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HomeMy WebLinkAboutWQ0039473_Monitoring - 03-2022_20220504 • • FORM:NDAR-1 10-13 NON-DISCHARGE APPLICATION REPORT(NDAR-1) Page of Permit No.: WQ0039473 I Facility Name: Atkinson Milling Company I County: Johnston Month: / ,1 a diNL Year: �6.4a— Field Name: Z1 Field Name: Z2 Field Name: Z3 Field Name: Did irrigation occur Area(acres): 0.52 Area(acres): 0.52 Area(acres): 0.52 Area(acres): at this facility? Cover Crop: Mix Cover Crop: Mix Cover Crop: Mix Cover Crop: Hourly Rate(in): 0.2 Hourly Rate(in): 0.2 Hourly Rate(in): 0.2 Hourly Rate(in): Annual Rate(in): 15.1 Annual Rate(in): 15.1 Annual Rate(in): 15.1 Annual Rate(in): Weather Freeboard Field Irrigated?Yes Field Irrigated?Yes Field Irrigated? Yes Field Irrigated? 4, 4 a, m °' v v v , E rn m � o of E rn a) 'D v c E T rn v � rn E O N A OI N N at al >. C 7 ?' E E 8 al d T C 7 �` E E d a ..0. T E 7 E E a1 a) T C 7 _ A U `m .. m j u p! E m 3 E 3 g a E o 3 6 •a E as '- E o@ a E a, A E o 0 `m a °- $ 3 a R La o x o 0 3 a i- .` O o o 0 3 a P '� 0 o g x o 3 a i •E c o m S o E ` N iv a .> Q J g = J > Q _ J 2 = J > Q _ J E J > Q J J m H a 8 m N °F in ft ft gal min in in gal min in in gal min in in gal min in in 1 2 3 4 5 CC-- of , 1.. -( f C-)-- 6 7 9 111 0 g �` 12 14 1 7-� l' y © &Z Jr7 15 C- 70 Z 8<( / e7 to ��. 16 at car- D,67 .. 2. r), F. 17 18 19 20 21 �J 22 70 C 1' 0,`a} 23 24 25 26 27 28 } �j 29 ((1 q 3 Cit r - t c Y'T'�l �t 1. r 1� •�._.. 30 31 Monthly Loading: ?de •, : �•�' ,,w ,y 7 t .Z 5past vi 12 Month Floating Total(in):r ;� % % tI►•�=" m.3_ .....:<, ' . FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Did the application rates exceed the limits in Attachment B of your permit? No Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Yes Was a suitable vegetative cover maintained on all sites as specified in your permit? Yes Were all setbacks listed in your permit maintained for every application to each permitted site? Yes Were all freeboards maintained in accordance with the specified freeboard heights in your permit? N/A If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective }t. /. N +,i o Aff—h-Mitinnal cheats if necessarv. Operator in Responsible Charge (ORC) Certification ORC: Andrew Wheeler Certification No.: 1006226 Grade: Phone Number: 919-631-7572 Has It ce the previous NDAR-1? No he O c anged sinLa___ Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. Permittee Certification Permittee: Atkinson Milling Company Signing official: Andrew Wheeler Signing Official's Title: Operations Manager Phone Number: 919-631-7572 Permit Exp.: 4/30/23 VV Signature Date I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDMR 03-12 NON-DISCHARGE MONITORING REPORT (NDMR) Page of Permit No.: W00039473 Facility Name: Atkinson Milling Company County: Johnston Month: /1 ctrcl Year: k. d- PPI: Flow Measuring Point: Effluent Parameter Monitoring Point: Effluent Parameter Code —► 50050 O @ Q E I- in o 0 U O u 0 O O 24-hr hrs GPD 1 C% 2 0 3 C1 4 C 5 6 7 0 8 7c e (( 9 0 10 0 11 (.7 12 �1 13 (` 14 15 7 C C if 114177 _ 16 7c.c, 17 C 18 C.) 19 20 0 21 22 7` c ! 