Allen Steam Facility - Duke Energy (19)

IkO
Duke
Energy.
February 17, 2011
Mr. Bradley Bennett
Division of Water Quality
Stormwater Permitting Unit
North Carolina Department of Environment
and Natural Resources
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: NPDES Stormwater Permit Application
Allen Steam Station
Dear Mr. Bennett:
CORPORATE EHS SERVICES
Duke Energy
526 South Church St.
Charlotte, NC 28202
Mailing Address:
EC13K / PO Box 1006
Charlotte, NC 28201-1006
��r= lLgOWR O
E
2 l 2011
DENR - WATER
Branch
Duke Energy requests a stormwater discharge permit for the Allen Steam Station located in
Gaston County, North Carolina. Please find attached three sets of the following documents
related to this permit request:
a. EPA Form 1;
b. EPA Form 2F;
C. EPA Form 2F Supplemental Information;
d. Available stormwater analytical data;
e. DWQ ROS Request Form;
f. ROS Form Supplemental Information;
g. Site Location Map
h. Site Stormwater Plan Drawing
Numerous stormwater outfalls are located at the Allen Steam Station. The accompanying
stormwater analytical data was obtained from samples collected at outfalls SWO08 and SWO15
during June 2009 and April 2009, respectively.
Please contact me at [e-mail] or at 704-634-7098 if you have any
questions or need any additional information.
Sincerely,
Mark McGary, P.E.
Environmental, Health & Safety
www.duke-energy.com

Please print or type in the unshaded areas
EPA ID Number (copy from item/ of Form 1)
Form Approved. OMB No. 2040-0086
Approval expires 5-31-92
Form
2F
NPDES
States Environmental Protection Agency
Washington, DC 20460
Washington,
��r�EP Application for Permit to Discharge Storm Water
Discharges Associated with Industrial Activit
Paperwork Reduction Act Notice
Public reporting burden for this application is estimated to average 28.6 hours per application, including time for reviewing instructions, searching existing data
sources, gathering and maintaining the data needed, and completing and reviewing the collection of information. Send oomments regarding the burden estimate,
any other aspect of this collection of information or suggestions for improving this form, including suggestions which may increase or reduce this burden to: Chief,
Information Policy Branch, PM -223, U.S. Environmental Protection Agency, 401 M St, SW, Washington, DC 20460, or Director, Offioe of Information and Regulatory
Affairs, Office of Management and Budget, Washington, DC 20503.
I. Outfall Location
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. Outfall Number D. Receiving Water
list B. Latitude C. Longitude name
SW 008
II. Improvements
A. Are you now required by any Federal, State, or local authority to meet any implementation schedule for the construction, upgrading or
operation of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described
in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance
schedule letters, sti ulations, court orders, and grant or loan conditions.
4. Final
1. Identification of Conditions, 2. Affected Outfalls Com liance Date
Agreements, Etc. number source of discharge 3. Brief Description of Project a. req. b. proj.
B. You may attach additional sheets describing any additional water pollution (or other environmental projects which may affect your discharges)
you now have under way or which you plan. Indicate whether each program is now under way or planned, and indicate your actual or planned
schedules for construction.
M. Site Draina a Ma
Attach a site map showing topography (or indicating the outline of drainage areas served by the outfall(s) covered in the application if a
topographic map Is unavailable) depicting the facility including: each of its intake and discharge structures; the drainage area of each storm
water outfall; paved areas and buildings within the drainage area of each stone water outfall, each known past or present areas used for
outdoor storage or disposal of significant materials, each existing structure control measure to reduce pollutants in storm water runoff,
materials loading and access areas, areas where pesticides, herbicides, soil conditioners and fertilizers are applied; each of its hazardous
waste treatment, storage or disposal units (including each are not required to have a RCRA permit which is used for accumulating hazardous
waste under 40 CFR 262.34); each well where fluids from the facility are injected underground; springs, and other surface water bodies which
receive storm water discharges from the facility.
EPA Form 3510-21' (Rev. 1-92) Page 1 of 3 Continued on Page 2

Cnnhnue(ttfmm4ha Frnnt
IV. Narrative, Description, of,Polltitai*Sources.
A For each'outfall,;provide an estimate, of the,area (include unds),of impervious surfaces^(including paved areas and buddmg1roofs) drained,
to,the outfall and -an estimate,of the total sutface�area drained by the outfall
Outfall
Area o&Impervious Surface,
Total Area Drained
Outfall
Area of Impervious Surface
Total Area Drained
Number
rovide units(provide
units)
Number
rowde,units(provide
units
SW008
B Provide a narrative description of significant materials that are currently or in the past three years have been°treated, stored or disposed
in a manner to allow exposure to storm water, method of treatment, storage, or disposal, past and present materials management
practices employed,to minimize contact by these materials with storm water runoff, materials loading and access areas, and the location,
manner, and1requency in which pesticides, herbicides,,soil conditioners, and fertilizers area lied
C For each outfall, provide the location and a description of existing structural and nonstructural control measure's to reduce pollutantsvn
storm water runoff, and a description of the treatment the storm water receives, including the schedule and type of maintenance for
control and treatment measures and the ultimate disposal of any solid or fluid wastes other than by discharge
Outfall
List Codes from`
Number
Treatment
Table 2F-1
S W008 3
V. Non Stormwater Discharges
A I certify under ,penalty of law that the outfall(s) covered by this application have been tested or evaluated for the presence of
nonstonnwaier discharges, and that all nonstormwater discharges from these outfall('s) are identified in either an accompanying Form'2C
or'Form 2E a lication for the outfall
Name of Official Title (type or pent)
Signature
Date Signed
B provide a,descri tion of the method used, the date of anyttesting, and the onsite drainage points that were directly observed during a test
Vi. Sign ificant'Leaks or S ills
Provide existing information regarding the history of significant leaks or spills of toxic or hazardous pollutants at the facility in the last three
ears, including the approximate date and location of the,s ill or leak, and the type and amount of material released
EPA Form,3510-2F (Rev 1-92) Page 2 of 3 Contmued on Page 3

EPA ID Number (copy from Item I of Form 1)
Continued from Page 2
VII. Discharge, I nformati LL
A,B,C, & D See,instruchon before proceeding Completwone,set of tables for each outfall, Annotate the outfall number in the space provided
Tables Vii -A, VII -B, and VII -C are'mcluded on,se arate sheets numbered \1114and VIP2
E Potential discharges not,covered by analysis - is any toxic,pollutant listed in table 2F-2, 2F-3, or 2F-4, a,substance or a component of a
substance which you currently use,or manufacture as an mterrnediate or final product or byproduct?
❑ Yes (bst,all such pollutants below) ❑ No (go to Section lX)
VIII. Biological Toxicity_ Testi ng Data
Do you have any knowledge or reason'to believe that any biological test for acute or chronic, toxicity has been made on any of your discharges or
on a,receiwng water in relation to,your discharge within the last 3 years?
❑ Yes (list all such pollutants below) ❑ No (go to Section DO
IX. Contact analysis Information
Were any of the analysis reported in item VII performed by a°contact laboratory or consulting firm?'
® Yes (list the name, address, and telephone number, of, and pollutants ❑ No (go, to Section X)
analyzed by, each such laborato or firm below
A Name
B Address
C Area Code & Phone No
D Pollutants Analyzed
Shealy Environmental,Services 106 Vantage Point Drive 803-791-9111 Wet chemistry &
West Columbia, SC 29172 metals
GEL Laboratories LLC 2040 Savage Road 843-556-8171 Radiologicals
Charleston, SC 29407
X. Certification
I certify under penalty of law that this documentand all attachments were prepared under my direction or
supervision- In accordance with a system designed, to assure that.'qualified'personnel properly gather and evaluate
the,informatron submitted BasedRon my, inquiry, oftheperson, orpersons who manage the �system,or those persons,
directly responsible for gathenng the information, the information submitted is, to the best, of my knowledge and
belief, true; accurate, and,complete I am,aware°that there are,slgniffcant penalties for,submitting.false information, ?
includin athe possibility. of fine,and imprisonment for knowing, violations
A Name &'Official Tale (type-orpnnt)
B -Area Code -and Phone,No
C Signature
D Date Signed
EPA Form 3510-2F (Rev 1-92) Page 3 of 3

