WQ0015487_Wastewater Pond Closure Report_20190618

828.669.3929 • 828.669.5289
24 Lookout Terrace Road • PO Box 1023 • Black Mountain, NC 28711

MARTIN&SLAGLE
Robert L. Martin, LG Principal Geologist Christine E. Slagle Principal Scientist
GeoSciences, PA

June 18, 2019

Mr. Brett Laverty
Water Quality Regional Operations
Asheville Regional Office
NC Department of Environmental Quality
2090 US Highway 70
Swannanoa, NC 28778

Subject: Closed-Loop Recycle Permit (WQ0015487)
Powell Industries, Inc.
Suncrest Chip Mill
Haywood County
________________________________________________________________________

Dear Mr. Laverty,

Powell Industries, Inc. submitted a closure plan to NC Department of Environmental,
Division of Water Resources (DWR) on August 14, 2018. The plan was approved on
November 5, 2018. The plan described sampling of water and wastewater residuals to
be conducted as part of the wastewater pond closure. This report summarizes results of
initial stormwater samples collected at the wastewater pond outfalls prior to rerouting
of stormwater from the wastewater pond, a wastewater grab sample, and wastewater
residuals samples collected from the dewatered wastewater pond (WWP).

A temporary stormwater bypass trench was excavated to reroute stormwater from the
WWP to the Lower pond. The trench is excavated west of the WWP extending from a
concrete junction box located immediately southwest of the WWP, around the west
side of the WWP, and discharging into the Lower Pond. A partial breach was excavated
by Powell Industries in the dam of the Lower Pond to manage flooding associated with
heavy rains last year and reduce the potential of an uncontrolled breach of the Lower
Pond dam. The area adjacent to the bypass trench was planted with grass and covered
with erosion control matting to stabilize the banks on either side. The partial breach in
the Lower Pond dam was stabilized by placing hay bales at intervals in the discharge
channel within and below the dam.

When the WWP closure is complete, culvert pipe may be placed in the trench and
backfilled, or the trench will be maintained with the sidewalls being laid back to a 2:1
slope and stabilized with vegetation and erosion control matting. Figure 1 shows the
WWP and the Lower Pond as well as sample locations and temporary stormwater
conveyances.
June 18, 2019
Page 2
MSGS
SAMPLING AND ANALYSIS

Over the past six months, stormwater, impounded wastewater and wastewater
residuals have been sampled and analyzed to monitor stormwater discharges, and
determine how water and sediment will be managed during closure of the pond.

Stormwater was sampled October 11, 2018 and a second time in February 2019. The
October 11, 2019 sample was analyzed for 13 metals including arsenic, cadmium,
calcium, chromium, copper, lead, magnesium, mercury, molybdenum, nickel, selenium,
sodium, zinc; volatile organic compounds (VOCs); semi-volatile organic compounds
(SVOCs); turbidity; total suspended solids (TSS); BOD; pH; ammonia; total Kjeldahl
nitrogen (TKN); nitrogen, NN2/NO3; nitrate; nitrite; total phosphorus; and total
phenolics. The February 2019 sample was analyzed for COD and TSS as required in the
General Stormwater Discharge Permit for the site. The October 2018 stormwater
samples were collected at the site drainage outfall into the WWP. After results were
received and the stormwater bypass trench was excavated, the outfalls were
disconnected at a concrete junction box and the pipes into the WWP blocked to prevent
any additional stormwater from entering into the WWP and preventing backflow of
wastewater into the stormwater bypass trench. The February 2019 sample was
collected at the discharge from the lower pond.

The turbidity concentration detected at 19.9 NTU in stormwater sample SW-02
exceeded the NC 15A NCAC 02B surface water quality standards for classified Trout
waters (<10 NTU). Total suspended solids (TSS) detected in sample SW-02 at 99.2
exceeded the Stormwater General Permit benchmark value of 50 mg/L. No VOCs or
SVOCs were detected in either sample. Results are summarized in Table 1. Analytical
reports are attached.

A wastewater sample was collected from the WWP on February 14, 2019 and analyzed
for the same parameters as the stormwater samples described above. The results are
summarized in Table 2. Wastewater was pumped from the pond into tankers and
transported to the local POTW for disposal.

After the WWP was dewatered, two wastewater residual samples were composited
from eight locations (four per composite) in the WWP. Eight grab samples were
collected for analysis of VOCs. From each set of four grab samples, composite samples
were prepared for analysis of inorganic and SVOC parameters. Grab samples of each
aliquot were collected for analysis of VOC constituents before combining for the two
composite samples.

The composite samples were analyzed for SVOCs; 13 metals including arsenic, cadmium,
calcium, chromium, copper, lead, magnesium, mercury molybdenum, nickel, selenium,
sodium, zinc; ammonia nitrogen; total Kjeldahl nitrogen (TKN); nitrogen, NN2/NO3,
June 18, 2019
Page 3
MSGS
nitrate; nitrite; total phosphorus; and total phenolics. The eight grab samples of
residuals were analyzed for VOCs. Sample results were compared to the NCDEQ
Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs).

Acetone was the only VOC detected in the wastewater residual grab samples. The
concentrations range from 434 ug/Kg to 586 ug/Kg. The detected concentrations are
below the Protection of Groundwater Standard PSRG. Table 3 summarizes the
composite wastewater residual analytical results.

A total of 10 metals were detected in wastewater residual composite samples. All were
below the Protection of Groundwater PSRGs. Chromium was analyzed as total
chromium (unspeciated). The concentrations detected were 59.9 and 66.5 mg/Kg. A
TCLP analysis was conducted to ensure that the leachable concentration s were below
the TCLP standard for total chromium. The TCLP result for chromium was 0.77 mg/L for
sample C-1 and non-detect for C-2.

Since the analytical results for all regulated inorganic analytes are below leachable
thresholds and VOCs were not detected except for acetone, which was well below its
Protection of Groundwater PSRG, soils beneath the residual layer were not sampled.

WWP Closure

Based on the analytical results, Powell Industries, Inc. proposes to close the WWP
residuals in place. The stormwater that has accumulated in the pond since sampling
was completed will be pumped into tankers and transported to the local Publically
Owned Treatment Works (POTW) for disposal. The residuals remaining in the pond will
be covered with clean backfill. The surface of the backfill will be graded to shed
stormwater and planted with grass to control erosion.

Stormwater Management

Based on stormwater sample results, stormwater management measures will be
designed. The preferred option is to the abandon upstream WWP rather than retrofit it
as a stormwater detention pond. Instead, in the preferred plan, stormwater would be
allowed to flow through lower pond basin, after the downstream dam has been fully
breached. Treatment function can be enhanced in the lower pond area by constructing
a stable sinuous treatment wetland flow path.

Plans for treating stormwater are in process. Stormwater sampling is proposed at two
sites as show on Figure 2 and depicted in Photographs 1 and 2. Stormwater
constituents required for sampling and testing are summarized in the Closure Plan. The
two sample sites selected are as follows: Site 1: Outflow from downstream property
limit downstream of lower pond. Site 2: Outflow from piped system, prior to entering
June 18, 2019
Page 4
MSGS
the temporary diversion channel. Proposed stormwater sampling plan and protocols
will be sent to NCDEQ Stormwater Division for review and concurrence prior to
commencing sampling.

The current temporary bypass channel includes steep side slopes that are subject to
erosion as shown in Photographs 3 and 4. Options for stabilizing a permanent bypass
system include: a. Installing a pipe along the alignment of the existing temporary bypass
channel; b. regrading the channel with 2:1 (H:V) or gentler side slopes, revegetating the
channel, and installing erosion control matting as needed.

The dam for the downstream pond was recently partially breached shown in
Photograph 5. Full breaching of the dam will allow the pond to drain and no longer
impound stormwater. A plan for breaching the downstream dam of the lower pond will
be developed to minimize the risk of releasing sediment from the downstream pond
into Jonathan Creek. This plan will be submitted for approval by NCDEQ.

Once the full stormwater treatment system has been implemented, a maintenance plan
will be developed and followed for regular maintenance of the downstream treatment
wetland.

Powell Industries, Inc. requests approval to close the wastewater residuals in-place in
the WWP and cover with clean fill. The analytical results do not indicate constituent
concentrations above regulatory standards or leachable concentrations of any
constituents detected in residual samples. The closure plan is also modified by the
proposed stormwater management plan summarized in this report. Approval of the
stormwater management concept is requested.

Please feel free to contact me by phone [phone]) or email at
[e-mail] with any questions or comments you may have. I look
forward to hearing from you.

Sincerely,

Martin & Slagle GeoSciences, PA

Robert L. Martin, P.G., R.S.M.
Principal

Enclosures

Cc: Carl Powell
Tim Ormond, PE
FIGURE 1PREPARED FOR: Powell Industries, Inc.
DATE: 6-18-19
DR: RLM
CHK:
SITE MAP
WASTEWATER POND
CLOSURE
Powell Industries, Inc
Waynesville, NC
MARTIN&SLAGLE
GeoSciences, PA
PO Box 1023
Black Mountain, NC 28711
828.669.3929 828.669.5289
C-1A
C-1B C-1C C-1D
WW-1
C-2B
C-2C
C-2DC-2A
WS-2
SW-1
Partial Breach in Dam
Stormwater Bypass Trench
FIGURE 2PREPARED FOR: Powell Industries, Inc.
DATE: 6-18-19
DR: RLM
CHK:
STORMWATER SAMPLE
LOCATION MAP
WASTEWATER POND
CLOSURE
Powell Industries, Inc
Waynesville, NC
MARTIN&SLAGLE
GeoSciences, PA
PO Box 1023
Black Mountain, NC 28711
828.669.3929 828.669.5289
SW Sample 2
Upstream of Bypass Trench
SW Sample 1
Outlet from Property
TABLE 1
INDUSTRIAL WASTEWATER POND CLOSURE
STORMWATER SAMPLE ANALYSIS
POWELL INDUSTRIES, INC.
HAYWOOD COUNTY, NC
Regulatory Limits
Parameters
NC 15A NCAC 02B
SURFACE WATER
QUALITY STDS
SW-01
(10/11/18)
SW-02
(10/11/18)
Turbidity (NTU)<10 (Trout, Tr)3.1 19.8
Total Suspended Solids (mg/L)50 (Trout, Tr)*6.2 99.2
BOD (mg/L)5,000 ND 2.3
pH (Std. Units)6.0-9.0 6.3 6.4
Nitrogen, Ammonia (mg/L)NR ND ND
Nitrogen, TKN (mg/L)NR 0.037J ND
Nitrogen, NO2 plus NO3 (mg/L)NR 0.047 0.29
Nitrogen, Nitrate (mg/L)NR 0.047 0.29
Nitrogen, Nitrite (mg/L)NR ND 0.011J
Phosphorus, Total (mg/L)NR 0.13 0.084
Phenolics, Total (mg/L)300 0.012 0.0070J
COD(mg/L)120*20.2J 24.7J
Volatile Organic Compounds ND ND
Semi-volatile Organic Compounds ND ND
* NC Stormwater General Permit benchmark values.
Analytical Results
TABLE 2
INDUSTRIAL WASTEWATER POND CLOSURE
WASTEWATER SAMPLE ANALYSIS
POWELL INDUSTRIES, INC.
HAYWOOD COUNTY, NC
Analytical Results
Parameters WW-01
(2/14/19)
Calcium 28,500
Magnesium 2,690
Sodium 5,350
Zinc 12.1
Turbidity (NTU)16.9
Total Suspended Solids (mg/L)3.0
BOD (mg/L)ND
pH (Std. Units)7.1
Nitrogen, Ammonia (mg/L)0.39
Nitrogen, TKN (mg/L)0.81
Nitrogen, NO2 plus NO3 (mg/L)0.054
Nitrogen, Nitrate (mg/L)0.028
Nitrogen, Nitrite (mg/L)0.027
Phosphorus, Total (mg/L)0.063
Phenolics, Total (mg/L)ND
Volatile Organic Compounds ND
Semi-volatile Organic Compounds ND
TABLE 3
INDUSTRIAL WASTEWATER POND CLOSURE
WASTEWATER RESIDUALS SAMPLE ANALYSIS
POWELL INDUSTRIES, INC.
HAYWOOD COUNTY, NC
Regulatory Limits
Parameters PSRG-Protection of
GW (mg/Kg)C-1
4/12/19
C-1a
4/12/19
C-1b
4/12/19
C-1c
4/12/19
C-1d
4/12/19
C-2
4/12/19
C-2a
4/12/19
C-2b
4/12/19
C-2c
4/12/19
C-2d
4/12/19
Inorganics (mg/Kg)
Arsenic 5.8 3.7 NA NA NA NA 2.0 NA NA NA NA
Calcium NR 7,860 NA NA NA NA 3,490 NA NA NA NA
Chromium 350,000 (3.8 Total)59.9 NA NA NA NA 66.5 NA NA NA NA
Copper 700 96.4 NA NA NA NA 88.9 NA NA NA NA
Lead 270 15.8 NA NA NA NA 15.5 NA NA NA NA
Magnesium NR 12,100 NA NA NA NA 13,200 NA NA NA NA
Molybdenum 7.1 3.1 NA NA NA NA 3.0 NA NA NA NA
Nickel 120 32.1 NA NA NA NA 33.8 NA NA NA NA
Zinc 1200 264 NA NA NA NA 204 NA NA NA NA
Mercury 1.0 0.046 NA NA NA NA 0.040 NA NA NA NA
Nitrogen (TKN)NR 3,560 NA NA NA NA 3,400 NA NA NA NA
Phosphorus NR 692 NA NA NA NA 623 NA NA NA NA
TCLP (mg/L)
Arsenic 5.0 ND NA NA NA NA ND NA NA NA NA
Chromium 5.0 0.077 NA NA NA NA ND NA NA NA NA
Lead 5.0 0.029 NA NA NA NA ND NA NA NA NA
Volatile Organics (µg/Kg)
Acetone 25,000 NA 457 ND (374)383 586 NA 434 ND (1020)ND (8380)ND (414)
Analytical Results

Photograph 1. Proposed stormwater sampling location #1 at downstream limit of property.

Site 1. Outlet
from property

Photograph 2. Proposed stormwater sampling location #2 upstream of bypass channel.

Site 2.
Upstream of
bypass channel

Photograph 3. Temporary diversion channel with eroded side slopes (looking downstream).

Photograph 4. Temporary diversion channel with eroded side slopes (looking upstream).

Photograph 5. Lower pond with downstream berm partially breached.