4c V i c, 23 c3 24 25 �f,9 26 0 27 0 28 0 29 c (I '1771 30 0 31 0 Average: (Dc't: Daily Maximum: Daily Minimum: Sampling Type: /'i-ll Monthly Avg. Limit: (1 Daily Limit: Sample Frequency: FORM:NDMR 03-12 NON-DISCHARGE MONITORING REPORT(NDMR) Page of_ Sampling Person(s) Certified Laboratories Name: Andrew Wheeler Name: Microbac Name: Name: Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? If the facility is non-compliant,please explain in the space below the reason(s)the facility was not in compliance. Provide in your explanation the date(s)of the non-compliance and describe the corrective action(s)taken.Attach additional sheets if necessary. Operator in Responsible Charge(ORC)Certification Permittee Certification ORC: Andrew Wheeler Permittee: Atkinson Milling Company Certification No.: 1006226 Signing Official: Andrew Wheeler Grade: Phone Number: 919-631-7572 Signing Official's Title: Operations Manager Has the ORC changed since the previous NDMR? No Phone Nu ber: 919-631-7572 Permit Expiration: 4/30/2023 Signature Date Signature Date By this signature,I certify that this report is accurrate and complete to the best of my knowledge. I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 4micRoBAco Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Project Description Wastewater Sample For: Andrew Wheeler Atkinson Milling Company 95 Atkinson Mill RD Selma, NC 27576 Administration Brittany Smith Wednesday,April 13,2022 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc.- Fayetteville. If you have any questions,comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report.Analytical results are reported on a'as received' basis unless specified otherwise.Analytical results for solids with units ending in (dry)are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request.This laboratory report shall not be reproduced, except in full,without the written approval of Microbac Laboratories.The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 9 OMICROBACk Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Atkinson Milling Company Project Name:Wastewater Sample Andrew Wheeler Project/PO Number: N/A 95 Atkinson Mill RD Received: 03/31/2022 Selma, NC 27576 Reported: 04/13/2022 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Spray Tank, Grab K2C0470-01 Aqueous Grab 03/31/22 09:00 03/31/22 14:13 Page 2 of 9 KMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Analytical Testing Parameters 1 Client Sample ID: Spray Tank,Grab Sample Matrix: Aqueous Collected By: Andrew Wheeler k Lab Sample ID: K2C0470-01 Collection Date: 03/31/2022 9:00 k Analyses Performed by: Microbac Laboratories, Inc. -Fayetteville Microbiology Result RL Units DF Note Prepared Analyzed Analyst SM 9222 D-2015 Fecal coliforms >60000 1.0 per 100mL 1 03/31/22 1528 04/01/22 1418 SXH Inorganics Total Result RL Units DF Note Prepared Analyzed Analyst Calculation Total Nitrogen 49.2 1.00 mg/L 1 04/05/22 1700 WPR EPA 351.2,Rv.2(1993) Total Kjeldahl Nitrogen(TKN) 49.2 1.00 mg/L 1 04/05/22 1700 WPR SM 2540 D-2015 Total Suspended Solids(TSS) 867 278 mg/L 111 04/05/22 1047 SXH SM 4500-H+B-2011 pH(at 25°C) 6.0 1.0 S.U. 1 H 04/01/22 1155 SXH SM 4500-NH3 G-2011 Ammonia as N 9.28 0.200 mg/L 1 04/01/22 1654 04/01/22 1654 WPR SM 4500-P F-2011 Phosphorus as P 48 0.20 mg/L 1 04/12/22 1819 04/12/22 1819 WPR SM 5210 B-2016 Biochemical Oxygen Demand(BOD5) 2830 2.00 mg/L 1 G1,G5 03/31/22 1527 04/05/22 1120 WPR Analyses Performed by: Microbac Laboratories, Inc., Maryville