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HomeMy WebLinkAboutWQ0015487_Wastewater Pond Closure Report_20200323 (2)INDUSTRIAL WASTEWATER POND CLOSURE REPORT CLOSED -LOOP RECYCLE PERMIT NO. WQ 0015487 POWELL INDUSTRIES, INC. SUNCREST CHIP MILL HAYWOOD COUNTY, NC Prepared for: POWELL INDUSTRIES, INC. March 23, 2020 INDUSTRIAL WASTEWATER POND CLOSURE REPORT CLOSED -LOOP RECYCLE PERMIT NO. WQ 0015487 POWELL INDUSTRIES, INC. SUNCREST CHIP MILL HAYWOOD COUNTY, NC Prepared for: POWELL INDUSTRIES, INC. Prepared by: MARTIN&SLAGLE GEOSCIENCES, PA PO BOX 1023 BLACK MOUNTAIN, NC 28711 828-669-3929 ,;'r�� �GENSFD��y''s 3/23/20 '9 i s 2 SEA. "yp� �FoLO�`��PQ-,�, Robert Martin, LG Principal Geologist Industrial Wastewater Pond Closure Report Powell Industries, Inc. TABLE OF CONTENTS Section 1.0 Introduction 2.0 Site Stormwater Sampling 3.0 WWP Closure 4.0 Post -Closure Monitoring Page 1 2 3 5 Figures Figure 1: Site Map Vicinity Map Figure 2: Site Map Figure 3: Sample Location Map Tables Table 1: Stormwater Sampling Results Table 2: Wastewater Sampling Results Table 3: Residuals Sampling Results Appendix Appendix A: Closure Checklist Appendix B: Analytical Reports Appendix C: Manifests and Weigh Tickets Appendix D: Photographs i INDUSTRIAL WASTEWATER POND CLOSURE REPORT POWELL INDUSTRIES, INC. SUNCREST CHIP MILL HAYWOOD COUNTY, NC CLOSED -LOOP RECYCLE PERMIT NO. WQ 0015487 1.0 INTRODUCTION On January 17, 2017, Powell Industries, Inc. (PI) located at 4595 Jonathan Creek Road, Waynesville, NC (Figure 1-Site Vicinity Map) requested that the Closed -Loop Recycle Permit for this facility be rescinded by the North Carolina Department of Environmental Quality, Division of Water Resources (DWR). In a letter from DWR on April 3, 2017, specific closure requirements for the WWP as well as "Guidelines for the Closure of Permitted Wastewater Ponds and Lagoons" (June 22, 2012) were forwarded to PI. Analytical results for wastewater samples collected from the WWP by DWR on May 25, 2016 and PI on November 8, 2016 were also attached. An "Industrial Wastewater Pond Closure Plan, Closed Loop Recycle Permit No. WQ 0015487" was submitted to NCDEQ on August 14, 2018. NCDEQ approved the closure plan with additional requirements by letter dated November 5, 2018. Closure of the WWP was conducted in accordance with the closure plan and requirements included in DWR's letter and the Guidelines provided to PI. This report only addresses closure of the WWP. Except for rerouting stormwater from the WWP to the Lower Pond, on -going stormwater issues are being addressed separately by design of a stormwater management system. The Checklist included in Attachment A of the closure guidelines has been completed and is included in Appendix A. Instruction Items associated with the checked items are referenced in this document. The WWP closure was accomplished by removal and proper disposal of impounded water and residual sediments in accordance with DWR Pond Closure Requirements. (Reference Checklist Item Il.a.) Industrial Wastewater Pond Closure Report Powell Industries, Inc. The 0.2-acre wastewater recycle pond located on the north side of the site was permitted as a non -discharge system which collected and recycled the wastewater discharge from the wet - decking process conducted as part of the chipping operation. In addition to receiving process wastewater, the WWP also received stormwater runoff from the various areas of the mill property. The wet -decking process which generated the permitted wastewater discharge has been discontinued. (Reference Checklist Item I.b.) Closure of the WWP was conducted in phases in order to continue to manage site stormwater, eliminate runoff into the WWP and allow site operations to continue during site work. A 0.3-acre pond, herein referred to as the "Lower Pond", situated immediately downstream of the WWP was used as a temporary stormwater retention pond during closure. The Lower Pond is not hydraulically connected to the WWP by outlet works other than a high-level spillway from the WWP. Management of stormwater during pond closure activities required evaluation of the water quality associated with site runoff prior to discharge into the WWP. Once water quality was characterized for the site runoff, stormwater runoff was routed to the Lower Pond by a by- pass trench excavated from the last junction box in the site storm sewer system west of the WWP, around the WWP dam and into the Lower Pond. Figure 2 shows the 11-acre property with process areas and stormwater conveyances. 2.0 SITE STORMWATER SAMPLING PI sampled stormwater on October 11, 2018 and a second time in February 2019. The October 11, 2019 sample was analyzed for 13 metals including arsenic, cadmium, calcium, chromium, copper, lead, magnesium, mercury, molybdenum, nickel, selenium, sodium, zinc; volatile organic compounds (VOCs); semi -volatile organic compounds (SVOCs); turbidity; total suspended solids (TSS); BOD; pH; ammonia; total Kjeldahl nitrogen (TKN); nitrogen, NN2/NO3; nitrate; nitrite; total phosphorus; and total phenolics. The February 2019 sample was analyzed for COD and TSS as required in the General Stormwater Discharge Permit for the site. The October 2018 stormwater samples were collected at the site drainage outfall into the WWP. After results were received and the stormwater bypass trench was excavated, the outfalls were disconnected at a concrete 2 Industrial Wastewater Pond Closure Report Powell Industries, Inc. junction box and the pipes into the WWP blocked to prevent any additional stormwater from entering into the WWP and preventing backflow of wastewater into the stormwater bypass trench. The February 2019 sample was collected at the discharge from the Lower Pond. The turbidity concentration detected at 19.9 NTU in stormwater sample SW-02 exceeded the NC 15A NCAC 02B surface water quality standards for classified Trout waters (<10 NTU). Total suspended solids (TSS) detected in sample SW-02 at 99.2 exceeded the Stormwater General Permit benchmark value of 50 mg/L. No VOCs or SVOCs were detected in either sample. Results are summarized in Table 1. Stormwater analytical reports are included in Appendix B. 3.0 WWP CLOSURE A. Wastewater Sampling, Analysis and Disposal Closure of the WWP involved dewatering of the impoundment and proper disposal of the water based on the analytical results (Reference Checklist Item IV.a.). Water in the WWP consisted of a mixture of stormwater and remnants of wastewater. A wastewater sample was collected from the WWP on February 14, 2019 and analyzed for the same expanded parameters as the stormwater samples described above. The results are summarized in Table 2. Laboratory reports are included in Appendix B. Wastewater was pumped from the pond into tankers and transported to the local POTW for disposal. Water removal was conducted over a period from November 15, 2019 through February 6, 2020. A total of 483,000 gallons of water were removed and properly disposed of. (Reference Checklist Item Ill.b.) B. Wastewater Residuals Analysis After the WWP was dewatered, two wastewater residual samples were composited from eight locations (four per composite) in the WWP. Eight grab samples were collected for analysis of VOCs. From each set of four grab samples, composite samples were prepared 3 Industrial Wastewater Pond Closure Report Powell Industries, Inc. for analysis of inorganic and SVOC parameters. Grab samples of each aliquot were collected for analysis of VOC constituents before combining for the two composite samples. The composite samples were analyzed for SVOCs; 13 metals including arsenic, cadmium, calcium, chromium, copper, lead, magnesium, mercury molybdenum, nickel, selenium, sodium, zinc; ammonia nitrogen; total Kjeldahl nitrogen (TKN); nitrogen, NN2/NO3, nitrate; nitrite; total phosphorus; and total phenolics. The eight grab samples of residuals were analyzed for VOCs. Sample results were compared to the NCDEQ Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs). Acetone was the only VOC detected in the wastewater residual grab samples. The concentrations range from 434 ug/Kg to 586 ug/Kg. The detected concentrations are below the Protection of Groundwater Standard PSRG. Table 3 summarizes the composite wastewater residual analytical results. A total of 10 metals were detected in wastewater residual composite samples. All were below the Protection of Groundwater PSRGs. Chromium was analyzed as total chromium (unspeciated). The concentrations detected were 59.9 and 66.5 mg/Kg. A TCLP analysis was conducted to ensure that the leachable concentrations were below the TCLP standard for total chromium. The TCLP result for chromium was 0.77 mg/L for sample C- 1 and non -detect for C-2. Laboratory reports are included in Appendix B. Since the analytical results for all regulated inorganic analytes are below leachable thresholds and VOCs were not detected except for acetone, which was well below its Protection of Groundwater PSRG, soils beneath the residual layer were not sampled. (Reference Checklist Item IV.b.) M Industrial Wastewater Pond Closure Report Powell Industries, Inc. C. Wastewater Residuals Disposal Disposal method(s) for wastewater residuals were determined following evaluation of analytical results. Since the WWP will be used for future stormwater management, wastewater residuals as determined by analysis were removed and disposed of. In order to pass the paint filter test as required for disposal at the solid waste facility, WWP residuals were mixed in the pond basin with sawdust to absorb free water prior to transport to the White Oak, Haywood County Landfill. A long reach trackhoe was used to excavate and mix residuals with sawdust. Residuals were loaded into dump -bed trailers and transported for disposal. Eighty-one loads totaling 1,409 tons of wastewater residuals were disposed of at the White Oak Landfill. Waste manifests and weigh tickets are included in Appendix C. (Reference Checklist Item Ill.c.) Photographs of WWP residuals removal are included in Appendix D. On February 7, 2020 Brett Laverty, NCDEQ representative visited the site to observe the work completed to date. He agreed that residuals had been adequately removed and indicated that residual removal was complete. Powell Industries hereby requests that the Closed -Loop Recycle Permit (Permit No. 0015487) be rescinded. 4.0 POST -CLOSURE MONITORING Post -closure monitoring of groundwater is not proposed since all analytes detected in the wastewater residuals were below PSRGs for industrial/commercial and protection of groundwater limits. E TOPO". map printed on 0.3/20/20 from "North Oarolina.tpo+' and "Untitled.tpg" 8.31,01.000, W WGS84 8.3000.000' Val �f � I 4 f KD C. • Subject Site f .} • I� # fig r FF - -_ - • I 11 LLJn M co til \4_ 'AD ff 1 Y M M �'M1 J rM i 'k' I, 'Y4�{'h �� R Jf ' �4 ' '� `�I+y, •, fffjffr{I RL 83001.000' W WGS84 83000.000' W 0 -5 1 MILE - Q AM FEET 0 1000 METES Frinted from TOFO'. 92001 National Coo,Eraphi--Holdings MARTIN S LAG LE DATE: 3/20/20 SITE VICINITY MAP GeoSciences, PA WASTEWATER POND PO Box 1023 Black Mountain, NC 28711 DR: RLM CLOSURE Powell Industries,lnc 828.669.3929 828.669.5289 CHK: Waynesville, NC PREPARED FOR: Powell Industries, Inc. FIGURE 1 z3.� : S� � — \ . 3y% MARTIN S LAG LE DATE: 3/20/20 SAMPLE LOCATION MAP GeoSciences, PA WASTEWATER POND PO Box 1023 Black Mountain, NC 28711 DR: RLM CLOSURE Powell Industries, Inc 828.669.3929 828.669.5289 CHK: Waynesville, NC PREPARED FOR: Powell Industries, Inc. FIGURE 3 TABLE 1 INDUSTRIAL WASTEWATER POND CLOSURE STORMWATER SAMPLE ANALYSIS POWELL INDUSTRIES, INC. HAYWOOD COUNTY, NC Regulatory Limits Analytical Results Parameters NC 15A NCAC 02B SURFACE WATER QUALITY STDS SW-01 (10/11/18) SW-02 (10/11/18) Turbidity (NTU) <10 (Trout, Tr) 3.1 19.8 Total Suspended Solids (mg/L) 50 (Trout, Tr)* 6.2 99.2 BOD (mg/L) 5,000 ND 2.3 pH (Std. Units) 6.0-9.0 6.3 6.4 Nitrogen, Ammonia (mg/L) NR ND ND Nitrogen, TKN (mg/L) NR 0.037J ND Nitrogen, NO2 plus NO3 (mg/L) NR 0.047 0.29 Nitrogen, Nitrate (mg/L) NR 0.047 0.29 Nitrogen, Nitrite (mg/L) NR ND 0.011J Phosphorus, Total (mg/L) NR 0.13 0.084 Phenolics, Total (mg/L) 300 0.012 0.0070J COD(mg/L) 120* 20.2J 24.7.1 Volatile Organic Compounds ND ND Semi -volatile Organic Compounds ND ND * NC Stormwater General Permit benchmark values. TABLE 2 INDUSTRIAL WASTEWATER POND CLOSURE WASTEWATER SAMPLE ANALYSIS POWELL INDUSTRIES, INC. HAYWOOD COUNTY, NC Analytical Results Parameters WW-01 (2/14/19) Calcium 28,500 Magnesium 2,690 Sodium 5,350 Zinc 12.1 Turbidity (NTU) 16.9 Total Suspended Solids (mg/L) 3.0 BOD (mg/L) ND pH (Std. Units) 7.1 Nitrogen, Ammonia (mg/L) 0.39 Nitrogen, TKN (mg/L) 0.81 Nitrogen, NO2 plus NO3 (mg/L) 0.054 Nitrogen, Nitrate (mg/L) 0.028 Nitrogen, Nitrite (mg/L) 0.027 Phosphorus, Total (mg/L) 0.063 Phenolics, Total (mg/L) ND Volatile Organic Compounds ND Semi -volatile Organic Compounds ND TABLE 3 INDUSTRIAL WASTEWATER POND CLOSURE WASTEWATER RESIDUALS SAMPLE ANALYSIS POWELL INDUSTRIES, INC. HAYWOOD COUNTY, NC Regulatory Limits Analytical Results Parameters PSRG-Protection of GW (mg/Kg) C-1 4/12/19 C-la 4/12/19 C-lb 4/12/19 C-1c 4/12/19 C-1d 4/12/19 C-2 4/12/19 C-2a 4/12/19 C-2b 4/12/19 C-2c 4/12/19 C-2d 4/12/19 Inorganics (mg/Kg) Arsenic 5.8 3.7 NA NA NA NA 2.0 NA NA NA NA Calcium NR 7,860 NA NA NA NA 3,490 NA NA NA NA Chromium 350,000 (3.8 Total) 59.9 NA NA NA NA 66.5 NA NA NA NA Copper 700 96.4 NA NA NA NA 88.9 NA NA NA NA Lead 270 15.8 NA NA NA NA 15.5 NA NA NA NA Magnesium NR 12,100 NA NA NA NA 13,200 NA NA NA NA Molybdenum 7.1 3.1 NA NA NA NA 3.0 NA NA NA NA Nickel 120 32.1 NA NA NA NA 33.8 NA NA NA NA Zinc 1200 264 NA NA NA NA 204 NA NA NA NA Mercury 1.0 0.046 NA NA NA NA 0.040 NA NA NA NA Nitrogen (TKN) NR 3,560 NA NA NA NA 3,400 NA NA NA NA Phosphorus NR 692 NA NA NA NA 623 NA NA NA NA TCLP (mg/L) Arsenic 5.0 ND NA NA NA NA ND NA NA NA NA Chromium 5.0 0.077 NA NA NA NA ND NA NA NA NA Lead 5.0 0.029 NA NA NA NA ND NA NA NA NA Volatile Organics (jig/Kg) Acetone 25,000 NA 457 ND (374) 383 586 NA 434 ND (1020) ND (8380) ND (414) APPENDIX A CHECKLIST AND INSTRUCTION ITEMS ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS Checklist and Instruction Items The purpose of the following checklist and instruction items is to aid in the development of a closure plan for a permitted Non -Discharge wastewater pond or lagoon to be submitted to the appropriate APS Regional office for approval. The following checklist allows the applicant to identify the type of lagoon to be closed, and the preferred closure and disposal options. The selected options include references to instruction items (e.g. Item A) found on subsequent pages of this attachment. The instruction items describe what steps are expected to be complete prior to approval of the closure plan,'including expected sampling and monitoring, and final certifications of complete closure. Note that the following steps are not all inclusive, as each site is unique and may have varying site conditions. In addition, flowcharts (Attachment B) have been provided as an alternate to the instructional Items A- H. These charts contain the same information, but give a visual representation of the closure process. For questions, contact the approving APS Regional Supervisor. Please check all items below that apply and submit a completed copy with the lagoon closure plan. Type of Pond or Lagoon System ' a. Primary and Secondary Biological Wastewater Lagoon Systems (examples: food processing treatment lagoons, municipal treatment systems without pretreatment programs, neighborhood treatment systems). ✓ b. Primary and Secondary Industrial Wastewater Lagoon Systems(examples: non-food type industrial treatment systems, municipal treatment systems with pretreatment program). _ c. Tertiary Wastewater Pond Systems ( examples: wastewater biological treatment systems with tertiary treatment to include infiltration disposal pond systems, effluent polishing pond systems). lI. Closure Options — Structure ✓ a. Conversion to Non -Wastewater Pond — Change of Use (Item B) Tb, Complete or partial removal -of stiructure: (Items..G)..- c. Site Reclamation (Item F and H) 111. Final Liquid and Solid Content Disposal Options _ a. Wastewater Disposal to Onsite Permitted Field (Item A) �b. Wastewater Disposal through Pump and Haul (Item A) c. Sludge Disposal to Permitted Site (Items C and D) d. Sludge Left in Place (Items C and E) TV. Sampling and Monitoring Requirements ✓ a. Wastewater Sampling Required (Items A and B) _ ✓ b. Soil and Sludge`Sampling Requited (Items C and F) c. Groundwater Monitoring Required (Item G) V. Final Certification Required for Closure Activities, as required in Item I. a. Structural Deconstruction (Professional Engineer or Hydrogeologist) ✓ b. Wastewater Disposal (Facility ORC) ✓ c. Sludge Disposal (ORC / Licensed Sludge Land Application Contractor) d. Other (Explain: A-1 Attachment A June 22, 2012 ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS Item A. Wastewater Sampling. Analysis, and Disposal 1.. Pond samples require a composite sampling technique. Samples should be composited from several locations. An adequate number of representative and composite samples should be taken and developed respectively. 2. For permitted disposal sites, sample and analyze wastewater in accordance with permit conditions. In the absence of permit specified monitoring, sample for the following parameters: a. Fecal coliform bacteria, chlorine residuals (if used as disinfectant), total nitrogen, BOD5, TSS, pH. b. Other parameters may be required based on waste streams, as directed by the APS Regional Supervisor. ' 3. All wastewater samples must be analyzed by a DWQ-certified laboratory. 4. Once the wastewater is sampled, the pond/lagoon can be dewatered to a permitted disposal site (uniform application of wastewater) or through a pump and haul permit. 5. Remove or plug all inflow and outflow piping, etc to the pond/lagoon Item B. Conversion to Non -Wastewater Pond (Tertiary Treatment Ponds Only) 6. Determine pond liquid volume (if water accumulates after complete disposal per Item A, Wastewater Sampling, Analysis, and Disposal). 7. If some sludge remains, sludge can be left in place, in accordance with Item E423 below. Otherwise, remove all residuals and dispose of properly per Item D, Sludge and Soil Disposal. 8. Disinfect and/or treat pond to meet Item B# 11 requirements below. 9. Sample pond (see Item A, Wastewater Sampling, Analysis, and Disposal) 10. No pond discharge is allowed to surface water without prior approval from an appropriate Surface Water Section Regional Office. Note that pond discharge to class SA waters is not allowable. i t . All discharges must meet water quality standards applicable to receiving stream classification or per limits provided by DWQ when water quality stream standards for monitored parameters are not defined. Item C. Soil and Sludge Analysis 12. All soil and sludge samples require a composite sampling technique. An adequate number of representative and composite samples should be taken and developed respectively. Thickness of sludge or soil and surface acreage should be considered. Example: one composite sample per acre foot. 13. All soil and sludge samples must be analyzed by a DWQ-certified laboratory. 14. For biological wastewater lagoons systems and tertiary wastewater pond systems, soil or sludge shall be sampled for: a. Pathogen and Vector Attraction Reductions. Testing should be done per 15A NCAC 02T . l 100. If project concerns only a tertiary pond, and pond sediments/sludge meets Class A pathogen reduction requirements (maximum of 1000 fecal coliform bacteria colonies per gram of total solids), additional characterization for pH, metals, nutrients, and solids as stated in 14.b and 14.c (below) may not be required, as determined on a case by case basis. b. Arsenic, cadmium, chromium, copper, lead, mercury, molybdenum, nickel, selenium, zinc, TKN, ammonia nitrogen, nitrate/nitrite, nitrogen, phosphorus, sodium, calcium, magnesium (mg/kg dry wt basis), percent total solids and pH. c. Other parameters may be required based on waste streams, as directed by the APS Regional Supervisor. A-2 Attachment A June 22, 2012 ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS 15. For industrial wastewater lagoon systems, this should be the same as biological wastewater lagoon system sampling plus site -specific parameters and hazardous characterization to include, but not limited to, TCLP, ignitability, corrosivity and reactivity, 16. If the sludge or soil samples are: a. Required to be analyzed for hazardous characteristics and results exceed hazardous characteristics regulatory limits, the material needs to be removed and reported to and managed in accordance with the Hazardous Waste Section in the Division of Waste Management. b. Not required to be analyzed for hazardous characteristics or results do not exceed the hazardous characteristics regulatory limits, the soil can be left in place if the following conditions are met: i. Total concentrations of contaminants in soil do not exceed protection of groundwater soil concentrations for North Carolina based on 2L standards, as calculated using theTransport Model for Calculation of Soil -to -Groundwater Concentrations from the USEPA 1996 Soil Screening Guidance document. (The EPA Transport model can be found in the "Soil Remediation Goals Table" at http:!4 rtal.ncdenr.or wweb/wm/sf/ihs/ihs uguide or the "2L, MCL, and Soil Screening Levels Table" at lit p:j�portal ncdenr oraweb/wm/hw/technical/euidance.) ii. Total concentrations of contaminants in the soil exceed protection of groundwater soil concentrations for North Carolina, but results do not exceed naturally -occurring background concentrations, iii. A more stringent soil clean-up level is not necessary due to site specific conditions as determined by the Division. For sludge left in place, see Item E, Sludge Left in Place. For sludge disposal, see Item D, Sludge and Soil Disposal. c. Not required to be analyzed for hazardous characteristics or results do not exceed hazardous characteristics regulatory limits, but total concentration results exceed corresponding protection of groundwater soil concentrations for North Carolina as calculated using the Transport Model from the USEPA 1996Soi1 Screening Guidance document described.in 16(b)(i), soil and sludge must be disposed of according to Item D, Sludge and Soil Disposal. For soils that exceed protection of groundwater levels, Item G, Groundwater Post Closure Monitoring, must also be considered. 17. For ponds or lagoon bottoms that intercept groundwater, Regional Offices will determine what type of sampling is required for the remaining contents on a case by case basis. Item D. Sludge and Soil Disposal 18. Measure surface area and depth of sludge and soil (if required) to determine disposal volume 19. Sample sludge and soil (if required) for permitted disposal option including pathogen and vector attraction reduction verification (see Item C, Soil and Sludge Analysis) 20. If a tertiary pond and sludge/sediments meet Class A pathogen and vector attraction reduction requirements, sludge/sediments can be land applied uniformly on site without sludge permitting action (additional sludge or soil characterization may not be required, as determined on a case by case basis). 21. If sludge or soil does not meet Class A pathogen and vector attraction reduction requirements, sludge/sediments may require a permit modification to land apply. 22. Pathogen and vector attraction reduction testing will not be required if sludge or soil is taken to a permitted compost or another treatment facility for further stabilization. A-3 Attachment A June 22, 2012 ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS Item E. Sludge Left in Place 23. For closure purposes, the Division of Water Quality considers it practical to remove sludge content from structures. The Division will evaluate the applicability of leaving any remaining volume of sludge content in the structure on a case -by case basis. Sufficient technical justification shall be provided to support such recommendation. Item F. Liner Demolition/Disposal 24. If a synthetic liner is present, remove synthetic liner, scarify/rip/disk underlying material in cases where there is no potential benefit for reuse of the structure based on projected future site use. a. If there are no historical problems with the lagoon (documented seepage, etc.) and the liner is intact after dewatering with no visible indications of seepage, soil sampling may still. be required on a case -by -case basis. b. If liner and/or lagoon issues are documented, the soil material under the synthetic liner should be sampled according to Item C, Soil and Sludge Analysis. 25. If clay liner is present, scarify/rip/disk and/or remove and reuse as cap if filling. If the liner is natural clay, sampling may be required on a case by case basis if the following conditions are not met: a. Based on existing groundwater monitoring data, no groundwater violations are present, b. Domestic wastewater systems only, c, Surficial layer of earthen material (top 6" — 12") removed, and d. All sludge removed and the remaining material is only soil and not co -mingled soil/sludge. 26. If the clay liner does not meet the conditions in #25 above, the clay liner should be sampled according to Item C, Soil and Sludge Analysis. 27. If a pond or lagoon does not have a liner, the underlying_ soil should be sampled according to Item C, Soil and Sludge Analysis. Item G. Groundwater Post Closure Monitorint> 29.-For faoi-lities=with-no.historic- groundwater monitoring, monitoring may be.rsquired based on post closure soil sample results. Contact Regional Office for directions. If groundwater monitoring is not required, permittee can petition the Division for rescission once the site is reclaimed. 29. For ponds or lagoons with historic groundwater monitoring and no groundwater violations were detected, no further groundwater monitoring will be required, as recommended by the Regional Office based on existing data. 30. For ponds or lagoons with historic groundwater monitoring and/or 15A NCAC 2L standards were exceeded, the following actions would be required: u a. Maintain permit with limited actions as recommended by the Regional Office (e.g. annual groundwater monitoring and reporting). b. Continue groundwater monitoring as permitted for a minimum of three sampling events. i. If there are no further groundwater exceedances detected or exceedances show a trend of lowering toward groundwater standards, the permittee could petition the Division for permit rescission. ii. If groundwater exceedances continue at the same level, continued monitoring and or site evaluation would be required at the Regional Office Supervisor's discretion. c. In lieu of groundwater monitoring, the Permittee may provide predictive calculations, acceptable to the Director, to demonstrate groundwater standards can be met at the property boundary. A-4 Attachment A June 22, 2012 ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS Item H. Berms/LaQoon Walls and Site Reclamation* 31. In cases where retention of municipal structures provides no value based on projected future site use, it is recommended that minimal demolition be performed to breach or remove sidewalls (dependent on the size) when the liner is demolished. Minimal demolition may be considered feasible in cases where retention of the structure or a portion thereof poses minimal risks based on conditions such as low population densities of surrounding areas, low hazard environment, low probability of encroaching development, etc. 32. For privately owned and higher risk municipal structures, more extensive structure demolition is recommended to include, but not be limited to, removal of berms/dike walls and general grading of project site. 33. If structure is completely constructed at or below grade, fill with clean material (partial or complete, depending on size) and/or grade site to minimize any hazards posed by existing conditions. 34. If structure is finished in the groundwater table, see Item C #17. 35. Stabilize the site with vegetation. Establishment of trees, grasses, and other viable cover crops should be considered to assist site stabilization and with removing any remaining nutrients. *Recognize the added value of planned reclamation efforts. Reclamation activities incorporating created artificial wetland systems, planted trees, and other pro -active actions viewed as either mitigation efforts or secondary environmental protection measures may assist with enabling the closure project to qualify for recognition and benefit from other environmental programs, such as those offered through conservation easements. Item I. Final CoWleations 36. For deconstruction including berm removal, berm breaching, or liner destruction, submit a letter certified by the overseeing professional engineer that action was taken according to the approved plan, as well as all local and state regulations. 37. For wastewater disposal, submit a copy of the monitoring report that documents lagoon wastewater disposal activities, certified by the facility ORC. - -3S: -For•sludge disposal; submit•a copy of the records documenting lagoon sludge disposal, certified by the licensed sludge land application contractor if land applied. If sludge was disposed of in a landfill, records from the receiving facility shall be provided. 39. Sampling results from any post -closure sampling conducted at the facility to document proper removal of sludge in accordance with the approved closure plan shall be submitted. 40. Photos of closure activities documenting conditions prior to initiating closure, closure activities, and post - closure conditions are recommended, but not required. 