EPA ID Number (copy from Item I of Form 1)I Form Approved. OMB No. 2040-0086
Approval expires 5-31-92
VII. Discharge Information Continued from page 3 of Form 2F)
Part A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See
instructions for additional details.
Maximum Values
Average Values
Number
Pollutant
include units
include units
Of
And
Grab Sample
Grab Sample
Storm
CAS Number
Taken During
Flow -weighted
Taken During
Flow -weighted
Events
(if available)
First 30
Composite
First 30
Composite
Sampled
Minutes
Minutes
1
Sources of Pollutants
Oil & Grease
<4.8 mg/L
Biological Oxygen
< 2.0 mgt
Demand BOD5
Chemical Oxygen
80 mg/L
Demand COD
Total Suspended
1500 mg/L
Solids TSS
Total
0.52 mg/L
j
Nitrogen
Total
0.98 mg/L
Phosphorus
H _ _
Minimum
Maximum
Minimum
Maximum
Part B - List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES
permit for its process wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall.
See the instructions for additional details and re uirements.
Maximum Values
Average Values
Number
Pollutant (include units)
(include units)
Of
And Grab Sample
Grab Sample
Storm
CAS Number Taken During Flow -weighted
Taken During
Flow -weighted
Events
(if available) First 30 Composite
First 30
Composite
Sampled
Minutes
Minutes
Sources of Pollutants
Bromide (24959-67-9)
Chlorine, Total
residual
Ammonia (as N)
Chloride
< 1.0 mg/L
Color
20 units
Fluoride (16984-48-8)
0.30 mgdL
Nitrate -Nitrite (as N)
< 0.020 mg/L
Radioactivity, alpha
21.4 t 3.78
total
Ci/L
Radioactivity, beta
42.8 t 3.84
total
pCi/L
Radioactivity, radium
3.86 t 0.877
total I
pCilL
Radioactivity, radium
1.02 t 0.349
226 total
pCilL
Sulfate (as SO4)
26 mg/L
1
14806-79-8
Sulfite (as S03)
14265-45-3
Aluminum, Total
27.0 mg/L
1
7429-90-5)
Barium, Total
0.470 mg/L
1
7440-39-3
Boron, Total (7440-
<0.050 mg/L
42-8)
Cobalt, Total (7440-
0.026 mg/L
48-4
Iron, Total (7439-89-6)
36.0 mg/L
Magnesium, Total
17.0 mg/L
7439-95-4
Molybdenum, Total
7439-98-7)
Manganese, Total
1.00 mg/L
7439-96-5
Tin, Total
<0.005 mg/L
7440-31-5
EPA Form 3510-2F (Rev. 1-92) Page VII -1 Continue on Reverse

Titanium, Total
2.20 mg1L
7440-32-6
Antimony, Total
7440-36-0
Arsenic, Total
<0.050 mg1L
1
7440-38-2
Beryllium, Total
< 0.001 mg/L
j
7440-41-7
Cadmium, Total <0.00010
7440-43-9 mg1L
Chromium, Total 0.020 mg/L
7440-47-3)
1
Copper, Total
0.058 mg/L
7440-50-8
Lead, Total
7439-92-1
Mercury, Total
0.00014 mg1L
7439-97-6
Nickel, Total
0.019 mg1L
7440-02-0
Selenium, Total
<0.050 mg1L
7782-49-2
Silver, Total
<0.005 mg1L
1
7440-22-4
Thallium, Total
7440-28-0
Zinc, Total
0.320 mg1L
7440-66-6
EPA Form 3510-2F (Rev. 1-92) Page VII -I Continue on Reverse

Continued from the Front
Part1C - List each pollutant showmin Tables 2F-2, 2F-3, and 2F-4 that you know or have reason -to beheveis present See the`mstrudrons for
additional details and,requirements ,Com lete`one table,for each outfall
Maximum Values AverageValues, Number
Pollutant include units include units Of
And Grab,Sample Grab Sample Storm
CAS'Number Taken During Flow -weighted Taken During Flow -weighted Events
(if available) First 30 Composite First 30 Composite Sampled
Minutes Minutes Sources of Pollutants
Cyanide, Total
(57-12-5)
Phenols,, Total
Surfactants (MBAs)
Fecal Coliform CHT` 546• col/100 1
mL
*analyzed outside
holding time
PartD - Provide, data for the'storm events which resulted in the maximum values for the flow weighted composite sample
1
Date of
Storm
Event
2
Duration
of Stone Event<
(in minutes)
3
Total rainfall
dunng,storrn event
(in inches )
4,
Number of hours,between
and beginningen storm measured
measurable d,oprevious+
ram event-
5
Total'flow,from
rain event,
(gallons or specify units)
7 Provide a description of the method, of flow measurement or,'estunate
EPA Form 3510-2F (Rev 1-92) Page VII -2

Duke
Analytical, Laboratory
'�1%e��Y®
13339 Hagers Perry Roads
Huntersville; NC 28078-7929,
Fl -07 -os -o7
McGuire Nuclear Complex — MG03A2
Phone [phone], Fax [phone]
J®b Summary Report
Job Number: F 09-JUN=0240
Project Name:
Customer, Name:
Copy To:
Customer Address:
Allen Storm Water
Brandy Starnes; Josh Quinn
Don Scru22s. Allen Stowe. Robert Wvhe
MG03A3
Lab Contact: Mary Ann Ogle
Lab Contact Phone: [phone]
Report Authorized By:
(Printed Name)
Report Authorized By:
(Signature)
Mary Ann Ogle
t -t_. Date. / (�
Data Package
This data package includes analytical results that are applicable only to the samples
described in this narrative An estimation of the uncertainty of measurement for the
results in the report is available upon request. This report shall not be reproduced, except
in.full, without the written consent,of the Analytical Laboratory. Please contact`the
Analytical Laboratory with any questions. The order of individual sections within this
report is as follows -
Job Summary Report
Analytical Laboratory,Certificate ofAnalysis
Analytical Laboratory QC Reports (if applicable)
Sub -contracted Laboratory Results
Customer Specific Data Sheets, Reports & Documentation (if applicable)
Customer Database Entries
Test Case Narratives
Chain of Custody (COC)

Duke, Analytical Laboratory
/Energy® 13339 Ferry Road
PHuntersvilleille, NC 28078-7929
Rev 07-09-07 McGuire Nuclear. Complex — MG03A2
Phone [phone] Fax [phone]
Job Summary Report
Certification
The Analytical,Laboratory holds the followmg'Certifications
New York State Department of Health Certification # 11717(NEL4C)
North Carolina Department of Health & Human,Services Certification # 37804
South Carolina (DHEC) Laboratory ID # 99005
North Carolina (DENR) Certification # 248
Analytical results listed in this report may not be certifie&by the authorities referenced above.
Contact the Analytical Laboratory for definitive- information about the certification status,of
specific methods. The results meet all requirements of NELAC except where deviations are
noted in this report
Data Flags
Any analytical tests,or individual analytes within a test'flagged with an "X" or a "1"' indicate a
deviation from the method quality system or quality control requirement
Calculations
All results are reported on a,wet weight basis unless otherwise noted
Sample Ill's & DescriDtions:
Collection Sample
Sample ID Plant/Station Date Collected By Description
-------------------------------------------------------
29015392 FOSSIL 6/05/2009 JOSH R QUINN ALLEN SWO08
-----------------
1 TOTAL SAMPLES
-----------------

Duke Analytical Laboratory
OEner, 13339 Hagers Ferry Road
a gy `Huntersville, NC 28078-7929
Re. 07-09-07 McGuire Nuclear Complex — MG03A2
Phone [phone] Fax [phone]
Job Summary Deport
Validation of Analytical Data Package
COC and- pdf report are in agreement with, sample totals
and analyses (compliance programs and procedures).
ii) All results are less than the laboratory reporting limits
iii) All laboratory QA/QC requirements are acceptable `
NPDES and TCLP results are below permit or regulatory
iv)' limits respectively
It iv) above is No, document below
Permit
Variable Result Limit Notes
Yes
1-` No
{ ,Yes
1✓ No
W Yes
r No
Customer Specific Data Sheets, Reports &
V) Components of the Job Summary Report arranged in order ryesNo
stipulated on page one Fr
Indicate components included:
I✓
Job Summary Report
F
Customer Specific Data Sheets, Reports &
Documentation (if applicable)
r
Analytical Laboratory Certificate of
1✓
Customer Database Entries
Analysis
F,
Analytical Laboratory'QC Report
r
Test Case Narratives
(if applicable)
r
Sub -contracted Laboratory Results
r'
Chain of Custody
vi) Notes and Additional Information
The,SW 008 sample for the fecal coliform test was,analyzed outside the holding time (6hours)
for this parameter. The sample was collected on, 6/5/09 at 06:06, but was not received by Shealy
until 16 15. The�sample results,for the fecal coliform test, should be considered estimates.
Mary'Ann•Ogle,
Duke,Energy Analytical' Lab
Office -704-875-5274
Cell 70-4-280-7956

h
C
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysts
Duke Energy Corporate EHS
13339 Hagers Ferry Rd
Bldg 7405
Huntersvllle, NC 28078
Attention Mary Ann Ogle
Project Name Allen Steam Station - Stormwater
Project Number LIMS #09 -JUN -0240
Lot Number KF05057
Date Completed 06/19/2009
4'pe0A
Grant Wilton
Project -Manager
'
This report shall not be reproduced, except in its entirety, without the written approval of Shealy, Environmental Services, Inc
The following non -paginated documents are considered part of this report Chain of Custody Record and Sample Receipt Checklist
I IIIIIIII II'I IIII I'III III�I'II'I VIII Ifll Ilii
Shealy Environmental Services. Inc Page 1 of 7
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Level 1 Report v2 1

