NCG030571_Monitoring Report_20220314

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form with n
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG03 0571
Person Collecting Samples: Tommy Maness
Facility Name: Norton Door Controls (Norton)
Laboratory Name: Pace Analytical
Facility County: Union
Laboratory Cert. No.: 5342
Discharge during this period: Yes No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? v Yes No
If so, which Tier (I, II, or III)? 1
A copy of this DMR has been uploaded electronically via https://edocs.dea.nc.gov/Forms/SW-DMR QYes No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities —Benchmarks in (Red)
Parameter
—..__..
Code
Parameter
Outfall SDO1
Outfall SD02
Outfall SD03
Outfall
Outfall
N/A
Receiving Stream Class
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
05/19/2020
05/19/2020
05/19/2020
i
46529
24-Hour Rainfall in inches
0.23
0.23
0.23
C0530
TSS in mg/L (100 or 50*)
4.7
4.5
11.3
00400
PH in standard units (6.0 - 9.0 FW,
6.8-8.5 SW)
n/a
n/a
n/a
01119
Copper, total recoverable in mg/L
(0.010 FW, 0.0058 SW)
0.0099
<0.005
0.0096
01051
Lead, total recoverable in mg/ L
(0.075 FW, 0,22 SW)
<0.005
<0.005
<0.005
01094
Zinc, total recoverable in mg/ L (0.126
FW, 0.095 SW)
0.0764
0.0475
0.0176
00340
Chemical Oxygen Demand (COD) in
mg/L (120)
<25.0
<25 0
<5.0
<25.0
_ -I
<5.0
00552
*
Non -Polar Oil & Grease in mg/L (15)
<5.0
OUtfalis to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional): TTO (78141) Benchmark 1 mg/L SDO-1: 0.0021 mg/l (Trichloroethene); SDO.2: ND; SDO-3: ND ��
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information including the possibility of fines and imprisonment for knowing violations."
ri,17g.nat re of Permi klee or Delegated Authorized Individual Date
on [e-mail] 7p Y 3 3 5 5
Email Address Phone Number

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llaceAnalylrcal
www,pacelabs.com
Project. Stormwater
Pace Project No. 92478444
Pace Analytical Services Charlotte
9800 Kincey Ave Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification # 37706
North Carolina Field Services Certification # 5342
North Carolina Wastewater Certification # 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FlondalNELAP Certification # E87648
Massachusetts Certification # M-NC030
North Carolina Drinking Water Certification # 37712
CERTIFICATIONS
South Carolina Certification # 99006001
Flonda/NELAP Certification # E87627
Kentucky UST Certification # 84
VlrginiaNELAP Certification #. 460221
North Carolina Wastewater Certification # 40
South Carolina Certification # 99030001
VirginiaNELAP Certification # 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
without the written consent of Pace Analytical Services. LLC
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 42

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/ PaceAnalydical
/ www.pacolabs.com
Project. Stormwater
Pace Project No. 92478444
Lab Sample ID
Method
Client Sample ID
Parameters
92478444001
SOO.1
EPA 200 7 Rev 4-4 1994
Copper
EPA 200.7 Rev 4 4 1994
Zinc
EPA 624 1
Trichloroethene
SM 254OD-2011
Total Suspended Solids
92478444002
SDO-2
EPA 200 7 Rev 4 4 1994
Zinc
SM 254OD-2011
Total Suspended Solids
92478444003
SDO.3
EPA 200 7 Rev 4 4 1994
Copper
EPA 200 7 Rev 4 4 1994
Zinc
SM 2540D-2011
Total Suspended Solids
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
SUMMARY OF DETECTION
Result
Units
Report Limit
Analyzed Qualifiers
99
ug/L
50
06/01/20 14 38
764
ug/L
100
06/01/20 14 38
21
ug/L
2.0
05/30/2014,32
4 7
mg/L
2.5
05/22/20 18.16
475
ug/L
100
06/01/20 14.48
45
mg/L
25
05/22/20 18 17
9.6
ug/L
50
06/01/20 14.58
176
ug/L
100
06/01/20 14:58
11.3
mg/L
34
05/22/20 18 18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 42

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fXaceAnalytical
,,,. pecelebs.com
PROJECT NARRATIVE
Project, Stormwater
Pace Project No 92478444
Method: EPA 200.7 Rev 4.41994
Description: 200.7 MET ICP
Client: Norton Door Controls
Date: June 03. 2020
Pace Analytical Services, LLC
9800KinceyAve, Suite100
Hunlersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 200.7 Rev 4.4 1994 by Pace Analytical Services Asheville All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Sample Preparation:
The samples were prepared in accordance with EPA 200 7 Rev 4 4 1994 with any exceptions noted below
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Method Blank:
All analytes were below the report limit In the method blank, where applicable. with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC Page 6 of 42

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ffaceAnalyfical
r www.pacolobs.com
i
Project. Stormwater
Pace Project No: 92478444
Method: EPA 625.1
Description: 625 RVE
Client: Norton Door Controls
Date: June 03, 2020
QC Batch 542827
PROJECT NARRATIVE
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s) 92469531022
Rt RPD value was outside control limits
Nitrobenzene
b is(2-C hloroethoxy) metha ne
QC Batch 542986
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s) 35551037001
R1 RPD value was outside control limits
• MSD (Lab ID: 2892645)
2, 4.6-Tri ch lorophenol
2.4-Dichlorophenol
2-Chlorophenol
4, 6-Di nitro-2-methyl phenol
• 4-Nitrophenol
Pentachlorophenol
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 42

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RaceAnalytical
/ www.pacelabs.com
Project Stormwater
Pace Project No. 92478444
Method: SM 254OD-2011
Description: 2540D Total Suspended Solids
Client: Norton Door Controls
Date: June 03, 2020
PROJECT NARRATIVE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for SM 2540D-2011 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 42