41. Other. A-5 Attachment A June 22, 2012 APPENDIX B ANALYTICAL REPORTS aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 October 19, 2018 Mr. Robert Martin Martin and Slagle 24 Lookout Terrace Black Mountain, NC 28711 RE: Project: Powell Industries 10/11 Pace Project No.: 92403169 Dear Mr. Martin: Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com 1(828)254-7176 Project Manager Enclosures �pQ AC RFb REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Powell Industries 10/11 Pace Project No.: 92403169 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Pace Project No.: Powell Industries 10/11 92403169 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92403169001 SW-01 EPA 625.1 PKS 58 PASI-C SM 6200B GAW 63 PASI-C EPA 180.1 Rev 2.0 1993 EWS 1 PASI-A SM 2540D-2011 CEH 1 PASI-A SM 521OB-2011 RLO 1 PASI-A EPA 9040C SMK 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 DMN 3 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A EPA420.4 Rev 1.0 1993 DMN 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92403169002 SW-02 EPA 625.1 PKS 58 PASI-C SM 6200B GAW 63 PASI-C EPA 180.1 Rev 2.0 1993 EWS 1 PASI-A SM 2540D-2011 CEH 1 PASI-A SM 521OB-2011 RLO 1 PASI-A EPA 9040C SMK 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 DMN 3 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A EPA420.4 Rev 1.0 1993 DMN 1 PASI-A SM 5220D-2011 MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-01 Lab ID: 92403169001 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Acenaphthene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 83-32-9 Acenaphthylene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 208-96-8 Anthracene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 120-12-7 Benzo(a)anthracene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 56-55-3 Benzo(a)pyrene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 50-32-8 Benzo(b)fluoranthene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 205-99-2 Benzo(g,h,i)perylene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 191-24-2 Benzo(k)fluoranthene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 207-08-9 4-Bromophenylphenyl ether ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 101-55-3 Butylbenzylphthalate ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 111-91-1 bis(2-Chloroethyl) ether ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 111-44-4 2-Chloronaphthalene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 91-58-7 2-Chlorophenol ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 95-57-8 4-Chlorophenylphenyl ether ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 7005-72-3 Chrysene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 218-01-9 Dibenz(a,h)anthracene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 53-70-3 3,3'-Dichlorobenzidine ND ug/L 24.5 1 10/13/18 15:00 10/15/18 19:58 91-94-1 2,4-Dichlorophenol ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 120-83-2 Diethylphthalate ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 84-66-2 2,4-Dimethylphenol ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 105-67-9 Dimethylphthalate ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 131-11-3 Di-n-butylphthalate ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 19.6 1 10/13/18 15:00 10/15/18 19:58 534-52-1 2,4-Dinitrophenol ND ug/L 49.0 1 10/13/18 15:00 10/15/18 19:58 51-28-5 2,4-Dinitrotoluene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 121-14-2 2,6-Dinitrotoluene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 606-20-2 Di-n-octylphthalate ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 117-81-7 Fluoranthene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 206-44-0 Fluorene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 86-73-7 Hexachloro-1,3-butadiene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 87-68-3 Hexachlorobenzene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 118-74-1 Hexachlorocyclopentadiene ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 77-47-4 Hexachloroethane ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 193-39-5 Isophorone ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 78-59-1 Naphthalene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 91-20-3 Nitrobenzene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 98-95-3 2-Nitrophenol ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 88-75-5 4-Nitrophenol ND ug/L 49.0 1 10/13/18 15:00 10/15/18 19:58 100-02-7 N-Nitrosodimethylamine ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 108-60-1 Pentachlorophenol ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 87-86-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-01 Lab ID: 92403169001 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Phenanthrene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 85-01-8 Phenol ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 108-95-2 Pyrene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 129-00-0 1,2,4-Trichlorobenzene ND ug/L 4.9 1 10/13/18 15:00 10/15/18 19:58 120-82-1 2,4,6-TrichIorophenol ND ug/L 9.8 1 10/13/18 15:00 10/15/18 19:58 88-06-2 Surrogates Nitrobenzene-d5 (S) 32 % 10-120 1 10/13/18 15:00 10/15/18 19:58 4165-60-0 2-Fluorobiphenyl (S) 30 % 15-120 1 10/13/18 15:00 10/15/18 19:58 321-60-8 Terphenyl-d14 (S) 45 % 11-131 1 10/13/18 15:00 10/15/18 19:58 1718-51-0 Phenol-d6 (S) 13 % 10-120 1 10/13/18 15:00 10/15/18 19:58 13127-88-3 2-Fluorophenol (S) 20 % 10-120 1 10/13/18 15:00 10/15/18 19:58 367-12-4 2,4,6-Tribromophenol (S) 37 % 10-137 1 10/13/18 15:00 10/15/18 19:58 118-79-6 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/17/18 15:42 71-43-2 Bromobenzene ND ug/L 0.50 1 10/17/18 15:42 108-86-1 Bromochloromethane ND ug/L 0.50 1 10/17/18 15:42 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/17/18 15:42 75-27-4 Bromoform ND ug/L 0.50 1 10/17/18 15:42 75-25-2 Bromomethane ND ug/L 5.0 1 10/17/18 15:42 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/17/18 15:42 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/17/18 15:42 135-98-8 tert-Butyl benzene ND ug/L 0.50 1 10/17/18 15:42 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/17/18 15:42 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/17/18 15:42 108-90-7 Chloroethane ND ug/L 1.0 1 10/17/18 15:42 75-00-3 Chloroform ND ug/L 0.50 1 10/17/18 15:42 67-66-3 Chloromethane ND ug/L 1.0 1 10/17/18 15:42 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10/17/18 15:42 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/17/18 15:42 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/17/18 15:42 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10/17/18 15:42 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/17/18 15:42 106-93-4 Dibromomethane ND ug/L 0.50 1 10/17/18 15:42 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/17/18 15:42 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/17/18 15:42 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/17/18 15:42 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 10/17/18 15:42 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 10/17/18 15:42 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/17/18 15:42 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/17/18 15:42 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10/17/18 15:42 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/17/18 15:42 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/17/18 15:42 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/17/18 15:42 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/17/18 15:42 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/17/18 15:42 563-58-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-01 Lab ID: 92403169001 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B cis-1,3-Dichloropropene ND ug/L 0.50 1 10/17/18 15:42 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 10/17/18 15:42 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10/17/18 15:42 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/17/18 15:42 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/17/18 15:42 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 10/17/18 15:42 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/17/18 15:42 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 10/17/18 15:42 1634-04-4 Naphthalene ND ug/L 2.0 1 10/17/18 15:42 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10/17/18 15:42 103-65-1 Styrene ND ug/L 0.50 1 10/17/18 15:42 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 10/17/18 15:42 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 10/17/18 15:42 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10/17/18 15:42 127-18-4 Toluene ND ug/L 0.50 1 10/17/18 15:42 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10/17/18 15:42 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10/17/18 15:42 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 10/17/18 15:42 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 10/17/18 15:42 79-00-5 Trichloroethene ND ug/L 0.50 1 10/17/18 15:42 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/17/18 15:42 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 1 10/17/18 15:42 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10/17/18 15:42 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 1 10/17/18 15:42 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/17/18 15:42 75-01-4 m&p-Xylene ND ug/L 1.0 1 10/17/18 15:42 179601-23-1 o-Xylene ND ug/L 0.50 1 10/17/18 15:42 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 10/17/18 15:42 17060-07-0 4-Bromofluorobenzene (S) 94 % 70-130 1 10/17/18 15:42 460-00-4 Toluene-d8 (S) 101 % 70-130 1 10/17/18 15:42 2037-26-5 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 3.1 NTU 1.0 1 10/12/1815:08 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 6.2 mg/L 2.5 1 10/13/18 00:55 5210B BOD, 5 day Analytical Method: SM 521OB-2011 BOD, 5 day ND mg/L 2.0 1 10/12/18 06:38 10/17/18 02:41 B2 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.3 Std. Units 0.10 1 10/15/18 14:56 H3 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia ND mg/L 0.10 1 10/15/18 11:06 7664-41-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-01 Lab ID: 92403169001 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total ND mg/L 0.50 1 10/14/18 14:41 10/16/18 00:24 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.047 mg/L 0.020 1 10/12/18 08:01 Nitrogen, Nitrate 0.047 mg/L 0.020 1 10/12/18 08:01 14797-55-8 Nitrogen, Nitrite ND mg/L 0.020 1 10/12/18 08:01 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.13 mg/L 0.050 1 10/12/18 18:30 10/12/18 23:08 7723-14-0 420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993 Phenol 0.012 mg/L 0.010 1 10/17/1818:31 10/18/1818:29 108-95-2 BC,M1 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 10/12/18 18:03 10/12/18 21:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-02 Lab ID: 92403169002 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Acenaphthene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 83-32-9 Acenaphthylene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 208-96-8 Anthracene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 120-12-7 Benzo(a)anthracene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 56-55-3 Benzo(a)pyrene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 50-32-8 Benzo(b)fluoranthene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 205-99-2 Benzo(g,h,i)perylene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 191-24-2 Benzo(k)fluoranthene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 207-08-9 4-Bromophenylphenyl ether ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 101-55-3 Butylbenzylphthalate ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 111-91-1 bis(2-Chloroethyl) ether ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 111-44-4 2-Chloronaphthalene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 91-58-7 2-Chlorophenol ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 95-57-8 4-Chlorophenylphenyl ether ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 7005-72-3 Chrysene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 218-01-9 Dibenz(a,h)anthracene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 53-70-3 3,3'-Dichlorobenzidine ND ug/L 24.0 1 10/13/18 15:00 10/15/18 20:29 91-94-1 2,4-Dichlorophenol ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 120-83-2 Diethylphthalate ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 84-66-2 2,4-Dimethylphenol ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 105-67-9 Dimethylphthalate ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 131-11-3 Di-n-butylphthalate ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 19.2 1 10/13/18 15:00 10/15/18 20:29 534-52-1 2,4-Dinitrophenol ND ug/L 48.1 1 10/13/18 15:00 10/15/18 20:29 51-28-5 2,4-Dinitrotoluene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 121-14-2 2,6-Dinitrotoluene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 606-20-2 Di-n-octylphthalate ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 117-81-7 Fluoranthene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 206-44-0 Fluorene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 86-73-7 Hexachloro-1,3-butadiene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 87-68-3 Hexachlorobenzene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 118-74-1 Hexachlorocyclopentadiene ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 77-47-4 Hexachloroethane ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 193-39-5 Isophorone ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 78-59-1 Naphthalene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 91-20-3 Nitrobenzene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 98-95-3 2-Nitrophenol ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 88-75-5 4-Nitrophenol ND ug/L 48.1 1 10/13/18 15:00 10/15/18 20:29 100-02-7 N-Nitrosodimethylamine ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 108-60-1 Pentachlorophenol ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 87-86-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-02 Lab ID: 92403169002 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Phenanthrene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 85-01-8 Phenol ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 108-95-2 Pyrene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 129-00-0 1,2,4-Trichlorobenzene ND ug/L 4.8 1 10/13/18 15:00 10/15/18 20:29 120-82-1 2,4,6-TrichIorophenol ND ug/L 9.6 1 10/13/18 15:00 10/15/18 20:29 88-06-2 Surrogates Nitrobenzene-d5 (S) 43 % 10-120 1 10/13/18 15:00 10/15/18 20:29 4165-60-0 2-Fluorobiphenyl (S) 41 % 15-120 1 10/13/18 15:00 10/15/18 20:29 321-60-8 Terphenyl-d14 (S) 59 % 11-131 1 10/13/18 15:00 10/15/18 20:29 1718-51-0 Phenol-d6 (S) 19 % 10-120 1 10/13/18 15:00 10/15/18 20:29 13127-88-3 2-Fluorophenol (S) 29 % 10-120 1 10/13/18 15:00 10/15/18 20:29 367-12-4 2,4,6-Tribromophenol (S) 46 % 10-137 1 10/13/18 15:00 10/15/18 20:29 118-79-6 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/17/18 15:58 71-43-2 Bromobenzene ND ug/L 0.50 1 10/17/18 15:58 108-86-1 Bromochloromethane ND ug/L 0.50 1 10/17/18 15:58 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/17/18 15:58 75-27-4 Bromoform ND ug/L 0.50 1 10/17/18 15:58 75-25-2 Bromomethane ND ug/L 5.0 1 10/17/18 15:58 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/17/18 15:58 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/17/18 15:58 135-98-8 tert-Butyl benzene ND ug/L 0.50 1 10/17/18 15:58 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/17/18 15:58 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/17/18 15:58 108-90-7 Chloroethane ND ug/L 1.0 1 10/17/18 15:58 75-00-3 Chloroform ND ug/L 0.50 1 10/17/18 15:58 67-66-3 Chloromethane ND ug/L 1.0 1 10/17/18 15:58 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10/17/18 15:58 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/17/18 15:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/17/18 15:58 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10/17/18 15:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/17/18 15:58 106-93-4 Dibromomethane ND ug/L 0.50 1 10/17/18 15:58 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/17/18 15:58 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/17/18 15:58 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/17/18 15:58 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 10/17/18 15:58 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 10/17/18 15:58 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/17/18 15:58 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/17/18 15:58 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10/17/18 15:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/17/18 15:58 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/17/18 15:58 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/17/18 15:58 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/17/18 15:58 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/17/18 15:58 563-58-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-02 Lab ID: 92403169002 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B cis-1,3-Dichloropropene ND ug/L 0.50 1 10/17/18 15:58 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 10/17/18 15:58 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10/17/18 15:58 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/17/18 15:58 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/17/18 15:58 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 10/17/18 15:58 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/17/18 15:58 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 10/17/18 15:58 1634-04-4 Naphthalene ND ug/L 2.0 1 10/17/18 15:58 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10/17/18 15:58 103-65-1 Styrene ND ug/L 0.50 1 10/17/18 15:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 10/17/18 15:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 10/17/18 15:58 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10/17/18 15:58 127-18-4 Toluene ND ug/L 0.50 1 10/17/18 15:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10/17/18 15:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10/17/18 15:58 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 10/17/18 15:58 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 10/17/18 15:58 79-00-5 Trichloroethene ND ug/L 0.50 1 10/17/18 15:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/17/18 15:58 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 1 10/17/18 15:58 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10/17/18 15:58 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 1 10/17/18 15:58 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/17/18 15:58 75-01-4 m&p-Xylene ND ug/L 1.0 1 10/17/18 15:58 179601-23-1 o-Xylene ND ug/L 0.50 1 10/17/18 15:58 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 10/17/18 15:58 17060-07-0 4-Bromofluorobenzene (S) 95 % 70-130 1 10/17/18 15:58 460-00-4 Toluene-d8 (S) 100 % 70-130 1 10/17/18 15:58 2037-26-5 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 19.8 NTU 1.0 1 10/12/1815:10 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 99.2 mg/L 10.0 1 10/13/18 00:56 5210B BOD, 5 day Analytical Method: SM 521OB-2011 BOD, 5 day 2.3 mg/L 2.0 1 10/12/18 06:38 10/17/18 02:43 B2 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.4 Std. Units 0.10 1 10/15/18 14:58 H3 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia ND mg/L 0.10 1 10/15/18 11:15 7664-41-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries 10/11 Pace Project No.: 92403169 Sample: SW-02 Lab ID: 92403169002 Collected: 10/11/18 03:30 Received: 10/11/18 15:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite 365.1 Phosphorus, Total Phosphorus 420.4 Phenolics, Total Phenol 5220D COD Chemical Oxygen Demand Date: 10/19/2018 07:48 AM Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 ND mg/L 0.50 1 10/14/18 14:41 10/16/18 00:28 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 0.29 mg/L 0.020 1 10/12/18 08:02 0.29 mg/L 0.020 1 10/12/18 08:02 14797-55-8 ND mg/L 0.020 1 10/12/18 08:02 14797-65-0 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 0.084 mg/L 0.050 1 10/12/18 18:30 10/12/18 23:08 7723-14-0 Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993 ND mg/L 0.010 1 10/17/1818:31 10/18/1818:31 108-95-2 BC Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 ND mg/L 25.0 1 10/12/18 18:03 10/12/18 21:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436679 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200E MSV Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2402294 Associated Lab Samples: 92403169001, 92403169002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/17/18 15:10 1,1,1-Trichloroethane ug/L ND 0.50 10/17/18 15:10 1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/17/18 15:10 1,1,2-Trichloroethane ug/L ND 0.50 10/17/18 15:10 1,1-Dichloroethane ug/L ND 0.50 10/17/18 15:10 1,1-Dichloroethene ug/L ND 0.50 10/17/18 15:10 1,1-Dichloropropene ug/L ND 0.50 10/17/18 15:10 1,2,3-Trichlorobenzene ug/L ND 2.0 10/17/18 15:10 1,2,3-Trichloropropane ug/L ND 0.50 10/17/18 15:10 1,2,4-Trichlorobenzene ug/L ND 2.0 10/17/18 15:10 1,2,4-Trimethylbenzene ug/L ND 0.50 10/17/18 15:10 1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/17/18 15:10 1,2-Dibromoethane (EDB) ug/L ND 0.50 10/17/18 15:10 1,2-Dichlorobenzene ug/L ND 0.50 10/17/18 15:10 1,2-Dichloroethane ug/L ND 0.50 10/17/18 15:10 1,2-Dichloropropane ug/L ND 0.50 10/17/18 15:10 1,3,5-Trimethylbenzene ug/L ND 0.50 10/17/18 15:10 1,3-Dichlorobenzene ug/L ND 0.50 10/17/18 15:10 1,3-Dichloropropane ug/L ND 0.50 10/17/18 15:10 1,4-Dichlorobenzene ug/L ND 0.50 10/17/18 15:10 2,2-Dichloropropane ug/L ND 0.50 10/17/18 15:10 2-Chlorotoluene ug/L ND 0.50 10/17/18 15:10 4-Chlorotoluene ug/L ND 0.50 10/17/18 15:10 Benzene ug/L ND 0.50 10/17/18 15:10 Bromobenzene ug/L ND 0.50 10/17/18 15:10 Bromochloromethane ug/L ND 0.50 10/17/18 15:10 Bromodichloromethane ug/L ND 0.50 10/17/18 15:10 Bromoform ug/L ND 0.50 10/17/18 15:10 Bromomethane ug/L ND 5.0 10/17/18 15:10 Carbon tetrachloride ug/L ND 0.50 10/17/18 15:10 Chlorobenzene ug/L ND 0.50 10/17/18 15:10 Chloroethane ug/L ND 1.0 10/17/18 15:10 Chloroform ug/L ND 0.50 10/17/18 15:10 Chloromethane ug/L ND 1.0 10/17/18 15:10 cis-1,2-Dichloroethene ug/L ND 0.50 10/17/18 15:10 cis-1,3-Dichloropropene ug/L ND 0.50 10/17/18 15:10 Dibromochloromethane ug/L ND 0.50 10/17/18 15:10 Dibromomethane ug/L ND 0.50 10/17/18 15:10 Dichlorodifluoromethane ug/L ND 0.50 10/17/18 15:10 Diisopropyl ether ug/L ND 0.50 10/17/18 15:10 Ethylbenzene ug/L ND 0.50 10/17/18 15:10 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 METHOD BLANK: 2402294 Associated Lab Samples: 92403169001, 92403169002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Hexachloro-1,3-butadiene ug/L ND 2.0 10/17/18 15:10 Isopropylbenzene (Cumene) ug/L ND 0.50 10/17/18 15:10 m&p-Xylene ug/L ND 1.0 10/17/18 15:10 Methyl-tert-butyl ether ug/L ND 0.50 10/17/18 15:10 Methylene Chloride ug/L ND 2.0 10/17/18 15:10 n-Butylbenzene ug/L ND 0.50 10/17/18 15:10 n-Propylbenzene ug/L ND 0.50 10/17/18 15:10 Naphthalene ug/L ND 2.0 10/17/18 15:10 o-Xylene ug/L ND 0.50 10/17/18 15:10 sec-Butylbenzene ug/L ND 0.50 10/17/18 15:10 Styrene ug/L ND 0.50 10/17/18 15:10 tert-Butyl benzene ug/L ND 0.50 10/17/18 15:10 Tetrachloroethene ug/L ND 0.50 10/17/18 15:10 Toluene ug/L ND 0.50 10/17/18 15:10 trans-1,2-Dichloroethene ug/L ND 0.50 10/17/18 15:10 trans- 1,3-Dichloropropene ug/L ND 0.50 10/17/18 15:10 Trichloroethene ug/L ND 0.50 10/17/18 15:10 Trichlorofluoromethane ug/L ND 1.0 10/17/18 15:10 Vinyl chloride ug/L ND 1.0 10/17/18 15:10 1,2-Dichloroethane-d4 (S) % 95 70-130 10/17/18 15:10 4-Bromofluorobenzene (S) % 95 70-130 10/17/18 15:10 Toluene-d8 (S) % 100 70-130 10/17/18 15:10 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2402295 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.0 98 60-140 1,1,1-Trichloroethane ug/L 50 44.8 90 60-140 1,1,2,2-Tetrachloroethane ug/L 50 47.5 95 60-140 1,1,2-Trichloroethane ug/L 50 48.3 97 60-140 1,1-Dichloroethane ug/L 50 43.6 87 60-140 1,1-Dichloroethene ug/L 50 45.8 92 60-140 1,1-Dichloropropene ug/L 50 47.3 95 60-140 1,2,3-Trichlorobenzene ug/L 50 49.6 99 60-140 1,2,3-Trichloropropane ug/L 50 51.5 103 60-140 1,2,4-Trichlorobenzene ug/L 50 50.9 102 60-140 1,2,4-Trimethylbenzene ug/L 50 47.1 94 60-140 1,2-Dibromo-3-chloropropane ug/L 50 48.3 97 60-140 1,2-Dibromoethane (EDB) ug/L 50 50.9 102 60-140 1,2-Dichlorobenzene ug/L 50 51.1 102 60-140 1,2-Dichloroethane ug/L 50 47.0 94 60-140 1,2-Dichloropropane ug/L 50 48.0 96 60-140 1,3,5-Trimethylbenzene ug/L 50 47.2 94 60-140 1,3-Dichlorobenzene ug/L 50 49.8 100 60-140 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 LABORATORY CONTROL SAMPLE: Parameter 2402295 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichloropropane ug/L 50 51.7 103 60-140 1,4-Dichlorobenzene ug/L 50 49.7 99 60-140 2,2-Dichloropropane ug/L 50 46.8 94 60-140 2-Chlorotoluene ug/L 50 46.5 93 60-140 4-Chlorotoluene ug/L 50 47.5 95 60-140 Benzene ug/L 50 47.4 95 60-140 Bromobenzene ug/L 50 50.2 100 60-140 Bromochloromethane ug/L 50 53.9 108 60-140 Bromodichloromethane ug/L 50 46.5 93 60-140 Bromoform ug/L 50 49.6 99 60-140 Bromomethane ug/L 50 39.2 78 60-140 Carbon tetrachloride ug/L 50 48.4 97 60-140 Chlorobenzene ug/L 50 49.9 100 60-140 Chloroethane ug/L 50 38.9 78 60-140 Chloroform ug/L 50 50.8 102 60-140 Chloromethane ug/L 50 35.9 72 60-140 cis-1,2-Dichloroethene ug/L 50 45.4 91 60-140 cis-1,3-Dichloropropene ug/L 50 50.1 100 60-140 Dibromochloromethane ug/L 50 52.3 105 60-140 Dibromomethane ug/L 50 52.8 106 60-140 Dichlorodifluoromethane ug/L 50 41.9 84 60-140 Diisopropyl ether ug/L 50 43.7 87 60-140 Ethylbenzene ug/L 50 47.6 95 60-140 Hexachloro-1,3-butadiene ug/L 50 46.6 93 60-140 Isopropylbenzene (Cumene) ug/L 50 49.9 100 60-140 m&p-Xylene ug/L 100 95.2 95 60-140 Methyl-tert-butyl ether ug/L 50 46.2 92 60-140 Methylene Chloride ug/L 50 45.6 91 60-140 n-Butylbenzene ug/L 50 48.7 97 60-140 n-Propylbenzene ug/L 50 47.3 95 60-140 Naphthalene ug/L 50 50.9 102 60-140 o-Xylene ug/L 50 49.6 99 60-140 sec-Butylbenzene ug/L 50 47.9 96 60-140 Styrene ug/L 50 48.9 98 60-140 tert-Butyl benzene ug/L 50 42.1 84 60-140 Tetrachloroethene ug/L 50 47.3 95 60-140 Toluene ug/L 50 44.8 90 60-140 trans-1,2-Dichloroethene ug/L 50 45.8 92 60-140 trans- 1,3-Dichloropropene ug/L 50 47.1 94 60-140 Trichloroethene ug/L 50 50.0 100 60-140 Trichlorofluoromethane ug/L 50 44.3 89 60-140 Vinyl chloride ug/L 50 46.7 93 60-140 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 95 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402296 2402297 MS MSD 92403169001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 20.2 19.9 101 99 60-140 2 1,1,1-Trichloroethane ug/L ND 20 20 18.5 18.5 93 92 60-140 1 1,1,2,2-Tetrachloroethane ug/L ND 20 20 19.6 19.3 98 96 60-140 2 1,1,2-Trichloroethane ug/L ND 20 20 19.0 18.9 95 95 60-140 1 1,1-Dichloroethane ug/L ND 20 20 18.2 17.9 91 90 60-140 2 1,1-Dichloroethene ug/L ND 20 20 18.9 19.4 95 97 60-140 2 1,1-Dichloropropene ug/L ND 20 20 19.5 19.3 97 97 60-140 1 1,2,3-Trichlorobenzene ug/L ND 20 20 17.8 18.7 89 93 60-140 5 1,2,3-Trichloropropane ug/L ND 20 20 20.2 20.6 101 103 60-140 2 1,2,4-Trichlorobenzene ug/L ND 20 20 18.6 19.5 93 97 60-140 4 1,2,4-Trimethylbenzene ug/L ND 20 20 18.5 18.8 92 94 60-140 2 1,2-Dibromo-3-chloropropane ug/L ND 20 20 18.0 18.6 90 93 60-140 3 1,2-Dibromoethane (EDB) ug/L ND 20 20 19.9 20.6 100 103 60-140 3 1,2-Dichlorobenzene ug/L ND 20 20 19.4 20.1 97 101 60-140 4 1,2-Dichloroethane ug/L ND 20 20 19.3 18.5 97 93 60-140 4 1,2-Dichloropropane ug/L ND 20 20 19.5 19.7 98 98 60-140 1 1,3,5-Trimethylbenzene ug/L ND 20 20 18.5 18.9 93 95 60-140 2 1,3-Dichlorobenzene ug/L ND 20 20 19.3 19.3 96 97 60-140 0 1,3-Dichloropropane ug/L ND 20 20 21.0 21.0 105 105 60-140 0 1,4-Dichlorobenzene ug/L ND 20 20 19.2 19.5 96 97 60-140 1 2,2-Dichloropropane ug/L ND 20 20 16.3 16.3 81 81 60-140 0 2-Chlorotoluene ug/L ND 20 20 18.3 18.7 92 93 60-140 2 4-Chlorotoluene ug/L ND 20 20 18.3 19.0 92 95 60-140 4 Benzene ug/L ND 20 20 19.5 19.1 98 96 60-140 2 Bromobenzene ug/L ND 20 20 19.9 20.4 100 102 60-140 2 Bromochloromethane ug/L ND 20 20 21.9 21.1 109 106 60-140 3 Bromodichloromethane ug/L ND 20 20 18.4 18.7 92 93 60-140 1 Bromoform ug/L ND 20 20 18.8 18.6 94 93 60-140 1 Bromomethane ug/L ND 20 20 14.2 14.1 71 71 60-140 0 Carbon tetrachloride ug/L ND 20 20 20.4 20.1 102 101 60-140 1 Chlorobenzene ug/L ND 20 20 20.7 19.9 103 99 60-140 4 Chloroethane ug/L ND 20 20 17.7 17.1 89 86 60-140 4 Chloroform ug/L ND 20 20 20.0 19.9 100 100 60-140 0 Chloromethane ug/L ND 20 20 15.1 15.1 75 75 60-140 0 cis-1,2-Dichloroethene ug/L ND 20 20 18.4 18.6 92 93 60-140 1 cis-1,3-Dichloropropene ug/L ND 20 20 19.3 19.0 96 95 60-140 1 Dibromochloromethane ug/L ND 20 20 19.9 19.9 99 100 60-140 0 Dibromomethane ug/L ND 20 20 21.3 21.5 106 108 60-140 1 Dichlorodifluoromethane ug/L ND 20 20 19.0 18.5 95 93 60-140 2 Diisopropyl ether ug/L ND 20 20 17.6 17.6 88 88 60-140 0 Ethylbenzene ug/L ND 20 20 19.7 19.6 98 98 60-140 1 Hexachloro-1,3-butadiene ug/L ND 20 20 17.2 17.9 86 90 60-140 4 Isopropylbenzene (Cumene) ug/L ND 20 20 20.7 20.2 103 101 60-140 2 m&p-Xylene ug/L ND 40 40 39.7 38.9 99 97 60-140 2 Methyl-tert-butyl ether ug/L ND 20 20 18.6 18.4 93 92 60-140 1 Methylene Chloride ug/L ND 20 20 16.6 16.4 83 82 60-140 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402296 2402297 MS MSD 92403169001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual n-Butylbenzene ug/L ND 20 20 18.4 19.0 92 95 60-140 3 n-Propylbenzene ug/L ND 20 20 18.8 19.1 94 95 60-140 1 Naphthalene ug/L ND 20 20 18.0 18.8 90 94 60-140 4 o-Xylene ug/L ND 20 20 20.4 20.2 102 101 60-140 1 sec-Butylbenzene ug/L ND 20 20 19.0 19.5 95 98 60-140 3 Styrene ug/L ND 20 20 19.5 19.5 98 97 60-140 0 tert-Butyl benzene ug/L ND 20 20 16.6 16.8 83 84 60-140 1 Tetrachloroethene ug/L ND 20 20 19.4 19.5 97 98 60-140 1 Toluene ug/L ND 20 20 19.0 18.4 95 92 60-140 3 trans-1,2-Dichloroethene ug/L ND 20 20 19.4 19.2 97 96 60-140 1 trans- 1,3-Dichloropropene ug/L ND 20 20 17.8 18.1 89 90 60-140 2 Trichloroethene ug/L ND 20 20 21.0 20.2 105 101 60-140 4 Trichlorofluoromethane ug/L ND 20 20 20.0 19.6 100 98 60-140 2 Vinyl chloride ug/L ND 20 20 19.5 19.7 97 99 60-140 1 1,2-Dichloroethane-d4 (S) % 95 95 70-130 4-Bromofluorobenzene (S) % 100 96 70-130 Toluene-d8(S) % 98 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 435901 Analysis Method: EPA 625.1 QC Batch Method: EPA 625.1 Analysis Description: 625 MSS Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2398861 Associated Lab Samples: 92403169001, 92403169002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 5.0 