WQ0000701_Sample Results_20080617

of V A rFR � /°4
�, William G. Ross Jr., Secretary . North Carolina Department of Environment and Natural Resources
,l
Coleen Sullins, Director
June 17, 2008
To: Owner /Resident •
Re: Water Sample Lab NO. AB30625
Michael F. Easley, Governor
Division of Water Quality
Recently, it has been discovered that some water supply wells in your area contain detectable
amounts of pesticides and associated 'agricultural chemicals.
Below, please find information related to sampling conducted on the water supply well for this
residence.
] Based on the sample results, your water is safe for all uses. It is recommended that the water be
tested every six months to make sure it is still safe.
Based on the sample results, elevated levels of the nitrates were detected. It is recommended
that the water should not be used for cooking or drinking.
The above usage guidelines were developed based on a maximum contaminate level of 10 mg/L. If
you have further questions about the usage recommendations, Dr. Rudo can be reached at
[phone] or through the division's main number at [phone].
This well was sampled by the North Carolina Division of Water Quality. Samples of water were
collected and analyzed for inorganic nutrients. Nutrients are introduced- into the groundwater in
many ways including both agricultural and residential land use activities.
The Division of Water Quality is committed to providing you with additional information, as may
be needed. If you have questions about the investigation of this issue, you may contact Stephen
Barnhardt, Aquifer Protection Section Supervisor for the Fayetteville Regional Office by calling
[phone].
North Carolina DWQ/Aquifer Protection Section 225 Green St./ Suite 714 Fayetteville, NC 28301 Phone [phone]
FAX [phone] Internet: h2o.enr.state.nc.us Customer Service 1-877-623-6748
An Equal Opportunity/Affirmative Action Employer- 50% Recycled/10% Post Consumer Paper
One
NorthCarolina
Naturally

WC DWQ Laboratory Section &sults
County: MONTGOMERY
River Basin_
Report To FROAP
Collector:. B TODD
Region: FRO
Sample Matrix: GROUNDWATER
Loc. Type: - WATER SUPPLY:
Emergency Yes/No
COC Yes/No YES
VisitID
Loc. Descr.: JEFFRRY AND ANGIE CARPENTER
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Date Reported:
Report Generated:
AB30625
8G0578
05/29/2008
08:00
MMATHIS
6/10/08
06/10/2008
90 /If /0 8
Location ID: 61062240REYNOLDSRD
Collect Date: 05/28/2008
Collect Time:: 11:45
Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
B1-Countable membranes with <20 colonies; Estimated
B2- Counts from all filters were zero.
B3- Countable membranes with more than 60 or 80 colonies; Estimated
B4-Filters have counts of both >60 or 80-and < 20; Estimated
B5-Too many colonies were present; too numerous to count (TNTC) -
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated -
N1-The component has been tentatively identified based on mass spectral library search and has an estimated value
N3-Estimated_ concentration is < PQL and >MDL
NE -No established PQL
P-Elevated PQL due to matrix interference and/or sample dilution
Q1-Holding time exceeded prior to receipt at lab.
Q2- Holding time exceeded following receipt by lab
PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
X1- Sample not analyzed for this compound
I AR
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2

Location ID: 61062240REYNOLDSRD -
Loc. Descr.: JEFFRRY AND ANGIE CARPENTER
Visit ID
NC DWQ Laboratory Section Results
Sample ID AB30625-
Collect Date: 05/28/2008
Collect Time:: 11:45
LAB
NUT
CAS # Analyte Name PQL Result Qualifier Units .Analyst/Date Approved. By /Date
Sample temperature at receipt by lab
Method Reference
1.6 °C DSAUNDERS MMATHIS
5/29/08 5/29/08
NH3 as N in liquid 0.02
Method Reference Lac10-107-06-1-J
0.02 U mg/L as N MOVERMAN CGREEN
5/30/08 6/10/08
NO2+NO3 as N in liquid 0.02 15 mg/L as N MOVERMAN CGREEN
Method Reference Lac10-107-04-1-c 5/30/08 6/10/08
Phosphorus_total as P in liquid
Method Reference Lac10-115-01-1EF
0.02 0.02 ,U mg/L as P MAJAYI CGREEN
6/2/08 6/4/08
Nitrate as N in liquid 0.02 15 mg/L as N MOVERMAN CGREEN
Method Reference Lacliat107-04-1-c 6/6/08 6/10/08
Nitrite as N in liquid 0.01
Method Reference Lachat107-04-1-c
0.01 U mg/L as N MOVERMAN CGREEN
5/29/08 6/4/08
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 2