Partial breach
of downstream
berm
#=CL#
October 22, 2018
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92403169
92403169
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
Powell Industries 10/11
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Revised Report. J-Flags and MDLs added to report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Lab ID Sample ID Matrix Date Collected Date Received
92403169001 SW-01 Water 10/11/18 03:30 10/11/18 15:25
92403169002 SW-02 Water 10/11/18 03:30 10/11/18 15:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92403169001 SW-01 EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CGAW
EPA 180.1 Rev 2.0 1993 1 PASI-AEWS
SM 2540D-2011 1 PASI-ACEH
SM 5210B-2011 1 PASI-ARLO
EPA 9040C 1 PASI-ASMK
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
EPA 365.1 Rev 2.0 1993 1 PASI-AGC
EPA 420.4 Rev 1.0 1993 1 PASI-ADMN
SM 5220D-2011 1 PASI-AMDW
92403169002 SW-02 EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CGAW
EPA 180.1 Rev 2.0 1993 1 PASI-AEWS
SM 2540D-2011 1 PASI-ACEH
SM 5210B-2011 1 PASI-ARLO
EPA 9040C 1 PASI-ASMK
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
EPA 365.1 Rev 2.0 1993 1 PASI-AGC
EPA 420.4 Rev 1.0 1993 1 PASI-ADMN
SM 5220D-2011 1 PASI-AMDW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-01 Lab ID:92403169001 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 MSSV
Acenaphthene ND ug/L 10/15/18 19:58 83-32-910/13/18 15:004.9 0.25 1
Acenaphthylene ND ug/L 10/15/18 19:58 208-96-810/13/18 15:004.9 0.21 1
Anthracene ND ug/L 10/15/18 19:58 120-12-710/13/18 15:004.9 0.14 1
Benzo(a)anthracene ND ug/L 10/15/18 19:58 56-55-310/13/18 15:004.9 0.32 1
Benzo(a)pyrene ND ug/L 10/15/18 19:58 50-32-810/13/18 15:004.9 0.29 1
Benzo(b)fluoranthene ND ug/L 10/15/18 19:58 205-99-210/13/18 15:004.9 0.27 1
Benzo(g,h,i)perylene ND ug/L 10/15/18 19:58 191-24-210/13/18 15:004.9 0.37 1
Benzo(k)fluoranthene ND ug/L 10/15/18 19:58 207-08-910/13/18 15:004.9 0.42 1
4-Bromophenylphenyl ether ND ug/L 10/15/18 19:58 101-55-310/13/18 15:004.9 0.80 1
Butylbenzylphthalate ND ug/L 10/15/18 19:58 85-68-710/13/18 15:004.9 0.77 1
4-Chloro-3-methylphenol ND ug/L 10/15/18 19:58 59-50-710/13/18 15:004.9 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 10/15/18 19:58 111-91-110/13/18 15:009.8 0.90 1
bis(2-Chloroethyl) ether ND ug/L 10/15/18 19:58 111-44-410/13/18 15:004.9 0.98 1
2-Chloronaphthalene ND ug/L 10/15/18 19:58 91-58-710/13/18 15:004.9 0.96 1
2-Chlorophenol ND ug/L 10/15/18 19:58 95-57-810/13/18 15:004.9 1.3 1
4-Chlorophenylphenyl ether ND ug/L 10/15/18 19:58 7005-72-310/13/18 15:004.9 0.85 1
Chrysene ND ug/L 10/15/18 19:58 218-01-910/13/18 15:004.9 0.21 1
Dibenz(a,h)anthracene ND ug/L 10/15/18 19:58 53-70-310/13/18 15:004.9 0.54 1
3,3'-Dichlorobenzidine ND ug/L 10/15/18 19:58 91-94-110/13/18 15:0024.5 2.1 1
2,4-Dichlorophenol ND ug/L 10/15/18 19:58 120-83-210/13/18 15:004.9 1.7 1
Diethylphthalate ND ug/L 10/15/18 19:58 84-66-210/13/18 15:004.9 0.57 1
2,4-Dimethylphenol ND ug/L 10/15/18 19:58 105-67-910/13/18 15:009.8 1.2 1
Dimethylphthalate ND ug/L 10/15/18 19:58 131-11-310/13/18 15:004.9 0.75 1
Di-n-butylphthalate ND ug/L 10/15/18 19:58 84-74-210/13/18 15:004.9 0.74 1
4,6-Dinitro-2-methylphenol ND ug/L 10/15/18 19:58 534-52-110/13/18 15:0019.6 2.5 1
2,4-Dinitrophenol ND ug/L 10/15/18 19:58 51-28-510/13/18 15:0049.0 8.8 1
2,4-Dinitrotoluene ND ug/L 10/15/18 19:58 121-14-210/13/18 15:004.9 0.88 1
2,6-Dinitrotoluene ND ug/L 10/15/18 19:58 606-20-210/13/18 15:004.9 0.96 1
Di-n-octylphthalate ND ug/L 10/15/18 19:58 117-84-010/13/18 15:004.9 0.65 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/15/18 19:58 117-81-710/13/18 15:004.9 0.77 1
Fluoranthene ND ug/L 10/15/18 19:58 206-44-010/13/18 15:004.9 0.21 1
Fluorene ND ug/L 10/15/18 19:58 86-73-710/13/18 15:004.9 0.21 1
Hexachloro-1,3-butadiene ND ug/L 10/15/18 19:58 87-68-310/13/18 15:004.9 0.92 1
Hexachlorobenzene ND ug/L 10/15/18 19:58 118-74-110/13/18 15:004.9 0.71 1
Hexachlorocyclopentadiene ND ug/L 10/15/18 19:58 77-47-410/13/18 15:009.8 0.86 1
Hexachloroethane ND ug/L 10/15/18 19:58 67-72-110/13/18 15:004.9 1.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/15/18 19:58 193-39-510/13/18 15:004.9 0.28 1
Isophorone ND ug/L 10/15/18 19:58 78-59-110/13/18 15:009.8 0.87 1
Naphthalene ND ug/L 10/15/18 19:58 91-20-310/13/18 15:004.9 0.33 1
Nitrobenzene ND ug/L 10/15/18 19:58 98-95-310/13/18 15:004.9 1.1 1
2-Nitrophenol ND ug/L 10/15/18 19:58 88-75-510/13/18 15:004.9 0.89 1
4-Nitrophenol ND ug/L 10/15/18 19:58 100-02-710/13/18 15:0049.0 4.0 1
N-Nitrosodimethylamine ND ug/L 10/15/18 19:58 62-75-910/13/18 15:004.9 0.89 1
N-Nitroso-di-n-propylamine ND ug/L 10/15/18 19:58 621-64-710/13/18 15:004.9 0.97 1
N-Nitrosodiphenylamine ND ug/L 10/15/18 19:58 86-30-610/13/18 15:009.8 0.98 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/15/18 19:58 108-60-110/13/18 15:004.9 0.93 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-01 Lab ID:92403169001 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 MSSV
Pentachlorophenol ND ug/L 10/15/18 19:58 87-86-510/13/18 15:009.8 4.5 1
Phenanthrene ND ug/L 10/15/18 19:58 85-01-810/13/18 15:004.9 0.22 1
Phenol ND ug/L 10/15/18 19:58 108-95-210/13/18 15:004.9 1.9 1
Pyrene ND ug/L 10/15/18 19:58 129-00-010/13/18 15:004.9 0.19 1
1,2,4-Trichlorobenzene ND ug/L 10/15/18 19:58 120-82-110/13/18 15:004.9 0.96 1
2,4,6-Trichlorophenol ND ug/L 10/15/18 19:58 88-06-210/13/18 15:009.8 1.3 1
Surrogates
Nitrobenzene-d5 (S)32 %10/15/18 19:58 4165-60-010/13/18 15:0010-120 1
2-Fluorobiphenyl (S)30 %10/15/18 19:58 321-60-810/13/18 15:0015-120 1
Terphenyl-d14 (S)45 %10/15/18 19:58 1718-51-010/13/18 15:0011-131 1
Phenol-d6 (S)13 %10/15/18 19:58 13127-88-310/13/18 15:0010-120 1
2-Fluorophenol (S)20 %10/15/18 19:58 367-12-410/13/18 15:0010-120 1
2,4,6-Tribromophenol (S)37 %10/15/18 19:58 118-79-610/13/18 15:0010-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/17/18 15:42 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/17/18 15:42 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/17/18 15:42 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/17/18 15:42 75-27-40.50 0.25 1
Bromoform ND ug/L 10/17/18 15:42 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/17/18 15:42 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/17/18 15:42 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/17/18 15:42 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/17/18 15:42 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/17/18 15:42 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/17/18 15:42 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/17/18 15:42 75-00-31.0 0.50 1
Chloroform ND ug/L 10/17/18 15:42 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/17/18 15:42 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/17/18 15:42 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/17/18 15:42 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/17/18 15:42 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/17/18 15:42 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/17/18 15:42 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/17/18 15:42 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 10/17/18 15:42 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/17/18 15:42 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/17/18 15:42 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/17/18 15:42 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/17/18 15:42 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/17/18 15:42 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/17/18 15:42 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/17/18 15:42 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/17/18 15:42 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/17/18 15:42 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/17/18 15:42 142-28-90.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-01 Lab ID:92403169001 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
2,2-Dichloropropane ND ug/L 10/17/18 15:42 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/17/18 15:42 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/17/18 15:42 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/17/18 15:42 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/17/18 15:42 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/17/18 15:42 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/17/18 15:42 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/17/18 15:42 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/17/18 15:42 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 10/17/18 15:42 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/17/18 15:42 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/17/18 15:42 103-65-10.50 0.25 1
Styrene ND ug/L 10/17/18 15:42 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/17/18 15:42 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/17/18 15:42 79-34-50.50 0.25 1
Tetrachloroethene ND ug/L 10/17/18 15:42 127-18-40.50 0.25 1
Toluene ND ug/L 10/17/18 15:42 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/17/18 15:42 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/17/18 15:42 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/17/18 15:42 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/17/18 15:42 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/17/18 15:42 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/17/18 15:42 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/17/18 15:42 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/17/18 15:42 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/17/18 15:42 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/17/18 15:42 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/17/18 15:42 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/17/18 15:42 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %10/17/18 15:42 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %10/17/18 15:42 460-00-470-130 1
Toluene-d8 (S)101 %10/17/18 15:42 2037-26-570-130 1
Analytical Method: EPA 180.1 Rev 2.0 1993180.1 Turbidity
Turbidity 3.1 NTU 10/12/18 15:081.0 0.50 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 6.2 mg/L 10/13/18 00:552.5 2.5 1
Analytical Method: SM 5210B-20115210B BOD, 5 day
BOD, 5 day ND mg/L 10/17/18 02:41 B210/12/18 06:382.0 2.0 1
Analytical Method: EPA 9040C9040 pH
pH at 25 Degrees C 6.3 Std. Units 10/15/18 14:56 H30.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-01 Lab ID:92403169001 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 350.1 Rev 2.0 1993350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/15/18 11:06 7664-41-70.10 0.050 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 0.37J mg/L 10/16/18 00:24 7727-37-910/14/18 14:410.50 0.25 1
Analytical Method: EPA 353.2 Rev 2.0 1993353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.047 mg/L 10/12/18 08:010.020 0.010 1
Nitrogen, Nitrate 0.047 mg/L 10/12/18 08:01 14797-55-80.020 0.010 1
Nitrogen, Nitrite ND mg/L 10/12/18 08:01 14797-65-00.020 0.010 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993365.1 Phosphorus, Total
Phosphorus 0.13 mg/L 10/12/18 23:08 7723-14-010/12/18 18:300.050 0.025 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993420.4 Phenolics, Total
Phenol 0.012 mg/L 10/18/18 18:29 108-95-2 BC,M110/17/18 18:310.010 0.0050 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-20115220D COD
Chemical Oxygen Demand 20.2J mg/L 10/12/18 21:0210/12/18 18:0325.0 12.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-02 Lab ID:92403169002 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 MSSV
Acenaphthene ND ug/L 10/15/18 20:29 83-32-910/13/18 15:004.8 0.24 1
Acenaphthylene ND ug/L 10/15/18 20:29 208-96-810/13/18 15:004.8 0.20 1
Anthracene ND ug/L 10/15/18 20:29 120-12-710/13/18 15:004.8 0.13 1
Benzo(a)anthracene ND ug/L 10/15/18 20:29 56-55-310/13/18 15:004.8 0.32 1
Benzo(a)pyrene ND ug/L 10/15/18 20:29 50-32-810/13/18 15:004.8 0.29 1
Benzo(b)fluoranthene ND ug/L 10/15/18 20:29 205-99-210/13/18 15:004.8 0.27 1
Benzo(g,h,i)perylene ND ug/L 10/15/18 20:29 191-24-210/13/18 15:004.8 0.37 1
Benzo(k)fluoranthene ND ug/L 10/15/18 20:29 207-08-910/13/18 15:004.8 0.41 1
4-Bromophenylphenyl ether ND ug/L 10/15/18 20:29 101-55-310/13/18 15:004.8 0.79 1
Butylbenzylphthalate ND ug/L 10/15/18 20:29 85-68-710/13/18 15:004.8 0.76 1
4-Chloro-3-methylphenol ND ug/L 10/15/18 20:29 59-50-710/13/18 15:004.8 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 10/15/18 20:29 111-91-110/13/18 15:009.6 0.88 1
bis(2-Chloroethyl) ether ND ug/L 10/15/18 20:29 111-44-410/13/18 15:004.8 0.96 1
2-Chloronaphthalene ND ug/L 10/15/18 20:29 91-58-710/13/18 15:004.8 0.94 1
2-Chlorophenol ND ug/L 10/15/18 20:29 95-57-810/13/18 15:004.8 1.2 1
4-Chlorophenylphenyl ether ND ug/L 10/15/18 20:29 7005-72-310/13/18 15:004.8 0.84 1
Chrysene ND ug/L 10/15/18 20:29 218-01-910/13/18 15:004.8 0.20 1
Dibenz(a,h)anthracene ND ug/L 10/15/18 20:29 53-70-310/13/18 15:004.8 0.53 1
3,3'-Dichlorobenzidine ND ug/L 10/15/18 20:29 91-94-110/13/18 15:0024.0 2.0 1
2,4-Dichlorophenol ND ug/L 10/15/18 20:29 120-83-210/13/18 15:004.8 1.6 1
Diethylphthalate ND ug/L 10/15/18 20:29 84-66-210/13/18 15:004.8 0.56 1
2,4-Dimethylphenol ND ug/L 10/15/18 20:29 105-67-910/13/18 15:009.6 1.2 1
Dimethylphthalate ND ug/L 10/15/18 20:29 131-11-310/13/18 15:004.8 0.73 1
Di-n-butylphthalate ND ug/L 10/15/18 20:29 84-74-210/13/18 15:004.8 0.72 1
4,6-Dinitro-2-methylphenol ND ug/L 10/15/18 20:29 534-52-110/13/18 15:0019.2 2.5 1
2,4-Dinitrophenol ND ug/L 10/15/18 20:29 51-28-510/13/18 15:0048.1 8.7 1
2,4-Dinitrotoluene ND ug/L 10/15/18 20:29 121-14-210/13/18 15:004.8 0.87 1
2,6-Dinitrotoluene ND ug/L 10/15/18 20:29 606-20-210/13/18 15:004.8 0.94 1
Di-n-octylphthalate ND ug/L 10/15/18 20:29 117-84-010/13/18 15:004.8 0.63 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/15/18 20:29 117-81-710/13/18 15:004.8 0.76 1
Fluoranthene ND ug/L 10/15/18 20:29 206-44-010/13/18 15:004.8 0.20 1
Fluorene ND ug/L 10/15/18 20:29 86-73-710/13/18 15:004.8 0.20 1
Hexachloro-1,3-butadiene ND ug/L 10/15/18 20:29 87-68-310/13/18 15:004.8 0.90 1
Hexachlorobenzene ND ug/L 10/15/18 20:29 118-74-110/13/18 15:004.8 0.69 1
Hexachlorocyclopentadiene ND ug/L 10/15/18 20:29 77-47-410/13/18 15:009.6 0.85 1
Hexachloroethane ND ug/L 10/15/18 20:29 67-72-110/13/18 15:004.8 1.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/15/18 20:29 193-39-510/13/18 15:004.8 0.28 1
Isophorone ND ug/L 10/15/18 20:29 78-59-110/13/18 15:009.6 0.86 1
Naphthalene ND ug/L 10/15/18 20:29 91-20-310/13/18 15:004.8 0.33 1
Nitrobenzene ND ug/L 10/15/18 20:29 98-95-310/13/18 15:004.8 1.1 1
2-Nitrophenol ND ug/L 10/15/18 20:29 88-75-510/13/18 15:004.8 0.88 1
4-Nitrophenol ND ug/L 10/15/18 20:29 100-02-710/13/18 15:0048.1 3.9 1
N-Nitrosodimethylamine ND ug/L 10/15/18 20:29 62-75-910/13/18 15:004.8 0.88 1
N-Nitroso-di-n-propylamine ND ug/L 10/15/18 20:29 621-64-710/13/18 15:004.8 0.95 1
N-Nitrosodiphenylamine ND ug/L 10/15/18 20:29 86-30-610/13/18 15:009.6 0.96 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/15/18 20:29 108-60-110/13/18 15:004.8 0.91 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-02 Lab ID:92403169002 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 MSSV
Pentachlorophenol ND ug/L 10/15/18 20:29 87-86-510/13/18 15:009.6 4.4 1
Phenanthrene ND ug/L 10/15/18 20:29 85-01-810/13/18 15:004.8 0.21 1
Phenol ND ug/L 10/15/18 20:29 108-95-210/13/18 15:004.8 1.8 1
Pyrene ND ug/L 10/15/18 20:29 129-00-010/13/18 15:004.8 0.18 1
1,2,4-Trichlorobenzene ND ug/L 10/15/18 20:29 120-82-110/13/18 15:004.8 0.94 1
2,4,6-Trichlorophenol ND ug/L 10/15/18 20:29 88-06-210/13/18 15:009.6 1.2 1
Surrogates
Nitrobenzene-d5 (S)43 %10/15/18 20:29 4165-60-010/13/18 15:0010-120 1
2-Fluorobiphenyl (S)41 %10/15/18 20:29 321-60-810/13/18 15:0015-120 1
Terphenyl-d14 (S)59 %10/15/18 20:29 1718-51-010/13/18 15:0011-131 1
Phenol-d6 (S)19 %10/15/18 20:29 13127-88-310/13/18 15:0010-120 1
2-Fluorophenol (S)29 %10/15/18 20:29 367-12-410/13/18 15:0010-120 1
2,4,6-Tribromophenol (S)46 %10/15/18 20:29 118-79-610/13/18 15:0010-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/17/18 15:58 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/17/18 15:58 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/17/18 15:58 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/17/18 15:58 75-27-40.50 0.25 1
Bromoform ND ug/L 10/17/18 15:58 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/17/18 15:58 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/17/18 15:58 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/17/18 15:58 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/17/18 15:58 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/17/18 15:58 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/17/18 15:58 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/17/18 15:58 75-00-31.0 0.50 1
Chloroform ND ug/L 10/17/18 15:58 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/17/18 15:58 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/17/18 15:58 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/17/18 15:58 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/17/18 15:58 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/17/18 15:58 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/17/18 15:58 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/17/18 15:58 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 10/17/18 15:58 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/17/18 15:58 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/17/18 15:58 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/17/18 15:58 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/17/18 15:58 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/17/18 15:58 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/17/18 15:58 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/17/18 15:58 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/17/18 15:58 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/17/18 15:58 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/17/18 15:58 142-28-90.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-02 Lab ID:92403169002 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
2,2-Dichloropropane ND ug/L 10/17/18 15:58 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/17/18 15:58 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/17/18 15:58 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/17/18 15:58 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/17/18 15:58 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/17/18 15:58 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/17/18 15:58 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/17/18 15:58 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/17/18 15:58 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 10/17/18 15:58 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/17/18 15:58 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/17/18 15:58 103-65-10.50 0.25 1
Styrene ND ug/L 10/17/18 15:58 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/17/18 15:58 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/17/18 15:58 79-34-50.50 0.25 1
Tetrachloroethene ND ug/L 10/17/18 15:58 127-18-40.50 0.25 1
Toluene ND ug/L 10/17/18 15:58 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/17/18 15:58 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/17/18 15:58 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/17/18 15:58 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/17/18 15:58 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/17/18 15:58 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/17/18 15:58 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/17/18 15:58 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/17/18 15:58 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/17/18 15:58 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/17/18 15:58 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/17/18 15:58 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/17/18 15:58 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %10/17/18 15:58 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %10/17/18 15:58 460-00-470-130 1
Toluene-d8 (S)100 %10/17/18 15:58 2037-26-570-130 1
Analytical Method: EPA 180.1 Rev 2.0 1993180.1 Turbidity
Turbidity 19.8 NTU 10/12/18 15:101.0 0.50 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 99.2 mg/L 10/13/18 00:5610.0 10.0 1
Analytical Method: SM 5210B-20115210B BOD, 5 day
BOD, 5 day 2.3 mg/L 10/17/18 02:43 B210/12/18 06:382.0 2.0 1
Analytical Method: EPA 9040C9040 pH
pH at 25 Degrees C 6.4 Std. Units 10/15/18 14:58 H30.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Sample:SW-02 Lab ID:92403169002 Collected:10/11/18 03:30 Received:10/11/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 350.1 Rev 2.0 1993350.1 Ammonia
Nitrogen, Ammonia ND mg/L 10/15/18 11:15 7664-41-70.10 0.050 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 10/16/18 00:28 7727-37-910/14/18 14:410.50 0.25 1
Analytical Method: EPA 353.2 Rev 2.0 1993353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.29 mg/L 10/12/18 08:020.020 0.010 1
Nitrogen, Nitrate 0.29 mg/L 10/12/18 08:02 14797-55-80.020 0.010 1
Nitrogen, Nitrite 0.011J mg/L 10/12/18 08:02 14797-65-00.020 0.010 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993365.1 Phosphorus, Total
Phosphorus 0.084 mg/L 10/12/18 23:08 7723-14-010/12/18 18:300.050 0.025 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993420.4 Phenolics, Total
Phenol 0.0070J mg/L 10/18/18 18:31 108-95-2 BC10/17/18 18:310.010 0.0050 1
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-20115220D COD
Chemical Oxygen Demand 24.7J mg/L 10/12/18 21:0210/12/18 18:0325.0 12.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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2225 Riverside Dr.
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[phone]
Page 12 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436679
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2402294
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/17/18 15:100.25
1,1,1-Trichloroethane ug/L ND 0.50 10/17/18 15:100.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/17/18 15:100.25
1,1,2-Trichloroethane ug/L ND 0.50 10/17/18 15:100.25
1,1-Dichloroethane ug/L ND 0.50 10/17/18 15:100.25
1,1-Dichloroethene ug/L ND 0.50 10/17/18 15:100.25
1,1-Dichloropropene ug/L ND 0.50 10/17/18 15:100.25
1,2,3-Trichlorobenzene ug/L ND 2.0 10/17/18 15:101.0
1,2,3-Trichloropropane ug/L ND 0.50 10/17/18 15:100.25
1,2,4-Trichlorobenzene ug/L ND 2.0 10/17/18 15:101.0
1,2,4-Trimethylbenzene ug/L ND 0.50 10/17/18 15:100.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/17/18 15:100.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/17/18 15:100.25
1,2-Dichlorobenzene ug/L ND 0.50 10/17/18 15:100.25
1,2-Dichloroethane ug/L ND 0.50 10/17/18 15:100.25
1,2-Dichloropropane ug/L ND 0.50 10/17/18 15:100.25
1,3,5-Trimethylbenzene ug/L ND 0.50 10/17/18 15:100.25
1,3-Dichlorobenzene ug/L ND 0.50 10/17/18 15:100.25
1,3-Dichloropropane ug/L ND 0.50 10/17/18 15:100.25
1,4-Dichlorobenzene ug/L ND 0.50 10/17/18 15:100.25
2,2-Dichloropropane ug/L ND 0.50 10/17/18 15:100.25
2-Chlorotoluene ug/L ND 0.50 10/17/18 15:100.25
4-Chlorotoluene ug/L ND 0.50 10/17/18 15:100.25
Benzene ug/L ND 0.50 10/17/18 15:100.25
Bromobenzene ug/L ND 0.50 10/17/18 15:100.25
Bromochloromethane ug/L ND 0.50 10/17/18 15:100.25
Bromodichloromethane ug/L ND 0.50 10/17/18 15:100.25
Bromoform ug/L ND 0.50 10/17/18 15:100.25
Bromomethane ug/L ND 5.0 10/17/18 15:102.5
Carbon tetrachloride ug/L ND 0.50 10/17/18 15:100.25
Chlorobenzene ug/L ND 0.50 10/17/18 15:100.25
Chloroethane ug/L ND 1.0 10/17/18 15:100.50
Chloroform ug/L ND 0.50 10/17/18 15:100.25
Chloromethane ug/L ND 1.0 10/17/18 15:100.50
cis-1,2-Dichloroethene ug/L ND 0.50 10/17/18 15:100.25
cis-1,3-Dichloropropene ug/L ND 0.50 10/17/18 15:100.25
Dibromochloromethane ug/L ND 0.50 10/17/18 15:100.25
Dibromomethane ug/L ND 0.50 10/17/18 15:100.25
Dichlorodifluoromethane ug/L ND 0.50 10/17/18 15:100.25
Diisopropyl ether ug/L ND 0.50 10/17/18 15:100.25
Ethylbenzene ug/L ND 0.50 10/17/18 15:100.25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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Page 13 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2402294
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 10/17/18 15:101.0
Isopropylbenzene (Cumene)ug/L ND 0.50 10/17/18 15:100.25
m&p-Xylene ug/L ND 1.0 10/17/18 15:100.50
Methyl-tert-butyl ether ug/L ND 0.50 10/17/18 15:100.25
Methylene Chloride ug/L ND 2.0 10/17/18 15:101.0
n-Butylbenzene ug/L ND 0.50 10/17/18 15:100.25
n-Propylbenzene ug/L ND 0.50 10/17/18 15:100.25
Naphthalene ug/L ND 2.0 10/17/18 15:101.0
o-Xylene ug/L ND 0.50 10/17/18 15:100.25
sec-Butylbenzene ug/L ND 0.50 10/17/18 15:100.25
Styrene ug/L ND 0.50 10/17/18 15:100.25
tert-Butylbenzene ug/L ND 0.50 10/17/18 15:100.25
Tetrachloroethene ug/L ND 0.50 10/17/18 15:100.25
Toluene ug/L ND 0.50 10/17/18 15:100.25
trans-1,2-Dichloroethene ug/L ND 0.50 10/17/18 15:100.25
trans-1,3-Dichloropropene ug/L ND 0.50 10/17/18 15:100.25
Trichloroethene ug/L ND 0.50 10/17/18 15:100.25
Trichlorofluoromethane ug/L ND 1.0 10/17/18 15:100.50
Vinyl chloride ug/L ND 1.0 10/17/18 15:100.50
1,2-Dichloroethane-d4 (S)%95 70-130 10/17/18 15:10
4-Bromofluorobenzene (S)%95 70-130 10/17/18 15:10
Toluene-d8 (S)%100 70-130 10/17/18 15:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2402295LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.050 98 60-140
1,1,1-Trichloroethane ug/L 44.850 90 60-140
1,1,2,2-Tetrachloroethane ug/L 47.550 95 60-140
1,1,2-Trichloroethane ug/L 48.350 97 60-140
1,1-Dichloroethane ug/L 43.650 87 60-140
1,1-Dichloroethene ug/L 45.850 92 60-140
1,1-Dichloropropene ug/L 47.350 95 60-140
1,2,3-Trichlorobenzene ug/L 49.650 99 60-140
1,2,3-Trichloropropane ug/L 51.550 103 60-140
1,2,4-Trichlorobenzene ug/L 50.950 102 60-140
1,2,4-Trimethylbenzene ug/L 47.150 94 60-140
1,2-Dibromo-3-chloropropane ug/L 48.350 97 60-140
1,2-Dibromoethane (EDB)ug/L 50.950 102 60-140
1,2-Dichlorobenzene ug/L 51.150 102 60-140
1,2-Dichloroethane ug/L 47.050 94 60-140
1,2-Dichloropropane ug/L 48.050 96 60-140
1,3,5-Trimethylbenzene ug/L 47.250 94 60-140
1,3-Dichlorobenzene ug/L 49.850 100 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2402295LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.750 103 60-140
1,4-Dichlorobenzene ug/L 49.750 99 60-140
2,2-Dichloropropane ug/L 46.850 94 60-140
2-Chlorotoluene ug/L 46.550 93 60-140
4-Chlorotoluene ug/L 47.550 95 60-140
Benzene ug/L 47.450 95 60-140
Bromobenzene ug/L 50.250 100 60-140
Bromochloromethane ug/L 53.950 108 60-140
Bromodichloromethane ug/L 46.550 93 60-140
Bromoform ug/L 49.650 99 60-140
Bromomethane ug/L 39.250 78 60-140
Carbon tetrachloride ug/L 48.450 97 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 38.950 78 60-140
Chloroform ug/L 50.850 102 60-140
Chloromethane ug/L 35.950 72 60-140
cis-1,2-Dichloroethene ug/L 45.450 91 60-140
cis-1,3-Dichloropropene ug/L 50.150 100 60-140
Dibromochloromethane ug/L 52.350 105 60-140
Dibromomethane ug/L 52.850 106 60-140
Dichlorodifluoromethane ug/L 41.950 84 60-140
Diisopropyl ether ug/L 43.750 87 60-140
Ethylbenzene ug/L 47.650 95 60-140
Hexachloro-1,3-butadiene ug/L 46.650 93 60-140
Isopropylbenzene (Cumene)ug/L 49.950 100 60-140
m&p-Xylene ug/L 95.2100 95 60-140
Methyl-tert-butyl ether ug/L 46.250 92 60-140
Methylene Chloride ug/L 45.650 91 60-140
n-Butylbenzene ug/L 48.750 97 60-140
n-Propylbenzene ug/L 47.350 95 60-140
Naphthalene ug/L 50.950 102 60-140
o-Xylene ug/L 49.650 99 60-140
sec-Butylbenzene ug/L 47.950 96 60-140
Styrene ug/L 48.950 98 60-140
tert-Butylbenzene ug/L 42.150 84 60-140
Tetrachloroethene ug/L 47.350 95 60-140
Toluene ug/L 44.850 90 60-140
trans-1,2-Dichloroethene ug/L 45.850 92 60-140
trans-1,3-Dichloropropene ug/L 47.150 94 60-140
Trichloroethene ug/L 50.050 100 60-140
Trichlorofluoromethane ug/L 44.350 89 60-140
Vinyl chloride ug/L 46.750 93 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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Asheville, NC 28804
[phone]
Page 15 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2402296MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403169001