10/15/18 15:43 2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 10/15/18 15:43 2,4,6-Trichlorophenol ug/L ND 10.0 10/15/18 15:43 2,4-Dichlorophenol ug/L ND 5.0 10/15/18 15:43 2,4-Dimethylphenol ug/L ND 10.0 10/15/18 15:43 2,4-Dinitrophenol ug/L ND 50.0 10/15/18 15:43 2,4-Dinitrotoluene ug/L ND 5.0 10/15/18 15:43 2,6-Dinitrotoluene ug/L ND 5.0 10/15/18 15:43 2-Chloronaphthalene ug/L ND 5.0 10/15/18 15:43 2-Chlorophenol ug/L ND 5.0 10/15/18 15:43 2-Nitrophenol ug/L ND 5.0 10/15/18 15:43 3,3'-Dichlorobenzidine ug/L ND 25.0 10/15/18 15:43 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 10/15/18 15:43 4-Bromophenylphenyl ether ug/L ND 5.0 10/15/18 15:43 4-Chloro-3-methylphenol ug/L ND 5.0 10/15/18 15:43 4-Chlorophenylphenyl ether ug/L ND 5.0 10/15/18 15:43 4-Nitrophenol ug/L ND 50.0 10/15/18 15:43 Acenaphthene ug/L ND 5.0 10/15/18 15:43 Acenaphthylene ug/L ND 5.0 10/15/18 15:43 Anthracene ug/L ND 5.0 10/15/18 15:43 Benzo(a)anthracene ug/L ND 5.0 10/15/18 15:43 Benzo(a)pyrene ug/L ND 5.0 10/15/18 15:43 Benzo(b)fluoranthene ug/L ND 5.0 10/15/18 15:43 Benzo(g,h,i)perylene ug/L ND 5.0 10/15/18 15:43 Benzo(k)fluoranthene ug/L ND 5.0 10/15/18 15:43 bis(2-Chloroethoxy)methane ug/L ND 10.0 10/15/18 15:43 bis(2-Chloroethyl) ether ug/L ND 5.0 10/15/18 15:43 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 10/15/18 15:43 Butylbenzylphthalate ug/L ND 5.0 10/15/18 15:43 Chrysene ug/L ND 5.0 10/15/18 15:43 Di-n-butylphthalate ug/L ND 5.0 10/15/18 15:43 Di-n-octylphthalate ug/L ND 5.0 10/15/18 15:43 Dibenz(a,h)anthracene ug/L ND 5.0 10/15/18 15:43 Diethylphthalate ug/L ND 5.0 10/15/18 15:43 Dimethylphthalate ug/L ND 5.0 10/15/18 15:43 Fluoranthene ug/L ND 5.0 10/15/18 15:43 Fluorene ug/L ND 5.0 10/15/18 15:43 Hexachloro-1,3-butadiene ug/L ND 5.0 10/15/18 15:43 Hexachlorobenzene ug/L ND 5.0 10/15/18 15:43 Hexachlorocyclopentadiene ug/L ND 10.0 10/15/18 15:43 Hexachloroethane ug/L ND 5.0 10/15/18 15:43 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 METHOD BLANK: 2398861 Associated Lab Samples: 92403169001, 92403169002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L ND 5.0 10/15/18 15:43 Isophorone ug/L ND 10.0 10/15/18 15:43 N-Nitroso-di-n-propylamine ug/L ND 5.0 10/15/18 15:43 N-Nitrosodimethylamine ug/L ND 5.0 10/15/18 15:43 N-Nitrosodiphenylamine ug/L ND 10.0 10/15/18 15:43 Naphthalene ug/L ND 5.0 10/15/18 15:43 Nitrobenzene ug/L ND 5.0 10/15/18 15:43 Pentachlorophenol ug/L ND 10.0 10/15/18 15:43 Phenanthrene ug/L ND 5.0 10/15/18 15:43 Phenol ug/L ND 5.0 10/15/18 15:43 Pyrene ug/L ND 5.0 10/15/18 15:43 2,4,6-Tribromophenol (S) % 81 10-137 10/15/18 15:43 2-Fluorobiphenyl (S) % 81 15-120 10/15/18 15:43 2-Fluorophenol (S) % 51 10-120 10/15/18 15:43 Nitrobenzene-d5 (S) % 80 10-120 10/15/18 15:43 Phenol-d6 (S) % 34 10-120 10/15/18 15:43 Terphenyl-d14 (S) % 112 11-131 10/15/18 15:43 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2398862 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/L 50 39.0 78 44-142 2,2'-Oxybis(1-chloropropane) ug/L 50 46.8 94 36-166 2,4,6-Trichlorophenol ug/L 50 48.4 97 37-144 2,4-Dichlorophenol ug/L 50 47.4 95 39-135 2,4-Dimethylphenol ug/L 50 50.7 101 32-120 2,4-Dinitrophenol ug/L 250 259 104 1-191 2,4-Dinitrotoluene ug/L 50 51.4 103 39-139 2,6-Dinitrotoluene ug/L 50 52.0 104 50-158 2-Chloronaphthalene ug/L 50 44.5 89 60-120 2-Chlorophenol ug/L 50 45.2 90 23-134 2-Nitrophenol ug/L 50 44.6 89 29-181 3,3'-Dichlorobenzidine ug/L 100 92.0 92 1-262 4,6-Dinitro-2-methyl phenol ug/L 100 112 112 1-181 4-Bromophenylphenyl ether ug/L 50 51.2 102 53-127 4-ChIoro-3-methyl phenol ug/L 100 92.4 92 22-147 4-Chlorophenylphenyl ether ug/L 50 47.8 96 25-158 4-Nitrophenol ug/L 250 113 45 1-132 Acenaphthene ug/L 50 48.8 98 47-145 Acenaphthylene ug/L 50 48.7 97 33-145 Anthracene ug/L 50 52.4 105 27-133 Benzo(a)anthracene ug/L 50 51.0 102 33-143 Benzo(a)pyrene ug/L 50 54.6 109 17-163 Benzo(b)fluoranthene ug/L 50 52.4 105 24-159 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 LABORATORY CONTROL SAMPLE: 2398862 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(g,h,i)perylene ug/L 50 56.0 112 1-219 Benzo(k)fluoranthene ug/L 50 56.2 112 11-162 bis(2-Chloroethoxy)methane ug/L 50 50.4 101 33-184 bis(2-Chloroethyl) ether ug/L 50 47.6 95 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 46.8 94 8-158 Butylbenzylphthalate ug/L 50 47.0 94 1-152 Chrysene ug/L 50 51.5 103 17-168 Di-n-butylphthalate ug/L 50 46.7 93 1-120 Di-n-octylphthalate ug/L 50 47.4 95 4-146 Dibenz(a,h)anthracene ug/L 50 55.5 111 1-227 Diethylphthalate ug/L 50 44.8 90 1-120 Dimethylphthalate ug/L 50 44.9 90 1-120 Fluoranthene ug/L 50 50.0 100 26-137 Fluorene ug/L 50 49.0 98 59-121 Hexachloro-1,3-butadiene ug/L 50 36.4 73 24-120 Hexachlorobenzene ug/L 50 48.9 98 1-152 Hexachlorocyclopentadiene ug/L 50 41.0 82 25-150 Hexachloroethane ug/L 50 36.4 73 40-120 Indeno(1,2,3-cd)pyrene ug/L 50 56.6 113 1-171 Isophorone ug/L 50 41.0 82 21-196 N-Nitroso-di-n-propylamine ug/L 50 47.5 95 1-230 N-Nitrosodimethylamine ug/L 50 38.8 78 25-150 N-Nitrosodiphenylamine ug/L 50 51.0 102 25-150 Naphthalene ug/L 50 42.8 86 21-133 Nitrobenzene ug/L 50 45.5 91 35-180 Pentachlorophenol ug/L 100 98.6 99 14-176 Phenanthrene ug/L 50 52.2 104 54-120 Phenol ug/L 50 21.1 42 5-120 Pyrene ug/L 50 53.0 106 52-120 2,4,6-Tribromophenol (S) % 100 10-137 2-Fluorobiphenyl (S) % 89 15-120 2-Fluorophenol (S) % 59 10-120 Nitrobenzene-d5 (S) % 92 10-120 Phenol-d6 (S) % 40 10-120 Terphenyl-d14 (S) % 116 11-131 MATRIX SPIKE SAMPLE: 2398863 92402922002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L ND 49 40.3 82 44-142 2,2'-Oxybis(1-chloropropane) ug/L ND 49 43.5 89 36-166 2,4,6-Trichlorophenol ug/L ND 49 46.8 95 37-144 2,4-Dichlorophenol ug/L ND 49 44.5 91 39-135 2,4-Dimethylphenol ug/L ND 49 47.2 96 32-120 2,4-Dinitrophenol ug/L ND 245 228 93 1-191 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 MATRIX SPIKE SAMPLE: 2398863 92402922002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2,4-Dinitrotoluene ug/L ND 49 48.4 99 39-139 2,6-Dinitrotoluene ug/L ND 49 49.6 101 50-158 2-Chloronaphthalene ug/L ND 49 44.5 91 60-120 2-Chlorophenol ug/L ND 49 43.1 88 23-134 2-Nitrophenol ug/L ND 49 45.1 92 29-182 3,3'-Dichlorobenzidine ug/L ND 98 99.4 101 1-262 4,6-Dinitro-2-methyl phenol ug/L ND 98 100 102 1-181 4-Bromophenylphenyl ether ug/L ND 49 45.8 93 53-127 4-Chloro-3-methylphenol ug/L ND 98 87.9 90 22-147 4-Chlorophenylphenyl ether ug/L ND 49 46.6 95 25-158 4-Nitrophenol ug/L ND 245 103 42 1-132 Acenaphthene ug/L ND 49 45.0 92 47-145 Acenaphthylene ug/L ND 49 45.1 92 33-145 Anthracene ug/L ND 49 46.6 95 27-133 Benzo(a)anthracene ug/L ND 49 48.5 99 33-143 Benzo(a)pyrene ug/L ND 49 48.0 98 17-163 Benzo(b)fluoranthene ug/L ND 49 49.0 100 24-159 Benzo(g,h,i)perylene ug/L ND 49 48.9 100 1-219 Benzo(k)fluoranthene ug/L ND 49 47.1 96 11-162 bis(2-Chloroethoxy)methane ug/L ND 49 47.4 97 33-184 bis(2-Chloroethyl) ether ug/L ND 49 43.8 89 12-158 bis(2-Ethylhexyl)phthalate ug/L ND 49 46.0 94 8-158 Butylbenzylphthalate ug/L ND 49 45.0 92 1-152 Chrysene ug/L ND 49 46.9 96 17-168 Di-n-butylphthalate ug/L ND 49 42.1 86 1-120 Di-n-octylphthalate ug/L ND 49 51.7 106 4-146 Dibenz(a,h)anthracene ug/L ND 49 50.0 102 1-227 Diethylphthalate ug/L ND 49 41.2 84 1-120 Dimethylphthalate ug/L ND 49 41.6 85 1-120 Fluoranthene ug/L ND 49 46.3 94 26-137 Fluorene ug/L ND 49 46.9 96 59-121 Hexachloro-1,3-butadiene ug/L ND 49 38.5 78 24-120 Hexachlorobenzene ug/L ND 49 43.5 89 1-152 Hexachlorocyclopentadiene ug/L ND 49 41.4 84 25-150 Hexachloroethane ug/L ND 49 38.0 77 40-120 Indeno(1,2,3-cd)pyrene ug/L ND 49 49.2 100 1-171 Isophorone ug/L ND 49 39.4 80 21-196 N-Nitroso-di-n-propylamine ug/L ND 49 43.1 88 1-230 N-Nitrosodimethylamine ug/L ND 49 36.4 74 25-150 N-Nitrosodiphenylamine ug/L ND 49 43.3 88 25-150 Naphthalene ug/L ND 49 42.1 86 21-133 Nitrobenzene ug/L ND 49 42.3 86 35-180 Pentachlorophenol ug/L ND 98 59.5 61 14-176 Phenanthrene ug/L ND 49 46.3 94 54-120 Phenol ug/L ND 49 18.4 38 5-120 Pyrene ug/L ND 49 44.7 91 52-120 2,4,6-Tribromophenol (S) % 93 10-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 MATRIX SPIKE SAMPLE: 2398863 92402922002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Fluorobiphenyl (S) % 91 15-120 2-Fluorophenol(S) % 57 10-120 Nitrobenzene-d5 (S) % 89 10-120 Phenol-d6 (S) % 37 10-120 Terphenyl-d14 (S) % 105 11-131 SAMPLE DUPLICATE: 2398864 Parameter Units 92403074001 Result Dup Result 1,2,4-Trichlorobenzene ug/L ND ND 2,2'-Oxybis(1-chloropropane) ug/L ND ND 2,4,6-Trichlorophenol ug/L ND ND 2,4-Dichlorophenol ug/L ND ND 2,4-Dimethylphenol ug/L ND ND 2,4-Dinitrophenol ug/L ND ND 2,4-Dinitrotoluene ug/L ND ND 2,6-Dinitrotoluene ug/L ND ND 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Nitrophenol ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 4,6-Dinitro-2-methyl phenol ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-methylphenol ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitrophenol ug/L ND ND Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Anthracene ug/L ND ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND ND Chrysene ug/L ND ND Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Diethylphthalate ug/L ND ND Dimethylphthalate ug/L ND ND Fluoranthene ug/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 SAMPLE DUPLICATE: 2398864 Parameter Units 92403074001 Result Dup Result Fluorene ug/L ND ND Hexachloro-1,3-butadiene ug/L ND ND Hexachlorobenzene ug/L ND ND Hexachlorocyclopentadiene ug/L ND ND Hexachloroethane ug/L ND ND Indeno(1,2,3-cd)pyrene ug/L ND ND Isophorone ug/L ND ND N-Nitroso-di-n-propylamine ug/L ND ND N-Nitrosodimethylamine ug/L ND ND N-Nitrosodiphenylamine ug/L ND ND Naphthalene ug/L ND ND Nitrobenzene ug/L ND ND Pentachlorophenol ug/L ND ND Phenanthrene ug/L ND ND Phenol ug/L ND ND Pyrene ug/L ND ND 2,4,6-Tribromophenol (S) % 71 78 2-Fluorobiphenyl (S) % 57 57 2-Fluorophenol(S) % 34 33 Nitrobenzene-d5 (S) % 60 61 Phenol-d6 (S) % 24 25 Terphenyl-d14 (S) % 100 71 RPD Qualifiers 9 1 6 2 0 35 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436005 Analysis Method: EPA 180.1 Rev 2.0 1993 QC Batch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2399365 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Turbidity NTU ND 1.0 10/12/1815:06 LABORATORY CONTROL SAMPLE: 2399366 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.1 101 90-110 SAMPLE DUPLICATE: 2399367 92403169001 Dup Parameter Units Result Result RPD Qualifiers Turbidity NTU 3.1 3.1 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436094 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2399711 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/13/18 00:51 LABORATORY CONTROL SAMPLE: 2399712 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 242 96 90-110 SAMPLE DUPLICATE: 2399713 92403108002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 2399714 92403275003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 179 206 14 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 435867 Analysis Method: SM 521 OB-2011 QC Batch Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2398785 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 10/17/18 00:57 LABORATORY CONTROL SAMPLE: 2398786 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 189 95 84.6-115 SAMPLE DUPLICATE: 2398788 92403102001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 312 318 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436234 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92403169001, 92403169002 SAMPLE DUPLICATE: 2400364 92403158001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.4 6.4 0 H3 SAMPLE DUPLICATE: 2400365 92403134003 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.2 6.2 0 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436155 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Associated Lab Samples: 92403169001 METHOD BLANK: 2399897 Matrix: Water Associated Lab Samples: 92403169001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 10/15/18 10:20 LABORATORY CONTROL SAMPLE: 2399898 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399899 2399900 MS MSD 92402667002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 4.8 5 5 9.7 9.7 99 98 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399901 2399902 MS MSD 92402721003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 1.2 5 5 6.6 6.6 108 108 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436156 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Associated Lab Samples: 92403169002 METHOD BLANK: 2399903 Matrix: Water Associated Lab Samples: 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 10/15/18 11:12 LABORATORY CONTROL SAMPLE: 2399904 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.3 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399905 2399906 MS MSD 92403169002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.4 5.4 108 108 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399907 2399908 MS MSD 92402682001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.30 5 5 5.7 5.7 107 108 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436147 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2399871 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/16/18 00:22 LABORATORY CONTROL SAMPLE: 2399872 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.7 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399873 2399874 MS MSD 92403169001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 9.7 10.2 93 98 90-110 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 435870 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2398790 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.020 10/12/18 07:54 Nitrogen, Nitrite mg/L ND 0.020 10/12/18 07:54 Nitrogen, NO2 plus NO3 mg/L ND 0.020 10/12/18 07:54 LABORATORY CONTROL SAMPLE: 2398791 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.6 107 90-110 Nitrogen, Nitrite mg/L 1 1.0 104 90-110 Nitrogen, NO2 plus NO3 mg/L 2.5 2.7 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2398792 2398793 MS MSD 92403038001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 4.2 1.5 1.5 6.1 6.2 122 130 90-110 2 Nitrogen, Nitrite mg/L ND 1 1 1.2 1.2 114 115 90-110 1 M1 Nitrogen, NO2 plus NO3 mg/L 4.2 2.5 2.5 7.2 7.4 119 125 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436037 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2399557 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 10/12/18 22:48 LABORATORY CONTROL SAMPLE: 2399558 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.7 107 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399559 2399560 MS MSD 92402990001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.7 2.7 107 108 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399561 2399562 MS MSD 92402990011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.10 2.5 2.5 2.8 2.6 108 99 90-110 9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436643 Analysis Method: EPA 420.4 Rev 1.0 1993 QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2402213 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phenol mg/L ND 0.010 10/18/1818:18 BC LABORATORY CONTROL SAMPLE: 2402214 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenol mg/L .05 0.049 97 90-110 BC MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402215 2402216 MS MSD 92403074001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenol mg/L 0.0093J .05 .05 0.076 0.074 133 130 90-110 2 BC,M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402217 2402218 MS MSD 92403169001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenol mg/L 0.012 .05 .05 0.083 0.082 143 140 90-110 2 BC,M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries 10/11 Pace Project No.: 92403169 QC Batch: 436048 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92403169001, 92403169002 METHOD BLANK: 2399595 Matrix: Water Associated Lab Samples: 92403169001, 92403169002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 10/12/18 20:57 LABORATORY CONTROL SAMPLE: 2399596 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 762 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399597 2399598 MS MSD 92402959003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 127 130 103 105 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399599 2399600 MS MSD 92403126003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 38.4 100 100 155 153 116 114 90-110 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 38 Pace Analytical Services, LLC ceAnalX cal ® hevi Riverside 04 Asheville, NC 28804 www.pacelabs.com (828)254-7176 QUALIFIERS Project: Powell Industries 10/11 Pace Project No.: 92403169 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 07:48 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 38 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Powell Industries 10/11 92403169 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92403169001 SW-01 EPA 625.1 435901 EPA 625.1 436134 92403169002 SW-02 EPA 625.1 435901 EPA 625.1 436134 92403169001 SW-01 SM 6200E 436679 92403169002 SW-02 SM 6200E 436679 92403169001 SW-01 EPA 180.1 Rev 2.0 1993 436005 92403169002 SW-02 EPA 180.1 Rev 2.0 1993 436005 92403169001 SW-01 SM 2540D-2011 436094 92403169002 SW-02 SM 2540D-2011 436094 92403169001 SW-01 SM 5210E-2011 435867 SM 5210B-2011 435887 92403169002 SW-02 SM 5210E-2011 435867 SM 5210B-2011 435887 92403169001 SW-01 EPA 9040C 436234 92403169002 SW-02 EPA 9040C 436234 92403169001 SW-01 EPA 350.1 Rev 2.0 1993 436155 92403169002 SW-02 EPA 350.1 Rev 2.0 1993 436156 92403169001 SW-01 EPA 351.2 Rev 2.0 1993 436147 EPA 351.2 Rev 2.0 1993 436329 92403169002 SW-02 EPA 351.2 Rev 2.0 1993 436147 EPA 351.2 Rev 2.0 1993 436329 92403169001 SW-01 EPA 353.2 Rev 2.0 1993 435870 92403169002 SW-02 EPA 353.2 Rev 2.0 1993 435870 92403169001 SW-01 EPA 365.1 Rev 2.0 1993 436037 EPA 365.1 Rev 2.0 1993 436079 92403169002 SW-02 EPA 365.1 Rev 2.0 1993 436037 EPA 365.1 Rev 2.0 1993 436079 92403169001 SW-01 EPA 420.4 Rev 1.0 1993 436643 EPA 420.4 Rev 1.0 1993 437038 92403169002 SW-02 EPA 420.4 Rev 1.0 1993 436643 EPA 420.4 Rev 1.0 1993 437038 92403169001 SW-01 SM 5220D-2011 436048 SM 5220D-2011 436083 92403169002 SW-02 SM 5220D-2011 436048 SM 5220D-2011 436083 Date: 10/19/2018 07:48 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 38 c7GEAIJciIj/CICc?i Document Name: Sample Condition Upon Receipt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples: Asheville [ / Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Sample Condition Client Name: Upon Receipt IYJ Project Courier: ❑Fed Ex ❑UPS ❑USPS lient ❑ Commercial ❑Pace []other: — Custody Seal Present? Yes ❑No Seals Intact? 3r,, [:]No WO#:92403169 111111111111111 IIIIIIIII Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap E3Bubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermome-tter: []Yes❑No DN/A Type of ❑GUet []Blue []None IR Gun ID: Cooler Temp (°C): j . '� Correction Factor: Add/Subtract (°C) r Temp should be above freezing to 6°C Cooler Temp Corrected (°C): `Z� ' []samples out of temp Criteria. Samples on ice, cooling process has begun USDA Regulated Soil (E�rN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {Internationally, ❑Yes ❑No including Hawaiienu rUUrLV R:Lu): u.— u •v Comments/Discrepancy: Chain of Custody Present? E Yeses ❑No ❑N/A 1. Samples Arrived within Hold Time? ❑No El N/A 2. Short Hold Time Analysis (<72 hr.)? Doves Pfyes []No ❑N/A 3. ItyC4CS BOD,LY• 17 . Rush Turn Around Time Requested? ❑Yes o ❑N/A 4. Sufficient Volume? [--fifes ❑No ❑N/A 5. Correct Containers Used? ( ❑N❑ ❑N/A 6. -Pace Containers Used? r/�es ❑ND [:]N/A Containers Intact? __ )ales ❑N❑ ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No ETN/A 8. Sample Labels Match COC? es ❑No ❑N/A i 9. W -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? ❑Yes [31Io ❑N/A 10. Trip Blank Present? ❑Yes o ❑N/A 11. Trip Blank Custody Seals Present? [-]Yes []No EJ'N/A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? ❑Yes ❑No Lot ID of split containers: Date: ! S 3 Date: Page 36 of 38 Document Name: Document Revised: February 7, 2018 /j / 2aceAnapical' Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project ' Wo# : 92403169 PM: UPDue Date: 10/18/18 CLIENT: 93-Martin&$1 It E a u a Z 2 a v Ln r-� S m ¢ Z m a V 0 Ln M 6 m Z v rya 0 O N 6 m a v a '.. a !Y r-i .i 6 m x a +n ,Nj 6 m N v o Z U J 0 M 6 m o Z m q N ui a CL m _a Q Z J Ln 6 m m m a ro n E a Z v Q E Q - ti L7 4 N 2 E Q 1-4 C7 4 U z -0 a)v = E q J E o N M l7 a w Q Q = E Q m - rl Q a N = ° N ¢ J E a M f7 a u y Z E J O ni 1 m l7 M W a Z V q > E a O ID Q a Z p N q 0 > E pV' a% l7 > 2 C 4 i E o C 0 J > ¢ C rrl 2 > E ° V m 0 O ¢ z m 0 •+ c. N v Q 0 > z „ = Q. a N m 5 M U > q 2 u N d in E tin u1 a u. I ¢ Z N 0] sa+ in J E o Ln N 6 vt m It to ry 2 V ra a J E Q M 6 m ¢ -0 (Ua� n C d 1 of o l7 a Q ? 'S f0 c ,i E 0 V1 > m C E a 0 G 2 Z 2 X"' ,' u 3 4 S 6 7 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 4 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification ottice (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 37 of 38 m nmm a0 cn N ca ca -4 al w a w ry + ITEM # c °�_. x _ y m CO ro m o m p I n o C w v y ; ET N 3 o G San m n e �y r+ T - a m m ri a m_ o 3 7 3 m z m lac ❑ X v v v n a -- a N C n N m m 0 o 1 m aZi w 0 v MATRIX CODE (see valid codas 40lefl} C a T Z SAMPLE TYPE (G=GRAB C=CCMP) C o _ rA m �E m g o m T Cn iJ m' [n 3 r '* m Z z In Z o z m 1 ❑ rn AB m a 9 m w. - -q-I m m C1 zv ° V W a Y CA {` o 9 v m m ,imp A > SAMPLE TEMP AT COLLECTION ^• C m w 0 `o #CFCONTAINERS o m 3 m Un reserved p y a D N m m P H2SQ4 m m m Cf a # m m w HNO3 b HCl A 0 m a NaOH v Na2S203 C N m y Methanol m 3 ; m Other N :0! r n m Analyses Test YIN TSS a a pH by 9040 re m z �, -F Phenol Total � o o 3 VOC 6200 a SVOA 625 a AmmonlaITKN N c °a m z",y m - V Nitrate or Nitrite C Boo 5-day Coo 1TP z ` Turbidily 3 m to a to TEMP in C y 1°fD Lp Residual Chlorine (Y/N) n °1 m a c w Received on Ice v ~!� T n (YIN) m p fJ -. o > m n usto y Sealed a Cooler S O WN z m Q, r' Samples Intact ' < (Y)N) Page 38 of 38 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 February 21, 2019 Mr. Robert Martin Martin and Slagle 24 Lookout Terrace Black Mountain, NC 28711 RE: Project: Powell Industries Pace Project No.: 92417986 Dear Mr. Martin: Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com 1(828)254-7176 Project Manager Enclosures �pQ AC RFb REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Powell Industries Pace Project No.: 92417986 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Pace Project No.: Powell Industries 92417986 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92417986001 WW-01 EPA 200.7 Rev 4.4 1994 IDS 12 PASI-A EPA 245.1 Rev 3.0 1994 RDT 1 PASI-A EPA 625.1 PKS 58 PASI-C SM 6200B GAW 63 PASI-C EPA 180.1 Rev 2.0 1993 GC 1 PASI-A SM 2540D-2011 MJP 1 PASI-A SM 521OB-2011 MFO 1 PASI-A EPA 9040C SMK 1 PASI-A EPA 350.1 Rev 2.0 1993 NAL 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A EPA420.4 Rev 1.0 1993 DMN 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries Pace Project No.: 92417986 Sample: WW-01 Lab ID: 92417986001 Collected: 02/14/19 14:50 Received: 02/15/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Arsenic ND ug/L 10.0 1 02/16/19 05:15 02/17/19 20:49 7440-38-2 Cadmium ND ug/L 1.0 1 02/16/19 05:15 02/17/19 20:49 7440-43-9 Calcium 28500 ug/L 100 1 02/16/19 05:15 02/17/19 20:49 7440-70-2 Chromium ND ug/L 5.0 1 02/16/19 05:15 02/17/19 20:49 7440-47-3 Copper ND ug/L 5.0 1 02/16/19 05:15 02/17/19 20:49 7440-50-8 Lead ND ug/L 5.0 1 02/16/19 05:15 02/17/19 20:49 7439-92-1 Magnesium 2690 ug/L 100 1 02/16/19 05:15 02/17/19 20:49 7439-95-4 Molybdenum ND ug/L 5.0 1 02/16/19 05:15 02/17/19 20:49 7439-98-7 Nickel ND ug/L 5.0 1 02/16/19 05:15 02/17/19 20:49 7440-02-0 Selenium ND ug/L 10.0 1 02/16/19 05:15 02/17/19 20:49 7782-49-2 Sodium 5350 ug/L 5000 1 02/16/19 05:15 02/17/19 20:49 7440-23-5 Zinc 12.1 ug/L 10.0 1 02/16/19 05:15 02/17/19 20:49 7440-66-6 245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Mercury ND ug/L 0.20 1 02/17/1919:29 02/18/1912:21 7439-97-6 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Acenaphthene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 83-32-9 Acenaphthylene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 208-96-8 Anthracene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 120-12-7 Benzo(a)anthracene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 56-55-3 Benzo(a)pyrene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 50-32-8 Benzo(b)fluoranthene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 205-99-2 Benzo(g,h,i)perylene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 191-24-2 Benzo(k)fluoranthene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 207-08-9 4-Bromophenylphenyl ether ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 101-55-3 Butylbenzylphthalate ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 111-91-1 bis(2-Chloroethyl) ether ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 111-44-4 2-Chloronaphthalene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 91-58-7 2-Chlorophenol ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 95-57-8 4-Chlorophenylphenyl ether ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 7005-72-3 Chrysene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 218-01-9 Dibenz(a,h)anthracene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 53-70-3 3,3'-Dichlorobenzidine ND ug/L 25.0 1 02/19/19 21:57 02/20/19 16:44 91-94-1 2,4-Dichlorophenol ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 120-83-2 Diethylphthalate ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 84-66-2 2,4-Dimethylphenol ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 105-67-9 Dimethylphthalate ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 131-11-3 Di-n-butylphthalate ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 20.0 1 02/19/19 21:57 02/20/19 16:44 534-52-1 2,4-Dinitrophenol ND ug/L 50.0 1 02/19/19 21:57 02/20/19 16:44 51-28-5 2,4-Dinitrotoluene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 121-14-2 2,6-Dinitrotoluene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 606-20-2 Di-n-octylphthalate ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 117-84-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Powell Industries Pace Project No.: 92417986 Sample: WW-01 Parameters ANALYTICAL RESULTS Lab ID: 92417986001 Collected: 02/14/19 14:50 Received: 02/15/19 12:20 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 117-81-7 Fluoranthene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 206-44-0 Fluorene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 87-68-3 Hexachlorobenzene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 77-47-4 Hexachloroethane ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 193-39-5 Isophorone ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 78-59-1 Naphthalene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 91-20-3 Nitrobenzene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 98-95-3 2-Nitrophenol ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 88-75-5 4-Nitrophenol ND ug/L 50.0 1 02/19/19 21:57 02/20/19 16:44 100-02-7 N-Nitrosodimethylamine ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 108-60-1 Pentachlorophenol ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 87-86-5 Phenanthrene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 85-01-8 Phenol ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 108-95-2 Pyrene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 129-00-0 1,2,4-Trichlorobenzene ND ug/L 5.0 1 02/19/19 21:57 02/20/19 16:44 120-82-1 2,4,6-TrichIorophenol ND ug/L 10.0 1 02/19/19 21:57 02/20/19 16:44 88-06-2 Surrogates Nitrobenzene-d5 (S) 67 % 10-120 1 02/19/19 21:57 02/20/19 16:44 4165-60-0 2-Fluorobiphenyl (S) 63 % 15-120 1 02/19/19 21:57 02/20/19 16:44 321-60-8 Terphenyl-d14 (S) 69 % 11-131 1 02/19/19 21:57 02/20/19 16:44 1718-51-0 Phenol-d6 (S) 25 % 10-120 1 02/19/19 21:57 02/20/19 16:44 13127-88-3 2-Fluorophenol (S) 30 % 10-120 1 02/19/19 21:57 02/20/19 16:44 367-12-4 2,4,6-Tribromophenol (S) 67 % 10-137 1 02/19/19 21:57 02/20/19 16:44 118-79-6 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 02/20/1915:56 71-43-2 Bromobenzene ND ug/L 0.50 1 02/20/1915:56 108-86-1 Bromochloromethane ND ug/L 0.50 1 02/20/1915:56 74-97-5 Bromodichloromethane ND ug/L 0.50 1 02/20/1915:56 75-27-4 Bromoform ND ug/L 0.50 1 02/20/1915:56 75-25-2 Bromomethane ND ug/L 5.0 1 02/20/1915:56 74-83-9 n-Butylbenzene ND ug/L 0.50 1 02/20/1915:56 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 02/20/1915:56 135-98-8 tert-Butyl benzene ND ug/L 0.50 1 02/20/1915:56 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 02/20/19 15:56 56-23-5 Chlorobenzene ND ug/L 0.50 1 02/20/1915:56 108-90-7 Chloroethane ND ug/L 1.0 1 02/20/1915:56 75-00-3 Chloroform ND ug/L 0.50 1 02/20/1915:56 67-66-3 Chloromethane ND ug/L 1.0 1 02/20/1915:56 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 02/20/1915:56 95-49-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries Pace Project No.: 92417986 Sample: WW-01 Lab ID: 92417986001 Collected: 02/14/19 14:50 Received: 02/15/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B 4-Chlorotoluene ND ug/L 0.50 1 02/20/19 15:56 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 02/20/19 15:56 96-12-8 Dibromochloromethane ND ug/L 0.50 1 02/20/19 15:56 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 02/20/19 15:56 106-93-4 Dibromomethane ND ug/L 0.50 1 02/20/19 15:56 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 02/20/19 15:56 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 02/20/19 15:56 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 02/20/19 15:56 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 02/20/19 15:56 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 02/20/19 15:56 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 02/20/19 15:56 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 02/20/19 15:56 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 02/20/19 15:56 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 02/20/19 15:56 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 02/20/19 15:56 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 02/20/19 15:56 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 02/20/19 15:56 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 02/20/19 15:56 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 