SHEALY EN==VIRONMENTAL SERVICES, INC.
SC DHECINo 320110 NELAC NoiE87653, NC DEHNRiNo 329
Case Narrative,
Duke Energy Corporate EHS
Lot Number KFO5057
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative The sample
receiving date is documented in the header information associated,with each sample
Sample receipt, sample analysis, and data review have been performed In accordance with,the,most current approved NELAC standards, the
Shealy Environmental Services, Inc ("Shealy") Quality Assurance, Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies Any exceptions to,the NELAC+standards, the QAMP„SOPs or policies are qualified,on;the results page or discussed,below
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc Page 2 of 7
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample -Summary
Duke Energy, Corporate EHS
Lot Number: KF05057
Sample Number Sample ID Matrix Date Sampled Date Received
001 Allen SW008 Aqueous 06/05/2009 0606 06/05/2009
(1 sample)
1 � �
Shealy Environmental Services Inc
106 Vantage,Pomt Drive West Columbia, SC 29172 (803)191'-9700 Fax [phone] www shealylab cam
Page 3 of 7
Leve) 1 Report v21

(20 detections)
Shealy Environmental Services, Inc, Page, 4 of 7
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab cam Level 1 Report v2 1
SHEALY ENVIRONMENTAL-
SERVICES, INC.
Executive, Summary
Duke Energy, Corporate
EHS
Lot Number: KF05057
Sample Sample ID
Matrix
_Parameter
Method
Result Q
Units
Page
001
Alien SWO08
Aqueous
COD
SM 5220D
80
mg/L
5
001
Allen SWO08
Aqueous
Fluoride
3000
030
mg/L
5
001
Allen SWO08
Aqueous
Phosphorus
3651
098
mg/L
5
001
Allen SW008
Aqueous
Platinum -Cobalt Color
SM 2120B
20
color
5
001
Allen SWO08
Aqueous
Sulfate
3000
26
mg/L
5
001
Allen SWO08
Aqueous
TKN
351 2
052
mg/L
5
001
Allen SWO08
Aqueous
TSS
SM 2540D
1500
mg/L
5
001
Allen SWO08
Aqueous
Fecal Coliform -MF
SM 9222D
546 H
col/100
5
001
Allen SW008
Aqueous
Aluminum
2008
27000
ug/L
6
,001
Allen SWO08
Aqueous
Barium
2008
470
ug/L
6
001
Allen SWO08
Aqueous
Chromium
2008
20
ug/L
6
001
Allen SWO08
Aqueous
Cobalt
2008
26
ug/L
6
,001
Alien SWO08
Aqueous
Copper
2008
58
ug/L
6
001
Allen SWO08
Aqueous
Iron
2008
36000
ug/L
6
001
Allen SW00B
Aqueous
Magnesium
2008
17000
ug/L
6
001
Allen SWO08
Aqueous
Manganese
2008
1000
ug/L
6
001
Allen SWO08
Aqueous
Nickel
2008
19
ug/L
6
001
Allen SW008
Aqueous
Titanium
2008
2200
ug/L
6
001
Allen SWO08
Aqueous
Zinc
2008
320
ug/L
6
001
Allen SWO08
Aqueous
Mercury
2451
000014
mg/L
7
(20 detections)
Shealy Environmental Services, Inc, Page, 4 of 7
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Inorganic non-metal's
Client Duke Energy Corporate EHS Laboratory ID 'KF05057-001
Description Allen,SW008 Matrix Aqueous
Date Sampled 06/05/2009 0606
)ate Received 06/05/2009
Run
Prep Method Analytical Method
Dilution
Analysis Date
Analyst
Prep Date
Batch
1
(BOD, 5,day) SMi5210B,
1
06/11/2009 1425
BM
06/06/2009 0802
5056
1
(Chloride) 300 0
1
06/17/2009 1042
DAS
3000
12601
1
(COD) SM 5220D
1
06/16/2009 1750
HBB
06/16/20091130
10
1
(Fiuonde) 300 0
1
06/17/2009 1042
DAS
010
12643
1
(Nitrate-Nltr) 353`2
1
06/16/2009 1615
WD
mg/L
12571
1
(Phosphorus) 3651
10
06/17/2009 2252
SLH
06/16/2009 1239
12522
1
(Platinum-Cob)'SM
1
06106/200911630
MML
'Sulfate
3000
1
(Sulfate) 300 0
1
06/17/2009 1042
DAS
351 2
12644
1
351 4 (TKN) 351 2
1
06/1712009 1745
SLH
06/,16/2009 1000
12503
1
(TSS) SM 25400
1
06/11/2009 1308
HBB
2
12248
1
(Fecal Collfo),SM
1
q%qffMZMMffM
MML
mg/L
1
1
(HEM (oil and) 1664A
1
06/09/2009 1600
JKP
12098
PQL - Practical Quantitabon limit B - Detected to the method blank E = Quantitation of compound exceeded the call bration range
No - Not detected at or above the PQL J - Estimated result c PQL and MDL F- The RPD between two GC columna exceeds 40%
Where applicable all soil sample analysts are reported on a dry weight basis unless gagged with a,•W' N = Recovery is out of criteria
Shealy, Environ mental Services; Inc Page 5 of 7
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
BOD, 5 day
SM 52108
ND
20
mg/L
1
Chloride
3000
ND
10
mg/L
1
COD
SM 5220D
80
10
mg/L
1
Fluoride'
3000
030
010
mg/L
1
Nitrate -Nitrite - N
3532
NO
0 020
mg/L
1
Phosphorus
7723.14-0 3651
098
010
mg/L
1
Platinum -Cobalt Color
SM 21208
20
so
color units
1
'Sulfate
3000
26
1 0
mg/L
1
TKN
351 2
052
0`50
mg/L
1
TSS
SM 2540D
1500
40
mg/L
1
Fecal Coliform -MF
SM 9222D
546 Vilb
2
col/100mL
1
HEM (oil and1grease)
1664A
ND
48
mg/L
1
PQL - Practical Quantitabon limit B - Detected to the method blank E = Quantitation of compound exceeded the call bration range
No - Not detected at or above the PQL J - Estimated result c PQL and MDL F- The RPD between two GC columna exceeds 40%
Where applicable all soil sample analysts are reported on a dry weight basis unless gagged with a,•W' N = Recovery is out of criteria
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ICP -MS
Client: Duke Energy Corporate EHS Laboratory ID: KF05057-001
Description: Allen SW008 Matrix: Aqueous
Date Sampled: 06105/2009 0606
Date Received: 06/05/2009
Run Prep Method
1 200.2
2 200.2
Analytical Method Dilution Analysis Date
200.8 1 06/12/2009 2149
200.8 10 06/19/2009 1533
Analyst
FTS
FTS
Prep Date
05/11/2009 2230
06/11/2009 2230
Batch
12292
12292
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Aluminum
7429.90-5
200.8
27000
50
ug/L
1
Arsenic
7440-38-2
200.8
NO
50
ug/L
2
Barium
7440-39-3
200.8
470
50
ug/L
1
Beryllium
7440-41.7
200.8
ND
1.0
ug/L
1
Boron
7440-42-8
200.8
NO
50
ug/L
1
Cadmium
7440-43-9
200.8
NO
0.10
ug/L
1
Chromium
7440-47-3
200.8
20
5.0
ug/L
1
Cobalt
7440-4811
200.8
26
5.0
ug/L
1
Copper
7440-50-8
200.8
58
10
ug/L
1
Iron
7439-89-6
200.8
36000
20
ug/L
1
Magnesium
7439-95.4
200.8
17000
50
ug/L
1
Manganese
7439-96-5
200.8
1000
10
ug/L
1
Nickel
7440-02-0
200.8
19
10
ug/L
1
Selenium
7782-49-2
200.8
NO
100
ug/L
Silver
7440-22-4
200.8
NO
5.0
ug/L
1
Tin
7440-31.5
200.8
ND
5.0
ug/L
1
Titanium
7440-32-6
200.8
2200
5.0
ug/L
1
Zinc
7440-66.6
200.8
320
100
ug/L
2
PQL . practical quanlllatlon limit B Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND - Not detected at or above the PQL J = Estimated result < POL and? MDL P = The RPD between two GC columns exceeds 40%
Where applicable, ail soil sample analyms are rationed on a dry weight basis unless flagged with a W N = Recovery is out of criteria H =Out of holding time
Shealy Environmental Services, Inc. Page: 6 of 7
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealy(ab.com Level 1 Report v2.1