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RaceAnalyiical
www.pecolabg.com
1
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater
Pace Project No. 92478444
Sample: SDO.1
Lab ID: 92478444001 Collected
05/19/20 18.00 Received: 05/20/20 13 36 Matrix Water
Parameters
Results
Units Report Limit
OF Prepared Analyzed CAS No Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
NO
mg/L
50
1 05/26/20 10 46
200.7 MET lCP
Analytical Method EPA 200 7 Rev 4.4
1994 Preparation Method. EPA 200 7 Rev 4 4 1994
Pace Analytical
Services - Asheville
Copper
Lead
9.9
ug/L
5 0
1 05/28/20 01 42 06/01/20 14 38 7440-50-8
Zinc
NO
ug/L
50
1 05/28/20 01:42 06/01/20 14 38 7439.92-1
76.4
ug/L
100
1 05/28/20 01:42 06/01/20 14.38 7440-66-6
625 RVE
Analytical Method EPA625 1 Preparation Method EPA625 1
Pace Analytical
Services - Charlotte
Acenaphthene
Acenaphthylene
NO
ug/L
50
1 05/21/20 2106 05/26/20 1342 83-32.9
Anthracene
NO
ug/L
5,0
1 05/21/20 21:06 05/26/20 1342 208-96-8
Benzo(a)anthracene
NO
NO
ug/L
5.0
1 05/21/20 21:06 05/26/20 1342 120-12-7
Benzo(a)pyrene
NO
ug/L
50
1 05/21/20 2106 05/26/20 13:42 56-55-3
Benzo(b)fluoranthene
NO
ug/L
ug/L
50
50
1 05/21/20 21,06 05/26/20 1342 50.32-8
Benzo(g.h,i)perylene
NO
ug/L
50
1 05/21/20 21,06 05/26/20 13 42 205-99-2
Benzo(k)fluorenthene
NO
1 05/21/202106 05/26/2013.42 191-24-2
4-Bromophenylpheny) ether
NO
ug/L
ug/L
50
1 05/21/20 2106 05/26/20 13.42 207-08-9
Butylbenzylphthalate
NO
ug/L
50
50
1 05/21/20 21.06 05/26/20 1342 101-55.3
4-Chloro-3-methylphenol
NO
ug/L
5.0
1 05/21/20 21 06 05/26/20 13 42 85-68-7
bls(2-Chloroethoxy)methane
NO
ug/L
1 05/21/20 21.06 05/26/20 13 42 59-50-7
bis(2-Chloroethyl) ether
ND
ug/L
100
50
1 05/21/20 2106 05/26/20 1342 111-91-1
2-Chloronaphthalene
NO
ug/L
50
1 05/21/20 21 i06 05/26/20 1342 111-44-4
2-Chlorophenol
NO
ug/L
5.0
1 05/21/20 21.06 05/26/20 13:42 91-58-7
4-Chlorophenylphenyl ether
NO
ug/L
5-0
1 05/21/20 21.06 05/26/20 13 42 95-57-8
Chrysene
1 05/21/20 21:06 05/26/20 1342 7005-72-3
Dibenz(a,h)anthracene
NO
NO
ug/L
ugll-
50
1 05/21/20 2106 05/26/20 1342 218-01-9
3.3'-Dichlorobenzidine
NO
50
1 05/21/20 21:06 05/26/20 13,42 53-70.3
2,4-Dichlorophenol
NO
ug/L
100
1 05/21/20 21:06 05/26/20 13-42 91-94-1
Diethylphthalate
ug/L
5.0
1 05/21/20 21.06 05/26/20 13 42 120-83-2
2,4-Dimethylphenol
NO
NO
ug/L
50
1 05/21/20 2106 05/26/20 13 42 84-66-2
Dimethylphthalate
NO
ug/L
10.0
1 05/21/20 21'06 05/26/20 13.42 105-67-9
Di-n-butylphthalate
NO
ug/L
50
1 05/21/202106 05/26/201342 131-11-3
4,6-Dinitro-2-methylphenol
NO
ug/L
ug/L
50
1 05/21/20 21 06 05/26/20 13 42 84-74-2
2,4-Dinitrophenol
NO
100
1 05/21/20 2106 05/26/20 13 42 534-52-1
2.4-Dinitrotoluene
ug/L
50.0
1 05/21/2021,06 05/26/201342 51-28-5
2,6-Dinitrotoluene
NO
uglL
50
1 05/21/20 21 06 05/26/20 13 42 121-14-2
Di-n-octylphthalate
NO
NO
ug/L
5 0
1 05/21/20 2106 05/26/20 1342 606-20.2
bis(2-Ethylhexyl)phthalate
NO
ug/L
ug/L
5.0
1 05/21/20 21 06 05/26/20 1342 117-84-0
Fluoranthene
NO
5 0
1 05121/20 21:06 05/26/20 1342 117-81-7
Fluorene
ug/L
5-0
1 05/21/20 21 06 05/26/20 13.42 206-44-0
Hexachloro-1,3-butadiene
NO
NO
ug/L
ug/L
50
1 05/21/20 2106 05/26/20 13 42 86-73.7
Hexachlorobenzene
NO
5 0
1 05/21/20 21:06 05/26/20 13 42 87-68-3
Hexachlorocyclopentadiene
NO
ug/L
ug/L
5 0
100
1 05/21/20 21:06 05/26/20 13 42 118-74-1
1 05/21/20 21:06 05/26/20 13 42 77-47-4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date 06/03/2020 02 40 PM
without
the written consent of Pace
Analytical
Services, LLC
Page 12 of 42

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/ IJaceAnalytical
wvnv.pacalabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Project Stormwater
Pace Project No.: 92478444
Sample: SDO.1
Lab ID: 92478444001 Collected
05/19/20 18:00 Received 05/20/20 13:36 MatrixWater
Parameters
Results Units Report Limit
OF
Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624 1
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND ug/L
2-0
1
05/30/20 14:32 10061-01-5
trans-1,3-Dichloropropene
NO ug/L
2 0
1
05/30/20 14 32 10061-02-6
Ethylbenzene
ND ug/L
1.0
1
05/30/20 14 32 100.41-4
Methylene Chloride
NO ug/L
2 0
1
05/30/20 14 32 75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
2 0
1
05/30/20 1432 79-34.5
Tetrachloroethene
ND ug/L
2 0
1
05/30/20 1432 127-18-4
Toluene
NO ug/L
10
1
05/30/20 14 32 108-88-3
1,1,1-Trichloroethane
NO ug/L
20
1
05/30/2014,32 71-55-6
1,1,2-Trichloroethane
NO ug/L
20
1
05130/2014.32 79.00-5
Trichloroethene
2.1 ug/L
2 0
1
05/30/20 14.32 79-01-6
Trichlorofluoromethane
NO ug/L
20
1
05/30/20 14.32 75-69.4
Vinyl chloride
ND ug/L
2 0
1
05/30/20 143275-01.4
Surrogates
4-Bromofluorobenzene(S)
105 %
70-130
1
05/30/20 14.32 460.00-4
Toluene-d8(S)
104 %
70-130
1
05/30/20 14 32 2037-26-5
1,2-Dichloroethane-d4 (S)
118 %
70-130
1
05/30/20 14 32 17060-07.0
2540D Total Suspended Solids
Analytical Method SM 2540D-2011
Pace Analytical Services - Asheville
Total Suspended Solids
4.7 mg/L
2 5
1
05/22/20 18 16
5220D COD
Analytical Method SM 5220D-2011 Preparation
Method SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
ND mg/L
250
1
05/21/20 17 00 05/22/20 15 57
Date 06/03/2020 02 40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC
Page 14 of 42

