NCG030571_Monitoring Report_20220322 (2)

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000��i
Metal Fabrication �� t`40
Click here for instructions °ora4°�Fiy
Complete, sign, scan and submit the DMR via the Stormwater_NPDES Permit Data Mori itorin Re oft DMR load
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the @pgropnate DEMLR, I
Certificate of Coverage No. NCGO-30571 -
- B ;Person Collecting Samples Tommy Maness
Facility Name: Norton Door Controls Norton -- -
_ ( ) Laboratory Name. Pace Analytical
Facility County. Union - --
Laboratory Cert. No.: 5342
Discharge during this period: MY. No (if no, skip to signature and date)
v NoHasYour facility implemented mandat ter response actions this sample period for any benchmark exceedances?YesIf so, which Tier I, II, or III ? I
) 5 /Uicd-
1 up ocs de .nc ov Forms r i
A copy of this DMR has been uploaded electronically via hit ls,: ,SL-_cL g / fSW�bMR � Yes � No ;
Date Uploaded:
i
An Monitoring Requirements for Outfalls with Industrial Activities - Benchmarks In (Red)
Parameter
Code
Parameter
Outfall SD01
Outfall S002
Outfall SDO3 Outfall Outfall
N/A
_-_
Receiving Stream Class
C
C
C -
N/A
---
Date Sample Collected MM/DD/YYYY
05,119`2020
05l1912020
05/19202/
46529
24 Hour Rainfall in inches
023
023
023
C0530
TSS in mg/L (100 or 50')
4 7
45
11 3
00400
pH in standard units (6.0 9.0 FW,
-
6.8.8.5 SW)
n'a
nla
n!a
01119
Copper, total recoverable in mg/t
--
(0.010 FW, O.00S8 SW)
00099
j <0 005
00096
01051
Lead, total recoverable in mg/ L
(0.075 FW, 0.22 SW)
0 005
1<0005
<0 005 i
01094
Zinc, total recoverable in mg/ L (0.126
FW, 0.095 SW)
00764
00475
00176
00340
Chemical Oxygen Demand (COD) in
mg/L (120)
<25 0
1<25 0
<25 0
00552
Non Polar Oil & Grease in mg/L (15)
<5 0
<5 0
<5 0
'Out falls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and PrimaryNursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
i "I (Freshwater) Sav (Saltwater)
Notes (optional). TTO (78141) Benchmark 1 mg/L SDO 1 0 0021 mgll (Tnchloroethene). SD0 2 NO SD0 3 NO
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information including the possibility of fines and imprisonment for knowing violations "
Signat re of Perini tee or Delegated Authorized Indiv►dual Date
o han.Hunler@assaabloy com / 7o Y 3 3 / 5-5-6
Email Address Phone Number

aceAnalytical ID
www.pacelabs.com
June 03, 2020
Grace Herbert
Norton Door Controls
3000 Highway 74 East
Monroe, NC 28112
RE: Project: Stormwater
Pace Project No.: 92478444
Dear Grace Herbert:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Co�djy
��
�0- ,
Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jeff Duke, Assa Abloy
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 1 of 42

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aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Stormwater
92478444
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92478444001
SDO-1
EPA 1664B
WAM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 2540D-2011
RED
1
PASI-A
SM 5220D-2011
LMS1
1
PASI-A
92478444002
SDO-2
EPA 1664E
WAM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 254OD-2011
RED
1
PASI-A
SM 5220D-2011
LMS1
1
PASI-A
92478444003
SDO-3
EPA 1664E
WAM
1
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 2540D-2011
RED
1
PASI-A
SM 5220D-2011
LMS1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 42

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(�Iacmnalyfical'
www.pacelahsxom
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92478444
Method: EPA 1664E
Description: 1664 SGT-HEM, TPH
Client: Norton Door Controls
Date: June 03, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 1664E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 42

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ceAnalytical
www.pacelabs.com
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92478444
Method: EPA 625.1
Description: 625 RVE
Client: Norton Door Controls
Date: June 03, 2020
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 625.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 542827
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92469531022
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MSD (Lab ID: 2891656)
• 2-Chloronaphthalene
R1: RPD value was outside control limits.
• MSD (Lab ID: 2891656)
• 2,4-Dichlorophenol
• 2-Chloronaphthalene
• Acenaphthene
• Hexachloro-1,3-butadiene
• Hexachlorocyclopentadiene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 42

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aceAnaIXical
www.pacelabs.com
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92478444
Method: EPA 624.1
Description: 624 Volatile Organics
Client: Norton Door Controls
Date: June 03, 2020
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 624.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 544278
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92478444001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MSD (Lab ID: 2898578)
• Carbon tetrachloride
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 42