02/20/19 15:56 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 02/20/19 15:56 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 02/20/19 15:56 108-20-3 Ethylbenzene ND ug/L 0.50 1 02/20/19 15:56 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 02/20/19 15:56 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 02/20/19 15:56 98-82-8 Methylene Chloride ND ug/L 2.0 1 02/20/19 15:56 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 02/20/19 15:56 1634-04-4 Naphthalene ND ug/L 2.0 1 02/20/19 15:56 91-20-3 n-Propylbenzene ND ug/L 0.50 1 02/20/19 15:56 103-65-1 Styrene ND ug/L 0.50 1 02/20/19 15:56 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 02/20/19 15:56 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 02/20/19 15:56 79-34-5 Tetrachloroethene ND ug/L 0.50 1 02/20/19 15:56 127-18-4 Toluene ND ug/L 0.50 1 02/20/19 15:56 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 02/20/19 15:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 02/20/19 15:56 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 02/20/19 15:56 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 02/20/19 15:56 79-00-5 Trichloroethene ND ug/L 0.50 1 02/20/19 15:56 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 02/20/19 15:56 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 1 02/20/19 15:56 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 02/20/19 15:56 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 1 02/20/19 15:56 108-67-8 Vinyl chloride ND ug/L 1.0 1 02/20/19 15:56 75-01-4 m&p-Xylene ND ug/L 1.0 1 02/20/19 15:56 179601-23-1 o-Xylene ND ug/L 0.50 1 02/20/19 15:56 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 02/20/19 15:56 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell Industries Pace Project No.: 92417986 Sample: WW-01 Lab ID: 92417986001 Collected: 02/14/19 14:50 Received: 02/15/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 02/20/19 15:56 460-00-4 Toluene-d8(S) 99 % 70-130 1 02/20/19 15:56 2037-26-5 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 16.9 NTU 1.0 1 02/16/19 01:08 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 3.0 mg/L 2.5 1 02/19/19 10:43 5210B BOD, 5 day Analytical Method: SM 521OB-2011 BOD, 5 day ND mg/L 2.0 1 02/16/19 03:52 02/21/19 04:25 B2 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.1 Std. Units 0.10 1 02/19/19 10:36 H3 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia 0.39 mg/L 0.10 1 02/20/19 10:36 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 0.81 mg/L 0.50 1 02/18/19 11:27 02/19/19 00:17 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.054 mg/L 0.020 1 02/16/19 03:35 Nitrogen, Nitrate 0.028 mg/L 0.020 1 02/16/19 03:35 14797-55-8 Nitrogen, Nitrite 0.027 mg/L 0.020 1 02/16/19 03:35 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.063 mg/L 0.050 1 02/18/19 18:12 02/18/19 21:18 7723-14-0 420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993 Phenol ND mg/L 0.020 1 02/18/1914:40 02/19/1914:41 108-95-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458622 Analysis Method: EPA 245.1 Rev 3.0 1994 QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury Associated Lab Samples: 92417986001 METHOD BLANK: 2500146 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 02/18/1911:27 LABORATORY CONTROL SAMPLE: 2500147 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.2 90 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500148 2500149 MS MSD 92417598001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 1.9 1.9 75 77 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500150 2500151 MS MSD 92417509005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 1.8 1.7 71 66 70-130 7 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458552 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92417986001 METHOD BLANK: 2499923 Associated Lab Samples: 92417986001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Qualifiers Arsenic ug/L ND 10.0 02/18/1917:42 Cadmium ug/L ND 1.0 02/18/1917:42 Calcium ug/L ND 100 02/18/1917:42 Chromium ug/L ND 5.0 02/18/1917:42 Copper ug/L ND 5.0 02/18/1917:42 Lead ug/L ND 5.0 02/18/1917:42 Magnesium ug/L ND 100 02/18/1917:42 Molybdenum ug/L ND 5.0 02/18/1917:42 Nickel ug/L ND 5.0 02/18/1917:42 Selenium ug/L ND 10.0 02/18/1917:42 Sodium ug/L ND 5000 02/18/1917:42 Zinc ug/L ND 10.0 02/18/1917:42 LABORATORY CONTROL SAMPLE: 2499924 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic ug/L 500 512 102 85-115 Cadmium ug/L 500 503 101 85-115 Calcium ug/L 5000 5100 102 85-115 Chromium ug/L 500 522 104 85-115 Copper ug/L 500 527 105 85-115 Lead ug/L 500 510 102 85-115 Magnesium ug/L 5000 4980 100 85-115 Molybdenum ug/L 500 526 105 85-115 Nickel ug/L 500 507 101 85-115 Selenium ug/L 500 505 101 85-115 Sodium ug/L 5000 4900J 98 85-115 Zinc ug/L 500 513 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2499925 2499926 MS MSD 92418025001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Arsenic ug/L 500 500 520 517 104 103 70-130 1 Cadmium ug/L 0.059 500 500 574 569 103 102 70-130 1 mg/L Calcium ug/L 5000 5000 18600 18400 111 106 70-130 1 Chromium ug/L 500 500 525 528 104 105 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2499925 2499926 MS MSD 92418025001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 500 500 531 530 105 105 70-130 0 Lead ug/L 0.066 500 500 565 563 100 99 70-130 0 mg/L Magnesium ug/L 5000 5000 7970 7980 103 103 70-130 0 Molybdenum ug/L 500 500 481 481 96 96 70-130 0 Nickel ug/L 500 500 508 509 101 101 70-130 0 Selenium ug/L 500 500 532 534 106 107 70-130 0 Sodium ug/L 5000 5000 30700 30100 118 106 70-130 2 Zinc ug/L 4.8 500 500 5400 5290 119 97 70-130 2 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2499927 2499928 MS MSD 92417780005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Arsenic ug/L ND 500 500 513 504 102 101 70-130 2 Cadmium ug/L ND 500 500 511 506 102 101 70-130 1 Calcium ug/L 0.98 5000 5000 6240 6110 105 103 70-130 2 mg/L Chromium ug/L ND 500 500 531 523 106 105 70-130 1 Copper ug/L 0.014 500 500 536 530 105 103 70-130 1 mg/L Lead ug/L ND 500 500 512 502 102 100 70-130 2 Magnesium ug/L 0.27 5000 5000 5420 5320 103 101 70-130 2 mg/L Molybdenum ug/L ND 500 500 478 475 96 95 70-130 1 Nickel ug/L ND 500 500 510 503 102 100 70-130 1 Selenium ug/L ND 500 500 528 524 105 105 70-130 1 Sodium ug/L ND 5000 5000 6420 6320 100 98 70-130 2 Zinc ug/L 0.093 500 500 613 604 104 102 70-130 1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 459154 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200E MSV Associated Lab Samples: 92417986001 METHOD BLANK: 2502351 Associated Lab Samples: 92417986001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/20/19 10:49 1,1,1-Trichloroethane ug/L ND 0.50 02/20/19 10:49 1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/20/19 10:49 1,1,2-Trichloroethane ug/L ND 0.50 02/20/19 10:49 1,1-Dichloroethane ug/L ND 0.50 02/20/19 10:49 1,1-Dichloroethene ug/L ND 0.50 02/20/19 10:49 1,1-Dichloropropene ug/L ND 0.50 02/20/19 10:49 1,2,3-Trichlorobenzene ug/L ND 2.0 02/20/19 10:49 1,2,3-Trichloropropane ug/L ND 0.50 02/20/19 10:49 1,2,4-Trichlorobenzene ug/L ND 2.0 02/20/19 10:49 1,2,4-Trimethylbenzene ug/L ND 0.50 02/20/19 10:49 1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/20/19 10:49 1,2-Dibromoethane (EDB) ug/L ND 0.50 02/20/19 10:49 1,2-Dichlorobenzene ug/L ND 0.50 02/20/19 10:49 1,2-Dichloroethane ug/L ND 0.50 02/20/19 10:49 1,2-Dichloropropane ug/L ND 0.50 02/20/19 10:49 1,3,5-Trimethylbenzene ug/L ND 0.50 02/20/19 10:49 1,3-Dichlorobenzene ug/L ND 0.50 02/20/19 10:49 1,3-Dichloropropane ug/L ND 0.50 02/20/19 10:49 1,4-Dichlorobenzene ug/L ND 0.50 02/20/19 10:49 2,2-Dichloropropane ug/L ND 0.50 02/20/19 10:49 2-Chlorotoluene ug/L ND 0.50 02/20/19 10:49 4-Chlorotoluene ug/L ND 0.50 02/20/19 10:49 Benzene ug/L ND 0.50 02/20/19 10:49 Bromobenzene ug/L ND 0.50 02/20/19 10:49 Bromochloromethane ug/L ND 0.50 02/20/19 10:49 Bromodichloromethane ug/L ND 0.50 02/20/19 10:49 Bromoform ug/L ND 0.50 02/20/19 10:49 Bromomethane ug/L ND 5.0 02/20/19 10:49 Carbon tetrachloride ug/L ND 0.50 02/20/19 10:49 Chlorobenzene ug/L ND 0.50 02/20/19 10:49 Chloroethane ug/L ND 1.0 02/20/19 10:49 Chloroform ug/L ND 0.50 02/20/19 10:49 Chloromethane ug/L ND 1.0 02/20/19 10:49 cis-1,2-Dichloroethene ug/L ND 0.50 02/20/19 10:49 cis-1,3-Dichloropropene ug/L ND 0.50 02/20/19 10:49 Dibromochloromethane ug/L ND 0.50 02/20/19 10:49 Dibromomethane ug/L ND 0.50 02/20/19 10:49 Dichlorodifluoromethane ug/L ND 0.50 02/20/19 10:49 Diisopropyl ether ug/L ND 0.50 02/20/19 10:49 Ethylbenzene ug/L ND 0.50 02/20/19 10:49 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 METHOD BLANK: 2502351 Associated Lab Samples: 92417986001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Hexachloro-1,3-butadiene ug/L ND 2.0 02/20/19 10:49 Isopropylbenzene (Cumene) ug/L ND 0.50 02/20/19 10:49 m&p-Xylene ug/L ND 1.0 02/20/19 10:49 Methyl-tert-butyl ether ug/L ND 0.50 02/20/19 10:49 Methylene Chloride ug/L ND 2.0 02/20/19 10:49 n-Butylbenzene ug/L ND 0.50 02/20/19 10:49 n-Propylbenzene ug/L ND 0.50 02/20/19 10:49 Naphthalene ug/L ND 2.0 02/20/19 10:49 o-Xylene ug/L ND 0.50 02/20/19 10:49 sec-Butylbenzene ug/L ND 0.50 02/20/19 10:49 Styrene ug/L ND 0.50 02/20/19 10:49 tert-Butyl benzene ug/L ND 0.50 02/20/19 10:49 Tetrachloroethene ug/L ND 0.50 02/20/19 10:49 Toluene ug/L ND 0.50 02/20/19 10:49 trans-1,2-Dichloroethene ug/L ND 0.50 02/20/19 10:49 trans- 1,3-Dichloropropene ug/L ND 0.50 02/20/19 10:49 Trichloroethene ug/L ND 0.50 02/20/19 10:49 Trichlorofluoromethane ug/L ND 1.0 02/20/19 10:49 Vinyl chloride ug/L ND 1.0 02/20/19 10:49 1,2-Dichloroethane-d4 (S) % 93 70-130 02/20/19 10:49 4-Bromofluorobenzene (S) % 97 70-130 02/20/19 10:49 Toluene-d8 (S) % 98 70-130 02/20/19 10:49 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2502352 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 51.6 103 60-140 1,1,1-Trichloroethane ug/L 50 46.7 93 60-140 1,1,2,2-Tetrachloroethane ug/L 50 47.3 95 60-140 1,1,2-Trichloroethane ug/L 50 49.2 98 60-140 1,1-Dichloroethane ug/L 50 43.8 88 60-140 1,1-Dichloroethene ug/L 50 44.6 89 60-140 1,1-Dichloropropene ug/L 50 46.1 92 60-140 1,2,3-Trichlorobenzene ug/L 50 53.4 107 60-140 1,2,3-Trichloropropane ug/L 50 46.5 93 60-140 1,2,4-Trichlorobenzene ug/L 50 53.4 107 60-140 1,2,4-Trimethylbenzene ug/L 50 47.8 96 60-140 1,2-Dibromo-3-chloropropane ug/L 50 51.8 104 60-140 1,2-Dibromoethane (EDB) ug/L 50 50.8 102 60-140 1,2-Dichlorobenzene ug/L 50 50.2 100 60-140 1,2-Dichloroethane ug/L 50 41.1 82 60-140 1,2-Dichloropropane ug/L 50 47.0 94 60-140 1,3,5-Trimethylbenzene ug/L 50 47.6 95 60-140 1,3-Dichlorobenzene ug/L 50 49.9 100 60-140 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 LABORATORY CONTROL SAMPLE: Parameter 2502352 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichloropropane ug/L 50 48.8 98 60-140 1,4-Dichlorobenzene ug/L 50 48.3 97 60-140 2,2-Dichloropropane ug/L 50 51.4 103 60-140 2-Chlorotoluene ug/L 50 47.1 94 60-140 4-Chlorotoluene ug/L 50 47.3 95 60-140 Benzene ug/L 50 47.3 95 60-140 Bromobenzene ug/L 50 49.4 99 60-140 Bromochloromethane ug/L 50 51.4 103 60-140 Bromodichloromethane ug/L 50 50.7 101 60-140 Bromoform ug/L 50 50.7 101 60-140 Bromomethane ug/L 50 52.7 105 60-140 Carbon tetrachloride ug/L 50 52.8 106 60-140 Chlorobenzene ug/L 50 48.0 96 60-140 Chloroethane ug/L 50 44.4 89 60-140 Chloroform ug/L 50 47.6 95 60-140 Chloromethane ug/L 50 46.4 93 60-140 cis-1,2-Dichloroethene ug/L 50 43.6 87 60-140 cis-1,3-Dichloropropene ug/L 50 53.4 107 60-140 Dibromochloromethane ug/L 50 53.2 106 60-140 Dibromomethane ug/L 50 52.6 105 60-140 Dichlorodifluoromethane ug/L 50 51.2 102 60-140 Diisopropyl ether ug/L 50 43.0 86 60-140 Ethylbenzene ug/L 50 47.7 95 60-140 Hexachloro-1,3-butadiene ug/L 50 53.6 107 60-140 Isopropylbenzene (Cumene) ug/L 50 49.1 98 60-140 m&p-Xylene ug/L 100 95.8 96 60-140 Methyl-tert-butyl ether ug/L 50 46.2 92 60-140 Methylene Chloride ug/L 50 45.2 90 60-140 n-Butylbenzene ug/L 50 49.3 99 60-140 n-Propylbenzene ug/L 50 47.7 95 60-140 Naphthalene ug/L 50 49.8 100 60-140 o-Xylene ug/L 50 48.4 97 60-140 sec-Butylbenzene ug/L 50 49.9 100 60-140 Styrene ug/L 50 50.1 100 60-140 tert-Butyl benzene ug/L 50 41.2 82 60-140 Tetrachloroethene ug/L 50 50.4 101 60-140 Toluene ug/L 50 46.6 93 60-140 trans-1,2-Dichloroethene ug/L 50 44.0 88 60-140 trans- 1,3-Dichloropropene ug/L 50 53.9 108 60-140 Trichloroethene ug/L 50 49.4 99 60-140 Trichlorofluoromethane ug/L 50 44.3 89 60-140 Vinyl chloride ug/L 50 47.3 95 60-140 1,2-Dichloroethane-d4 (S) % 93 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 98 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2502353 2502354 MS MSD 92418247004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 4000 4000 4020 4060 101 102 60-140 1 1,1,1-Trichloroethane ug/L ND 4000 4000 3900 3800 97 95 60-140 2 1,1,2,2-Tetrachloroethane ug/L ND 4000 4000 3710 3650 93 91 60-140 2 1,1,2-Trichloroethane ug/L ND 4000 4000 4020 3890 101 97 60-140 3 1,1-Dichloroethane ug/L ND 4000 4000 3730 3620 93 90 60-140 3 1,1-Dichloroethene ug/L ND 4000 4000 3800 3810 95 95 60-140 0 1,1-Dichloropropene ug/L ND 4000 4000 3830 3700 96 92 60-140 4 1,2,3-Trichlorobenzene ug/L ND 4000 4000 4030 4190 101 105 60-140 4 1,2,3-Trichloropropane ug/L ND 4000 4000 3650 3510 91 88 60-140 4 1,2,4-Trichlorobenzene ug/L ND 4000 4000 4010 4120 100 103 60-140 3 1,2,4-Trimethylbenzene ug/L 1680 4000 4000 5440 5470 94 95 60-140 0 1,2-Dibromo-3-chloropropane ug/L ND 4000 4000 3780 3680 95 92 60-140 3 1,2-Dibromoethane (EDB) ug/L ND 4000 4000 3950 4090 99 102 60-140 3 1,2-Dichlorobenzene ug/L ND 4000 4000 3920 3980 98 100 60-140 2 1,2-Dichloroethane ug/L 67.5J 4000 4000 3400 3400 83 83 60-140 0 1,2-Dichloropropane ug/L ND 4000 4000 3840 3760 96 94 60-140 2 1,3,5-Trimethylbenzene ug/L 424 4000 4000 4230 4350 95 98 60-140 3 1,3-Dichlorobenzene ug/L ND 4000 4000 3910 3900 98 98 60-140 0 1,3-Dichloropropane ug/L ND 4000 4000 3890 3860 97 97 60-140 1 1,4-Dichlorobenzene ug/L ND 4000 4000 3890 3890 97 97 60-140 0 2,2-Dichloropropane ug/L ND 4000 4000 3900 3880 97 97 60-140 1 2-Chlorotoluene ug/L ND 4000 4000 3950 3800 99 95 60-140 4 4-Chlorotoluene ug/L ND 4000 4000 3850 3820 96 95 60-140 1 Benzene ug/L 11900 4000 4000 15700 15700 93 95 60-140 0 Bromobenzene ug/L ND 4000 4000 3980 4010 99 100 60-140 1 Bromochloromethane ug/L ND 4000 4000 4080 3970 102 99 60-140 3 Bromodichloromethane ug/L ND 4000 4000 3850 3930 96 98 60-140 2 Bromoform ug/L ND 4000 4000 3490 3460 87 86 60-140 1 Bromomethane ug/L ND 4000 4000 2950 3690 74 92 60-140 22 Carbon tetrachloride ug/L ND 4000 4000 4100 4240 103 106 60-140 3 Chlorobenzene ug/L ND 4000 4000 3910 3900 98 98 60-140 0 Chloroethane ug/L ND 4000 4000 4260 3590 106 90 60-140 17 Chloroform ug/L ND 4000 4000 4060 3970 101 99 60-140 2 Chloromethane ug/L ND 4000 4000 3960 3980 99 100 60-140 0 cis-1,2-Dichloroethene ug/L ND 4000 4000 3730 3630 93 91 60-140 3 cis-1,3-Dichloropropene ug/L ND 4000 4000 3960 4060 99 101 60-140 2 Dibromochloromethane ug/L ND 4000 4000 3770 3920 94 98 60-140 4 Dibromomethane ug/L ND 4000 4000 4090 4170 102 104 60-140 2 Dichlorodifluoromethane ug/L ND 4000 4000 4400 4170 110 104 60-140 5 Diisopropyl ether ug/L 1560 4000 4000 5120 5010 89 86 60-140 2 Ethylbenzene ug/L 1620 4000 4000 5500 5560 97 98 60-140 1 Hexachloro-1,3-butadiene ug/L ND 4000 4000 4100 4370 102 109 60-140 6 Isopropylbenzene (Cumene) ug/L ND 4000 4000 4070 4130 102 103 60-140 2 m&p-Xylene ug/L 7170 8000 8000 14700 14900 94 97 60-140 2 Methyl-tert-butyl ether ug/L 21900 4000 4000 26000 25400 102 88 60-140 2 Methylene Chloride ug/L ND 4000 4000 3710 3570 93 89 60-140 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2502353 2502354 MS MSD 92418247004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual n-Butylbenzene ug/L ND 4000 4000 3740 3880 94 97 60-140 4 n-Propylbenzene ug/L 165 4000 4000 3990 4050 96 97 60-140 1 Naphthalene ug/L 621 4000 4000 4380 4460 94 96 60-140 2 o-Xylene ug/L 3340 4000 4000 7350 7270 100 98 60-140 1 sec-Butylbenzene ug/L ND 4000 4000 4070 4040 102 101 60-140 1 Styrene ug/L 53.5J 4000 4000 4110 4080 101 101 60-140 1 tert-Butyl benzene ug/L ND 4000 4000 3390 3430 85 86 60-140 1 Tetrachloroethene ug/L ND 4000 4000 4120 4060 103 101 60-140 2 Toluene ug/L 21800 4000 4000 25000 25200 79 85 60-140 1 trans-1,2-Dichloroethene ug/L ND 4000 4000 3710 3630 93 91 60-140 2 trans- 1,3-Dichloropropene ug/L ND 4000 4000 3980 4060 100 101 60-140 2 Trichloroethene ug/L ND 4000 4000 4080 4210 102 105 60-140 3 Trichlorofluoromethane ug/L ND 4000 4000 4240 4170 106 104 60-140 2 Vinyl chloride ug/L ND 4000 4000 4120 4000 103 100 60-140 3 1,2-Dichloroethane-d4 (S) % 94 90 70-130 4-Bromofluorobenzene (S) % 97 98 70-130 Toluene-d8(S) % 97 96 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 459041 Analysis Method: EPA 625.1 QC Batch Method: EPA 625.1 Analysis Description: 625 MSS Associated Lab Samples: 92417986001 METHOD BLANK: 2501900 Associated Lab Samples: 92417986001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 5.0 02/20/19 15:43 2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 02/20/19 15:43 2,4,6-Trichlorophenol ug/L ND 10.0 02/20/19 15:43 2,4-Dichlorophenol ug/L ND 5.0 02/20/19 15:43 2,4-Dimethylphenol ug/L ND 10.0 02/20/19 15:43 2,4-Dinitrophenol ug/L ND 50.0 02/20/19 15:43 2,4-Dinitrotoluene ug/L ND 5.0 02/20/19 15:43 2,6-Dinitrotoluene ug/L ND 5.0 02/20/19 15:43 2-Chloronaphthalene ug/L ND 5.0 02/20/19 15:43 2-Chlorophenol ug/L ND 5.0 02/20/19 15:43 2-Nitrophenol ug/L ND 5.0 02/20/19 15:43 3,3'-Dichlorobenzidine ug/L ND 25.0 02/20/19 15:43 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 02/20/19 15:43 4-Bromophenylphenyl ether ug/L ND 5.0 02/20/19 15:43 4-Chloro-3-methylphenol ug/L ND 5.0 02/20/19 15:43 4-Chlorophenylphenyl ether ug/L ND 5.0 02/20/19 15:43 4-Nitrophenol ug/L ND 50.0 02/20/19 15:43 Acenaphthene ug/L ND 5.0 02/20/19 15:43 Acenaphthylene ug/L ND 5.0 02/20/19 15:43 Anthracene ug/L ND 5.0 02/20/19 15:43 Benzo(a)anthracene ug/L ND 5.0 02/20/19 15:43 Benzo(a)pyrene ug/L ND 5.0 02/20/19 15:43 Benzo(b)fluoranthene ug/L ND 5.0 02/20/19 15:43 Benzo(g,h,i)perylene ug/L ND 5.0 02/20/19 15:43 Benzo(k)fluoranthene ug/L ND 5.0 02/20/19 15:43 bis(2-Chloroethoxy)methane ug/L ND 10.0 02/20/19 15:43 bis(2-Chloroethyl) ether ug/L ND 5.0 02/20/19 15:43 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 02/20/19 15:43 Butylbenzylphthalate ug/L ND 5.0 02/20/19 15:43 Chrysene ug/L ND 5.0 02/20/19 15:43 Di-n-butylphthalate ug/L ND 5.0 02/20/19 15:43 Di-n-octylphthalate ug/L ND 5.0 02/20/19 15:43 Dibenz(a,h)anthracene ug/L ND 5.0 02/20/19 15:43 Diethylphthalate ug/L ND 5.0 02/20/19 15:43 Dimethylphthalate ug/L ND 5.0 02/20/19 15:43 Fluoranthene ug/L ND 5.0 02/20/19 15:43 Fluorene ug/L ND 5.0 02/20/19 15:43 Hexachloro-1,3-butadiene ug/L ND 5.0 02/20/19 15:43 Hexachlorobenzene ug/L ND 5.0 02/20/19 15:43 Hexachlorocyclopentadiene ug/L ND 10.0 02/20/19 15:43 Hexachloroethane ug/L ND 5.0 02/20/19 15:43 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 METHOD BLANK: 2501900 Associated Lab Samples: 92417986001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L ND 5.0 02/20/19 15:43 Isophorone ug/L ND 10.0 02/20/19 15:43 N-Nitroso-di-n-propylamine ug/L ND 5.0 02/20/19 15:43 N-Nitrosodimethylamine ug/L ND 5.0 02/20/19 15:43 N-Nitrosodiphenylamine ug/L ND 10.0 02/20/19 15:43 Naphthalene ug/L ND 5.0 02/20/19 15:43 Nitrobenzene ug/L ND 5.0 02/20/19 15:43 Pentachlorophenol ug/L ND 10.0 02/20/19 15:43 Phenanthrene ug/L ND 5.0 02/20/19 15:43 Phenol ug/L ND 5.0 02/20/19 15:43 Pyrene ug/L ND 5.0 02/20/19 15:43 2,4,6-Tribromophenol (S) % 69 10-137 02/20/19 15:43 2-Fluorobiphenyl (S) % 58 15-120 02/20/19 15:43 2-Fluorophenol (S) % 34 10-120 02/20/19 15:43 Nitrobenzene-d5 (S) % 67 10-120 02/20/19 15:43 Phenol-d6 (S) % 27 10-120 02/20/19 15:43 Terphenyl-d14 (S) % 73 11-131 02/20/19 15:43 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2501901 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/L 50 27.5 55 44-142 2,2'-Oxybis(1-chloropropane) ug/L 50 43.0 86 36-166 2,4,6-Trichlorophenol ug/L 50 42.5 85 37-144 2,4-Dichlorophenol ug/L 50 35.6 71 39-135 2,4-Dimethylphenol ug/L 50 40.9 82 32-120 2,4-Dinitrophenol ug/L 250 228 91 1-191 2,4-Dinitrotoluene ug/L 50 39.0 78 39-139 2,6-Dinitrotoluene ug/L 50 40.4 81 50-158 2-Chloronaphthalene ug/L 50 35.0 70 60-120 2-Chlorophenol ug/L 50 33.5 67 23-134 2-Nitrophenol ug/L 50 35.1 70 29-181 3,3'-Dichlorobenzidine ug/L 100 61.7 62 1-262 4,6-Dinitro-2-methyl phenol ug/L 100 93.5 94 1-181 4-Bromophenylphenyl ether ug/L 50 42.0 84 53-127 4-ChIoro-3-methyl phenol ug/L 100 86.0 86 22-147 4-Chlorophenylphenyl ether ug/L 50 42.4 85 25-158 4-Nitrophenol ug/L 250 122 49 1-132 Acenaphthene ug/L 50 39.6 79 47-145 Acenaphthylene ug/L 50 41.4 83 33-145 Anthracene ug/L 50 40.6 81 27-133 Benzo(a)anthracene ug/L 50 44.5 89 33-143 Benzo(a)pyrene ug/L 50 45.1 90 17-163 Benzo(b)fluoranthene ug/L 50 41.0 82 24-159 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 LABORATORY CONTROL SAMPLE: Parameter 2501901 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Benzo(g,h,i)perylene ug/L 50 42.8 86 1-219 Benzo(k)fluoranthene ug/L 50 41.2 82 11-162 bis(2-Chloroethoxy)methane ug/L 50 37.6 75 33-184 bis(2-Chloroethyl) ether ug/L 50 35.2 70 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 48.3 97 8-158 Butylbenzylphthalate ug/L 50 41.9 84 1-152 Chrysene ug/L 50 38.9 78 17-168 Di-n-butylphthalate ug/L 50 44.9 90 1-120 Di-n-octylphthalate ug/L 50 41.1 82 4-146 Dibenz(a,h)anthracene ug/L 50 42.0 84 1-227 Diethylphthalate ug/L 50 43.7 87 1-120 Dimethylphthalate ug/L 50 42.3 85 1-120 Fluoranthene ug/L 50 38.9 78 26-137 Fluorene ug/L 50 44.1 88 59-121 Hexachloro-1,3-butadiene ug/L 50 25.6 51 24-120 Hexachlorobenzene ug/L 50 38.3 77 1-152 Hexachlorocyclopentadiene ug/L 50 28.3 57 25-150 Hexachloroethane ug/L 50 26.1 52 40-120 Indeno(1,2,3-cd)pyrene ug/L 50 42.1 84 1-171 Isophorone ug/L 50 40.3 81 21-196 N-Nitroso-di-n-propylamine ug/L 50 44.4 89 1-230 N-Nitrosodimethylamine ug/L 50 23.3 47 25-150 N-Nitrosodiphenylamine ug/L 50 44.5 89 25-150 Naphthalene ug/L 50 36.0 72 21-133 Nitrobenzene ug/L 50 39.8 80 35-180 Pentachlorophenol ug/L 100 90.8 91 14-176 Phenanthrene ug/L 50 41.1 82 54-120 Phenol ug/L 50 17.7 35 5-120 Pyrene ug/L 50 45.4 91 52-120 2,4,6-Tribromophenol (S) % 81 10-137 2-Fluorobiphenyl (S) % 73 15-120 2-Fluorophenol (S) % 45 10-120 Nitrobenzene-d5 (S) % 83 10-120 Phenol-d6 (S) % 35 10-120 Terphenyl-d14 (S) % 78 11-131 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2501902 2501903 MS MSD 35448068001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,2,4-Trichlorobenzene ug/L 0.981-11 100 100 35.4 35.3 35 35 44-142 0 M1 2,2'-Oxybis(1-chloropropane) ug/L 0.951-11 100 100 52.9 54.1 53 54 36-166 2 2,4,6-Trichlorophenol ug/L 1.31-11 100 100 51.1 54.5 51 55 37-144 7 2,4-Dichlorophenol ug/L 1.71-11 100 100 46.7 45.3 47 45 39-135 3 2,4-Dimethylphenol ug/L 1.21-11 100 100 53.1 50.8 53 51 32-120 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 34 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2501902 2501903 MS MSD 35448068001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 2,4-Dinitrophenol ug/L 9.01-1 500 500 193 223 39 45 1-191 14 2,4-Dinitrotoluene ug/L 0.901-1 100 100 56.6 77.0 57 77 39-139 30 2,6-Dinitrotoluene ug/L 0.981-1 100 100 55.2 69.5 55 69 50-158 23 2-Chloronaphthalene ug/L 0.981-1 100 100 43.5 43.0 43 43 60-120 1 M1 2-Chlorophenol ug/L 1.31-1 100 100 42.5 42.3 42 42 23-134 0 2-Nitrophenol ug/L 0.91 U 100 100 44.9 45.4 45 45 29-182 1 3,3'-Dichlorobenzidine ug/L 2.1U 200 200 74.9 85.6 37 43 1-262 13 4,6-Dinitro-2-methyl phenol ug/L 2.61-1 200 200 112 151 56 76 1-181 29 4-Bromophenylphenyl ether ug/L 0.821-1 100 100 53.5 64.8 54 65 53-127 19 4-Chloro-3-methylphenol ug/L 3.71-1 200 200 113 121 56 60 22-147 7 4-Chlorophenylphenyl ether ug/L 0.871-1 100 100 54.0 62.8 54 63 25-158 15 4-Nitrophenol ug/L 4.1U 500 500 170 234 34 47 1-132 32 Acenaphthene ug/L 0.251-1 100 100 50.8 54.7 51 55 47-145 8 Acenaphthylene ug/L 0.21U 100 100 57.1 59.2 57 59 33-145 4 Anthracene ug/L 0.141-1 100 100 58.4 75.2 58 75 27-133 25 Benzo(a)anthracene ug/L 0.331-1 100 100 62.3 83.9 62 84 33-143 29 Benzo(a)pyrene ug/L 0.301-1 100 100 63.5 90.2 64 90 17-163 35 Benzo(b)fluoranthene ug/L 0.281-1 100 100 64.2 93.6 64 94 24-159 37 Benzo(g,h,i)perylene ug/L 0.381-1 100 100 55.7 72.2 56 72 1-219 26 Benzo(k)fluoranthene ug/L 0.431-1 100 100 62.6 92.3 63 92 11-162 38 bis(2-Chloroethoxy)methane ug/L 0.921-1 100 100 46.9 45.3 47 45 33-184 4 bis(2-Chloroethyl) ether ug/L 1.01-1 100 100 45.0 45.5 45 45 12-158 1 bis(2-Ethylhexyl)phthalate ug/L 0.791-1 100 100 68.9 94.6 69 95 8-158 31 Butylbenzylphthalate ug/L 0.791-1 100 100 66.4 90.7 66 91 1-152 31 Chrysene ug/L 0.21 U 100 100 54.7 78.0 55 78 17-168 35 Di-n-butylphthalate ug/L 0.751-1 100 100 63.0 83.7 63 84 1-120 28 Di-n-octylphthalate ug/L 0.661-1 100 100 63.5 89.5 63 89 4-146 34 Dibenz(a,h)anthracene ug/L 0.551-1 100 100 54.0 86.2 54 86 1-227 46 Diethylphthalate ug/L 0.581-1 100 100 63.1 84.9 63 85 1-120 29 Dimethylphthalate ug/L 0.761-1 100 100 57.2 71.5 57 71 1-120 22 Fluoranthene ug/L 0.21U 100 100 58.2 80.2 58 80 26-137 32 Fluorene ug/L 0.21U 100 100 58.3 69.1 58 69 59-121 17 M1 Hexachloro-1,3-butadiene ug/L 0.941-1 100 100 30.8 31.7 31 32 24-120 3 Hexachlorobenzene ug/L 0.721-1 100 100 48.8 65.2 49 65 1-152 29 Hexachlorocyclopentadiene ug/L 0.881-1 100 100 29.2 29.5 29 30 25-150 1 Hexachloroethane ug/L 1.1U 100 100 29.9 29.8 30 30 40-120 0 M1 Indeno(1,2,3-cd)pyrene ug/L 0.291-1 100 100 58.6 87.7 59 88 1-171 40 Isophorone ug/L 0.891-1 100 100 53.6 51.1 54 51 21-196 5 N-Nitroso-di-n-propylamine ug/L 0.991-1 100 100 55.7 52.6 56 53 1-230 6 N-Nitrosodimethylamine ug/L 0.91 U 100 100 27.5 29.6 28 30 25-150 7 N-Nitrosodiphenylamine ug/L 1.01-1 100 100 60.2 80.7 60 81 25-150 29 Naphthalene ug/L 0.34U 100 100 45.0 44.8 45 45 21-133 0 Nitrobenzene ug/L 1.1U 100 100 57.5 60.9 57 61 35-180 6 Pentachlorophenol ug/L 4.61-1 200 200 68.7 97.3 34 49 14-176 35 Phenanthrene ug/L 0.221-1 100 100 58.5 76.5 58 76 54-120 27 Phenol ug/L 1.91-1 100 100 21.6 23.3 22 23 5-120 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2501902 2501903 MS MSD 35448068001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Pyrene ug/L 0.19U 100 100 66.2 89.6 66 90 52-120 30 2,4,6-Tribromophenol (S) % 53 69 10-137 2-Fluorobiphenyl (S) % 47 46 15-120 2-Fluorophenol(S) % 25 26 10-120 Nitrobenzene-d5(S) % 53 52 10-120 Phenol-d6 (S) % 20 22 10-120 Terphenyl-d14(S) % 54 67 11-131 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458546 Analysis Method: EPA 180.1 Rev 2.0 1993 QC Batch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92417986001 METHOD BLANK: 2499908 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Turbidity NTU ND 1.0 02/16/19 01:07 LABORATORY CONTROL SAMPLE: 2499909 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.3 103 90-110 SAMPLE DUPLICATE: 2499910 92417986001 Dup Parameter Units Result Result RPD Qualifiers Turbidity NTU 16.9 17.0 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458883 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92417986001 METHOD BLANK: 2501073 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02/19/19 10:42 LABORATORY CONTROL SAMPLE: 2501074 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 2501075 92417854002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 2501076 92417510007 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 16.0 17.0 6 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458542 Analysis Method: SM 521 OB-2011 QC Batch Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92417986001 METHOD BLANK: 2499904 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 02/21/19 04:02 LABORATORY CONTROL SAMPLE: 2499905 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 191 97 84.6-115 SAMPLE DUPLICATE: 2499907 92417974001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 242 293 19 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458610 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92417986001 SAMPLE DUPLICATE: 2500129 Parameter pH at 25 Degrees C 92417518001 Dup Units Result Result RPD Qualifiers Std. Units 13.1 13.2 1 E,H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458909 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Associated Lab Samples: 92417986001 METHOD BLANK: 2501197 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 02/20/19 10:17 LABORATORY CONTROL SAMPLE: 2501198 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2501199 2501200 MS MSD 92417769001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.34 5 5 5.6 5.7 106 107 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2501201 2501202 MS MSD 92417503008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.1 102 101 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458642 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92417986001 METHOD BLANK: 2500196 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 02/19/19 00:11 LABORATORY CONTROL SAMPLE: 2500197 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.9 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500198 2500199 MS MSD 92418025001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 10.4 10.1 100 97 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500202 2500203 MS MSD 92417788001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 28.0 10 10 41.0 42.0 130 140 90-110 3 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458548 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92417986001 METHOD BLANK: 2499911 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.020 02/16/19 03:32 Nitrogen, Nitrite mg/L ND 0.020 02/16/19 03:32 Nitrogen, NO2 plus NO3 mg/L ND 0.020 02/16/19 03:32 LABORATORY CONTROL SAMPLE: 2499912 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 97 90-110 Nitrogen, Nitrite mg/L 1 1.0 104 90-110 Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2499913 2499914 MS MSD 92417986001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.028 1.5 1.5 1.5 1.6 100 106 90-110 5 Nitrogen, Nitrite mg/L 0.027 1 1 1.1 1.1 105 106 90-110 0 Nitrogen, NO2 plus NO3 mg/L 0.054 2.5 2.5 2.6 2.7 102 106 90-110 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458781 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92417986001 METHOD BLANK: 2500810 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 02/18/19 21:08 LABORATORY CONTROL SAMPLE: 2500811 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500812 2500813 MS MSD 92418025001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.086 2.5 2.5 2.6 2.6 100 99 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500814 2500815 MS MSD 92417501007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.9 2.5 2.5 4.2 4.6 93 107 90-110 8 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell Industries Pace Project No.: 92417986 QC Batch: 458669 Analysis Method: EPA 420.4 Rev 1.0 1993 QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics Associated Lab Samples: 92417986001 METHOD BLANK: 2500293 Matrix: Water Associated Lab Samples: 92417986001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phenol mg/L ND 0.020 02/19/1914:29 LABORATORY CONTROL SAMPLE: 2500294 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenol mg/L 0.05 0.050 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500295 2500296 MS MSD 92417266001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenol mg/L ND 0.05 0.05 0.052 0.051 94 92 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2500297 2500298 MS MSD 92417646002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenol mg/L 0.029 0.05 0.05 0.076 0.079 95 100 90-110 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 34 Pace Analytical Services, LLC ceAnalX cal ® hevi Riverside 04 Asheville, NC 28804 www.pacelabs.com (828)254-7176 QUALIFIERS Project: Powell Industries Pace Project No.: 92417986 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. D6 The precision between the sample and sample duplicate exceeded laboratory control limits. E Analyte concentration exceeded the calibration range. The reported result is estimated. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Powell Industries 92417986 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92417986001 WW-01 EPA 200.7 Rev 4.4 1994 458552 EPA 200.7 Rev 4.4 1994 458568 92417986001 WW-01 EPA 245.1 Rev 3.0 1994 458622 EPA 245.1 Rev 3.0 1994 458646 92417986001 WW-01 EPA 625.1 459041 EPA 625.1 459202 92417986001 WW-01 SM 6200B 459154 92417986001 WW-01 EPA 180.1 Rev 2.0 1993 458546 92417986001 WW-01 SM 2540D-2011 458883 92417986001 WW-01 SM 5210B-2011 458542 SM 5210B-2011 458561 92417986001 WW-01 EPA 9040C 458610 92417986001 WW-01 EPA 350.1 Rev 2.0 1993 458909 92417986001 WW-01 EPA 351.2 Rev 2.0 1993 458642 EPA 351.2 Rev 2.0 1993 458829 92417986001 WW-01 EPA 353.2 Rev 2.0 1993 458548 92417986001 WW-01 EPA 365.1 Rev 2.0 1993 458781 EPA 365.1 Rev 2.0 1993 458813 92417986001 WW-01 EPA 420.4 Rev 1.0 1993 458669 EPA 420.4 Rev 1.0 1993 458868 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/21 /2019 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 34 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Receipt(SCUR) Page 1 of 2 ac ceAnalVtical Document No.: Issuing Authority: F-CAR-05-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Courier: ❑ Commercial Custody Seal Present? Client Name: WO� 92417986 y Project #: l G " ) _C 111H I I❑Fed Ex UPS ❑OtherClient 1111111111111111 Pace_39!� ❑ II [:]Yes; ❑No Seals Intact? ❑Yes gNo Packing Material: ❑Bubble Wrap Rubble Bags ❑None ❑ other Thermometgr: }� Type of Ice: owet ❑Blue /O IR Gun ID: Cooler Temp (°C): �.__ Correction Factor: Add/Subtract CC) Cooler Temp Corrected (°C): Is USDA Regulated Soil (EQ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? 92417986 Date/Initials Person Examining Contents: J — 2-15 Biological Tissue Frozen? El❑No PN/A ❑None Temp should be above freezing to 6°C ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source (internation0y, .—I..ai.,o t4—roil anri Puarto Ricol? MYes ❑No COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes 0No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager 5RF Review: Date:C Page 32 of 34 s Document Name: Document Revised: February 7, 2018 / Sample Condition Upon Receipt(SCUR) Page 1 of 2 acehjalytic l Document No.: Issuing Authority: F-CAR-CS-033-Rev.05 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project f WO# : 92417986 PM: UP Due Date: 02/22/19 CLIENT: 93-Mart.im&S1 E 41 V z 61 a v c E to ri ❑ V M. m z Gl iu c 5 E 0 N ❑ M a m z Gl c� c a E o N a m z L a C _125 Y ❑ rl GL m N V a -r J E 1!1 a G m N V n 2 Q E N Z M a m 0 Z 0) M Z N J E N 7 a m V .N-I A n J E cN-I V 7 a m v y Q ❑ .ro E L=L C Z 0,-- Q ❑ EE¢ v �' r-I rl 0 Q V 2 v = a-1 2 1i kD Q V z '❑ ` ti E J of ,,,� N 7 rn 0 4 `, z O = a `V = ,.y VI .-I l7 G _ N V �- a N 2 E ry V1 en 0 U Q z '— C s Z 4 o m C7 ❑ Q en C7 Q Z a � E 0 a 2 dl 0 ❑ C Z O ¢ E ♦- M W > Z e >CL C 0 C ' CI 0 > Q PO ¢ E o C 6 Q} 0 0 _ Z X Q 0 > C ro 7 e ° y Y l:7 7 v E .Na F N 6 in a a ? �na E a N F N M. V) s M 2 a o N N Q m �• m Q @ a+ c QJE o o C la 4 0 G E o 6 0 ✓1 > ¢ Z Q E ¢ E Q5 17 ❑ 1X/ jjQ r 2 3 4 5 \ N F 7t 8 9 10 N\ 11 1z \-, \N\N pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Pr added Lot # Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 33 of 34 N O �➢ W V Q� A W N ITEM # O N a � � C t�l E(11_� N 3 (n n c Q ~J ii N s� nv O D ? v e t C Y o 1 v I ni o m 3 Z m. p m r A V' ` T m o Z v V m m m r Zi ON pg4v,���o z O °W f'o ➢ o o 0 c o O 0 m n D C,_ Z Z m o n= 3 o �w C MATRIXCOOF {see va'Idcodesto left, m n P r n SAMPLE "TYPE (G=GRAB C-COMP} p z^ 0 N m y m tl J > a 41 D m a o F 'n m fly D m � O A m z Z Z r C b --I3 z m 0 m om IT o mm N Z ro N ti W v in ro m r r > m SAMPLE TEMP AT COLLECTION A 3 fA m a w # OF CONTAINERS v � v ;u Y C7 0 N m a N Unpreserved Hz50a - v n fi HNO3 � � HCI 2 NaOH �- Na2S203 3 m Methanol m Other 0 jAnalysis Test Z YIN j m D -C o y n v K Z �4 G' f a z tu fn m m O C z G� ireN LL m -4 fn n w o r 1 .ts m m m � f3r�t� m _ lV 6.141, a D t� m m m z C n fl n N Temp in `C - -s Residual Chlorine (YIN) y n Received on Ice {YIN) > ni,\ 0 m, CD N O r o Custody Sealed Cooler O Lo (YIN) a O � a -ES G; fin 0 Samples Intact Q Pag ,, m a ;0 3 CD 6 Y m Q 0 y 0 rr Cv CD O m a � n � C G m lD 34 of 34 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 April 30, 2019 Mr. Robert Martin Martin and Slagle 24 Lookout Terrace Black Mountain, NC 28711 RE: Project: Powell4/12 Pace Project No.: 92425518 Dear Mr. Martin: Enclosed are the analytical results for sample(s) received by the laboratory on April 12, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com 1(828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Powell4/12 Pace Project No.: 92425518 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Pace Project No.: Powell4/12 92425518 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92425518001 C-1 EPA 601 OD IDS 12 PASI-A EPA 7471B JMW1 1 PASI-A EPA 8270E PKS 74 PASI-C ASTM D2974-87 KDF 1 PASI-C EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A 92425518002 C-1A EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518003 C-1 B EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518004 C-1C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518005 C-1 D EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518006 C-2 EPA 601 OD IDS 12 PASI-A EPA 7471B JMW1 1 PASI-A EPA 8270E PKS 74 PASI-C ASTM D2974-87 KDF 1 PASI-C EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A 92425518008 C-2A EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518009 C-213 EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518010 C-2C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92425518011 C-21D EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1 Lab ID: 92425518001 Collected: 04/12/19 14:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Arsenic 3.7 mg/kg 1.8 1 04/25/1917:25 04/27/1918:07 7440-38-2 M1 Cadmium ND mg/kg 0.18 1 04/25/1917:25 04/27/1918:07 7440-43-9 M1 Calcium 7860 mg/kg 17.8 1 04/25/1917:25 04/27/1918:07 7440-70-2 M1 Chromium 59.9 mg/kg 0.89 1 04/25/1917:25 04/27/1918:07 7440-47-3 Copper 96.4 mg/kg 0.89 1 04/25/1917:25 04/27/1918:07 7440-50-8 Lead 15.8 mg/kg 0.89 1 04/25/1917:25 04/27/1918:07 7439-92-1 M1 Magnesium 12100 mg/kg 17.8 1 04/25/1917:25 04/27/1918:07 7439-95-4 M1 Molybdenum 3.1 mg/kg 0.89 1 04/25/1917:25 04/27/1918:07 7439-98-7 M1 Nickel 32.1 mg/kg 0.89 1 04/25/1917:25 04/27/1918:07 7440-02-0 M1 Selenium ND mg/kg 1.8 1 04/25/1917:25 04/27/1918:07 7782-49-2 M1 Sodium ND mg/kg 888 1 04/25/1917:25 04/27/1918:07 7440-23-5 Zinc 264 mg/kg 1.8 1 04/25/1917:25 04/27/1918:07 7440-66-6 M1 7471 Mercury Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B Mercury 0.046 mg/kg 0.014 1 04/22/1916:34 04/23/1913:33 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Acenaphthene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 83-32-9 Acenaphthylene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 208-96-8 Aniline ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 62-53-3 Anthracene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 120-12-7 Benzo(a)anthracene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 56-55-3 Benzo(a)pyrene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 50-32-8 Benzo(b)fluoranthene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 205-99-2 Benzo(g,h,i)perylene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 191-24-2 Benzo(k)fluoranthene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 207-08-9 Benzoic Acid ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 65-85-0 v1 Benzyl alcohol ND ug/kg 1700 1 04/22/19 12:29 04/22/19 23:51 100-51-6 4-Bromophenylphenyl ether ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 101-55-3 Butylbenzylphthalate ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 85-68-7 4-Chloro-3-methyl phenol ND ug/kg 1700 1 04/22/19 12:29 04/22/19 23:51 59-50-7 4-Chloroaniline ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 111-44-4 2-Chloronaphthalene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 91-58-7 2-Chlorophenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 7005-72-3 Chrysene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 218-01-9 Dibenz(a,h)anthracene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 53-70-3 Dibenzofuran ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 132-64-9 1,2-Dichlorobenzene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 95-50-1 1,3-Dichlorobenzene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 541-73-1 1,4-Dichlorobenzene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 91-94-1 v1 2,4-Dichlorophenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 120-83-2 v1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1 Lab ID: 92425518001 Collected: 04/12/19 14:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Diethylphthalate ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 84-66-2 2,4-Dimethylphenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 105-67-9 Dimethylphthalate ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 131-11-3 Di-n-butylphthalate ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 1700 1 04/22/19 12:29 04/22/19 23:51 534-52-1 v1 2,4-Dinitrophenol ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 51-28-5 v1 2,4-Dinitrotoluene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 121-14-2 2,6-Dinitrotoluene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 606-20-2 Di-n-octylphthalate ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 117-81-7 Fluoranthene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 206-44-0 Fluorene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 87-68-3 Hexachlorobenzene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 118-74-1 Hexachlorocyclopentadiene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 77-47-4 Hexachloroethane ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 193-39-5 Isophorone ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 78-59-1 1-Methylnaphthalene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 90-12-0 2-Methylnaphthalene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 15831-10-4 Naphthalene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 91-20-3 2-Nitroaniline ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 88-74-4 3-Nitroaniline ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 99-09-2 4-Nitroaniline ND ug/kg 1700 1 04/22/19 12:29 04/22/19 23:51 100-01-6 Nitrobenzene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 98-95-3 2-Nitrophenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 88-75-5 v1 4-Nitrophenol ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 100-02-7 N-Nitrosodimethylamine ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 621-64-7 N-Nitrosodiphenylamine ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 108-60-1 Pentachlorophenol ND ug/kg 4250 1 04/22/19 12:29 04/22/19 23:51 87-86-5 Phenanthrene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 85-01-8 Phenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 108-95-2 v1 Pyrene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 129-00-0 1,2,4-Trichlorobenzene ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 120-82-1 2,4,5-Trichlorophenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 95-95-4 2,4,6-Trichlorophenol ND ug/kg 849 1 04/22/19 12:29 04/22/19 23:51 88-06-2 Surrogates Nitrobenzene-d5 (S) 66 % 23-110 1 04/22/19 12:29 04/22/19 23:51 4165-60-0 2-Fluorobiphenyl (S) 66 % 30-110 1 04/22/19 12:29 04/22/19 23:51 321-60-8 Terphenyl-d14 (S) 72 % 28-110 1 04/22/19 12:29 04/22/19 23:51 1718-51-0 Phenol-d6 (S) 70 % 22-110 1 04/22/19 12:29 04/22/19 23:51 13127-88-3 2-Fluorophenol (S) 69 % 13-110 1 04/22/19 12:29 04/22/19 23:51 367-12-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1 Lab ID: 92425518001 Collected: 04/12/19 14:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Surrogates 2,4,6-Tribromophenol (S) Percent Moisture Percent Moisture 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite 365.1 Phosphorus, Total Phosphorus Date: 04/30/2019 03:11 PM Analytical Method: EPA 8270E Preparation Method: EPA 3546 88 % 27-110 1 04/22/19 12:29 04/22/19 23:51 118-79-6 Analytical Method: ASTM D2974-87 60.9 % 0.10 1 04/16/1914:00 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 3560 mg/kg 94.7 1 04/19/19 07:10 04/20/19 00:44 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 9.9 1 04/15/19 23:47 04/16/19 01:49 H1,H2 ND mg/kg 9.9 1 04/15/19 23:47 04/16/19 01:49 14797-55-8 ND mg/kg 9.9 1 04/15/19 23:47 04/16/19 01:49 14797-65-0 H1,H2 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 692 mg/kg 10.5 5 04/16/1918:35 04/16/1923:48 7723-14-0 M1,R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1A Lab ID: 92425518002 Collected: 04/12/19 15:02 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone 457 ug/kg 374 1 04/19/19 14:03 04/22/19 16:25 67-64-1 Benzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 71-43-2 Bromobenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 108-86-1 Bromochloromethane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 74-97-5 Bromodichloromethane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 75-27-4 Bromoform ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 75-25-2 Bromomethane ND ug/kg 37.4 1 04/19/19 14:03 04/22/19 16:25 74-83-9 2-Butanone (MEK) ND ug/kg 374 1 04/19/19 14:03 04/22/19 16:25 78-93-3 n-Butylbenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 104-51-8 sec-Butylbenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 135-98-8 tert-Butyl benzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 98-06-6 Carbon tetrachloride ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 56-23-5 Chlorobenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 108-90-7 Chloroethane ND ug/kg 37.4 1 04/19/19 14:03 04/22/19 16:25 75-00-3 Chloroform ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 67-66-3 Chloromethane ND ug/kg 37.4 1 04/19/19 14:03 04/22/19 16:25 74-87-3 2-Chlorotoluene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 95-49-8 4-Chlorotoluene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 96-12-8 Dibromochloromethane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 106-93-4 Dibromomethane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 74-95-3 1,2-Dichlorobenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 95-50-1 1,3-Dichlorobenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 541-73-1 1,4-Dichlorobenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 106-46-7 Dichlorodifluoromethane ND ug/kg 37.4 1 04/19/19 14:03 04/22/19 16:25 75-71-8 1,1-Dichloroethane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 75-34-3 1,2-Dichloroethane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 107-06-2 1,1-Dichloroethene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 75-35-4 cis-1,2-Dichloroethene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 156-59-2 trans-1,2-Dichloroethene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 156-60-5 1,2-Dichloropropane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 78-87-5 1,3-Dichloropropane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 142-28-9 2,2-Dichloropropane ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 594-20-7 1,1-Dichloropropene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 563-58-6 cis-1,3-Dichloropropene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 10061-02-6 Diisopropyl ether ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 108-20-3 Ethylbenzene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 87-68-3 2-Hexanone ND ug/kg 187 1 04/19/19 14:03 04/22/19 16:25 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 98-82-8 p-Isopropyltoluene ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 99-87-6 Methylene Chloride ND ug/kg 74.7 1 04/19/19 14:03 04/22/19 16:25 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 187 1 04/19/19 14:03 04/22/19 16:25 108-10-1 Methyl-tert-butyl ether ND ug/kg 18.7 1 04/19/19 14:03 04/22/19 16:25 1634-04-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1A Lab ID: 92425518002 Collected: 04/12/19 15:02 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 91-20-3 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 103-65-1 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 100-42-5 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 630-20-6 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 79-34-5 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 127-18-4 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 108-88-3 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 87-61-6 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 120-82-1 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 71-55-6 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 79-00-5 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 79-01-6 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 75-69-4 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 96-18-4 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 95-63-6 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 108-67-8 ND ug/kg 187 1 04/19/1914:03 04/22/1916:25 108-05-4 ND ug/kg 37.4 1 04/19/1914:03 04/22/1916:25 75-01-4 ND ug/kg 37.4 1 04/19/1914:03 04/22/1916:25 1330-20-7 ND ug/kg 37.4 1 04/19/1914:03 04/22/1916:25 179601-23-1 ND ug/kg 18.7 1 04/19/1914:03 04/22/1916:25 95-47-6 95 % 70-130 1 04/19/1914:03 04/22/1916:25 2037-26-5 82 % 70-130 1 04/19/1914:03 04/22/1916:25 460-00-4 103 % 70-132 1 04/19/1914:03 04/22/1916:25 17060-07-0 Analytical Method: ASTM D2974-87 62.8 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:22 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1B Lab ID: 92425518003 Collected: 04/12/19 15:10 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone ND ug/kg 374 1 04/19/19 13:00 04/19/19 23:01 67-64-1 Benzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 71-43-2 Bromobenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 108-86-1 Bromochloromethane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 74-97-5 Bromodichloromethane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 75-27-4 Bromoform ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 75-25-2 Bromomethane ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 74-83-9 2-Butanone (MEK) ND ug/kg 374 1 04/19/19 13:00 04/19/19 23:01 78-93-3 n-Butylbenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 104-51-8 sec-Butylbenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 135-98-8 tert-Butyl benzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 98-06-6 Carbon tetrachloride ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 56-23-5 Chlorobenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 108-90-7 Chloroethane ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 75-00-3 Chloroform ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 67-66-3 Chloromethane ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 74-87-3 2-Chlorotoluene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 95-49-8 4-Chlorotoluene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 96-12-8 Dibromochloromethane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 106-93-4 Dibromomethane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 74-95-3 1,2-Dichlorobenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 95-50-1 1,3-Dichlorobenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 541-73-1 1,4-Dichlorobenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 106-46-7 Dichlorodifluoromethane ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 75-71-8 1,1-Dichloroethane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 75-34-3 1,2-Dichloroethane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 107-06-2 1,1-Dichloroethene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 75-35-4 cis-1,2-Dichloroethene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 156-59-2 trans-1,2-Dichloroethene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 156-60-5 1,2-Dichloropropane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 78-87-5 1,3-Dichloropropane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 142-28-9 2,2-Dichloropropane ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 594-20-7 1,1-Dichloropropene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 563-58-6 cis-1,3-Dichloropropene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 10061-02-6 Diisopropyl ether ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 108-20-3 Ethylbenzene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 87-68-3 2-Hexanone ND ug/kg 187 1 04/19/19 13:00 04/19/19 23:01 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 98-82-8 p-Isopropyltoluene ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 99-87-6 Methylene Chloride ND ug/kg 74.7 1 04/19/19 13:00 04/19/19 23:01 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 187 1 04/19/19 13:00 04/19/19 23:01 108-10-1 Methyl-tert-butyl ether ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 1634-04-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-113 Lab ID: 92425518003 Collected: 04/12/19 15:10 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 91-20-3 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 103-65-1 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 100-42-5 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 630-20-6 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 79-34-5 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 127-18-4 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 108-88-3 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 87-61-6 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 120-82-1 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 71-55-6 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 79-00-5 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 79-01-6 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 75-69-4 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 96-18-4 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 95-63-6 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 108-67-8 ND ug/kg 187 1 04/19/19 13:00 04/19/19 23:01 108-05-4 ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 75-01-4 ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 1330-20-7 ND ug/kg 37.4 1 04/19/19 13:00 04/19/19 23:01 179601-23-1 ND ug/kg 18.7 1 04/19/19 13:00 04/19/19 23:01 95-47-6 93 % 70-130 1 04/19/19 13:00 04/19/19 23:01 2037-26-5 84 % 70-130 1 04/19/19 13:00 04/19/19 23:01 460-00-4 100 % 70-132 1 04/19/19 13:00 04/19/19 23:01 17060-07-0 Analytical Method: ASTM D2974-87 65.9 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1C Lab ID: 92425518004 Collected: 04/12/19 14:15 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone 383 ug/kg 318 1 04/19/19 13:00 04/19/19 23:26 67-64-1 Benzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 71-43-2 Bromobenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 108-86-1 Bromochloromethane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 74-97-5 Bromodichloromethane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 75-27-4 Bromoform ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 75-25-2 Bromomethane ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 74-83-9 2-Butanone (MEK) ND ug/kg 318 1 04/19/19 13:00 04/19/19 23:26 78-93-3 n-Butylbenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 104-51-8 sec-Butylbenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 135-98-8 tert-Butyl benzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 98-06-6 Carbon tetrachloride ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 56-23-5 Chlorobenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 108-90-7 Chloroethane ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 75-00-3 Chloroform ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 67-66-3 Chloromethane ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 74-87-3 2-Chlorotoluene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 95-49-8 4-Chlorotoluene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 96-12-8 Dibromochloromethane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 106-93-4 Dibromomethane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 74-95-3 1,2-Dichlorobenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 95-50-1 1,3-Dichlorobenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 541-73-1 1,4-Dichlorobenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 106-46-7 Dichlorodifluoromethane ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 75-71-8 1,1-Dichloroethane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 75-34-3 1,2-Dichloroethane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 107-06-2 1,1-Dichloroethene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 75-35-4 cis-1,2-Dichloroethene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 156-59-2 trans-1,2-Dichloroethene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 156-60-5 1,2-Dichloropropane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 78-87-5 1,3-Dichloropropane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 142-28-9 2,2-Dichloropropane ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 594-20-7 1,1-Dichloropropene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 563-58-6 cis-1,3-Dichloropropene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 10061-02-6 Diisopropyl ether ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 108-20-3 Ethylbenzene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 87-68-3 2-Hexanone ND ug/kg 159 1 04/19/19 13:00 04/19/19 23:26 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 98-82-8 p-Isopropyltoluene ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 99-87-6 Methylene Chloride ND ug/kg 63.7 1 04/19/19 13:00 04/19/19 23:26 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 159 1 04/19/19 13:00 04/19/19 23:26 108-10-1 Methyl-tert-butyl ether ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 1634-04-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-1C Lab ID: 92425518004 Collected: 04/12/19 14:15 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 91-20-3 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 103-65-1 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 100-42-5 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 630-20-6 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 79-34-5 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 127-18-4 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 108-88-3 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 87-61-6 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 120-82-1 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 71-55-6 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 79-00-5 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 79-01-6 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 75-69-4 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 96-18-4 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 95-63-6 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 108-67-8 ND ug/kg 159 1 04/19/19 13:00 04/19/19 23:26 108-05-4 ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 75-01-4 ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 1330-20-7 ND ug/kg 31.8 1 04/19/19 13:00 04/19/19 23:26 179601-23-1 ND ug/kg 15.9 1 04/19/19 13:00 04/19/19 23:26 95-47-6 94 % 70-130 1 04/19/19 13:00 04/19/19 23:26 2037-26-5 83 % 70-130 1 04/19/19 13:00 04/19/19 23:26 460-00-4 96 % 70-132 1 04/19/19 13:00 04/19/19 23:26 17060-07-0 Analytical Method: ASTM D2974-87 63.5 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-111) Lab ID: 92425518005 Collected: 04/12/19 14:30 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone 586 ug/kg 415 1 04/19/19 14:03 04/22/19 17:41 67-64-1 Benzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 71-43-2 Bromobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 108-86-1 Bromochloromethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 74-97-5 Bromodichloromethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 75-27-4 Bromoform ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 75-25-2 Bromomethane ND ug/kg 41.5 1 04/19/19 14:03 04/22/19 17:41 74-83-9 2-Butanone (MEK) ND ug/kg 415 1 04/19/19 14:03 04/22/19 17:41 78-93-3 n-Butylbenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 104-51-8 sec-Butylbenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 135-98-8 tert-Butyl benzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 98-06-6 Carbon tetrachloride ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 56-23-5 Chlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 108-90-7 Chloroethane ND ug/kg 41.5 1 