GROUNDWATER FIELD/LAB FORM
Location code_61062 240 Reynolds Rd
County Montgomery
Quad No Serial No.
Lat. Long.
Report To: ARO FRO MRO, RRO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus, ourier, Hand Del., Other:
Collector(s):_BillTodd
SAMPLE TYPE
21 Water
❑ Soil
Other
E Chain of Custody
SAMPLE PRIORITY
❑ Routine
I. Emergency
Purpose:
Date 5'". 07 Time //.'cLS'9 f Baseline,omplaiCompliance, LUST, Pesticide Study, Federal Trust, Other:
(circle one)
FIELD ANALYSES Owner T�>'4� t/ �- /�i✓cl i e �<1,epe„(le,e
pH 400 - Spec. Cond.94 at 25°C Location or Site -2 ' 0 ,e(2q "Adds Ad, /-)v & ,X l c,1 s> ( 4/14,e./ de -. r2 2 c 2 ?
Temp.lo °C Odor /io r4 Description of sampling point
Appearance !e.,_:,-;.r?
Field Analysis ,
By:_BillTodd'
LABORATORY ANALYSES
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Lab Number
Date Receive
Rec'd By:
Other:
Data Entry By: Ck:
Date Reported:
BOD 310
- mg/L
COD High 340 J
mg/L
COD Low 335
mg/L
Coliform: MF Fecal 31616
/100m1
Coliform: MF Total 31504
/100m1
TOC 680
mg/L
Turbidity 76
NTU
Residue, Suspended 530
mg/L
pH 403
units
Alkalinity to pH 4.5 410
mg/L.
Alkalinity to pH 8.3 415
mg/L
Carbonate 445 -
'mg/L --
Bicarbonate 440 -
mg/L
Carbon dioxide 405
mg/L ,
Chloride 940 '
mg/L
Chromium: Hex 1032
ug/L
Color: True 80
CU
Cyanide 720
mg/L
Lab Comments
Sampling Method
Remarks
n'umo. bailer. etc.l
Sample Interval
Diss. Solids70300
mg/L
Fluoride 951
mg/L
Hardness: Total 900
mg/L
Hardness (non-carb) 902
mg/L
Phenols 32730
. ug/l -
Specific Cond. 95
uMhos/cm
Sulfate 945
mg/L
Sulfide 745
mg/L
Oil and Grease .
mg/L
X
NH3.as N 610
mg/L
TKN as N 625 ,
mg/L
X
NO2 + NO3 as N 630
mg/L
X
P: Total as P 665
mg/L
X
Nitrate (NO3as N) 620
mg/L.
X
Nitrite (NO2 as N) 615
mg/L
(Pumping time, air temp., etc.)
Ag-Silver 46566
ug/L
Al -Aluminum 46557
ug/L
As -Arsenic 46551
ug/L
Ba-Barium 46558
ug/L
Ca -Calcium 46552
mg/L
Cd-Cadmium 46559
ug/L
Cr-Chromium 46559
-ug/L
Cu-Copper 46562
ug/L
Fe -Iron 46563
ug/L
Hg-Mercury 71900
ug/L
K-Potassium 46555
mg/L
Mg -Magnesium 46554
mg/L
Mn-Manganese 46565
ug/L
Na-Sodium 46556
mg/L
Ni-Nickel
ug/L
Pb-Lead 46564
ug/L
Se -Selenium
ug/L
Zn-Zinc 46567
ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
X
Volatile Organics (VOA bottles/
TPH-Gasoline Range .
TPH-BTEX Gasoline Range
LAB USE ONLYc
Temperature
Temperature onn arrival (°C):
GW-54 REV. 7/03
For Dissolved Analysis -submit filtered sample and write "DIS" in block.