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ceAnalytical
www.pacelabs.com
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92478444
Method: SM 5220D-2011
Description: 5220D COD
Client: Norton Door Controls
Date: June 03, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 700
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for SM 5220D-2011 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with SM 5220D-2011 with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 542945
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92478352001,92478389001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2892349)
• Chemical Oxygen Demand
• MS (Lab ID: 2892351)
• Chemical Oxygen Demand
• MSD (Lab ID: 2892350)
• Chemical Oxygen Demand
• MSD (Lab ID: 2892352)
• Chemical Oxygen Demand
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 42

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aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater
Pace Project No.: 92478444
Sample: SDO-1
Lab ID: 92478444001 Collected: 05/19/20 18:00 Received: 05/20/20 13:36 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed CAS No. Qua]
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Hexachloroethane
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 193-39-5
Isophorone
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 13:42 78-59-1
Naphthalene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 91-20-3
Nitrobenzene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 13:42 100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
05/21/20 21:06 05/26/20 13:42 86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 13:42 87-86-5
Phenanthrene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 85-01-8
Phenol
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 108-95-2
Pyrene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 13:42 120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 13:42 88-06-2
Surrogates
Nitrobenzene-d5 (S)
88
%
10-120
1
05/21/20 21:06 05/26/20 13:42 4165-60-0
2-Fluorobiphenyl (S)
74
%
15-120
1
05/21/20 21:06 05/26/20 13:42 321-60-8
Terphenyl-d14 (S)
110
%
11-131
1
05/21/20 21:06 05/26/20 13:42 1718-51-0
Phenol-d6 (S)
48
%
10-120
1
05/21/20 21:06 05/26/20 13:42 13127-88-3
2-Fluorophenol (S)
66
%
10-120
1
05/21/20 21:06 05/26/20 13:42 367-12-4
2,4,6-Tribromophenol (S)
74
%
10-137
1
05/21/20 21:06 05/26/20 13:42 118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
1.0
1
05/30/2014:32 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
05/30/2014:32 75-27-4
Bromoform
ND
ug/L
2.0
1
05/30/2014:32 75-25-2
Bromomethane
ND
ug/L
2.0
1
05/30/2014:32 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
05/30/20 14:32 56-23-5 M1
Chlorobenzene
ND
ug/L
2.0
1
05/30/2014:32 108-90-7
Chloroethane
ND
ug/L
2.0
1
05/30/2014:32 75-00-3
Chloroform
ND
ug/L
2.0
1
05/30/2014:32 67-66-3
Chloromethane
ND
ug/L
2.0
1
05/30/2014:32 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
05/30/2014:32 124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
05/30/2014:32 95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
05/30/2014:32 541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
05/30/2014:32 106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
05/30/2014:32 75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
05/30/2014:32 107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
05/30/2014:32 75-35-4
cis- 1, 2-Dichloroethene
ND
ug/L
2.0
1
05/30/2014:32 156-59-2
trans- 1,2-Dichloroethene
ND
ug/L
2.0
1
05/30/2014:32 156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
05/30/2014:32 78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 42

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aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater
Pace Project No.: 92478444
Sample: S130-2 Lab ID: 92478444002 Collected: 05/19/20 18:15 Received: 05/20/20 13:36 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND
mg/L
5.0
1
05/26/20 10:46
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND
ug/L
5.0
1
05/28/20 01:42 06/01/20 14:48 7440-50-8
Lead
ND
ug/L
5.0
1
05/28/20 01:42 06/01/20 14:48 7439-92-1
Zinc
47.5
ug/L
10.0
1
05/28/20 01:42 06/01/20 14:48 7440-66-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 83-32-9
Acenaphthylene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 208-96-8
Anthracene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 59-50-7
bi s(2-Ch loroethoxy) methane
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 14:07 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 95-57-8
4-Chlorophenylphenylether
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 7005-72-3
Chrysene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 14:07 91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 120-83-2
Diethylphthalate
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 14:07 105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 14:07 534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/21/20 21:06 05/26/20 14:07 51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 117-81-7
Fluoranthene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 206-44-0
Fluorene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
05/21/20 21:06 05/26/20 14:07 118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/21/20 21:06 05/26/20 14:07 77-47-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 42