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llaceAnalytical
/ www.pacolabs.com
ANALYTICAL RESULTS
Project Stormwater
Pace Project No 92478444
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
sample: zjuu-2 Lab ID: 92478444002 Collected: 05/19/20 18 15 Received. 05/20/20 13:36 Matrix Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 RVE
Hexachloroethane
Indeno(1,2.3-cd)pyrene
isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-N itrosodimethylamine
N-Nitroso-di-n-pro pylamine
N-N i trosod iph enyla m i n e
2, 2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1, 2.4-Trichl orobenzene
2,4, 6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl(S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
624 Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dib romochioromethane
1,2-Dichlorobenzene
1, 3-Dichlorobenzene
1,4-Dichlorobenzene
1. 1 -Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1, 2-Dichloroethene
trans-1, 2-Dichloroethene
1, 2-Dichloropropane
Date 06/03/2020 02 40 PM
Analytical Method EPA 625 1 Preparation Method. EPA625 1
Pace Analytical Services - Charlotte
ND
ug/L
50
1
05/21/20 2106 05/26/20 14:07 67-72-1
ND
ug/L
5.0
1
05/21/20 2106 05/26/20 14 07 193.39.5
NO
ug/L
100
1
05/21/20 2106 05/26/20 14,07 78.59-1
NO
ug/L
5.0
1
05/21/20 2106 05/26/20 14 07 91-20-3
NO
ug/L
50
1
05/21/20 21.06 05/26/20 14:07 98-95.3
NO
ug/L
5.0
1
05/21/20 21 *06 05/26/20 1407 88-75-5
ND
ug/L
100
1
05/21/20 2106 05/26/20 14 07 100-02-7
NO
ug/L
5.0
1
05/21/20 2106 05/26/20 1407 62-75-9
NO
ug/L
5.0
1
05/21/20 2106 05/26/20 1407 621.64-7
NO
ug/L
100
1
05/21/20 21:06 05/26/20 1407 86-30.6
NO
ug/L
50
1
05/21/20 2106 05/26/20 1407 108-60-1
NO
ug/L
100
1
05/21/20 2106 05/26/20 14:07 87-86.5
ND
ug/L
50
1
05/21/20 2106 05/26/20 1407 85.01.8
NO
ug/L
50
1
05/21/20 2106 05/26/20 14 07 108.95.2
NO
ug/L
50
1
05/21/20 21:06 05/26/20 14 07 129.00.0
NO
ug/L
&0
1
05/21/20 2106 05/26/20 14:07 120-82-1
NO
ug/L
100
1
05/21/20 21:06 05/26/20 1407 88.06.2
108
%
91
%
129
%
55
%
77
83
%
Analytical Method' EPA624.1
Pace Analytical
Services - Charlotte
NO
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
10.120
1
05/21/20 21.06 05/26/20 1407 4165-60-0
15-120
1
05/21/20 21 06 05/26/20 14,07 321-60-8
11.131
1
05/21/20 2106 05/26/20 14.07 1718-51.0
10.120
1
05/21/20 21:06 05/26/20 14 07 13127.88-3
10-120
1
05/21/20 2106 05/26/20 14 07 367.12-4
10-137
1
05/21/20 21 06 05/26/20 14 07 118-79-6
10
1
05/30/20 14 50 71-43-2
20
1
05/30/20 14.50 75-27-4
2A
1
05/30/2014.50 75-25-2
2.0
1
05/30/20 1450 74-83-9
20
1
05/30/20 1450 56-23-5
20
1
05/30/20 1450 108-90-7
20
1
05/30/20 14 50 75-00-3
20
1
05/30/20 14 50 67-66-3
20
1
05/30/20 14 50 74.87-3
20
1
05/30/20 1450 124-48-1
20
1
05/30/20 1450 95.50-1
20
1
05/30/20 14 50 541-73-1
20
1
05/30/20 14.50 106-46.7
20
1
05/30/20 1450 75-34.3
20
1
05/30/20 14.50 107.06-2
20
1
05/30/20 14 50 75.35.4
20
1
05/30/20 14.50 156-59.2
20
1
05/30/20 14:50 156-60.5
2.0
1
05/30/2014,50 78.87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC
Page 16 of 42