Inorganics Total Result RL Units DF Note Prepared Analyzed Analyst EPA 300.0,Rv.2.1 (1993) Nitrate as N <0.500 0.500 mg/L 5 04/01/22 1524 04/01/22 1524 CSE Nitrite as N <0.500 0.500 mg/L 5 04/01/22 1524 04/01/22 1524 CSE Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 I 910.864.1920 p I www.microbac.com Page 3 of 9 ( MICROBACH Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Batch Log Summary Method Batch Laboratory ID Client/Source ID EPA 300.0, Rv.2.1 (1993) 2214301 2214301-BLK1 2214301-BS1 2214301-MS1 R2D0086-02 2214301-MSD1 R2D0086-02 K2C0470-01 Spray Tank,Grab Method Batch Laboratory ID Client/Source ID SM 5210 B-2016 KC23110 K2C0470-01 Spray Tank,Grab KC23110-BS 1 KC23110-DUP1 K2C0181-01 KC23110-BLK1 Method Batch Laboratory ID Client/Source ID SM 4500-NH3 G-2011 KD20001 KD20001-BS1 K2C0470-01 Spray Tank,Grab KD20001-DUP1 K2CO253-01 KD20001-MS1 K2CO253-01 Method Batch Laboratory ID Client/Source ID SM 9222 D-2015 KD20004 KD20004-BLK1 KD20004-BS1 K2C0470-01 Spray Tank,Grab Method Batch Laboratory ID Client/Source ID SM 4500-H+B-2011 KD20005 K2C0470-01 Spray Tank,Grab KD20005-DUP1 K2CO252-01 Method Batch Laboratory ID Client/Source ID SM 2540 D-2015 KD20411 KD20411-BLK1 KD20411-DUP1 K2C0377-01 KD20411-BS1 K2C0470-01 Spray Tank,Grab Method Batch Laboratory ID Client/Source ID EPA 351.2, Rv.2(1993) KD20412 K2C0470-01 Spray Tank,Grab KD20412-MS1 K2CO256-01 K020412-MSD1 K2CO256-01 Method Batch Laboratory ID Client/Source ID SM 4500-P F-2011 KD20814 KD20814-MS2 K2D0059-02 KD20814-MS1 K2D0007-01 KD20814-MSD1 K2D0007-01 Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 9 ( MICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 SM 4500-P F-2011 KD20814 KD20814-MSD2 K2D0059-02 KD20814-MS3 K2D0109-01 KD20814-MSD3 K2D0109-01 K2C0470-01 Spray Tank,Grab Batch Quality Control Summary: Microbac Laboratories,Inc.-Fayetteville Spike Source %REC RPD Microbiology Result RL Units Level Result %REC Limits RPD Limit Notes Batch KD20004-Wet Chem Aqueous-SM 9222 D-2015 Blank(KD20004-BLK1) Prepared:03/31/2022 Analyzed:04/01/2022 Fecal coliforms >Blank 1.0 per initial 100mL passed, but the blank final failed LCS(KD20004-BS1) Prepared:03/31/2022 Analyzed:04/01/2022 Fecal coliforms 3600 1.0 per 0-200 100mL Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch KC23110-Wet Chem Aqueous-SM 5210 B-2016 Blank(KC23110-BLK1) Prepared:03/31/2022 Analyzed:04/05/2022 Biochemical Oxygen Demand <2.00 2.00 mg/L (BOD5) LCS(KC23110-BS1) Prepared:03/31/2022 Analyzed:04/05/2022 Biochemical Oxygen Demand 136 mg/L 198 69 .59596-115.4 (BOD5) Duplicate(KC23110-DUP1) Source:K2C0181-01 Prepared:03/31/2022 Analyzed:04/05/2022 Biochemical Oxygen Demand 210 2.00 mg/L 209 0.2 30 (BOD5) Batch KD20001 -Wet Chem Aqueous-SM 4500-NH3 G-2011 LCS(KD20001-BS1) Prepared&Analyzed:04/01/2022 Ammonia as N 1.06 0.200 mg/L 1.00 106 90-110 Duplicate(KD20001-DUP7) Source:K2CO253-01 Prepared&Analyzed:04/01/2022 Ammonia as N 5.48 0.200 mg/L 5.66 3 10 Matrix Spike(KD20001-MS1) Source:K2CO253-01 Prepared&Analyzed:04/01/2022 Ammonia as N 6.99 0.200 mg/L 1.00 5.66 132 80-120 Batch KD20005-Wet Chem Aqueous-SM 4500-H+B-2011 Storm water,grabD(KD20005-DUP7) Source:K2CO252-01 Prepared&Analyzed:04/01/2022 pH(at 25°C) 5.3 1.0 S.U. 5.0 4 10 Batch KD20411 -Wet Chem Aqueous-SM 2540 D-2015 Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 9 < MICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch KD20411 -Wet Chem Aqueous-SM 2540 D-2015 Blank(KD20411-BLK1) Prepared&Analyzed:04/05/2022 Total Suspended Solids(TSS) <83.3 83.3 mg/L LCS(KD20411-BS1) Prepared&Analyzed:04/05/2022 Total Suspended Solids(TSS) 88.7 2.50 mg/L 91.0 97 95-105 Duplicate(KD20411-DUP1) Source:K2C0377-01 Prepared&Analyzed:04/05/2022 Total Suspended Solids(TSS) 6380 500 mg/L 6540 2 10 Batch KD20412-Wet Chem Aqueous-EPA 351.2, Rv.2(1993) Matrix Spike(KD20412-MS1) Source:K2CO256-01 Prepared&Analyzed:04/05/2022 Total Kjeldahl Nitrogen(TKN) 80.2 1.00 mg/L 5.00 43.4 738 90-110 Matrix Spike Dup(KD20412-MSD1) Source:K2CO256-01 Prepared&Analyzed:04/05/2022 Total Kjeldahl Nitrogen(TKN) 79.1 1.00 mg/L 5.00 43.4 715 90-110 1 10 Batch KD20814-Wet Chem Aqueous-SM 4500-P F-2011 Effluent,compositeS(KD20814-MS1) Source:K2D0007-01 Prepared&Analyzed:04/12/2022 Phosphorus as P 2.3 0.20 mg/L 2.0 0.46 94 90-110 Effluent,CompositeS(KD20814-MS2) Source:K2D0059-02 Prepared&Analyzed:04/12/2022 Phosphorus as P 2.3 0.20 mg/L 2.0 0.22 103 90-110 Effluent,CompositeS(KD20814-MS3) Source:K2D0109-01 Prepared&Analyzed:04/12/2022 Phosphorus as P 19 0.20 mg/L 2.0 16 116 90-110 Matrix Spike Dup(KD20814-MSD1) Source:K2D0007-01 Prepared&Analyzed:04/12/2022 Phosphorus as P 2.4 0.20 mg/L 2.0 0.46 97 90-110 2 200 Matrix Spike Dup(KD20814-MSD2) Source:K2D0059-02 Prepared&Analyzed:04/12/2022 Phosphorus as P 2.3 0.20 mg/L 2.0 0.22 104 90-110 0.8 200 Matrix Spike Dup(KD20814-MSD3) Source:K2D0109-01 Prepared&Analyzed:04/12/2022 Phosphorus as P 18 0.20 mg/L 2.0 16 86 90-110 3 200 Batch Quality Control Summary: Microbac Laboratories,Inc., Maryville Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch 2214301 -WetChem_IC-EPA 300.0, Rv.2.1 (1993) Blank(2214301-BLK1) Prepared&Analyzed:04/01/2022 Nitrate as N <0.100 0.100 mg/L Nitrite as N <0.100 0.100 mg/L LCS(2214301-BS1) Prepared&Analyzed:04/01/2022 Nitrate as N 2.33 0.100 mg/L 2.26 103 90-110 Nitrite as N 10.6 0.100 mg/L 10.0 106 90-110 Matrix Spike(2214301-MS1) Source:R2D0086-02 Prepared&Analyzed:04/01/2022 Nitrate as N 39.8 2.24 mg/L 3.99 36.0 96.2 90-110 Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 9 ( MICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch 2214301 -WetChem_IC-EPA 300.0, Rv.2.1 (1993) Matrix Spike(2214301-MS1) Source:R2D0086-02 Prepared&Analyzed:04/01/2022 Nitrite as N 32.3 2.24 mg/L 17.6 15.5 95.6 90-110 Matrix Spike Dup(2214301-MSD1) Source:R2D0086-02 Prepared&Analyzed:04/01/2022 Nitrate as N 40.3 2.24 mg/L 3.99 36.0 110 90-110 1.34 20 Nitrite as N 32.3 2.24 mg/L 17.6 15.5 95.1 90-110 0.277 20 Definitions B9: Target analyte is detected in the method blank at or above the method detection limit but below the method reporting limit. G1: The dissolved oxygen (DO)depletion of the dilution water blank exceeded 0.20 mg/L. G5: The glucose/glutamic acid standard exceeded the range of 198±30.5 mg/L. H: Analyte was prepared and/or analyzed outside of the analytical method holding time mg/L: Milligrams per Liter NAD: Normalized Absolute difference RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Cooler Receipt Log Cooler ID: Default Cooler Temp: 18.6°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody(COC)Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC(Name, Date&Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace,or not recd.? Yes Project Requested Certification(s) Microbac Laboratories, Inc.