11
f CVAA
Client Duke Energy Corporate➢EHS' Laboratory ID KFO5057-001
Description Allen SWO08 Matrix Aqueous
Date Sampled 06/05120090606
Date Received 06/05/2009
Run Prep Method
1
Analytical Method, r Dilution Analysis,Date Analyst
2451 1 06/69/2009 2248 BNW
Prep'Date
06/09/2009 1630
Batch
12063
CAS Analytical
Parameter
Number Method
Result Q
PQL Units Run
Mercury
7439.97-6 2451
0.00014
000010 mg/L 1
POL - Practical quantitation limit, a a Detected in the method blank E - Odantdabon of compound exceeded the calibration range
ND = Not detected at or above the POL J Estimated result x,POL and > MDL P = The RPD between two OC Columns exceeds 40%
Where applicable all soil sample analysis are reporlad on a dry weight basis unless flagged with a W" = Recovery is out of onions H = Out of holding 4me
Shealy Environmental Services, IncPage 7 of l
106 Vantage Point`Drive 'West Columbia, SC 29172' [phone] Fax,(803) 791- 9111 www shealylab com Level PReport v2 f
L1

j
0
QC Summary
Shealy Environmental Services, IncQC' Data for Lot Number KF05057
106Wantage,Point Dnve West,Columbia, SC 29172 [phone], Fax[phone] www shealylab com Level VReport Q 1
r

Inorganic non-metals - MB,
Sample ID KQ12248-001 Matrix Aqueous
Batch.12248
Analytical Method SM 2540D
Parameter Result Q Dil PQL Units Analysis Date
TSS ND 1 10 mg/L 06/11/20091308,
-✓
PQL - Practical QuaMitabon limit P - The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
ND - Not detected at or, above the POL J - Estimated result < POL and _> MDL +- RPD is out of criteria
Where applicable ail sod sample analysis are reported on a dry welght basis unless flagged with a
Note. Calculationsyare performed before round Ing4oravoldiround-offlerrorsllrocalculated results,
Shealy Environmental Services, Inc. QC Data for Lot Number- KFO5057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shaalylab cam Level 1 Report v21

i
E,
Inorganic non-metals, - LCS=
Sample ID KQ12248-002 Matrix Aqueous
Batch 12248
Analytical -Method SM 2540D
Spike
Amount Result % Ree
Parameter (mg/L) (mg/L) Q Dil % Rec Limit AnalysisiDate
TSS 500 490 1 98 90-110 06/11/20091308
PQL - Practical quantltation limit P - The RPD between two GC columns exceeds 40% N Recovery is out of criteria
ND - Not detected at cr above the PQL- J - Estimated result < PGL and > MDL • - RPD Is out of criteria
Where applicable all sod sample analysis are reported on a dry weight basis unless nagged with a W
Note Calculations are performed -before rounding to avoid round -off errorslin calculated�results
Shealy Environmental Services, Inc QC Data for Lot Number KF05057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab com Level 1 Report v2 1

( - Inorganic non-metals - MB
Sample ID KQ12503-001 Matrix. Aqueous
Batch 12503 Prep Method 351 4
Analytical Method 351 2 Prep Date 06/y16/2009, 1000
Parameter Result Q DII PQL Units Analysis Date
TKN ND 1 050 mg/L 06/17/2009 2025
r
POL - Practical quanlltation limit P = The RPD between two l9C,00lumns exceeds 40% N - Recovery is out of criteria
�NO = Not detected at or above the POL J - Estimated result < PQL and - MDL +- RPD is out of, criteria
' Where applicable, all sail sample analysts are reported on a dry weight basis unless flagged with a,"W' -
f
j Note- Calculations+are performed before,rounding,to avoid round-off,errore,,in,calculated results
u
iI
Shealy Environmental Services, Inc QC Data for Lot,Number KFO5057
E 106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Levet 1 Report v2 1

Inorganic non-metals- LCS,'
SampleJD KQ12503-002 Matrix •Aqueous
Batch 12503 Prep Method: 3514 1
Analytical; Method 3512 PreplDate 06/16/2009.1000
Spike
Amount. 'Result % Rec
_Parameter (mg/L), (mg/L) Q Dil % Rao Limit Analysis Date
TKN 20 1 9 1 94 90-110 06/17/20091736
i
PQL - Practical Quantitation limit P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
i ND - Not detected at or above the PQL J = Estimated result - PQL and > MDL + - RPD Is out of criteria
Where applicable, all soil sample analis are reported on a dry weight basis unless gagged with a'W'
Note Calculations are performed before rounding to,avold round -off errors in calculated results
Shealy Environmental Services, Inc QC Data for Lot Number KFO5057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab com Laval 1 Report v21

Inorganic non-metals - MB,
Sample ID KQ12522=001 Matrix Aqueous
Batch +12522 Prep Method, 3651
Analytical Method 365 1 Prep Date 06/16/2009 1239
Parameter Result Q Oil PQL Units_ Analysis Date
Phosphorus ND 1 0 010 mg/L 06/17/2009 2237
PQL = Practical quantitation limit P - The RPD'between two GC columns exceeds 40% N - Recovery is out of altena
ND - Not detected at or above the PQL J - Estimated result < PQL and > MDL • - RPD is out of criteria
Where applicable all soil sample analysis are reported on a dry weight basis unless flagged with a
Note Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc QC Data for Lot Number KF05057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax[phone],1 www shealylab com 'Level 1 Repon v21

Inorganic non-metal`s -'L-CS
Sample4D -KQ12522-002 Matrix -Aqueous
Batch 12522, Prep" Method- 365.1
Analytical)Method 365.1 P_rep,Date. 06/16/2009 ,1239
Spike'
Amount Result % Ree
Parameter (mg/L)' (rn61L) Q DI_I%Aec Limit Analysis Date,
Phosphorus 0125 d24 1 97 90-110 06/17/2009 2237
PQL - Practical gaantitation4imd P—The RPD between two GC columns exceeds 40% N Recovery is out of criteria,
NO -Not detected at or above the)PQL J = Estimated result < PQL and'>iMDL RPD Is out of criteria
Where applicable all soil sample analysts are reported on a dry weight basis unless flagged with a W, '
Note , Calculations are perfortriedlbefore rounding to avold,round-off errors in calculated results
Shealy, Environmental Services, Inc QC'Dataifor'Lot Number KF05057
106 Vantage PointiDnve West, Columbia,, SC 29172 [phone] Fax [phone], www shealylab com, LavelO Reportv2 t,

Inorganic non-metals - LCSD
i
( Sample ID KQ12522-003 Matrix Aqueous
! Batch 12522 Prep Method 365 1
!j Analytical Method 365 1 Prep Date 06/16/2009 1239
Spike
Amount, 'Result % Roo % RPD
Parameter (mg/l.) (mg/L) Q Dil % Rec %,RPD_ Limit Limit Analysis Date
Phosphorus 025 024 1 98 075 90-110 20 06/17/2009 2237
POL - Pracbcal quantitation limit P - The RPD between two GC columns exceeds 40% N -Recovery is out of criterla
NO = Not detected at or above the POL J = Estimated result < PQL and > MDL +- RPD is out of critena
Where applicable all sad sample analysis are reported on a dry weight basis unless flagged with a "W'
Note Calculations,are,performed beforeirounding to avoid round-off'errors in calculated results
Shealy Environmental Services, Inc QC'Data for'Lot Number KFO5057
168Vantage Point Drive West Columbia, SC 29172 (803);791-9700 Fax [phone] www shealylab com Level 11Report Q11
i

Inorganic, non-metals - MB
+ SampleJD' KQ12571-001 Matrix Aqueous,
j Batch 12571
Analytical Method 353 2
Parameter Result Q Dil PQL Units Analysis Date
Nitrate-Nitnte - N ND 1 0 020 mg/L 06/16/2009 1551
U
PQL - Practical quantitation limit P = The'RPD between two GC columns exceeds 40% N - Recovery is out of criteria
NO - Not detected at or above the,PQL J - Estimated result <PQL and > MDL +- RPD is out of criteria
Where applicable all sod sample analysis are reported on a dry weight basis unless flagged with a'W
Note Calculations are performed before rounding to avoid found -off, errors, In calculated results
Shealy Environmental Services, Inc QC Data for Lot Number KFO5057
106 Vantage Point Drive West Columbia SC 29172 [phone] Fax [phone] www shealylab com Level t Report v21

Inorganic non-metals - LCS
Sample ID K012571-002 Matrix Aqueous
Batch 12571
Analytical, Method 353 2
Spike
Amount Result % Rea
Parameter (mg/L) (mg/L) Q DII % Rec Limit Analysis Date
Nitrate -Nitrite - N 080 082 1 102 90-110 06/16/2009 1552
POL - Practical quantitation IimIV P = The RPD between two OC columns exceeds 40% N Recovery Is out of oriteda
NO - Not detected at or above the POL J = Estimated result < POL anC - MDL • - RPD is out of cnteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
Note Calculations are performed before rounding,to avol8,round-off errors,in(calculated results
Shealy Environmental Services Inc QC Data for Lot Number KF05057
106 Vantage Point Drive West,Columbia, SC 29172 [phone] Fax (803) 7,91.9111 www shealylab corn Levet 1 Report v21
t