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Pace Analytical Services, LLC
1eAnai(Vfical 9800Kincey Ave. te 100
Hunte svlle, NC'28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Stormwater
Pace Project No.: 92478444
Sample: SDO-2
Lab ID: 92478444002 Collected:
05/19/20 18:15
Received: 05/20/20 13:36 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA624.1
Pace Analytical Services - Charlotte
cis- 1, 3-Dichloropropene
ND ug/L
2.0
1
05/30/20 14:50 10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
2.0
1
05130/2014:50 10061-02-6
Ethylbenzene
ND ug/L
1.0
1
05/30/20 14:50 100-41-4
Methylene Chloride
ND ug/L
2.0
1
05/30/20 14:50 75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
2.0
1
05/30/20 14:50 79-34-5
Tetrachloroethene
ND ug/L
2.0
1
05/30/20 14:50 127-18-4
Toluene
ND ug/L
1.0
1
05/30/20 14:50 108-88-3
1, 1, 1 -Trichloroethane
ND ug/L
2.0
1
05/30/20 14:50 71-55-6
1,1,2-Trichloroethane
ND ug/L
2.0
1
05/30/20 14:50 79-00-5
Trichloroethene
ND ug/L
2.0
1
05/30/20 14:50 79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1
05/30/20 14:50 75-69-4
Vinyl chloride
ND ug/L
2.0
1
05/30/20 14:50 75-01-4
Surrogates
4-Bromofluorobenzene (S)
106 %
70-130
1
05/30/20 14:50 460-00-4
Toluene-d8 (S)
104 %
70-130
1
05/30/20 14:50 2037-26-5
1,2-Dichloroethane-d4 (S)
116 %
70-130
1
05/30/20 14:50 17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Asheville
Total Suspended Solids
4.5 mg/L
2.5
1
05/22/20 18:17
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg/L
25.0
1
05/21/20 17:00 05/22/20 15:57
Date: 06/03/2020 02A0 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 42

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0
Pace Analytical Services, LLC
PlaceAnalytical 9800 Kincey Ave. Suite 100
www.pacelahs.com Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Stormwater
Pace Project No.: 92478444
Sample: SDO-3
Lab ID: 92478444003 Collected: 05/19/20 18:30 Received: 05/20/20 13:36 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Hexachloroethane
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 193-39-5
Isophorone
ND
ug/L
10.0
1
05/22/20 11:08
05/23/20 20:38 78-59-1
Naphthalene
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 91-20-3
Nitrobenzene
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
05/22/20 11:08
05/23/20 20:38 100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/22/20 11:08
05/23/20 20:38 86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
05/22/20 11:08
05/23/20 20:38 87-86-5
Phenanthrene
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 85-01-8
Phenol
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 108-95-2
Pyrene
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
05/22/20 11:08
05/23/20 20:38 120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/22/20 11:08
05/23/20 20:38 88-06-2
Surrogates
Nitrobenzene-d5 (S)
49
%
10-120
1
05/22/20 11:08
05/23/20 20:38 4165-60-0
2-Fluorobiphenyl (S)
45
%
15-120
1
05/22/20 11:08
05/23/20 20:38 321-60-8
Terphenyl-d14 (S)
90
%
11-131
1
05/22/20 11:08
05/23/20 20:38 1718-51-0
Phenol-d6 (S)
29
%
10-120
1
05/22/20 11:08
05/23/20 20:38 13127-88-3
2-Fluorophenol (S)
65
%
10-120
1
05/22/20 11:08
05/23/20 20:38 367-12-4
2,4,6-Tribromophenol (S)
71
%
10-137
1
05/22/20 11:08
05/23/20 20:38 118-79-6
624 Volatile Organics
Analytical Method:
EPA624.1
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
1.0
1
05/30/2015:08 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
05/30/2015:08 75-27-4
Bromoform
ND
ug/L
2.0
1
05/30/2015:08 75-25-2
Bromomethane
ND
ug/L
2.0
1
05/30/2015:08 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
05/30/20 15:08 56-23-5
Chlorobenzene
ND
ug/L
2.0
1
05/30/2015:08 108-90-7
Chloroethane
ND
ug/L
2.0
1
05/30/2015:08 75-00-3
Chloroform
ND
ug/L
2.0
1
05/30/2015:08 67-66-3
Chloromethane
ND
ug/L
2.0
1
05/30/2015:08 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
05130/2015:08 124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
05/30/2015:08 95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
05/30/2015:08 541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
05/30/2015:08 106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
05/30/2015:08 75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
05/30/2015:08 107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
05/30/2015:08 75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
2.0
1
05/30/2015:08 156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
05/30/2015:08 156-60-5
1,2-Dichioropropane
ND
ug/L
2.0
1
05/30/2015:08 78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 42

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acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92478444
QC Batch: 543358
Analysis Method:
EPA 1664E
QC Batch Method: EPA 1664B
Analysis Description:
1664 SGT-HEM, TPH
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92478444001,
92478444002, 92478444003
METHOD BLANK: 2894086
Matrix: Water
Associated Lab Samples: 92478444001,
92478444002, 92478444003
Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L ND 5.0 05/26/20 10:46
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2894087
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 15.1
76
64-132
MATRIX SPIKE SAMPLE:
2894088
2632027001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
8.0 20
26.8
94.
64-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 42

