
50
31.2
38.7
62
77
29-182
21
3,3'-Dichlorobenzidine
ug/L
8.1U
100
100
52.4
11.3
52
11
1-262
129 R1
4.6-Dinitro-2-methylphenol
ug/L
3.4U
100
100
ND
23.0
0
23
1-181
M1
4-Bromophenylphenyl ether
ug/L
1.8U
50
50
34.3
42.5
69
85
53-127
21
4-Chloro-3-methylphenol
ug/L
3.3U
100
100
91.0
111
91
111
22-147
20
4-Chlorophenylphenyl ether
ug/L
2.0U
50
50
34.8
43.6
70
87
25-158
23
4-Nitrophenol
ug/L
6.6U
250
250
57.8
138
23
55
1-132
82 R1
Acenaphthene
ug/L
2.OU
50
50
31.5
39.5
63
79
47-145
23
Acenaphthylene
ug/L
2.OU
50
50
35.0
43.0
70
86
33-145
20
Anthracene
ug/L
2.3U
50
50
31.7
39.4
63
79
1-166
22
Benzo(a)anthracene
ug/L
2.7U
50
50
34.8
42.5
70
85
33-143
20
Benzo(a)pyrene
ug/L
2.8U
50
50
32.3
38.3
65
77
17-163
17
Benzo(b)fluoranthene
ug/L
2.6U
50
50
30.7
36.7
61
73
24-159
18
Benzo(g,h,i)perylene
ug/L
2.8U
50
50
35.8
44.4
72
89
1-219
21
Benzo(k)fluoranthene
ug/L
2.7U
50
50
30.5
35.8
61
72
11-162
16
bis(2-Chloroethoxy)methane
ug/L
1.8U
50
50
34.9
41.7
70
83
33-184
18
bis(2-Chloroethyl) ether
ug/L
1.9U
50
50
35.4
43.8
71
88
12-158
21
bis(2-Ethyl hexyl)phthalate
ug/L
3.7U
50
50
35.6
42.5
71
85
8-158
18
Butylbenzylphthalate
ug/L
3.1U
50
50
37.8
44.2
76
88
1-152
16
Chrysene
ug/L
2.8U
50
50
33.9
40.9
68
82
17-168
19
Di-n-butylphthalate
ug/L
2.21_1
50
50
33.9
41.1
68
82
1.118
19
Di-n-octylphthalate
ug/L
3.9U
50
50
420
48.8
84
98
4-146
15
Dibenz(a,h)anthracene
ug/L
3.OU
50
50
35.2
43.7
70
87
1-227
22
Diethylphthalate
ug/L
2.OU
50
50
34.4
40.5
69
81
1-114
16
Dimethylphthalate
ug/L
2.1U
50
50
34.9
41.0
70
82
1-112
16
Fluoranthene
ug/L
2.2U
50
50
35.8
43.8
72
88
26-137
20
Fluorene
ug/L
2.1 U
50
50
33.7
41.9
67
84
59-121
22
Hexachloro-1,3-butadiene
ug/L
1.81_1
50
50
28.0
35.0
56
70
24-116
22
Hexachlorobenzene
ug/L
2.2U
50
50
30.6
37.4
61
75
1-152
20
Hexachlorocyclopentadiene
ug/L
1.6U
50
50
27.1
29.0
54
58
25-150
7
Hexachloroethane
ug/L
1.4U
50
50
24.8
32.2
50
64
40-113
26
Indeno(1,2,3-cd)pyrene
ug/L
2.9U
50
50
34.8
42.8
70
86
1-171
21
Isophorone
ug/L
1.7U
50
50
31A
37.6
63
75
21-196
18
N-Nitroso-di-n-propylamine
ug/L
1.3U
50
50
33.5
39.7
67
79
1-230
17
N-Nitrosodimethylamine
ug/L
1.9U
50
50
28.4
32.7
57
65
25-150
14
N-Nitrosodiphenylamine
ug/L
3.OU
50
50
34.3
41.0
69
82
25-150
18
Naphthalene
ug/L
2.1U
50
50
31.7
36.4
63
73
21-133
14
Nitrobenzene
ug/L
1.9U
50
50
33.0
38.5
66
77
35-180
16
Pentachlorophenol
ug/L
3.81.11
100
100
46.8
81.6
47
82
14-176
54 R1
Phenanthrene
ug/L
2.OU
50
50
32.0
39.9
64
80
54-120
22
Results presented on
this page are in the units indicated by the "Units" column
except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 36

,�anekia/ 'Cal
w,mN.pacelahs.com
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3582050
3582051
MS
MSD
35703096001
Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits RPD Qual
Phenol
ug/L
1.41-1 50
50 27.8
31.6
56
63
5-112 13
Pyrene
ug/L
2.2U 5G
50 34.3
41.5
69
83
52-115 19
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
88
101
10-137
2-Fluorophenol (S)
%
69
83
15-120
Nitrobenzene-d5 (S)
%
59
68
10-120
Phenol-d6 (S)
%
73
85
10-120
Terphenyl-d14 (S)
%
55
62
10-120
71
83
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date. 03/25//2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 36

acmnalytical
www.pacelabsxom
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
QC Batch: 684317 Analysis Method: SM 2540D-2015
QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92593091001, 92593091002
METHOD BLANK: 3579131 Matrix: Water
Associated Lab Samples: 92593091001, 92593091002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 03/12/22 10:54
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3579132
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 242 97 90-110
SAMPLE DUPLICATE: 3579168
92592695001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L ND ND
SAMPLE DUPLICATE: 3579169
92592702001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 16.5 15.5 6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 36

aceAnaIXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92593091
QC Batch: 684421 Analysis Method: SM 4500-H+B-2011
QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92593091001, 92593091002
SAMPLE DUPLICATE: 3579443
30468176002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.8 6.8 0 H3
SAMPLE DUPLICATE: 3579444
92593091002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Sid. Units 6.4 6.5 0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 36

leAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92593091
QC Batch: 685913
Analysis Method:
SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description:
5220D COD
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92593091001, 92593091002
METHOD BLANK: 3586684
Matrix: Water
Associated Lab Samples: 92593091001, 92593091002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0 03/19/22 04:38
LABORATORY CONTROL SAMPLE: 3586685
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 762
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3586686 3586687
MS MSD
92593091001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qua[
Chemical Oxygen Demand mg/L 31.1
100 100 149
144 118 113
90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3586688 3586689
MS MSD
92593358003
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 52.3
100 100 161
161 108 108
90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/25/2022 02:12 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 36

(�IaneAnalyfical
eivnv.pacelabs.com
QUALIFIERS
Project: STORMWATER
Pace Project No.: 92593091
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
Date: 03/25/2022 02:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 36

ac Mnalj4ical
www.pacelabs.com
Project: STORMWATER
Pace Project No.: 92593091
Lab ID
92593091001
92593091002
92593091001
92593091002
92593091001
92593091002
92593091001
92593091002
92593091001
92593091002
92593091001
92593091002
92593091001
92593091002
92593091001
92593091002
Sample ID
SDO.1
SDO-2
SDO-1
SDO-2
SDO.1
SDO-2
SDO-1
SDO.2
SDO-1
SDO-2
SDO-1
SDO-2
SDO-1
SDO-2
SDO-1
SDO-2
Date: 03/25/2022 02:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Analytical
QC Batch Method QC Batch Analytical Method Batch
EPA 16646
684368
EPA 1664E
684368
EPA 200.7 Rev 4.4 1994
684672
EPA 200.7 Rev 4.4 1994
684672
EPA 625.1
684999
EPA 625.1
684999
EPA 624.1
684527
EPA 624.1
684527
SM 2540D-2015
684317
SM 2540D-2015
684317
SM 4500-H+6-2011
684421
SM 4500-H+B-2011
684421
SM 5220D-2011
685913
SM 5220D-2011
685913
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4.4 1994 684707
EPA 200.7 Rev 4.4 1994 684707
EPA 625.1 685261
EPA 625A 685261
SM 5220D-2011 685928
SM 5220D-2011 685928
Page 33 of 36

. t.
Document Name: Document Revised: November 15, 2021
Sample Condition Upon Receipt SCUR) Page 1 of 2
aceAnalyfical _ Document No,: Issuing Authority:
F-CAR-CS-033-Rev.08 Pace Carolinas Quality Office
Laboratory receiving samples:
/Raleigh❑
Asheville ❑ Lden❑ Greenwood n Huntersville [l✓
Mechanicsvillen Atlanta❑ Kernersviile❑
Client Name:
Project
W(V91
k dt t
It:
Courier: ❑Fed Ex ❑UPS CUSPS
[]Client
❑ Commercial ❑Pace Pother:_
92593091
Custody Seal Present? ❑Yes ❑No Seals Intact? [-]Yes
❑No
Dale/Iritlals Person Examining Contents:__'
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None
❑ Other
Biological Tissue Frozen?
Thermometer:
Q IRGun to: y11. {. Gl l' [ ]]N/et
❑glue
[]Yes❑No ❑N/A
❑None
Type o(Ice:
t Correction Factor.
Cooler Temp: Add/Subtract VQ
Temp should be above freezing to VC
out of temp criteria. Samples an ice, cooling process
EoolerTemp Earrected ('C�. - - + - —
-[]Samples
--
"Ttlegun
USDA Regulated Soll (0 N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check
maps►?
old samples originate from a foreign source (internationally,
rIv.. MN.
i—I 11—W 1; —d 0...n. M-11 I-Ive. r7w.,
Comments Olscrepanc :
Chain of Custody Present?
- Yes
ONO
N/A
1.
Samples Arrived within Hold Time?
Yes
ONO
N/A
2.
Short Hold Time Analysts 02 hr.)?
Yes
fJo
N/A
3.
Rush Turn Around Time Requested?
❑Yes
•No
❑N/A
4.
Sufficient Volume?
Dyes
QNo
N/A
S.
Correct Containers Used?
-Pace Containers Used?
Oyes
Elie,
[]No
ONo
❑N/A
❑N/A
6.
Containers Intact?
Yes
No
NIA
7.
Dissolved analysis: Samples Feld Filtered?
❑Yes
❑No
. N/A
8,
Sample Labels Match COC?
-Includes Date ime/ID/Anal is Matrix:
❑6es
[ '-) I
[]No
❑N/A
9.
Heads ace in VOA Viats >S-6mm)?
Oyes
No
. N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑No
No
[ N/A .
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
vate/ I ime:
Project Manager SCURF Review: Date:
Project Manager SRF Review:
Oate:
Page 34 of 36

Document Name: Document Revised: November 15, 2021
A Sample Condition Upon Receipt iSCUR) Page 2 of 2
8C8f1R8lyfICr7j . ' Document Nb.: Issuing Authority:
F•CAR•CS•033•Rev.08 Pace Carolinas.Qualit Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coiiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Project a W0 : 92r593091
PM: TTH Due Date: 03/22/22
CLIEN'r: 82—Norton
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Sample ID
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pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot x
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a couv of u.0 "o..„
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 35 of 36

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Page 36 of 36