5 "+vT 6 -/f --O 2'
-'j:,ounty: MONTGOMERY
River Basin
.Report To FROAP
Collector: B TODD
Region: FRO
Sample Matrix; GROUNDWATER
Loc. Type: WATER SUPPLY
Emergency Yes/No
COC Yes/No YES
Location ID: 61062225MORGANRD
NC DWQ Laboratory Section Results
VisitID
Loc. Descr.: TOMMY AND JUDY RITTER
Collect Date: 05/28/2008
Collect Time:: 11:30
Sample ID:
PO Number#
Date Received:
Time Received:
Labworks LoginlD
Date Reported:
Report Generated:
Sample Depth
AB30624
8G0577
05/29/2008
08:00
MMATHIS
6/10/08
06/10/2008
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
B1-Countable membranes with <20 colonies; Estimated
B2- Counts from all filters were zero.
B3- Countable membranes with more than 60 or 80 colonies; Estimated
B4-Filters have counts of both >60 or 80 and < 20; Estimated
B5-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
N3-Estimated concentration is < PQL and >MDL
NE -No established PQL
P-Elevated PQL due to matrix interference and/or sample dilution
Q1-Holding time 'exceeded prior to receipt at lab.
Q2- Holding time exceeded following receipt by lab
PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
X1- Sample not analyzed for this compound
N1-The component has been tentatively identified based on mass spectral library search and has an estimated value
I AR
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2

Sample ID
AB30624
Location ID: 61062225MORGANRD
L'oc. Descr.: TOMMY AND JUDY RITTER
Visit ID ;s
gVC DWQ Laboratory Section Results
Collect Date: 05/28/2008
Collect Time:: 11:30
LAB
CAS # Analyte Name
PQL
Result Qualifier Units Analyst/Date Approved By /Date
NUT
Sample temperature at receipt by lab
Method Reference
1.6 `C DSAUNDERS MMATHIS
5/29/08 5/29/08
NH3 as N in liquid
Method Reference Lac10-107-06-1-J
NO2+NO3 as N in liquid
Method Reference Lac10-107-04-1-c
0.02 0.02 U mg/L as N MOVERMAN CGREEN
5/30/08 6/10/08
Phosphorus_total as P In liquid
Method Reference Lac10-115-01-1EF
Nitrate as N in liquid
Method Reference. Lachat107-04-1-c
0.02 5.3 mg/L as N MOVERMAN CGREEN
5/30/08 6/10/08
0.02 0.02 U mg/L as P MAJAYI CGREEN
6/2/08 6/4/08
Nitrite as N in liquid
Method Reference Lachat107-04-1-c.
0.02 _ 5.3 mg/L as N MOVERMAN CGREEN
6/6/08 6/10/08
0.01 - 0.01 U mg/L as N - MOVERMAN CGREEN
5/29/08 6/4/08
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 2