2402297
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 101 60-14099 2 3020ND20.2 19.9
1,1,1-Trichloroethane ug/L 20 93 60-14092 1 3020ND18.5 18.5
1,1,2,2-Tetrachloroethane ug/L 20 98 60-14096 2 3020ND19.6 19.3
1,1,2-Trichloroethane ug/L 20 95 60-14095 1 3020ND19.0 18.9
1,1-Dichloroethane ug/L 20 91 60-14090 2 3020ND18.2 17.9
1,1-Dichloroethene ug/L 20 95 60-14097 2 3020ND18.9 19.4
1,1-Dichloropropene ug/L 20 97 60-14097 1 3020ND19.5 19.3
1,2,3-Trichlorobenzene ug/L 20 89 60-14093 5 3020ND17.8 18.7
1,2,3-Trichloropropane ug/L 20 101 60-140103 2 3020ND20.2 20.6
1,2,4-Trichlorobenzene ug/L 20 93 60-14097 4 3020ND18.6 19.5
1,2,4-Trimethylbenzene ug/L 20 92 60-14094 2 3020ND18.5 18.8
1,2-Dibromo-3-
chloropropane
ug/L 20 90 60-14093 3 3020ND18.0 18.6
1,2-Dibromoethane (EDB)ug/L 20 100 60-140103 3 3020ND19.9 20.6
1,2-Dichlorobenzene ug/L 20 97 60-140101 4 3020ND19.4 20.1
1,2-Dichloroethane ug/L 20 97 60-14093 4 3020ND19.3 18.5
1,2-Dichloropropane ug/L 20 98 60-14098 1 3020ND19.5 19.7
1,3,5-Trimethylbenzene ug/L 20 93 60-14095 2 3020ND18.5 18.9
1,3-Dichlorobenzene ug/L 20 96 60-14097 0 3020ND19.3 19.3
1,3-Dichloropropane ug/L 20 105 60-140105 0 3020ND21.0 21.0
1,4-Dichlorobenzene ug/L 20 96 60-14097 1 3020ND19.2 19.5
2,2-Dichloropropane ug/L 20 81 60-14081 0 3020ND16.3 16.3
2-Chlorotoluene ug/L 20 92 60-14093 2 3020ND18.3 18.7
4-Chlorotoluene ug/L 20 92 60-14095 4 3020ND18.3 19.0
Benzene ug/L 20 98 60-14096 2 3020ND19.5 19.1
Bromobenzene ug/L 20 100 60-140102 2 3020ND19.9 20.4
Bromochloromethane ug/L 20 109 60-140106 3 3020ND21.9 21.1
Bromodichloromethane ug/L 20 92 60-14093 1 3020ND18.4 18.7
Bromoform ug/L 20 94 60-14093 1 3020ND18.8 18.6
Bromomethane ug/L 20 71 60-14071 0 3020ND14.2 14.1
Carbon tetrachloride ug/L 20 102 60-140101 1 3020ND20.4 20.1
Chlorobenzene ug/L 20 103 60-14099 4 3020ND20.7 19.9
Chloroethane ug/L 20 89 60-14086 4 3020ND17.7 17.1
Chloroform ug/L 20 100 60-140100 0 3020ND20.0 19.9
Chloromethane ug/L 20 75 60-14075 0 3020ND15.1 15.1
cis-1,2-Dichloroethene ug/L 20 92 60-14093 1 3020ND18.4 18.6
cis-1,3-Dichloropropene ug/L 20 96 60-14095 1 3020ND19.3 19.0
Dibromochloromethane ug/L 20 99 60-140100 0 3020ND19.9 19.9
Dibromomethane ug/L 20 106 60-140108 1 3020ND21.3 21.5
Dichlorodifluoromethane ug/L 20 95 60-14093 2 3020ND19.0 18.5
Diisopropyl ether ug/L 20 88 60-14088 0 3020ND17.6 17.6
Ethylbenzene ug/L 20 98 60-14098 1 3020ND19.7 19.6
Hexachloro-1,3-butadiene ug/L 20 86 60-14090 4 3020ND17.2 17.9
Isopropylbenzene (Cumene)ug/L 20 103 60-140101 2 3020ND20.7 20.2
m&p-Xylene ug/L 40 99 60-14097 2 3040ND39.7 38.9
Methyl-tert-butyl ether ug/L 20 93 60-14092 1 3020ND18.6 18.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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Page 16 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2402296MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403169001
2402297
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 83 60-14082 1 3020ND16.6 16.4
n-Butylbenzene ug/L 20 92 60-14095 3 3020ND18.4 19.0
n-Propylbenzene ug/L 20 94 60-14095 1 3020ND18.8 19.1
Naphthalene ug/L 20 90 60-14094 4 3020ND18.0 18.8
o-Xylene ug/L 20 102 60-140101 1 3020ND20.4 20.2
sec-Butylbenzene ug/L 20 95 60-14098 3 3020ND19.0 19.5
Styrene ug/L 20 98 60-14097 0 3020ND19.5 19.5
tert-Butylbenzene ug/L 20 83 60-14084 1 3020ND16.6 16.8
Tetrachloroethene ug/L 20 97 60-14098 1 3020ND19.4 19.5
Toluene ug/L 20 95 60-14092 3 3020ND19.0 18.4
trans-1,2-Dichloroethene ug/L 20 97 60-14096 1 3020ND19.4 19.2
trans-1,3-Dichloropropene ug/L 20 89 60-14090 2 3020ND17.8 18.1
Trichloroethene ug/L 20 105 60-140101 4 3020ND21.0 20.2
Trichlorofluoromethane ug/L 20 100 60-14098 2 3020ND20.0 19.6
Vinyl chloride ug/L 20 97 60-14099 1 3020ND19.5 19.7
1,2-Dichloroethane-d4 (S)%95 70-13095
4-Bromofluorobenzene (S)%100 70-13096
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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Page 17 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435901
EPA 625.1
EPA 625.1
625 MSS
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2398861
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 10/15/18 15:430.98
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 10/15/18 15:430.95
2,4,6-Trichlorophenol ug/L ND 10.0 10/15/18 15:431.3
2,4-Dichlorophenol ug/L ND 5.0 10/15/18 15:431.7
2,4-Dimethylphenol ug/L ND 10.0 10/15/18 15:431.2
2,4-Dinitrophenol ug/L ND 50.0 10/15/18 15:439.0
2,4-Dinitrotoluene ug/L ND 5.0 10/15/18 15:430.90
2,6-Dinitrotoluene ug/L ND 5.0 10/15/18 15:430.98
2-Chloronaphthalene ug/L ND 5.0 10/15/18 15:430.98
2-Chlorophenol ug/L ND 5.0 10/15/18 15:431.3
2-Nitrophenol ug/L ND 5.0 10/15/18 15:430.91
3,3'-Dichlorobenzidine ug/L ND 25.0 10/15/18 15:432.1
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/15/18 15:432.6
4-Bromophenylphenyl ether ug/L ND 5.0 10/15/18 15:430.82
4-Chloro-3-methylphenol ug/L ND 5.0 10/15/18 15:433.7
4-Chlorophenylphenyl ether ug/L ND 5.0 10/15/18 15:430.87
4-Nitrophenol ug/L ND 50.0 10/15/18 15:434.1
Acenaphthene ug/L ND 5.0 10/15/18 15:430.25
Acenaphthylene ug/L ND 5.0 10/15/18 15:430.21
Anthracene ug/L ND 5.0 10/15/18 15:430.14
Benzo(a)anthracene ug/L ND 5.0 10/15/18 15:430.33
Benzo(a)pyrene ug/L ND 5.0 10/15/18 15:430.30
Benzo(b)fluoranthene ug/L ND 5.0 10/15/18 15:430.28
Benzo(g,h,i)perylene ug/L ND 5.0 10/15/18 15:430.38
Benzo(k)fluoranthene ug/L ND 5.0 10/15/18 15:430.43
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/15/18 15:430.92
bis(2-Chloroethyl) ether ug/L ND 5.0 10/15/18 15:431.0
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 10/15/18 15:430.79
Butylbenzylphthalate ug/L ND 5.0 10/15/18 15:430.79
Chrysene ug/L ND 5.0 10/15/18 15:430.21
Di-n-butylphthalate ug/L ND 5.0 10/15/18 15:430.75
Di-n-octylphthalate ug/L ND 5.0 10/15/18 15:430.66
Dibenz(a,h)anthracene ug/L ND 5.0 10/15/18 15:430.55
Diethylphthalate ug/L ND 5.0 10/15/18 15:430.58
Dimethylphthalate ug/L ND 5.0 10/15/18 15:430.76
Fluoranthene ug/L ND 5.0 10/15/18 15:430.21
Fluorene ug/L ND 5.0 10/15/18 15:430.21
Hexachloro-1,3-butadiene ug/L ND 5.0 10/15/18 15:430.94
Hexachlorobenzene ug/L ND 5.0 10/15/18 15:430.72
Hexachlorocyclopentadiene ug/L ND 10.0 10/15/18 15:430.88
Hexachloroethane ug/L ND 5.0 10/15/18 15:431.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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[phone]
Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2398861
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 10/15/18 15:430.29
Isophorone ug/L ND 10.0 10/15/18 15:430.89
N-Nitroso-di-n-propylamine ug/L ND 5.0 10/15/18 15:430.99
N-Nitrosodimethylamine ug/L ND 5.0 10/15/18 15:430.91
N-Nitrosodiphenylamine ug/L ND 10.0 10/15/18 15:431.0
Naphthalene ug/L ND 5.0 10/15/18 15:430.34
Nitrobenzene ug/L ND 5.0 10/15/18 15:431.1
Pentachlorophenol ug/L ND 10.0 10/15/18 15:434.6
Phenanthrene ug/L ND 5.0 10/15/18 15:430.22
Phenol ug/L ND 5.0 10/15/18 15:431.9
Pyrene ug/L ND 5.0 10/15/18 15:430.19
2,4,6-Tribromophenol (S)%81 10-137 10/15/18 15:43
2-Fluorobiphenyl (S)%81 15-120 10/15/18 15:43
2-Fluorophenol (S)%51 10-120 10/15/18 15:43
Nitrobenzene-d5 (S)%80 10-120 10/15/18 15:43
Phenol-d6 (S)%34 10-120 10/15/18 15:43
Terphenyl-d14 (S)%112 11-131 10/15/18 15:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2398862LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 39.050 78 44-142
2,2'-Oxybis(1-chloropropane)ug/L 46.850 94 36-166
2,4,6-Trichlorophenol ug/L 48.450 97 37-144
2,4-Dichlorophenol ug/L 47.450 95 39-135
2,4-Dimethylphenol ug/L 50.750 101 32-120
2,4-Dinitrophenol ug/L 259250 104 1-191
2,4-Dinitrotoluene ug/L 51.450 103 39-139
2,6-Dinitrotoluene ug/L 52.050 104 50-158
2-Chloronaphthalene ug/L 44.550 89 60-120
2-Chlorophenol ug/L 45.250 90 23-134
2-Nitrophenol ug/L 44.650 89 29-181
3,3'-Dichlorobenzidine ug/L 92.0100 92 1-262
4,6-Dinitro-2-methylphenol ug/L 112100 112 1-181
4-Bromophenylphenyl ether ug/L 51.250 102 53-127
4-Chloro-3-methylphenol ug/L 92.4100 92 22-147
4-Chlorophenylphenyl ether ug/L 47.850 96 25-158
4-Nitrophenol ug/L 113250 45 1-132
Acenaphthene ug/L 48.850 98 47-145
Acenaphthylene ug/L 48.750 97 33-145
Anthracene ug/L 52.450 105 27-133
Benzo(a)anthracene ug/L 51.050 102 33-143
Benzo(a)pyrene ug/L 54.650 109 17-163
Benzo(b)fluoranthene ug/L 52.450 105 24-159
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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2225 Riverside Dr.
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[phone]
Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2398862LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(g,h,i)perylene ug/L 56.050 112 1-219
Benzo(k)fluoranthene ug/L 56.250 112 11-162
bis(2-Chloroethoxy)methane ug/L 50.450 101 33-184
bis(2-Chloroethyl) ether ug/L 47.650 95 12-158
bis(2-Ethylhexyl)phthalate ug/L 46.850 94 8-158
Butylbenzylphthalate ug/L 47.050 94 1-152
Chrysene ug/L 51.550 103 17-168
Di-n-butylphthalate ug/L 46.750 93 1-120
Di-n-octylphthalate ug/L 47.450 95 4-146
Dibenz(a,h)anthracene ug/L 55.550 111 1-227
Diethylphthalate ug/L 44.850 90 1-120
Dimethylphthalate ug/L 44.950 90 1-120
Fluoranthene ug/L 50.050 100 26-137
Fluorene ug/L 49.050 98 59-121
Hexachloro-1,3-butadiene ug/L 36.450 73 24-120
Hexachlorobenzene ug/L 48.950 98 1-152
Hexachlorocyclopentadiene ug/L 41.050 82 25-150
Hexachloroethane ug/L 36.450 73 40-120
Indeno(1,2,3-cd)pyrene ug/L 56.650 113 1-171
Isophorone ug/L 41.050 82 21-196
N-Nitroso-di-n-propylamine ug/L 47.550 95 1-230
N-Nitrosodimethylamine ug/L 38.850 78 25-150
N-Nitrosodiphenylamine ug/L 51.050 102 25-150
Naphthalene ug/L 42.850 86 21-133
Nitrobenzene ug/L 45.550 91 35-180
Pentachlorophenol ug/L 98.6100 99 14-176
Phenanthrene ug/L 52.250 104 54-120
Phenol ug/L 21.150 42 5-120
Pyrene ug/L 53.050 106 52-120
2,4,6-Tribromophenol (S)%100 10-137
2-Fluorobiphenyl (S)%89 15-120
2-Fluorophenol (S)%59 10-120
Nitrobenzene-d5 (S)%92 10-120
Phenol-d6 (S)%40 10-120
Terphenyl-d14 (S)%116 11-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2398863MATRIX SPIKE SAMPLE:
MSSpike
Result
92402922002
1,2,4-Trichlorobenzene ug/L 40.349 82 44-142ND
2,2'-Oxybis(1-chloropropane)ug/L 43.549 89 36-166ND
2,4,6-Trichlorophenol ug/L 46.849 95 37-144ND
2,4-Dichlorophenol ug/L 44.549 91 39-135ND
2,4-Dimethylphenol ug/L 47.249 96 32-120ND
2,4-Dinitrophenol ug/L 228245 93 1-191ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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2225 Riverside Dr.
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[phone]
Page 20 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2398863MATRIX SPIKE SAMPLE:
MSSpike
Result
92402922002
2,4-Dinitrotoluene ug/L 48.449 99 39-139ND
2,6-Dinitrotoluene ug/L 49.649 101 50-158ND
2-Chloronaphthalene ug/L 44.549 91 60-120ND
2-Chlorophenol ug/L 43.149 88 23-134ND
2-Nitrophenol ug/L 45.149 92 29-182ND
3,3'-Dichlorobenzidine ug/L 99.498 101 1-262ND
4,6-Dinitro-2-methylphenol ug/L 10098 102 1-181ND
4-Bromophenylphenyl ether ug/L 45.849 93 53-127ND
4-Chloro-3-methylphenol ug/L 87.998 90 22-147ND
4-Chlorophenylphenyl ether ug/L 46.649 95 25-158ND
4-Nitrophenol ug/L 103245 42 1-132ND
Acenaphthene ug/L 45.049 92 47-145ND
Acenaphthylene ug/L 45.149 92 33-145ND
Anthracene ug/L 46.649 95 27-133ND
Benzo(a)anthracene ug/L 48.549 99 33-143ND
Benzo(a)pyrene ug/L 48.049 98 17-163ND
Benzo(b)fluoranthene ug/L 49.049 100 24-159ND
Benzo(g,h,i)perylene ug/L 48.949 100 1-219ND
Benzo(k)fluoranthene ug/L 47.149 96 11-162ND
bis(2-Chloroethoxy)methane ug/L 47.449 97 33-184ND
bis(2-Chloroethyl) ether ug/L 43.849 89 12-158ND
bis(2-Ethylhexyl)phthalate ug/L 46.049 94 8-158ND
Butylbenzylphthalate ug/L 45.049 92 1-152ND
Chrysene ug/L 46.949 96 17-168ND
Di-n-butylphthalate ug/L 42.149 86 1-120ND
Di-n-octylphthalate ug/L 51.749 106 4-146ND
Dibenz(a,h)anthracene ug/L 50.049 102 1-227ND
Diethylphthalate ug/L 41.249 84 1-120ND
Dimethylphthalate ug/L 41.649 85 1-120ND
Fluoranthene ug/L 46.349 94 26-137ND
Fluorene ug/L 46.949 96 59-121ND
Hexachloro-1,3-butadiene ug/L 38.549 78 24-120ND
Hexachlorobenzene ug/L 43.549 89 1-152ND
Hexachlorocyclopentadiene ug/L 41.449 84 25-150ND
Hexachloroethane ug/L 38.049 77 40-120ND
Indeno(1,2,3-cd)pyrene ug/L 49.249 100 1-171ND
Isophorone ug/L 39.449 80 21-196ND
N-Nitroso-di-n-propylamine ug/L 43.149 88 1-230ND
N-Nitrosodimethylamine ug/L 36.449 74 25-150ND
N-Nitrosodiphenylamine ug/L 43.349 88 25-150ND
Naphthalene ug/L 42.149 86 21-133ND
Nitrobenzene ug/L 42.349 86 35-180ND
Pentachlorophenol ug/L 59.598 61 14-176ND
Phenanthrene ug/L 46.349 94 54-120ND
Phenol ug/L 18.449 38 5-120ND
Pyrene ug/L 44.749 91 52-120ND
2,4,6-Tribromophenol (S)%93 10-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2398863MATRIX SPIKE SAMPLE:
MSSpike
Result
92402922002
2-Fluorobiphenyl (S)%91 15-120
2-Fluorophenol (S)%57 10-120
Nitrobenzene-d5 (S)%89 10-120
Phenol-d6 (S)%37 10-120
Terphenyl-d14 (S)%105 11-131
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403074001
2398864SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Fluoranthene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403074001
2398864SAMPLE DUPLICATE:
Fluorene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isophorone ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
Naphthalene ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Pyrene ug/L ND 30ND
2,4,6-Tribromophenol (S)%78 971
2-Fluorobiphenyl (S)%57 157
2-Fluorophenol (S)%33 634
Nitrobenzene-d5 (S)%61 260
Phenol-d6 (S)%25 024
Terphenyl-d14 (S)%71 35100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436005
EPA 180.1 Rev 2.0 1993
EPA 180.1 Rev 2.0 1993
180.1 Turbidity
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399365
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Turbidity NTU ND 1.0 10/12/18 15:060.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399366LABORATORY CONTROL SAMPLE:
LCSSpike
Turbidity NTU 10.110 101 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403169001
2399367SAMPLE DUPLICATE:
Turbidity NTU 3.1 3 103.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436094
SM 2540D-2011
SM 2540D-2011
2540D Total Suspended Solids
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399711
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Total Suspended Solids mg/L ND 2.5 10/13/18 00:512.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399712LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 242251 96 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403108002
2399713SAMPLE DUPLICATE:
Total Suspended Solids mg/L ND 5ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403275003
2399714SAMPLE DUPLICATE:
Total Suspended Solids mg/L 206 D6145179
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435867
SM 5210B-2011
SM 5210B-2011
5210B BOD, 5 day
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2398785
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
BOD, 5 day mg/L ND 2.0 10/17/18 00:572.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2398786LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day mg/L 189198 95 84.6-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403102001
2398788SAMPLE DUPLICATE:
BOD, 5 day mg/L 318 2 10312
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436234
EPA 9040C
EPA 9040C
9040 pH
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403158001
2400364SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 6.4 H3096.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92403134003
2400365SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 6.2 H3096.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436155
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Associated Lab Samples:92403169001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399897
Associated Lab Samples:92403169001
Matrix:Water
AnalyzedMDL
Nitrogen, Ammonia mg/L ND 0.10 10/15/18 10:200.050
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399898LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.15 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399899MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402667002
2399900
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 99 90-11098 0 1054.8 9.7 9.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399901MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402721003
2399902
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 108 90-110108 0 1051.2 6.6 6.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436156
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Associated Lab Samples:92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399903
Associated Lab Samples:92403169002
Matrix:Water
AnalyzedMDL
Nitrogen, Ammonia mg/L ND 0.10 10/15/18 11:120.050
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399904LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.35 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399905MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403169002
2399906
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 108 90-110108 0 105ND5.4 5.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399907MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402682001
2399908
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 107 90-110108 1 1050.30 5.7 5.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436147
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399871
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/16/18 00:220.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399872LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 9.710 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399873MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403169001
2399874
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 93 90-11098 5 10100.37J 9.7 10.2
REPORT OF LABORATORY ANALYSIS
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Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435870
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2398790
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate mg/L ND 0.020 10/12/18 07:540.010
Nitrogen, Nitrite mg/L ND 0.020 10/12/18 07:540.010
Nitrogen, NO2 plus NO3 mg/L ND 0.020 10/12/18 07:540.010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2398791LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.61.5 107 90-110
Nitrogen, Nitrite mg/L 1.01 104 90-110
Nitrogen, NO2 plus NO3 mg/L 2.72.5 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2398792MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403038001
2398793
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 122 90-110130 2 101.54.2 6.1 6.2
Nitrogen, Nitrite mg/L M1111490-110115 1 101ND1.2 1.2
Nitrogen, NO2 plus NO3 mg/L M12.5 119 90-110125 2 102.54.2 7.2 7.4
REPORT OF LABORATORY ANALYSIS
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Page 31 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436037
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399557
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Phosphorus mg/L ND 0.050 10/12/18 22:480.025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399558LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/L 2.72.5 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399559MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402990001
2399560
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus mg/L 2.5 107 90-110108 1 102.5ND 2.7 2.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399561MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402990011
2399562
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus mg/L 2.5 108 90-11099 9 102.50.10 2.8 2.6
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 32 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436643
EPA 420.4 Rev 1.0 1993
EPA 420.4 Rev 1.0 1993
420.4 Phenolics
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2402213
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Phenol mg/L 0.0052J 0.010 BC10/18/18 18:180.0050
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2402214LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol mg/L 0.049 BC.05 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2402215MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403074001
2402216
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol mg/L BC,M1.05 133 90-110130 2 10.050.0093J 0.076 0.074
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2402217MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403169001
2402218
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol mg/L BC,M1.05 143 90-110140 2 10.050.012 0.083 0.082
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436048
SM 5220D-2011
SM 5220D-2011
5220D COD
Associated Lab Samples:92403169001, 92403169002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399595
Associated Lab Samples:92403169001, 92403169002
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand mg/L ND 25.0 10/12/18 20:5712.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399596LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand mg/L 762750 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399597MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402959003
2399598
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L 100 103 90-110105 2 3100ND127130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399599MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403126003
2399600
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L M110011690-110114 1 310038.4 155 153
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92403169
Powell Industries 10/11
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.BC
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92403169
Powell Industries 10/11
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92403169001 435901 436134SW-01 EPA 625.1 EPA 625.1
92403169002 435901 436134SW-02 EPA 625.1 EPA 625.1
92403169001 436679SW-01 SM 6200B
92403169002 436679SW-02 SM 6200B
92403169001 436005SW-01 EPA 180.1 Rev 2.0 1993
92403169002 436005SW-02 EPA 180.1 Rev 2.0 1993
92403169001 436094SW-01 SM 2540D-2011
92403169002 436094SW-02 SM 2540D-2011
92403169001 435867 435887SW-01 SM 5210B-2011 SM 5210B-2011
92403169002 435867 435887SW-02 SM 5210B-2011 SM 5210B-2011
92403169001 436234SW-01 EPA 9040C
92403169002 436234SW-02 EPA 9040C
92403169001 436155SW-01 EPA 350.1 Rev 2.0 1993
92403169002 436156SW-02 EPA 350.1 Rev 2.0 1993
92403169001 436147 436329SW-01 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92403169002 436147 436329SW-02 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92403169001 435870SW-01 EPA 353.2 Rev 2.0 1993
92403169002 435870SW-02 EPA 353.2 Rev 2.0 1993
92403169001 436037 436079SW-01 EPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92403169002 436037 436079SW-02 EPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92403169001 436643 437038SW-01 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92403169002 436643 437038SW-02 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
92403169001 436048 436083SW-01 SM 5220D-2011 SM 5220D-2011
92403169002 436048 436083SW-02 SM 5220D-2011 SM 5220D-2011
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 04:00 PM
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Page 37 of 39
Page 38 of 39
Page 39 of 39
#=CL#
February 21, 2019
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92417986
92417986
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
Powell Industries
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92417986
Powell Industries
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92417986
Powell Industries
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92417986001 WW-01 EPA 200.7 Rev 4.4 1994 12 PASI-ADS
EPA 245.1 Rev 3.0 1994 1 PASI-ARDT
EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CGAW
EPA 180.1 Rev 2.0 1993 1 PASI-AGC
SM 2540D-2011 1 PASI-AMJP
SM 5210B-2011 1 PASI-AMFO
EPA 9040C 1 PASI-ASMK
EPA 350.1 Rev 2.0 1993 1 PASI-ANAL
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AGC
EPA 420.4 Rev 1.0 1993 1 PASI-ADMN
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417986
Powell Industries
Sample:WW-01 Lab ID:92417986001 Collected:02/14/19 14:50 Received:02/15/19 12:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Arsenic ND ug/L 02/17/19 20:49 7440-38-202/16/19 05:1510.0 1
Cadmium ND ug/L 02/17/19 20:49 7440-43-902/16/19 05:151.0 1
Calcium 28500 ug/L 02/17/19 20:49 7440-70-202/16/19 05:151001
Chromium ND ug/L 02/17/19 20:49 7440-47-302/16/19 05:155.0 1
Copper ND ug/L 02/17/19 20:49 7440-50-802/16/19 05:155.0 1
Lead ND ug/L 02/17/19 20:49 7439-92-102/16/19 05:155.0 1
Magnesium 2690 ug/L 02/17/19 20:49 7439-95-402/16/19 05:151001
Molybdenum ND ug/L 02/17/19 20:49 7439-98-702/16/19 05:155.0 1
Nickel ND ug/L 02/17/19 20:49 7440-02-002/16/19 05:155.0 1
Selenium ND ug/L 02/17/19 20:49 7782-49-202/16/19 05:1510.0 1
Sodium 5350 ug/L 02/17/19 20:49 7440-23-502/16/19 05:1550001
Zinc 12.1 ug/L 02/17/19 20:49 7440-66-602/16/19 05:1510.0 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 02/18/19 12:21 7439-97-602/17/19 19:290.20 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 MSSV
Acenaphthene ND ug/L 02/20/19 16:44 83-32-902/19/19 21:575.0 1
Acenaphthylene ND ug/L 02/20/19 16:44 208-96-802/19/19 21:575.0 1
Anthracene ND ug/L 02/20/19 16:44 120-12-702/19/19 21:575.0 1
Benzo(a)anthracene ND ug/L 02/20/19 16:44 56-55-302/19/19 21:575.0 1
Benzo(a)pyrene ND ug/L 02/20/19 16:44 50-32-802/19/19 21:575.0 1
Benzo(b)fluoranthene ND ug/L 02/20/19 16:44 205-99-202/19/19 21:575.0 1
Benzo(g,h,i)perylene ND ug/L 02/20/19 16:44 191-24-202/19/19 21:575.0 1
Benzo(k)fluoranthene ND ug/L 02/20/19 16:44 207-08-902/19/19 21:575.0 1
4-Bromophenylphenyl ether ND ug/L 02/20/19 16:44 101-55-302/19/19 21:575.0 1
Butylbenzylphthalate ND ug/L 02/20/19 16:44 85-68-702/19/19 21:575.0 1
4-Chloro-3-methylphenol ND ug/L 02/20/19 16:44 59-50-702/19/19 21:575.0 1
bis(2-Chloroethoxy)methane ND ug/L 02/20/19 16:44 111-91-102/19/19 21:5710.0 1
bis(2-Chloroethyl) ether ND ug/L 02/20/19 16:44 111-44-402/19/19 21:575.0 1
2-Chloronaphthalene ND ug/L 02/20/19 16:44 91-58-702/19/19 21:575.0 1
2-Chlorophenol ND ug/L 02/20/19 16:44 95-57-802/19/19 21:575.0 1
4-Chlorophenylphenyl ether ND ug/L 02/20/19 16:44 7005-72-302/19/19 21:575.0 1
Chrysene ND ug/L 02/20/19 16:44 218-01-902/19/19 21:575.0 1
Dibenz(a,h)anthracene ND ug/L 02/20/19 16:44 53-70-302/19/19 21:575.0 1
3,3'-Dichlorobenzidine ND ug/L 02/20/19 16:44 91-94-102/19/19 21:5725.0 1
2,4-Dichlorophenol ND ug/L 02/20/19 16:44 120-83-202/19/19 21:575.0 1
Diethylphthalate ND ug/L 02/20/19 16:44 84-66-202/19/19 21:575.0 1
2,4-Dimethylphenol ND ug/L 02/20/19 16:44 105-67-902/19/19 21:5710.0 1
Dimethylphthalate ND ug/L 02/20/19 16:44 131-11-302/19/19 21:575.0 1
Di-n-butylphthalate ND ug/L 02/20/19 16:44 84-74-202/19/19 21:575.0 1
4,6-Dinitro-2-methylphenol ND ug/L 02/20/19 16:44 534-52-102/19/19 21:5720.0 1
2,4-Dinitrophenol ND ug/L 02/20/19 16:44 51-28-502/19/19 21:5750.0 1
2,4-Dinitrotoluene ND ug/L 02/20/19 16:44 121-14-202/19/19 21:575.0 1
2,6-Dinitrotoluene ND ug/L 02/20/19 16:44 606-20-202/19/19 21:575.0 1
Di-n-octylphthalate ND ug/L 02/20/19 16:44 117-84-002/19/19 21:575.0 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417986
Powell Industries
Sample:WW-01 Lab ID:92417986001 Collected:02/14/19 14:50 Received:02/15/19 12:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 02/20/19 16:44 117-81-702/19/19 21:575.0 1
Fluoranthene ND ug/L 02/20/19 16:44 206-44-002/19/19 21:575.0 1
Fluorene ND ug/L 02/20/19 16:44 86-73-702/19/19 21:575.0 1
Hexachloro-1,3-butadiene ND ug/L 02/20/19 16:44 87-68-302/19/19 21:575.0 1
Hexachlorobenzene ND ug/L 02/20/19 16:44 118-74-102/19/19 21:575.0 1
Hexachlorocyclopentadiene ND ug/L 02/20/19 16:44 77-47-402/19/19 21:5710.0 1
Hexachloroethane ND ug/L 02/20/19 16:44 67-72-102/19/19 21:575.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/20/19 16:44 193-39-502/19/19 21:575.0 1
Isophorone ND ug/L 02/20/19 16:44 78-59-102/19/19 21:5710.0 1
Naphthalene ND ug/L 02/20/19 16:44 91-20-302/19/19 21:575.0 1
Nitrobenzene ND ug/L 02/20/19 16:44 98-95-302/19/19 21:575.0 1
2-Nitrophenol ND ug/L 02/20/19 16:44 88-75-502/19/19 21:575.0 1
4-Nitrophenol ND ug/L 02/20/19 16:44 100-02-702/19/19 21:5750.0 1
N-Nitrosodimethylamine ND ug/L 02/20/19 16:44 62-75-902/19/19 21:575.0 1
N-Nitroso-di-n-propylamine ND ug/L 02/20/19 16:44 621-64-702/19/19 21:575.0 1