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A e
acmnalytical
www.pacolabs.com
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92478444
QC Batch: 544278 Analysis Method: EPA 624.1
QC Batch Method: EPA624.1 Analysis Description: 624 MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92478444001, 92478444002, 92478444003
METHOD BLANK: 2898575 Matrix:
Associated Lab Samples: 92478444001, 92478444002, 92478444003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1, 1, 1 -Trichloroethane
ug/L
ND
2.0
05/30/20 13:02
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
05/30/20 13:02
1,1,2-Trichloroethane
ug/L
ND
2.0
05/30/20 13:02
1,1-Dichloroethane
ug/L
ND
2.0
05/30/20 13:02
1,1-Dichloroethene
ug/L
ND
2.0
05/30/20 13:02
1,2-Dichlorobenzene
ug/L
ND
2.0
05/3012013:02
1,2-Dichloroethane
ug/L
ND
2.0
05130/2013:02
1,2-Dichloropropane
ug/L
ND
2.0
05/30/20 13:02
1,3-Dichlorobenzene
ug/L
ND
2.0
05/30/20 13:02
1,4-Dichlorobenzene
ug/L
NO
2.0
05/30/20 13:02
Benzene
ug/L
ND
1.0
05/30/20 13:02
Bromodichloromethane
ug/L
ND
2.0
05130/2013:02
Bromoform
ug/L
ND
2.0
05/30/20 13:02
Bromomethane
ug/L
ND
2.0
05/30/20 13:02
Carbon tetrachloride
ug/L
ND
2.0
05/30/20 13:02
Chlorobenzene
ug/L
ND
2.0
05/30/20 13:02
Chloroethane
ug/L
ND
2.0
05/30/20 13:02
Chloroform
ug/L
NO
2.0
05/30/20 13:02
Chloromethane
ug/L
ND
2.0
05/30/20 13:02
cis-1,2-Dichloroethene
ug/L
ND
2.0
05/30/20 13:02
cis- 1,3-Dichloropropene
ug/L
ND
2.0
05/30/20 13:02
Dibromochloromethane
ug/L
ND
2.0
05/30/20 13:02
Ethylbenzene
ug/L
ND
1.0
05/30/20 13:02
Methylene Chloride
ug/L
ND
2.0
05/30/20 13:02
Tetrachloroethene
ug/L
ND
2.0
05/30/20 13:02
Toluene
ug/L
ND
1.0
05/30/20 13:02
trans-1,2-Dichloroethene
ug/L
ND
2.0
05/30/20 13:02
trans-1,3-Dichloropropene
ug/L
ND
2.0
05130/2013:02
Trichloroethene
ug/L
ND
2.0
05/30/20 13:02
Trichlorofluoromethane
ug/L
ND
2.0
05/30/20 13:02
Vinyl chloride
ug/L
NO
2.0
05/30/20 13:02
1,2-Dichloroethane-d4 (S)
%
112
70-130
05/30/20 13:02
4-Bromofluorobenzene (S)
%
113
70-130
05/30/20 13:02
Toluene-d8 (S)
%
105
70-130
05/30/20 13:02
LABORATORY CONTROL SAMPLE: 2898576
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1, 1, 1 -Trichloroethane ug/L 20 19.2 96 70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02A0 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 42

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11
Pace Analytical Services, LLC
acmnalXit✓al 9800 KinceyAve. Suite 100
l' www.pacelabsl.com Huntersville, NC 28078
(704)875-.9092
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92478444
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2898577
2898578
MS
MSD
92478444001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Clual
1,2-Dichloropropane
ug/L
ND
20
20
22.5
22.7
112
113
1-210
1
1,3-Dichlorobenzene
ug/L
ND
20
20
21.0
24.9
105
125
59-156
17
1,4-Dichlorobenzene
ug/L
ND
20
20
21.0
24.5
105
122
18-190
15
Benzene
ug/L
ND
20
20
23.4
24.2
117
121
37-151
4
Bromodichloromethane
ug/L
ND
20
20
23.6
24.9
118
124
35-155
5
Bromoform
ug/L
ND
20
20
18.0
22.2
90
111
45-169
21
Bromomethane
ug/L
ND
20
20
23.3
21.9
115
108
1-242
6
Carbon tetrachloride
ug/L
ND
20
20
27.6
29.0
138
145
70-140
5 M1
Chlorobenzene
ug/L
ND
20
20
20.9
23.1
104
116
37-160
10
Chloroethane
ug/L
ND
20
20
23.7
24.6
119
123
14-230
3
Chloroform
ug/L
ND
20
20
23.1
23.7
115
119
51-138
3
Chloromethane
ug/L
ND
20
20
20.6
19.9
102
99
1-273
3
cis- 1,2-Dichloroethene
ug/L
ND
20
20
23.2
22.8
116
114
45-174
2
cis- 1,3-Dichloropropene
ug/L
ND
20
20
22.8
23.3
114
117
1-227
2
Dibromochloromethane
ug/L
ND
20
20
20.0
22.3
100
111
53-149
11
Ethylbenzene
ug/L
ND
20
20
20.4
21.7
102
109
37-162
7
Methylene Chloride
ug/L
ND
20
20
24.6
24.9
123
124
1-221
1
Tetrachloroethene
ug/L
ND
20
20
21.3
24.1
107
121
64-148
12
Toluene
ug/L
ND
20
20
22.2
23.2
108
113
47-150
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
26.2
26.3
131
131
54-156
0
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.7
24.3
114
121
17-183
7
Trichloroethene
ug/L
2.1
20
20
25.6
26.2
118
120
70-157
2
Trichlorofluoromethane
ug/L
ND
20
20
24.2
25.2
121
126
17-181
4
Vinyl chloride
ug/L
ND
20
20
25.6
25.3
128
126
1-251
1
1,2-Dichloroethane-d4 (S)
%
112
99
70-130
4-Bromofluorobenzene (S)
%
102
100
70-130
Toluene-d8 (S)
%
96
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 42