`GROUNDWATER FIELD/LAB FORM
Location coae_61062 225 Morgan Rd.
County. Montgomery
Quad No Serial No.
Lat. Long.
Report To: ARO FR& MRO, RRO, WaRO, WiRO,
WSRO, Kinston FO ed. Trust, Central Off., Other:
Shipped by: Bus, ourie., Hand Del., Other:
SAMPLE TYPE
® Water
❑ Soil
❑ Other
El Chain of Custody
SAMPLE PRIORITY
❑ Routine
Emergency
Collector(s):BiIITo. d
FIELD ANALYSES
pH 400 :1.
Temp.lo °C Odor ti 0214.
Appearance a /e
Field Analysis
By:_BillTodd
Date. 2tP '
Purpose:
Time '//,:CAM Baseline,
Spec. Cond.s4 at 25°C
LABORATORY A
BOD 310
mg/L
COD High 340
mg/L
COD Low 335
mg/L
Coliform: MF Fecal 31616 .
/100m1
Coliform: MF Total 31504
/100m1
TOC 680
mglL
Turbidity 76
NTU
Residue, Suspended 530
mg/L
pH 403
units
Alkalinity to pH 4.5 410
mg/L
Alkalinity to pH 8.3 415
mg/L
Carbonate 445
mg/L
Bicarbonate 440
mglL
Carbon dioxide 405
mg/L
Chloride 940
mg/L
Chromium: Hex 1032
ug/L
Color: True 80
CU
Cyanide 720
mg/L
Lab Comments
Sampling Method
Remarks
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
%0S 1b921)D
Lab Number Q�
Date Received
Rec'd By: rom:Bu
Other:
Data Entry By: Ck:
Date Reported:
Compliance, LUST, Pesticide Study, Federal Trust, Other:
(circle one)
Hand Del.,
Owner' % /4/4 y Judy. ,i'714
Location or Site .,1-13 /Mo,egl7--J £S.
is2 o(22eI/a2. 7.el'e /144 .2 7,3 2/
Description of sampling point
Sample Interval
(Pump. bailer. etc.)
Diss. Solids 70300
mg/L
Fluoride 951
mg/L
Hardness: Total 900
mg/L
Hardness (non-carb) 902
mg/L
Phenols"32730
ug/I
Specific Cond. 95
uMhos/cm
Sulfate 945
mg/L'
Sulfide 745
mg/L
Oil and Grease
mg/L
X
NH3 as N 610
. mg/L
TKN as NI 625
mg/L
X
.NO2 + NO3 as N 630
mg/L
X
P: Total as P 665
mg/L
X
Nitrate (NO3 as N) 620
mg/L
X
Nitrite (NO2 as N) 615
mg/L
(Pumping time, air temp., etc.)
Ag-Silver 46566
ug/L
Al -Aluminum 46557
ug/L
As -Arsenic 46551
ug/L
Ba-Barium 46558
ug/L
Ca -Calcium 46552
mg/L
Cd-Cadmium 46559
ug/L
Cr-Chromium 46559
ug/L
Cu-Copper 46562
ug/L
Fe -Iron 46563
ug/L'
Hg-Mercury 71900
ug/L
K-Potassium 46555
mg/L
Mg -Magnesium 46554
mg/L
Mn-Manganese 46565
ug/L
Na-Sodium 46556
mg/L
Ni-Nickel
ug/L
.
Pb-Lead 46564
ug/L
Se -Selenium
ug/L
Zn-Zinc 46567
ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
• Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
X Volatile Organics (VOA bottle) J' 1 1 2
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (°C):
GW-54 REV. 7/03
For Dissolved Analysis -submit filtered sample and write "DIS" in block.

a(S/1/7 v — —v17
NC DWQ Laboratory Section results
County:
.River Basin
Report To FROAP
Collector:
Region:
Sample Matrix:
Loc. Type:
MONTGOMERY
B TODD
FRO
GROUNDWATER
WATER SUPPLY
Emergency Yes/No
COC Yes/No YES
VisitID
Loc. Descr.: WADE AND BEVERLY SLOAN
Sample ID:
PO Number #
Date Received:
Time Received:
Labworks LoginlD
Date Reported:
Report Generated:
9a
Location ID: 61062117SANDYVALLEY
Collect Date: 05/28/2008
Collect Time:: r 12:05
Sample Depth
AB30622
8G0575
05/29/2008
08:00
MMATHIS
6/10/08
06/10/2008
tilde
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
B1-Countable membranes with <20 colonies; Estimated
B2- Counts from all filters were zero.
B3- Countable membranes with more than 60 or 80 colonies; Estimated
B4-Filters have counts of both >60 or 80 and < 20; Estimated
B5-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
J6-The lab analysis was from ah unpreserved or improperly chemically preserved sample; Estimated
N1-The component has been tentatively identified based on mass spectral library search and has an estimated value
N3-Estimated concentration is < PQL and >MDL
NE-No.established PQL
P-Elevated PQL due to matrix interference and/or sample dilution
Q1-Holding time exceeded prior to receipt at lab.
Q2- Holding time exceeded following receipt by lab
PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
X1- Sample not analyzed for this compound
I AR
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2