N-Nitrosodiphenylamine ND ug/L 02/20/19 16:44 86-30-602/19/19 21:5710.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 02/20/19 16:44 108-60-102/19/19 21:575.0 1
Pentachlorophenol ND ug/L 02/20/19 16:44 87-86-502/19/19 21:5710.0 1
Phenanthrene ND ug/L 02/20/19 16:44 85-01-802/19/19 21:575.0 1
Phenol ND ug/L 02/20/19 16:44 108-95-202/19/19 21:575.0 1
Pyrene ND ug/L 02/20/19 16:44 129-00-002/19/19 21:575.0 1
1,2,4-Trichlorobenzene ND ug/L 02/20/19 16:44 120-82-102/19/19 21:575.0 1
2,4,6-Trichlorophenol ND ug/L 02/20/19 16:44 88-06-202/19/19 21:5710.0 1
Surrogates
Nitrobenzene-d5 (S)67 %02/20/19 16:44 4165-60-002/19/19 21:5710-120 1
2-Fluorobiphenyl (S)63 %02/20/19 16:44 321-60-802/19/19 21:5715-120 1
Terphenyl-d14 (S)69 %02/20/19 16:44 1718-51-002/19/19 21:5711-131 1
Phenol-d6 (S)25 %02/20/19 16:44 13127-88-302/19/19 21:5710-120 1
2-Fluorophenol (S)30 %02/20/19 16:44 367-12-402/19/19 21:5710-120 1
2,4,6-Tribromophenol (S)67 %02/20/19 16:44 118-79-602/19/19 21:5710-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/20/19 15:56 71-43-20.50 1
Bromobenzene ND ug/L 02/20/19 15:56 108-86-10.50 1
Bromochloromethane ND ug/L 02/20/19 15:56 74-97-50.50 1
Bromodichloromethane ND ug/L 02/20/19 15:56 75-27-40.50 1
Bromoform ND ug/L 02/20/19 15:56 75-25-20.50 1
Bromomethane ND ug/L 02/20/19 15:56 74-83-95.0 1
n-Butylbenzene ND ug/L 02/20/19 15:56 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/20/19 15:56 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/20/19 15:56 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/20/19 15:56 56-23-50.50 1
Chlorobenzene ND ug/L 02/20/19 15:56 108-90-70.50 1
Chloroethane ND ug/L 02/20/19 15:56 75-00-31.0 1
Chloroform ND ug/L 02/20/19 15:56 67-66-30.50 1
Chloromethane ND ug/L 02/20/19 15:56 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/20/19 15:56 95-49-80.50 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417986
Powell Industries
Sample:WW-01 Lab ID:92417986001 Collected:02/14/19 14:50 Received:02/15/19 12:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
4-Chlorotoluene ND ug/L 02/20/19 15:56 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/20/19 15:56 96-12-81.0 1
Dibromochloromethane ND ug/L 02/20/19 15:56 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/20/19 15:56 106-93-40.50 1
Dibromomethane ND ug/L 02/20/19 15:56 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/20/19 15:56 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/20/19 15:56 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/20/19 15:56 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/20/19 15:56 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/20/19 15:56 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/20/19 15:56 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/20/19 15:56 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/20/19 15:56 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/20/19 15:56 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/20/19 15:56 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/20/19 15:56 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/20/19 15:56 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/20/19 15:56 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/20/19 15:56 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/20/19 15:56 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/20/19 15:56 108-20-30.50 1
Ethylbenzene ND ug/L 02/20/19 15:56 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/20/19 15:56 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/20/19 15:56 98-82-80.50 1
Methylene Chloride ND ug/L 02/20/19 15:56 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/20/19 15:56 1634-04-40.50 1
Naphthalene ND ug/L 02/20/19 15:56 91-20-32.0 1
n-Propylbenzene ND ug/L 02/20/19 15:56 103-65-10.50 1
Styrene ND ug/L 02/20/19 15:56 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/20/19 15:56 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/20/19 15:56 79-34-50.50 1
Tetrachloroethene ND ug/L 02/20/19 15:56 127-18-40.50 1
Toluene ND ug/L 02/20/19 15:56 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/20/19 15:56 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/20/19 15:56 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/20/19 15:56 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/20/19 15:56 79-00-50.50 1
Trichloroethene ND ug/L 02/20/19 15:56 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/20/19 15:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/20/19 15:56 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/20/19 15:56 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/20/19 15:56 108-67-80.50 1
Vinyl chloride ND ug/L 02/20/19 15:56 75-01-41.0 1
m&p-Xylene ND ug/L 02/20/19 15:56 179601-23-11.0 1
o-Xylene ND ug/L 02/20/19 15:56 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %02/20/19 15:56 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417986
Powell Industries
Sample:WW-01 Lab ID:92417986001 Collected:02/14/19 14:50 Received:02/15/19 12:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Surrogates
4-Bromofluorobenzene (S)96 %02/20/19 15:56 460-00-470-130 1
Toluene-d8 (S)99 %02/20/19 15:56 2037-26-570-130 1
Analytical Method: EPA 180.1 Rev 2.0 1993180.1 Turbidity
Turbidity 16.9 NTU 02/16/19 01:081.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 3.0 mg/L 02/19/19 10:432.5 1
Analytical Method: SM 5210B-20115210B BOD, 5 day
BOD, 5 day ND mg/L 02/21/19 04:25 B202/16/19 03:522.0 1
Analytical Method: EPA 9040C9040 pH
pH at 25 Degrees C 7.1 Std. Units 02/19/19 10:36 H30.10 1
Analytical Method: EPA 350.1 Rev 2.0 1993350.1 Ammonia
Nitrogen, Ammonia 0.39 mg/L 02/20/19 10:36 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 0.81 mg/L 02/19/19 00:17 7727-37-902/18/19 11:270.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.054 mg/L 02/16/19 03:350.020 1
Nitrogen, Nitrate 0.028 mg/L 02/16/19 03:35 14797-55-80.020 1
Nitrogen, Nitrite 0.027 mg/L 02/16/19 03:35 14797-65-00.020 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993365.1 Phosphorus, Total
Phosphorus 0.063 mg/L 02/18/19 21:18 7723-14-002/18/19 18:120.050 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993420.4 Phenolics, Total
Phenol ND mg/L 02/19/19 14:41 108-95-202/18/19 14:400.020 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458622
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
245.1 Mercury
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2500146
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 02/18/19 11:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500147LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.22.5 90 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500148MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417598001
2500149
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 75 70-13077 22.5ND 1.9 1.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500150MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417509005
2500151
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L M12.5 71 70-13066 72.5ND 1.8 1.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458552
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2499923
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 02/18/19 17:42
Cadmium ug/L ND 1.0 02/18/19 17:42
Calcium ug/L ND 100 02/18/19 17:42
Chromium ug/L ND 5.0 02/18/19 17:42
Copper ug/L ND 5.0 02/18/19 17:42
Lead ug/L ND 5.0 02/18/19 17:42
Magnesium ug/L ND 100 02/18/19 17:42
Molybdenum ug/L ND 5.0 02/18/19 17:42
Nickel ug/L ND 5.0 02/18/19 17:42
Selenium ug/L ND 10.0 02/18/19 17:42
Sodium ug/L ND 5000 02/18/19 17:42
Zinc ug/L ND 10.0 02/18/19 17:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2499924LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 512500 102 85-115
Cadmium ug/L 503500 101 85-115
Calcium ug/L 51005000 102 85-115
Chromium ug/L 522500 104 85-115
Copper ug/L 527500 105 85-115
Lead ug/L 510500 102 85-115
Magnesium ug/L 49805000 100 85-115
Molybdenum ug/L 526500 105 85-115
Nickel ug/L 507500 101 85-115
Selenium ug/L 505500 101 85-115
Sodium ug/L 4900J5000 98 85-115
Zinc ug/L 513500 103 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2499925MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92418025001
2499926
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 104 70-130103 1500520517
Cadmium ug/L 500 103 70-130102 15000.059
mg/L
574 569
Calcium ug/L 5000 111 70-130106 150001860018400
Chromium ug/L 500 104 70-130105 1500525528
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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Asheville, NC 28804
[phone]
Page 9 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2499925MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92418025001
2499926
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Copper ug/L 500 105 70-130105 0500531530
Lead ug/L 500 100 70-13099 05000.066
mg/L
565 563
Magnesium ug/L 5000 103 70-130103 0500079707980
Molybdenum ug/L 500 96 70-13096 0500481481
Nickel ug/L 500 101 70-130101 0500508509
Selenium ug/L 500 106 70-130107 0500532534
Sodium ug/L 5000 118 70-130106 250003070030100
Zinc ug/L 500 119 70-13097 25004.8
mg/L
5400 5290
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2499927MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417780005
2499928
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 102 70-130101 2500ND513504
Cadmium ug/L 500 102 70-130101 1500ND511506
Calcium ug/L 5000 105 70-130103 250000.98
mg/L
6240 6110
Chromium ug/L 500 106 70-130105 1500ND531523
Copper ug/L 500 105 70-130103 15000.014
mg/L
536 530
Lead ug/L 500 102 70-130100 2500ND512502
Magnesium ug/L 5000 103 70-130101 250000.27
mg/L
5420 5320
Molybdenum ug/L 500 96 70-13095 1500ND478475
Nickel ug/L 500 102 70-130100 1500ND510503
Selenium ug/L 500 105 70-130105 1500ND528524
Sodium ug/L 5000 100 70-13098 25000ND64206320
Zinc ug/L 500 104 70-130102 15000.093
mg/L
613 604
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
459154
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2502351
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/20/19 10:49
1,1,1-Trichloroethane ug/L ND 0.50 02/20/19 10:49
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/20/19 10:49
1,1,2-Trichloroethane ug/L ND 0.50 02/20/19 10:49
1,1-Dichloroethane ug/L ND 0.50 02/20/19 10:49
1,1-Dichloroethene ug/L ND 0.50 02/20/19 10:49
1,1-Dichloropropene ug/L ND 0.50 02/20/19 10:49
1,2,3-Trichlorobenzene ug/L ND 2.0 02/20/19 10:49
1,2,3-Trichloropropane ug/L ND 0.50 02/20/19 10:49
1,2,4-Trichlorobenzene ug/L ND 2.0 02/20/19 10:49
1,2,4-Trimethylbenzene ug/L ND 0.50 02/20/19 10:49
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/20/19 10:49
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/20/19 10:49
1,2-Dichlorobenzene ug/L ND 0.50 02/20/19 10:49
1,2-Dichloroethane ug/L ND 0.50 02/20/19 10:49
1,2-Dichloropropane ug/L ND 0.50 02/20/19 10:49
1,3,5-Trimethylbenzene ug/L ND 0.50 02/20/19 10:49
1,3-Dichlorobenzene ug/L ND 0.50 02/20/19 10:49
1,3-Dichloropropane ug/L ND 0.50 02/20/19 10:49
1,4-Dichlorobenzene ug/L ND 0.50 02/20/19 10:49
2,2-Dichloropropane ug/L ND 0.50 02/20/19 10:49
2-Chlorotoluene ug/L ND 0.50 02/20/19 10:49
4-Chlorotoluene ug/L ND 0.50 02/20/19 10:49
Benzene ug/L ND 0.50 02/20/19 10:49
Bromobenzene ug/L ND 0.50 02/20/19 10:49
Bromochloromethane ug/L ND 0.50 02/20/19 10:49
Bromodichloromethane ug/L ND 0.50 02/20/19 10:49
Bromoform ug/L ND 0.50 02/20/19 10:49
Bromomethane ug/L ND 5.0 02/20/19 10:49
Carbon tetrachloride ug/L ND 0.50 02/20/19 10:49
Chlorobenzene ug/L ND 0.50 02/20/19 10:49
Chloroethane ug/L ND 1.0 02/20/19 10:49
Chloroform ug/L ND 0.50 02/20/19 10:49
Chloromethane ug/L ND 1.0 02/20/19 10:49
cis-1,2-Dichloroethene ug/L ND 0.50 02/20/19 10:49
cis-1,3-Dichloropropene ug/L ND 0.50 02/20/19 10:49
Dibromochloromethane ug/L ND 0.50 02/20/19 10:49
Dibromomethane ug/L ND 0.50 02/20/19 10:49
Dichlorodifluoromethane ug/L ND 0.50 02/20/19 10:49
Diisopropyl ether ug/L ND 0.50 02/20/19 10:49
Ethylbenzene ug/L ND 0.50 02/20/19 10:49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2502351
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 02/20/19 10:49
Isopropylbenzene (Cumene)ug/L ND 0.50 02/20/19 10:49
m&p-Xylene ug/L ND 1.0 02/20/19 10:49
Methyl-tert-butyl ether ug/L ND 0.50 02/20/19 10:49
Methylene Chloride ug/L ND 2.0 02/20/19 10:49
n-Butylbenzene ug/L ND 0.50 02/20/19 10:49
n-Propylbenzene ug/L ND 0.50 02/20/19 10:49
Naphthalene ug/L ND 2.0 02/20/19 10:49
o-Xylene ug/L ND 0.50 02/20/19 10:49
sec-Butylbenzene ug/L ND 0.50 02/20/19 10:49
Styrene ug/L ND 0.50 02/20/19 10:49
tert-Butylbenzene ug/L ND 0.50 02/20/19 10:49
Tetrachloroethene ug/L ND 0.50 02/20/19 10:49
Toluene ug/L ND 0.50 02/20/19 10:49
trans-1,2-Dichloroethene ug/L ND 0.50 02/20/19 10:49
trans-1,3-Dichloropropene ug/L ND 0.50 02/20/19 10:49
Trichloroethene ug/L ND 0.50 02/20/19 10:49
Trichlorofluoromethane ug/L ND 1.0 02/20/19 10:49
Vinyl chloride ug/L ND 1.0 02/20/19 10:49
1,2-Dichloroethane-d4 (S)%93 70-130 02/20/19 10:49
4-Bromofluorobenzene (S)%97 70-130 02/20/19 10:49
Toluene-d8 (S)%98 70-130 02/20/19 10:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2502352LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 60-140
1,1,1-Trichloroethane ug/L 46.750 93 60-140
1,1,2,2-Tetrachloroethane ug/L 47.350 95 60-140
1,1,2-Trichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethane ug/L 43.850 88 60-140
1,1-Dichloroethene ug/L 44.650 89 60-140
1,1-Dichloropropene ug/L 46.150 92 60-140
1,2,3-Trichlorobenzene ug/L 53.450 107 60-140
1,2,3-Trichloropropane ug/L 46.550 93 60-140
1,2,4-Trichlorobenzene ug/L 53.450 107 60-140
1,2,4-Trimethylbenzene ug/L 47.850 96 60-140
1,2-Dibromo-3-chloropropane ug/L 51.850 104 60-140
1,2-Dibromoethane (EDB)ug/L 50.850 102 60-140
1,2-Dichlorobenzene ug/L 50.250 100 60-140
1,2-Dichloroethane ug/L 41.150 82 60-140
1,2-Dichloropropane ug/L 47.050 94 60-140
1,3,5-Trimethylbenzene ug/L 47.650 95 60-140
1,3-Dichlorobenzene ug/L 49.950 100 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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[phone]
Page 12 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2502352LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.850 98 60-140
1,4-Dichlorobenzene ug/L 48.350 97 60-140
2,2-Dichloropropane ug/L 51.450 103 60-140
2-Chlorotoluene ug/L 47.150 94 60-140
4-Chlorotoluene ug/L 47.350 95 60-140
Benzene ug/L 47.350 95 60-140
Bromobenzene ug/L 49.450 99 60-140
Bromochloromethane ug/L 51.450 103 60-140
Bromodichloromethane ug/L 50.750 101 60-140
Bromoform ug/L 50.750 101 60-140
Bromomethane ug/L 52.750 105 60-140
Carbon tetrachloride ug/L 52.850 106 60-140
Chlorobenzene ug/L 48.050 96 60-140
Chloroethane ug/L 44.450 89 60-140
Chloroform ug/L 47.650 95 60-140
Chloromethane ug/L 46.450 93 60-140
cis-1,2-Dichloroethene ug/L 43.650 87 60-140
cis-1,3-Dichloropropene ug/L 53.450 107 60-140
Dibromochloromethane ug/L 53.250 106 60-140
Dibromomethane ug/L 52.650 105 60-140
Dichlorodifluoromethane ug/L 51.250 102 60-140
Diisopropyl ether ug/L 43.050 86 60-140
Ethylbenzene ug/L 47.750 95 60-140
Hexachloro-1,3-butadiene ug/L 53.650 107 60-140
Isopropylbenzene (Cumene)ug/L 49.150 98 60-140
m&p-Xylene ug/L 95.8100 96 60-140
Methyl-tert-butyl ether ug/L 46.250 92 60-140
Methylene Chloride ug/L 45.250 90 60-140
n-Butylbenzene ug/L 49.350 99 60-140
n-Propylbenzene ug/L 47.750 95 60-140
Naphthalene ug/L 49.850 100 60-140
o-Xylene ug/L 48.450 97 60-140
sec-Butylbenzene ug/L 49.950 100 60-140
Styrene ug/L 50.150 100 60-140
tert-Butylbenzene ug/L 41.250 82 60-140
Tetrachloroethene ug/L 50.450 101 60-140
Toluene ug/L 46.650 93 60-140
trans-1,2-Dichloroethene ug/L 44.050 88 60-140
trans-1,3-Dichloropropene ug/L 53.950 108 60-140
Trichloroethene ug/L 49.450 99 60-140
Trichlorofluoromethane ug/L 44.350 89 60-140
Vinyl chloride ug/L 47.350 95 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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[phone]
Page 13 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2502353MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92418247004
2502354
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 101 60-140102 14000ND40204060
1,1,1-Trichloroethane ug/L 4000 97 60-14095 24000ND39003800
1,1,2,2-Tetrachloroethane ug/L 4000 93 60-14091 24000ND37103650
1,1,2-Trichloroethane ug/L 4000 101 60-14097 34000ND40203890
1,1-Dichloroethane ug/L 4000 93 60-14090 34000ND37303620
1,1-Dichloroethene ug/L 4000 95 60-14095 04000ND38003810
1,1-Dichloropropene ug/L 4000 96 60-14092 44000ND38303700
1,2,3-Trichlorobenzene ug/L 4000 101 60-140105 44000ND40304190
1,2,3-Trichloropropane ug/L 4000 91 60-14088 44000ND36503510
1,2,4-Trichlorobenzene ug/L 4000 100 60-140103 34000ND40104120
1,2,4-Trimethylbenzene ug/L 4000 94 60-14095 04000168054405470
1,2-Dibromo-3-chloropropane ug/L 4000 95 60-14092 34000ND37803680
1,2-Dibromoethane (EDB)ug/L 4000 99 60-140102 34000ND39504090
1,2-Dichlorobenzene ug/L 4000 98 60-140100 24000ND39203980
1,2-Dichloroethane ug/L 4000 83 60-14083 0400067.5J 3400 3400
1,2-Dichloropropane ug/L 4000 96 60-14094 24000ND38403760
1,3,5-Trimethylbenzene ug/L 4000 95 60-14098 3400042442304350
1,3-Dichlorobenzene ug/L 4000 98 60-14098 04000ND39103900
1,3-Dichloropropane ug/L 4000 97 60-14097 14000ND38903860
1,4-Dichlorobenzene ug/L 4000 97 60-14097 04000ND38903890
2,2-Dichloropropane ug/L 4000 97 60-14097 14000ND39003880
2-Chlorotoluene ug/L 4000 99 60-14095 44000ND39503800
4-Chlorotoluene ug/L 4000 96 60-14095 14000ND38503820
Benzene ug/L 4000 93 60-14095 04000119001570015700
Bromobenzene ug/L 4000 99 60-140100 14000ND39804010
Bromochloromethane ug/L 4000 102 60-14099 34000ND40803970
Bromodichloromethane ug/L 4000 96 60-14098 24000ND38503930
Bromoform ug/L 4000 87 60-14086 14000ND34903460
Bromomethane ug/L 4000 74 60-14092 224000ND29503690
Carbon tetrachloride ug/L 4000 103 60-140106 34000ND41004240
Chlorobenzene ug/L 4000 98 60-14098 04000ND39103900
Chloroethane ug/L 4000 106 60-14090 174000ND42603590
Chloroform ug/L 4000 101 60-14099 24000ND40603970
Chloromethane ug/L 4000 99 60-140100 04000ND39603980
cis-1,2-Dichloroethene ug/L 4000 93 60-14091 34000ND37303630
cis-1,3-Dichloropropene ug/L 4000 99 60-140101 24000ND39604060
Dibromochloromethane ug/L 4000 94 60-14098 44000ND37703920
Dibromomethane ug/L 4000 102 60-140104 24000ND40904170
Dichlorodifluoromethane ug/L 4000 110 60-140104 54000ND44004170
Diisopropyl ether ug/L 4000 89 60-14086 24000156051205010
Ethylbenzene ug/L 4000 97 60-14098 14000162055005560
Hexachloro-1,3-butadiene ug/L 4000 102 60-140109 64000ND41004370
Isopropylbenzene (Cumene)ug/L 4000 102 60-140103 24000ND40704130
m&p-Xylene ug/L 8000 94 60-14097 2800071701470014900
Methyl-tert-butyl ether ug/L 4000 102 60-14088 24000219002600025400
Methylene Chloride ug/L 4000 93 60-14089 44000ND37103570
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2502353MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92418247004
2502354
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 4000 94 60-14097 44000ND37403880
n-Propylbenzene ug/L 4000 96 60-14097 1400016539904050
Naphthalene ug/L 4000 94 60-14096 2400062143804460
o-Xylene ug/L 4000 100 60-14098 14000334073507270
sec-Butylbenzene ug/L 4000 102 60-140101 14000ND40704040
Styrene ug/L 4000 101 60-140101 1400053.5J 4110 4080
tert-Butylbenzene ug/L 4000 85 60-14086 14000ND33903430
Tetrachloroethene ug/L 4000 103 60-140101 24000ND41204060
Toluene ug/L 4000 79 60-14085 14000218002500025200
trans-1,2-Dichloroethene ug/L 4000 93 60-14091 24000ND37103630
trans-1,3-Dichloropropene ug/L 4000 100 60-140101 24000ND39804060
Trichloroethene ug/L 4000 102 60-140105 34000ND40804210
Trichlorofluoromethane ug/L 4000 106 60-140104 24000ND42404170
Vinyl chloride ug/L 4000 103 60-140100 34000ND41204000
1,2-Dichloroethane-d4 (S)%94 70-13090
4-Bromofluorobenzene (S)%97 70-13098
Toluene-d8 (S)%97 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
459041
EPA 625.1
EPA 625.1
625 MSS
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2501900
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 02/20/19 15:43
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 02/20/19 15:43
2,4,6-Trichlorophenol ug/L ND 10.0 02/20/19 15:43
2,4-Dichlorophenol ug/L ND 5.0 02/20/19 15:43
2,4-Dimethylphenol ug/L ND 10.0 02/20/19 15:43
2,4-Dinitrophenol ug/L ND 50.0 02/20/19 15:43
2,4-Dinitrotoluene ug/L ND 5.0 02/20/19 15:43
2,6-Dinitrotoluene ug/L ND 5.0 02/20/19 15:43
2-Chloronaphthalene ug/L ND 5.0 02/20/19 15:43
2-Chlorophenol ug/L ND 5.0 02/20/19 15:43
2-Nitrophenol ug/L ND 5.0 02/20/19 15:43
3,3'-Dichlorobenzidine ug/L ND 25.0 02/20/19 15:43
4,6-Dinitro-2-methylphenol ug/L ND 20.0 02/20/19 15:43
4-Bromophenylphenyl ether ug/L ND 5.0 02/20/19 15:43
4-Chloro-3-methylphenol ug/L ND 5.0 02/20/19 15:43
4-Chlorophenylphenyl ether ug/L ND 5.0 02/20/19 15:43
4-Nitrophenol ug/L ND 50.0 02/20/19 15:43
Acenaphthene ug/L ND 5.0 02/20/19 15:43
Acenaphthylene ug/L ND 5.0 02/20/19 15:43
Anthracene ug/L ND 5.0 02/20/19 15:43
Benzo(a)anthracene ug/L ND 5.0 02/20/19 15:43
Benzo(a)pyrene ug/L ND 5.0 02/20/19 15:43
Benzo(b)fluoranthene ug/L ND 5.0 02/20/19 15:43
Benzo(g,h,i)perylene ug/L ND 5.0 02/20/19 15:43
Benzo(k)fluoranthene ug/L ND 5.0 02/20/19 15:43
bis(2-Chloroethoxy)methane ug/L ND 10.0 02/20/19 15:43
bis(2-Chloroethyl) ether ug/L ND 5.0 02/20/19 15:43
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 02/20/19 15:43
Butylbenzylphthalate ug/L ND 5.0 02/20/19 15:43
Chrysene ug/L ND 5.0 02/20/19 15:43
Di-n-butylphthalate ug/L ND 5.0 02/20/19 15:43
Di-n-octylphthalate ug/L ND 5.0 02/20/19 15:43
Dibenz(a,h)anthracene ug/L ND 5.0 02/20/19 15:43
Diethylphthalate ug/L ND 5.0 02/20/19 15:43
Dimethylphthalate ug/L ND 5.0 02/20/19 15:43
Fluoranthene ug/L ND 5.0 02/20/19 15:43
Fluorene ug/L ND 5.0 02/20/19 15:43
Hexachloro-1,3-butadiene ug/L ND 5.0 02/20/19 15:43
Hexachlorobenzene ug/L ND 5.0 02/20/19 15:43
Hexachlorocyclopentadiene ug/L ND 10.0 02/20/19 15:43
Hexachloroethane ug/L ND 5.0 02/20/19 15:43
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2501900
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 02/20/19 15:43
Isophorone ug/L ND 10.0 02/20/19 15:43
N-Nitroso-di-n-propylamine ug/L ND 5.0 02/20/19 15:43
N-Nitrosodimethylamine ug/L ND 5.0 02/20/19 15:43
N-Nitrosodiphenylamine ug/L ND 10.0 02/20/19 15:43
Naphthalene ug/L ND 5.0 02/20/19 15:43
Nitrobenzene ug/L ND 5.0 02/20/19 15:43
Pentachlorophenol ug/L ND 10.0 02/20/19 15:43
Phenanthrene ug/L ND 5.0 02/20/19 15:43
Phenol ug/L ND 5.0 02/20/19 15:43
Pyrene ug/L ND 5.0 02/20/19 15:43
2,4,6-Tribromophenol (S)%69 10-137 02/20/19 15:43
2-Fluorobiphenyl (S)%58 15-120 02/20/19 15:43
2-Fluorophenol (S)%34 10-120 02/20/19 15:43
Nitrobenzene-d5 (S)%67 10-120 02/20/19 15:43
Phenol-d6 (S)%27 10-120 02/20/19 15:43
Terphenyl-d14 (S)%73 11-131 02/20/19 15:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2501901LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.550 55 44-142
2,2'-Oxybis(1-chloropropane)ug/L 43.050 86 36-166
2,4,6-Trichlorophenol ug/L 42.550 85 37-144
2,4-Dichlorophenol ug/L 35.650 71 39-135
2,4-Dimethylphenol ug/L 40.950 82 32-120
2,4-Dinitrophenol ug/L 228250 91 1-191
2,4-Dinitrotoluene ug/L 39.050 78 39-139
2,6-Dinitrotoluene ug/L 40.450 81 50-158
2-Chloronaphthalene ug/L 35.050 70 60-120
2-Chlorophenol ug/L 33.550 67 23-134
2-Nitrophenol ug/L 35.150 70 29-181
3,3'-Dichlorobenzidine ug/L 61.7100 62 1-262
4,6-Dinitro-2-methylphenol ug/L 93.5100 94 1-181
4-Bromophenylphenyl ether ug/L 42.050 84 53-127
4-Chloro-3-methylphenol ug/L 86.0100 86 22-147
4-Chlorophenylphenyl ether ug/L 42.450 85 25-158
4-Nitrophenol ug/L 122250 49 1-132
Acenaphthene ug/L 39.650 79 47-145
Acenaphthylene ug/L 41.450 83 33-145
Anthracene ug/L 40.650 81 27-133
Benzo(a)anthracene ug/L 44.550 89 33-143
Benzo(a)pyrene ug/L 45.150 90 17-163
Benzo(b)fluoranthene ug/L 41.050 82 24-159
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2501901LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(g,h,i)perylene ug/L 42.850 86 1-219
Benzo(k)fluoranthene ug/L 41.250 82 11-162
bis(2-Chloroethoxy)methane ug/L 37.650 75 33-184
bis(2-Chloroethyl) ether ug/L 35.250 70 12-158
bis(2-Ethylhexyl)phthalate ug/L 48.350 97 8-158
Butylbenzylphthalate ug/L 41.950 84 1-152
Chrysene ug/L 38.950 78 17-168
Di-n-butylphthalate ug/L 44.950 90 1-120
Di-n-octylphthalate ug/L 41.150 82 4-146
Dibenz(a,h)anthracene ug/L 42.050 84 1-227
Diethylphthalate ug/L 43.750 87 1-120
Dimethylphthalate ug/L 42.350 85 1-120
Fluoranthene ug/L 38.950 78 26-137
Fluorene ug/L 44.150 88 59-121
Hexachloro-1,3-butadiene ug/L 25.650 51 24-120
Hexachlorobenzene ug/L 38.350 77 1-152
Hexachlorocyclopentadiene ug/L 28.350 57 25-150
Hexachloroethane ug/L 26.150 52 40-120
Indeno(1,2,3-cd)pyrene ug/L 42.150 84 1-171
Isophorone ug/L 40.350 81 21-196
N-Nitroso-di-n-propylamine ug/L 44.450 89 1-230
N-Nitrosodimethylamine ug/L 23.350 47 25-150
N-Nitrosodiphenylamine ug/L 44.550 89 25-150
Naphthalene ug/L 36.050 72 21-133
Nitrobenzene ug/L 39.850 80 35-180
Pentachlorophenol ug/L 90.8100 91 14-176
Phenanthrene ug/L 41.150 82 54-120
Phenol ug/L 17.750 35 5-120
Pyrene ug/L 45.450 91 52-120
2,4,6-Tribromophenol (S)%81 10-137
2-Fluorobiphenyl (S)%73 15-120
2-Fluorophenol (S)%45 10-120
Nitrobenzene-d5 (S)%83 10-120
Phenol-d6 (S)%35 10-120
Terphenyl-d14 (S)%78 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2501902MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35448068001
2501903
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M11003544-14235 01000.98U 35.4 35.3
2,2'-Oxybis(1-chloropropane)ug/L 100 53 36-16654 21000.95U 52.9 54.1
2,4,6-Trichlorophenol ug/L 100 51 37-14455 71001.3U 51.1 54.5
2,4-Dichlorophenol ug/L 100 47 39-13545 31001.7U 46.7 45.3
2,4-Dimethylphenol ug/L 100 53 32-12051 51001.2U 53.1 50.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
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[phone]
Page 18 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2501902MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35448068001
2501903
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dinitrophenol ug/L 500 39 1-19145 145009.0U 193 223
2,4-Dinitrotoluene ug/L 100 57 39-13977 301000.90U 56.6 77.0
2,6-Dinitrotoluene ug/L 100 55 50-15869 231000.98U 55.2 69.5
2-Chloronaphthalene ug/L M11004360-12043 11000.98U 43.5 43.0
2-Chlorophenol ug/L 100 42 23-13442 01001.3U 42.5 42.3
2-Nitrophenol ug/L 100 45 29-18245 11000.91U 44.9 45.4
3,3'-Dichlorobenzidine ug/L 200 37 1-26243 132002.1U 74.9 85.6
4,6-Dinitro-2-methylphenol ug/L 200 56 1-18176 292002.6U 112 151
4-Bromophenylphenyl ether ug/L 100 54 53-12765 191000.82U 53.5 64.8
4-Chloro-3-methylphenol ug/L 200 56 22-14760 72003.7U 113 121
4-Chlorophenylphenyl ether ug/L 100 54 25-15863 151000.87U 54.0 62.8
4-Nitrophenol ug/L 500 34 1-13247 325004.1U 170 234
Acenaphthene ug/L 100 51 47-14555 81000.25U 50.8 54.7
Acenaphthylene ug/L 100 57 33-14559 41000.21U 57.1 59.2
Anthracene ug/L 100 58 27-13375 251000.14U 58.4 75.2
Benzo(a)anthracene ug/L 100 62 33-14384 291000.33U 62.3 83.9
Benzo(a)pyrene ug/L 100 64 17-16390 351000.30U 63.5 90.2
Benzo(b)fluoranthene ug/L 100 64 24-15994 371000.28U 64.2 93.6
Benzo(g,h,i)perylene ug/L 100 56 1-21972 261000.38U 55.7 72.2
Benzo(k)fluoranthene ug/L 100 63 11-16292 381000.43U 62.6 92.3
bis(2-Chloroethoxy)methane ug/L 100 47 33-18445 41000.92U 46.9 45.3
bis(2-Chloroethyl) ether ug/L 100 45 12-15845 11001.0U 45.0 45.5
bis(2-Ethylhexyl)phthalate ug/L 100 69 8-15895 311000.79U 68.9 94.6
Butylbenzylphthalate ug/L 100 66 1-15291 311000.79U 66.4 90.7
Chrysene ug/L 100 55 17-16878 351000.21U 54.7 78.0
Di-n-butylphthalate ug/L 100 63 1-12084 281000.75U 63.0 83.7
Di-n-octylphthalate ug/L 100 63 4-14689 341000.66U 63.5 89.5
Dibenz(a,h)anthracene ug/L 100 54 1-22786 461000.55U 54.0 86.2
Diethylphthalate ug/L 100 63 1-12085 291000.58U 63.1 84.9
Dimethylphthalate ug/L 100 57 1-12071 221000.76U 57.2 71.5
Fluoranthene ug/L 100 58 26-13780 321000.21U 58.2 80.2
Fluorene ug/L M11005859-12169 171000.21U 58.3 69.1
Hexachloro-1,3-butadiene ug/L 100 31 24-12032 31000.94U 30.8 31.7
Hexachlorobenzene ug/L 100 49 1-15265 291000.72U 48.8 65.2
Hexachlorocyclopentadiene ug/L 100 29 25-15030 11000.88U 29.2 29.5
Hexachloroethane ug/L M11003040-12030 01001.1U 29.9 29.8
Indeno(1,2,3-cd)pyrene ug/L 100 59 1-17188 401000.29U 58.6 87.7
Isophorone ug/L 100 54 21-19651 51000.89U 53.6 51.1
N-Nitroso-di-n-propylamine ug/L 100 56 1-23053 61000.99U 55.7 52.6
N-Nitrosodimethylamine ug/L 100 28 25-15030 71000.91U 27.5 29.6