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/ EjaceAnalytical
wvnv.pacelabs.com
i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville. NC 28078
[phone]
Project Stormwater
Pace Project No 92478444
Sample: SDO-3
Lab ID: 92478444003 Collected:
05/19/20 18:30 Received 05/20/20 13:36 MatrixWater
Parameters
Results
Units Report Limit
OF Prepared Analyzed CAS No Qual
1664 SGT-HEM, TPH
Analytical Method. EPA 16648
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND
mg/L
5.0
1 05/26/20 10A6
200.7 MET ICP
Analytical Method EPA 200.7 Rev 4 4
1994 Preparation Method EPA 200 7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
9.6
ug/L
50
1 05/28/20 0142 06/01/20 14 58 7440-50.8
Lead
NO
ug/L
50
1 05/28/20 0142 06/01/20 14 58 7439-92.1
Zinc
17.6
ug/L
100
1 05/28/20 01 42 06/01/20 14.58 7440-66.6
625 RVE
Analytical Method EPA 625 1 Preparation
Method EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthene
NO
uglL
50
1 05/22/20 1108 05/23/20 20,38 83-32-9
Acenaphthylene
NO
ug/L
5-0
1 05/22/20 1108 05/23/20 20 38 208-96-8
Anthracene
NO
ug/L
5.0
1 05/22/20 1108 05/23/20 20 38 120-12-7
Benzo(a)anthracene
NO
ug/L
5.0
1 05/22/20 1108 05/23/20 20,38 56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
1 05/22/20 1108 05/23/20 20 38 50-32.8
Benzo(b)0uoranthene
NO
ug/L
50
1 05/22/20 1108 05/23/20 20.38 205.99-2
Benzo(g.h,i)perylene
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 191.24-2
Benzo(k)8uoranthene
NO
ug/L
50
1 05/22/20 11 08 05/23/20 20:38 207-08-9
4-Bromophenylphenyl ether
NO
ug/L
50
1 05/22/20 11-08 05/23/20 20:38 101-55-3
Butylbenzylphthalate
NO
ug/L
50
1 05/22/20 1108 05/23/20 20:38 85-68-7
4-Chloro-3-methylphenol
NO
ug/L
50
1 05/22/20 1108 05/23/20 20:38 59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
100
1 05/22/20 11'08 05/23/20 20 38 111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
50
1 05/22/20 1108 05/23/20 20:38 111-44.4
2-Chloronaphthalene
NO
ug/L
50
1 05/22/201108 05/23/2020'38 91-58.7
2-Chlorophenol
NO
ug/L
5.0
1 05/22/20 11.08 05/23/20 20:38 95-57.8
4-Chlorophenylphenyl ether
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 7005-72-3
Chrysene
NO
ug/L
5.0
1 05/22/20 1108 05/23/20 20:38 218-01-9
Dibenz(a,h)anthracene
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
100
1 05/22/20 1108 05/23/20 20:38 91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1 05/22/20 1108 05/23/20 2038 120-83-2
Diethylphthalate
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 84-66-2
2,4-Dimethylphenol
NO
ug/L
100
1 05/22/2011.08 05/23/20 20,38 105.67-9
Dimethylphthalate
NO
ug/L
5 0
1 05/22/20 1108 05/23/20 20:38 131-11.3
Di-n-butylphlhalate
NO
ug/L
50
1 05/22/20 11 08 05/23/20 20:38 84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/L
10,0
1 05/22/20 11.08 05/23/20 20 38 534-52-1
2,4-Dinitrophenol
NO
ug/L
500
1 05/22/20 1108 05/23/20 20:38 51-28-5
2,4-Dinitrotoluene
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 121-14-2
2,6-Dinitrotoluene
ND
ug/L
5 0
1 05/22/20 11 08 05/23/20 20 38 606-20-2
Di-n-octylphthalate
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
50
1 05/22/20 11 08 05/23/20 20.38 117-81-7
Fluoranthene
ND
ug/L
50
1 05/22/2011.08 05/23/20 20.38 206-44.0
Fluorene
NO
ug/L
50
1 05/22/20 1108 05/23/20 20 38 86-73.7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1 05/22/20 1108 05/23/20 20 38 87.68-3
Hexachlorobenzene
NO
ug/L
50
1 05/22/20 11 08 05/23/20 2038 118-74-1
Hexachlorocyclopentadiene
NO
ug/L
100
1 05/22/20 11 08 05/23/20 20 38 77.47.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2020 02 40 PM
without the written consent of Pace
Analytical
Services, LLC Page 18 of 42

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Pace Analytical Services, LLC
�-.Pa'lceAnalyfical 9800 Kincey Ave. Suite too
wvnv.peeelabs.eam
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project Stormwater
Pace Project No.: 92478444
Sample: SDO-3
Lab ID: 92478444003 Collected: 05/19/20 18 30 Received: 05/20/20 13 36 Matrix Mter
Parameters
Results Units Report Limit
OF
Prepared Analyzed CAS No Qual
624 Volatile Organics
Analytical Method EPA624.1
Pace Analytical Services - Charlotte
cis- 1.3-Dichloropropene
NO ug/L
2.0
1
05/30/2015.08 10061-01-5
trans-1,3-Dichloropropene
NO ug/L
20
1
05/30/20 15-08 10061-02-6
Ethylbenzene
NO ug/L
1.0
1
05/30/20 15 08 100-41.4
Methylene Chloride
ND ug/L
20
1
05/30/20 15,08 75-09-2
1,1,2,2-Tetrachloroethane
NO ug/L
20
1
05/30/20 15-08 79-34-5
Tetrachloroethene
ND ug/L
2.0
1
05/30/20 15:08 127-16-4
Toluene
NO ug/L
1.0
1
05/30/20 15 08 108-88-3
1.1,1-Trichloroethane
NO ug/L
20
1
05/30/20 15:08 71-55-6
1,1,2-Trichloroethane
NO ug/L
20
1
05/30/20 15 08 79.00-5
Trichloroethene
NO ug/L
20
1
05/30/20 1508 79-01-6
Trichloro8uoromethane
NO ug/L
2 0
1
05/30/20 15-08 75.69-4
Vinyl chloride
Surrogates
ND ug/L
2 0
1
05/30/20 15:08 75-01-4
4-BromoBuorobenzene(S)
104 %
70.130
1
05/30/20 15 08 460-00.4
Toluene-d8 (S)
103 %
70.130
1
05/30/20 15 08 2037-26.5
1,2-Dichloroethane-d4 (S)
116 %
70-130
1
05/30/20 15 08 17060-07.0
2540D Total Suspended Solids
Analytical Method SM 2540D-2011
Pace Analytical Services -Asheville
Total Suspended Solids
11.3 mg/L
3 4
1
05/22/20 18 18
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method. SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
NO mg/L
25 0
1
05/21/20 17:00 05/22/20 15.57
Date 06/03/2020 02 40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
vnthout the written consent of Pace Analytical Services, LLC
Page 20 of 42