04/19/19 14:03 04/22/19 17:41 75-00-3 Chloroform ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 67-66-3 Chloromethane ND ug/kg 41.5 1 04/19/19 14:03 04/22/19 17:41 74-87-3 2-Chlorotoluene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 95-49-8 4-Chlorotoluene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 96-12-8 Dibromochloromethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 106-93-4 Dibromomethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 74-95-3 1,2-Dichlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 95-50-1 1,3-Dichlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 541-73-1 1,4-Dichlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 106-46-7 Dichlorodifluoromethane ND ug/kg 41.5 1 04/19/19 14:03 04/22/19 17:41 75-71-8 1,1-Dichloroethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 75-34-3 1,2-Dichloroethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 107-06-2 1,1-Dichloroethene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 75-35-4 cis-1,2-Dichloroethene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 156-59-2 trans-1,2-Dichloroethene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 156-60-5 1,2-Dichloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 78-87-5 1,3-Dichloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 142-28-9 2,2-Dichloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 594-20-7 1,1-Dichloropropene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 563-58-6 cis-1,3-Dichloropropene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 10061-02-6 Diisopropyl ether ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 108-20-3 Ethylbenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 87-68-3 2-Hexanone ND ug/kg 207 1 04/19/19 14:03 04/22/19 17:41 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 98-82-8 p-Isopropyltoluene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 99-87-6 Methylene Chloride ND ug/kg 83.0 1 04/19/19 14:03 04/22/19 17:41 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 207 1 04/19/19 14:03 04/22/19 17:41 108-10-1 Methyl-tert-butyl ether ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 17:41 1634-04-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-11D Lab ID: 92425518005 Collected: 04/12/19 14:30 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 91-20-3 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 103-65-1 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 100-42-5 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 630-20-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 79-34-5 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 127-18-4 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 108-88-3 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 87-61-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 120-82-1 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 71-55-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 79-00-5 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 79-01-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 75-69-4 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 96-18-4 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 95-63-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 108-67-8 ND ug/kg 207 1 04/19/1914:03 04/22/1917:41 108-05-4 ND ug/kg 41.5 1 04/19/1914:03 04/22/1917:41 75-01-4 ND ug/kg 41.5 1 04/19/1914:03 04/22/1917:41 1330-20-7 ND ug/kg 41.5 1 04/19/1914:03 04/22/1917:41 179601-23-1 ND ug/kg 20.7 1 04/19/1914:03 04/22/1917:41 95-47-6 95 % 70-130 1 04/19/1914:03 04/22/1917:41 2037-26-5 81 % 70-130 1 04/19/1914:03 04/22/1917:41 460-00-4 104 % 70-132 1 04/19/1914:03 04/22/1917:41 17060-07-0 Analytical Method: ASTM D2974-87 64.9 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2 Lab ID: 92425518006 Collected: 04/12/19 16:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Arsenic 2.0 mg/kg 1.5 1 04/25/1917:25 04/27/1918:31 7440-38-2 Cadmium ND mg/kg 0.15 1 04/25/1917:25 04/27/1918:31 7440-43-9 Calcium 3490 mg/kg 15.2 1 04/25/1917:25 04/27/1918:31 7440-70-2 Chromium 66.5 mg/kg 0.76 1 04/25/1917:25 04/27/1918:31 7440-47-3 Copper 88.9 mg/kg 0.76 1 04/25/1917:25 04/27/1918:31 7440-50-8 Lead 15.5 mg/kg 0.76 1 04/25/1917:25 04/27/1918:31 7439-92-1 Magnesium 13200 mg/kg 15.2 1 04/25/1917:25 04/27/1918:31 7439-95-4 Molybdenum 3.0 mg/kg 0.76 1 04/25/1917:25 04/27/1918:31 7439-98-7 Nickel 33.8 mg/kg 0.76 1 04/25/1917:25 04/27/1918:31 7440-02-0 Selenium ND mg/kg 1.5 1 04/25/1917:25 04/27/1918:31 7782-49-2 Sodium ND mg/kg 762 1 04/25/1917:25 04/27/1918:31 7440-23-5 Zinc 204 mg/kg 1.5 1 04/25/1917:25 04/27/1918:31 7440-66-6 7471 Mercury Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B Mercury 0.040 mg/kg 0.0054 1 04/22/1916:34 04/23/1913:35 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Acenaphthene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 83-32-9 Acenaphthylene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 208-96-8 Aniline ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 62-53-3 Anthracene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 120-12-7 Benzo(a)anthracene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 56-55-3 Benzo(a)pyrene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 50-32-8 Benzo(b)fluoranthene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 205-99-2 Benzo(g,h,i)perylene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 191-24-2 Benzo(k)fluoranthene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 207-08-9 Benzoic Acid ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 65-85-0 Benzyl alcohol ND ug/kg 1620 1 04/16/19 12:34 04/17/19 13:13 100-51-6 4-Bromophenylphenyl ether ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 101-55-3 Butylbenzylphthalate ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 85-68-7 4-Chloro-3-methyl phenol ND ug/kg 1620 1 04/16/19 12:34 04/17/19 13:13 59-50-7 4-Chloroaniline ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 111-44-4 2-Chloronaphthalene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 91-58-7 2-Chlorophenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 7005-72-3 Chrysene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 218-01-9 Dibenz(a,h)anthracene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 53-70-3 Dibenzofuran ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 132-64-9 1,2-Dichlorobenzene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 95-50-1 1,3-Dichlorobenzene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 541-73-1 1,4-Dichlorobenzene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 91-94-1 2,4-Dichlorophenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 120-83-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2 Lab ID: 92425518006 Collected: 04/12/19 16:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Diethylphthalate ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 84-66-2 2,4-Dimethylphenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 105-67-9 Dimethylphthalate ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 131-11-3 Di-n-butylphthalate ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 1620 1 04/16/19 12:34 04/17/19 13:13 534-52-1 2,4-Dinitrophenol ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 51-28-5 2,4-Dinitrotoluene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 121-14-2 2,6-Dinitrotoluene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 606-20-2 Di-n-octylphthalate ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 117-81-7 Fluoranthene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 206-44-0 Fluorene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 87-68-3 Hexachlorobenzene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 118-74-1 Hexachlorocyclopentadiene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 77-47-4 Hexachloroethane ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 193-39-5 Isophorone ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 78-59-1 1-Methylnaphthalene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 90-12-0 2-Methylnaphthalene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 15831-10-4 Naphthalene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 91-20-3 2-Nitroaniline ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 88-74-4 3-Nitroaniline ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 99-09-2 4-Nitroaniline ND ug/kg 1620 1 04/16/19 12:34 04/17/19 13:13 100-01-6 Nitrobenzene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 98-95-3 2-Nitrophenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 88-75-5 4-Nitrophenol ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 100-02-7 N-Nitrosodimethylamine ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 621-64-7 N-Nitrosodiphenylamine ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 108-60-1 Pentachlorophenol ND ug/kg 4040 1 04/16/19 12:34 04/17/19 13:13 87-86-5 Phenanthrene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 85-01-8 Phenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 108-95-2 Pyrene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 129-00-0 1,2,4-Trichlorobenzene ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 120-82-1 2,4,5-Trichlorophenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 95-95-4 2,4,6-Trichlorophenol ND ug/kg 809 1 04/16/19 12:34 04/17/19 13:13 88-06-2 Surrogates Nitrobenzene-d5 (S) 57 % 23-110 1 04/16/19 12:34 04/17/19 13:13 4165-60-0 2-Fluorobiphenyl (S) 54 % 30-110 1 04/16/19 12:34 04/17/19 13:13 321-60-8 Terphenyl-d14 (S) 66 % 28-110 1 04/16/19 12:34 04/17/19 13:13 1718-51-0 Phenol-d6 (S) 58 % 22-110 1 04/16/19 12:34 04/17/19 13:13 13127-88-3 2-Fluorophenol (S) 58 % 13-110 1 04/16/19 12:34 04/17/19 13:13 367-12-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2 Lab ID: 92425518006 Collected: 04/12/19 16:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Surrogates 2,4,6-Tribromophenol (S) Percent Moisture Percent Moisture 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite 365.1 Phosphorus, Total Phosphorus Date: 04/30/2019 03:11 PM Analytical Method: EPA 8270E Preparation Method: EPA 3546 72 % 27-110 1 04/16/1912:34 04/17/1913:13 118-79-6 Analytical Method: ASTM D2974-87 59.5 % 0.10 1 04/16/1914:00 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 3400 mg/kg 91.4 1 04/19/19 07:10 04/20/19 00:45 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 9.7 1 04/15/19 23:47 04/16/19 01:50 H1,H2 ND mg/kg 9.7 1 04/15/19 23:47 04/16/19 01:50 14797-55-8 ND mg/kg 9.7 1 04/15/19 23:47 04/16/19 01:50 14797-65-0 H1,H2 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 623 mg/kg 9.3 5 04/16/19 18:35 04/16/19 23:51 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2A Lab ID: 92425518008 Collected: 04/12/19 15:45 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone 434 ug/kg 282 1 04/19/19 13:00 04/19/19 23:51 67-64-1 Benzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 71-43-2 Bromobenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 108-86-1 Bromochloromethane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 74-97-5 Bromodichloromethane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 75-27-4 Bromoform ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 75-25-2 Bromomethane ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 74-83-9 2-Butanone (MEK) ND ug/kg 282 1 04/19/19 13:00 04/19/19 23:51 78-93-3 n-Butylbenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 104-51-8 sec-Butylbenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 135-98-8 tert-Butyl benzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 98-06-6 Carbon tetrachloride ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 56-23-5 Chlorobenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 108-90-7 Chloroethane ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 75-00-3 Chloroform ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 67-66-3 Chloromethane ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 74-87-3 2-Chlorotoluene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 95-49-8 4-Chlorotoluene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 96-12-8 Dibromochloromethane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 106-93-4 Dibromomethane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 74-95-3 1,2-Dichlorobenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 95-50-1 1,3-Dichlorobenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 541-73-1 1,4-Dichlorobenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 106-46-7 Dichlorodifluoromethane ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 75-71-8 1,1-Dichloroethane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 75-34-3 1,2-Dichloroethane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 107-06-2 1,1-Dichloroethene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 75-35-4 cis-1,2-Dichloroethene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 156-59-2 trans-1,2-Dichloroethene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 156-60-5 1,2-Dichloropropane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 78-87-5 1,3-Dichloropropane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 142-28-9 2,2-Dichloropropane ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 594-20-7 1,1-Dichloropropene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 563-58-6 cis-1,3-Dichloropropene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 10061-02-6 Diisopropyl ether ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 108-20-3 Ethylbenzene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 87-68-3 2-Hexanone ND ug/kg 141 1 04/19/19 13:00 04/19/19 23:51 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 98-82-8 p-Isopropyltoluene ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 99-87-6 Methylene Chloride ND ug/kg 56.4 1 04/19/19 13:00 04/19/19 23:51 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 141 1 04/19/19 13:00 04/19/19 23:51 108-10-1 Methyl-tert-butyl ether ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 1634-04-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2A Lab ID: 92425518008 Collected: 04/12/19 15:45 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 91-20-3 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 103-65-1 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 100-42-5 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 630-20-6 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 79-34-5 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 127-18-4 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 108-88-3 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 87-61-6 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 120-82-1 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 71-55-6 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 79-00-5 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 79-01-6 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 75-69-4 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 96-18-4 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 95-63-6 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 108-67-8 ND ug/kg 141 1 04/19/19 13:00 04/19/19 23:51 108-05-4 ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 75-01-4 ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 1330-20-7 ND ug/kg 28.2 1 04/19/19 13:00 04/19/19 23:51 179601-23-1 ND ug/kg 14.1 1 04/19/19 13:00 04/19/19 23:51 95-47-6 94 % 70-130 1 04/19/19 13:00 04/19/19 23:51 2037-26-5 81 % 70-130 1 04/19/19 13:00 04/19/19 23:51 460-00-4 101 % 70-132 1 04/19/19 13:00 04/19/19 23:51 17060-07-0 Analytical Method: ASTM D2974-87 59.3 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2B Lab ID: 92425518009 Collected: 04/12/19 15:50 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone ND ug/kg 1020 1 04/19/19 14:03 04/22/19 18:31 67-64-1 Benzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 71-43-2 Bromobenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 108-86-1 Bromochloromethane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 74-97-5 Bromodichloromethane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 75-27-4 Bromoform ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 75-25-2 Bromomethane ND ug/kg 102 1 04/19/19 14:03 04/22/19 18:31 74-83-9 2-Butanone (MEK) ND ug/kg 1020 1 04/19/19 14:03 04/22/19 18:31 78-93-3 n-Butylbenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 104-51-8 sec-Butylbenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 135-98-8 tert-Butyl benzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 98-06-6 Carbon tetrachloride ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 56-23-5 Chlorobenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 108-90-7 Chloroethane ND ug/kg 102 1 04/19/19 14:03 04/22/19 18:31 75-00-3 Chloroform ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 67-66-3 Chloromethane ND ug/kg 102 1 04/19/19 14:03 04/22/19 18:31 74-87-3 2-Chlorotoluene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 95-49-8 4-Chlorotoluene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 96-12-8 Dibromochloromethane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 106-93-4 Dibromomethane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 74-95-3 1,2-Dichlorobenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 95-50-1 1,3-Dichlorobenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 541-73-1 1,4-Dichlorobenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 106-46-7 Dichlorodifluoromethane ND ug/kg 102 1 04/19/19 14:03 04/22/19 18:31 75-71-8 1,1-Dichloroethane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 75-34-3 1,2-Dichloroethane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 107-06-2 1,1-Dichloroethene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 75-35-4 cis-1,2-Dichloroethene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 156-59-2 trans-1,2-Dichloroethene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 156-60-5 1,2-Dichloropropane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 78-87-5 1,3-Dichloropropane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 142-28-9 2,2-Dichloropropane ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 594-20-7 1,1-Dichloropropene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 563-58-6 cis-1,3-Dichloropropene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 10061-02-6 Diisopropyl ether ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 108-20-3 Ethylbenzene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 87-68-3 2-Hexanone ND ug/kg 510 1 04/19/19 14:03 04/22/19 18:31 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 98-82-8 p-Isopropyltoluene ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 99-87-6 Methylene Chloride ND ug/kg 204 1 04/19/19 14:03 04/22/19 18:31 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 510 1 04/19/19 14:03 04/22/19 18:31 108-10-1 Methyl-tert-butyl ether ND ug/kg 51.0 1 04/19/19 14:03 04/22/19 18:31 1634-04-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-213 Lab ID: 92425518009 Collected: 04/12/19 15:50 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 91-20-3 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 103-65-1 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 100-42-5 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 630-20-6 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 79-34-5 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 127-18-4 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 108-88-3 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 87-61-6 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 120-82-1 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 71-55-6 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 79-00-5 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 79-01-6 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 75-69-4 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 96-18-4 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 95-63-6 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 108-67-8 ND ug/kg 510 1 04/19/1914:03 04/22/1918:31 108-05-4 ND ug/kg 102 1 04/19/1914:03 04/22/1918:31 75-01-4 ND ug/kg 102 1 04/19/1914:03 04/22/1918:31 1330-20-7 ND ug/kg 102 1 04/19/1914:03 04/22/1918:31 179601-23-1 ND ug/kg 51.0 1 04/19/1914:03 04/22/1918:31 95-47-6 97 % 70-130 1 04/19/1914:03 04/22/1918:31 2037-26-5 93 % 70-130 1 04/19/1914:03 04/22/1918:31 460-00-4 104 % 70-132 1 04/19/1914:03 04/22/1918:31 17060-07-0 Analytical Method: ASTM D2974-87 65.7 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2C Lab ID: 92425518010 Collected: 04/12/19 15:40 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone ND ug/kg 8380 25 04/19/19 14:03 04/20/19 01:31 67-64-1 Benzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 71-43-2 Bromobenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 108-86-1 Bromochloromethane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 74-97-5 Bromodichloromethane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 75-27-4 Bromoform ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 75-25-2 Bromomethane ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 74-83-9 2-Butanone (MEK) ND ug/kg 8380 25 04/19/19 14:03 04/20/19 01:31 78-93-3 n-Butylbenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 104-51-8 sec-Butylbenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 135-98-8 tert-Butyl benzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 98-06-6 Carbon tetrachloride ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 56-23-5 Chlorobenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 108-90-7 Chloroethane ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 75-00-3 Chloroform ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 67-66-3 Chloromethane ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 74-87-3 2-Chlorotoluene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 95-49-8 4-Chlorotoluene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 96-12-8 Dibromochloromethane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 106-93-4 Dibromomethane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 74-95-3 1,2-Dichlorobenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 95-50-1 1,3-Dichlorobenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 541-73-1 1,4-Dichlorobenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 106-46-7 Dichlorodifluoromethane ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 75-71-8 1,1-Dichloroethane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 75-34-3 1,2-Dichloroethane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 107-06-2 1,1-Dichloroethene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 75-35-4 cis-1,2-Dichloroethene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 156-59-2 trans-1,2-Dichloroethene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 156-60-5 1,2-Dichloropropane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 78-87-5 1,3-Dichloropropane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 142-28-9 2,2-Dichloropropane ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 594-20-7 1,1-Dichloropropene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 563-58-6 cis-1,3-Dichloropropene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 10061-02-6 Diisopropyl ether ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 108-20-3 Ethylbenzene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 87-68-3 2-Hexanone ND ug/kg 4190 25 04/19/19 14:03 04/20/19 01:31 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 98-82-8 p-Isopropyltoluene ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 99-87-6 Methylene Chloride ND ug/kg 1680 25 04/19/19 14:03 04/20/19 01:31 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 4190 25 04/19/19 14:03 04/20/19 01:31 108-10-1 Methyl-tert-butyl ether ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 1634-04-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-2C Lab ID: 92425518010 Collected: 04/12/19 15:40 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 91-20-3 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 103-65-1 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 100-42-5 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 630-20-6 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 79-34-5 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 127-18-4 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 108-88-3 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 87-61-6 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 120-82-1 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 71-55-6 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 79-00-5 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 79-01-6 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 75-69-4 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 96-18-4 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 95-63-6 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 108-67-8 ND ug/kg 4190 25 04/19/19 14:03 04/20/19 01:31 108-05-4 ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 75-01-4 ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 1330-20-7 ND ug/kg 838 25 04/19/19 14:03 04/20/19 01:31 179601-23-1 ND ug/kg 419 25 04/19/19 14:03 04/20/19 01:31 95-47-6 97 % 70-130 25 04/19/19 14:03 04/20/19 01:31 2037-26-5 99 % 70-130 25 04/19/19 14:03 04/20/19 01:31 460-00-4 104 % 70-132 25 04/19/19 14:03 04/20/19 01:31 17060-07-0 Analytical Method: ASTM D2974-87 59.9 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-211) Lab ID: 92425518011 Collected: 04/12/19 15:15 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 82601D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone ND ug/kg 414 1 04/19/19 14:03 04/22/19 19:21 67-64-1 Benzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 71-43-2 Bromobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 108-86-1 Bromochloromethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 74-97-5 Bromodichloromethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 75-27-4 Bromoform ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 75-25-2 Bromomethane ND ug/kg 41.4 1 04/19/19 14:03 04/22/19 19:21 74-83-9 2-Butanone (MEK) ND ug/kg 414 1 04/19/19 14:03 04/22/19 19:21 78-93-3 n-Butylbenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 104-51-8 sec-Butylbenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 135-98-8 tert-Butyl benzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 98-06-6 Carbon tetrachloride ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 56-23-5 Chlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 108-90-7 Chloroethane ND ug/kg 41.4 1 04/19/19 14:03 04/22/19 19:21 75-00-3 Chloroform ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 67-66-3 Chloromethane ND ug/kg 41.4 1 04/19/19 14:03 04/22/19 19:21 74-87-3 2-Chlorotoluene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 95-49-8 4-Chlorotoluene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 96-12-8 Dibromochloromethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 106-93-4 Dibromomethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 74-95-3 1,2-Dichlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 95-50-1 1,3-Dichlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 541-73-1 1,4-Dichlorobenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 106-46-7 Dichlorodifluoromethane ND ug/kg 41.4 1 04/19/19 14:03 04/22/19 19:21 75-71-8 1,1-Dichloroethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 75-34-3 1,2-Dichloroethane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 107-06-2 1,1-Dichloroethene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 75-35-4 cis-1,2-Dichloroethene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 156-59-2 trans-1,2-Dichloroethene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 156-60-5 1,2-Dichloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 78-87-5 1,3-Dichloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 142-28-9 2,2-Dichloropropane ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 594-20-7 1,1-Dichloropropene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 563-58-6 cis-1,3-Dichloropropene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 10061-02-6 Diisopropyl ether ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 108-20-3 Ethylbenzene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 87-68-3 2-Hexanone ND ug/kg 207 1 04/19/19 14:03 04/22/19 19:21 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 98-82-8 p-Isopropyltoluene ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 99-87-6 Methylene Chloride ND ug/kg 82.7 1 04/19/19 14:03 04/22/19 19:21 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 207 1 04/19/19 14:03 04/22/19 19:21 108-10-1 Methyl-tert-butyl ether ND ug/kg 20.7 1 04/19/19 14:03 04/22/19 19:21 1634-04-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell4/12 Pace Project No.: 92425518 Sample: C-21D Lab ID: 92425518011 Collected: 04/12/19 15:15 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826013/5035A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 91-20-3 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 103-65-1 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 100-42-5 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 630-20-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 79-34-5 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 127-18-4 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 108-88-3 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 87-61-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 120-82-1 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 71-55-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 79-00-5 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 79-01-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 75-69-4 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 96-18-4 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 95-63-6 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 108-67-8 ND ug/kg 207 1 04/19/1914:03 04/22/1919:21 108-05-4 ND ug/kg 41.4 1 04/19/1914:03 04/22/1919:21 75-01-4 ND ug/kg 41.4 1 04/19/1914:03 04/22/1919:21 1330-20-7 ND ug/kg 41.4 1 04/19/1914:03 04/22/1919:21 179601-23-1 ND ug/kg 20.7 1 04/19/1914:03 04/22/1919:21 95-47-6 99 % 70-130 1 04/19/1914:03 04/22/1919:21 2037-26-5 96 % 70-130 1 04/19/1914:03 04/22/1919:21 460-00-4 102 % 70-132 1 04/19/1914:03 04/22/1919:21 17060-07-0 Analytical Method: ASTM D2974-87 63.9 % 0.10 1 REPORT OF LABORATORY ANALYSIS 04/16/19 14:23 This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 470793 Analysis Method: EPA 7471 B QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury Associated Lab Samples: 92425518001, 92425518006 METHOD BLANK: 2555602 Matrix: Solid Associated Lab Samples: 92425518001, 92425518006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury mg/kg ND 0.0060 04/23/1912:52 LABORATORY CONTROL SAMPLE: 2555603 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/kg 0.083 0.080 96 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2555604 2555605 MS MSD 92424988014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury mg/kg 0.0089 0.078 0.067 0.084 0.073 96 96 75-125 14 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 471202 Analysis Method: EPA 6010D QC Batch Method: EPA 3050E Analysis Description: 6010 MET Associated Lab Samples: 92425518001, 92425518006 METHOD BLANK: 2557031 Associated Lab Samples: 92425518001, 92425518006 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed Arsenic mg/kg ND 1.0 04/27/1918:01 Cadmium mg/kg ND 0.10 04/27/1918:01 Calcium mg/kg ND 10.0 04/27/1918:01 Chromium mg/kg ND 0.50 04/27/1918:01 Copper mg/kg ND 0.50 04/27/1918:01 Lead mg/kg ND 0.50 04/27/1918:01 Magnesium mg/kg ND 10.0 04/27/1918:01 Molybdenum mg/kg ND 0.50 04/27/1918:01 Nickel mg/kg ND 0.50 04/27/1918:01 Selenium mg/kg ND 1.0 04/27/1918:01 Sodium mg/kg ND 500 04/27/1918:01 Zinc mg/kg ND 1.0 04/27/1918:01 LABORATORY CONTROL SAMPLE: 2557032 Parameter Units Arsenic mg/kg Cadmium mg/kg Calcium mg/kg Chromium mg/kg Copper mg/kg Lead mg/kg Magnesium mg/kg Molybdenum mg/kg Nickel mg/kg Selenium mg/kg Sodium mg/kg Zinc mg/kg Qualifiers Spike Conc. LCS Result LCS % Rec % Rec Limits 50 43.2 86 80-120 50 44.8 90 80-120 500 472 94 80-120 50 47.7 95 80-120 50 47.7 95 80-120 50 46.1 92 80-120 500 462 92 80-120 50 45.8 92 80-120 50 46.1 92 80-120 50 42.0 84 80-120 500 477J 95 80-120 50 44.3 89 80-120 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2557033 2557034 MS MSD 92425518001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Arsenic mg/kg 3.7 80.8 91.3 55.9 65.0 64 67 75-125 15 M1 Cadmium mg/kg ND 80.8 91.3 56.6 66.6 70 73 75-125 16 M1 Calcium mg/kg 7860 808 913 8400 8970 67 121 75-125 6 M1 Chromium mg/kg 59.9 80.8 91.3 121 137 75 85 75-125 13 Copper mg/kg 96.4 80.8 91.3 169 189 89 102 75-125 12 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2557033 2557034 MS MSD 92425518001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead mg/kg 15.8 80.8 91.3 72.2 83.1 70 74 75-125 14 M1 Magnesium mg/kg 12100 808 913 13300 14500 148 268 75-125 9 M1 Molybdenum mg/kg 3.1 80.8 91.3 57.3 66.1 67 69 75-125 14 M1 Nickel mg/kg 32.1 80.8 91.3 90.1 103 72 78 75-125 14 M1 Selenium mg/kg ND 80.8 91.3 50.1 58.8 62 64 75-125 16 M1 Sodium mg/kg ND 808 913 868 989 84 87 75-125 13 Zinc mg/kg 264 80.8 91.3 320 346 69 89 75-125 8 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 470498 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics Associated Lab Samples: 92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010, 92425518011 METHOD BLANK: 2554406 Matrix: Solid Associated Lab Samples: 92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010, 92425518011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/19/19 20:05 1,1,1-Trichloroethane ug/kg ND 5.0 04/19/19 20:05 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/19/19 20:05 1,1,2-Trichloroethane ug/kg ND 5.0 04/19/19 20:05 1,1-Dichloroethane ug/kg ND 5.0 04/19/19 20:05 1,1-Dichloroethene ug/kg ND 5.0 04/19/19 20:05 1,1-Dichloropropene ug/kg ND 5.0 04/19/19 20:05 1,2,3-Trichlorobenzene ug/kg ND 5.0 04/19/19 20:05 1,2,3-Trichloropropane ug/kg ND 5.0 04/19/19 20:05 1,2,4-Trichlorobenzene ug/kg ND 5.0 04/19/19 20:05 1,2,4-Trimethylbenzene ug/kg ND 5.0 04/19/19 20:05 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/19/19 20:05 1,2-Dibromoethane (EDB) ug/kg ND 5.0 04/19/19 20:05 1,2-Dichlorobenzene ug/kg ND 5.0 04/19/19 20:05 1,2-Dichloroethane ug/kg ND 5.0 04/19/19 20:05 1,2-Dichloropropane ug/kg ND 5.0 04/19/19 20:05 1,3,5-Trimethylbenzene ug/kg ND 5.0 04/19/19 20:05 1,3-Dichlorobenzene ug/kg ND 5.0 04/19/19 20:05 1,3-Dichloropropane ug/kg ND 5.0 04/19/19 20:05 1,4-Dichlorobenzene ug/kg ND 5.0 04/19/19 20:05 2,2-Dichloropropane ug/kg ND 5.0 04/19/19 20:05 2-Butanone (MEK) ug/kg ND 100 04/19/19 20:05 2-Chlorotoluene ug/kg ND 5.0 04/19/19 20:05 2-Hexanone ug/kg ND 50.0 04/19/19 20:05 4-Chlorotoluene ug/kg ND 5.0 04/19/19 20:05 4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 04/19/19 20:05 Acetone ug/kg ND 100 04/19/19 20:05 Benzene ug/kg ND 5.0 04/19/19 20:05 Bromobenzene ug/kg ND 5.0 04/19/19 20:05 Bromochloromethane ug/kg ND 5.0 04/19/19 20:05 Bromodichloromethane ug/kg ND 5.0 04/19/19 20:05 Bromoform ug/kg ND 5.0 04/19/19 20:05 Bromomethane ug/kg ND 10.0 04/19/19 20:05 Carbon tetrachloride ug/kg ND 5.0 04/19/19 20:05 Chlorobenzene ug/kg ND 5.0 04/19/19 20:05 Chloroethane ug/kg ND 10.0 04/19/19 20:05 Chloroform ug/kg ND 5.0 04/19/19 20:05 Chloromethane ug/kg ND 10.0 04/19/19 20:05 cis-1,2-Dichloroethene ug/kg ND 5.0 04/19/19 20:05 cis-1,3-Dichloropropene ug/kg ND 5.0 04/19/19 20:05 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 METHOD BLANK: 2554406 Matrix: Solid Associated Lab Samples: 92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010, 92425518011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromochloromethane ug/kg ND 5.0 04/19/19 20:05 Dibromomethane ug/kg ND 5.0 04/19/19 20:05 Dichlorodifluoromethane ug/kg ND 10.0 04/19/19 20:05 Diisopropyl ether ug/kg ND 5.0 04/19/19 20:05 Ethylbenzene ug/kg ND 5.0 04/19/19 20:05 Hexachloro-1,3-butadiene ug/kg ND 5.0 04/19/19 20:05 Isopropylbenzene (Cumene) ug/kg ND 5.0 04/19/19 20:05 m&p-Xylene ug/kg ND 10.0 04/19/19 20:05 Methyl-tert-butyl ether ug/kg ND 5.0 04/19/19 20:05 Methylene Chloride ug/kg ND 20.0 04/19/19 20:05 n-Butylbenzene ug/kg ND 5.0 04/19/19 20:05 n-Propylbenzene ug/kg ND 5.0 04/19/19 20:05 Naphthalene ug/kg ND 5.0 04/19/19 20:05 o-Xylene ug/kg ND 5.0 04/19/19 20:05 p-Isopropyltoluene ug/kg ND 5.0 04/19/19 20:05 sec-Butylbenzene ug/kg ND 5.0 04/19/19 20:05 Styrene ug/kg ND 5.0 04/19/19 20:05 tert-Butyl benzene ug/kg ND 5.0 04/19/19 20:05 Tetrachloroethene ug/kg ND 5.0 04/19/19 20:05 Toluene ug/kg ND 5.0 04/19/19 20:05 trans-1,2-Dichloroethene ug/kg ND 5.0 04/19/19 20:05 trans- 1,3-Dichloropropene ug/kg ND 5.0 04/19/19 20:05 Trichloroethene ug/kg ND 5.0 04/19/19 20:05 Trichlorofluoromethane ug/kg ND 5.0 04/19/19 20:05 Vinyl acetate ug/kg ND 50.0 04/19/19 20:05 Vinyl chloride ug/kg ND 10.0 04/19/19 20:05 Xylene (Total) ug/kg ND 10.0 04/19/19 20:05 1,2-Dichloroethane-d4 (S) % 103 70-132 04/19/19 20:05 4-Bromofluorobenzene (S) % 99 70-130 04/19/19 20:05 Toluene-d8 (S) % 99 70-130 04/19/19 20:05 LABORATORY CONTROL SAMPLE: 2554407 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 50 49.9 100 70-130 1,1,1-Trichloroethane ug/kg 50 43.2 86 70-130 1,1,2,2-Tetrachloroethane ug/kg 50 48.2 96 55-130 1,1,2-Trichloroethane ug/kg 50 47.0 94 70-130 1,1-Dichloroethane ug/kg 50 42.4 85 68-130 1,1-Dichloroethene ug/kg 50 43.0 86 70-130 1,1-Dichloropropene ug/kg 50 42.8 86 70-130 1,2,3-Trichlorobenzene ug/kg 50 47.5 95 70-130 1,2,3-Trichloropropane ug/kg 50 51.4 103 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 67 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 LABORATORY CONTROL SAMPLE: Parameter 2554407 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/kg 50 46.7 93 70-130 1,2,4-Trimethylbenzene ug/kg 50 44.0 88 69-130 1,2-Dibromo-3-chloropropane ug/kg 50 45.1 90 57-141 1,2-Dibromoethane (EDB) ug/kg 50 47.7 95 70-130 1,2-Dichlorobenzene ug/kg 50 44.9 90 70-130 1,2-Dichloroethane ug/kg 50 44.6 89 70-130 1,2-Dichloropropane ug/kg 50 46.5 93 70-130 1,3,5-Trimethylbenzene ug/kg 50 44.8 90 70-130 1,3-Dichlorobenzene ug/kg 50 44.2 88 70-130 1,3-Dichloropropane ug/kg 50 47.0 94 70-130 1,4-Dichlorobenzene ug/kg 50 44.2 88 70-130 2,2-Dichloropropane ug/kg 50 44.8 90 70-130 2-Butanone (MEK) ug/kg 100 101 101 60-130 2-Chlorotoluene ug/kg 50 44.8 90 70-130 2-Hexanone ug/kg 100 93.1 93 70-132 4-Chlorotoluene ug/kg 50 44.7 89 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 100 93.1 93 69-130 Acetone ug/kg 100 102 102 49-148 Benzene ug/kg 50 45.6 91 70-130 Bromobenzene ug/kg 50 45.6 91 70-130 Bromochloromethane ug/kg 50 45.7 91 70-130 Bromodichloromethane ug/kg 50 46.8 94 70-130 Bromoform ug/kg 50 42.0 84 68-136 Bromomethane ug/kg 50 43.0 86 60-140 Carbon tetrachloride ug/kg 50 44.0 88 70-130 Chlorobenzene ug/kg 50 43.3 87 70-130 Chloroethane ug/kg 50 49.2 98 51-147 Chloroform ug/kg 50 43.8 88 70-130 Chloromethane ug/kg 50 42.4 85 48-130 cis-1,2-Dichloroethene ug/kg 50 43.8 88 70-130 cis-1,3-Dichloropropene ug/kg 50 47.8 96 70-130 Dibromochloromethane ug/kg 50 47.3 95 70-130 Dibromomethane ug/kg 50 47.3 95 70-130 Dichlorodifluoromethane ug/kg 50 43.1 86 49-130 Diisopropyl ether ug/kg 50 48.7 97 66-130 Ethylbenzene ug/kg 50 45.1 90 70-130 Hexachloro-1,3-butadiene ug/kg 50 45.1 90 70-130 Isopropylbenzene (Cumene) ug/kg 50 44.6 89 70-130 m&p-Xylene ug/kg 100 89.9 90 70-130 Methyl-tert-butyl ether ug/kg 50 48.2 96 70-130 Methylene Chloride ug/kg 50 38.3 77 50-137 n-Butylbenzene ug/kg 50 45.0 90 70-130 n-Propylbenzene ug/kg 50 45.0 90 70-130 Naphthalene ug/kg 50 47.1 94 70-131 o-Xylene ug/kg 50 44.2 88 70-130 p-Isopropyltoluene ug/kg 50 45.2 90 70-130 sec-Butylbenzene ug/kg 50 45.8 92 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 LABORATORY CONTROL SAMPLE: Parameter 2554407 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Styrene ug/kg 50 44.3 89 70-130 tert-Butyl benzene ug/kg 50 40.1 80 69-130 Tetrachloroethene ug/kg 50 44.7 89 56-130 Toluene ug/kg 50 44.4 89 70-130 trans-1,2-Dichloroethene ug/kg 50 43.1 86 70-130 trans- 1,3-Dichloropropene ug/kg 50 49.0 98 70-130 Trichloroethene ug/kg 50 43.9 88 70-141 Trichlorofluoromethane ug/kg 50 43.5 87 67-130 Vinyl acetate ug/kg 100 92.7 93 10-136 Vinyl chloride ug/kg 50 43.2 86 67-130 Xylene (Total) ug/kg 150 134 89 70-130 1,2-Dichloroethane-d4 (S) % 96 70-132 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: Parameter 2555712 Units 92425764001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND 437 469 107 52-133 1,1,1-Trichloroethane ug/kg ND 437 426 98 49-137 1,1,2,2-Tetrachloroethane ug/kg ND 437 320 73 39-150 1,1,2-Trichloroethane ug/kg ND 437 377 86 48-140 1,1-Dichloroethane ug/kg ND 437 424 97 46-135 1,1-Dichloroethene ug/kg ND 437 530 121 38-149 1,1-Dichloropropene ug/kg ND 437 420 96 41-140 1,2,3-Trichlorobenzene ug/kg ND 437 427 98 10-158 1,2,3-Trichloropropane ug/kg ND 437 322 74 33-157 1,2,4-Trichlorobenzene ug/kg ND 437 451 103 10-155 1,2,4-Trimethylbenzene ug/kg ND 437 499 114 24-154 1,2-Dibromo-3-chloropropane ug/kg ND 437 237 54 33-158 1,2-Dibromoethane (EDB) ug/kg ND 437 330 76 40-136 1,2-Dichlorobenzene ug/kg ND 437 440 101 27-146 1,2-Dichloroethane ug/kg ND 437 335 77 49-140 1,2-Dichloropropane ug/kg ND 437 411 94 44-143 1,3,5-Trimethylbenzene ug/kg ND 437 456 104 40-144 1,3-Dichlorobenzene ug/kg ND 437 443 102 33-140 1,3-Dichloropropane ug/kg ND 437 408 93 47-147 1,4-Dichlorobenzene ug/kg ND 437 447 102 35-139 2,2-Dichloropropane ug/kg ND 437 446 102 41-140 2-Butanone (MEK) ug/kg ND 873 397J 45 10-181 2-Chlorotoluene ug/kg ND 437 457 105 38-147 2-Hexanone ug/kg ND 873 468J 54 18-169 4-Chlorotoluene ug/kg ND 437 462 106 36-145 4-Methyl-2-pentanone (MIBK) ug/kg ND 873 5091 58 16-175 Acetone ug/kg ND 873 ND 22 10-200 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 MATRIX SPIKE SAMPLE: 2555712 92425764001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Benzene ug/kg ND 437 435 100 46-136 Bromobenzene ug/kg ND 437 464 106 38-149 Bromochloromethane ug/kg ND 437 335 77 44-142 Bromodichloromethane ug/kg ND 437 369 85 41-140 Bromoform ug/kg ND 437 331 76 34-145 Bromomethane ug/kg ND 437 385 88 14-162 Carbon tetrachloride ug/kg ND 437 442 101 44-141 Chlorobenzene ug/kg ND 437 446 102 39-141 Chloroethane ug/kg ND 437 215 49 10-182 Chloroform ug/kg ND 437 387 89 45-140 Chloromethane ug/kg ND 437 517 119 19-149 cis-1,2-Dichloroethene ug/kg ND 437 401 92 38-150 cis-1,3-Dichloropropene ug/kg ND 437 459 105 30-144 Dibromochloromethane ug/kg ND 437 405 93 36-145 Dibromomethane ug/kg ND 437 291 67 41-145 Dichlorodifluoromethane ug/kg ND 437 241 55 16-146 Diisopropyl ether ug/kg ND 437 445 102 41-143 Ethylbenzene ug/kg ND 437 473 108 35-144 Hexachloro-1,3-butadiene ug/kg ND 437 411 94 10-160 Isopropylbenzene (Cumene) ug/kg ND 437 440 101 30-152 m&p-Xylene ug/kg ND 873 1020 116 33-145 Methyl-tert-butyl ether ug/kg ND 437 361 83 49-140 Methylene Chloride ug/kg ND 437 489 112 10-174 n-Butylbenzene ug/kg ND 437 428 98 10-160 n-Propylbenzene ug/kg ND 437 468 107 24-159 Naphthalene ug/kg ND 437 336 77 10-171 o-Xylene ug/kg ND 437 507 116 31-150 p-Isopropyltoluene ug/kg ND 437 445 102 21-154 sec-Butylbenzene ug/kg ND 437 452 104 19-159 Styrene ug/kg ND 437 442 101 15-152 tert-Butyl benzene ug/kg ND 437 395 91 31-141 Tetrachloroethene ug/kg ND 437 432 99 19-141 Toluene ug/kg ND 437 517 118 31-146 trans-1,2-Dichloroethene ug/kg ND 437 425 97 28-157 trans- 1,3-Dichloropropene ug/kg ND 437 376 86 25-146 Trichloroethene ug/kg ND 437 442 101 34-149 Trichlorofluoromethane ug/kg ND 437 427 98 10-167 Vinyl acetate ug/kg ND 873 807J 92 10-200 Vinyl chloride ug/kg ND 437 248 57 36-155 Xylene (Total) ug/kg ND 1310 1520 116 29-148 1,2-Dichloroethane-d4 (S) % 72 70-132 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 102 70-130 P2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 SAMPLE DUPLICATE: 2555711 Parameter Units 92425574001 Result Dup Result 1,1,1,2-Tetrachloroethane ug/kg ND ND 1,1,1-Trichloroethane ug/kg ND ND 1,1,2,2-Tetrachloroethane ug/kg ND ND 1,1,2-Trichloroethane ug/kg ND ND 1,1-Dichloroethane ug/kg ND ND 1,1-Dichloroethene ug/kg ND ND 1,1-Dichloropropene ug/kg ND ND 1,2,3-Trichlorobenzene ug/kg ND ND 1,2,3-Trichloropropane ug/kg ND ND 1,2,4-Trichlorobenzene ug/kg ND ND 1,2,4-Trimethylbenzene ug/kg ND ND 1,2-Dibromo-3-chloropropane ug/kg ND ND 1,2-Dibromoethane (EDB) ug/kg ND ND 1,2-Dichlorobenzene ug/kg ND ND 1,2-Dichloroethane ug/kg ND ND 1,2-Dichloropropane ug/kg ND ND 1,3,5-Trimethylbenzene ug/kg ND ND 1,3-Dichlorobenzene ug/kg ND ND 1,3-Dichloropropane ug/kg ND ND 1,4-Dichlorobenzene ug/kg ND ND 2,2-Dichloropropane ug/kg ND ND 2-Butanone (MEK) ug/kg ND ND 2-Chlorotoluene ug/kg ND ND 2-Hexanone ug/kg ND ND 4-Chlorotoluene ug/kg ND ND 4-Methyl-2-pentanone (MIBK) ug/kg ND ND Acetone ug/kg 146 240 Benzene ug/kg ND ND Bromobenzene ug/kg ND ND Bromochloromethane ug/kg ND ND Bromodichloromethane ug/kg ND ND Bromoform ug/kg ND ND Bromomethane ug/kg ND ND Carbon tetrachloride ug/kg ND ND Chlorobenzene ug/kg ND ND Chloroethane ug/kg ND ND Chloroform ug/kg ND ND Chloromethane ug/kg ND ND cis-1,2-Dichloroethene ug/kg ND ND cis-1,3-Dichloropropene ug/kg ND ND Dibromochloromethane ug/kg ND ND Dibromomethane ug/kg ND ND Dichlorodifluoromethane ug/kg ND ND Diisopropyl ether ug/kg ND ND Ethylbenzene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Isopropylbenzene (Cumene) ug/kg ND ND RPD Qualifiers 49 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 SAMPLE DUPLICATE: 2555711 Parameter Units 92425574001 Result Dup Result m&p-Xylene ug/kg ND ND Methyl-tert-butyl ether ug/kg ND ND Methylene Chloride ug/kg ND ND n-Butylbenzene ug/kg ND ND n-Propylbenzene ug/kg ND ND Naphthalene ug/kg ND ND o-Xylene ug/kg ND ND p-Isopropyltoluene ug/kg ND ND sec-Butylbenzene ug/kg ND ND Styrene ug/kg ND ND tert-Butyl benzene ug/kg ND ND Tetrachloroethene ug/kg ND ND Toluene ug/kg ND ND trans-1,2-Dichloroethene ug/kg ND ND trans- 1,3-Dichloropropene ug/kg ND ND Trichloroethene ug/kg ND ND Trichlorofluoromethane ug/kg ND ND Vinyl acetate ug/kg ND ND Vinyl chloride ug/kg ND ND Xylene (Total) ug/kg ND ND 1,2-Dichloroethane-d4 (S) % 100 92 4-Bromofluorobenzene (S) % 97 98 Toluene-d8 (S) % 99 102 RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 469616 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Associated Lab Samples: 92425518006 METHOD BLANK: 2550191 Associated Lab Samples: 92425518006 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/kg ND 330 04/16/19 17:54 1,2-Dichlorobenzene ug/kg ND 330 04/16/19 17:54 1,3-Dichlorobenzene ug/kg ND 330 04/16/19 17:54 1,4-Dichlorobenzene ug/kg ND 330 04/16/19 17:54 1-Methylnaphthalene ug/kg ND 330 04/16/19 17:54 2,2'-Oxybis(1-chloropropane) ug/kg ND 330 04/16/19 17:54 2,4,5-Trichlorophenol ug/kg ND 330 04/16/19 17:54 2,4,6-Trichlorophenol ug/kg ND 330 04/16/19 17:54 2,4-Dichlorophenol ug/kg ND 330 04/16/19 17:54 2,4-Dimethylphenol ug/kg ND 330 04/16/19 17:54 2,4-Dinitrophenol ug/kg ND 1650 04/16/19 17:54 2,4-Dinitrotoluene ug/kg ND 330 04/16/19 17:54 2,6-Dinitrotoluene ug/kg ND 330 04/16/19 17:54 2-Chloronaphthalene ug/kg ND 330 04/16/19 17:54 2-Chlorophenol ug/kg ND 330 04/16/19 17:54 2-Methylnaphthalene ug/kg ND 330 04/16/19 17:54 2-Methylphenol(o-Cresol) ug/kg ND 330 04/16/19 17:54 2-Nitroaniline ug/kg ND 1650 04/16/19 17:54 2-Nitrophenol ug/kg ND 330 04/16/19 17:54 3&4-Methyl phenol (m&p Cresol) ug/kg ND 330 04/16/19 17:54 3,3'-Dichlorobenzidine ug/kg ND 1650 04/16/19 17:54 3-Nitroaniline ug/kg ND 1650 04/16/19 17:54 4,6-Dinitro-2-methyl phenol ug/kg ND 660 04/16/19 17:54 4-Bromophenylphenyl ether ug/kg ND 330 04/16/19 17:54 4-ChIoro-3-methyl phenol ug/kg ND 660 04/16/19 17:54 4-Chloroaniline ug/kg ND 1650 04/16/19 17:54 4-Chlorophenylphenyl ether ug/kg ND 330 04/16/19 17:54 4-Nitroaniline ug/kg ND 660 04/16/19 17:54 4-Nitrophenol ug/kg ND 1650 04/16/19 17:54 Acenaphthene ug/kg ND 330 04/16/19 17:54 Acenaphthylene ug/kg ND 330 04/16/19 17:54 Aniline ug/kg ND 330 04/16/19 17:54 Anthracene ug/kg ND 330 04/16/19 17:54 Benzo(a)anthracene ug/kg ND 330 04/16/19 17:54 Benzo(a)pyrene ug/kg ND 330 04/16/19 17:54 Benzo(b)fluoranthene ug/kg ND 330 04/16/19 17:54 Benzo(g,h,i)perylene ug/kg ND 330 04/16/19 17:54 Benzo(k)fluoranthene ug/kg ND 330 04/16/19 17:54 Benzoic Acid ug/kg ND 1650 04/16/19 17:54 Benzyl alcohol ug/kg ND 660 04/16/19 17:54 bis(2-Chloroethoxy)methane ug/kg ND 330 04/16/19 17:54 v1 v1 v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 METHOD BLANK: 2550191 Associated Lab Samples: 92425518006 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed bis(2-Chloroethyl) ether ug/kg ND 330 04/16/19 17:54 bis(2-Ethylhexyl)phthalate ug/kg ND 330 04/16/19 17:54 Butylbenzylphthalate ug/kg ND 330 04/16/19 17:54 Chrysene ug/kg ND 330 04/16/19 17:54 Di-n-butylphthalate ug/kg ND 330 04/16/19 17:54 Di-n-octylphthalate ug/kg ND 330 04/16/19 17:54 Dibenz(a,h)anthracene ug/kg ND 330 04/16/19 17:54 Dibenzofuran ug/kg ND 330 04/16/19 17:54 Diethylphthalate ug/kg ND 330 04/16/19 17:54 Dimethylphthalate ug/kg ND 330 04/16/19 17:54 Fluoranthene ug/kg ND 330 04/16/19 17:54 Fluorene ug/kg ND 330 04/16/19 17:54 Hexachloro-1,3-butadiene ug/kg ND 330 04/16/19 17:54 Hexachlorobenzene ug/kg ND 330 04/16/19 17:54 Hexachlorocyclopentadiene ug/kg ND 330 04/16/19 17:54 Hexachloroethane ug/kg ND 330 04/16/19 17:54 Indeno(1,2,3-cd)pyrene ug/kg ND 330 04/16/19 17:54 Isophorone ug/kg ND 330 04/16/19 17:54 N-Nitroso-di-n-propylamine ug/kg ND 330 04/16/19 17:54 N-Nitrosodimethylamine ug/kg ND 330 04/16/19 17:54 N-Nitrosodiphenylamine ug/kg ND 330 04/16/19 17:54 Naphthalene ug/kg ND 330 04/16/19 17:54 Nitrobenzene ug/kg ND 330 04/16/19 17:54 Pentachlorophenol ug/kg ND 1650 04/16/19 17:54 Phenanthrene ug/kg ND 330 04/16/19 17:54 Phenol ug/kg ND 330 04/16/19 17:54 Pyrene ug/kg ND 330 04/16/19 17:54 2,4,6-Tribromophenol (S) % 82 27-110 04/16/19 17:54 2-Fluorobiphenyl (S) % 69 30-110 04/16/19 17:54 2-Fluorophenol (S) % 70 13-110 04/16/19 17:54 Nitrobenzene-d5 (S) % 67 23-110 04/16/19 17:54 Phenol-d6 (S) % 72 22-110 04/16/19 17:54 Terphenyl-d14 (S) % 89 28-110 04/16/19 17:54 v1 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2550192 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1670 1270 76 52-130 1,2-Dichlorobenzene ug/kg 1670 1420 85 51-130 1,3-Dichlorobenzene ug/kg 1670 1360 81 50-130 1,4-Dichlorobenzene ug/kg 1670 1400 84 49-130 1-Methylnaphthalene ug/kg 1670 1520 91 55-130 2,2'-Oxybis(1-chloropropane) ug/kg 1670 1440 86 30-130 v1 2,4,5-Trichlorophenol ug/kg 1670 1330 80 55-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 LABORATORY CONTROL SAMPLE: Parameter 2550192 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4,6-TrichIorophenol ug/kg 1670 1360 81 57-130 2,4-DichIorophenol ug/kg 1670 1370 82 56-130 2,4-Dimethylphenol ug/kg 1670 1310 79 51-130 2,4-Dinitrophenol ug/kg 8330 6890 83 27-133 2,4-Dinitrotoluene ug/kg 1670 1410 85 61-130 2,6-Dinitrotoluene ug/kg 1670 1430 86 60-130 2-Chloronaphthalene ug/kg 1670 1340 80 52-130 2-Chlorophenol ug/kg 1670 1480 89 54-130 2-Methylnaphthalene ug/kg 1670 1540 92 54-130 2-Methylphenol(o-Cresol) ug/kg 1670 1520 91 51-130 v1 2-Nitroaniline ug/kg 3330 2620 79 51-130 2-Nitrophenol ug/kg 1670 1330 80 49-130 3&4-Methyl phenol (m&p Cresol) ug/kg 1670 1480 89 11-163 v1 3,3'-Dichlorobenzidine ug/kg 3330 2470 74 10-132 3-Nitroaniline ug/kg 3330 2420 73 55-130 4,6-Dinitro-2-methyl phenol ug/kg 3330 3190 96 47-142 4-Bromophenylphenyl ether ug/kg 1670 1480 89 59-130 4-Chloro-3-methylphenol ug/kg 3330 2720 82 55-130 4-Chloroaniline ug/kg 3330 2660 80 54-130 4-Chlorophenylphenyl ether ug/kg 1670 1380 83 58-130 4-Nitroaniline ug/kg 3330 2830 85 54-130 4-Nitrophenol ug/kg 8330 6580 79 48-130 Acenaphthene ug/kg 1670 1530 92 60-130 Acenaphthylene ug/kg 1670 1610 97 60-130 Aniline ug/kg 1670 1260 75 43-130 Anthracene ug/kg 1670 1590 96 63-130 Benzo(a)anthracene ug/kg 1670 1580 95 59-130 Benzo(a)pyrene ug/kg 1670 1560 94 57-130 Benzo(b)fluoranthene ug/kg 1670 1530 92 54-130 Benzo(g,h,i)perylene ug/kg 1670 1650 99 59-130 Benzo(k)fluoranthene ug/kg 1670 1620 97 54-130 Benzoic Acid ug/kg 8330 5640 68 19-130 Benzyl alcohol ug/kg 3330 3050 91 50-130 bis(2-Chloroethoxy)methane ug/kg 1670 1270 76 54-130 bis(2-Chloroethyl) ether ug/kg 1670 1340 80 48-130 bis(2-Ethylhexyl)phthalate ug/kg 1670 1440 86 45-134 Butylbenzylphthalate ug/kg 1670 1410 85 46-138 Chrysene ug/kg 1670 1570 94 58-130 Di-n-butylphthalate ug/kg 1670 1460 88 60-130 Di-n-octylphthalate ug/kg 1670 1490 89 53-130 Dibenz(a,h)anthracene ug/kg 1670 1620 97 59-130 Dibenzofuran ug/kg 1670 1380 83 60-130 Diethylphthalate ug/kg 1670 1410 85 60-130 Dimethylphthalate ug/kg 1670 1410 85 60-130 Fluoranthene ug/kg 1670 1650 99 65-130 Fluorene ug/kg 1670 1530 92 63-130 Hexachloro-1,3-butadiene ug/kg 1670 1250 75 46-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 LABORATORY CONTROL SAMPLE: Parameter 2550192 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Hexachlorobenzene ug/kg 1670 1510 91 58-130 Hexachlorocyclopentadiene ug/kg 1670 1230 74 23-130 Hexachloroethane ug/kg 1670 1300 78 47-130 Indeno(1,2,3-cd)pyrene ug/kg 1670 1660 99 60-130 Isophorone ug/kg 1670 1270 76 49-130 N-Nitroso-di-n-propylamine ug/kg 1670 1330 80 47-130 N-Nitrosodimethylamine ug/kg 1670 1300 78 45-130 N-Nitrosodiphenylamine ug/kg 1670 1440 86 59-130 Naphthalene ug/kg 1670 1500 90 55-130 Nitrobenzene ug/kg 1670 1220 73 49-130 Pentachlorophenol ug/kg 3330 2610 78 10-132 Phenanthrene ug/kg 1670 1610 97 62-130 Phenol ug/kg 1670 1560 94 46-130 v1 Pyrene ug/kg 1670 1550 93 53-130 2,4,6-Tribromophenol (S) % 95 27-110 2-Fluorobiphenyl (S) % 79 30-110 2-Fluorophenol(S) % 86 13-110 Nitrobenzene-d5 (S) % 76 23-110 Phenol-d6 (S) % 89 22-110 Terphenyl-d14 (S) % 86 28-110 MATRIX SPIKE SAMPLE: Parameter 2550193 Units 92425126005 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg ND 2380 1380 58 18-130 1,2-Dichlorobenzene ug/kg ND 2380 1480 62 14-130 1,3-Dichlorobenzene ug/kg ND 2380 1430 60 12-130 1,4-Dichlorobenzene ug/kg ND 2380 1460 61 10-130 1-Methylnaphthalene ug/kg ND 2380 1640 69 12-130 2,2'-Oxybis(1-chloropropane) ug/kg ND 2380 1660 70 10-130 v1 2,4,5-Trichlorophenol ug/kg ND 2380 1670 70 13-130 2,4,6-Trichlorophenol ug/kg ND 2380 1750 74 17-130 2,4-Dichlorophenol ug/kg ND 2380 1770 74 10-130 2,4-Dimethylphenol ug/kg ND 2380 1650 69 10-130 2,4-Dinitrophenol ug/kg ND 11900 5130 43 10-130 2,4-Dinitrotoluene ug/kg ND 2380 1650 69 24-130 2,6-Dinitrotoluene ug/kg ND 2380 1690 71 23-130 2-Chloronaphthalene ug/kg ND 2380 1390 58 19-130 2-Chlorophenol ug/kg ND 2380 1780 75 10-130 2-Methylnaphthalene ug/kg ND 2380 1640 69 18-130 2-Methylphenol(o-Cresol) ug/kg ND 2380 1890 79 10-130 v1 2-Nitroaniline ug/kg ND 4760 3510 74 17-130 2-Nitrophenol ug/kg ND 2380 1730 73 10-130 3&4-Methyl phenol (m&p Cresol) ug/kg ND 2380 1800 76 10-130 v1 3,3'-Dichlorobenzidine ug/kg ND 4760 3080 65 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 MATRIX SPIKE SAMPLE: 2550193 92425126005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 3-Nitroaniline ug/kg ND 4760 3590 76 24-130 4,6-Dinitro-2-methyl phenol ug/kg ND 4760 3940 83 10-152 4-Bromophenylphenyl ether ug/kg ND 2380 1520 64 29-130 4-Chloro-3-methylphenol ug/kg ND 4760 3600 76 17-130 4-Chloroaniline ug/kg ND 4760 3700 78 14-130 4-Chlorophenylphenyl ether ug/kg ND 2380 1450 61 25-130 4-Nitroaniline ug/kg ND 4760 3840 81 22-130 4-Nitrophenol ug/kg ND 11900 8340 70 10-130 Acenaphthene ug/kg ND 2380 1620 68 20-130 Acenaphthylene ug/kg ND 2380 1750 74 25-130 Aniline ug/kg ND 2380 1540 65 10-130 Anthracene ug/kg ND 2380 1700 72 29-130 Benzo(a)anthracene ug/kg ND 2380 1650 70 19-130 Benzo(a)pyrene ug/kg ND 2380 1650 69 12-130 Benzo(b)fluoranthene ug/kg ND 2380 1650 70 14-130 Benzo(g,h,i)perylene ug/kg ND 2380 1700 71 10-130 Benzo(k)fluoranthene ug/kg ND 2380 1680 71 14-130 Benzoic Acid ug/kg ND 11900 554J 5 10-130 M1 Benzyl alcohol ug/kg ND 4760 3700 78 13-130 bis(2-Chloroethoxy)methane ug/kg ND 2380 1640 69 16-130 bis(2-Chloroethyl) ether ug/kg ND 2380 1640 69 11-130 bis(2-Ethylhexyl)phthalate ug/kg ND 2380 1570 66 21-130 Butylbenzylphthalate ug/kg ND 2380 1520 64 23-130 Chrysene ug/kg ND 2380 1660 70 22-130 Di-n-butylphthalate ug/kg ND 2380 1540 65 30-130 Di-n-octylphthalate ug/kg ND 2380 1580 67 23-142 Dibenz(a,h)anthracene ug/kg ND 2380 1690 71 10-130 Dibenzofuran ug/kg ND 2380 1460 61 24-130 Diethylphthalate ug/kg ND 2380 1540 65 26-130 Dimethylphthalate ug/kg ND 2380 1740 73 22-130 Fluoranthene ug/kg ND 2380 1730 73 33-130 Fluorene ug/kg ND 2380 1600 67 22-130 Hexachloro-1,3-butadiene ug/kg ND 2380 1310 55 13-130 Hexachlorobenzene ug/kg ND 2380 1580 67 29-130 Hexachlorocyclopentadiene ug/kg ND 2380 1260 53 10-130 Hexachloroethane ug/kg ND 2380 1290 54 10-130 Indeno(1,2,3-cd)pyrene ug/kg ND 2380 1700 72 10-130 Isophorone ug/kg ND 2380 1670 70 13-130 N-Nitroso-di-n-propylamine ug/kg ND 2380 1600 67 12-130 N-Nitrosodimethylamine ug/kg ND 2380 1600 67 11-130 N-Nitrosodiphenylamine ug/kg ND 2380 1580 67 15-130 Naphthalene ug/kg ND 2380 1730 73 15-130 Nitrobenzene ug/kg ND 2380 1550 65 12-130 Pentachlorophenol ug/kg ND 4760 3340 70 10-130 Phenanthrene ug/kg ND 2380 1680 71 27-130 Phenol ug/kg ND 2380 1820 76 10-130 v1 Pyrene ug/kg ND 2380 1660 70 19-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 MATRIX SPIKE SAMPLE: 2550193 92425126005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2,4,6-Tribromophenol (S) % 83 27-110 2-Fluorobiphenyl (S) % 45 30-110 2-Fluorophenol(S) % 74 13-110 Nitrobenzene-d5(S) % 67 23-110 Phenol-d6 (S) % 74 22-110 Terphenyl-d14 (S) % 47 28-110 SAMPLE DUPLICATE: 2550194 Parameter Units 92425126005 Result Dup Result 1,2,4-Trichlorobenzene ug/kg ND ND 1,2-Dichlorobenzene ug/kg ND ND 1,3-Dichlorobenzene ug/kg ND ND 1,4-Dichlorobenzene ug/kg ND ND 1-Methylnaphthalene ug/kg ND ND 2,2'-Oxybis(1-chloropropane) ug/kg ND ND 2,4,5-Trichlorophenol ug/kg ND ND 2,4,6-Trichlorophenol ug/kg ND ND 2,4-Dichlorophenol ug/kg ND ND 2,4-Dimethylphenol ug/kg ND ND 2,4-Dinitrophenol ug/kg ND ND 2,4-Dinitrotoluene ug/kg ND ND 2,6-Dinitrotoluene ug/kg ND ND 2-Chloronaphthalene ug/kg ND ND 2-Chlorophenol ug/kg ND ND 2-Methylnaphthalene ug/kg ND ND 2-Methylphenol(o-Cresol) ug/kg ND ND 2-Nitroaniline ug/kg ND ND 2-Nitrophenol ug/kg ND ND 3&4-Methyl phenol (m&p Cresol) ug/kg ND ND 3,3'-Dichlorobenzidine ug/kg ND ND 3-Nitroaniline ug/kg ND ND 4,6-Dinitro-2-methyl phenol ug/kg ND ND 4-Bromophenylphenyl ether ug/kg ND ND 4-ChIoro-3-methyl phenol ug/kg ND ND 4-Chloroaniline ug/kg ND ND 4-Chlorophenylphenyl ether ug/kg ND ND 4-Nitroaniline ug/kg ND ND 4-Nitrophenol ug/kg ND ND Acenaphthene ug/kg ND ND Acenaphthylene ug/kg ND ND Aniline ug/kg ND ND Anthracene ug/kg ND ND Benzo(a)anthracene ug/kg ND ND Benzo(a)pyrene ug/kg ND ND RPD Qualifiers v1 v1 v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 SAMPLE DUPLICATE: 2550194 Parameter Units 92425126005 Result Dup Result Benzo(b)fluoranthene ug/kg ND ND Benzo(g,h,i)perylene ug/kg ND ND Benzo(k)fluoranthene ug/kg ND ND Benzoic Acid ug/kg ND ND Benzyl alcohol ug/kg ND ND bis(2-Chloroethoxy)methane ug/kg ND ND bis(2-Chloroethyl) ether ug/kg ND ND bis(2-Ethylhexyl)phthalate ug/kg ND ND Butylbenzylphthalate ug/kg ND ND Chrysene ug/kg ND ND Di-n-butylphthalate ug/kg ND ND Di-n-octylphthalate ug/kg ND ND Dibenz(a,h)anthracene ug/kg ND ND Dibenzofuran ug/kg ND ND Diethylphthalate ug/kg ND ND Dimethylphthalate ug/kg ND ND Fluoranthene ug/kg ND ND Fluorene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Hexachlorobenzene ug/kg ND ND Hexachlorocyclopentadiene ug/kg ND ND Hexachloroethane ug/kg ND ND Indeno(1,2,3-cd)pyrene ug/kg ND ND Isophorone ug/kg ND ND N-Nitroso-di-n-propylamine ug/kg ND ND N-Nitrosodimethylamine ug/kg ND ND N-Nitrosodiphenylamine ug/kg ND ND Naphthalene ug/kg ND ND Nitrobenzene ug/kg ND ND Pentachlorophenol ug/kg ND ND Phenanthrene ug/kg ND ND Phenol ug/kg ND ND Pyrene ug/kg ND ND 2,4,6-Tribromophenol (S) % 76 75 2-Fluorobiphenyl (S) % 51 57 2-Fluorophenol (S) % 63 56 Nitrobenzene-d5 (S) % 63 58 Phenol-d6 (S) % 63 57 Terphenyl-d14 (S) % 33 69 RPD Qualifiers v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 470714 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Associated Lab Samples: 92425518001 METHOD BLANK: 2555336 Associated Lab Samples: 92425518001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/kg ND 327 04/22/19 19:42 1,2-Dichlorobenzene ug/kg ND 327 04/22/19 19:42 1,3-Dichlorobenzene ug/kg ND 327 04/22/19 19:42 1,4-Dichlorobenzene ug/kg ND 327 04/22/19 19:42 1-Methylnaphthalene ug/kg ND 327 04/22/19 19:42 2,2'-Oxybis(1-chloropropane) ug/kg