Inorganic, non-metals - LCSD
Sample ID KQ12571-003 Matrix Aqueous
Batch 12571
Analytical Method 353 2 -
Spike
Amount Result % Ree % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Nitrate -Nitrite- N 080 082 1 103 073 90-110 20 06/,1612009 1554
PQL - Practical quantitation limit P = The RPD between two GC columns exceeds 40% N Recovery is out of criteria
SND - Not detected at or above the PQL J = Estimated result < PQL and > MDL + • RPD is out of cntena
Where applicable gall soil sample analysis are reported on a dry weight basis unless flagged with a'W'
Note Calculationswe performed before rounding to avoldiround-off errors,in calculated, results
Shealy Environmental Services Inc QC Data for Lot Number. 1 RFp05�0 Z7
I 1Level 06 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab com

Inorganic non-metals - MB,
Sample ID KQ12601-001 Matrix Aqueous
Batch 12601
Analytical Method 3000
Parameter_ Result Q DII PQL Units Analysis Date
Chloride ND 1 1 0 mg/L 06/17/2009 0850
PQV= Practical quantitation limit, P -The RPD between two GC columns exceeds 40% N Recoveryis out of criteria
ND - Not detected at or above the PQL J - Estimated result < PQU and alMDL + • RPD is out of criteria
Where applicable all soil sample analysis are reported on a dry weight basis unless flagged with a
Note, Calculations- are, performedibefore rounding,to avoid round -off errors In calculated`results
Shealy Environmental Services, Inc QC Data for Lot Number KF05057
106 Vantage Point Drive West Columbia SC 29172 [phone] Fax [phone] vuvviv shealylab corn Level 1 Report v21

Inorganic, non-metals - LCS
SaMPIGM K012601-002 Matriz Aqueous
Batch 12601
Analyttcal'Method 300 Q
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q DII % Rec Limit Analysis Date
Chloride 20 18 1 92 90-110 06/17/2009 0828
4
POL - Practical quantitation limit, P The RPD between two GC mtumns exceeds 409E N - Recovery is out of cnteria
ND - Not detected at or above the POL J s Estimated result < POE' and > MDL RPD is out of criteria
Where applicable all soil sample analysis aro reported on a dry weight basis unless flagged with a -W
Note Calculations are,performed before rounding to avoKround-off errors to calculated results
Shealy Environmental Services, Inc QC Data for Lot°Number KFO5057
166Mantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Level 1 Report v2 1

Inorganic, non-metals - LCSD
Sample ID K012601-003 Matrix Aqueous
Batch 12601
Analytical Method 300 0,
Spike
Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) Q DII % Rec % RPD Limit Limit Analysts Date
Chloride 20 18 1 91 15 90-110 20 06/17/20090935
POL - Praoecal quantitation limit P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
ND = Not detected at at above the POL J = Estimated result < POL and > MDL + - RPO is out of cnlens
Where applicable, all soil sample analysis are reported on a dry welght basis unless flagged with a W
Note Calculations are performed before rounding to avoid round -off errors In calculated results
Shealy Environmental Services;,lnc QC Data for Lot`Number KFO5057
106 Vantage IPoint rive West Columbia, SC 29172 [phone]' Fax [phone] Www shealylab com Level f ReporiQ t
P

I
Inorganic non-metals- MB
Sample ID KQ12643-001 Matrix: Aqueous,
Batch- 12643
Analytical Method 300 0
Parameter Result Q DII PQL Units Analysis,Date
Fluoride NU 1 010 mg/L 06/17/2009 0850
0
PQL - Practical quantitation limit P - The RPO between two GC columns exceeds 40% N Recovery is out of criteria
NO - Not detected at or above the PQL J -Estimated result c POL and >_ MDL « RPD is out of critena
Where applicable -all sal sample analysis are reported on a dry weight basis unless nagged with a "W'
Note, Calculations are performed,before rounding tolavoldiround-off'errors In calculated results
Shealy Environmental Services Inc CIC Datajor'Lot Number KF05057
106'Vantage Point Drive West Columbia, SC 29172 [phone] Fax[phone] www shealylab corn Level 1 ReportQ 1

Inorganicrnon-,metals LCS
Sample ID KQ12643-002 Matrix ,Aqueoust
Batch 12643*
r
AnalyticalrMethod 3000 --
Spike
Amount Result % Rec
Parameter _ (mg/L)—_ (mg%L) 'Q DII %Rec Limit __ AnalysistDate
Fluonde - 40 46 1 100 90-110 06/17/2009 0913,
I.
0
PQL - Practical Quantitation limit, P =,The RPD between two DC columns exceeds 409E N Recovery is out of entena
ND = Not detected at or above the PQL J - Estimated result < PQL and > MDL + - RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W'
Note Calculat(ons,are performed befor'e,roueding to,avoid'round-off errorslin caiculatedrresults
Shealy Environmental Services, Inc QC DatwforrLot Nufnber,IKF05057
106 Vantage Pomo Dnve West Columbia, SC 29172 (803)'791-97001 FaX,[phone] www shealylab corn Level ReportQ I

Inorganic non-metals - LCSD
Sample ID K012643-003 Matrix Aqueous
r
Batch, 12643
Analytical Method 3000
Spike
Amount Result % Roe % RPD
Parameter (mg/L) (mg/L) Q DO % Rec % RPD Limit Limit Analysis Date
Fluoride 40 39 1 97 26 90-110 20 06/17/2009 0935
POL - Practical quantitation limit P = The RPD between two GC columns exceeds 40% N - Recovery is out cl criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL - RPD Is out of criteria
Where applicable, all sal sample analysis are reported on a dry weight basis unless flagged with a
Note Calculations are, performed before rounding,to avoid round -off errors in calculated -results
Shealy Environmental Services, Inc QC`Data for Lot Number KF05057
106 Vantage Point Drive West Columbia, SC 29172, [phone] Fax (803);791-9111 www shealylab corn Level 1 Report 1

Inorganic non-metals - MB
Sample,ID K012644-001 Matrix Aqueous
Batch 12644
AnalyticallMethod 3000 -
Parameter Result Q DII PQL Units Analysis Date
Sulfate ND 1 1 0 mg/L 06/17/2009 0850
PQL - Practical quanbtabon limit P = The RPD between two OC columns exceeds 40% N • Recovery is out of criteria
ND = Not detected at or above the PQL J = Esllmated result < PQL and > MDL + • RPO is out of criteria
Where applicable, all soil,sample analysis are reported on a dry,weight basis'unless flagged with a'W'
Note Calculatlons,arelperformed before, rounding lto avoI&round-offerrors In calculated results,
Shealy Environmental Services, Inc QC Data for Lot Number. KF05057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] '1 www, shealylab com Level l Report Q l

Inorganic non-metals, - LCS
Sample ID .KQ12644-002 Matrix Aqueous
Batch 12644
Analytical Method 300 0
Spike,
Amount Result % Ree
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 19 1, 95 90-110 06/17/20090913
PQL - Practical quantitation limit P = The RPD between two GC'columns exceeds 40% N Recovery is out of cntena
ND = Not detected at or above the PQL J - Estimated result < PQL and > MDL - RPD is out of cntena
Where applicable all sod sample analysis are reported on a dry weight basis unless flagged with 0 W
Note. Calculations are performed before roundinglto avoid round -off errors in calculated results
Shealy EnvironmentaPServtces, Inc I QC' Data for Lot Number KFO5057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803),791-9111 www shealylab Com Level 1 Report Q 1

` Inorganic non-metals-- LCSD'
Samplell) KQ12644-003 Matrix Aqueous
Batch 12644
Analytical Method 300 0
Spike
Amount Result % Roe % RPD
Parameter (mg/L) (mg/L) Q Dill % Roo % RPD Limit Limit Analysis Date
Sulfate 20 18 1 92 40 90-110 20 06/17/2009 0935
PQL = Practical quantitation land P = The RPD between two DC columns exceeds 409E N - Recovery is out of cniena
ND = Not detected at or above the PoL J = Estimated result < PDL and > MDL + • RPD Is out of crdena
Where applicable all sod sample analysis are reported on a dry weight basis unless flagged with a'W'
Note. Calculationsrare performed before rounding to avoidtround-offierrors imcalculatedtresuIts,
Shealy Environmental Services,, nc QCtData for Lot Number KF05057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803)'791-9111 www shealylab com Level 1 Repor62 1