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)"anceAnalylical
www.pacolabs.com
I
QUALITY CONTROL DATA
Project Stormwater
Pace Project No 92478444
WU oaten. 043a11 Analysis Method
QC Batch Method- EPA 200.7 Rev 4 4 1994 Analysis Description
Laboratory
Associated Lab Samples 92478444001, 92478444002, 92478444003
EPA 200 7 Rev 4.4 1994
200 7 MET
Pace Analytical Services - Asheville
METHOD BLANK 2896150
Matrix- Water
Associated Lab Samples-
92478444001. 92478444002. 92478444003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
NO 5.0
06/01/20 14 22
Lead
ug/L
NO 5.0
06101/2014.22
Zinc
ug/L
NO 10 0
06/01/20 14,22
LABORATORY CONTROL SAMPLE
2896151
Spike
Parameter
Units
Conc.
Copper
ug/L
500
Lead
ug/L
500
Zinc
ug/L
500
LCS LCS
Result Rec
450 90
450 90
442 88
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
85-115
85-115
85.115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE
2806152
2896153
MS
MSD
92478444001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper ug/L
9 9
500
500
524
476
103
93
70-130 9
Lead ug/L
ND
500
500
530
480
105
96
70.130 10
Zinc ug/L
764
500
500
626
540
110
93
70-130 15
MATRIX SPIKE & MATRIX SPIKE DUPLICATE
2896154
2896155
MS
MSD
92478787001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc
Conc
Result
Result
/o Rec
/o Rec
Limits RPD Qual
Copper ug/L
ND
500
500
490
473
97
94
70-130 3
Lead ug/L
NO
500
500
485
466
97
93
70-130 4
Zinc ug/L
139
500
500
493
479
96
93
70-130 3
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date 06/03/2020 02 40 PM without the written consent of Pace Analytical Services, LLC,
Page 22 of 42

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fpaceAnalylical
www.pocolabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kmcey Ave. Suite too
Huntersville, NC 28078
[phone]
Project Stormwater
Pace Project No.: 92478444
LABORATORY CONTROL SAMPLE: 2898576
Spike LCS
LCS
% Rec
Parameter
Units
Cono. Result
% Rec
Limits
Qualifiers
1. 1, 2,2-Tetrachloroethene
ug/L
20
17.0
85
60-140
1, 1. 2-Trichloroetha ne
ug/L
20
15.8
79
70.130
1,1-Dichloroethane
ug/L
20
185
93
70-130
1.1-Dichloroethene
ug/L
20
211
105
50.150
1.2-Dichlorobenzene
ug/L
20
16.8
84
65.135
1.2-Dichloroethane
ug/L
20
194
97
49-155
1 2-Dichloropropane
ug/L
20
160
80
35-165
1.3-D chlorobenzene
ug/L
20
16 7
83
70.130
1.4-Dichlorobenzene
ug/L
20
154
77
65-135
Benzene
ug/L
20
169
85
65.135
Bromodichloromethane
ug/L
20
176
88
65-135
Bromoform
ug/L
20
144
72
70-130
Bromomethane
ug/L
20
177
89
15.185
Carbon tetrachloride
ug/L
20
196
98
70-130
Chlorobenzene
ug/L
20
15.4
77
65-135
Chloroethane
ug/L
20
179
90
40-160
Chloroform
ug/L
20
200
100
70-135
Chloromethane
uglL
20
172
86
1-205
cis- 1, 2-Dichloroethene
ug/L
20
173
87
68-146
cis- 1, 3-Dichloropropene
ug/L
20
168
84
25.175
Dibromochloromethane
ug/L
20
15 6
78
70-135
Ethylbenzene
ug/L
20
14.6
73
60.140
Methylene Chloride
ug/L
20
19.1
95
60.140
Tetrachloroethene
ug/L
20
168
84
70-130
Toluene
ug/L
20
153
76
70.130
trans-1,2-Dichloroethene
ug/L
20
19.6
98
70-130
trans-1,3-Dichloropropene
ug/L
20
171
86
50-150
Trichloroethene
ug/L
20
161
81
65.135
Trchlorofluoromethane
ug/L
20
19.8
99
50-150
Vinyl chloride
ug/L
20
195
98
5-195
1.2-Dichloroethane-d4 (S)
%
115
70-130
4-Bromofluorobenzene(S)
%
108
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE 2898577
2898578
MS MSD
92478444001
Spike Spike
MS
MSD
MS MSD
% Rec
Parameter _
_Units Result
Conc Conc
Result
Result % Rec eh Rec
Limits RPD Qual
1.1.1-Trichloroethane
ug/L ND
20 20
253
26.5
126 133
52-162 5
1 1.22•Tetrachloroethane
ug/L ND
20 20
215
227
108 113
46.157 5
1.1.2-Trichloroethane
ug/L NO
20 20
221
222
110 111
52-150 1
1,1-Dichloroethane
ug/L ND
20 20
224
24.2
112 121
59-155 8
1. 1 -Dichloroethene
ug/L ND
20 20
274
29.1
137 146
1.234 6
1.2-Dichlorobenzene
ug/L NO
20 20
209
24 3
105 121
18-190 15
12-Dichloroethane
ug/L ND
20 20
24.4
24.0
122 120
49-155 1
Results presented on this page are In the units Indicated by the "Units" column
except where an alternate unit
is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This
report shall not be reproduced, except
in full,
Date 06/03/2020 02 40 PM
without the written consent of Pace Analytical Services, I.I.C.
Page 24 of 42