N-Nitrosodiphenylamine ug/L 100 60 25-15081 291001.0U 60.2 80.7
Naphthalene ug/L 100 45 21-13345 01000.34U 45.0 44.8
Nitrobenzene ug/L 100 57 35-18061 61001.1U 57.5 60.9
Pentachlorophenol ug/L 200 34 14-17649 352004.6U 68.7 97.3
Phenanthrene ug/L 100 58 54-12076 271000.22U 58.5 76.5
Phenol ug/L 100 22 5-12023 71001.9U 21.6 23.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2501902MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35448068001
2501903
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pyrene ug/L 100 66 52-12090 301000.19U 66.2 89.6
2,4,6-Tribromophenol (S)%53 10-13769
2-Fluorobiphenyl (S)%47 15-12046
2-Fluorophenol (S)%25 10-12026
Nitrobenzene-d5 (S)%53 10-12052
Phenol-d6 (S)%20 10-12022
Terphenyl-d14 (S)%54 11-13167
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458546
EPA 180.1 Rev 2.0 1993
EPA 180.1 Rev 2.0 1993
180.1 Turbidity
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2499908
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Turbidity NTU ND 1.0 02/16/19 01:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2499909LABORATORY CONTROL SAMPLE:
LCSSpike
Turbidity NTU 10.310 103 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92417986001
2499910SAMPLE DUPLICATE:
Turbidity NTU 17.0 116.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/21/2019 04:02 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458883
SM 2540D-2011
SM 2540D-2011
2540D Total Suspended Solids
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2501073
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Total Suspended Solids mg/L ND 2.5 02/19/19 10:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2501074LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 252250 101 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92417854002
2501075SAMPLE DUPLICATE:
Total Suspended Solids mg/L NDND
Parameter Units
Dup
Result QualifiersRPDResult
92417510007
2501076SAMPLE DUPLICATE:
Total Suspended Solids mg/L 17.0 D6616.0
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458542
SM 5210B-2011
SM 5210B-2011
5210B BOD, 5 day
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2499904
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
BOD, 5 day mg/L ND 2.0 02/21/19 04:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2499905LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day mg/L 191198 97 84.6-115
Parameter Units
Dup
Result QualifiersRPDResult
92417974001
2499907SAMPLE DUPLICATE:
BOD, 5 day mg/L 293 D619242
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458610
EPA 9040C
EPA 9040C
9040 pH
Associated Lab Samples:92417986001
Parameter Units
Dup
Result QualifiersRPDResult
92417518001
2500129SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 13.2 E,H3113.1
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458909
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2501197
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 02/20/19 10:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2501198LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.15 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2501199MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417769001
2501200
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 106 90-110107 150.34 5.6 5.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2501201MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417503008
2501202
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 102 90-110101 15ND5.2 5.1
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458642
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2500196
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Nitrogen, Kjeldahl, Total mg/L ND 0.50 02/19/19 00:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500197LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 9.910 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500198MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92418025001
2500199
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 100 90-11097 310ND10.4 10.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500202MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417788001
2500203
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L M11013090-110140 31028.0 41.0 42.0
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458548
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2499911
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 02/16/19 03:32
Nitrogen, Nitrite mg/L ND 0.020 02/16/19 03:32
Nitrogen, NO2 plus NO3 mg/L ND 0.020 02/16/19 03:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2499912LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.51.5 97 90-110
Nitrogen, Nitrite mg/L 1.01 104 90-110
Nitrogen, NO2 plus NO3 mg/L 2.52.5 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2499913MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417986001
2499914
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 100 90-110106 51.50.028 1.5 1.6
Nitrogen, Nitrite mg/L 1 105 90-110106 010.027 1.1 1.1
Nitrogen, NO2 plus NO3 mg/L 2.5 102 90-110106 32.50.054 2.6 2.7
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458781
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2500810
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Phosphorus mg/L ND 0.050 02/18/19 21:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500811LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/L 2.52.5 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500812MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92418025001
2500813
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/L 2.5 100 90-11099 12.50.086 2.6 2.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500814MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417501007
2500815
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/L 2.5 93 90-110107 82.51.9 4.2 4.6
REPORT OF LABORATORY ANALYSIS
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Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417986
Powell Industries
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458669
EPA 420.4 Rev 1.0 1993
EPA 420.4 Rev 1.0 1993
420.4 Phenolics
Associated Lab Samples:92417986001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2500293
Associated Lab Samples:92417986001
Matrix:Water
Analyzed
Phenol mg/L ND 0.020 02/19/19 14:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500294LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol mg/L 0.0500.05 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500295MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417266001
2500296
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol mg/L 0.05 94 90-11092 20.05ND 0.052 0.051
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2500297MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417646002
2500298
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol mg/L 0.05 95 90-110100 30.050.029 0.076 0.079
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92417986
Powell Industries
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92417986
Powell Industries
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92417986001 458552 458568WW-01 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92417986001 458622 458646WW-01 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92417986001 459041 459202WW-01 EPA 625.1 EPA 625.1
92417986001 459154WW-01 SM 6200B
92417986001 458546WW-01 EPA 180.1 Rev 2.0 1993
92417986001 458883WW-01 SM 2540D-2011
92417986001 458542 458561WW-01 SM 5210B-2011 SM 5210B-2011
92417986001 458610WW-01 EPA 9040C
92417986001 458909WW-01 EPA 350.1 Rev 2.0 1993
92417986001 458642 458829WW-01 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92417986001 458548WW-01 EPA 353.2 Rev 2.0 1993
92417986001 458781 458813WW-01 EPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92417986001 458669 458868WW-01 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
REPORT OF LABORATORY ANALYSIS
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Page 31 of 34
Page 32 of 34
Page 33 of 34
Page 34 of 34
#=CL#
April 30, 2019
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92425518
92425518
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
Powell 4/12
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on April 12, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 67
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92425518
Powell 4/12
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 67
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92425518
Powell 4/12
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92425518001 C-1 EPA 6010D 12 PASI-ADS
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AGC
92425518002 C-1A EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518003 C-1B EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518004 C-1C EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518005 C-1D EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518006 C-2 EPA 6010D 12 PASI-ADS
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AGC
92425518008 C-2A EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518009 C-2B EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518010 C-2C EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92425518011 C-2D EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1 Lab ID:92425518001 Collected:04/12/19 14:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 3.7 mg/kg 04/27/19 18:07 7440-38-2 M104/25/19 17:251.8 1
Cadmium ND mg/kg 04/27/19 18:07 7440-43-9 M104/25/19 17:250.18 1
Calcium 7860 mg/kg 04/27/19 18:07 7440-70-2 M104/25/19 17:2517.8 1
Chromium 59.9 mg/kg 04/27/19 18:07 7440-47-304/25/19 17:250.89 1
Copper 96.4 mg/kg 04/27/19 18:07 7440-50-804/25/19 17:250.89 1
Lead 15.8 mg/kg 04/27/19 18:07 7439-92-1 M104/25/19 17:250.89 1
Magnesium 12100 mg/kg 04/27/19 18:07 7439-95-4 M104/25/19 17:2517.8 1
Molybdenum 3.1 mg/kg 04/27/19 18:07 7439-98-7 M104/25/19 17:250.89 1
Nickel 32.1 mg/kg 04/27/19 18:07 7440-02-0 M104/25/19 17:250.89 1
Selenium ND mg/kg 04/27/19 18:07 7782-49-2 M104/25/19 17:251.8 1
Sodium ND mg/kg 04/27/19 18:07 7440-23-504/25/19 17:258881
Zinc 264 mg/kg 04/27/19 18:07 7440-66-6 M104/25/19 17:251.8 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.046 mg/kg 04/23/19 13:33 7439-97-604/22/19 16:340.014 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 04/22/19 23:51 83-32-904/22/19 12:298491
Acenaphthylene ND ug/kg 04/22/19 23:51 208-96-804/22/19 12:298491
Aniline ND ug/kg 04/22/19 23:51 62-53-304/22/19 12:298491
Anthracene ND ug/kg 04/22/19 23:51 120-12-704/22/19 12:298491
Benzo(a)anthracene ND ug/kg 04/22/19 23:51 56-55-304/22/19 12:298491
Benzo(a)pyrene ND ug/kg 04/22/19 23:51 50-32-804/22/19 12:298491
Benzo(b)fluoranthene ND ug/kg 04/22/19 23:51 205-99-204/22/19 12:298491
Benzo(g,h,i)perylene ND ug/kg 04/22/19 23:51 191-24-204/22/19 12:298491
Benzo(k)fluoranthene ND ug/kg 04/22/19 23:51 207-08-904/22/19 12:298491
Benzoic Acid ND ug/kg 04/22/19 23:51 65-85-0 v104/22/19 12:2942501
Benzyl alcohol ND ug/kg 04/22/19 23:51 100-51-604/22/19 12:2917001
4-Bromophenylphenyl ether ND ug/kg 04/22/19 23:51 101-55-304/22/19 12:298491
Butylbenzylphthalate ND ug/kg 04/22/19 23:51 85-68-704/22/19 12:298491
4-Chloro-3-methylphenol ND ug/kg 04/22/19 23:51 59-50-704/22/19 12:2917001
4-Chloroaniline ND ug/kg 04/22/19 23:51 106-47-804/22/19 12:2942501
bis(2-Chloroethoxy)methane ND ug/kg 04/22/19 23:51 111-91-104/22/19 12:298491
bis(2-Chloroethyl) ether ND ug/kg 04/22/19 23:51 111-44-404/22/19 12:298491
2-Chloronaphthalene ND ug/kg 04/22/19 23:51 91-58-704/22/19 12:298491
2-Chlorophenol ND ug/kg 04/22/19 23:51 95-57-804/22/19 12:298491
4-Chlorophenylphenyl ether ND ug/kg 04/22/19 23:51 7005-72-304/22/19 12:298491
Chrysene ND ug/kg 04/22/19 23:51 218-01-904/22/19 12:298491
Dibenz(a,h)anthracene ND ug/kg 04/22/19 23:51 53-70-304/22/19 12:298491
Dibenzofuran ND ug/kg 04/22/19 23:51 132-64-904/22/19 12:298491
1,2-Dichlorobenzene ND ug/kg 04/22/19 23:51 95-50-104/22/19 12:298491
1,3-Dichlorobenzene ND ug/kg 04/22/19 23:51 541-73-104/22/19 12:298491
1,4-Dichlorobenzene ND ug/kg 04/22/19 23:51 106-46-704/22/19 12:298491
3,3'-Dichlorobenzidine ND ug/kg 04/22/19 23:51 91-94-1 v104/22/19 12:2942501
2,4-Dichlorophenol ND ug/kg 04/22/19 23:51 120-83-2 v104/22/19 12:298491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1 Lab ID:92425518001 Collected:04/12/19 14:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Diethylphthalate ND ug/kg 04/22/19 23:51 84-66-204/22/19 12:298491
2,4-Dimethylphenol ND ug/kg 04/22/19 23:51 105-67-904/22/19 12:298491
Dimethylphthalate ND ug/kg 04/22/19 23:51 131-11-304/22/19 12:298491
Di-n-butylphthalate ND ug/kg 04/22/19 23:51 84-74-204/22/19 12:298491
4,6-Dinitro-2-methylphenol ND ug/kg 04/22/19 23:51 534-52-1 v104/22/19 12:2917001
2,4-Dinitrophenol ND ug/kg 04/22/19 23:51 51-28-5 v104/22/19 12:2942501
2,4-Dinitrotoluene ND ug/kg 04/22/19 23:51 121-14-204/22/19 12:298491
2,6-Dinitrotoluene ND ug/kg 04/22/19 23:51 606-20-204/22/19 12:298491
Di-n-octylphthalate ND ug/kg 04/22/19 23:51 117-84-004/22/19 12:298491
bis(2-Ethylhexyl)phthalate ND ug/kg 04/22/19 23:51 117-81-704/22/19 12:298491
Fluoranthene ND ug/kg 04/22/19 23:51 206-44-004/22/19 12:298491
Fluorene ND ug/kg 04/22/19 23:51 86-73-704/22/19 12:298491
Hexachloro-1,3-butadiene ND ug/kg 04/22/19 23:51 87-68-304/22/19 12:298491
Hexachlorobenzene ND ug/kg 04/22/19 23:51 118-74-104/22/19 12:298491
Hexachlorocyclopentadiene ND ug/kg 04/22/19 23:51 77-47-404/22/19 12:298491
Hexachloroethane ND ug/kg 04/22/19 23:51 67-72-104/22/19 12:298491
Indeno(1,2,3-cd)pyrene ND ug/kg 04/22/19 23:51 193-39-504/22/19 12:298491
Isophorone ND ug/kg 04/22/19 23:51 78-59-104/22/19 12:298491
1-Methylnaphthalene ND ug/kg 04/22/19 23:51 90-12-004/22/19 12:298491
2-Methylnaphthalene ND ug/kg 04/22/19 23:51 91-57-604/22/19 12:298491
2-Methylphenol(o-Cresol)ND ug/kg 04/22/19 23:51 95-48-704/22/19 12:298491
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/22/19 23:51 15831-10-404/22/19 12:298491
Naphthalene ND ug/kg 04/22/19 23:51 91-20-304/22/19 12:298491
2-Nitroaniline ND ug/kg 04/22/19 23:51 88-74-404/22/19 12:2942501
3-Nitroaniline ND ug/kg 04/22/19 23:51 99-09-204/22/19 12:2942501
4-Nitroaniline ND ug/kg 04/22/19 23:51 100-01-604/22/19 12:2917001
Nitrobenzene ND ug/kg 04/22/19 23:51 98-95-304/22/19 12:298491
2-Nitrophenol ND ug/kg 04/22/19 23:51 88-75-5 v104/22/19 12:298491
4-Nitrophenol ND ug/kg 04/22/19 23:51 100-02-704/22/19 12:2942501
N-Nitrosodimethylamine ND ug/kg 04/22/19 23:51 62-75-904/22/19 12:298491
N-Nitroso-di-n-propylamine ND ug/kg 04/22/19 23:51 621-64-704/22/19 12:298491
N-Nitrosodiphenylamine ND ug/kg 04/22/19 23:51 86-30-604/22/19 12:298491
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/22/19 23:51 108-60-104/22/19 12:298491
Pentachlorophenol ND ug/kg 04/22/19 23:51 87-86-504/22/19 12:2942501
Phenanthrene ND ug/kg 04/22/19 23:51 85-01-804/22/19 12:298491
Phenol ND ug/kg 04/22/19 23:51 108-95-2 v104/22/19 12:298491
Pyrene ND ug/kg 04/22/19 23:51 129-00-004/22/19 12:298491
1,2,4-Trichlorobenzene ND ug/kg 04/22/19 23:51 120-82-104/22/19 12:298491
2,4,5-Trichlorophenol ND ug/kg 04/22/19 23:51 95-95-404/22/19 12:298491
2,4,6-Trichlorophenol ND ug/kg 04/22/19 23:51 88-06-204/22/19 12:298491
Surrogates
Nitrobenzene-d5 (S)66 %04/22/19 23:51 4165-60-004/22/19 12:2923-110 1
2-Fluorobiphenyl (S)66 %04/22/19 23:51 321-60-804/22/19 12:2930-110 1
Terphenyl-d14 (S)72 %04/22/19 23:51 1718-51-004/22/19 12:2928-110 1
Phenol-d6 (S)70 %04/22/19 23:51 13127-88-304/22/19 12:2922-110 1
2-Fluorophenol (S)69 %04/22/19 23:51 367-12-404/22/19 12:2913-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1 Lab ID:92425518001 Collected:04/12/19 14:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)88 %04/22/19 23:51 118-79-604/22/19 12:2927-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 60.9 %04/16/19 14:000.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 3560 mg/kg 04/20/19 00:44 7727-37-904/19/19 07:1094.7 1
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 04/16/19 01:49 H1,H204/15/19 23:479.9 1
Nitrogen, Nitrate ND mg/kg 04/16/19 01:49 14797-55-804/15/19 23:479.9 1
Nitrogen, Nitrite ND mg/kg 04/16/19 01:49 14797-65-0 H1,H204/15/19 23:479.9 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993365.1 Phosphorus, Total
Phosphorus 692 mg/kg 04/16/19 23:48 7723-14-0 M1,R104/16/19 18:3510.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1A Lab ID:92425518002 Collected:04/12/19 15:02 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 457 ug/kg 04/22/19 16:25 67-64-104/19/19 14:033741
Benzene ND ug/kg 04/22/19 16:25 71-43-204/19/19 14:0318.7 1
Bromobenzene ND ug/kg 04/22/19 16:25 108-86-104/19/19 14:0318.7 1
Bromochloromethane ND ug/kg 04/22/19 16:25 74-97-504/19/19 14:0318.7 1
Bromodichloromethane ND ug/kg 04/22/19 16:25 75-27-404/19/19 14:0318.7 1
Bromoform ND ug/kg 04/22/19 16:25 75-25-204/19/19 14:0318.7 1
Bromomethane ND ug/kg 04/22/19 16:25 74-83-904/19/19 14:0337.4 1
2-Butanone (MEK)ND ug/kg 04/22/19 16:25 78-93-304/19/19 14:033741
n-Butylbenzene ND ug/kg 04/22/19 16:25 104-51-804/19/19 14:0318.7 1
sec-Butylbenzene ND ug/kg 04/22/19 16:25 135-98-804/19/19 14:0318.7 1
tert-Butylbenzene ND ug/kg 04/22/19 16:25 98-06-604/19/19 14:0318.7 1
Carbon tetrachloride ND ug/kg 04/22/19 16:25 56-23-504/19/19 14:0318.7 1
Chlorobenzene ND ug/kg 04/22/19 16:25 108-90-704/19/19 14:0318.7 1
Chloroethane ND ug/kg 04/22/19 16:25 75-00-304/19/19 14:0337.4 1
Chloroform ND ug/kg 04/22/19 16:25 67-66-304/19/19 14:0318.7 1
Chloromethane ND ug/kg 04/22/19 16:25 74-87-304/19/19 14:0337.4 1
2-Chlorotoluene ND ug/kg 04/22/19 16:25 95-49-804/19/19 14:0318.7 1
4-Chlorotoluene ND ug/kg 04/22/19 16:25 106-43-404/19/19 14:0318.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/22/19 16:25 96-12-804/19/19 14:0318.7 1
Dibromochloromethane ND ug/kg 04/22/19 16:25 124-48-104/19/19 14:0318.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/22/19 16:25 106-93-404/19/19 14:0318.7 1
Dibromomethane ND ug/kg 04/22/19 16:25 74-95-304/19/19 14:0318.7 1
1,2-Dichlorobenzene ND ug/kg 04/22/19 16:25 95-50-104/19/19 14:0318.7 1
1,3-Dichlorobenzene ND ug/kg 04/22/19 16:25 541-73-104/19/19 14:0318.7 1
1,4-Dichlorobenzene ND ug/kg 04/22/19 16:25 106-46-704/19/19 14:0318.7 1
Dichlorodifluoromethane ND ug/kg 04/22/19 16:25 75-71-804/19/19 14:0337.4 1
1,1-Dichloroethane ND ug/kg 04/22/19 16:25 75-34-304/19/19 14:0318.7 1
1,2-Dichloroethane ND ug/kg 04/22/19 16:25 107-06-204/19/19 14:0318.7 1
1,1-Dichloroethene ND ug/kg 04/22/19 16:25 75-35-404/19/19 14:0318.7 1
cis-1,2-Dichloroethene ND ug/kg 04/22/19 16:25 156-59-204/19/19 14:0318.7 1
trans-1,2-Dichloroethene ND ug/kg 04/22/19 16:25 156-60-504/19/19 14:0318.7 1
1,2-Dichloropropane ND ug/kg 04/22/19 16:25 78-87-504/19/19 14:0318.7 1
1,3-Dichloropropane ND ug/kg 04/22/19 16:25 142-28-904/19/19 14:0318.7 1
2,2-Dichloropropane ND ug/kg 04/22/19 16:25 594-20-704/19/19 14:0318.7 1
1,1-Dichloropropene ND ug/kg 04/22/19 16:25 563-58-604/19/19 14:0318.7 1
cis-1,3-Dichloropropene ND ug/kg 04/22/19 16:25 10061-01-504/19/19 14:0318.7 1
trans-1,3-Dichloropropene ND ug/kg 04/22/19 16:25 10061-02-604/19/19 14:0318.7 1
Diisopropyl ether ND ug/kg 04/22/19 16:25 108-20-304/19/19 14:0318.7 1
Ethylbenzene ND ug/kg 04/22/19 16:25 100-41-404/19/19 14:0318.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/22/19 16:25 87-68-304/19/19 14:0318.7 1
2-Hexanone ND ug/kg 04/22/19 16:25 591-78-604/19/19 14:031871
Isopropylbenzene (Cumene)ND ug/kg 04/22/19 16:25 98-82-804/19/19 14:0318.7 1
p-Isopropyltoluene ND ug/kg 04/22/19 16:25 99-87-604/19/19 14:0318.7 1
Methylene Chloride ND ug/kg 04/22/19 16:25 75-09-204/19/19 14:0374.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/22/19 16:25 108-10-104/19/19 14:031871
Methyl-tert-butyl ether ND ug/kg 04/22/19 16:25 1634-04-404/19/19 14:0318.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1A Lab ID:92425518002 Collected:04/12/19 15:02 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/22/19 16:25 91-20-304/19/19 14:0318.7 1
n-Propylbenzene ND ug/kg 04/22/19 16:25 103-65-104/19/19 14:0318.7 1
Styrene ND ug/kg 04/22/19 16:25 100-42-504/19/19 14:0318.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/22/19 16:25 630-20-604/19/19 14:0318.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/22/19 16:25 79-34-504/19/19 14:0318.7 1
Tetrachloroethene ND ug/kg 04/22/19 16:25 127-18-404/19/19 14:0318.7 1
Toluene ND ug/kg 04/22/19 16:25 108-88-304/19/19 14:0318.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/22/19 16:25 87-61-604/19/19 14:0318.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/22/19 16:25 120-82-104/19/19 14:0318.7 1
1,1,1-Trichloroethane ND ug/kg 04/22/19 16:25 71-55-604/19/19 14:0318.7 1
1,1,2-Trichloroethane ND ug/kg 04/22/19 16:25 79-00-504/19/19 14:0318.7 1
Trichloroethene ND ug/kg 04/22/19 16:25 79-01-604/19/19 14:0318.7 1
Trichlorofluoromethane ND ug/kg 04/22/19 16:25 75-69-404/19/19 14:0318.7 1
1,2,3-Trichloropropane ND ug/kg 04/22/19 16:25 96-18-404/19/19 14:0318.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/22/19 16:25 95-63-604/19/19 14:0318.7 1
1,3,5-Trimethylbenzene ND ug/kg 04/22/19 16:25 108-67-804/19/19 14:0318.7 1
Vinyl acetate ND ug/kg 04/22/19 16:25 108-05-404/19/19 14:031871
Vinyl chloride ND ug/kg 04/22/19 16:25 75-01-404/19/19 14:0337.4 1
Xylene (Total)ND ug/kg 04/22/19 16:25 1330-20-704/19/19 14:0337.4 1
m&p-Xylene ND ug/kg 04/22/19 16:25 179601-23-104/19/19 14:0337.4 1
o-Xylene ND ug/kg 04/22/19 16:25 95-47-604/19/19 14:0318.7 1
Surrogates
Toluene-d8 (S)95 %04/22/19 16:25 2037-26-504/19/19 14:0370-130 1
4-Bromofluorobenzene (S)82 %04/22/19 16:25 460-00-404/19/19 14:0370-130 1
1,2-Dichloroethane-d4 (S)103 %04/22/19 16:25 17060-07-004/19/19 14:0370-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 62.8 %04/16/19 14:220.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1B Lab ID:92425518003 Collected:04/12/19 15:10 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 04/19/19 23:01 67-64-104/19/19 13:003741
Benzene ND ug/kg 04/19/19 23:01 71-43-204/19/19 13:0018.7 1
Bromobenzene ND ug/kg 04/19/19 23:01 108-86-104/19/19 13:0018.7 1
Bromochloromethane ND ug/kg 04/19/19 23:01 74-97-504/19/19 13:0018.7 1
Bromodichloromethane ND ug/kg 04/19/19 23:01 75-27-404/19/19 13:0018.7 1
Bromoform ND ug/kg 04/19/19 23:01 75-25-204/19/19 13:0018.7 1
Bromomethane ND ug/kg 04/19/19 23:01 74-83-904/19/19 13:0037.4 1
2-Butanone (MEK)ND ug/kg 04/19/19 23:01 78-93-304/19/19 13:003741
n-Butylbenzene ND ug/kg 04/19/19 23:01 104-51-804/19/19 13:0018.7 1
sec-Butylbenzene ND ug/kg 04/19/19 23:01 135-98-804/19/19 13:0018.7 1
tert-Butylbenzene ND ug/kg 04/19/19 23:01 98-06-604/19/19 13:0018.7 1
Carbon tetrachloride ND ug/kg 04/19/19 23:01 56-23-504/19/19 13:0018.7 1
Chlorobenzene ND ug/kg 04/19/19 23:01 108-90-704/19/19 13:0018.7 1
Chloroethane ND ug/kg 04/19/19 23:01 75-00-304/19/19 13:0037.4 1
Chloroform ND ug/kg 04/19/19 23:01 67-66-304/19/19 13:0018.7 1
Chloromethane ND ug/kg 04/19/19 23:01 74-87-304/19/19 13:0037.4 1
2-Chlorotoluene ND ug/kg 04/19/19 23:01 95-49-804/19/19 13:0018.7 1
4-Chlorotoluene ND ug/kg 04/19/19 23:01 106-43-404/19/19 13:0018.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/19/19 23:01 96-12-804/19/19 13:0018.7 1
Dibromochloromethane ND ug/kg 04/19/19 23:01 124-48-104/19/19 13:0018.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/19/19 23:01 106-93-404/19/19 13:0018.7 1
Dibromomethane ND ug/kg 04/19/19 23:01 74-95-304/19/19 13:0018.7 1
1,2-Dichlorobenzene ND ug/kg 04/19/19 23:01 95-50-104/19/19 13:0018.7 1
1,3-Dichlorobenzene ND ug/kg 04/19/19 23:01 541-73-104/19/19 13:0018.7 1
1,4-Dichlorobenzene ND ug/kg 04/19/19 23:01 106-46-704/19/19 13:0018.7 1
Dichlorodifluoromethane ND ug/kg 04/19/19 23:01 75-71-804/19/19 13:0037.4 1
1,1-Dichloroethane ND ug/kg 04/19/19 23:01 75-34-304/19/19 13:0018.7 1
1,2-Dichloroethane ND ug/kg 04/19/19 23:01 107-06-204/19/19 13:0018.7 1
1,1-Dichloroethene ND ug/kg 04/19/19 23:01 75-35-404/19/19 13:0018.7 1
cis-1,2-Dichloroethene ND ug/kg 04/19/19 23:01 156-59-204/19/19 13:0018.7 1
trans-1,2-Dichloroethene ND ug/kg 04/19/19 23:01 156-60-504/19/19 13:0018.7 1
1,2-Dichloropropane ND ug/kg 04/19/19 23:01 78-87-504/19/19 13:0018.7 1
1,3-Dichloropropane ND ug/kg 04/19/19 23:01 142-28-904/19/19 13:0018.7 1
2,2-Dichloropropane ND ug/kg 04/19/19 23:01 594-20-704/19/19 13:0018.7 1
1,1-Dichloropropene ND ug/kg 04/19/19 23:01 563-58-604/19/19 13:0018.7 1
cis-1,3-Dichloropropene ND ug/kg 04/19/19 23:01 10061-01-504/19/19 13:0018.7 1
trans-1,3-Dichloropropene ND ug/kg 04/19/19 23:01 10061-02-604/19/19 13:0018.7 1
Diisopropyl ether ND ug/kg 04/19/19 23:01 108-20-304/19/19 13:0018.7 1
Ethylbenzene ND ug/kg 04/19/19 23:01 100-41-404/19/19 13:0018.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/19/19 23:01 87-68-304/19/19 13:0018.7 1
2-Hexanone ND ug/kg 04/19/19 23:01 591-78-604/19/19 13:001871
Isopropylbenzene (Cumene)ND ug/kg 04/19/19 23:01 98-82-804/19/19 13:0018.7 1
p-Isopropyltoluene ND ug/kg 04/19/19 23:01 99-87-604/19/19 13:0018.7 1
Methylene Chloride ND ug/kg 04/19/19 23:01 75-09-204/19/19 13:0074.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/19 23:01 108-10-104/19/19 13:001871
Methyl-tert-butyl ether ND ug/kg 04/19/19 23:01 1634-04-404/19/19 13:0018.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1B Lab ID:92425518003 Collected:04/12/19 15:10 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/19/19 23:01 91-20-304/19/19 13:0018.7 1
n-Propylbenzene ND ug/kg 04/19/19 23:01 103-65-104/19/19 13:0018.7 1
Styrene ND ug/kg 04/19/19 23:01 100-42-504/19/19 13:0018.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/19/19 23:01 630-20-604/19/19 13:0018.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/19/19 23:01 79-34-504/19/19 13:0018.7 1
Tetrachloroethene ND ug/kg 04/19/19 23:01 127-18-404/19/19 13:0018.7 1
Toluene ND ug/kg 04/19/19 23:01 108-88-304/19/19 13:0018.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/19/19 23:01 87-61-604/19/19 13:0018.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/19/19 23:01 120-82-104/19/19 13:0018.7 1
1,1,1-Trichloroethane ND ug/kg 04/19/19 23:01 71-55-604/19/19 13:0018.7 1
1,1,2-Trichloroethane ND ug/kg 04/19/19 23:01 79-00-504/19/19 13:0018.7 1
Trichloroethene ND ug/kg 04/19/19 23:01 79-01-604/19/19 13:0018.7 1
Trichlorofluoromethane ND ug/kg 04/19/19 23:01 75-69-404/19/19 13:0018.7 1
1,2,3-Trichloropropane ND ug/kg 04/19/19 23:01 96-18-404/19/19 13:0018.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/19/19 23:01 95-63-604/19/19 13:0018.7 1
1,3,5-Trimethylbenzene ND ug/kg 04/19/19 23:01 108-67-804/19/19 13:0018.7 1
Vinyl acetate ND ug/kg 04/19/19 23:01 108-05-404/19/19 13:001871
Vinyl chloride ND ug/kg 04/19/19 23:01 75-01-404/19/19 13:0037.4 1
Xylene (Total)ND ug/kg 04/19/19 23:01 1330-20-704/19/19 13:0037.4 1
m&p-Xylene ND ug/kg 04/19/19 23:01 179601-23-104/19/19 13:0037.4 1
o-Xylene ND ug/kg 04/19/19 23:01 95-47-604/19/19 13:0018.7 1
Surrogates
Toluene-d8 (S)93 %04/19/19 23:01 2037-26-504/19/19 13:0070-130 1
4-Bromofluorobenzene (S)84 %04/19/19 23:01 460-00-404/19/19 13:0070-130 1
1,2-Dichloroethane-d4 (S)100 %04/19/19 23:01 17060-07-004/19/19 13:0070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 65.9 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1C Lab ID:92425518004 Collected:04/12/19 14:15 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 383 ug/kg 04/19/19 23:26 67-64-104/19/19 13:003181
Benzene ND ug/kg 04/19/19 23:26 71-43-204/19/19 13:0015.9 1
Bromobenzene ND ug/kg 04/19/19 23:26 108-86-104/19/19 13:0015.9 1
Bromochloromethane ND ug/kg 04/19/19 23:26 74-97-504/19/19 13:0015.9 1
Bromodichloromethane ND ug/kg 04/19/19 23:26 75-27-404/19/19 13:0015.9 1
Bromoform ND ug/kg 04/19/19 23:26 75-25-204/19/19 13:0015.9 1
Bromomethane ND ug/kg 04/19/19 23:26 74-83-904/19/19 13:0031.8 1
2-Butanone (MEK)ND ug/kg 04/19/19 23:26 78-93-304/19/19 13:003181
n-Butylbenzene ND ug/kg 04/19/19 23:26 104-51-804/19/19 13:0015.9 1
sec-Butylbenzene ND ug/kg 04/19/19 23:26 135-98-804/19/19 13:0015.9 1
tert-Butylbenzene ND ug/kg 04/19/19 23:26 98-06-604/19/19 13:0015.9 1
Carbon tetrachloride ND ug/kg 04/19/19 23:26 56-23-504/19/19 13:0015.9 1
Chlorobenzene ND ug/kg 04/19/19 23:26 108-90-704/19/19 13:0015.9 1
Chloroethane ND ug/kg 04/19/19 23:26 75-00-304/19/19 13:0031.8 1
Chloroform ND ug/kg 04/19/19 23:26 67-66-304/19/19 13:0015.9 1