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A
aceAnaIXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92478444
METHOD BLANK: 2891653
Associated Lab Samples: 92478444003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloroethane
ug/L
ND
5.0
05/23/20 10:50
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
05/23/20 10:50
Isophorone
ug/L
ND
10.0
05/23/20 10:50
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
05/23/20 10:50
N-Nitrosodimethylamine
ug/L
ND
5.0
05/23/20 10:50
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/23/20 10:50
Naphthalene
ug/L
ND
5.0
05/23/20 10:50
Nitrobenzene
ug/L
ND
5.0
05/23/20 10:50
Pentachlorophenol
ug/L
ND
10.0
05/2312010:50
Phenanthrene
ug/L
ND
5.0
05/23/20 10:50
Phenol
ug/L
ND
5.0
05/23/20 10:50
Pyrene
ug/L
ND
5.0
05/23/20 10:50
2,4,6-Tribromophenol (S)
%
73
10-137
05/23/20 10:50
2-Fluorobiphenyl (S)
%
73
15-120
05/23/20 10:50
2-Fluorophenol (S)
%
76
10-120
05/23/20 10:50
Nitrobenzene-d5 (S)
%
86
10-120
05/23/20 10:50
Phenol-d6 (S)
%
56
10-120
05/23/20 10:50
Terphenyl-d14 (S)
%
104
11-131
05/23/20 10:50
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2891654
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
27.0
54
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
46.7
93
36-166
2,4,6-Trichlorophenol
ug/L
50
32.0
64
37-144
2,4-Dichlorophenol
ug/L
50
34.8
70
1-191
2,4-Dimethylphenol
ug/L
50
36.3
73
32-119
2,4-Dinitrophenol
ug/L
250
104
42
1-181
2,4-Dinitrotoluene
ug/L
50
43.0
86
39-139
2,6-Dinitrotoluene
ug/L
50
39.5
79
50-158
2-Chloronaphthalene
ug/L
50
31.4
63
60-118
2-Chlorophenol
ug/L
50
34.0
68
23-134
2-Nitrophenol
ug/L
50
35.9
72
29-182
3,3'-Dichlorobenzidine
ug/L
100
86.8
87
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
85.4
85
1-181
4-Bromophenylphenyl ether
ug/L
50
32.0
64
53-127
4-Chloro-3-methylphenol
ug/L
100
68.3
68
22-147
4-Chlorophenylphenyl ether
ug/L
50
30.2
60
25-158
4-Nitrophenol
ug/L
250
152
61
1-132
Acenaphthene
ug/L
50
32.6
65
47-145
Acenaphthylene
ug/L
50
33.1
66
33-145
Anthracene
ug/L
50
38.9
78
1-166
Benzo(a)anthracene
ug/L
50
44.4
89
33-143
Benzo(a)pyrene
ug/L
50
43.3
87
17-163
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 06/03/2020 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 42