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ljaceAnalXical
www.pacelabs.com
Project
Stormwater
Pace Project No.
92478444
QC Batch:
642827
QC Batch Method
EPA 625 1
Associated Lab Samples. 92478444003
METHOD BLANK: 2891653
Associated Lab Samples: 92478444003
QUALITY CONTROL DATA
Analysis Method
Analysis Description:
Laboratory.
Matrix Water
EPA 625.1
625 MSS
Pace Analytical Services - Charlotte
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/L
i NO
5.0
05/23/20 10:50
2,2'-Oxybis(1-chloropropane)
ug/L
NO
50
05/23/2010.50
2,4,6-Trichlorophenol
ug/L
NO
100
05/23/20 10 50
2,4.Oichlorophenol
ug/L
NO
50
05/23/20 10.50
2,4-Dimethylphenol
ug/L
NO
100
05/23/20 10.50
2,4-Dinitrophenol
ug/L
NO
500
05/23/20 10 50
2,4-Dinitrotoluene
ug/L
NO
50
05/23/20 10:50
2,6-Dinitrotoluene
ug/L
NO
5.0
05/23/20 10 50
2-Chicronaphthalene
ug/L
NO
50
05/23/2010.50
2-Chlorophenoi
ug/L
NO
50
05/2312010'50
2-Nitrophenol
ug/L
NO
50
05/23/20 10 50
3,3'-Dichlorobenzidine
ug/L
NO
10.0
05/23/20 10 50
4,6-Dinitro-2-methylphenol
ug/L
NO
100
05/23/20 10 50
4-Bromophenylphenyl ether
ug/L
NO
50
05/23/20 10.50
4-Chloro-3-methylphenol
ug/L
NO
50
05/23/20 10 50
4-Chlorophenylphenyl ether
ug/L
NO
50
05/23/20 10:50
4-Nitrophenol
ug/L
NO
100
05/23/20 10:50
Acenaphthene
ug/L
NO
5.0
05/2312010:50
Acenaphthylene
ug/L
NO
5.0
05/23/20 10 50
Anthracene
ug/L
NO
50
05/23/20 10 50
Benzo(a)anthracene
ug/L
NO
5.0
05/23/20 10,50
Benzo(a)pyrene
ug/L
NO
5.0
05/23/2010.50
Benzo(b)fluoranthene
ug/L
NO
50
05/23/20 10 50
Benzo(g,h,i)perylene
ug/L
NO
50
05/23/2010.50
Benzo(k)fluoranlhene
ug/L
NO
5.0
05/23/20 10 50
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
05/23/2010:50
bis(2-Chloroethyl) ether
ug/L
NO
5.0
05/23/20 10 50
bis(2-Ethylhexyl)phthalate
ug/L
NO
50
05/23/20 10 50
Bulylbenzylphthalate
ug/L
NO
50
05/23/20 10 50
Chrysene
ug/L
NO
50
05/23/20 10 50
Di-n-butylphthalate
ug/L
NO
5.0
05/23/2010:50
Di-n-octyiphthalate
ug/L
NO
50
05/23/20 1050
Dibenz(a.h)anthracene
ug/L
NO
50
05/23/20 10.50
Diethylphthalate
ug/L
NO
50
05/23/20 1050
Dimethylphthalate
ug/L
NO
50
05/23/20 10 50
Fluoranlhene
ug/L
NO
50
05/23/20 1050
Fluorene
ug/L
NO
5.0
05/23/20 10 50
Hexachloro-1,3-butadiene
ug/L
NO
50
05/23/2010:50
Hexachlorobenzene
ug/L
NO
5.0
05/23/20 10 50
Hexachlorocyclopentadiene
ug/L
NO
100
05/23/20 10.50
Results presented on this page are
in the units indicated
by the "Units" column
except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date 06/03/2020 02 40 PM without the wniten consent of Pace Analytical Services, LLC.
Page 26 of 42

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flaceAnalj4ical
www.pacolabs.com
QUALITY CONTROL DATA
Project Stormwater
Pace Project No.: 92478444
LABORATORY CONTROL SAMPLE' 2891654
Parameter
Units
Spike
Cone
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(b)fluoranthene
ug/L
— 50
46.1
-
92
--
24-159
Benzo(g.h,i)perylene
ug/L
50
41.3
83
1.219
Benzo(k)fluoranthene
ug/L
50
454
91
11.162
bis(2-Chloroethoxy)methane
ug/L
50
32-4
65
33-184
bis(2-Chloroethyi) ether
ug/L
50
309
62
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
400
80
8-158
Butylbenzylphthalate
ug/L
50
44.0
88
1-152
Chrysene
ug/L
50
425
85
17-168
Di-n-butylphthalate
ug/L
50
41.3
83
1-118
Di-n-octylphthalate
ug/L
50
43.0
86
4-146
Dibenz(a.h)anthracene
ug/L
50
42.0
84
1-227
Diethylphthalate
ug/L
50
380
76
1-114
Dimethylphthalate
ug/L
50
366
73
1-112
Fluoranthene
ug/L
50
39.6
79
26-137
Fluorene
ug/L
50
334
67
59-121
Hexachloro-1,3-butadiene
ug/L
50
225
45
24-116
Hexachlorobenzene
ug/L
50
343
69
1.152
Hexachlorocyclopentadiene
ug/L
50
25-6
51
25.150
Hexachloroethane
ug/L
50
267
53
40-113
Indeno(1.2,3-cd)pyrene
ug/L
50
40.6
81
1-171
Isophorone
ug/L
50
342
68
21-196
N-Nitroso-di-n-propylamine
ug/L
50
352
70
1-230
N-Nitrosodimethylamine
ug/L
50
360
72
25.150
N-Nitrosodiphenylamine
ug/L
50
379
76
25-150
Naphthalene
ug/L
50
307
61
21-133
Nitrobenzene
ug/L
50
339
68
35.180
Pentachlorophenol
ug/L
100
858
86
14.176
Phenanthrene
ug/L
50
387
77
54-120
Phenol
ug/L
50
260
52
5-112
Pyrene
ug/L
50
480
96
52-115
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
63
10 137
2-Fluorophenol (S)
%
52
15.120
Nitrobenzene-d5 (S)
%
55
10-120
Phenol-d6 (S)
%
59
10-120
Terphenyl-d14 (S)
%
45
10.120
86
11 131
MAI NIX SPIKE & MATRIX SPIKE DUPLICATE
2891655
MS
92469531022 Spike
Parameter
Units
Result Cone
1,2,4-Trichlorobenzene
ug/L
ND 50
2,2'-Oxybis(1-chloropropane)
ug/L
ND 50
2,4,6-Trichlorophenol
ug/L
ND 50
2,4-Dichlorophenol
ug/L
ND 50
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Qualifiers
2891656
MSD
Spike
MS
MSD
MS
MSD
%Rec
Cone
Result
Result
% Rec
% Rec
Limits
RPD Qual
50
305
227
61
45
44-142
29
50
51 7
388
103
78
36-166
28
50
401
29.6
80
59
37.144
30
50
380
27.1
76
54
1.191
33 R1
Results presented an this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/03/2020 02 40 PM without the written consent of Pace Analytical Services. LLC
Page 28 of 42

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4_ )
II'mAnalytical
j WWW.pacelabs,com
QUALITY CONTROL DATA
Project. Stormwater
Pace Project No.: 92478444
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2891655
MS
92469531022 Spike
Parameter
Units
Result Conc
Phenol
ug/L
ND 50
Pyrene
ug/L
ND 50
2,4,6-Tnbromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%,
2891656
MSD
Spike MS
MSD
Conc. Result
Result
50 �23.0
17.3
50 53.6
51.9
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
MS
% Rec
MSD
% Rec
% Rec
Limits RPD
46
35
5-112 28
107
104
52-115 3
79
72
10-137
69
49
15-120
56
41
10.120
71
52
10.120
43
32
10.120
104
104
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date 06/03/2020 02 40 PM without the written consent of Pace Analytical Services, LLC
Qual
Page 30 of 42