Chloromethane ND ug/kg 04/19/19 23:26 74-87-304/19/19 13:0031.8 1
2-Chlorotoluene ND ug/kg 04/19/19 23:26 95-49-804/19/19 13:0015.9 1
4-Chlorotoluene ND ug/kg 04/19/19 23:26 106-43-404/19/19 13:0015.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/19/19 23:26 96-12-804/19/19 13:0015.9 1
Dibromochloromethane ND ug/kg 04/19/19 23:26 124-48-104/19/19 13:0015.9 1
1,2-Dibromoethane (EDB)ND ug/kg 04/19/19 23:26 106-93-404/19/19 13:0015.9 1
Dibromomethane ND ug/kg 04/19/19 23:26 74-95-304/19/19 13:0015.9 1
1,2-Dichlorobenzene ND ug/kg 04/19/19 23:26 95-50-104/19/19 13:0015.9 1
1,3-Dichlorobenzene ND ug/kg 04/19/19 23:26 541-73-104/19/19 13:0015.9 1
1,4-Dichlorobenzene ND ug/kg 04/19/19 23:26 106-46-704/19/19 13:0015.9 1
Dichlorodifluoromethane ND ug/kg 04/19/19 23:26 75-71-804/19/19 13:0031.8 1
1,1-Dichloroethane ND ug/kg 04/19/19 23:26 75-34-304/19/19 13:0015.9 1
1,2-Dichloroethane ND ug/kg 04/19/19 23:26 107-06-204/19/19 13:0015.9 1
1,1-Dichloroethene ND ug/kg 04/19/19 23:26 75-35-404/19/19 13:0015.9 1
cis-1,2-Dichloroethene ND ug/kg 04/19/19 23:26 156-59-204/19/19 13:0015.9 1
trans-1,2-Dichloroethene ND ug/kg 04/19/19 23:26 156-60-504/19/19 13:0015.9 1
1,2-Dichloropropane ND ug/kg 04/19/19 23:26 78-87-504/19/19 13:0015.9 1
1,3-Dichloropropane ND ug/kg 04/19/19 23:26 142-28-904/19/19 13:0015.9 1
2,2-Dichloropropane ND ug/kg 04/19/19 23:26 594-20-704/19/19 13:0015.9 1
1,1-Dichloropropene ND ug/kg 04/19/19 23:26 563-58-604/19/19 13:0015.9 1
cis-1,3-Dichloropropene ND ug/kg 04/19/19 23:26 10061-01-504/19/19 13:0015.9 1
trans-1,3-Dichloropropene ND ug/kg 04/19/19 23:26 10061-02-604/19/19 13:0015.9 1
Diisopropyl ether ND ug/kg 04/19/19 23:26 108-20-304/19/19 13:0015.9 1
Ethylbenzene ND ug/kg 04/19/19 23:26 100-41-404/19/19 13:0015.9 1
Hexachloro-1,3-butadiene ND ug/kg 04/19/19 23:26 87-68-304/19/19 13:0015.9 1
2-Hexanone ND ug/kg 04/19/19 23:26 591-78-604/19/19 13:001591
Isopropylbenzene (Cumene)ND ug/kg 04/19/19 23:26 98-82-804/19/19 13:0015.9 1
p-Isopropyltoluene ND ug/kg 04/19/19 23:26 99-87-604/19/19 13:0015.9 1
Methylene Chloride ND ug/kg 04/19/19 23:26 75-09-204/19/19 13:0063.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/19 23:26 108-10-104/19/19 13:001591
Methyl-tert-butyl ether ND ug/kg 04/19/19 23:26 1634-04-404/19/19 13:0015.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1C Lab ID:92425518004 Collected:04/12/19 14:15 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/19/19 23:26 91-20-304/19/19 13:0015.9 1
n-Propylbenzene ND ug/kg 04/19/19 23:26 103-65-104/19/19 13:0015.9 1
Styrene ND ug/kg 04/19/19 23:26 100-42-504/19/19 13:0015.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/19/19 23:26 630-20-604/19/19 13:0015.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/19/19 23:26 79-34-504/19/19 13:0015.9 1
Tetrachloroethene ND ug/kg 04/19/19 23:26 127-18-404/19/19 13:0015.9 1
Toluene ND ug/kg 04/19/19 23:26 108-88-304/19/19 13:0015.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/19/19 23:26 87-61-604/19/19 13:0015.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/19/19 23:26 120-82-104/19/19 13:0015.9 1
1,1,1-Trichloroethane ND ug/kg 04/19/19 23:26 71-55-604/19/19 13:0015.9 1
1,1,2-Trichloroethane ND ug/kg 04/19/19 23:26 79-00-504/19/19 13:0015.9 1
Trichloroethene ND ug/kg 04/19/19 23:26 79-01-604/19/19 13:0015.9 1
Trichlorofluoromethane ND ug/kg 04/19/19 23:26 75-69-404/19/19 13:0015.9 1
1,2,3-Trichloropropane ND ug/kg 04/19/19 23:26 96-18-404/19/19 13:0015.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/19/19 23:26 95-63-604/19/19 13:0015.9 1
1,3,5-Trimethylbenzene ND ug/kg 04/19/19 23:26 108-67-804/19/19 13:0015.9 1
Vinyl acetate ND ug/kg 04/19/19 23:26 108-05-404/19/19 13:001591
Vinyl chloride ND ug/kg 04/19/19 23:26 75-01-404/19/19 13:0031.8 1
Xylene (Total)ND ug/kg 04/19/19 23:26 1330-20-704/19/19 13:0031.8 1
m&p-Xylene ND ug/kg 04/19/19 23:26 179601-23-104/19/19 13:0031.8 1
o-Xylene ND ug/kg 04/19/19 23:26 95-47-604/19/19 13:0015.9 1
Surrogates
Toluene-d8 (S)94 %04/19/19 23:26 2037-26-504/19/19 13:0070-130 1
4-Bromofluorobenzene (S)83 %04/19/19 23:26 460-00-404/19/19 13:0070-130 1
1,2-Dichloroethane-d4 (S)96 %04/19/19 23:26 17060-07-004/19/19 13:0070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 63.5 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1D Lab ID:92425518005 Collected:04/12/19 14:30 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 586 ug/kg 04/22/19 17:41 67-64-104/19/19 14:034151
Benzene ND ug/kg 04/22/19 17:41 71-43-204/19/19 14:0320.7 1
Bromobenzene ND ug/kg 04/22/19 17:41 108-86-104/19/19 14:0320.7 1
Bromochloromethane ND ug/kg 04/22/19 17:41 74-97-504/19/19 14:0320.7 1
Bromodichloromethane ND ug/kg 04/22/19 17:41 75-27-404/19/19 14:0320.7 1
Bromoform ND ug/kg 04/22/19 17:41 75-25-204/19/19 14:0320.7 1
Bromomethane ND ug/kg 04/22/19 17:41 74-83-904/19/19 14:0341.5 1
2-Butanone (MEK)ND ug/kg 04/22/19 17:41 78-93-304/19/19 14:034151
n-Butylbenzene ND ug/kg 04/22/19 17:41 104-51-804/19/19 14:0320.7 1
sec-Butylbenzene ND ug/kg 04/22/19 17:41 135-98-804/19/19 14:0320.7 1
tert-Butylbenzene ND ug/kg 04/22/19 17:41 98-06-604/19/19 14:0320.7 1
Carbon tetrachloride ND ug/kg 04/22/19 17:41 56-23-504/19/19 14:0320.7 1
Chlorobenzene ND ug/kg 04/22/19 17:41 108-90-704/19/19 14:0320.7 1
Chloroethane ND ug/kg 04/22/19 17:41 75-00-304/19/19 14:0341.5 1
Chloroform ND ug/kg 04/22/19 17:41 67-66-304/19/19 14:0320.7 1
Chloromethane ND ug/kg 04/22/19 17:41 74-87-304/19/19 14:0341.5 1
2-Chlorotoluene ND ug/kg 04/22/19 17:41 95-49-804/19/19 14:0320.7 1
4-Chlorotoluene ND ug/kg 04/22/19 17:41 106-43-404/19/19 14:0320.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/22/19 17:41 96-12-804/19/19 14:0320.7 1
Dibromochloromethane ND ug/kg 04/22/19 17:41 124-48-104/19/19 14:0320.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/22/19 17:41 106-93-404/19/19 14:0320.7 1
Dibromomethane ND ug/kg 04/22/19 17:41 74-95-304/19/19 14:0320.7 1
1,2-Dichlorobenzene ND ug/kg 04/22/19 17:41 95-50-104/19/19 14:0320.7 1
1,3-Dichlorobenzene ND ug/kg 04/22/19 17:41 541-73-104/19/19 14:0320.7 1
1,4-Dichlorobenzene ND ug/kg 04/22/19 17:41 106-46-704/19/19 14:0320.7 1
Dichlorodifluoromethane ND ug/kg 04/22/19 17:41 75-71-804/19/19 14:0341.5 1
1,1-Dichloroethane ND ug/kg 04/22/19 17:41 75-34-304/19/19 14:0320.7 1
1,2-Dichloroethane ND ug/kg 04/22/19 17:41 107-06-204/19/19 14:0320.7 1
1,1-Dichloroethene ND ug/kg 04/22/19 17:41 75-35-404/19/19 14:0320.7 1
cis-1,2-Dichloroethene ND ug/kg 04/22/19 17:41 156-59-204/19/19 14:0320.7 1
trans-1,2-Dichloroethene ND ug/kg 04/22/19 17:41 156-60-504/19/19 14:0320.7 1
1,2-Dichloropropane ND ug/kg 04/22/19 17:41 78-87-504/19/19 14:0320.7 1
1,3-Dichloropropane ND ug/kg 04/22/19 17:41 142-28-904/19/19 14:0320.7 1
2,2-Dichloropropane ND ug/kg 04/22/19 17:41 594-20-704/19/19 14:0320.7 1
1,1-Dichloropropene ND ug/kg 04/22/19 17:41 563-58-604/19/19 14:0320.7 1
cis-1,3-Dichloropropene ND ug/kg 04/22/19 17:41 10061-01-504/19/19 14:0320.7 1
trans-1,3-Dichloropropene ND ug/kg 04/22/19 17:41 10061-02-604/19/19 14:0320.7 1
Diisopropyl ether ND ug/kg 04/22/19 17:41 108-20-304/19/19 14:0320.7 1
Ethylbenzene ND ug/kg 04/22/19 17:41 100-41-404/19/19 14:0320.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/22/19 17:41 87-68-304/19/19 14:0320.7 1
2-Hexanone ND ug/kg 04/22/19 17:41 591-78-604/19/19 14:032071
Isopropylbenzene (Cumene)ND ug/kg 04/22/19 17:41 98-82-804/19/19 14:0320.7 1
p-Isopropyltoluene ND ug/kg 04/22/19 17:41 99-87-604/19/19 14:0320.7 1
Methylene Chloride ND ug/kg 04/22/19 17:41 75-09-204/19/19 14:0383.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/22/19 17:41 108-10-104/19/19 14:032071
Methyl-tert-butyl ether ND ug/kg 04/22/19 17:41 1634-04-404/19/19 14:0320.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-1D Lab ID:92425518005 Collected:04/12/19 14:30 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/22/19 17:41 91-20-304/19/19 14:0320.7 1
n-Propylbenzene ND ug/kg 04/22/19 17:41 103-65-104/19/19 14:0320.7 1
Styrene ND ug/kg 04/22/19 17:41 100-42-504/19/19 14:0320.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/22/19 17:41 630-20-604/19/19 14:0320.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/22/19 17:41 79-34-504/19/19 14:0320.7 1
Tetrachloroethene ND ug/kg 04/22/19 17:41 127-18-404/19/19 14:0320.7 1
Toluene ND ug/kg 04/22/19 17:41 108-88-304/19/19 14:0320.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/22/19 17:41 87-61-604/19/19 14:0320.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/22/19 17:41 120-82-104/19/19 14:0320.7 1
1,1,1-Trichloroethane ND ug/kg 04/22/19 17:41 71-55-604/19/19 14:0320.7 1
1,1,2-Trichloroethane ND ug/kg 04/22/19 17:41 79-00-504/19/19 14:0320.7 1
Trichloroethene ND ug/kg 04/22/19 17:41 79-01-604/19/19 14:0320.7 1
Trichlorofluoromethane ND ug/kg 04/22/19 17:41 75-69-404/19/19 14:0320.7 1
1,2,3-Trichloropropane ND ug/kg 04/22/19 17:41 96-18-404/19/19 14:0320.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/22/19 17:41 95-63-604/19/19 14:0320.7 1
1,3,5-Trimethylbenzene ND ug/kg 04/22/19 17:41 108-67-804/19/19 14:0320.7 1
Vinyl acetate ND ug/kg 04/22/19 17:41 108-05-404/19/19 14:032071
Vinyl chloride ND ug/kg 04/22/19 17:41 75-01-404/19/19 14:0341.5 1
Xylene (Total)ND ug/kg 04/22/19 17:41 1330-20-704/19/19 14:0341.5 1
m&p-Xylene ND ug/kg 04/22/19 17:41 179601-23-104/19/19 14:0341.5 1
o-Xylene ND ug/kg 04/22/19 17:41 95-47-604/19/19 14:0320.7 1
Surrogates
Toluene-d8 (S)95 %04/22/19 17:41 2037-26-504/19/19 14:0370-130 1
4-Bromofluorobenzene (S)81 %04/22/19 17:41 460-00-404/19/19 14:0370-130 1
1,2-Dichloroethane-d4 (S)104 %04/22/19 17:41 17060-07-004/19/19 14:0370-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 64.9 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2 Lab ID:92425518006 Collected:04/12/19 16:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 2.0 mg/kg 04/27/19 18:31 7440-38-204/25/19 17:251.5 1
Cadmium ND mg/kg 04/27/19 18:31 7440-43-904/25/19 17:250.15 1
Calcium 3490 mg/kg 04/27/19 18:31 7440-70-204/25/19 17:2515.2 1
Chromium 66.5 mg/kg 04/27/19 18:31 7440-47-304/25/19 17:250.76 1
Copper 88.9 mg/kg 04/27/19 18:31 7440-50-804/25/19 17:250.76 1
Lead 15.5 mg/kg 04/27/19 18:31 7439-92-104/25/19 17:250.76 1
Magnesium 13200 mg/kg 04/27/19 18:31 7439-95-404/25/19 17:2515.2 1
Molybdenum 3.0 mg/kg 04/27/19 18:31 7439-98-704/25/19 17:250.76 1
Nickel 33.8 mg/kg 04/27/19 18:31 7440-02-004/25/19 17:250.76 1
Selenium ND mg/kg 04/27/19 18:31 7782-49-204/25/19 17:251.5 1
Sodium ND mg/kg 04/27/19 18:31 7440-23-504/25/19 17:257621
Zinc 204 mg/kg 04/27/19 18:31 7440-66-604/25/19 17:251.5 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.040 mg/kg 04/23/19 13:35 7439-97-604/22/19 16:340.0054 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 04/17/19 13:13 83-32-904/16/19 12:348091
Acenaphthylene ND ug/kg 04/17/19 13:13 208-96-804/16/19 12:348091
Aniline ND ug/kg 04/17/19 13:13 62-53-304/16/19 12:348091
Anthracene ND ug/kg 04/17/19 13:13 120-12-704/16/19 12:348091
Benzo(a)anthracene ND ug/kg 04/17/19 13:13 56-55-304/16/19 12:348091
Benzo(a)pyrene ND ug/kg 04/17/19 13:13 50-32-804/16/19 12:348091
Benzo(b)fluoranthene ND ug/kg 04/17/19 13:13 205-99-204/16/19 12:348091
Benzo(g,h,i)perylene ND ug/kg 04/17/19 13:13 191-24-204/16/19 12:348091
Benzo(k)fluoranthene ND ug/kg 04/17/19 13:13 207-08-904/16/19 12:348091
Benzoic Acid ND ug/kg 04/17/19 13:13 65-85-004/16/19 12:3440401
Benzyl alcohol ND ug/kg 04/17/19 13:13 100-51-604/16/19 12:3416201
4-Bromophenylphenyl ether ND ug/kg 04/17/19 13:13 101-55-304/16/19 12:348091
Butylbenzylphthalate ND ug/kg 04/17/19 13:13 85-68-704/16/19 12:348091
4-Chloro-3-methylphenol ND ug/kg 04/17/19 13:13 59-50-704/16/19 12:3416201
4-Chloroaniline ND ug/kg 04/17/19 13:13 106-47-804/16/19 12:3440401
bis(2-Chloroethoxy)methane ND ug/kg 04/17/19 13:13 111-91-104/16/19 12:348091
bis(2-Chloroethyl) ether ND ug/kg 04/17/19 13:13 111-44-404/16/19 12:348091
2-Chloronaphthalene ND ug/kg 04/17/19 13:13 91-58-704/16/19 12:348091
2-Chlorophenol ND ug/kg 04/17/19 13:13 95-57-804/16/19 12:348091
4-Chlorophenylphenyl ether ND ug/kg 04/17/19 13:13 7005-72-304/16/19 12:348091
Chrysene ND ug/kg 04/17/19 13:13 218-01-904/16/19 12:348091
Dibenz(a,h)anthracene ND ug/kg 04/17/19 13:13 53-70-304/16/19 12:348091
Dibenzofuran ND ug/kg 04/17/19 13:13 132-64-904/16/19 12:348091
1,2-Dichlorobenzene ND ug/kg 04/17/19 13:13 95-50-104/16/19 12:348091
1,3-Dichlorobenzene ND ug/kg 04/17/19 13:13 541-73-104/16/19 12:348091
1,4-Dichlorobenzene ND ug/kg 04/17/19 13:13 106-46-704/16/19 12:348091
3,3'-Dichlorobenzidine ND ug/kg 04/17/19 13:13 91-94-104/16/19 12:3440401
2,4-Dichlorophenol ND ug/kg 04/17/19 13:13 120-83-204/16/19 12:348091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
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Page 15 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2 Lab ID:92425518006 Collected:04/12/19 16:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Diethylphthalate ND ug/kg 04/17/19 13:13 84-66-204/16/19 12:348091
2,4-Dimethylphenol ND ug/kg 04/17/19 13:13 105-67-904/16/19 12:348091
Dimethylphthalate ND ug/kg 04/17/19 13:13 131-11-304/16/19 12:348091
Di-n-butylphthalate ND ug/kg 04/17/19 13:13 84-74-204/16/19 12:348091
4,6-Dinitro-2-methylphenol ND ug/kg 04/17/19 13:13 534-52-104/16/19 12:3416201
2,4-Dinitrophenol ND ug/kg 04/17/19 13:13 51-28-504/16/19 12:3440401
2,4-Dinitrotoluene ND ug/kg 04/17/19 13:13 121-14-204/16/19 12:348091
2,6-Dinitrotoluene ND ug/kg 04/17/19 13:13 606-20-204/16/19 12:348091
Di-n-octylphthalate ND ug/kg 04/17/19 13:13 117-84-004/16/19 12:348091
bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/19 13:13 117-81-704/16/19 12:348091
Fluoranthene ND ug/kg 04/17/19 13:13 206-44-004/16/19 12:348091
Fluorene ND ug/kg 04/17/19 13:13 86-73-704/16/19 12:348091
Hexachloro-1,3-butadiene ND ug/kg 04/17/19 13:13 87-68-304/16/19 12:348091
Hexachlorobenzene ND ug/kg 04/17/19 13:13 118-74-104/16/19 12:348091
Hexachlorocyclopentadiene ND ug/kg 04/17/19 13:13 77-47-404/16/19 12:348091
Hexachloroethane ND ug/kg 04/17/19 13:13 67-72-104/16/19 12:348091
Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/19 13:13 193-39-504/16/19 12:348091
Isophorone ND ug/kg 04/17/19 13:13 78-59-104/16/19 12:348091
1-Methylnaphthalene ND ug/kg 04/17/19 13:13 90-12-004/16/19 12:348091
2-Methylnaphthalene ND ug/kg 04/17/19 13:13 91-57-604/16/19 12:348091
2-Methylphenol(o-Cresol)ND ug/kg 04/17/19 13:13 95-48-704/16/19 12:348091
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/19 13:13 15831-10-404/16/19 12:348091
Naphthalene ND ug/kg 04/17/19 13:13 91-20-304/16/19 12:348091
2-Nitroaniline ND ug/kg 04/17/19 13:13 88-74-404/16/19 12:3440401
3-Nitroaniline ND ug/kg 04/17/19 13:13 99-09-204/16/19 12:3440401
4-Nitroaniline ND ug/kg 04/17/19 13:13 100-01-604/16/19 12:3416201
Nitrobenzene ND ug/kg 04/17/19 13:13 98-95-304/16/19 12:348091
2-Nitrophenol ND ug/kg 04/17/19 13:13 88-75-504/16/19 12:348091
4-Nitrophenol ND ug/kg 04/17/19 13:13 100-02-704/16/19 12:3440401
N-Nitrosodimethylamine ND ug/kg 04/17/19 13:13 62-75-904/16/19 12:348091
N-Nitroso-di-n-propylamine ND ug/kg 04/17/19 13:13 621-64-704/16/19 12:348091
N-Nitrosodiphenylamine ND ug/kg 04/17/19 13:13 86-30-604/16/19 12:348091
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/19 13:13 108-60-104/16/19 12:348091
Pentachlorophenol ND ug/kg 04/17/19 13:13 87-86-504/16/19 12:3440401
Phenanthrene ND ug/kg 04/17/19 13:13 85-01-804/16/19 12:348091
Phenol ND ug/kg 04/17/19 13:13 108-95-204/16/19 12:348091
Pyrene ND ug/kg 04/17/19 13:13 129-00-004/16/19 12:348091
1,2,4-Trichlorobenzene ND ug/kg 04/17/19 13:13 120-82-104/16/19 12:348091
2,4,5-Trichlorophenol ND ug/kg 04/17/19 13:13 95-95-404/16/19 12:348091
2,4,6-Trichlorophenol ND ug/kg 04/17/19 13:13 88-06-204/16/19 12:348091
Surrogates
Nitrobenzene-d5 (S)57 %04/17/19 13:13 4165-60-004/16/19 12:3423-110 1
2-Fluorobiphenyl (S)54 %04/17/19 13:13 321-60-804/16/19 12:3430-110 1
Terphenyl-d14 (S)66 %04/17/19 13:13 1718-51-004/16/19 12:3428-110 1
Phenol-d6 (S)58 %04/17/19 13:13 13127-88-304/16/19 12:3422-110 1
2-Fluorophenol (S)58 %04/17/19 13:13 367-12-404/16/19 12:3413-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2 Lab ID:92425518006 Collected:04/12/19 16:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)72 %04/17/19 13:13 118-79-604/16/19 12:3427-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 59.5 %04/16/19 14:000.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 3400 mg/kg 04/20/19 00:45 7727-37-904/19/19 07:1091.4 1
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 04/16/19 01:50 H1,H204/15/19 23:479.7 1
Nitrogen, Nitrate ND mg/kg 04/16/19 01:50 14797-55-804/15/19 23:479.7 1
Nitrogen, Nitrite ND mg/kg 04/16/19 01:50 14797-65-0 H1,H204/15/19 23:479.7 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993365.1 Phosphorus, Total
Phosphorus 623 mg/kg 04/16/19 23:51 7723-14-004/16/19 18:359.3 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2A Lab ID:92425518008 Collected:04/12/19 15:45 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 434 ug/kg 04/19/19 23:51 67-64-104/19/19 13:002821
Benzene ND ug/kg 04/19/19 23:51 71-43-204/19/19 13:0014.1 1
Bromobenzene ND ug/kg 04/19/19 23:51 108-86-104/19/19 13:0014.1 1
Bromochloromethane ND ug/kg 04/19/19 23:51 74-97-504/19/19 13:0014.1 1
Bromodichloromethane ND ug/kg 04/19/19 23:51 75-27-404/19/19 13:0014.1 1
Bromoform ND ug/kg 04/19/19 23:51 75-25-204/19/19 13:0014.1 1
Bromomethane ND ug/kg 04/19/19 23:51 74-83-904/19/19 13:0028.2 1
2-Butanone (MEK)ND ug/kg 04/19/19 23:51 78-93-304/19/19 13:002821
n-Butylbenzene ND ug/kg 04/19/19 23:51 104-51-804/19/19 13:0014.1 1
sec-Butylbenzene ND ug/kg 04/19/19 23:51 135-98-804/19/19 13:0014.1 1
tert-Butylbenzene ND ug/kg 04/19/19 23:51 98-06-604/19/19 13:0014.1 1
Carbon tetrachloride ND ug/kg 04/19/19 23:51 56-23-504/19/19 13:0014.1 1
Chlorobenzene ND ug/kg 04/19/19 23:51 108-90-704/19/19 13:0014.1 1
Chloroethane ND ug/kg 04/19/19 23:51 75-00-304/19/19 13:0028.2 1
Chloroform ND ug/kg 04/19/19 23:51 67-66-304/19/19 13:0014.1 1
Chloromethane ND ug/kg 04/19/19 23:51 74-87-304/19/19 13:0028.2 1
2-Chlorotoluene ND ug/kg 04/19/19 23:51 95-49-804/19/19 13:0014.1 1
4-Chlorotoluene ND ug/kg 04/19/19 23:51 106-43-404/19/19 13:0014.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/19/19 23:51 96-12-804/19/19 13:0014.1 1
Dibromochloromethane ND ug/kg 04/19/19 23:51 124-48-104/19/19 13:0014.1 1
1,2-Dibromoethane (EDB)ND ug/kg 04/19/19 23:51 106-93-404/19/19 13:0014.1 1
Dibromomethane ND ug/kg 04/19/19 23:51 74-95-304/19/19 13:0014.1 1
1,2-Dichlorobenzene ND ug/kg 04/19/19 23:51 95-50-104/19/19 13:0014.1 1
1,3-Dichlorobenzene ND ug/kg 04/19/19 23:51 541-73-104/19/19 13:0014.1 1
1,4-Dichlorobenzene ND ug/kg 04/19/19 23:51 106-46-704/19/19 13:0014.1 1
Dichlorodifluoromethane ND ug/kg 04/19/19 23:51 75-71-804/19/19 13:0028.2 1
1,1-Dichloroethane ND ug/kg 04/19/19 23:51 75-34-304/19/19 13:0014.1 1
1,2-Dichloroethane ND ug/kg 04/19/19 23:51 107-06-204/19/19 13:0014.1 1
1,1-Dichloroethene ND ug/kg 04/19/19 23:51 75-35-404/19/19 13:0014.1 1
cis-1,2-Dichloroethene ND ug/kg 04/19/19 23:51 156-59-204/19/19 13:0014.1 1
trans-1,2-Dichloroethene ND ug/kg 04/19/19 23:51 156-60-504/19/19 13:0014.1 1
1,2-Dichloropropane ND ug/kg 04/19/19 23:51 78-87-504/19/19 13:0014.1 1
1,3-Dichloropropane ND ug/kg 04/19/19 23:51 142-28-904/19/19 13:0014.1 1
2,2-Dichloropropane ND ug/kg 04/19/19 23:51 594-20-704/19/19 13:0014.1 1
1,1-Dichloropropene ND ug/kg 04/19/19 23:51 563-58-604/19/19 13:0014.1 1
cis-1,3-Dichloropropene ND ug/kg 04/19/19 23:51 10061-01-504/19/19 13:0014.1 1
trans-1,3-Dichloropropene ND ug/kg 04/19/19 23:51 10061-02-604/19/19 13:0014.1 1
Diisopropyl ether ND ug/kg 04/19/19 23:51 108-20-304/19/19 13:0014.1 1
Ethylbenzene ND ug/kg 04/19/19 23:51 100-41-404/19/19 13:0014.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/19/19 23:51 87-68-304/19/19 13:0014.1 1
2-Hexanone ND ug/kg 04/19/19 23:51 591-78-604/19/19 13:001411
Isopropylbenzene (Cumene)ND ug/kg 04/19/19 23:51 98-82-804/19/19 13:0014.1 1
p-Isopropyltoluene ND ug/kg 04/19/19 23:51 99-87-604/19/19 13:0014.1 1
Methylene Chloride ND ug/kg 04/19/19 23:51 75-09-204/19/19 13:0056.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/19 23:51 108-10-104/19/19 13:001411
Methyl-tert-butyl ether ND ug/kg 04/19/19 23:51 1634-04-404/19/19 13:0014.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2A Lab ID:92425518008 Collected:04/12/19 15:45 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/19/19 23:51 91-20-304/19/19 13:0014.1 1
n-Propylbenzene ND ug/kg 04/19/19 23:51 103-65-104/19/19 13:0014.1 1
Styrene ND ug/kg 04/19/19 23:51 100-42-504/19/19 13:0014.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/19/19 23:51 630-20-604/19/19 13:0014.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/19/19 23:51 79-34-504/19/19 13:0014.1 1
Tetrachloroethene ND ug/kg 04/19/19 23:51 127-18-404/19/19 13:0014.1 1
Toluene ND ug/kg 04/19/19 23:51 108-88-304/19/19 13:0014.1 1
1,2,3-Trichlorobenzene ND ug/kg 04/19/19 23:51 87-61-604/19/19 13:0014.1 1
1,2,4-Trichlorobenzene ND ug/kg 04/19/19 23:51 120-82-104/19/19 13:0014.1 1
1,1,1-Trichloroethane ND ug/kg 04/19/19 23:51 71-55-604/19/19 13:0014.1 1
1,1,2-Trichloroethane ND ug/kg 04/19/19 23:51 79-00-504/19/19 13:0014.1 1
Trichloroethene ND ug/kg 04/19/19 23:51 79-01-604/19/19 13:0014.1 1
Trichlorofluoromethane ND ug/kg 04/19/19 23:51 75-69-404/19/19 13:0014.1 1
1,2,3-Trichloropropane ND ug/kg 04/19/19 23:51 96-18-404/19/19 13:0014.1 1
1,2,4-Trimethylbenzene ND ug/kg 04/19/19 23:51 95-63-604/19/19 13:0014.1 1
1,3,5-Trimethylbenzene ND ug/kg 04/19/19 23:51 108-67-804/19/19 13:0014.1 1
Vinyl acetate ND ug/kg 04/19/19 23:51 108-05-404/19/19 13:001411
Vinyl chloride ND ug/kg 04/19/19 23:51 75-01-404/19/19 13:0028.2 1
Xylene (Total)ND ug/kg 04/19/19 23:51 1330-20-704/19/19 13:0028.2 1
m&p-Xylene ND ug/kg 04/19/19 23:51 179601-23-104/19/19 13:0028.2 1
o-Xylene ND ug/kg 04/19/19 23:51 95-47-604/19/19 13:0014.1 1
Surrogates
Toluene-d8 (S)94 %04/19/19 23:51 2037-26-504/19/19 13:0070-130 1
4-Bromofluorobenzene (S)81 %04/19/19 23:51 460-00-404/19/19 13:0070-130 1
1,2-Dichloroethane-d4 (S)101 %04/19/19 23:51 17060-07-004/19/19 13:0070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 59.3 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2B Lab ID:92425518009 Collected:04/12/19 15:50 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 04/22/19 18:31 67-64-104/19/19 14:0310201
Benzene ND ug/kg 04/22/19 18:31 71-43-204/19/19 14:0351.0 1
Bromobenzene ND ug/kg 04/22/19 18:31 108-86-104/19/19 14:0351.0 1
Bromochloromethane ND ug/kg 04/22/19 18:31 74-97-504/19/19 14:0351.0 1
Bromodichloromethane ND ug/kg 04/22/19 18:31 75-27-404/19/19 14:0351.0 1
Bromoform ND ug/kg 04/22/19 18:31 75-25-204/19/19 14:0351.0 1
Bromomethane ND ug/kg 04/22/19 18:31 74-83-904/19/19 14:031021
2-Butanone (MEK)ND ug/kg 04/22/19 18:31 78-93-304/19/19 14:0310201
n-Butylbenzene ND ug/kg 04/22/19 18:31 104-51-804/19/19 14:0351.0 1
sec-Butylbenzene ND ug/kg 04/22/19 18:31 135-98-804/19/19 14:0351.0 1
tert-Butylbenzene ND ug/kg 04/22/19 18:31 98-06-604/19/19 14:0351.0 1
Carbon tetrachloride ND ug/kg 04/22/19 18:31 56-23-504/19/19 14:0351.0 1
Chlorobenzene ND ug/kg 04/22/19 18:31 108-90-704/19/19 14:0351.0 1
Chloroethane ND ug/kg 04/22/19 18:31 75-00-304/19/19 14:031021
Chloroform ND ug/kg 04/22/19 18:31 67-66-304/19/19 14:0351.0 1
Chloromethane ND ug/kg 04/22/19 18:31 74-87-304/19/19 14:031021
2-Chlorotoluene ND ug/kg 04/22/19 18:31 95-49-804/19/19 14:0351.0 1
4-Chlorotoluene ND ug/kg 04/22/19 18:31 106-43-404/19/19 14:0351.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/22/19 18:31 96-12-804/19/19 14:0351.0 1
Dibromochloromethane ND ug/kg 04/22/19 18:31 124-48-104/19/19 14:0351.0 1
1,2-Dibromoethane (EDB)ND ug/kg 04/22/19 18:31 106-93-404/19/19 14:0351.0 1
Dibromomethane ND ug/kg 04/22/19 18:31 74-95-304/19/19 14:0351.0 1
1,2-Dichlorobenzene ND ug/kg 04/22/19 18:31 95-50-104/19/19 14:0351.0 1
1,3-Dichlorobenzene ND ug/kg 04/22/19 18:31 541-73-104/19/19 14:0351.0 1
1,4-Dichlorobenzene ND ug/kg 04/22/19 18:31 106-46-704/19/19 14:0351.0 1
Dichlorodifluoromethane ND ug/kg 04/22/19 18:31 75-71-804/19/19 14:031021
1,1-Dichloroethane ND ug/kg 04/22/19 18:31 75-34-304/19/19 14:0351.0 1
1,2-Dichloroethane ND ug/kg 04/22/19 18:31 107-06-204/19/19 14:0351.0 1
1,1-Dichloroethene ND ug/kg 04/22/19 18:31 75-35-404/19/19 14:0351.0 1
cis-1,2-Dichloroethene ND ug/kg 04/22/19 18:31 156-59-204/19/19 14:0351.0 1
trans-1,2-Dichloroethene ND ug/kg 04/22/19 18:31 156-60-504/19/19 14:0351.0 1
1,2-Dichloropropane ND ug/kg 04/22/19 18:31 78-87-504/19/19 14:0351.0 1
1,3-Dichloropropane ND ug/kg 04/22/19 18:31 142-28-904/19/19 14:0351.0 1
2,2-Dichloropropane ND ug/kg 04/22/19 18:31 594-20-704/19/19 14:0351.0 1
1,1-Dichloropropene ND ug/kg 04/22/19 18:31 563-58-604/19/19 14:0351.0 1
cis-1,3-Dichloropropene ND ug/kg 04/22/19 18:31 10061-01-504/19/19 14:0351.0 1
trans-1,3-Dichloropropene ND ug/kg 04/22/19 18:31 10061-02-604/19/19 14:0351.0 1
Diisopropyl ether ND ug/kg 04/22/19 18:31 108-20-304/19/19 14:0351.0 1
Ethylbenzene ND ug/kg 04/22/19 18:31 100-41-404/19/19 14:0351.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/22/19 18:31 87-68-304/19/19 14:0351.0 1
2-Hexanone ND ug/kg 04/22/19 18:31 591-78-604/19/19 14:035101
Isopropylbenzene (Cumene)ND ug/kg 04/22/19 18:31 98-82-804/19/19 14:0351.0 1
p-Isopropyltoluene ND ug/kg 04/22/19 18:31 99-87-604/19/19 14:0351.0 1
Methylene Chloride ND ug/kg 04/22/19 18:31 75-09-204/19/19 14:032041
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/22/19 18:31 108-10-104/19/19 14:035101
Methyl-tert-butyl ether ND ug/kg 04/22/19 18:31 1634-04-404/19/19 14:0351.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2B Lab ID:92425518009 Collected:04/12/19 15:50 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/22/19 18:31 91-20-304/19/19 14:0351.0 1
n-Propylbenzene ND ug/kg 04/22/19 18:31 103-65-104/19/19 14:0351.0 1
Styrene ND ug/kg 04/22/19 18:31 100-42-504/19/19 14:0351.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/22/19 18:31 630-20-604/19/19 14:0351.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/22/19 18:31 79-34-504/19/19 14:0351.0 1
Tetrachloroethene ND ug/kg 04/22/19 18:31 127-18-404/19/19 14:0351.0 1
Toluene ND ug/kg 04/22/19 18:31 108-88-304/19/19 14:0351.0 1
1,2,3-Trichlorobenzene ND ug/kg 04/22/19 18:31 87-61-604/19/19 14:0351.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/22/19 18:31 120-82-104/19/19 14:0351.0 1
1,1,1-Trichloroethane ND ug/kg 04/22/19 18:31 71-55-604/19/19 14:0351.0 1
1,1,2-Trichloroethane ND ug/kg 04/22/19 18:31 79-00-504/19/19 14:0351.0 1
Trichloroethene ND ug/kg 04/22/19 18:31 79-01-604/19/19 14:0351.0 1
Trichlorofluoromethane ND ug/kg 04/22/19 18:31 75-69-404/19/19 14:0351.0 1
1,2,3-Trichloropropane ND ug/kg 04/22/19 18:31 96-18-404/19/19 14:0351.0 1
1,2,4-Trimethylbenzene ND ug/kg 04/22/19 18:31 95-63-604/19/19 14:0351.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/22/19 18:31 108-67-804/19/19 14:0351.0 1
Vinyl acetate ND ug/kg 04/22/19 18:31 108-05-404/19/19 14:035101
Vinyl chloride ND ug/kg 04/22/19 18:31 75-01-404/19/19 14:031021
Xylene (Total)ND ug/kg 04/22/19 18:31 1330-20-704/19/19 14:031021
m&p-Xylene ND ug/kg 04/22/19 18:31 179601-23-104/19/19 14:031021
o-Xylene ND ug/kg 04/22/19 18:31 95-47-604/19/19 14:0351.0 1
Surrogates
Toluene-d8 (S)97 %04/22/19 18:31 2037-26-504/19/19 14:0370-130 1
4-Bromofluorobenzene (S)93 %04/22/19 18:31 460-00-404/19/19 14:0370-130 1
1,2-Dichloroethane-d4 (S)104 %04/22/19 18:31 17060-07-004/19/19 14:0370-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 65.7 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2C Lab ID:92425518010 Collected:04/12/19 15:40 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 04/20/19 01:31 67-64-104/19/19 14:03838025
Benzene ND ug/kg 04/20/19 01:31 71-43-204/19/19 14:0341925
Bromobenzene ND ug/kg 04/20/19 01:31 108-86-104/19/19 14:0341925
Bromochloromethane ND ug/kg 04/20/19 01:31 74-97-504/19/19 14:0341925
Bromodichloromethane ND ug/kg 04/20/19 01:31 75-27-404/19/19 14:0341925
Bromoform ND ug/kg 04/20/19 01:31 75-25-204/19/19 14:0341925
Bromomethane ND ug/kg 04/20/19 01:31 74-83-904/19/19 14:0383825
2-Butanone (MEK)ND ug/kg 04/20/19 01:31 78-93-304/19/19 14:03838025
n-Butylbenzene ND ug/kg 04/20/19 01:31 104-51-804/19/19 14:0341925
sec-Butylbenzene ND ug/kg 04/20/19 01:31 135-98-804/19/19 14:0341925