Sample ID
AB30622
.Location ID: 61062117SANDYVALLEY
Loc. Desch: WADE AND BEVERLY SLOAN
Visit ID
NC DWQ La6.oratory Section Results
Collect Date: 05/28/2008
Collect Time:: 12:05
CAS #
Analyte Name
PQL
Result Qualifier Units
Analyst/Date
Approved By /Date
LAB
NUT
Sample temperature at receipt by lab
Method Reference
1.6
'C
DSAUNDERS MMATHIS
5/29/08 5/29/08
NH3 as N in liquid
Method Reference Lac10-107-06-1-J
0.02 .. 0.02 U mg/L as N MOVERMAN CGREEN
5/30/08 6/10/08
NO2+NO3 as N in liquid ' 0.02 15 mg/L as N MOVERMAN CGREEN
Method Reference ' Lac10-107-04-1-c
5/30/08 6/10/08
Phosphorus_total as P in liquid 0.02
Method Reference Lac10-115-01-1EF
0.02 U mg/L as P MAJAYI CGREEN
6/2/08 6/4/08
Nitrate as N in liquid
Method Reference Lachat107-04-1-c
0.02 15 mg/L as N MOVERMAN CGREEN
6/6/08 6/10/08
Nitrite as N in liquid 0.01
Method Reference Lachat107-04-1-c
0.01 U mg/L as N MOVERMAN CGREEN
5/29/08 6/4/08
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 2

GROUNDWATER FIELD/LAB FORM
Location code_61062 117 Sandy Valley
County Montgomery
Quad No Serial No.
Lat. Long.
Report To: ARO, ROB MRO, RRO, WaRO, WiRO,
WSRO, Kinston FO ed. Trust, Central Off., Other:
Shipped by: Bus, Courier, Hand Del., Other:
Col lector(s):_Bi I ITo.
FIELD ANALYSES
pH 40o
Temp 10
oC
Appearance G;4
SAMPLE TYPE
® Water
El Soil
❑ Other
® Chain of Custody
SAMPLE PRIORITY
❑ Routine
® Emergency
Purpose:
e j2 o'..P4 Baseline, Complaint Compliance, LUST, Pesticide Study, Federal Trust, Other:
(circle one)
Datess'.2 g--of
Tim
Spec. Cond.94 at 25°C
Odor 0404e
Field Analysis
By:_BillTodd
LABORATORY ANALYSES
BOD 310
mg/L
.
COD High 340
mg/L
COD Low 335
mg/L
Coliform: MF Fecal 31616
/100m1
Coliform: MF Total 31504
/100m1
TOC 680
mg/L
Turbidity 76
NTU
Residue, Suspended 530
mg/L
pH 403
units
Alkalinity to pH 4.5 410
- mg/L
Alkalinity to pH 8.3 415
mg/L
Carbonate 445
mg/L
Bicarbonate 440
mg/L
Carbon dioxide 405
mg/L
Chloride 940
mg/L
Chromium: Hex 1032
ug/L'
Color: True 80
CU
Cyanide 720
mg/L
Lab Comments
Owner 1 , e. ,Wet/e,eI7 ''lo l»,1
Location or Site /17 6..E-,1lc/7 Aba2st,/f' /4,ern/2— Si /
Description of sampling oint W e /! // eAd
Sampling Method bum p Sample Interval
iF'umo. bailer. etc.1
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATERQUALITY-GROUNDWATER SECTION
Date Receive
Rec'd By:
Other:
Data`Entry By: Ck:
Date Reported:
Remarks
Diss. Solids 70300
mg/L
Fluoride 951
mg/L
Hardness: Total 900
- mg/L
Hardness (non-carb) 902
mg/L
Phenols 32730
ug/l
Specific Cond. 95
uMhos/cm
Sulfate 945
. mg/L
Sulfide 745
mg/L
Oil and Grease
mg/L
X
NH3 as N 610
mg/L
TKN as N 625
mg/L '
X
NO2 + NO3 as N 630
mg/L
X
P: Total as P 665
mg/L
X
Nitrate (NO3 as N) 620
mg/L
X
Nitrite (NO2 as N) 615
mg/L
(Pumping time, air temp., etc.)
Ag-Silver 46566
ug/L
Al -Aluminum 46557
ug/L
As -Arsenic 46551
ug/L
Ba-Barium 46558
ug/L
Ca -Calcium 46552
mg/L
Cd-Cadmium 46559
ug/L
Cr-Chromium 46559
ug/L
Cu-Copper 46562
ug/L
Fe -Iron 46563
ug/L
Hg-Mercury 71900
ug/L
K-Potassium 46555
•
mg/L
Mg -Magnesium 46554
mg/L
Mn-Manganese 46565
ug/L
Na-Sodium 46556
mg/L
Ni-Nickel
ug/L
Pb-Lead 46564
ug/L
Se -Selenium t
ug/L
Zn-Zinc 4656t
ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics _
TPH-Diesel Range
X
Volatile Organics (VOA bottle) pi�� 05'
TPH-Gasoline Range
TPH-BTEX Gasoline Range .
LAB USE ONLY
Temperature on arrival (°C): ' 1. (.0
•
rT
GW-54 REV. 7/03
For Dissolved Analysis -submit filtered sample and write "DIS" in block.