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0 ljaceAnalj tical
/ www.pacelabs.com
QUALITY CONTROL DATA
Project Stormwater
Pace Project No. 92478444
METHOD BLANK 2892642 Matrix Water
Associated Lab Samples 92478444001 92478444002
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
Hexachloroethane
ug/L
NO
50
05/23/20 11 41
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
05/23/20 11 41
Isophorone
ug/L
NO
10.0
05/23/2011:41
N-Nitroso-di-n-propylamine
ug/L
NO
5 0
05/23/20 11 41
N-Nitrosodimethylamine
ug/L
NO
5.0
05/23/201141
N-Nitrosodiphenylamine
ug/L
NO
10.0
05/23/201141
Naphthalene
ug/L
ND
5 0
05/23/20 1141
Nitrobenzene
ug/L
NO
5.0
05/23/20 11 41
Pentachlorophenol
ug/L
NO
10 0
05/23/20 1141
Phenanthrene
ug/L
NO
5,0
05/23/201141
Phenol
ug/L
NO
5 0
05/23/20 1141
Pyrene
ug/L
NO
5.0
05/23/20 11 41
2,4,6-Tribromophenol (S)
%
46
10-137
05/23/20 1141
2-Fluorobiphenyl (S)
%
82
15-120
05/23/20 11 41
2-Fluorophenol(S)
%
41
10-120
05/23/20 11'41
Nitrobenzene-d5 (S)
%
95
10-120
05/23/20 1141
Phenol-d6 (S)
%
44
10-120
05/23/20 1141
Terphenyl-d14 (S)
%
120
11-131
05/23/20 1141
Qualifiers
LABORATORY CONTROL SAMPLE
Parameter
2892643
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
320
64
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
585
117
36-166
2,4,6-Trichlorophenol
ug/L
50
423
85
37-144
2.4-Dichlorophenol
ug/L
50
421
84
1-191
2.4-Dimethylphenol
ug/L
50
423
85
32-119
2.4-Dinitrophenol
ug/L
250
254
101
1.181
2,4-Dinitrotoluene
ug/L
50
444
89
39-139
2.6-Dinitrotoluene
ug/L
50
44.3
89
50.158
2-Chloronaphthalene
ug/L
50
38 7
77
60-118
2-Chlorophenol
ug/L
50
39.9
80
23-134
2-Nitrophenol
ug/L
50
437
87
29-182
3,3'-Dichlorobenzidine
ug/L
100
910
91
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
101
101
1-181
4-Bromophenylphenyl ether
uglL
50
405
81
53-127
4-Chloro-3-methylphenol
ug/L
100
816
82
22-147
4-Chlorophenylphenyl ether
ug/L
50
38.2
76
25-158
4-Nitrophenol
ug/L
250
125
50
1-132
Acenaphthene
ug/L
50
416
83
47.145
Acenaphthylene
ug/L
50
41 7
83
33-145
Anthracene
ug/L
50
446
89
1-166
Benzo(a)anthracene
ug/L
50
482
96
33.143
Benzo(a)pyrene
ug/L
50
470
94
17-163
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale 06/03/2020 02 40 PM without the written consent of Pace Analytical Services, LLC
Page 32 of 42

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(.� Pace Analytical Services, LLC
ra5 9800 Kincey Ave. Suite 100
f aCeAnacy�ica� www.peeelahs.cam Hunlersville, NC 28078
j [phone]
QUALITY CONTROL DATA
Project Stormwater
Pace Project No 92478444
MATRIX SPIKE & MATRIX SPIKE DUPLICATE
2892644
2892645
MS
MSD
35551037001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
- --
Units
Result
---------
Conc.
Conc
Result
Result
% Rec
% Rec
Limits
RPD Qual
2,4-Dimethylphenol
ug/L
1. 5U
-
50
- - -
50
45.7
52.7
-
91
-
105
-
32-119
--
14
2,4-Dinitrophenol
ug/L
7 3U
250
250
90.8
80.9
36
32
1-181
12
2.4-Dinitrotoluene
ug/L
17U
50
50
49.6
50.1
99
100
39-139
1
2.6-Dinitrotoluene
ug/L
1 7U
50
50
485
50.6
97
101
50-158
4
2-Chloronaphthalene
ug/L
14U
50
50
43.0
415
86
83
60.118
4
2-Chlorophenol
ug/L
14U
50
50
40.4
28A
81
57
23.134
35 R1
2-Nitrophenol
ug/L
1 7U
50
50
44 1
356
88
71
29-182
21
3,3'-Dichlorobenzidine
ug/L
2 7U
100
100
855
892
86
89
1-262
4
4,6-Dinitro-2-methylphenoi
ug/L
4 51-1
100
100
51 7
370
52
37
1-181
33 R1
4-Bromophenylphenyl ether
ug/L
1 2U
50
50
440
462
88
92
53-127
5
4-Chioro-3-methylphenol
ug/L
2 8U
100
100
838
81.2
84
81
22-147
3
4-Chlorophenylphenyl ether
ug/L
1 5U
50
50
44 5
450
89
90
25-158
1
4-Nitrophenol
ug/L
9.4U
250
250
560
38.2
22
15
1-132
38 R1
Acenaphthene
ug/L
1AU
50
50
457
428
91
86
47-145
7
Acenaphthylene
ug/L
1 51-1
50
50
456
433
91
87
33-145
5
Anthracene
ug/L
16U
50
50
47.0
494
94
99
1-166
5
Benzo(a)anthracene
ug/L
1 5U
50
50
51 8
533
104
107
33-143
3
Senzo(a)pyrene
ug/L
18U
50
50
49.6
517
99
103
17-163
4
Benzo(b)fluoranthene
ug/L
1 7U
50
50
51 6
542
103
108
24-159
5
Benzo(g,h,i)perylene
ug/L
1 6U
50
50
488
476
98
95
1-219
2
Benzo(k)fuoranthene
ug/L
151-1
50
50
505
525
101
105
11-162
4
bis(2-Chloroethoxy)methane
ug/L
1 3U
50
50
436
51 2
87
102
33-184
16
bis(2-Chloroethyl) ether
ug/L
1 7U
50
50
426
382
85
76
12-158
11
bis(2-Ethylhexyl)phthalate
ug/L
2 OU
50
50
47-6
48.5
95
97
8.158
2
Butylbenzylphthalate
ug/L
19U
50
50
51.0
513
102
103
1-152
1
Chrysene
ug/L
14U
50
50
499
49.4
100
99
17.168
1
Di-n-butylphthalate
ug/L
1.6U
50
50
45.6
492
91
98
1-118
8
Di-n•octylphthalate
ug/L
2 2U
50
50
499
48 3
100
97
4-146
3
Dibenz(a.h)anthracene
ug/L
1 6U
50
50
503
491
101
98
1-227
2
Diethylphthalate
ug/L
1 6U
50
50
458
45 7
92
91
1-114
0
Dimethylphlhalate
ug/L
14U
50
50
444
465
89
93
1-112
5
Fluoranthene
ug/L
1 6U
50
50
474
52 6
95
105
26-137
10
Fluorene
ug/L
14U
50
50
471
46.5
94
93
59.121
1
Hexachloro-1.3-butadlene
ug/L
16U
50
50
37.0
319
74
64
24-116
15
Hexachlorobenzene
ug/L
1.3U
50
50
439
455
88
91
1-152
4
Hexachlorocyclopentadiene
ug/L
2 4U
50
50
38 0
352
76
70
25-150
8
Hexachloroethane
ug/L
1.3U
50
50
35 5
34.6
71
69
40-113
3
Indeno(1.2.3•cd)pyrene
ug/L
1 7U
50
50
483
47.5
97
95
1-171
2
Isophorone
ug/L
1 3U
50
50
447
528
89
106
21-196
17
N-Nitroso-di-n-propylamine
ug/L
13U
50
50
43,7
409
87
82
1-230
6
N-Nltrosodimethylamine
ug/L
1 8U
50
50
44 1
397
88
79
25-150
11
N-Nltrosodiphenylamine
ug/L
1 4U
50
50
46.8
475
94
95
25-150
1
Naphthalene
ug/L
1.6U
50
50
426
39.2
85
78
21.133
8
Nitrobenzene
ug/L
1 51-1
50
50
438
507
88
101
35-180
14
Pentachlorophenol
ug/L
2 8U
100
100
574
348
57
35
14-176
49 R1
Phenanthrene
ug/L
14U
50
50
478
493
96
99
54-120
3
Results presented on this page are In the
units Indicated
by the "Units"
column
except where an alternate unit
is presented to the right
of the result.
REPORT
OF LABORATORY ANALYSIS
This
report shall
not be reproduced, except
in full,
Date 06/03/2020 02 40 PM
without the written consent of Pace Analytical Services, LLC
Page 34 of 42