tert-Butylbenzene ND ug/kg 04/20/19 01:31 98-06-604/19/19 14:0341925
Carbon tetrachloride ND ug/kg 04/20/19 01:31 56-23-504/19/19 14:0341925
Chlorobenzene ND ug/kg 04/20/19 01:31 108-90-704/19/19 14:0341925
Chloroethane ND ug/kg 04/20/19 01:31 75-00-304/19/19 14:0383825
Chloroform ND ug/kg 04/20/19 01:31 67-66-304/19/19 14:0341925
Chloromethane ND ug/kg 04/20/19 01:31 74-87-304/19/19 14:0383825
2-Chlorotoluene ND ug/kg 04/20/19 01:31 95-49-804/19/19 14:0341925
4-Chlorotoluene ND ug/kg 04/20/19 01:31 106-43-404/19/19 14:0341925
1,2-Dibromo-3-chloropropane ND ug/kg 04/20/19 01:31 96-12-804/19/19 14:0341925
Dibromochloromethane ND ug/kg 04/20/19 01:31 124-48-104/19/19 14:0341925
1,2-Dibromoethane (EDB)ND ug/kg 04/20/19 01:31 106-93-404/19/19 14:0341925
Dibromomethane ND ug/kg 04/20/19 01:31 74-95-304/19/19 14:0341925
1,2-Dichlorobenzene ND ug/kg 04/20/19 01:31 95-50-104/19/19 14:0341925
1,3-Dichlorobenzene ND ug/kg 04/20/19 01:31 541-73-104/19/19 14:0341925
1,4-Dichlorobenzene ND ug/kg 04/20/19 01:31 106-46-704/19/19 14:0341925
Dichlorodifluoromethane ND ug/kg 04/20/19 01:31 75-71-804/19/19 14:0383825
1,1-Dichloroethane ND ug/kg 04/20/19 01:31 75-34-304/19/19 14:0341925
1,2-Dichloroethane ND ug/kg 04/20/19 01:31 107-06-204/19/19 14:0341925
1,1-Dichloroethene ND ug/kg 04/20/19 01:31 75-35-404/19/19 14:0341925
cis-1,2-Dichloroethene ND ug/kg 04/20/19 01:31 156-59-204/19/19 14:0341925
trans-1,2-Dichloroethene ND ug/kg 04/20/19 01:31 156-60-504/19/19 14:0341925
1,2-Dichloropropane ND ug/kg 04/20/19 01:31 78-87-504/19/19 14:0341925
1,3-Dichloropropane ND ug/kg 04/20/19 01:31 142-28-904/19/19 14:0341925
2,2-Dichloropropane ND ug/kg 04/20/19 01:31 594-20-704/19/19 14:0341925
1,1-Dichloropropene ND ug/kg 04/20/19 01:31 563-58-604/19/19 14:0341925
cis-1,3-Dichloropropene ND ug/kg 04/20/19 01:31 10061-01-504/19/19 14:0341925
trans-1,3-Dichloropropene ND ug/kg 04/20/19 01:31 10061-02-604/19/19 14:0341925
Diisopropyl ether ND ug/kg 04/20/19 01:31 108-20-304/19/19 14:0341925
Ethylbenzene ND ug/kg 04/20/19 01:31 100-41-404/19/19 14:0341925
Hexachloro-1,3-butadiene ND ug/kg 04/20/19 01:31 87-68-304/19/19 14:0341925
2-Hexanone ND ug/kg 04/20/19 01:31 591-78-604/19/19 14:03419025
Isopropylbenzene (Cumene)ND ug/kg 04/20/19 01:31 98-82-804/19/19 14:0341925
p-Isopropyltoluene ND ug/kg 04/20/19 01:31 99-87-604/19/19 14:0341925
Methylene Chloride ND ug/kg 04/20/19 01:31 75-09-204/19/19 14:03168025
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/20/19 01:31 108-10-104/19/19 14:03419025
Methyl-tert-butyl ether ND ug/kg 04/20/19 01:31 1634-04-404/19/19 14:0341925
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2C Lab ID:92425518010 Collected:04/12/19 15:40 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/20/19 01:31 91-20-304/19/19 14:0341925
n-Propylbenzene ND ug/kg 04/20/19 01:31 103-65-104/19/19 14:0341925
Styrene ND ug/kg 04/20/19 01:31 100-42-504/19/19 14:0341925
1,1,1,2-Tetrachloroethane ND ug/kg 04/20/19 01:31 630-20-604/19/19 14:0341925
1,1,2,2-Tetrachloroethane ND ug/kg 04/20/19 01:31 79-34-504/19/19 14:0341925
Tetrachloroethene ND ug/kg 04/20/19 01:31 127-18-404/19/19 14:0341925
Toluene ND ug/kg 04/20/19 01:31 108-88-304/19/19 14:0341925
1,2,3-Trichlorobenzene ND ug/kg 04/20/19 01:31 87-61-604/19/19 14:0341925
1,2,4-Trichlorobenzene ND ug/kg 04/20/19 01:31 120-82-104/19/19 14:0341925
1,1,1-Trichloroethane ND ug/kg 04/20/19 01:31 71-55-604/19/19 14:0341925
1,1,2-Trichloroethane ND ug/kg 04/20/19 01:31 79-00-504/19/19 14:0341925
Trichloroethene ND ug/kg 04/20/19 01:31 79-01-604/19/19 14:0341925
Trichlorofluoromethane ND ug/kg 04/20/19 01:31 75-69-404/19/19 14:0341925
1,2,3-Trichloropropane ND ug/kg 04/20/19 01:31 96-18-404/19/19 14:0341925
1,2,4-Trimethylbenzene ND ug/kg 04/20/19 01:31 95-63-604/19/19 14:0341925
1,3,5-Trimethylbenzene ND ug/kg 04/20/19 01:31 108-67-804/19/19 14:0341925
Vinyl acetate ND ug/kg 04/20/19 01:31 108-05-404/19/19 14:03419025
Vinyl chloride ND ug/kg 04/20/19 01:31 75-01-404/19/19 14:0383825
Xylene (Total)ND ug/kg 04/20/19 01:31 1330-20-704/19/19 14:0383825
m&p-Xylene ND ug/kg 04/20/19 01:31 179601-23-104/19/19 14:0383825
o-Xylene ND ug/kg 04/20/19 01:31 95-47-604/19/19 14:0341925
Surrogates
Toluene-d8 (S)97 %04/20/19 01:31 2037-26-504/19/19 14:0370-130 25
4-Bromofluorobenzene (S)99 %04/20/19 01:31 460-00-404/19/19 14:0370-130 25
1,2-Dichloroethane-d4 (S)104 %04/20/19 01:31 17060-07-004/19/19 14:0370-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 59.9 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2D Lab ID:92425518011 Collected:04/12/19 15:15 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 04/22/19 19:21 67-64-104/19/19 14:034141
Benzene ND ug/kg 04/22/19 19:21 71-43-204/19/19 14:0320.7 1
Bromobenzene ND ug/kg 04/22/19 19:21 108-86-104/19/19 14:0320.7 1
Bromochloromethane ND ug/kg 04/22/19 19:21 74-97-504/19/19 14:0320.7 1
Bromodichloromethane ND ug/kg 04/22/19 19:21 75-27-404/19/19 14:0320.7 1
Bromoform ND ug/kg 04/22/19 19:21 75-25-204/19/19 14:0320.7 1
Bromomethane ND ug/kg 04/22/19 19:21 74-83-904/19/19 14:0341.4 1
2-Butanone (MEK)ND ug/kg 04/22/19 19:21 78-93-304/19/19 14:034141
n-Butylbenzene ND ug/kg 04/22/19 19:21 104-51-804/19/19 14:0320.7 1
sec-Butylbenzene ND ug/kg 04/22/19 19:21 135-98-804/19/19 14:0320.7 1
tert-Butylbenzene ND ug/kg 04/22/19 19:21 98-06-604/19/19 14:0320.7 1
Carbon tetrachloride ND ug/kg 04/22/19 19:21 56-23-504/19/19 14:0320.7 1
Chlorobenzene ND ug/kg 04/22/19 19:21 108-90-704/19/19 14:0320.7 1
Chloroethane ND ug/kg 04/22/19 19:21 75-00-304/19/19 14:0341.4 1
Chloroform ND ug/kg 04/22/19 19:21 67-66-304/19/19 14:0320.7 1
Chloromethane ND ug/kg 04/22/19 19:21 74-87-304/19/19 14:0341.4 1
2-Chlorotoluene ND ug/kg 04/22/19 19:21 95-49-804/19/19 14:0320.7 1
4-Chlorotoluene ND ug/kg 04/22/19 19:21 106-43-404/19/19 14:0320.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/22/19 19:21 96-12-804/19/19 14:0320.7 1
Dibromochloromethane ND ug/kg 04/22/19 19:21 124-48-104/19/19 14:0320.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/22/19 19:21 106-93-404/19/19 14:0320.7 1
Dibromomethane ND ug/kg 04/22/19 19:21 74-95-304/19/19 14:0320.7 1
1,2-Dichlorobenzene ND ug/kg 04/22/19 19:21 95-50-104/19/19 14:0320.7 1
1,3-Dichlorobenzene ND ug/kg 04/22/19 19:21 541-73-104/19/19 14:0320.7 1
1,4-Dichlorobenzene ND ug/kg 04/22/19 19:21 106-46-704/19/19 14:0320.7 1
Dichlorodifluoromethane ND ug/kg 04/22/19 19:21 75-71-804/19/19 14:0341.4 1
1,1-Dichloroethane ND ug/kg 04/22/19 19:21 75-34-304/19/19 14:0320.7 1
1,2-Dichloroethane ND ug/kg 04/22/19 19:21 107-06-204/19/19 14:0320.7 1
1,1-Dichloroethene ND ug/kg 04/22/19 19:21 75-35-404/19/19 14:0320.7 1
cis-1,2-Dichloroethene ND ug/kg 04/22/19 19:21 156-59-204/19/19 14:0320.7 1
trans-1,2-Dichloroethene ND ug/kg 04/22/19 19:21 156-60-504/19/19 14:0320.7 1
1,2-Dichloropropane ND ug/kg 04/22/19 19:21 78-87-504/19/19 14:0320.7 1
1,3-Dichloropropane ND ug/kg 04/22/19 19:21 142-28-904/19/19 14:0320.7 1
2,2-Dichloropropane ND ug/kg 04/22/19 19:21 594-20-704/19/19 14:0320.7 1
1,1-Dichloropropene ND ug/kg 04/22/19 19:21 563-58-604/19/19 14:0320.7 1
cis-1,3-Dichloropropene ND ug/kg 04/22/19 19:21 10061-01-504/19/19 14:0320.7 1
trans-1,3-Dichloropropene ND ug/kg 04/22/19 19:21 10061-02-604/19/19 14:0320.7 1
Diisopropyl ether ND ug/kg 04/22/19 19:21 108-20-304/19/19 14:0320.7 1
Ethylbenzene ND ug/kg 04/22/19 19:21 100-41-404/19/19 14:0320.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/22/19 19:21 87-68-304/19/19 14:0320.7 1
2-Hexanone ND ug/kg 04/22/19 19:21 591-78-604/19/19 14:032071
Isopropylbenzene (Cumene)ND ug/kg 04/22/19 19:21 98-82-804/19/19 14:0320.7 1
p-Isopropyltoluene ND ug/kg 04/22/19 19:21 99-87-604/19/19 14:0320.7 1
Methylene Chloride ND ug/kg 04/22/19 19:21 75-09-204/19/19 14:0382.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/22/19 19:21 108-10-104/19/19 14:032071
Methyl-tert-butyl ether ND ug/kg 04/22/19 19:21 1634-04-404/19/19 14:0320.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92425518
Powell 4/12
Sample:C-2D Lab ID:92425518011 Collected:04/12/19 15:15 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 04/22/19 19:21 91-20-304/19/19 14:0320.7 1
n-Propylbenzene ND ug/kg 04/22/19 19:21 103-65-104/19/19 14:0320.7 1
Styrene ND ug/kg 04/22/19 19:21 100-42-504/19/19 14:0320.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/22/19 19:21 630-20-604/19/19 14:0320.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/22/19 19:21 79-34-504/19/19 14:0320.7 1
Tetrachloroethene ND ug/kg 04/22/19 19:21 127-18-404/19/19 14:0320.7 1
Toluene ND ug/kg 04/22/19 19:21 108-88-304/19/19 14:0320.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/22/19 19:21 87-61-604/19/19 14:0320.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/22/19 19:21 120-82-104/19/19 14:0320.7 1
1,1,1-Trichloroethane ND ug/kg 04/22/19 19:21 71-55-604/19/19 14:0320.7 1
1,1,2-Trichloroethane ND ug/kg 04/22/19 19:21 79-00-504/19/19 14:0320.7 1
Trichloroethene ND ug/kg 04/22/19 19:21 79-01-604/19/19 14:0320.7 1
Trichlorofluoromethane ND ug/kg 04/22/19 19:21 75-69-404/19/19 14:0320.7 1
1,2,3-Trichloropropane ND ug/kg 04/22/19 19:21 96-18-404/19/19 14:0320.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/22/19 19:21 95-63-604/19/19 14:0320.7 1
1,3,5-Trimethylbenzene ND ug/kg 04/22/19 19:21 108-67-804/19/19 14:0320.7 1
Vinyl acetate ND ug/kg 04/22/19 19:21 108-05-404/19/19 14:032071
Vinyl chloride ND ug/kg 04/22/19 19:21 75-01-404/19/19 14:0341.4 1
Xylene (Total)ND ug/kg 04/22/19 19:21 1330-20-704/19/19 14:0341.4 1
m&p-Xylene ND ug/kg 04/22/19 19:21 179601-23-104/19/19 14:0341.4 1
o-Xylene ND ug/kg 04/22/19 19:21 95-47-604/19/19 14:0320.7 1
Surrogates
Toluene-d8 (S)99 %04/22/19 19:21 2037-26-504/19/19 14:0370-130 1
4-Bromofluorobenzene (S)96 %04/22/19 19:21 460-00-404/19/19 14:0370-130 1
1,2-Dichloroethane-d4 (S)102 %04/22/19 19:21 17060-07-004/19/19 14:0370-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 63.9 %04/16/19 14:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
470793
EPA 7471B
EPA 7471B
7471 Mercury
Associated Lab Samples:92425518001, 92425518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2555602
Associated Lab Samples:92425518001, 92425518006
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 04/23/19 12:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2555603LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0800.083 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2555604MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92424988014
2555605
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg 0.078 96 75-12596 140.0670.0089 0.084 0.073
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
471202
EPA 3050B
EPA 6010D
6010 MET
Associated Lab Samples:92425518001, 92425518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2557031
Associated Lab Samples:92425518001, 92425518006
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 04/27/19 18:01
Cadmium mg/kg ND 0.10 04/27/19 18:01
Calcium mg/kg ND 10.0 04/27/19 18:01
Chromium mg/kg ND 0.50 04/27/19 18:01
Copper mg/kg ND 0.50 04/27/19 18:01
Lead mg/kg ND 0.50 04/27/19 18:01
Magnesium mg/kg ND 10.0 04/27/19 18:01
Molybdenum mg/kg ND 0.50 04/27/19 18:01
Nickel mg/kg ND 0.50 04/27/19 18:01
Selenium mg/kg ND 1.0 04/27/19 18:01
Sodium mg/kg ND 500 04/27/19 18:01
Zinc mg/kg ND 1.0 04/27/19 18:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2557032LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 43.250 86 80-120
Cadmium mg/kg 44.850 90 80-120
Calcium mg/kg 472500 94 80-120
Chromium mg/kg 47.750 95 80-120
Copper mg/kg 47.750 95 80-120
Lead mg/kg 46.150 92 80-120
Magnesium mg/kg 462500 92 80-120
Molybdenum mg/kg 45.850 92 80-120
Nickel mg/kg 46.150 92 80-120
Selenium mg/kg 42.050 84 80-120
Sodium mg/kg 477J500 95 80-120
Zinc mg/kg 44.350 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2557033MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92425518001
2557034
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg M180.8 64 75-12567 1591.33.7 55.9 65.0
Cadmium mg/kg M180.8 70 75-12573 1691.3ND 56.6 66.6
Calcium mg/kg M18086775-125121 6913786084008970
Chromium mg/kg 80.8 75 75-12585 1391.359.9 121 137
Copper mg/kg 80.8 89 75-125102 1291.396.4 169 189
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2557033MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92425518001
2557034
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead mg/kg M180.8 70 75-12574 1491.315.8 72.2 83.1
Magnesium mg/kg M180814875-125268 9913121001330014500
Molybdenum mg/kg M180.8 67 75-12569 1491.33.1 57.3 66.1
Nickel mg/kg M180.8 72 75-12578 1491.332.1 90.1 103
Selenium mg/kg M180.8 62 75-12564 1691.3ND 50.1 58.8
Sodium mg/kg 808 84 75-12587 13913ND868989
Zinc mg/kg M180.8 69 75-12589 891.3264 320 346
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
470498
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010,
92425518011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2554406
Associated Lab Samples:92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010,
92425518011
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/19/19 20:05
1,1,1-Trichloroethane ug/kg ND 5.0 04/19/19 20:05
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/19/19 20:05
1,1,2-Trichloroethane ug/kg ND 5.0 04/19/19 20:05
1,1-Dichloroethane ug/kg ND 5.0 04/19/19 20:05
1,1-Dichloroethene ug/kg ND 5.0 04/19/19 20:05
1,1-Dichloropropene ug/kg ND 5.0 04/19/19 20:05
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/19/19 20:05
1,2,3-Trichloropropane ug/kg ND 5.0 04/19/19 20:05
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/19/19 20:05
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/19/19 20:05
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/19/19 20:05
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/19/19 20:05
1,2-Dichlorobenzene ug/kg ND 5.0 04/19/19 20:05
1,2-Dichloroethane ug/kg ND 5.0 04/19/19 20:05
1,2-Dichloropropane ug/kg ND 5.0 04/19/19 20:05
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/19/19 20:05
1,3-Dichlorobenzene ug/kg ND 5.0 04/19/19 20:05
1,3-Dichloropropane ug/kg ND 5.0 04/19/19 20:05
1,4-Dichlorobenzene ug/kg ND 5.0 04/19/19 20:05
2,2-Dichloropropane ug/kg ND 5.0 04/19/19 20:05
2-Butanone (MEK)ug/kg ND 100 04/19/19 20:05
2-Chlorotoluene ug/kg ND 5.0 04/19/19 20:05
2-Hexanone ug/kg ND 50.0 04/19/19 20:05
4-Chlorotoluene ug/kg ND 5.0 04/19/19 20:05
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/19/19 20:05
Acetone ug/kg ND 100 04/19/19 20:05
Benzene ug/kg ND 5.0 04/19/19 20:05
Bromobenzene ug/kg ND 5.0 04/19/19 20:05
Bromochloromethane ug/kg ND 5.0 04/19/19 20:05
Bromodichloromethane ug/kg ND 5.0 04/19/19 20:05
Bromoform ug/kg ND 5.0 04/19/19 20:05
Bromomethane ug/kg ND 10.0 04/19/19 20:05
Carbon tetrachloride ug/kg ND 5.0 04/19/19 20:05
Chlorobenzene ug/kg ND 5.0 04/19/19 20:05
Chloroethane ug/kg ND 10.0 04/19/19 20:05
Chloroform ug/kg ND 5.0 04/19/19 20:05
Chloromethane ug/kg ND 10.0 04/19/19 20:05
cis-1,2-Dichloroethene ug/kg ND 5.0 04/19/19 20:05
cis-1,3-Dichloropropene ug/kg ND 5.0 04/19/19 20:05
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2554406
Associated Lab Samples:92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010,
92425518011
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 04/19/19 20:05
Dibromomethane ug/kg ND 5.0 04/19/19 20:05
Dichlorodifluoromethane ug/kg ND 10.0 04/19/19 20:05
Diisopropyl ether ug/kg ND 5.0 04/19/19 20:05
Ethylbenzene ug/kg ND 5.0 04/19/19 20:05
Hexachloro-1,3-butadiene ug/kg ND 5.0 04/19/19 20:05
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/19/19 20:05
m&p-Xylene ug/kg ND 10.0 04/19/19 20:05
Methyl-tert-butyl ether ug/kg ND 5.0 04/19/19 20:05
Methylene Chloride ug/kg ND 20.0 04/19/19 20:05
n-Butylbenzene ug/kg ND 5.0 04/19/19 20:05
n-Propylbenzene ug/kg ND 5.0 04/19/19 20:05
Naphthalene ug/kg ND 5.0 04/19/19 20:05
o-Xylene ug/kg ND 5.0 04/19/19 20:05
p-Isopropyltoluene ug/kg ND 5.0 04/19/19 20:05
sec-Butylbenzene ug/kg ND 5.0 04/19/19 20:05
Styrene ug/kg ND 5.0 04/19/19 20:05
tert-Butylbenzene ug/kg ND 5.0 04/19/19 20:05
Tetrachloroethene ug/kg ND 5.0 04/19/19 20:05
Toluene ug/kg ND 5.0 04/19/19 20:05
trans-1,2-Dichloroethene ug/kg ND 5.0 04/19/19 20:05
trans-1,3-Dichloropropene ug/kg ND 5.0 04/19/19 20:05
Trichloroethene ug/kg ND 5.0 04/19/19 20:05
Trichlorofluoromethane ug/kg ND 5.0 04/19/19 20:05
Vinyl acetate ug/kg ND 50.0 04/19/19 20:05
Vinyl chloride ug/kg ND 10.0 04/19/19 20:05
Xylene (Total)ug/kg ND 10.0 04/19/19 20:05
1,2-Dichloroethane-d4 (S)%103 70-132 04/19/19 20:05
4-Bromofluorobenzene (S)%99 70-130 04/19/19 20:05
Toluene-d8 (S)%99 70-130 04/19/19 20:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2554407LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.950 100 70-130
1,1,1-Trichloroethane ug/kg 43.250 86 70-130
1,1,2,2-Tetrachloroethane ug/kg 48.250 96 55-130
1,1,2-Trichloroethane ug/kg 47.050 94 70-130
1,1-Dichloroethane ug/kg 42.450 85 68-130
1,1-Dichloroethene ug/kg 43.050 86 70-130
1,1-Dichloropropene ug/kg 42.850 86 70-130
1,2,3-Trichlorobenzene ug/kg 47.550 95 70-130
1,2,3-Trichloropropane ug/kg 51.450 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2554407LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 46.750 93 70-130
1,2,4-Trimethylbenzene ug/kg 44.050 88 69-130
1,2-Dibromo-3-chloropropane ug/kg 45.150 90 57-141
1,2-Dibromoethane (EDB)ug/kg 47.750 95 70-130
1,2-Dichlorobenzene ug/kg 44.950 90 70-130
1,2-Dichloroethane ug/kg 44.650 89 70-130
1,2-Dichloropropane ug/kg 46.550 93 70-130
1,3,5-Trimethylbenzene ug/kg 44.850 90 70-130
1,3-Dichlorobenzene ug/kg 44.250 88 70-130
1,3-Dichloropropane ug/kg 47.050 94 70-130
1,4-Dichlorobenzene ug/kg 44.250 88 70-130
2,2-Dichloropropane ug/kg 44.850 90 70-130
2-Butanone (MEK)ug/kg 101100 101 60-130
2-Chlorotoluene ug/kg 44.850 90 70-130
2-Hexanone ug/kg 93.1100 93 70-132
4-Chlorotoluene ug/kg 44.750 89 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 93.1100 93 69-130
Acetone ug/kg 102100 102 49-148
Benzene ug/kg 45.650 91 70-130
Bromobenzene ug/kg 45.650 91 70-130
Bromochloromethane ug/kg 45.750 91 70-130
Bromodichloromethane ug/kg 46.850 94 70-130
Bromoform ug/kg 42.050 84 68-136
Bromomethane ug/kg 43.050 86 60-140
Carbon tetrachloride ug/kg 44.050 88 70-130
Chlorobenzene ug/kg 43.350 87 70-130
Chloroethane ug/kg 49.250 98 51-147
Chloroform ug/kg 43.850 88 70-130
Chloromethane ug/kg 42.450 85 48-130
cis-1,2-Dichloroethene ug/kg 43.850 88 70-130
cis-1,3-Dichloropropene ug/kg 47.850 96 70-130
Dibromochloromethane ug/kg 47.350 95 70-130
Dibromomethane ug/kg 47.350 95 70-130
Dichlorodifluoromethane ug/kg 43.150 86 49-130
Diisopropyl ether ug/kg 48.750 97 66-130
Ethylbenzene ug/kg 45.150 90 70-130
Hexachloro-1,3-butadiene ug/kg 45.150 90 70-130
Isopropylbenzene (Cumene)ug/kg 44.650 89 70-130
m&p-Xylene ug/kg 89.9100 90 70-130
Methyl-tert-butyl ether ug/kg 48.250 96 70-130
Methylene Chloride ug/kg 38.350 77 50-137
n-Butylbenzene ug/kg 45.050 90 70-130
n-Propylbenzene ug/kg 45.050 90 70-130
Naphthalene ug/kg 47.150 94 70-131
o-Xylene ug/kg 44.250 88 70-130
p-Isopropyltoluene ug/kg 45.250 90 70-130
sec-Butylbenzene ug/kg 45.850 92 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2554407LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene ug/kg 44.350 89 70-130
tert-Butylbenzene ug/kg 40.150 80 69-130
Tetrachloroethene ug/kg 44.750 89 56-130
Toluene ug/kg 44.450 89 70-130
trans-1,2-Dichloroethene ug/kg 43.150 86 70-130
trans-1,3-Dichloropropene ug/kg 49.050 98 70-130
Trichloroethene ug/kg 43.950 88 70-141
Trichlorofluoromethane ug/kg 43.550 87 67-130
Vinyl acetate ug/kg 92.7100 93 10-136
Vinyl chloride ug/kg 43.250 86 67-130
Xylene (Total)ug/kg 134150 89 70-130
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2555712MATRIX SPIKE SAMPLE:
MSSpike
Result
92425764001
1,1,1,2-Tetrachloroethane ug/kg 469437 107 52-133ND
1,1,1-Trichloroethane ug/kg 426437 98 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 320437 73 39-150ND
1,1,2-Trichloroethane ug/kg 377437 86 48-140ND
1,1-Dichloroethane ug/kg 424437 97 46-135ND
1,1-Dichloroethene ug/kg 530437 121 38-149ND
1,1-Dichloropropene ug/kg 420437 96 41-140ND
1,2,3-Trichlorobenzene ug/kg 427437 98 10-158ND
1,2,3-Trichloropropane ug/kg 322437 74 33-157ND
1,2,4-Trichlorobenzene ug/kg 451437 103 10-155ND
1,2,4-Trimethylbenzene ug/kg 499437 114 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 237437 54 33-158ND
1,2-Dibromoethane (EDB)ug/kg 330437 76 40-136ND
1,2-Dichlorobenzene ug/kg 440437 101 27-146ND
1,2-Dichloroethane ug/kg 335437 77 49-140ND
1,2-Dichloropropane ug/kg 411437 94 44-143ND
1,3,5-Trimethylbenzene ug/kg 456437 104 40-144ND
1,3-Dichlorobenzene ug/kg 443437 102 33-140ND
1,3-Dichloropropane ug/kg 408437 93 47-147ND
1,4-Dichlorobenzene ug/kg 447437 102 35-139ND
2,2-Dichloropropane ug/kg 446437 102 41-140ND
2-Butanone (MEK)ug/kg 397J873 45 10-181ND
2-Chlorotoluene ug/kg 457437 105 38-147ND
2-Hexanone ug/kg 468J873 54 18-169ND
4-Chlorotoluene ug/kg 462437 106 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 509J873 58 16-175ND
Acetone ug/kg ND873 22 10-200ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2555712MATRIX SPIKE SAMPLE:
MSSpike
Result
92425764001
Benzene ug/kg 435437 100 46-136ND
Bromobenzene ug/kg 464437 106 38-149ND
Bromochloromethane ug/kg 335437 77 44-142ND
Bromodichloromethane ug/kg 369437 85 41-140ND
Bromoform ug/kg 331437 76 34-145ND
Bromomethane ug/kg 385437 88 14-162ND
Carbon tetrachloride ug/kg 442437 101 44-141ND
Chlorobenzene ug/kg 446437 102 39-141ND
Chloroethane ug/kg 215437 49 10-182ND
Chloroform ug/kg 387437 89 45-140ND
Chloromethane ug/kg 517437 119 19-149ND
cis-1,2-Dichloroethene ug/kg 401437 92 38-150ND
cis-1,3-Dichloropropene ug/kg 459437 105 30-144ND
Dibromochloromethane ug/kg 405437 93 36-145ND
Dibromomethane ug/kg 291437 67 41-145ND
Dichlorodifluoromethane ug/kg 241437 55 16-146ND
Diisopropyl ether ug/kg 445437 102 41-143ND
Ethylbenzene ug/kg 473437 108 35-144ND
Hexachloro-1,3-butadiene ug/kg 411437 94 10-160ND
Isopropylbenzene (Cumene)ug/kg 440437 101 30-152ND
m&p-Xylene ug/kg 1020873 116 33-145ND
Methyl-tert-butyl ether ug/kg 361437 83 49-140ND
Methylene Chloride ug/kg 489437 112 10-174ND
n-Butylbenzene ug/kg 428437 98 10-160ND
n-Propylbenzene ug/kg 468437 107 24-159ND
Naphthalene ug/kg 336437 77 10-171ND
o-Xylene ug/kg 507437 116 31-150ND
p-Isopropyltoluene ug/kg 445437 102 21-154ND
sec-Butylbenzene ug/kg 452437 104 19-159ND
Styrene ug/kg 442437 101 15-152ND
tert-Butylbenzene ug/kg 395437 91 31-141ND
Tetrachloroethene ug/kg 432437 99 19-141ND
Toluene ug/kg 517437 118 31-146ND
trans-1,2-Dichloroethene ug/kg 425437 97 28-157ND
trans-1,3-Dichloropropene ug/kg 376437 86 25-146ND
Trichloroethene ug/kg 442437 101 34-149ND
Trichlorofluoromethane ug/kg 427437 98 10-167ND
Vinyl acetate ug/kg 807J873 92 10-200ND
Vinyl chloride ug/kg 248437 57 36-155ND
Xylene (Total)ug/kg 15201310 116 29-148ND
1,2-Dichloroethane-d4 (S)%72 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%P210270-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92425574001
2555711SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 240 D649146
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92425574001
2555711SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%92100
4-Bromofluorobenzene (S)%9897
Toluene-d8 (S)%10299
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
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[phone]
Page 35 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
469616
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92425518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2550191
Associated Lab Samples:92425518006
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 04/16/19 17:54
1,2-Dichlorobenzene ug/kg ND 330 04/16/19 17:54
1,3-Dichlorobenzene ug/kg ND 330 04/16/19 17:54
1,4-Dichlorobenzene ug/kg ND 330 04/16/19 17:54
1-Methylnaphthalene ug/kg ND 330 04/16/19 17:54
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 v104/16/19 17:54
2,4,5-Trichlorophenol ug/kg ND 330 04/16/19 17:54
2,4,6-Trichlorophenol ug/kg ND 330 04/16/19 17:54
2,4-Dichlorophenol ug/kg ND 330 04/16/19 17:54
2,4-Dimethylphenol ug/kg ND 330 04/16/19 17:54
2,4-Dinitrophenol ug/kg ND 1650 04/16/19 17:54
2,4-Dinitrotoluene ug/kg ND 330 04/16/19 17:54
2,6-Dinitrotoluene ug/kg ND 330 04/16/19 17:54
2-Chloronaphthalene ug/kg ND 330 04/16/19 17:54
2-Chlorophenol ug/kg ND 330 04/16/19 17:54
2-Methylnaphthalene ug/kg ND 330 04/16/19 17:54
2-Methylphenol(o-Cresol)ug/kg ND 330 v104/16/19 17:54
2-Nitroaniline ug/kg ND 1650 04/16/19 17:54
2-Nitrophenol ug/kg ND 330 04/16/19 17:54
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 v104/16/19 17:54
3,3'-Dichlorobenzidine ug/kg ND 1650 04/16/19 17:54
3-Nitroaniline ug/kg ND 1650 04/16/19 17:54
4,6-Dinitro-2-methylphenol ug/kg ND 660 04/16/19 17:54
4-Bromophenylphenyl ether ug/kg ND 330 04/16/19 17:54
4-Chloro-3-methylphenol ug/kg ND 660 04/16/19 17:54
4-Chloroaniline ug/kg ND 1650 04/16/19 17:54
4-Chlorophenylphenyl ether ug/kg ND 330 04/16/19 17:54
4-Nitroaniline ug/kg ND 660 04/16/19 17:54
4-Nitrophenol ug/kg ND 1650 04/16/19 17:54
Acenaphthene ug/kg ND 330 04/16/19 17:54
Acenaphthylene ug/kg ND 330 04/16/19 17:54
Aniline ug/kg ND 330 04/16/19 17:54
Anthracene ug/kg ND 330 04/16/19 17:54
Benzo(a)anthracene ug/kg ND 330 04/16/19 17:54
Benzo(a)pyrene ug/kg ND 330 04/16/19 17:54
Benzo(b)fluoranthene ug/kg ND 330 04/16/19 17:54
Benzo(g,h,i)perylene ug/kg ND 330 04/16/19 17:54
Benzo(k)fluoranthene ug/kg ND 330 04/16/19 17:54
Benzoic Acid ug/kg ND 1650 04/16/19 17:54
Benzyl alcohol ug/kg ND 660 04/16/19 17:54
bis(2-Chloroethoxy)methane ug/kg ND 330 04/16/19 17:54
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2550191
Associated Lab Samples:92425518006
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 330 04/16/19 17:54
bis(2-Ethylhexyl)phthalate ug/kg ND 330 04/16/19 17:54
Butylbenzylphthalate ug/kg ND 330 04/16/19 17:54
Chrysene ug/kg ND 330 04/16/19 17:54
Di-n-butylphthalate ug/kg ND 330 04/16/19 17:54
Di-n-octylphthalate ug/kg ND 330 04/16/19 17:54
Dibenz(a,h)anthracene ug/kg ND 330 04/16/19 17:54
Dibenzofuran ug/kg ND 330 04/16/19 17:54
Diethylphthalate ug/kg ND 330 04/16/19 17:54
Dimethylphthalate ug/kg ND 330 04/16/19 17:54
Fluoranthene ug/kg ND 330 04/16/19 17:54
Fluorene ug/kg ND 330 04/16/19 17:54
Hexachloro-1,3-butadiene ug/kg ND 330 04/16/19 17:54
Hexachlorobenzene ug/kg ND 330 04/16/19 17:54
Hexachlorocyclopentadiene ug/kg ND 330 04/16/19 17:54
Hexachloroethane ug/kg ND 330 04/16/19 17:54
Indeno(1,2,3-cd)pyrene ug/kg ND 330 04/16/19 17:54
Isophorone ug/kg ND 330 04/16/19 17:54
N-Nitroso-di-n-propylamine ug/kg ND 330 04/16/19 17:54
N-Nitrosodimethylamine ug/kg ND 330 04/16/19 17:54
N-Nitrosodiphenylamine ug/kg ND 330 04/16/19 17:54
Naphthalene ug/kg ND 330 04/16/19 17:54
Nitrobenzene ug/kg ND 330 04/16/19 17:54
Pentachlorophenol ug/kg ND 1650 04/16/19 17:54
Phenanthrene ug/kg ND 330 04/16/19 17:54
Phenol ug/kg ND 330 v104/16/19 17:54
Pyrene ug/kg ND 330 04/16/19 17:54
2,4,6-Tribromophenol (S)%82 27-110 04/16/19 17:54
2-Fluorobiphenyl (S)%69 30-110 04/16/19 17:54
2-Fluorophenol (S)%70 13-110 04/16/19 17:54
Nitrobenzene-d5 (S)%67 23-110 04/16/19 17:54
Phenol-d6 (S)%72 22-110 04/16/19 17:54
Terphenyl-d14 (S)%89 28-110 04/16/19 17:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2550192LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12701670 76 52-130
1,2-Dichlorobenzene ug/kg 14201670 85 51-130
1,3-Dichlorobenzene ug/kg 13601670 81 50-130
1,4-Dichlorobenzene ug/kg 14001670 84 49-130
1-Methylnaphthalene ug/kg 15201670 91 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 1440 v116708630-130
2,4,5-Trichlorophenol ug/kg 13301670 80 55-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2550192LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 13601670 81 57-130
2,4-Dichlorophenol ug/kg 13701670 82 56-130
2,4-Dimethylphenol ug/kg 13101670 79 51-130
2,4-Dinitrophenol ug/kg 68908330 83 27-133
2,4-Dinitrotoluene ug/kg 14101670 85 61-130
2,6-Dinitrotoluene ug/kg 14301670 86 60-130
2-Chloronaphthalene ug/kg 13401670 80 52-130
2-Chlorophenol ug/kg 14801670 89 54-130
2-Methylnaphthalene ug/kg 15401670 92 54-130
2-Methylphenol(o-Cresol)ug/kg 1520 v116709151-130
2-Nitroaniline ug/kg 26203330 79 51-130
2-Nitrophenol ug/kg 13301670 80 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 1480 v116708911-163
3,3'-Dichlorobenzidine ug/kg 24703330 74 10-132
3-Nitroaniline ug/kg 24203330 73 55-130