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lacmnalyfical
www.pace]abs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Project: Stormwater
Pace Project No.: 92478444
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2891655
2891656
MS
MSD
92469531022
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
2,4-Dimethylphenol
ug/L
ND
50
50
39.7
30.0
79
60
32-119
28
2,4-Dinitrophenol
ug/L
ND
250
250
281
249
113
100
1-181
12
2,4-Dinitrotoluene
ug/L
ND
50
50
50.3
45.3
101
91
39-139
11
2,6-Dinitrotoluene
ug/L
ND
50
50
48.4
40.0
97
80
50-158
19
2-Chloronaphthalene
ug/L
ND
50
50
38.3
28.1
77
56
60-118
31 M1,R1
2-Chlorophenol
ug/L
ND
50
50
34.9
26.9
70
54
23-134
26
2-Nitrophenol
ug/L
ND
50
50
38.1
28.5
76
57
29-182
29
3,3'-Dichlorobenzidine
ug/L
ND
100
100
101
101
101
101
1-262
0
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
104
101
104
101
1-181
3
4-Bromophenylphenyl ether
ug/L
ND
50
50
41.1
34.5
82
69
53-127
17
4-Chloro-3-methylphenol
ug/L
ND
100
100
75.5
57.3
76
57
22-147
27
4-Chlorophenylphenyl ether
ug/L
ND
50
50
39.1
29.4
78
59
25-158
28
4-Nitrophenol
ug/L
ND
250
250
160
153
64
61
1-132
5
Acenaphthene
ug/L
ND
50
50
40.5
29.6
81
59
47-145
31 R1
Acenaphthylene
ug/L
ND
50
50
40.5
30.0
81
60
33-145
30
Anthracene
ug/L
ND
50
50
46.7
42.8
93
86
1-166
9
Benzo(a)anthracene
ug/L
ND
50
50
52.2
50.4
104
101
33-143
4
Benzo(a)pyrene
ug/L
ND
50
50
52.3
49.2
105
98
17-163
6
Benzo(b)fluoranthene
ug/L
ND
50
50
54.9
53.6
110
107
24-159
2
Benzo(g,h,i)perylene
ug/L
ND
50
50
54.3
49.6
109
99
1-219
9
Benzo(k)fluoranthene
ug/L
ND
50
50
54.1
48.6
108
97
11-162
11
bis(2-Ch loroethoxy) methane
ug/L
ND
50
50
36.9
27.1
74
54
33-184
31 R1
bis(2-Chloroethyl) ether
ug/L
ND
50
50
34.8
27.0
70
54
12-158
25
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
50
49.8
46.3
100
93
8-158
7
Butylbenzylphthalate
ug/L
ND
50
50
51.7
49.4
103
99
1-152
4
Chrysene
ug/L
ND
50
50
50.4
48.6
101
97
17-168
4
Di-n-butylphthalate
ug/L
ND
50
50
47.5
45.6
95
91
1-118
4
Di-n-octylphthalate
ug/L
ND
50
50
52.3
52.1
105
104
4-146
0
Dibenz(a,h)anthracene
ug/L
ND
50
50
55.9
50.9
112
102
1-227
9
Diethylphthalate
ug/L
ND
50
50
45.7
40.9
91
82
1-114
11
Dimethylphthalate
ug/L
ND
50
50
45.1
38.3
90
77
1-112
16
Fluoranthene
ug/L
ND
50
50
46.9
42.8
94
86
26-137
9
Fluorene
ug/L
ND
50
50
43.2
33.1
86
66
59-121
26
Hexachloro-1,3-butadiene
ug/L
ND
50
50
25.5
18.4
51
37
24-116
32 R1
Hexachlorobenzene
ug/L
ND
50
50
42.0
36.7
84
73
1-152
14
Hexachlorocyclopentadiene
ug/L
ND
50
50
31.4
22.0
63
44
25-150
35 R1
Hexachloroethane
ug/L
ND
50
50
28.2
22.2
56
44
40-113
24
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
53.3
49.4
107
99
1-171
8
Isophorone
ug/L
ND
50
50
38.0
28.4
76
57
21-196
29
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
37.9
29.5
76
59
1-230
25
N-Nitrosodimethylamine
ug/L
ND
50
50
34.5
26.7
69
53
25-150
25
N-Nitrosodiphenylamine
ug/L
ND
50
50
46.2
40.7
92
81
25-150
13
Naphthalene
ug/L
ND
50
50
34.4
25.8
69
52
21-133
29
Nitrobenzene
ug/L
ND
50
50
38.1
27.6
76
55
35-180
32 R1
Pentachlorophenol
ug/L
ND
100
100
98.9
96.3
99
96
14-176
3
Phenanthrene
ug/L
ND
50
50
46.0
42.3
92
85
54-120
8
Results presented on this
page are in the units indicated by the "Units"
column
except where
an alternate unit
Is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 42