/tAir- G -1? - "Fr
Q unty:
Wier Basin
Report To
Collector:
Region:
Sample Matrix:
Loc. Type:
Emergency Yes/No
COC Yes/No
MONTGOMERY
FROAP
B TODD. ' .
FRO
GROUNDWATER
WATER SUPPLY
YES
NC DWQ La6oratory Section ResuCts
Visitlb
Loc. Descr.: VELMA B HAILEY
Sample ID:
PO Number#
Date Received:
Time Received:
Labworks LoginlD
Date Reported:
Report Generated:
Location ID:
61062USHWY220
Collect Date: - 05/28/2008
Collect Time:: 12:45
Sample Depth
AB30623
8G0576
05/29/2008
08:00
MMATHIS
6/10/08
06/10/2008
(0/, 170.g
Sample Qualifiers and Comments
Routine Qualifiers
Fora more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
B1-Countable membranes with <20 colonies; Estimated
B2- Counts from all filters were zero.
B3- Countable membranes with more than 60 or 80 colonies; Estimated
B4-Filters have counts of both >60 or 80 and <20; Estimated
B5-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
N1-The component has been tentatively identified based on mass spectral library search and has -an estimated value.
N3-Estimated concentration is < PQL and >MDL
NE -No established PQL
P-Elevated PQL due to matrix interference and/or sample dilution
Q1-Holding time exceeded prior to receipt at lab.
Q2- Holding time exceeded following receipt by lab
PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
X1- Sample not analyzed for this compound
I AR
Laboratory Section» 1623 Mail Service Center,Raleigh, NC 27699-1623 [phone]
Page 1 of 2

ca •
LoUation ID:., 61062USHWY220
Loc, ssr::x4 • VELMA B HAILEY
Visit ID•
NC CDWQ Laboratory Section Results
Sample ID AB30623
Collect Date: 05/28/2008
Collect Time:: 12:45
CAS #
Analyte Name
PQL
Result Qualifier Units
Analyst/Date
Approved By /Date
LAB
NUT
Sample temperature at receipt by lab
Method Reference
1.6
"C
DSAUNDERS MMATHIS
5/29/08 5/29/08
NH3 as N in liquid
Method Reference Lac10-107-06-1-J
NO2+NO3 as N in liquid
Method Reference Lac10-107-04-1-c
0.02 0.02 U
mg/L as N
MOVERMAN CGREEN
5/30/08 6/10/08
= 0.02 5.2
Phosphorus_total as P in liquid 0.02
Method Reference Lac10-115-01-1EF
Nitrate as N in liquid
Method Reference Lachat107-04-1-c
mg/L as N
.MOVERMAN CGREEN
5/30/086/10/08
0.02 U mg/L as P MAJAYI CGREEN
6/2/08 6/4/08
0.02 5.2 mg/L as N MOVERMAN CGREEN
6/6/08 6/10/08
Nitrite as N in liquid 0.01
Method Reference Lachat107-04-1-c
0.01 U mg/L as N MOVERMAN CGREEN
5/29/08 6/4/08
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 2