4,6-Dinitro-2-methylphenol ug/kg 31903330 96 47-142
4-Bromophenylphenyl ether ug/kg 14801670 89 59-130
4-Chloro-3-methylphenol ug/kg 27203330 82 55-130
4-Chloroaniline ug/kg 26603330 80 54-130
4-Chlorophenylphenyl ether ug/kg 13801670 83 58-130
4-Nitroaniline ug/kg 28303330 85 54-130
4-Nitrophenol ug/kg 65808330 79 48-130
Acenaphthene ug/kg 15301670 92 60-130
Acenaphthylene ug/kg 16101670 97 60-130
Aniline ug/kg 12601670 75 43-130
Anthracene ug/kg 15901670 96 63-130
Benzo(a)anthracene ug/kg 15801670 95 59-130
Benzo(a)pyrene ug/kg 15601670 94 57-130
Benzo(b)fluoranthene ug/kg 15301670 92 54-130
Benzo(g,h,i)perylene ug/kg 16501670 99 59-130
Benzo(k)fluoranthene ug/kg 16201670 97 54-130
Benzoic Acid ug/kg 56408330 68 19-130
Benzyl alcohol ug/kg 30503330 91 50-130
bis(2-Chloroethoxy)methane ug/kg 12701670 76 54-130
bis(2-Chloroethyl) ether ug/kg 13401670 80 48-130
bis(2-Ethylhexyl)phthalate ug/kg 14401670 86 45-134
Butylbenzylphthalate ug/kg 14101670 85 46-138
Chrysene ug/kg 15701670 94 58-130
Di-n-butylphthalate ug/kg 14601670 88 60-130
Di-n-octylphthalate ug/kg 14901670 89 53-130
Dibenz(a,h)anthracene ug/kg 16201670 97 59-130
Dibenzofuran ug/kg 13801670 83 60-130
Diethylphthalate ug/kg 14101670 85 60-130
Dimethylphthalate ug/kg 14101670 85 60-130
Fluoranthene ug/kg 16501670 99 65-130
Fluorene ug/kg 15301670 92 63-130
Hexachloro-1,3-butadiene ug/kg 12501670 75 46-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2550192LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 15101670 91 58-130
Hexachlorocyclopentadiene ug/kg 12301670 74 23-130
Hexachloroethane ug/kg 13001670 78 47-130
Indeno(1,2,3-cd)pyrene ug/kg 16601670 99 60-130
Isophorone ug/kg 12701670 76 49-130
N-Nitroso-di-n-propylamine ug/kg 13301670 80 47-130
N-Nitrosodimethylamine ug/kg 13001670 78 45-130
N-Nitrosodiphenylamine ug/kg 14401670 86 59-130
Naphthalene ug/kg 15001670 90 55-130
Nitrobenzene ug/kg 12201670 73 49-130
Pentachlorophenol ug/kg 26103330 78 10-132
Phenanthrene ug/kg 16101670 97 62-130
Phenol ug/kg 1560 v116709446-130
Pyrene ug/kg 15501670 93 53-130
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%79 30-110
2-Fluorophenol (S)%86 13-110
Nitrobenzene-d5 (S)%76 23-110
Phenol-d6 (S)%89 22-110
Terphenyl-d14 (S)%86 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2550193MATRIX SPIKE SAMPLE:
MSSpike
Result
92425126005
1,2,4-Trichlorobenzene ug/kg 13802380 58 18-130ND
1,2-Dichlorobenzene ug/kg 14802380 62 14-130ND
1,3-Dichlorobenzene ug/kg 14302380 60 12-130ND
1,4-Dichlorobenzene ug/kg 14602380 61 10-130ND
1-Methylnaphthalene ug/kg 16402380 69 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 1660 v123807010-130ND
2,4,5-Trichlorophenol ug/kg 16702380 70 13-130ND
2,4,6-Trichlorophenol ug/kg 17502380 74 17-130ND
2,4-Dichlorophenol ug/kg 17702380 74 10-130ND
2,4-Dimethylphenol ug/kg 16502380 69 10-130ND
2,4-Dinitrophenol ug/kg 513011900 43 10-130ND
2,4-Dinitrotoluene ug/kg 16502380 69 24-130ND
2,6-Dinitrotoluene ug/kg 16902380 71 23-130ND
2-Chloronaphthalene ug/kg 13902380 58 19-130ND
2-Chlorophenol ug/kg 17802380 75 10-130ND
2-Methylnaphthalene ug/kg 16402380 69 18-130ND
2-Methylphenol(o-Cresol)ug/kg 1890 v123807910-130ND
2-Nitroaniline ug/kg 35104760 74 17-130ND
2-Nitrophenol ug/kg 17302380 73 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 1800 v123807610-130ND
3,3'-Dichlorobenzidine ug/kg 30804760 65 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2550193MATRIX SPIKE SAMPLE:
MSSpike
Result
92425126005
3-Nitroaniline ug/kg 35904760 76 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 39404760 83 10-152ND
4-Bromophenylphenyl ether ug/kg 15202380 64 29-130ND
4-Chloro-3-methylphenol ug/kg 36004760 76 17-130ND
4-Chloroaniline ug/kg 37004760 78 14-130ND
4-Chlorophenylphenyl ether ug/kg 14502380 61 25-130ND
4-Nitroaniline ug/kg 38404760 81 22-130ND
4-Nitrophenol ug/kg 834011900 70 10-130ND
Acenaphthene ug/kg 16202380 68 20-130ND
Acenaphthylene ug/kg 17502380 74 25-130ND
Aniline ug/kg 15402380 65 10-130ND
Anthracene ug/kg 17002380 72 29-130ND
Benzo(a)anthracene ug/kg 16502380 70 19-130ND
Benzo(a)pyrene ug/kg 16502380 69 12-130ND
Benzo(b)fluoranthene ug/kg 16502380 70 14-130ND
Benzo(g,h,i)perylene ug/kg 17002380 71 10-130ND
Benzo(k)fluoranthene ug/kg 16802380 71 14-130ND
Benzoic Acid ug/kg 554J M111900510-130ND
Benzyl alcohol ug/kg 37004760 78 13-130ND
bis(2-Chloroethoxy)methane ug/kg 16402380 69 16-130ND
bis(2-Chloroethyl) ether ug/kg 16402380 69 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 15702380 66 21-130ND
Butylbenzylphthalate ug/kg 15202380 64 23-130ND
Chrysene ug/kg 16602380 70 22-130ND
Di-n-butylphthalate ug/kg 15402380 65 30-130ND
Di-n-octylphthalate ug/kg 15802380 67 23-142ND
Dibenz(a,h)anthracene ug/kg 16902380 71 10-130ND
Dibenzofuran ug/kg 14602380 61 24-130ND
Diethylphthalate ug/kg 15402380 65 26-130ND
Dimethylphthalate ug/kg 17402380 73 22-130ND
Fluoranthene ug/kg 17302380 73 33-130ND
Fluorene ug/kg 16002380 67 22-130ND
Hexachloro-1,3-butadiene ug/kg 13102380 55 13-130ND
Hexachlorobenzene ug/kg 15802380 67 29-130ND
Hexachlorocyclopentadiene ug/kg 12602380 53 10-130ND
Hexachloroethane ug/kg 12902380 54 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 17002380 72 10-130ND
Isophorone ug/kg 16702380 70 13-130ND
N-Nitroso-di-n-propylamine ug/kg 16002380 67 12-130ND
N-Nitrosodimethylamine ug/kg 16002380 67 11-130ND
N-Nitrosodiphenylamine ug/kg 15802380 67 15-130ND
Naphthalene ug/kg 17302380 73 15-130ND
Nitrobenzene ug/kg 15502380 65 12-130ND
Pentachlorophenol ug/kg 33404760 70 10-130ND
Phenanthrene ug/kg 16802380 71 27-130ND
Phenol ug/kg 1820 v123807610-130ND
Pyrene ug/kg 16602380 70 19-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2550193MATRIX SPIKE SAMPLE:
MSSpike
Result
92425126005
2,4,6-Tribromophenol (S)%83 27-110
2-Fluorobiphenyl (S)%45 30-110
2-Fluorophenol (S)%74 13-110
Nitrobenzene-d5 (S)%67 23-110
Phenol-d6 (S)%74 22-110
Terphenyl-d14 (S)%47 28-110
Parameter Units
Dup
Result QualifiersRPDResult
92425126005
2550194SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
1-Methylnaphthalene ug/kg NDND
2,2'-Oxybis(1-chloropropane)ug/kg ND v1ND
2,4,5-Trichlorophenol ug/kg NDND
2,4,6-Trichlorophenol ug/kg NDND
2,4-Dichlorophenol ug/kg NDND
2,4-Dimethylphenol ug/kg NDND
2,4-Dinitrophenol ug/kg NDND
2,4-Dinitrotoluene ug/kg NDND
2,6-Dinitrotoluene ug/kg NDND
2-Chloronaphthalene ug/kg NDND
2-Chlorophenol ug/kg NDND
2-Methylnaphthalene ug/kg NDND
2-Methylphenol(o-Cresol)ug/kg ND v1ND
2-Nitroaniline ug/kg NDND
2-Nitrophenol ug/kg NDND
3&4-Methylphenol(m&p Cresol)ug/kg ND v1ND
3,3'-Dichlorobenzidine ug/kg NDND
3-Nitroaniline ug/kg NDND
4,6-Dinitro-2-methylphenol ug/kg NDND
4-Bromophenylphenyl ether ug/kg NDND
4-Chloro-3-methylphenol ug/kg NDND
4-Chloroaniline ug/kg NDND
4-Chlorophenylphenyl ether ug/kg NDND
4-Nitroaniline ug/kg NDND
4-Nitrophenol ug/kg NDND
Acenaphthene ug/kg NDND
Acenaphthylene ug/kg NDND
Aniline ug/kg NDND
Anthracene ug/kg NDND
Benzo(a)anthracene ug/kg NDND
Benzo(a)pyrene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92425126005
2550194SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg NDND
Benzo(g,h,i)perylene ug/kg NDND
Benzo(k)fluoranthene ug/kg NDND
Benzoic Acid ug/kg NDND
Benzyl alcohol ug/kg NDND
bis(2-Chloroethoxy)methane ug/kg NDND
bis(2-Chloroethyl) ether ug/kg NDND
bis(2-Ethylhexyl)phthalate ug/kg NDND
Butylbenzylphthalate ug/kg NDND
Chrysene ug/kg NDND
Di-n-butylphthalate ug/kg NDND
Di-n-octylphthalate ug/kg NDND
Dibenz(a,h)anthracene ug/kg NDND
Dibenzofuran ug/kg NDND
Diethylphthalate ug/kg NDND
Dimethylphthalate ug/kg NDND
Fluoranthene ug/kg NDND
Fluorene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Hexachlorobenzene ug/kg NDND
Hexachlorocyclopentadiene ug/kg NDND
Hexachloroethane ug/kg NDND
Indeno(1,2,3-cd)pyrene ug/kg NDND
Isophorone ug/kg NDND
N-Nitroso-di-n-propylamine ug/kg NDND
N-Nitrosodimethylamine ug/kg NDND
N-Nitrosodiphenylamine ug/kg NDND
Naphthalene ug/kg NDND
Nitrobenzene ug/kg NDND
Pentachlorophenol ug/kg NDND
Phenanthrene ug/kg NDND
Phenol ug/kg ND v1ND
Pyrene ug/kg NDND
2,4,6-Tribromophenol (S)%7576
2-Fluorobiphenyl (S)%5751
2-Fluorophenol (S)%5663
Nitrobenzene-d5 (S)%5863
Phenol-d6 (S)%5763
Terphenyl-d14 (S)%6933
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/30/2019 03:11 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
Page 42 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
470714
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92425518001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2555336
Associated Lab Samples:92425518001
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 327 04/22/19 19:42
1,2-Dichlorobenzene ug/kg ND 327 04/22/19 19:42
1,3-Dichlorobenzene ug/kg ND 327 04/22/19 19:42
1,4-Dichlorobenzene ug/kg ND 327 04/22/19 19:42
1-Methylnaphthalene ug/kg ND 327 04/22/19 19:42
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 04/22/19 19:42
2,4,5-Trichlorophenol ug/kg ND 327 04/22/19 19:42
2,4,6-Trichlorophenol ug/kg ND 327 04/22/19 19:42
2,4-Dichlorophenol ug/kg ND 327 v104/22/19 19:42
2,4-Dimethylphenol ug/kg ND 327 04/22/19 19:42
2,4-Dinitrophenol ug/kg ND 1630 v104/22/19 19:42
2,4-Dinitrotoluene ug/kg ND 327 04/22/19 19:42
2,6-Dinitrotoluene ug/kg ND 327 04/22/19 19:42
2-Chloronaphthalene ug/kg ND 327 04/22/19 19:42
2-Chlorophenol ug/kg ND 327 04/22/19 19:42
2-Methylnaphthalene ug/kg ND 327 04/22/19 19:42
2-Methylphenol(o-Cresol)ug/kg ND 327 04/22/19 19:42
2-Nitroaniline ug/kg ND 1630 04/22/19 19:42
2-Nitrophenol ug/kg ND 327 v104/22/19 19:42
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 04/22/19 19:42
3,3'-Dichlorobenzidine ug/kg ND 1630 v104/22/19 19:42
3-Nitroaniline ug/kg ND 1630 04/22/19 19:42
4,6-Dinitro-2-methylphenol ug/kg ND 653 v104/22/19 19:42
4-Bromophenylphenyl ether ug/kg ND 327 04/22/19 19:42
4-Chloro-3-methylphenol ug/kg ND 653 04/22/19 19:42
4-Chloroaniline ug/kg ND 1630 04/22/19 19:42
4-Chlorophenylphenyl ether ug/kg ND 327 04/22/19 19:42
4-Nitroaniline ug/kg ND 653 04/22/19 19:42
4-Nitrophenol ug/kg ND 1630 04/22/19 19:42
Acenaphthene ug/kg ND 327 04/22/19 19:42
Acenaphthylene ug/kg ND 327 04/22/19 19:42
Aniline ug/kg ND 327 04/22/19 19:42
Anthracene ug/kg ND 327 04/22/19 19:42
Benzo(a)anthracene ug/kg ND 327 04/22/19 19:42
Benzo(a)pyrene ug/kg ND 327 04/22/19 19:42
Benzo(b)fluoranthene ug/kg ND 327 04/22/19 19:42
Benzo(g,h,i)perylene ug/kg ND 327 04/22/19 19:42
Benzo(k)fluoranthene ug/kg ND 327 04/22/19 19:42
Benzoic Acid ug/kg ND 1630 v104/22/19 19:42
Benzyl alcohol ug/kg ND 653 04/22/19 19:42
bis(2-Chloroethoxy)methane ug/kg ND 327 04/22/19 19:42
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2555336
Associated Lab Samples:92425518001
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 327 04/22/19 19:42
bis(2-Ethylhexyl)phthalate ug/kg ND 327 04/22/19 19:42
Butylbenzylphthalate ug/kg ND 327 04/22/19 19:42
Chrysene ug/kg ND 327 04/22/19 19:42
Di-n-butylphthalate ug/kg ND 327 04/22/19 19:42
Di-n-octylphthalate ug/kg ND 327 04/22/19 19:42
Dibenz(a,h)anthracene ug/kg ND 327 04/22/19 19:42
Dibenzofuran ug/kg ND 327 04/22/19 19:42
Diethylphthalate ug/kg ND 327 04/22/19 19:42
Dimethylphthalate ug/kg ND 327 04/22/19 19:42
Fluoranthene ug/kg ND 327 04/22/19 19:42
Fluorene ug/kg ND 327 04/22/19 19:42
Hexachloro-1,3-butadiene ug/kg ND 327 04/22/19 19:42
Hexachlorobenzene ug/kg ND 327 04/22/19 19:42
Hexachlorocyclopentadiene ug/kg ND 327 04/22/19 19:42
Hexachloroethane ug/kg ND 327 04/22/19 19:42
Indeno(1,2,3-cd)pyrene ug/kg ND 327 04/22/19 19:42
Isophorone ug/kg ND 327 04/22/19 19:42
N-Nitroso-di-n-propylamine ug/kg ND 327 04/22/19 19:42
N-Nitrosodimethylamine ug/kg ND 327 04/22/19 19:42
N-Nitrosodiphenylamine ug/kg ND 327 04/22/19 19:42
Naphthalene ug/kg ND 327 04/22/19 19:42
Nitrobenzene ug/kg ND 327 04/22/19 19:42
Pentachlorophenol ug/kg ND 1630 04/22/19 19:42
Phenanthrene ug/kg ND 327 04/22/19 19:42
Phenol ug/kg ND 327 v104/22/19 19:42
Pyrene ug/kg ND 327 04/22/19 19:42
2,4,6-Tribromophenol (S)%81 27-110 04/22/19 19:42
2-Fluorobiphenyl (S)%65 30-110 04/22/19 19:42
2-Fluorophenol (S)%63 13-110 04/22/19 19:42
Nitrobenzene-d5 (S)%64 23-110 04/22/19 19:42
Phenol-d6 (S)%64 22-110 04/22/19 19:42
Terphenyl-d14 (S)%77 28-110 04/22/19 19:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2555337LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13801690 81 52-130
1,2-Dichlorobenzene ug/kg 14001690 83 51-130
1,3-Dichlorobenzene ug/kg 13301690 78 50-130
1,4-Dichlorobenzene ug/kg 14001690 83 49-130
1-Methylnaphthalene ug/kg 14901690 88 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 12801690 76 30-130
2,4,5-Trichlorophenol ug/kg 13801690 81 55-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2555337LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 14301690 84 57-130
2,4-Dichlorophenol ug/kg 1430 v116908456-130
2,4-Dimethylphenol ug/kg 13001690 77 51-130
2,4-Dinitrophenol ug/kg 66208470 78 27-133
2,4-Dinitrotoluene ug/kg 13701690 81 61-130
2,6-Dinitrotoluene ug/kg 14301690 84 60-130
2-Chloronaphthalene ug/kg 14901690 88 52-130
2-Chlorophenol ug/kg 14101690 83 54-130
2-Methylnaphthalene ug/kg 15001690 89 54-130
2-Methylphenol(o-Cresol)ug/kg 14701690 87 51-130
2-Nitroaniline ug/kg 24303390 72 51-130
2-Nitrophenol ug/kg 1390 v116908249-130
3&4-Methylphenol(m&p Cresol)ug/kg 14001690 83 11-163
3,3'-Dichlorobenzidine ug/kg 2970 v133908710-132
3-Nitroaniline ug/kg 27703390 82 55-130
4,6-Dinitro-2-methylphenol ug/kg 3260 v133909647-142
4-Bromophenylphenyl ether ug/kg 14801690 87 59-130
4-Chloro-3-methylphenol ug/kg 26903390 79 55-130
4-Chloroaniline ug/kg 28003390 83 54-130
4-Chlorophenylphenyl ether ug/kg 13701690 81 58-130
4-Nitroaniline ug/kg 26103390 77 54-130
4-Nitrophenol ug/kg 5970 v184707048-130
Acenaphthene ug/kg 15001690 89 60-130
Acenaphthylene ug/kg 15501690 92 60-130
Aniline ug/kg 12801690 76 43-130
Anthracene ug/kg 15401690 91 63-130
Benzo(a)anthracene ug/kg 15501690 92 59-130
Benzo(a)pyrene ug/kg 15301690 90 57-130
Benzo(b)fluoranthene ug/kg 17101690 101 54-130
Benzo(g,h,i)perylene ug/kg 16101690 95 59-130
Benzo(k)fluoranthene ug/kg 15801690 93 54-130
Benzoic Acid ug/kg 4660 v184705519-130
Benzyl alcohol ug/kg 28303390 83 50-130
bis(2-Chloroethoxy)methane ug/kg 12901690 76 54-130
bis(2-Chloroethyl) ether ug/kg 12601690 74 48-130
bis(2-Ethylhexyl)phthalate ug/kg 14401690 85 45-134
Butylbenzylphthalate ug/kg 14401690 85 46-138
Chrysene ug/kg 15301690 90 58-130
Di-n-butylphthalate ug/kg 13801690 82 60-130
Di-n-octylphthalate ug/kg 15401690 91 53-130
Dibenz(a,h)anthracene ug/kg 16401690 97 59-130
Dibenzofuran ug/kg 13901690 82 60-130
Diethylphthalate ug/kg 13001690 77 60-130
Dimethylphthalate ug/kg 13801690 81 60-130
Fluoranthene ug/kg 15601690 92 65-130
Fluorene ug/kg 14201690 84 63-130
Hexachloro-1,3-butadiene ug/kg 13901690 82 46-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2555337LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 15001690 89 58-130
Hexachlorocyclopentadiene ug/kg 13901690 82 23-130
Hexachloroethane ug/kg 12601690 74 47-130
Indeno(1,2,3-cd)pyrene ug/kg 16401690 97 60-130
Isophorone ug/kg 12701690 75 49-130
N-Nitroso-di-n-propylamine ug/kg 13301690 78 47-130
N-Nitrosodimethylamine ug/kg 11501690 68 45-130
N-Nitrosodiphenylamine ug/kg 14501690 86 59-130
Naphthalene ug/kg 14801690 88 55-130
Nitrobenzene ug/kg 12301690 73 49-130
Pentachlorophenol ug/kg 26703390 79 10-132
Phenanthrene ug/kg 15201690 90 62-130
Phenol ug/kg 1420 v116908446-130
Pyrene ug/kg 16501690 98 53-130
2,4,6-Tribromophenol (S)%98 27-110
2-Fluorobiphenyl (S)%78 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%75 23-110
Phenol-d6 (S)%82 22-110
Terphenyl-d14 (S)%88 28-110
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
469658
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92425518001, 92425518006
Parameter Units
Dup
Result QualifiersRPDResult
92424661001
2550407SAMPLE DUPLICATE:
Percent Moisture %99.8 099.6
Parameter Units
Dup
Result QualifiersRPDResult
92425496002
2550414SAMPLE DUPLICATE:
Percent Moisture %9.5 29.7
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
469671
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010,
92425518011
Parameter Units
Dup
Result QualifiersRPDResult
92425496003
2550481SAMPLE DUPLICATE:
Percent Moisture %11.0 1112.3
Parameter Units
Dup
Result QualifiersRPDResult
92425518011
2550482SAMPLE DUPLICATE:
Percent Moisture %64.0 063.9
REPORT OF LABORATORY ANALYSIS
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
470156
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Associated Lab Samples:92425518001, 92425518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2552646
Associated Lab Samples:92425518001, 92425518006
Matrix:Solid
Analyzed
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 04/20/19 00:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2552647LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/kg 9701000 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2553953MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
2617273001
2553954
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/kg M6,R1735-5490 90-110-1720 95858529001410039800
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
469525
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite
Associated Lab Samples:92425518001, 92425518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2549793
Associated Lab Samples:92425518001, 92425518006
Matrix:Solid
Analyzed
Nitrogen, Nitrate mg/kg ND 4.0 04/16/19 01:45
Nitrogen, Nitrite mg/kg ND 4.0 04/16/19 01:45
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 04/16/19 01:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2549794LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/kg 15.415 103 90-110
Nitrogen, Nitrite mg/kg 10.310 103 90-110
Nitrogen, NO2 plus NO3 mg/kg 25.725 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2549795MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92425518006
2549796
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/kg 36 111 90-110104 636ND39.9 37.4
Nitrogen, Nitrite mg/kg H123.9 101 90-11095 623.9ND 25.4 23.9
Nitrogen, NO2 plus NO3 mg/kg H160.2 105 90-11098 660.2ND 65.3 61.3
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92425518
Powell 4/12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
469716
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Associated Lab Samples:92425518001, 92425518006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2550760
Associated Lab Samples:92425518001, 92425518006
Matrix:Solid
Analyzed
Phosphorus mg/kg ND 1.0 04/16/19 23:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2550761LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/kg 52.850 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2550762MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92425518001
2550763
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/kg M1,R1116290-110-227 46114692694433
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92425518
Powell 4/12
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analysis conducted outside the EPA method holding time.H1
Extraction or preparation conducted outside EPA method holding time.H2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92425518
Powell 4/12
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92425518001 471202 471670C-1 EPA 3050B EPA 6010D
92425518006 471202 471670C-2 EPA 3050B EPA 6010D
92425518001 470793 470897C-1 EPA 7471B EPA 7471B
92425518006 470793 470897C-2 EPA 7471B EPA 7471B
92425518001 470714 470836C-1 EPA 3546 EPA 8270E
92425518006 469616 469682C-2 EPA 3546 EPA 8270E
92425518002 470498 470560C-1A EPA 5035A EPA 8260D
92425518003 470498 470560C-1B EPA 5035A EPA 8260D
92425518004 470498 470560C-1C EPA 5035A EPA 8260D
92425518005 470498 470560C-1D EPA 5035A EPA 8260D
92425518008 470498 470560C-2A EPA 5035A EPA 8260D
92425518009 470498 470560C-2B EPA 5035A EPA 8260D
92425518010 470498 470560C-2C EPA 5035A EPA 8260D
92425518011 470498 470560C-2D EPA 5035A EPA 8260D
92425518001 469658C-1 ASTM D2974-87
92425518002 469671C-1A ASTM D2974-87
92425518003 469671C-1B ASTM D2974-87
92425518004 469671C-1C ASTM D2974-87
92425518005 469671C-1D ASTM D2974-87
92425518006 469658C-2 ASTM D2974-87
92425518008 469671C-2A ASTM D2974-87
92425518009 469671C-2B ASTM D2974-87
92425518010 469671C-2C ASTM D2974-87
92425518011 469671C-2D ASTM D2974-87
92425518001 470156 470610C-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92425518006 470156 470610C-2 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92425518001 469525 469534C-1 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92425518006 469525 469534C-2 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92425518001 469716 469780C-1 EPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92425518006 469716 469780C-2 EPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
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Page 55 of 67
ANALYTICAL REPORT
April 29, 2019
Pace Analytical - Asheville, NC
Sample Delivery Group:L1091257
Samples Received:04/20/2019
Project Number:92425518
Description:powel 4/12
Site:001
Report To:Lorri Patton
2225 Riverside Drive
Asheville, NC 28804
Entire Report Reviewed By:
April 29, 2019
[Preliminary Report]
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Asheville, NC 92425518 L1091257 04/29/19 12:28 1 of 12
April 29, 2019
Nancy McLain
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Asheville, NC 92425518 L1091257 04/29/19 12:33 1 of 12
Page 56 of 67
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
C-1 L1091257-01 5
C-2 L1091257-02 6
Qc: Quality Control Summary 7
Total Solids by Method 2540 G-2011 7
Wet Chemistry by Method 9066 8
Gl: Glossary of Terms 9
Al: Accreditations & Locations 10
Sc: Sample Chain of Custody 11
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
C-1 L1091257-01 Solid 04/12/19 14:05 04/20/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1272269 1 04/27/19 09:15 04/27/19 09:25 JD Mt. Juliet, TN
Wet Chemistry by Method 9066 WG1270924 1 04/24/19 12:00 04/24/19 23:36 JER Mt. Juliet, TN
Collected by Collected date/time Received date/time
C-2 L1091257-02 Solid 04/12/19 16:05 04/20/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1272269 1 04/27/19 09:15 04/27/19 09:25 JD Mt. Juliet, TN
Wet Chemistry by Method 9066 WG1270924 1 04/24/19 12:00 04/24/19 23:37 JER Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Nancy McLain
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Nancy McLain
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 59 of 67
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1091257
C-1
Collected date/time: 04/12/19 14:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 37.0 1 04/27/2019 09:25 WG1272269
Wet Chemistry by Method 9066
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Total Phenol by 4AAP 2.53 B 0.594 1.81 1 04/24/2019 23:36 WG1270924
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1091257
C-2
Collected date/time: 04/12/19 16:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 41.4 1 04/27/2019 09:25 WG1272269
Wet Chemistry by Method 9066
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Total Phenol by 4AAP 1.81 B 0.532 1.62 1 04/24/2019 23:37 WG1270924
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1272269
Total Solids by Method 2540 G-2011 L1091257-01,02
Method Blank (MB)
(MB) R3406278-1 04/27/19 09:25
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1091268-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1091268-01 04/27/19 09:25 • (DUP) R3406278-3 04/27/19 09:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 76.0 76.0 1 0.00605 10
Laboratory Control Sample (LCS)
(LCS) R3406278-2 04/27/19 09:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1270924
Wet Chemistry by Method 9066 L1091257-01,02
Method Blank (MB)
(MB) R3405141-1 04/24/19 23:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Total Phenol by 4AAP 0.333 J 0.220 0.670
L1090654-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1090654-01 04/24/19 23:32 • (DUP) R3405141-3 04/24/19 23:33
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Total Phenol by 4AAP 1.56 2.35 1 40.3 P1 20
Laboratory Control Sample (LCS)
(LCS) R3405141-2 04/24/19 23:31
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Total Phenol by 4AAP 8.33 8.45 101 90.0-110
L1090836-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1090836-02 04/24/19 23:34 • (MS) R3405141-4 04/24/19 23:35 • (MSD) R3405141-5 04/24/19 23:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Total Phenol by 4AAP 1900 U 1590 1570 83.6 82.9 1 90.0-110 J6 J6 0.808 20
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Page 66 of 67
Page 67 of 67
#=CL#
May 10, 2019
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92427675
92427675
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
Powell TCLP Metals
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on April 12, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 9
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92427675
Powell TCLP Metals
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 9
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92427675
Powell TCLP Metals
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92427675001 C-1 EPA 6010D 3 PASI-ASH1
92427675002 C-2 EPA 6010D 3 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 9
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92427675
Powell TCLP Metals
Sample:C-1 Lab ID:92427675001 Collected:04/12/19 14:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 05/07/19 20:01 Initial pH: 7.24; Final pH: 4.5
6010 MET ICP, TCLP
Arsenic ND mg/L 05/09/19 12:16 7440-38-205/08/19 16:080.050 1
Chromium 0.077 mg/L 05/09/19 12:16 7440-47-305/08/19 16:080.050 1
Lead 0.029 mg/L 05/09/19 12:16 7439-92-105/08/19 16:080.025 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2019 07:58 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 9
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92427675
Powell TCLP Metals
Sample:C-2 Lab ID:92427675002 Collected:04/12/19 16:05 Received:04/12/19 17:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 05/07/19 20:01 Initial pH: 6.86; Final pH: 4.5
6010 MET ICP, TCLP
Arsenic ND mg/L 05/09/19 12:19 7440-38-205/08/19 16:080.050 1
Chromium ND mg/L 05/09/19 12:19 7440-47-305/08/19 16:080.050 1
Lead ND mg/L 05/09/19 12:19 7439-92-105/08/19 16:080.025 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2019 07:58 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 9
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92427675
Powell TCLP Metals
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
474059
EPA 3010A
EPA 6010D
6010 MET TCLP
Associated Lab Samples:92427675001, 92427675002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2568708
Associated Lab Samples:92427675001, 92427675002
Matrix:Water
Analyzed
Arsenic mg/L ND 0.050 05/09/19 11:57
Chromium mg/L ND 0.050 05/09/19 11:57
Lead mg/L ND 0.025 05/09/19 11:57
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2568709
Associated Lab Samples:92427675001, 92427675002
Matrix:Water
Analyzed
Arsenic mg/L ND 0.050 05/09/19 14:03
Chromium mg/L ND 0.050 05/09/19 14:03
Lead mg/L ND 0.025 05/09/19 14:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2570200LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.42.5 96 80-120
Chromium mg/L 2.42.5 96 80-120
Lead mg/L 2.32.5 92 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2570201LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.42.5 98 80-120
Chromium mg/L 2.52.5 100 80-120
Lead mg/L 2.42.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2570202MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92427574001
2570203
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 99 75-12599 02.5ND 2.5 2.5
Chromium mg/L 2.5 96 75-12596 02.5ND 2.4 2.4
Lead mg/L 2.5 93 75-12593 02.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2019 07:58 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 9
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92427675
Powell TCLP Metals
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2019 07:58 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 9
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92427675
Powell TCLP Metals
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92427675001 474059 474139C-1 EPA 3010A EPA 6010D
92427675002 474059 474139C-2 EPA 3010A EPA 6010D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2019 07:58 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 9
Page 9 of 9