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HomeMy WebLinkAboutNCG030535_Monitoring Report_20211206 (2)NCDEQ Division of Energy, Mineral and Land Resources Click here for instructions ©�b Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report DMR U or ithMO 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEML a Certificate of Coverage No. NCG03 0535 Person Collecting Samples: William Edens �P Facility Name: ZF Chassis Components, LLC. Laboratory Name: Pace Analytical Facility County: Catawba Laboratory Cert. No.: 92572462 Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ❑✓ No If so, which Tier (I,11, or III)? A copy of this DMR has been uploaded electronically via https:Hedocs.deg.nc.goy/Forms/SW-DMR ❑✓ Yes ❑ No Date uploaded:12/3/2021 Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall#1 Outfall#2 Outfall Outfall Outfall Code N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 11 /12/2021 11 /12/2021 46529 24-Hour Rainfall in inches .2 .2 C0530 TSS in mg/L (100 or 50') 4.8 7.5 00400 pH in standard units (6.0-9.0) 6.3 6.4 01119 Copper, total recoverable in mg/L ND .016 (0.010) 01051 Lead, total recoverable in mg/ L ND ND (0.075) 01094 zinc, total recoverable in mg/ L .049 .079 (0.126) 78141 Total Toxic Organics (TTO) in mg/L(1) N/A N/A (if required) 00552 Non -Polar Oil & Grease in mg/L (15) 1ND ND Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month + Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark T551Imit of 50 mg/L All other water classifications have a benchmark of 100 mg/L Notes (optional): Very low flow from the previous night's rainfall "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and Imprisonment for knowing violations." of Permittee or Delegated Authorized Individual 12/3/2021 Date Email address william.edens@zf.com Phone Number 828-468-3340 Total Toxic Organics Certification: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no leak, spill, or dumping of concentrated toxic organics into the stormwater or onto areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the Solvent Management Plan included in the Stormwater Pollution Prevention Plan." Signature of Permittee or Delegated Authorized Individual 12/3/2021 Date Email Address william.edens@zf.com Phone Number 828-468-3340 ��eAnalj4ical' www.pacelabsxom November 29, 2021 William Edens ZF Chassis Components LLC 1570 E. P St. Ext. Newton, NC 28658 RE: Project: STORMWATER SAMPLING Pace Project No.: 92572462 Dear William Edens: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, .,R Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, vdthout the vmtten consent of Pace Analytical Services, LLC. Page 1 of 15 ace Analytical www.pacelobs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92572462 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification M 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certfcation M 40 CERTIFICATIONS South Carolina Certification M 99006001 South Carolina Drinking Water Cert. M 99006003 Florida/NELAP Certification M E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification M 460221 South Carolina Laboratory ID: 99030 South Carolina Certification M 99030001 Virginia/VELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalXical www.patelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: STORMWATER SAMPLING Pace Project No.: 92572462 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92672462001 11-2021 #1 EPA 1664B ICO 1 PASI-C EPA 200.7 Rev 4A 1994 CBV 3 PASI-A SM 254OD-2015 ZMC 1 PASI-A EPA 9040C SMK 1 PASI-A 92572462002 11-2021 #2 EPA 1664B ICO 1 PASI-C EPA 200.7 Rev 4.4 1994 CBV 3 PASI A SM 254OD-2015 MJP 1 PASI-A EPA 9040C SMK 1 PASI-A PASI A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 aceAnalXical www pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER SAMPLING Pace Project No.: 92572462 Sample: 11-2021 #1 Parameters Lab ID: 92672462001 Collected: 11/12/21 09:00 Results Units Report Limit DF Received: 11/12/21 10:40 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 4.8 1 11/16/21 08:50 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper ND mg/L 0.0050 1 11/19/2111:16 11/24/2105:28 7440-50-8 Lead ND mg/L 0.0050 1 11/19/2111:16 11/24/2105:28 7439-92-1 Zinc 0.049 mg/L 0.010 1 11/19/2111:16 11/24/2105:28 7440-66-6 