Inorganic non-metals - MB
Sample,ID KQ12098-001 Matrix Aqueous
Batch 12098
Analytical Method 1664A,
Parameter Result Q Dil PQL Units Analysis Date
HEM (oil and grease) ND 1 40 mg/L 06/09/2009 0000
` PGL = Practical quantitation gmlt P = The RPD between two GC columns exceeds 40% N • Recovery is out of criteria
r NO - Not detected at or above the PGL J = Estimated result c PGL and> MDL - RPD is out of,cntene
Where applicable, all sod sample analysis are reported on a dry weight basis untess (lagged with a W
Note Calculations are performed before rounding to avoid round -off errors In calculated'resuits
Shealy Environmentai,Services, Inc QC Data for Lot Number KFO5057
106 Vantage Point Dnve West Columbia, SC 29172 [phone] Fax [phone] www shealylab Com Level 1 Report v2 7

i
Inorganic non-metals - LCS
Sample ID- kQ12098-002% Matrix Aqueous
Batch 12098
Analytical Method 1664A
Spike
Amount Result `ys,Rec
Parameter (mg/L) (mg/L) Q DII _% Roo Limit Analysis Date
HEM`(oll and grease) 40 38 1 94 78-114 06/09/200910000
PQL - Practical quanblahon limit P = The RPD between two GC columns exceeds 40% tN • Recovery is out of rritena
ND = Not detected at or above the PQL J = Estimated result < PQL and> MDL + - RPD Is out of criteria,
Where applicable all soil sample analysts are reported on a dry weight basis unless flagged with a'W
Note Calculations are�performsd before rounding Wavoid'round-off errors In calculated, results
Shealy)Environmental,Services, Inc QC Data for Lot Number KFOS057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (803),791 9111 www shealylab com Level Ii Report v2 1

ICP -MS - MB
Sample ID KQ12292-001
Matrix. Aqueous
Batch 12292
Prep Method 200 2
Analytical Method% 200 8,
Prep Date 106/11/2009 2230
_
Parameter
Result
Q Dil
PQL
Units
Analyses Date
Aluminum
NO
1
50
ug/L
06/12/2009 2040
Arsenic
NO
1
510
ug/L
06/12/2009 2040
Barium
NO
1
50
ug/L
06/,1212009 2040
Beryllium
NO
1
10
ug/L
06/12/20092040
Boron
NO
1
50
ug/L
06/21/20091502
Cadmium
NO
1
010
ug/L
06/12/2009 2040
Chromium
NO
1
50
ug/L
06/12/2009 2040
Cobalt
NO
1
50
ug/L
06/12/2009 2040
Copper
ND
1
10
ug/L
06/1212009 2040
Iron
NO
1
20
ug/L
06/12/2009 2040
Magnesium
NO
1
50
ug/L
06/12/2009 2040
Manganese
NO
1
10
ug/L
06/12/2009 2040
Nickel
NO
1
10
ug/L
06/12/2009 2040
Selenium
ND
1
5 0
ug/L '
06/12/2009 2040
Silver
NO
1
5 0
ug/L
06/12/2009 2040
Tin
NO
1
5 0
ug/L
06/12/2009 2040
Titanium
NO
1
5 0
ug/L
06/12/2009 2040
Zinc
NO
1
10
ug/L
06/12/2009 2040
PDL = Practical quantitation Omlt P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria
ND = Not detected at or above the PDL J - Estimated result < PQL and a MDL + - RPD is out of criteria
Where applicable all sod sample analysis are reported on a dry weight basis unless flagged with a NJ'
Note, Calculations,are-performed before; roundinglto,avoid;round-off,errors in calculated ,resuIts
Shealy Environmental Services Inc QC Data for Lot Number KF05057
106 Vantage Point Drive West Columbia. SC 29172 (803),791-9700 Fax[phone] www shealylab corn Level I Report v2 I

ICP -MS,- LCS
Sample ID KQ12292„002
Matrix ,Aqueous
Batch 12292,
Prep Method. 200 2
Analytical Method 200 8
Prep Date 06/11/2009 2230
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q DII_ _ % Rec
Limit
Analysis Date
Aluminum
100
94
1 94
85-115
06/12/2009 2050
,Arsenic
100
96
1 96
85-115
06/12/2009 2050
Barium
100
98
1 98
85-115
06/12/2009 2050
Beryllium
100
100
I 104
85-115
06/12/2009 2050
Boron
100
110
1 108
85-115
06/21/20091513,
Cadmium
100
93
1 93
85-115
06/12/2009 2050
Chromium
100
97
1 97
�85-115
06/12/20092050
Cobalt
100
98
1 98
85-115
06/12/2009 2050
Copper
100
98
1 98
85-115
06/12/2009 2050
Iron
1000
980
1 98
85-115
06/,12/20092050
Magnesium
1000
990
1 99
85-115
06/12/2009 2050
Manganese
100
97
1 97
85-115
06/12/2009 2050
Nickel
100
99
1 99
85-115
06/12/2009 2050
Selenium
100
99
1 99
85-115
06/12/2009 2050
Sliver
100
100
1 101
85-115
06/,12/2009 2050
Tin
100
94
1 94
85-115
06/,1212009 2050,
Titanium
100
99
1 99
85-115
06/12/2009 2050
Zinc
100
100
1 102
85-115
06/12/2009 2050
POL - Practical quantitation limit P - The RPD between twd GC columns exceeds 40% N' Recovery Is out of criteria
ND - Not detected at or above the,PQL J - Estimated result < POL and a MDL • - RPD is out of criteria
Where applicable^all sod sample analysis are reported on a dry weight basis unless flagged with a -W'
Note Calculations are performed before rounding to,avold,round-oft errors in calculated results
Shealy Environmental Services, Inc OC Data for Lot Number' KF05057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Level i, Report v2 1

ICP -MS - LCSD
Sample,ID KQ12292-003
Matrix Aqueous
Batch 12292
Prep+Method
200 2,
Analytical Method 200 8
Prep+Date 001/20092230,
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug%L)
(ug/L) Q
DII
% Rec
% RPD
Limit
Limit
Analysis Date
Aluminum
100
93
1
93
1 7
85-1115
20
06/12/2009 2100
Arsenic
100
98
1
98
23
85-115
20
06/12/2009 2100
Barium
100
98
1
98
043
85-115
20
06/12/2009 2100
Beryllium
100
100
1
105
1 0
85-115
20
06/12/2009 2100
Boron
100
110
1
108
028
85-115
20
06/21/20091524
Cadmium
100
94'
1
94
082
85-115
20
06/12/2009,2100
Chromium
100
97
1
97
0'010
85-115
20
06/12/2009 2100
Cobalt
100
97
1
97
044
85-115
20
06/12/2009 2100
Copper
100
98
1
98
021
85-115
20
06/12/2009 2100
Iron
1000
980
1
98
11
85-115
20
06/12/20092100
Magnesium
1000
990
1
99
0'25
85-1,15
20
06/,12/20092100
Manganese
100
98
1
98
066
85-115
20
06/12/2009 2100
Nickel
100
99
1
99
0 010
85-115
20
06/12/2009 2100
Selenium
100
100
1
104
4 8
85-115
20
06/12/2009 2100
Silver
100
100
1
101
0 0
85-115
20
06/12/2009 2100
Tin
100
95
1
95
038
85-145
20
06/12/2009 2100
Titanium
100
98
1
98
1 3
85-115
20
06/12/2009 2100
Zinc
100
100
1
103
0 68
85-115
20
06/12/2009 2100
PQL - Practical Quanhtahon limit P = The RPD between two GC columns exceeds 40% N Recovery is out of criteria
NO - Not detected at or above the PQL J = Estlmatod result ic PQL and > MOL r - RPD Is out of criteria
Where applicable all soil sample analysis are reported on a dry,welghl basis unless flagged with e'W"
Note. Calculations arw,performed before rounding toiavoid,round-off•errors Imcaiculate&resuits
Shealy Environmental Services, Inc QC Data for Lot Number KF05057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Level t Report v2 1

'CVAA - MB
Sample ID. KQ12063-001 Matrix Aqueous
Batch 12063 Prep Method 7470A,
Analytical Method 245 1 Prep Date 06/09/2009 1630
Parameter Result Q DII PQL Units Analysis Date
Mercury ND 1 000010 mg/L- 06/09/2009 2239
PQL - Practical quantitation limit P = The RPD between two GC columns exceeds 40% N Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < POL and 2 MDL + - RPD Is out of criteria
Where applicable all soil sample analysis are reported on a dry weight basis unless flagged with a W
Note. Calculatlons,are performed before rounding to,avoid round -off errors,in calculated,results
Shealy Environmental Services, Inc QC Data for Lot Number KFO5057
106 Vantage�Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Level t Report v2 1

CVAA,- LCS
Sample ID' KQ12063-002 Matrix Aqueous
Batch 42063 Prep^Method 7470A,
Analytical Method 2451 Prep Date 06/09/2009 1630
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q DII % Rec Limit Analysis Date
Mercury 00020 00020 1 102 85-115 06/09/2009 2241
PQL - Practical quenbtabon limit P -.The RPD between two CC columns exceeds 4D% N Recovery is out of criteria
ND - Not detected at or above the PQL J -Estimated result < PQL and > MDL - RPD Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 1N'
Note Calculations are performed before rounding to avoid round-offferrors in calculated results
I -
Shealy Environmental Services, Inc QC Data'for Lot Number KFOS057
Level f Report t
106 Vantage Point Drive West Columbia SC 29172 [phone] Fax [phone] www shealylab cam
l
a
r