-Fayetteville 11 North Carolina DENR NPDES Microbac Laboratories, Inc., Maryville 678 NC Dept.of Environmental Quality Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 9 (.1 ) MICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K2C0470 Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to j^ applicable accreditation standard unless otherwise noted. The data and information on this,and other accompanying documents,represents only the sample(s)analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and Administration subject to Microbac's standard terms and conditions which can be located and reviewed at<https://www.microbac.com/standard-terms-conditions>. Reported: 04/13/2022 18:20 Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 9 Microbac-Fayetteville SHORT HOLDS ACCEPTED IvIONDAY- THURSDAY UNTIL . *K2C0470* rCHAIN OF ( 1 ! ��ROBAG Fa3e Hope Milis Rd. Number 201111 Fayetteville, NC 28306 Instructions _ — — — — TO BE COMA ,ii.9\ Turnaround Time Lab Report Address <is 6�f'T111 -5'-. �2iv C,-,in Cliente Name: Address �� t i Koutine (5 to i uusiness says)Temp. Upon Receipt(sC) I$�� Therm ID Client Name: �ry1.7C� lNli�lt7� Name: Address: C3S 11 P150.4 /KM�v p } [] RUSH*(notify lab) Holding TimeAddress: City,State,Zi( Woe- t et)L i a'75�0 City,State,Zip (needed by) Samples Received on Ice? Yes No N/A y lid l Report Type Custody Seals Intact? Yes No N/A Contact: �ppr't'w W Contact: Telephone No. q L 9 43 t -7Sj7D- Telephone N .: Results Only [ ] Level 1 -[ ] Level 2 [ ] Level3 [ ]Level 4 [ ] EDO Send Report via( j Mail [ )Fax [u a-mail LZ..L.);A .e �F'de—ry4.411 Ck •Send Invoice vi ( )Mail [ I Fax [-)a-mail �,f Location: 1 c M � 4'L5• ii) Z .[► PO No.: Compliance Monitoring? �I Yes [ I No [ ]Agency/Program Project: / _ Lee-sampler Signature: ;ampler Phone No.: q te L✓0 t 75-7, - Sampled by(PRINT): ��h"' _ amp - - Matrix Types:Soil/Solid(S),Sludge,Oil,Wipe, Drinking Water(DW),Groundwater(GW),Surface Water(SW).Waste Water(WW),Other(specify) , **Preservative Types:(1)HNO3,(2)H2SO4,(3)HCI,(4)NaOH,(5)Zinc Acetate.(6)Methanol,(7)Sodium Bisulfate,(8)Sodium Thiosulfate,(9)Hexane,(U)Unpreserved REQUESTED ANALYSIS / 1 I / / I / / / l l I /r i / k / 1 1 Grab / / / 1 / i 1 '�l l / r / / /a / / r No. of Preservative r y� + / r r O + Z r Q'r r r 1 , J r / Additional Notes • Date Time OY ! \e?/ l'n/ r v-1 "r r r + + Lab ID Client Sample ID Container atrix ** type t r� .- - G� :�/k/ / r / ! / r Collected Collected ' + ` �' ••r �' r ' r ' + + r I ' 5 Comp - [' r �I/ • / i'" �/ / / I / / , r ; 0\ Spy`'( (_ 3 -3l a� ... ;��ca E t «l tl 1•--•^_._.�...i---..�._... __..T-----• r +-_-..._4 4 +...-.. • . v N. ) I 1 Sam C] Di •ose as appropriat turn . ]Archive Possible Hazard Identifi< [] Hazardous [] N n-Hazardous [] Radioactive - — Comments t, -atu• j3 - c(�t . -,,'. �J 3 Date/TimP ` ived ture , �R ngwshed By{signature) ` 45- _- •-„- i•n.t' ., m+ ..;.4.,-. ,mP To Rel. ,wished By(si nature) Date/Time ,�� � - „( � (!� '�.J a 63. 31 ja 0. - ( i -...... .- . ` . _... e B - na " -T_ Re eived By(signetIiii •;Relinquished By (signature) Date/Time I Page 9 Of 9 1� l (tmo