2640D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services -Asheville Total Suspended Solids 4.8 mg/L 2.5 1 11/17/21 16:24 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.3 Std. Units 0.10 1 11/23/21 10:55 H3 Date: 111291202105:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalXkal www paaelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER SAMPLING Pace Project No.: 92572462 Sample: 11-2021 #2 Lab ID: 92572462002 Collected: 11/12/21 09:00 Received: 11/12/21 10:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 4.8 1 11/16/21 08:50 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 0.016 mg/L 0.0050 1 11/19/2111:16 11124/2105:32 7440-50-8 Lead ND mg/L 0.0050 1 11 /19/21 11:16 11 /24/21 05:32 7439-92-1 Zinc 0.079 mg/L 0.010 1 11/19/2111:16 11/24/2105:32 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids 7.6 mg/L 2.5 1 11/18/21 13:40 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.4 Std. Units 0.10 1 11/23/21 10:57 H3 Date: 11129/202105:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5of15 aceAnalXical www.pacelabs.com s Pace Analytical Services, LLC 9800 IGncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92572462 QC Batch: 659972 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572462001, 92572462002 METHOD BLANK: 3458296 Matrix: Water Associated Lab Samples: 92572462001, 92572462002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L • ND 5.0 11/16/21 08:50 LABORATORY CONTROL SAMPLE: 3458297 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 36.3 91 78-114 MATRIX SPIKE SAMPLE: 3458298 Parameter Units Oil and Grease mg/L SAMPLE DUPLICATE: 3458299 Parameter Oil and Grease 35676265001 Spike MS MS Result Conc. Result % Rec 1 A U 39.2 31.8 % Rec Limits Qualifiers 81 78-114 35676262001 Dup Units Result Result RPD Qualifiers mg/L 11.6.1 1.9J Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/29/2021 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 15 '* ace Analj cal www.patelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92572462 QC Batch: 661080 Analysis Method: EPA 200.7 Rev 4.41994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92572462001, 92572462002 METHOD BLANK: 3463891 Associated Lab Samples: 92572462001, 92572462002 Parameter Units Copper Lead Zinc mg/L mg/L LABORATORY CONTROL SAMPLE: 3463892 Parameter Units Copper Lead Zinc ... I. - mg/L mg/L Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 11/24/21 05:02 ND 0.0050 11/24/2105:02 ND 0.010 11/24/21 05:02 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 0.5 0.50 99 85-115 0.5 0.50 100 85-115 0.5 0.50 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3463893 3463894 MS MSD 92572323001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Copper mg/L 0.0075 0.5 0.5 0.49 0.56 97 111 70-130 13 Lead mg/L ND 0.5 0.5 0.50 0.56 100 112 70-130 12 Zinc mg/L 0.035 0.5 0.5 0.54 0.62 101 116 70-130 13 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3463895 MS 92572999001 Spike Parameter Units Result Conc. Copper mg/L 7.9 ug/L 0.5 Lead mg/L ND 0.5 Zinc mg/L ND 0.5 3463896 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD Qual 0.5 0.54 0.55 107 108 70-130 1 0.5 0.51 0.52 102 104 70-130 2 0.5 0.50 0.51 100 101 70-130 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/29/202105:23 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92572462 QC Batch: 660563 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92572462001 METHOD BLANK: 3461115 Associated Lab Samples: 92572462001 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11/17/21 16:17 LABORATORY CONTROL SAMPLE: 3461116 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 3461446 92572266002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 184 180 2 SAMPLE DUPLICATE: 3461447 Parameter Total Suspended Solids 92572266004 Dup Units Result Result RPD Qualifiers mg/L 83.0 77.0 8 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /29/2021 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 15 aCmalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92572462 QC Batch: 660791 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572462002 METHOD BLANK: 3462269 Matrix: Water Associated Lab Samples: 92572462002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/18/21 13:39 LABORATORY CONTROL SAMPLE: 3462270 Spike LCS Parameter Units Conc. Result