CVAA - LUD
Sample ID K012063-003 Matrix Aqueous _
Batch 12063 Prep Method 7470A
Analytical Method 245 1 - PFep Date 06/09/2009 1630
Spike
Amount Result % Roo % RPD
Parameter, (mg/L) (mg/L) Q DO % Rec %,RPD Limit Limit Analysis Date
Mercury 00020 00021 1 f04 1 4 85-115 20 06/09/2009 2243
a
I
PQL = Practical quantitation limit P -The RPD between two GC columns exceeds 40% N • Recovery Is out of criteria
ND - Not detected at or above the PQL J = Estimated result <IPOL and > MDL +- RPD is out of criteria
Where applicable all soft sample analysis are reported on a dry weight basis unless flagged with a'W'
Note Calculations are performed before roundingdo avoid round -off errors Inrcalculatediresults
Shealy Environmental Services Inc QC Data for Lot Number KFO5057
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab corn Level 1'Report Q 1

F
I
j' Inorganics Non-metals Quality Control Summary
Method Blank Sample'Evaluabon
Parameter
(mg
Acceptable
Analysis+Date
Flag,
Parameter
L)
(mg L)
Date
BOD
<0 20
2 0
06/06/09
Seed Control Factor Evaluation
Parameter
Result
Acceptable
Analysis
Flag
Parameter
m /L
1
Limit
Date
BOD
1 08
1 06-1 0
06/06/09
Glucose Glutamid Acid,Sampie Evaluation
Amount Recovered
Acceptable
Analysis
Flag
Parameter
m /L
1
Limit
Date
BOD
203
1 167 5-228 5
06/06/09
L
l
Sample ID
KF05057

Inorganics Non-metals Quality Control Summary
Method Blank Sample Evaluation
SampleAD
Parameter Result PQL (mg/L)
Analysis
Flag
(m g/L)
Date,
KFO5057
COD ND 10`
06/,16/09'
Laboratory Control Sample / Laboratory Control Sample Duplicate Evaluation
PRPWControllimit';
20
Amount
Amount
Amount
°
�0
Parameter
Spike
Recovered
% Recovery
Recovered
Recovery
Control
RPD
Analysis
Flag
(mg/L)
LCS
LCS
LCSD
LCSD
Limit
Date
(m/L
m !L
COD
400
40866
102
411 03
103
95-105
06
06/16/09
0
4 '

Inorganics Non-metals Quality Control' Summary
MethodiBlank(Sample Evaluation
Parameter
Result. PQL (CU) Analysis
Flag
(CU) Date
Color
ND 50 06/06/09
0
I
Sample ID
KF05057

i
Shealy Environmental Services, Inc
Document Number,,F-AD-016
1 Revision Number 6
i f Sample Receipt Checklist (SRC)
Client �OW ei� Cooler Inspected by/date / w/eO /(olSrlO Lot #
Pa;e)l of 1
Replaces Date 09/22/06,
Effective Date 05/''9/07
F0.5_6'5- %
Means of receipt
SESI
❑ Client ❑ UPS ❑ FedEx ❑ Airborne Exp ❑ Other
Yes
No
NA ❑
1 Were custody seals resent on the cooler?
Yes ❑
No ❑
NA
2 If custod seals were resent, were they intact and unbroken?
Cooler ID/temperature upon receipt °C / °C / °C / °C
/ °C /__ OC / °C / °C
Method- [94emperat a Blank ❑ Against Bottles
Method of coolant- E27 Wet Ice ❑ Blue Ice ❑ Dry Ice ❑ None
If res onse is No
or Yes for 14, 15, 1,6), an explanation/resolution. must be provided.
Yes ❑
No,❑
NA
3 If temperature of any cooler exceeded 6 0°C, was Project Manaaer notified?
PM notified by SRC, phone, note�(circle one), other, (For
coolers received via commercial courier, PMs are to be notified immediate)
Yes I
No ❑
NA
4 _ Is the commercial courier's packing slip attached to this fbnii?
Yes -1
No ❑
NA ❑
5 Were proper custody procedures (relinquished/received) followed?
Yes
No ❑
NA ❑
6 Were sample IDs listed?
Yes ET I
No' ❑
I NA ❑
1,7 Was collection date & time listed? .
Yes
No ❑
I NA ❑
18_ Were tests to be petformed listed on the COC or'was quote #provided?
Yes Q' I
No ❑
I NA ❑
9 Did all samples arrive in the proper containers for each test?
Yes
No ❑
NA ❑
10 Did all container label information (ID, date, tune) agree with COC?
Yes [a'
No ❑
NA ❑
I 1 ,Did,all containers arrive,in oo& condition (unbroken, lids on ,etc )?
Yes
No
NA ❑
12 Was adequate sample volume available? _
Yes ..
No ❑
NA ❑
13 Were all samples received witliui %2 the holding tune or 48 hours, whichever
comes first?
Yes ❑
No Rr
N'A ❑
14 Were any samples containers missino9
NA ❑
15 Were there any excess samples not listed on COC?
Yes ❑
No ❑
NAD-
16 Were bubbles present>"pea-size" ('/<"or 6mm in diameter) in any VOA
vials?
No ❑
NA ❑
17 Were all metals/O&G/HEM/nutnent samples received at a_pH of <2?
NA ❑
18 Were all c anide and/or sulfide sain les received ata H >12?
FY,s
No ❑
NA❑
19 Were all applicable NH3/TKN/cyanide/phenol/BNA/pest/PCB/herb
<0 2mQ ) and toxics <0 Img/L) sam les free of residual chlorine?
❑
No ❑
NA
20 Were collection teen eratures documented on the COC for NC sam" les?
Sample Preservation (Must be completed for any sample(s) incorrectly preserved or with headspace )
Sample(s) were received incorrectly preserved and were adjusted
accordingly`in Sample receiving with (H-,SO4,HNO3,HCI,NaOH) with the SR # (number)
Sample(s)
were ieceived with bubbles >6 mm in diameter
Sample(s) were received with TRC >0 2 mg/L for NH3/
TKN/c anide/BNA/ est/PCB/herb
Toxicity sainple(s)
analyzed',by method.330:5
were received with TRC >0' 1 mg/L and were
Corrective Action,taken, if.necessan,:
Was client -notified Yes ❑ No ❑ Did client -respond' Yes ❑ No ❑
SESI employee Date of response
Comments
k

Subcontracted Data
,�

N
LaboratoneS LLG
a mernber'of The GEL Group udc Po Box,3o712 Charleston SC 29417
2040 Savage Road Charleston, SC,29407
P'843 556 8171 F843766'1178
June 24, 2009
Ms Brooke Montgomery
Shealy Environmental
106 Vantage Point Drive
Cayce, SouthaCarolma,29033
Re Routine Analysis
Work Order 231387
Dear Ms Montgomery
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results,for the
sample(s) we received on June 10, 2009 This revised -data report'has been prepared and reviewed in accordance
with GEL's standard operating procedures
Our policy is to provide high quality, personalized analytical services to enable you to'meet your analytical
needs on time every time We trust that you'will find everything in order and'to your satisfaction If you have
any questions, please,do not hesitate to call,me,at (843) 556-817 1, ext 4422
Sincer ly,
At
Jak Crook
Project Manager
Chain of Custody 98759
Enclosures
Page 1, of, 10
problem solvedF
WWW gel com

GEL LABORATORIES LLC '
2040 Savage Road Charleston SC 29407 — [phone] — www gel corn
Certificate of Analysis Report
for
SESI001 Shealy Environmental Services, Inc
Client SDG 231387 GEL Work Order 231387
The Qualifiers in this report are defined asfollows:
* AYquality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the MDL„MDA, or LOD
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysts
The,designation ND, if present, appears in the result column when the,andlyte concentration is not detected above
the detection limit
Thisdata report has been prepared and reviewed in accordance with GEL Laboratones LLC
standard operating procedures Pleasp,direct any questions to your Project Manager, Jake Crook -
Reviewed by
Page 2 of 10

a
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 — [phone] — www gel corn
Certificate of Analysis
Company
Shealy Environmental
Address
106 Vantage Point Drive
Matrix
Cayce, South Carolina 29033
Contact
Ms Brooke Montgomery
Project
Routine Analysts
Client Sample ID
Allen SW008
Sample ID
231387001
Matrix
Water
Collect -Date
05—JUN-09 06 06
Receive Date
]0—JUN-09
Collector
Client
Report Date June 25,-2009
Project SES100203
Client ID SESI001
Parameter Qualifier Result
Uncertainty
DL
RL
Units
DF AnalystDate Time Batch Method
Rad Gas Flow Proportional, Counting
GF, PC, Gross AM, liquid "A's Received"
Alpha' 21 4
+/-378
400
56o
pCi/L
DXF3 06/19/09 0858 876459 1
Beta 428
+/-384
493
500
pCi/L
GFPC, Total Alpha Radium, liquid 'Ar Received"
Total Radium 386
+/-0877
0 728
too
pCi/L.
JXCS 06/17/09 1100 876478 2
Rad Radium -226
Lucas Cell, Ra226, liquid 'As Received"
Radium -226 102
+/-0349
0296
100
pCi/L
KSD1 06/17/09 1700 875610 3,
Thefollowing Analytical Methods were performed
_
Method Description
Analyst, Comments
1 ;EPA 900 0
2 EPA 900 1 Modified
3 EPA 903 l Modified
Surrogate/fracer'recovery Test
Result
Nominal
Recovery% Acceptable Limits,
Barium Carrier GFPC, Total Alpha Radium, Liquid "As
Received"
Page 3 of 10
r
630 (25%-125%)