‘R-OUNDWATER FIELD/LAB FORM
Location code_61062 US Hwy 220
County Montgomery
Quad No Serial No.
Lat. Long.
Report To: ARO,(FROj MRO, RRO, WaRO, WiRO,
WSRO, Kinston FO ed. Trust, Central Off., Other:
Shipped by: Bus, ourie Hand Del., Other:
Collector(s):BillTodd
FIELD ANALYSES
pH 400 �CL . o
SAMPLE TYPE
a Water
❑ Soil
❑ Other
Chain of Custody
011/ North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
❑ Routine
E. Emergency
Date $ aT- t e
Purpose:
Time f1', S PtA Baseline,
Owner 1Je/M
Spec. Cond.94 at 25°C
Temp.lo °C Odor /tro.d e
Appearance Nall -a
Field Analysis
By:_BillTodd
LABORATORY ANALYSES
BOD 310
mg/L
COD High 340
mg/L
COD Low 335
mg/L
Coliform: MF Fecal 31616
/100m1
Coliform: MF Total 31504
/100m1
TOC 680
mg/L
Turbidity 76
NTU
Residue, Suspended 530
mg/L
pH 403
units
Alkalinity to pH 4.5 410
mg/L
Alkalinity to pH 8.3 415
mg/L
Carbonate 445
mg/L
Bicarbonate 440
mg/L
Carbon dioxide 405
mg/L
Chloride 940
mg/L
Chromium: Hex 1032
ug/L
Color: True 80
CU
Cyanide 720
mg/L
Lab Comments
Location or Site
Description of sampling
Sampling Method
Remarks
Lab Number
Date Receive
Rec'd By:From:Bu ouri- , Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
omplail Compliance, LUST, Pesticide Study, Federal Trust, Other:
// (ccircle one)
f 1
L/6 114a.Y auD — 15199 /�a ail /�esf End', , , - ' id 76
point Lv�+
c// &d
�N M {r�J
(Pump. bailer. etc.i
Sample Interval
Diss. Solids 70300
mg/L
Fluoride 951
mg/L
Hardness: Total 900
mg/L
Hardness (non-carb) 902
mg/L
Phenols 32730
ug/I
Specific Cond. 95
uMhos/cm
Sulfate 945
mg/L
Sulfide 745
mg/L
Oil and Grease
mg/L
X
NH3 as N 610
mg/L
TKN as N 625
mg/L
X
NO2 + NO3 as N 630
mg/L
X
P: Total as P 665
mg/L
X
Nitrate (NO3 as N) 620
mg/L
X
Nitrite (NO2 as N) 615
mg/L
(Pumping time, air temp., etc.)
Ag-Silver 46566
ug/L
Al -Aluminum 46557
ug/L
As -Arsenic 46551
ug/L
Ba-Barium 46558
ug/L
Ca -Calcium 46552
mg/L
Cd-Cadmium 46559
ug/L
Cr-Chromium 46559
ug/L
Cu-Copper 46562
. ug/L
Fe -Iron 46563
ug/L
Hg-Mercury 71900
ug/L
K-Potassium 46555
mg/L
Mg -Magnesium 46554
mg/L
Mn-Manganese 46565
ug/L
Na-Sodium 46556
mg/L
Ni-Nickel
ug/L
Pb-Lead 46564
ug/L
Se -Selenium
ug/L
Zn-Zinc 46567
ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
X
Volatile Organics (VOA bottle) 1\15 e
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY j
Temperature on arrival (°C): ( 1 l
GW-54 REV. 7/03
For Dissolved Analysis -submit filtered sample and write "DIS" in block.