Total Suspended Solids mg/L 250 LCS % Rec 246 98 % Rec Limits Qualifiers 90-110 SAMPLE DUPLICATE: 3462555 92572876001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 242 242 0 SAMPLE DUPLICATE: 3462556 Parameter Total Suspended Solids 92572607009 Dup Units Result Result RPD Qualifiers mg/L 193 212 9 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/29/202105:23 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 aceAnalj&al www.pacolabs.com s Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92572462 QC Batch: 661789 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92572462001, 92572462002 SAMPLE DUPLICATE: 3467284 Parameter pH at 25 Degrees C SAMPLE DUPLICATE: 3467285 Parameter pH at 25 Degrees C Units Std. Units 92572259001 Dup Result Result RPD Qualifiers 7.9 7.9 0 H3 92572800001 Dup Units Result Result Std. Units 6.8 RPD Qualifiers 6.8 0 H3 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 11 /29/2021 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 IGncey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QUALIFIERS Project: STORMWATER SAMPLING Pace Project No.: 92572462 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TN I - The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /29/2021 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 aceAnalytical www.pacetabs.com Pace Analytical Services, LLC 9800 IGncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER SAMPLING Pace Project No.: 92572462 Lab ID Sample ID QC Batch Method QC Batch Analytical Analytical Method Batch 92572462001 11-2021 #1 EPA1664B 659972 92672462002 11-2021 #2 EPA1664B 659972 92572462001 11-2021 #1 EPA 200.7 Rev 4.4 1994 661080 EPA 200.7 Rev 4.4 1994 661260 92572462002 11-2021 #2 EPA 200.7 Rev 4.41994 661080 EPA 200.7 Rev 4.41994 661260 92572462001 11-2021 #1 SM 254OD-2015 660563 92572462002 11-2021 #2 SM 254OD-2015 660791 92572462001 11-2021 #1 EPA 9040C 661789 92572462002 11-2021 #2 EPA 9040C 661789 Date: 11129/202105:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 15 Document No.: Laboratory receiving Samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville1K Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑ Client Name: .Z r- <.(�ss; s-��w1,L'� ProjectgWO## :92572462 Courier: ❑Fed Ex ❑UPS ❑USPS []Client ❑ Commercial [pace ❑Other._ Custody Seal Present? ❑Yes 2No Seals Intact? []Yes "�JLo Packing Material: Nubble Wrap gEBubble Bags ❑None ❑ Other ThermometeJ: DU cre In. 92, W F j>�Wet [:]Blue ypeo ce: Correction Factor: Cooler Temp: Add/Subtract (°C) (/ • L Cooler Temp Corrected( Q USDA Regulated Soil (bN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? P 1111 I111111111111111 92572462 Dne/In ials Person Examining Contents:) Biological Tissue Frozen? []Yes ❑No ❑N/A Temp sNuld be above freezing to 6'C ❑sanples out of temp cdteda. Samples on ice, cooling process has btvn Did samo!sonpnate from a foreign source (Internationally, Yes ❑No IndudlnlHiwaD and Puerto Nrn)?❑Yes ONO Comments/Discrepancy: Chain of Custody Present? Yes ❑No ❑N/A 1. Samiles Arrived within Hold Time? Yes ONO ❑N/A 2. Short Hold Tons Analysis j<72 hr.)? byes MNo ❑N/A 3. Rush Turn Around Time Requested? ❑Yes jpNo ❑N/A 4. Sufficient Volume? WYW QNo ON/A S. Correct Containers Used? -Pace Containers Used? J§Yes Dyes ON. ONO ❑N/A ❑N/A 6. Containers Intact? es ONE ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ONE 'MNIA 8. Sample Labels Match COC? -Includes DatetrimeAD/Analysis Matrix: rzfyes vV f ONO ❑N/A 9. Heads ace in VOA Vials >S-6mm)7 OYES ONO N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes QY1[:]No Efso ❑N/A /A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of spit containers: CLIENT NOTIFICATION/RESOLUTION Project Manager SCURF Review: tale: Project Manager SRF Review: late: Field Data Required? []Yes ❑No r. 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(m� 2 1 ` D rlr O p � h � i o till O n N 3 z O m � no no 3 y � SMIPLE TEMP AT COLLECTION p40F CONTNNE3S N m a as M 3 $ Unpreserved p H2304 a HNO3 -1 \ m IN HCI »pc NaOH Na23203 0R N �. j --tipfffi F Methanol Other m R r Analyses Teat YIN �pI p q x X Tss Metals-Cu, Pq 2n p 8 Oil and Greeae by 16U a pH by W40 n a" 3 m TEMP lo C 'Ti N o ,e - o' n Residual Chlorine (YIN) Russ ad on Ice (YIN) 9 phpi - — ,'� C use. Sealed 93 Cooler YIN 3 Sad Inlad (YIN)