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�aceAnalytical
www.pacelabs.com
Project: Stormwater
Pace Project No.: 92478444
QC Batch: 542986
QC Batch Method: EPA625.1
Associated Lab Samples: 92478444001, 92478444002
QUALITY CONTROL DATA
Analysis Method: EPA 625.1
Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 2892642
Associated Lab Samples: 92478444001, 92478444002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
05123/2011:41
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
05/23/20 11:41
2,4,6-Trichlorophenol
ug/L
ND
10.0
05/23/20 11:41
2,4-Dichlorophenol
ug/L
ND
5.0
05/23/20 11:41
2,4-Dimethylphenol
ug/L
ND
10.0
05/23/20 11:41
2,4-Dinitrophenol
ug/L
ND
50.0
05/23/20 11:41
2,4-Dinitrotoluene
ug/L
ND
5.0
05/23/20 11:41
2,6-Dinitrotoluene
ug/L
ND
5.0
05/23/20 11:41
2-Chloronaphthalene
ug/L
ND
5.0
05/23/20 11:41
2-Chlorophenol
ug/L
ND
5.0
05123/2011:41
2-Nitrophenol
ug/L
ND
5.0
05/23/20 11:41
3,3'-Dichlorobenzidine
ug/L
ND
10.0
05/23/20 11:41
4,6-Dinitro-2-methylphenol
ug/L
ND
10.0
05/23/20 11:41
4-Bromophenylphenyl ether
ug/L
ND
5.0
05/23/20 11:41
4-Chloro-3-methylphenol
ug/L
ND
5.0
05/23/20 11:41
4-Chlorophenylphenyl ether
ug/L
ND
5.0
05/23/20 11:41
4-Nitrophenol
ug/L
ND
10.0
05/23/20 11:41
Acenaphthene
ug/L
ND
5.0
05/23/20 11:41
Acenaphthylene
ug/L
ND
5.0
05/23/20 11:41
Anthracene
ug/L
ND
5.0
05/23/20 11:41
Benzo(a)anthracene
ug/L
ND
5.0
05/23/20 11:41
Benzo(a)pyrene
ug/L
ND
5.0
05/23/20 11:41
Benzo(b)fluoranthene
ug/L
ND
5.0
05/23/20 11:41
Benzo(g,h,i)perylene
ug/L
ND
5.0
05/23/20 11:41
Benzo(k)fluoranthene
ug/L
ND
5.0
05/23/20 11:41
bis(2-Ch loroethoxy) methane
ug/L
ND
10.0
05/23/20 11:41
bis(2-Chloroethyl) ether
ug/L
ND
5.0
05/23/20 11:41
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
05/23/20 11:41
Butylbenzylphthalate
ug/L
ND
5.0
05/23/20 11:41
Chrysene
ug/L
ND
5.0
05/23/20 11:41
Di-n-butylphthalate
ug/L
ND
5.0
05/23/20 11:41
Di-n-octylphthalate
ug/L
ND
5.0
05/23/20 11:41
Dibenz(a,h)anthracene
ug/L
ND
5.0
05/23/20 11:41
Diethylphthalate
ug/L
ND
5.0
05/23/20 11:41
Dimethylphthalate
ug/L
ND
5.0
05/23/20 11:41
Fluoranthene
ug/L
ND
5.0
05/23/20 11:41
Fluorene
ug/L
ND
5.0
05/23/20 11:41
Hexachloro-1,3-butadiene
ug/L
ND
5.0
05/23/20 11:41
Hexachlorobenzene
ug/L
ND
5.0
05/23/20 11:41
Hexachlorocyclopentadiene
ug/L
ND
10.0
05/23/20 11:41
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 42