jr
I
i
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www gel corn
Page 5 of 10
OC Summary
Report Date
June 24, 2009
Shealy Environmental
Page 1 of 3
106 Vantage Point Drive
Cayce, South Carolina
Contact
Ms. Brooke Montgomery
Workorder-
231387
Parmname,
NOM
Sample
Qual
_ QC Units
RPD%
_RK—CT.
Ranee Artist
Date Time
Rad Gas Flow
Batch 876459
QC1201860100
23107,7001 DUP
Alpha
556
559
pCi/L
0 484
(0%-,20%) DXF3
06/19/090857
+/-321
+/-349
Beta
191
189
pCi/L
1 17
(0% - 20%)
+/-409
+/-421
QC1201860103
LCS
Alpha
117
137
pCi/L
117
(75%-125%)
06/19/09 08 57
+1-5 13
Beta
391
371
pCi/L
949
(75%-125%)
+/-565
QC 1201860099
MB
Alpha
U
0 135
pCi/L
-'06119/09 09 41
+1-0538
Beta
U
-0173
pCi/L
+/-1 17
QC1201860101
231077001 MS
Alpha
234
556
319,
pCi/L
113
(75%-125%)
06/19/09 08 57
+/-321
+1-109
Beta
781
191
1000
pCl/L
104
(75%-125%)
+/-409
+/-13,0
QC1201860102
231077001 MSD
Alpha
234
556
315
pCi/L
1 48
111
(0%-20%)
06/19/09 08 57
+/-321
+/-106
Beta
781
191
1020
pCi/L
211
106
(0%-20%)
+/-409
+/-130
Batch 876478
QC1201860144
231387002 DUP
Total Radium
U
-031
U
0 322
pCi/L
000
N/A JXC5
06/17/09 1101
+/-0309
+/-0319
QC1201860146
LCS
Total Radium
271
248
lick
915
(75%-125%)
06/17/09 1101
+/-724
QC1201860143
MB
Total Radium
U
0 214
pCi/L
06/17/09 It 01
+/-0393
QC1201860345
231387002 MS
Total Radium
545 U
-031
431,
pCi/L
792
(75%-125%)
06/17/09 1 1 01
+/-0309
+/-127
Rad Ra -226
Batch 875610
QC1201858127
231387001 DUP
Radium -226
102
0 922
pCi/L
995
(095 - 100%) KSD1
06/17/09,17 00
+/-0349
+/-0324
Page 5 of 10

GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www gel corn
QC Summary
Workorder 231387
Page 2 of 3
Parmname
NOM Sample Qua[ 0C Units RPD%
RITC% Range Artist
Date Time
Rad Ra -226
Batch 875610
QC1201858129 LCS
Radium -226
242 18'2 pCt/L
75 1 (75%-125%) KSDI
06/17/09 17 35
+/-128
QC1201958126 MB
Radium -226
U 0 125 pCi/L
06/17/09 17 00
+/-0213
QC1201858128 231387001 MS
Radium -226
121 102 148 pCi/L
122 (75%-125%)
06/17/09 17 35
+/-0349 +/-978
Notes
The Qualifiers in this report are defined as follows
** Analytcns a surrogate compound
< Result is,less�than value reported
> Result is greater than.value reported
A The TlCfis a,suspected aldol -condensation product
B For General Chemistry and Organic analysis the target analyte was detected in the associated blank
BD Results are either below the MDC ontracenrecovery,isdow
C Analyte has been confirmed by GC/MS analysis
D Results are reported from a diluted aliquot of the sample
F Estimated Value
H Analytical holding time was exceeded
J Value is estimated
M Maf above MDC and less than LLD
M Matrix Related Failure
N/A RPD or tRecovery limits do not apply
ND Analyte concentration is not detected above,the detection limit
NJ Consult Case Narrative, Data Summary package, or Project -Manager concerning this,qualifier
R Sample results are rejected
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD
UI Gamma Spectroscopy --Uncertain identification
X Consult Case Narrative, Data Summary package, or Project+Manager concerning this qualifier
Y QC,Samples were not spiked with this compound
A RPD of sample'and duplicate evaluated using +/-RL Concentrations are <5X the,RL Qualifier Not Applicable for Radiochemistry
,h Prepardtion orlpreservation holding time was exceeded
Page 6 of 10

GEL LABORATORIES'LLC
2040 Savage Road Charleston, SC 29407- [phone] - www'gel com
QC Summary
Workorder• 231387 Page 3 of 3
Parmname NOM Sample Qual QC Units RPD% REC% Rang; Anlst Date Time
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cont by a factor of 4 or more
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance,cntena when the sample is greater than
five times,(5X) the contract required detection limit (RL) In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result
* Indicates that a Quality Control parameter was not within specifications
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations
Where the analytical method lias,bemperformed under NELAP certification, the analysts has merall of the
requtremenwof the NELAOstandard unless, qualified on the QC Summary
Page 7 of 10
i i �

J
ILaboratories LLC
SAMPLE RECEIPT & REVIEW FORM
Client: -�� i SDGIARCOC/Work Order:•
Received,By: Date'Beceived:, 6(0,11(3 Q
Suspected 1`Iazarddnformatlon�
o
*1F Counts,> x2'area,baekground on'samples not mark6V'radioactive", contact
the'Radiation Safety Group of f irtheiuivesngatton.
COGSamples marked as radioactive.
Maxuruun C_ o_unts Observed_*. tAO
Classified Radioactive 11 or III by RSO?
COC/Samples marked containing PCBs?
Shipped as a DOT hazardous?
Hazard Class Shipped: UN#-
Samples�identified asTorelgn'Sotl?,77
Sample Receipt Criteria
�� z
z
Comments/Qualitiers (Required for Non -Conforming Items)
Cycle Applicable
I
Shipping containers=received intact and
seals broken damaged container lealaog container other (describe)
sealed?
Preservation
2
Samples requtnng cold preservation
ice bags blue ice dry ice cone other (describe)
within 0:5 6 deg C9
Cham of custody documents included
3
with shipment?
Circle Applicable
4
Sample containers intact and sealed9
seats broken damaged contains laking contains other (desmbe)
SarrPle ID's, cont a dco affected and observed pH
5
Samples requiring,chemicaL
preservation at proper pH?
If Ptesw4tion added LO&
VOA vials free of headspace (defined as
Sample ID's and contain= affected.
6
< 6mm bubble)'
(byes immediately deliver to volatilesiabowtory)
7
Are Encore containers, present?
ws and tests affected
8
Samples received within holding time?
9
Sample ID's on COC match ID's on
` SWopg ,mQ�a d Q S s� �► o�
�l
bottles?
C
Date, & time on COC match date & tune
Sample ID's affected _
10
on bottles9
Number of containers received match
Sample ID's affected
11 'number
indicated on COM
COC form is properly signed in
12
relmquished(received sections?
Comments,
ct Ei CiroLn ek
�y 0 —( 4 (D 7 9
y 32 3 Z
A ir/ ea
PM (or PMA) review Initials ' " Date !
Page 9 of 10

List of current GEL Certifications as of 24 June 2009
State
Certification
Arizona _ _ a
AZ0668
Arkansas
88-0651
CLIA
42D0904046
California — NELAP
01 151CA
Colorado
GEL
Connecticut
PH -0169
Dept of Navy
NFESC 413
EPA Region 5
WG -15j -
Florida — NELAP
E87156
Georgia
E87156 (FL/NELAP)
Georgia DW
967
Hawaii
N/A
_ _ISO 17025
256701
Idaho
SCOOOI 2
Illinois — NELAP
200029
Indiana
C—SC-01
Kansas — NELAP_
E-10332
Kentucky
90129
Louisiana — NELAP
03046
Maryland
270
Massachusetts_
M—SCO12;
Nevada
SC00012
New Jersey — NELAP
SC002 _
New Mexico
FL NELAP E97156
New York — NELAP
11501
North Carolina
233
North Carolina DW
45709
Oklahoma
9904
Pennsylvania — NELAP
68-00485
South Carolina
10120001/10) 20002
Tennessee
TN 02934
Texas — NELAP
7104704235-07B—TX
U_S_ Dept`ofAgncul_ture
S-52597
Utah — NELAP
GEL
Vermont
VT87156
Virginia
00151
Washington
C1641
Page 1`0 of 10

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