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flaceAnalytical
www.pacolabsxom
QUALITY CONTROL DATA
Project Stormwater
Pace Project No 92476444
QC Batch: 543184 Analysis Method
QC Batch Method SM 254OD-2011 Analysis Description:
Laboratory:
Associated Lab Samples: 92478444001, 92478444002. 92478444003
SM 254OD-2011
2540D Total Suspended Solids
Pace Analytical Services - Asheville
METHOD BLANK 2893565 Matrix: Water
Associated Lab Samples 92478444001, 92478444002. 92478444003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2 5 05/22/20 17 56
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
-----------
ABORATORY CONTROL SAMPLE & LCSD 2893566 2893746
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc Result Result % Rec % Rec Limits RPD RPD Qualifiers
-------- ------ --
Total Suspended Solids mg/L 251 238 246 95 98 90.110 3 25
SAMPLE DUPLICATE 2893710
92478310001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids m /L 37 36 3
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date 06/03/2020 02 40 PM without the written consent of Pace Analytical Services. LLC
Page 36 of 42

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Pace Analytical Services, LLC
/ Pac Ana,(XiCal
9800 KinceyAve, Suite 100
/ wenv.pecalebs.com
Huntersville, NC 28078
(/
[phone]
QUALIFIERS
Project Stormwater
Pace Project No 92478444
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot
NO - Not Detected at or above adjusted reporting limit
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270 The result for each analyte is
a combined concentration
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for. but not detected
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260
N-Nitrosodiphenylarnme decomposes and cannot be separated from Diphenylamine using Method 8270 The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited Contact your Pace PM for the current list of accredited analytes
TNI - The NELAC Institute
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits Batch accepted based on laboratory control sample (LCS) recovery
R1 RPD value was outside control limits
Date: 06/03/2020 02 40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 38 of 42

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�ceh?alyfical*
Document Name:
Sample Condltlon Upon Recel t(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Q� Ralelgh❑ Mechanicsville❑
i Cilent Name: I WO# : 92478444
Nor I �n PcoT &\A id�
�ProJectk
® r
Courier: ed Ex ❑UPS USPS Cilent ❑ Commercial Pace ❑Other:— U
02478444
Custody Seal Present? ❑Yes C�-No Seals Intact? ❑Yes QNo ,t
Date/InItIelsPerson ExeminingContents:� �Q._�U-���tp
Packing Material: ❑Bubble Wrap LJ/ Bubble Rags ❑None ❑ Other Biological Tissue frozen?
Thermometer: ,�.,/wet ❑Blue ©None []Yes[]NoN/A
❑IR Gun Type l_f ID 92TO61
Cooler Temp ('C): -i •� 3 o Corr >ctlo Factor: Add/Subtract ('C) +0.1
3 7 Temp should be above freezing to VC
Cooler Temp Corrected ('C): []Samples out of temp criteria Samples on ice, cooling process
has begun
USDA Regulated Soil ([1f N/A, water sample)
Did samples originate in a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source pnternationally,
1 IYes nNn m—
Comments/Dlscre anc :
Chain of Custody Present?
34'es
No
N/A
1.
Samples Arrived within Hold Time?
yes
MN.
QWA
2.
Short Hold Time Analysis (02 hr.l?
❑Yes
Q90
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
Mo
N/A
4.
Sufficient Volume?
Qfes
QNo
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
&Tes
Q'(es
❑No
EINO
❑N/A
❑N/A
6.
Containers Intact?
J
es
dNcs
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
rJNo
/A
8.
—Sample Labels Match COC?
Yes
17INo
QN/A
9.
Includes Date/Time/ID/Analysls Matrix:
(/I
V I
Heads ace In VOA Vials (>5-6mm)?
QYes
[?rNo
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
5Yes.
No
❑No
❑N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID off split containers
CLIENT NOTIFICATION/RESOLUTION
Person contactedDate/Time,
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
field Data Required? ❑Yes (:]No
----------
Page 40 of 42

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