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(�IaneAnalyfical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92478444
LABORATORY CONTROL SAMPLE:
Parameter
2892643
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(b)fluoranthene
ug/L
50
48.7
97
24-159
Benzo(g,h,i)perylene
ug/L
50
46.1
92
1-219
Benzo(k)fluoranthene
ug/L
50
48.2
96
11-162
bis(2-Ch loroethoxy) methane
ug/L
50
42.1
84
33-184
bis(2-Chloroethyl) ether
ug/L
50
39.9
80
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
45.8
92
8-158
Butylbenzylphthalate
ug/L
50
49.0
98
1-152
Chrysene
ug/L
50
46.9
94
17-168
Di-n-butylphthalate
ug/L
50
45.1
90
1-118
Di-n-octylphthalate
ug/L
50
46.0
92
4-146
Dibenz(a,h)anthracene
ug/L
50
47.4
95
1-227
Diethylphthalate
ug/L
50
40.4
81
1-114
Dimethylphthalate
ug/L
50
41.5
83
1-112
Fluoranthene
ug/L
50
43.7
87
26-137
Fluorene
ug/L
50
41.4
83
59-121
Hexachloro-1,3-butadiene
ug/L
50
27.1
54
24-116
Hexachlorobenzene
ug/L
50
40.2
80
1-152
Hexachlorocyclopentadiene
ug/L
50
32.1
64
25-150
Hexachloroethane
ug/L
50
31.4
63
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
44.6
89
1-171
Isophorone
ug/L
50
42.9
86
21-196
N-Nitroso-di-n-propylamine
ug/L
50
42.8
86
1-230
N-Nitrosodimethylamine
ug/L
50
39.2
78
25-150
N-Nitrosodiphenylamine
ug/L
50
44.1
88
25-150
Naphthalene
ug/L
50
36.6
73
21-133
Nitrobenzene
ug/L
50
41.5
83
35-180
Pentachlorophenol
ug/L
100
91.7
92
14-176
Phenanthrene
ug/L
50
44.5
89
54-120
Phenol
ug/L
50
25.2
50
5-112
Pyrene
ug/L
50
51.3
103
52-115
2,4,6-Tribromophenol (S)
%
88
10-137
2-Fluorobiphenyl (S)
%
83
15-120
2-Fluorophenol (S)
%
67
10-120
Nitrobenzene-d5 (S)
%
85
10-120
Phenol-d6 (S)
%
50
10-120
Terphenyl-d14 (S)
%
111
11-131
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2892644
2892645
MS
MSD
35551037001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
1.61-1 50
50
40.5
36.6
81
73
44-142
10
2,2'-Oxybis(1-chloropropane)
ug/L
1.31-1 50
50
65.8
64.7
132
129
36-166
2
2,4,6-Trichlorophenol
ug/L
1.41-1 50
50
36.1
21.3
72
43
37-144
52 R1
2,4-Dichlorophenol
ug/L
1.51-1 50
50
44.6
32.5
89
65
1-191
31 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 42

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aceAnalXical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater
Pace Project No.: 92478444
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2892644
2892645
MS
MSD
35551037001
Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits RPD Qual
Phenol
ug/L
1.51-1 50
50 24.0
18.9
48
38
5-112 24
Pyrene
ug/L
1.5U 50
50 54.5
57.2
109
114
52-115 5
2,4,6-Tribromophenol (S)
%
96
64
10-137
2-Fluorobiphenyl (S)
%
97
93
15-120
2-Fluorophenol (S)
%
62
36
10-120
Nitrobenzene-d5(S)
%
100
113
10-120
Phenol-d6 (S)
%
53
41
10-120
Terphenyl-d14 (S)
%
123
131
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 35 of 42

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1plpfleubaa

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater
Pace Project No.: 92478444
QC Batch: 542945
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 5220D
COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92478444001, 92478444002, 92478444003
METHOD BLANK: 2892347
Matrix: Water
Associated Lab Samples: 92478444001, 92478444002, 92478444003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
05/22/20 15:54
LABORATORY CONTROL SAMPLE: 2892348
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 766
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2892349 2892350
MS MSD
92478352001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 96.4
100 100 208
208 112 112
90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2892351 2892352
MS MSD
92478389001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 44.0
100 100 160
160 116 116
90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 42

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aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater
Pace Project No.: 92478444
Lab ID Sample ID QC Batch Method QC Batch
92478444001
SDO-1
EPA 1664B
543358
92478444002
SDO-2
EPA 16646
543358
92478444003
SDO-3
EPA 1664B
543358
92478444001
SDO-1
EPA 200.7 Rev 4.4 1994
543811
92478444002
SDO-2
EPA 200.7 Rev 4.4 1994
543811
92478444003
SDO-3
EPA 200.7 Rev 4.4 1994
543811
92478444001
SDO-1
EPA 625.1
542986
92478444002
SDO-2
EPA 625.1
542986
92478444003
SDO-3
EPA 625.1
542827
92478444001
SDO-1
EPA624.1
544278
92478444002
SDO-2
EPA 624.1
544278
92478444003
SDO3
EPA 624.1
544278
92478444001
SDO-1
SM 2540D-2011
543184
92478444002
S130-2
SM 254OD-2011
543184
92478444003
SDO-3
SM 2540D-2011
543184
92478444001
S130-1
SM 5220D-2011
542945
92478444002
SDO-2
SM 5220D-2011
542945
92478444003
SDO-3
SM 5220D-2011
542945
Date: 06/03/2020 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical Method
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
EPA 625.1
EPA 625.1
EPA 625.1
SM 5220D-2011
SM 5220D-2011
SM 5220D-2011
Analytical
Batch
543837
543837
543837
543206
543206
543204
543187
543187
543187
Page 39 of 42

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Document Name:
Document Revised: February 7, 2018
v
Analytical
Sample Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and wlthin the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # WO# : 92478444
PM: NMG Due Date: 06/01/20
CLIENT: 82-Norton
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Sample ID
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pH upon receipt
Date preservation adjusted
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adjusted
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added
Lot H
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of lemp, Incorrect containers.
Page 41 of 42

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