ND 327 04/22/19 19:42 2,4,5-Trichlorophenol ug/kg ND 327 04/22/19 19:42 2,4,6-Trichlorophenol ug/kg ND 327 04/22/19 19:42 2,4-Dichlorophenol ug/kg ND 327 04/22/19 19:42 2,4-Dimethylphenol ug/kg ND 327 04/22/19 19:42 2,4-Dinitrophenol ug/kg ND 1630 04/22/19 19:42 2,4-Dinitrotoluene ug/kg ND 327 04/22/19 19:42 2,6-Dinitrotoluene ug/kg ND 327 04/22/19 19:42 2-Chloronaphthalene ug/kg ND 327 04/22/19 19:42 2-Chlorophenol ug/kg ND 327 04/22/19 19:42 2-Methylnaphthalene ug/kg ND 327 04/22/19 19:42 2-Methylphenol(o-Cresol) ug/kg ND 327 04/22/19 19:42 2-Nitroaniline ug/kg ND 1630 04/22/19 19:42 2-Nitrophenol ug/kg ND 327 04/22/19 19:42 3&4-Methyl phenol (m&p Cresol) ug/kg ND 327 04/22/19 19:42 3,3'-Dichlorobenzidine ug/kg ND 1630 04/22/19 19:42 3-Nitroaniline ug/kg ND 1630 04/22/19 19:42 4,6-Dinitro-2-methyl phenol ug/kg ND 653 04/22/19 19:42 4-Bromophenylphenyl ether ug/kg ND 327 04/22/19 19:42 4-ChIoro-3-methyl phenol ug/kg ND 653 04/22/19 19:42 4-Chloroaniline ug/kg ND 1630 04/22/19 19:42 4-Chlorophenylphenyl ether ug/kg ND 327 04/22/19 19:42 4-Nitroaniline ug/kg ND 653 04/22/19 19:42 4-Nitrophenol ug/kg ND 1630 04/22/19 19:42 Acenaphthene ug/kg ND 327 04/22/19 19:42 Acenaphthylene ug/kg ND 327 04/22/19 19:42 Aniline ug/kg ND 327 04/22/19 19:42 Anthracene ug/kg ND 327 04/22/19 19:42 Benzo(a)anthracene ug/kg ND 327 04/22/19 19:42 Benzo(a)pyrene ug/kg ND 327 04/22/19 19:42 Benzo(b)fluoranthene ug/kg ND 327 04/22/19 19:42 Benzo(g,h,i)perylene ug/kg ND 327 04/22/19 19:42 Benzo(k)fluoranthene ug/kg ND 327 04/22/19 19:42 Benzoic Acid ug/kg ND 1630 04/22/19 19:42 Benzyl alcohol ug/kg ND 653 04/22/19 19:42 bis(2-Chloroethoxy)methane ug/kg ND 327 04/22/19 19:42 v1 v1 v1 v1 v1 v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 METHOD BLANK: 2555336 Associated Lab Samples: 92425518001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed bis(2-Chloroethyl) ether ug/kg ND 327 04/22/19 19:42 bis(2-Ethylhexyl)phthalate ug/kg ND 327 04/22/19 19:42 Butylbenzylphthalate ug/kg ND 327 04/22/19 19:42 Chrysene ug/kg ND 327 04/22/19 19:42 Di-n-butylphthalate ug/kg ND 327 04/22/19 19:42 Di-n-octylphthalate ug/kg ND 327 04/22/19 19:42 Dibenz(a,h)anthracene ug/kg ND 327 04/22/19 19:42 Dibenzofuran ug/kg ND 327 04/22/19 19:42 Diethylphthalate ug/kg ND 327 04/22/19 19:42 Dimethylphthalate ug/kg ND 327 04/22/19 19:42 Fluoranthene ug/kg ND 327 04/22/19 19:42 Fluorene ug/kg ND 327 04/22/19 19:42 Hexachloro-1,3-butadiene ug/kg ND 327 04/22/19 19:42 Hexachlorobenzene ug/kg ND 327 04/22/19 19:42 Hexachlorocyclopentadiene ug/kg ND 327 04/22/19 19:42 Hexachloroethane ug/kg ND 327 04/22/19 19:42 Indeno(1,2,3-cd)pyrene ug/kg ND 327 04/22/19 19:42 Isophorone ug/kg ND 327 04/22/19 19:42 N-Nitroso-di-n-propylamine ug/kg ND 327 04/22/19 19:42 N-Nitrosodimethylamine ug/kg ND 327 04/22/19 19:42 N-Nitrosodiphenylamine ug/kg ND 327 04/22/19 19:42 Naphthalene ug/kg ND 327 04/22/19 19:42 Nitrobenzene ug/kg ND 327 04/22/19 19:42 Pentachlorophenol ug/kg ND 1630 04/22/19 19:42 Phenanthrene ug/kg ND 327 04/22/19 19:42 Phenol ug/kg ND 327 04/22/19 19:42 Pyrene ug/kg ND 327 04/22/19 19:42 2,4,6-Tribromophenol (S) % 81 27-110 04/22/19 19:42 2-Fluorobiphenyl (S) % 65 30-110 04/22/19 19:42 2-Fluorophenol (S) % 63 13-110 04/22/19 19:42 Nitrobenzene-d5 (S) % 64 23-110 04/22/19 19:42 Phenol-d6 (S) % 64 22-110 04/22/19 19:42 Terphenyl-d14 (S) % 77 28-110 04/22/19 19:42 v1 Qualifiers LABORATORY CONTROL SAMPLE: 2555337 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1690 1380 81 52-130 1,2-Dichlorobenzene ug/kg 1690 1400 83 51-130 1,3-Dichlorobenzene ug/kg 1690 1330 78 50-130 1,4-Dichlorobenzene ug/kg 1690 1400 83 49-130 1-Methylnaphthalene ug/kg 1690 1490 88 55-130 2,2'-Oxybis(1-chloropropane) ug/kg 1690 1280 76 30-130 2,4,5-Trichlorophenol ug/kg 1690 1380 81 55-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 LABORATORY CONTROL SAMPLE: Parameter 2555337 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4,6-TrichIorophenol ug/kg 1690 1430 84 57-130 2,4-DichIorophenol ug/kg 1690 1430 84 56-130 v1 2,4-Dimethylphenol ug/kg 1690 1300 77 51-130 2,4-Dinitrophenol ug/kg 8470 6620 78 27-133 2,4-Dinitrotoluene ug/kg 1690 1370 81 61-130 2,6-Dinitrotoluene ug/kg 1690 1430 84 60-130 2-Chloronaphthalene ug/kg 1690 1490 88 52-130 2-Chlorophenol ug/kg 1690 1410 83 54-130 2-Methylnaphthalene ug/kg 1690 1500 89 54-130 2-Methylphenol(o-Cresol) ug/kg 1690 1470 87 51-130 2-Nitroaniline ug/kg 3390 2430 72 51-130 2-Nitrophenol ug/kg 1690 1390 82 49-130 v1 3&4-Methyl phenol (m&p Cresol) ug/kg 1690 1400 83 11-163 3,3'-Dichlorobenzidine ug/kg 3390 2970 87 10-132 v1 3-Nitroaniline ug/kg 3390 2770 82 55-130 4,6-Dinitro-2-methyl phenol ug/kg 3390 3260 96 47-142 v1 4-Bromophenylphenyl ether ug/kg 1690 1480 87 59-130 4-Chloro-3-methylphenol ug/kg 3390 2690 79 55-130 4-Chloroaniline ug/kg 3390 2800 83 54-130 4-Chlorophenylphenyl ether ug/kg 1690 1370 81 58-130 4-Nitroaniline ug/kg 3390 2610 77 54-130 4-Nitrophenol ug/kg 8470 5970 70 48-130 v1 Acenaphthene ug/kg 1690 1500 89 60-130 Acenaphthylene ug/kg 1690 1550 92 60-130 Aniline ug/kg 1690 1280 76 43-130 Anthracene ug/kg 1690 1540 91 63-130 Benzo(a)anthracene ug/kg 1690 1550 92 59-130 Benzo(a)pyrene ug/kg 1690 1530 90 57-130 Benzo(b)fluoranthene ug/kg 1690 1710 101 54-130 Benzo(g,h,i)perylene ug/kg 1690 1610 95 59-130 Benzo(k)fluoranthene ug/kg 1690 1580 93 54-130 Benzoic Acid ug/kg 8470 4660 55 19-130 v1 Benzyl alcohol ug/kg 3390 2830 83 50-130 bis(2-Chloroethoxy)methane ug/kg 1690 1290 76 54-130 bis(2-Chloroethyl) ether ug/kg 1690 1260 74 48-130 bis(2-Ethylhexyl)phthalate ug/kg 1690 1440 85 45-134 Butylbenzylphthalate ug/kg 1690 1440 85 46-138 Chrysene ug/kg 1690 1530 90 58-130 Di-n-butylphthalate ug/kg 1690 1380 82 60-130 Di-n-octylphthalate ug/kg 1690 1540 91 53-130 Dibenz(a,h)anthracene ug/kg 1690 1640 97 59-130 Dibenzofuran ug/kg 1690 1390 82 60-130 Diethylphthalate ug/kg 1690 1300 77 60-130 Dimethylphthalate ug/kg 1690 1380 81 60-130 Fluoranthene ug/kg 1690 1560 92 65-130 Fluorene ug/kg 1690 1420 84 63-130 Hexachloro-1,3-butadiene ug/kg 1690 1390 82 46-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 LABORATORY CONTROL SAMPLE: Parameter 2555337 Units Spike Conc. LCS LCS Result % Rec Hexachlorobenzene ug/kg 1690 1500 Hexachlorocyclopentadiene ug/kg 1690 1390 Hexachloroethane ug/kg 1690 1260 Indeno(1,2,3-cd)pyrene ug/kg 1690 1640 Isophorone ug/kg 1690 1270 N-Nitroso-di-n-propylamine ug/kg 1690 1330 N-Nitrosodimethylamine ug/kg 1690 1150 N-Nitrosodiphenylamine ug/kg 1690 1450 Naphthalene ug/kg 1690 1480 Nitrobenzene ug/kg 1690 1230 Pentachlorophenol ug/kg 3390 2670 Phenanthrene ug/kg 1690 1520 Phenol ug/kg 1690 1420 Pyrene ug/kg 1690 1650 2,4,6-Tribromophenol (S) % 2-Fluorobiphenyl (S) % 2-Fluorophenol(S) % Nitrobenzene-d5 (S) % Phenol-d6 (S) % Terphenyl-d14 (S) % % Rec Limits Qualifiers 89 58-130 82 23-130 74 47-130 97 60-130 75 49-130 78 47-130 68 45-130 86 59-130 88 55-130 73 49-130 79 10-132 90 62-130 84 46-130 v1 98 53-130 98 27-110 78 30-110 80 13-110 75 23-110 82 22-110 88 28-110 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 469658 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92425518001, 92425518006 SAMPLE DUPLICATE: 2550407 92424661001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 99.6 99.8 0 SAMPLE DUPLICATE: 2550414 92425496002 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 9.7 9.5 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 469671 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92425518002, 92425518003, 92425518004, 92425518005, 92425518008, 92425518009, 92425518010, 92425518011 SAMPLE DUPLICATE: 2550481 92425496003 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 12.3 11.0 11 SAMPLE DUPLICATE: 2550482 92425518011 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 63.9 64.0 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 470156 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92425518001, 92425518006 METHOD BLANK: 2552646 Matrix: Solid Associated Lab Samples: 92425518001, 92425518006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/kg ND 50.0 04/20/19 00:29 LABORATORY CONTROL SAMPLE: 2552647 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/kg 1000 970 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2553953 2553954 MS MSD 2617273001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/kg 52900 735 858 14100 39800 -5490 -1720 90-110 95 M6, R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 469525 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite Associated Lab Samples: 92425518001, 92425518006 METHOD BLANK: 2549793 Associated Lab Samples: 92425518001, 92425518006 Parameter Units Nitrogen, Nitrate mg/kg Nitrogen, Nitrite mg/kg Nitrogen, NO2 plus NO3 mg/kg Matrix: Solid Blank Reporting Result Limit Analyzed ND 4.0 04/16/19 01:45 ND 4.0 04/16/19 01:45 ND 4.0 04/16/19 01:45 Qualifiers LABORATORY CONTROL SAMPLE: 2549794 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/kg 15 15.4 103 90-110 Nitrogen, Nitrite mg/kg 10 10.3 103 90-110 Nitrogen, NO2 plus NO3 mg/kg 25 25.7 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2549795 2549796 MS MSD 92425518006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/kg ND 36 36 39.9 37.4 111 104 90-110 6 Nitrogen, Nitrite mg/kg ND 23.9 23.9 25.4 23.9 101 95 90-110 6 H1 Nitrogen, NO2 plus NO3 mg/kg ND 60.2 60.2 65.3 61.3 105 98 90-110 6 H1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell4/12 Pace Project No.: 92425518 QC Batch: 469716 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92425518001, 92425518006 METHOD BLANK: 2550760 Matrix: Solid Associated Lab Samples: 92425518001, 92425518006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/kg ND 1.0 04/16/19 23:46 LABORATORY CONTROL SAMPLE: 2550761 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/kg 50 52.8 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2550762 2550763 MS MSD 92425518001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/kg 692 116 114 694 433 2 -227 90-110 46 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 67 Pace Analytical Services, LLC ceAnalX cal ® hevi Riverside 04 Asheville, NC 28804 www.pacelabs.com (828)254-7176 QUALIFIERS Project: Powell4/12 Pace Project No.: 92425518 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H2 Extraction or preparation conducted outside EPA method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. P2 Re -extraction or re -analysis could not be performed due to insufficient sample amount. R1 RPD value was outside control limits. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2019 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Powell4/12 92425518 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92425518001 C-1 EPA 3050B 471202 EPA 6010D 471670 92425518006 C-2 EPA 3050B 471202 EPA 6010D 471670 92425518001 C-1 EPA 7471B 470793 EPA 7471B 470897 92425518006 C-2 EPA 7471 B 470793 EPA 7471 B 470897 92425518001 C-1 EPA 3546 470714 EPA 8270E 470836 92425518006 C-2 EPA 3546 469616 EPA 8270E 469682 92425518002 C-1A EPA 5035A 470498 EPA 8260D 470560 92425518003 C-1 B EPA 5035A 470498 EPA 8260D 470560 92425518004 C-1 C EPA 5035A 470498 EPA 8260D 470560 92425518005 C-1 D EPA 5035A 470498 EPA 8260D 470560 92425518008 C-2A EPA 5035A 470498 EPA 8260D 470560 92425518009 C-2B EPA 5035A 470498 EPA 8260D 470560 92425518010 C-2C EPA 5035A 470498 EPA 8260D 470560 92425518011 C-21D EPA 5035A 470498 EPA 8260D 470560 92425518001 C-1 ASTM D2974-87 469658 92425518002 C-1A ASTM D2974-87 469671 92425518003 C-1B ASTM D2974-87 469671 92425518004 C-1C ASTM D2974-87 469671 92425518005 C-1D ASTM D2974-87 469671 92425518006 C-2 ASTM D2974-87 469658 92425518008 C-2A ASTM D2974-87 469671 92425518009 C-2B ASTM D2974-87 469671 92425518010 C-2C ASTM D2974-87 469671 92425518011 C-21D ASTM D2974-87 469671 92425518001 C-1 EPA 351.2 Rev 2.0 1993 470156 EPA 351.2 Rev 2.0 1993 470610 92425518006 C-2 EPA 351.2 Rev 2.0 1993 470156 EPA 351.2 Rev 2.0 1993 470610 92425518001 C-1 EPA 353.2 Rev 2.0 1993 469525 EPA 353.2 Rev 2.0 1993 469534 92425518006 C-2 EPA 353.2 Rev 2.0 1993 469525 EPA 353.2 Rev 2.0 1993 469534 92425518001 C-1 EPA 365.1 Rev 2.0 1993 469716 EPA 365.1 Rev 2.0 1993 469780 92425518006 C-2 EPA 365.1 Rev 2.0 1993 469716 EPA 365.1 Rev 2.0 1993 469780 Date: 04/30/2019 03:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 53 of 67 z �o n n . ._ .-• •-. a o 3 N o m on. a a N w -c o o - X ro -. 7 0 n N n s fD ry ro b' N v w n CD C .. m a- C 0 C 0. a Q 4 ,K m rrDD 7o j ) m v Q d ro o n ro a a - C 3_ m -,w ro CD c m A n o= m a� a P F W l_ r� = 7 6 w w z O O m v w O ; 7 m 7 v 7 w 7 n p 0 � a m o �r A _ w CD N m w C n ID ro n rrDD O 7O O v o y , 3 x a w p < D o I C p D C �� wo a� rL c a vi m LF Lek 1 A n m w r N N r3o CL S ? o t D 'np% N O �_ v P9 ro 3 o'm^ w� D n ° D v m mCD m a ^� o 7 on _ o M21 v ii► �J Lr, O `� m m < ` 0 n A z n n a _ rz °�- - a 3 `� - 3 70 M. n . r90 o n O 1 m m y ! N M <. m y T y or o n v rD v a v ❑ m l ° m w m rn f° o o rna v m m fD n n n }�j _J rD O w a si n ^ a O 00 rrD m m p� O 7 u m 3 3-P 3 a _ O� r$ n u 7 Z Z �-' r6 -a p rb 0 v v p a a cr in in in -� n z ra (no n ( a a ffl n n C, d LLD 3 � � SVbC. �z_ v 3 rs fl D 1C1 opi m n "r N w p ` 3 v C. � = a ii C + O a p aN y C C O fl r3o m C r➢ \v • V �" V�G�7 7 � N n 1 °a � 7-. 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O %o — N m rD _ n �� V7■ p Z o l m rr v y? r- !D n a rr�rounacnccmvmm�nn r6 m a m v Y ro w rn o v s RIG* a c c w a tY W W Y 3 m b 5' 3 rn K rr Y N N tY 0 N aromrowN+v9 roronrtIDrt1) o A o w m Yrt m O O y M 0 n a M m n❑ m x m Q o m I n m N• r- D N m m N w rt N rr `G `C n n00 ro 'D ro Y "I m m O 'D Z m ro Y o fD W e rt ro m x m r c w a m m y m v Y CD n n�Ypm roa r-m mm w ° =� n- `^` '\ 0 rr 0 o a 3 m mz r R wn Q� M m 7 v m n rt r+ N j w o r +romertwr-0)0 7 m rm N�000m 3 w k mn mOM m a oPmvwo Ynnam m wn �n 3 m m m 3 wz m nran e�-•mr�n rt ° X t rt ro r. a m rD 01 v❑ ro m 3 tt N• U; 0 �3 3 o z ID �^ F-+ W F-• m rFr a s�o m n o M rt 7 N• m !A rt ry a r- t u ion m �m m a7 3 m °F+ n 0 N N N O m �C F ro 1 J y RI F' rob n er or O 7 = N rho 'a m 7 rD NHNm Y• 'CODY hi K rt ti rnD C N r' C m D f9 d r* N N m Tf m N H n 'n 17 m w m _ m 2 a O ,m C •• m 7 h IF+ a ;+ 7 �^ rD 'Tt ]0 m m 7 M w r rt n N 3 0, m O -G y 9� Yq n5 •R+9'3� Z o z o n 0 0 n r+ s ape 54 of 67 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: .-Pace Analytical F-CAR-CS-033-Rev.06 I Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, I **bottom half of box is to list number of bottle Project # E v _ U Z 41 y m a 7 m a E a o. m Z a a m a E m a m -a > 2o a E r�i a m a a a ti a ao N P N a E a a a ry V m O = E m a m N cvi q z a E a a m ti T Y O ra Z a E a m j = ,u v �i 'i Z v v Q. n Q m 7 .� c7 a a U 2 E v = .i C7 ¢ '6 } a c E ¢ O m q ¢ ry V a O i E q v — Jh .� 0 a ry V Y O E q E cn m 4D a � V Y E o ry m a m 0 a Q Z V ¢ O> E O r m 0 o ¢ m @ q O 7 O s Q > C Z ¢ ¢ [ O 7 m 0 > Z v m ¢ 0 E O a s 0 a Z m a & y a cn } �p Y ¢ O > y a u a ° M � > I Q u 2 Y E N a Q `_' ai a v"i E N a V ry = z vi; a E Q Q m a m v c E J 4 CD o U a z > c O m — c E O � > 41 ;> m a C 7 a ¢ E m l7 a 1 f i. 2 r { 3 a s 1 6 L 7 r 8 9 �.a { it 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot tt Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wiflhe sent to the North Carolina DII Certification Office (Le, Out of hold, incorrect preservative, out of temp, nocorrect containers. Page 55 of 67 I �FaceAnalytical o National Center for Testing & Innovation ANALYTICAL REPORT April 29, 2019 Pace Analytical - Asheville, NC Sample Delivery Group: L1091257 Samples Received: 04/20/2019 Project Number: 92425518 Description: powel 4/12 Site: 001 Report To: Lorri Patton 2225 Riverside Drive Asheville, NC 28804 Entire Report Reviewed By: �vUnn �v, �. L L111-� Nancy McLain Project Manager t Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V 49 it Page 56 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912.33 1 of 12 I TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 FS C-1 L1091257-01 5 [Cn] C-2 L1091257-02 6 Qc: Quality Control Summary 7 Fr Total Solids by Method 2540 G-2011 7 Wet Chemistry by Method 9066 8 RC GI: Glossary of Terms 9 F Al: Accreditations & Locations 10 Sc: Sample Chain of Custody 11 rAl FSC Page 57 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 2 of 12 C-1 L1091257-01 Solid SAMPLE SUMMARY Collected by Collected date/time 04/12/1914:05 ONE LAB. NATIONWIDE. Received date/time 04/20/1908:45 FP1 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FTC Total Solids by Method 2540 G-2011 WG1272269 1 04/27/19 09:15 04/27/19 09:25 JD Mt. Juliet, TN Wet Chemistry by Method 9066 WG1270924 1 04/24/1912:00 04/24/19 23:36 JER Mt. Juliet, TN Collected by Collected date/time Received date/time C-2 L1091257-02 Solid 04/12/1916:05 04/20/1908:45 [Cn] Method Batch Dilution Preparation Analysis Analyst Location date/time FSrdate/time Total Solids by Method 2540 G-2011 WG1272269 1 04/27/19 09:15 04/27/19 09:25 JD Mt. Juliet, TN Wet Chemistry by Method 9066 WG1270924 1 04/24/1912:00 04/24/19 23:37 JER Mt. Juliet, TN RC F, FAI FSC Page 58 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 3 of 12 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. VV VV� � �t La�'_ Nancy McLain Project Manager FP1 FTC FSS FSr FC-1 F, FAI FSC Page 59 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 4 of 12 C-1 Collected date/time: 04/12/19 14:05 Total Solids by Method 2540 G-2011 SAMPLE RESULTS - 01 L1091257 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 37.0 1 04/27/2019 09:25 WG1272269 Wet Chemistry by Method 9066 Result (dry) Analyte mg/kg Total Phenol by4AAP 2.53 Qualifier MDL (dry) RDL (dry) Dilution Analysis mg/kg mg/kg date / time B 0.594 1.81 1 04/24/2019 23:36 ONE LAB. NATIONWIDE. Cp FTC FSS Batch WG1270924 4 Crl FC F, FAI FSC Page 60 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 5 of 12 C-2 Collected date/time: 04/12/19 16:05 Total Solids by Method 2540 G-2011 Result Analyte % Total Solids 41.4 Wet Chemistry by Method 9066 Result (dry) Analyte mg/kg Total Phenol by4AAP 1.81 SAMPLE RESULTS - 02 L1091257 Qualifier Dilution Analysis Batch date / time 1 04/27/2019 09:25 WG1272269 Qualifier MDL (dry) RDL (dry) Dilution Analysis mg/kg mg/kg date / time B 0.532 1.62 1 04/24/2019 23:37 ONE LAB. NATIONWIDE. Cp FTC FSS Batch WG1270924 4 Crl FC F, FAI FSC Page 61 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 6 of 12 WG1272269 QUALITY CONTROL SUMMARY Total Solids by Method 2540 G-2011 1-1091257-01,02 Method Blank (MB) (MB) R3406278-1 04/27/19 09:25 MB Result MB Qualifier MB MDL MB RDL Analyte % % % Total Solids 0.000 L1091268-01 Original Sample (OS) • Duplicate (DUP) (OS) L1091268-01 04/27/19 09:25 • (DUP) R3406278-3 04/27/19 09:25 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte % % % % Total Solids 76.0 76.0 1 0.00605 10 Laboratory Control Sample (LCS) (LCS) R3406278-2 04/27/19 09:25 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % %_ % % Total Solids 50.0 50.0 100 85.0-115 ONE LAB. NATIONWIDE. — I Cp FTc FSS 4 — Cn FSr — �GI FAI FSC ACCOUNT: Pace Analytical - Asheville, NC PROJECT: SDG: DATE/TIME: 92425518 L1091257 04/29/19 12:33 Page 62 of 67 PAGE: 7of12 M WG1270924 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9066 1-1091257-01,02 Method Blank (MB) (MB) R3405141-1 04/24/19 23:31 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Total Phenol by4AAP 0.333 J 0.220 0.670 L1090654-01 Original Sample (OS) • Duplicate (DUP) (OS) L1090654-01 04/24/19 23:32 • (DUP) R3405141-3 04/24/19 23:33 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg % % Total Phenol by4AAP 1.56 2.35 1 40.3 P1 20 Laboratory Control Sample (LCS) (LCS) R3405141-2 04/24/19 23:31 Spike Amount LCS Result LCS Rec. Analyte mg/kg mg/kg Total Phenol by4AAP 8.33 8.45 101 Rec. Limits LCS Qualifier 90.0-110 L1090836-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) ONE LAB. NATIONWIDE. (OS) L1090836-02 04/24/19 23:34 • (MS) R3405141-4 04/24/19 23:35 • (MSD) R3405141-5 04/24/19 23:35 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Total Phenol by4AAP 1900 U 1590 1570 83.6 82.9 1 90.0-110 J6 J6 0.808 20 ACCOUNT: Pace Analytical - Asheville, NC PROJECT: SDG: DATE/TIME: 92425518 L1091257 04/29/19 12:33 Page 63 of 67 PAGE: 8 of 12 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. MDL (dry) Method Detection Limit. RDL Reported Detection Limit. RDL (dry) Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. Page 64 of 67 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 9 of 12 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T104704245-18-15 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT ND OR MN T ID T WI NY SD WY MI NV T NE IA OH T PA T f IL Ills WY vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Pace Analytical - Asheville, NC 92425518 L1091257 04/29/1912:33 ME Page 65 of 67 PAGE: 10 of 12 Chain of Custody aceAnalyical www.pacelabs.com lei Results Requested By: 41261201� � o Workorder: 92425518 Workorder Name: Powell 4112 Re( Re ort / Invoice To Subcontract To Lorri Patton P.O. it A U f 75 & ' Pace Analytical Asheville Dr. ����a✓A� 2225 Riverside Asheville, NC 28804 ��� Phone 1(828)254-7176 i -2 C? ° c Ernail:lorri.patton@pacelabs.com --r PU 32 a State of Sample Origin: NC Preserved Containers a ll Collect N . Item Sample ID Date/Time Lab ID Matrix X 1 c1 4/12/201914:05 92425518001 Solid X 2 C-2 4/12/201916:05 92425518006 Solid 3 4 5 Transfers Released By Date/Time Received By Date/Time is 2 14 3 Cooler Temperature on Receipt °C Custod Seal Y or N Received on Ice Y or IN D�4j 0 ( 3LU�6 D:PS F1?2 Comments LAB USE ONLY Y or Friday. April 19, 2019 3:34:34 PM FMT-ALL-C-002rev.00 24March2009 Page &Of61 oI 1 Page 67 of 67 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 May 10, 2019 Mr. Robert Martin Martin and Slagle 24 Lookout Terrace Black Mountain, NC 28711 RE: Project: Powell TCLP Metals Pace Project No.: 92427675 Dear Mr. Martin: Enclosed are the analytical results for sample(s) received by the laboratory on April 12, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com 1(828)254-7176 Project Manager Enclosures �pQ AC RFb REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Powell TCLP Metals Pace Project No.: 92427675 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Powell TCLP Metals Pace Project No.: 92427675 Analytes Lab lD Sample ID Method Analysts Reported Laboratory 92427675001 C-1 EPA 6010D SH1 3 PASI-A 92427675002 C-2 EPA 6010D SH1 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell TCLP Metals Pace Project No.: 92427675 Sample: C-1 Lab ID: 92427675001 Collected: 04/12/19 14:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 05/07/19 20:01 Initial pH: 7.24; Final pH: 4.5 Arsenic ND mg/L 0.050 1 05/08/1916:08 05/09/1912:16 7440-38-2 Chromium 0.077 mg/L 0.050 1 05/08/1916:08 05/09/1912:16 7440-47-3 Lead 0.029 mg/L 0.025 1 05/08/1916:08 05/09/1912:16 7439-92-1 Date: 05/10/2019 07:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Powell TCLP Metals Pace Project No.: 92427675 Sample: C-2 Lab ID: 92427675002 Collected: 04/12/19 16:05 Received: 04/12/19 17:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 05/07/19 20:01 Initial pH: 6.86; Final pH: 4.5 Arsenic ND mg/L 0.050 1 05/08/1916:08 05/09/1912:19 7440-38-2 Chromium ND mg/L 0.050 1 05/08/1916:08 05/09/1912:19 7440-47-3 Lead ND mg/L 0.025 1 05/08/1916:08 05/09/1912:19 7439-92-1 Date: 05/10/2019 07:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Powell TCLP Metals Pace Project No.: 92427675 QC Batch: 474059 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP Associated Lab Samples: 92427675001, 92427675002 METHOD BLANK: 2568708 Associated Lab Samples: 92427675001, 92427675002 Parameter Units Arsenic mg/L Chromium mg/L Lead mg/L METHOD BLANK: 2568709 Associated Lab Samples: 92427675001, 92427675002 Parameter Units Arsenic mg/L Chromium mg/L Lead mg/L Matrix: Water Blank Reporting Result Limit Analyzed ND 0.050 05/09/1911:57 ND 0.050 05/09/1911:57 ND 0.025 05/09/1911:57 Matrix: Water Blank Reporting Result Limit Analyzed ND 0.050 05/09/1914:03 ND 0.050 05/09/1914:03 ND 0.025 05/09/1914:03 Qualifiers Qualifiers LABORATORY CONTROL SAMPLE: 2570200 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic mg/L 2.5 2.4 96 80-120 Chromium mg/L 2.5 2.4 96 80-120 Lead mg/L 2.5 2.3 92 80-120 LABORATORY CONTROL SAMPLE: 2570201 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic mg/L 2.5 2.4 98 80-120 Chromium mg/L 2.5 2.5 100 80-120 Lead mg/L 2.5 2.4 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2570202 2570203 MS MSD 92427574001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Arsenic mg/L ND 2.5 2.5 2.5 2.5 99 99 75-125 0 Chromium mg/L ND 2.5 2.5 2.4 2.4 96 96 75-125 0 Lead mg/L ND 2.5 2.5 2.3 2.3 93 93 75-125 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2019 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Project: Powell TCLP Metals Pace Project No.: 92427675 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/10/2019 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 9 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Powell TCLP Metals Pace Project No.: 92427675 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92427675001 C-1 EPA 3010A 474059 EPA 6010D 474139 92427675002 C-2 EPA 3010A 474059 EPA 6010D 474139 Date: 05/10/2019 07:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 9 CHAIN -OF -CUSTODY Analytical Request Document Pace Analytical Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields Company: Billing Information: S Address: Report To: Ema;I To: 4 Copy To: Site Collection Info/Address: Customer project Name/Number, State: ounty/City: Time Zone Collected. L 9� V r �A t }PT[ 1MT1 ]CT ( ET' Phone: Site/Facility ID A: Compliance Monitoring? [ I Yes [ ]No Email: Collected By (print): Purchase Order th DW PWS M t,: Quote #: DW Location Code: Collected By (signature): 1, Turnaround Dale Required: tmmedimely Packed on Ice: ( 1 Yes I ]No Sample Disposal: Rush: Kidd Filtered (if applicable), [ ) Dispose as ipPropriare I )Return ( 1 Same Day I I Next Day I I Yes I ] No I I Archive: I ] 2 Day [ 1 3 Day ] 14 Day I I S Day Analysis: i I bold: (Expedite Charges Apply) ' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GWy, Wastewater (WW), Product (P), Soil/Solid (SL), Oil (OL), Wipe (W P), Air (AR), Tissue (TS], Bioassay (B), Vapor (V), Other (OT) m/ Collected (or Res t, of Composite End Customer Sample ID Matrix ' Grab Composite Start) CI Ctns 7. Date Time Date Time t�iri �35r.�C'?Im l `.Kc-A � ., IMF ON sy■�i Customer Customer Remarks / Special Conditions / Possible Hazards- Type of Ice Used: t Blue Dry None Packing Material Used: Rol uished by/Company:(Signature) Relinq i,hcd by om any: (Signature) Relinquished by/Company: (Signature) i J Radchem sampte(s) screened (<500 cpm); Y N Date/Time: R ved by/Company: (SSignatue)) V;A-i ! '? 14 isvt_ rf by/Compao; (Si0fiAture) Date/Time: [Received by/Company: (Signature) LAD USE O WO# : 92427675 ror IIIIII III III 1111111111 92421675 Container P, _.. - -- Ldu rrolect ivianager: • Preservative Types: (1i nitric add, hi sutluric acid, (3) hydrochloric acid, (4) sodium hydrolpdean5um suRate. tc {6) methanol, (7) sodium htsu;late, (81 sodium thiosulfate, f9) hexane, (A) ascorbic acid, [B) IC) ammon-um hydroxide. (D) TSP, (U) Unpresvned, (0) Orner Custody seals Present/Intact Y 3r NA Custody Signatures Present Y W NA Collector Signature Present Y V NA BottleS intact rY N NA Correct Battles �' N NA Safi€icient volume 7� N NA Sample:; received on Ice '� H NA VOA - Headspace Acceptable Y [J Uso Regullted soils Y NA Samples in !folding itae N NA Re:i duct Chldrinc. errs cat Y N /-„ CStrips-. _- --- Sampie pH Acceptable Y 11 pil Strips: _ Sulride Present Y t7 Y,ead Acetate Strips: Li:R USE ONLY: Lob Sam�jle a / Comments: cLr� SNORT HOLDS PRCSENT (e72 hours): Y ;e N/A Lab Tracking tt: 2350248 moles received via: FEDEX UPS CJknt Courier Pace Courier Date/Time: MT)L LAB USE ONLY f` f f ! f Table u: Acc[num: Onte! ime: Prelogin: PM: PS: l� Lab Sample Temperature info: Temp Blank Re e'v Y R'�NA Therm iDu: D Cooler 1 Temp Upon Receipt: -,?—oC Cooler 1 Therm Corr. Factor: 0 oC Cooler 1 Corrected Temp: oC Comments: Trip Blank Received: Y NA HCL McOH TSP Other Non Conformance(s): I?age: YES / XO of: Page 9 of 9 APPENDIX C MANIFESTS AND WEIGH TICKETS O w z N < =I c z z (7 m O r D m D O J O W 0 o S 6 6 6 0 O p p Fi n U NTERE JAN 2 8 2020 ,y O Z N Z p�z� N� z>z T �` n = rn CD N O T z C O Z m m m � m r zj Z p S m D o �, z MS Z -i W -mi Z cn m f•' Z r n a r O T Z O M 2 n a a 0 G Z 0 0 3 � D C) m CD \ m N z (Y) O o D m m N m m O M o o c� m Go 7N w n r - L m in Go m 3 z N m �-' m D O mo 3 � c z 3 Z OZE C7 O z m m m D = < n D m o ;, c v O 3 i D z 0 O O r 0 O i L SANTE K WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 G B.Address: 4595 �i✓o /^ ,j 3 v d) e N G C. Phone: D. Profile Number: N I of 19 - E. Generating Location: 50A, e G. Phone: It owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: K. Containers. - Type U TYPE UNITS D- Drum P- Pounds Quantity ) B- Bag TN- Tons X- Box CY- Cubic Yards Units 71V 0- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT 7HE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. �, Generator Authorized Agent (Please Print) Shipment Date 66621 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST L C. Phone: iqa f) f� HP -Sff�P D. Truck No./Type: y Fz E. Vehicle License No./State: MVJ Lill'&I % NCO F. Driver Name: (Please Pont) Acknowledgement of Receipt Materials:) HEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIST) jCIN THE GENERAT�O " ORTION THIS MANIFEST. t Date I (156er Signature) A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./State: F. Driver Name: � (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 307O5.2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evensville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill L3 Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill State Road 1336 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. Receipt Date Authorized Signature 0 o p 0 0 0 z c� M v U = Z 0 ui > 0 Z_ � z O a w 1 � M Z p_ W It CD LU M H N U Y W W Uo H F O K Z) N u O N LU K W N p O co �r O Z N W U C) Z J le a U S F O Z L O J Z 'i H lL Z n U ism O M C: yW. H w Z Z Q W S o a H HLU N W W E Z O W Z W i0 fn w w U � � N zce p co Y `L) zaz W, .� UD z n. 0 Z Z Z Q) L8 N 0 o � u � o � m moj � � w WERE JAN 2 2020 r. Q 0 J H W W H 0 Z � Q W U Z Z O H d U N W p z W W d U) z Z cii F00 N It- C1 z co SANTE K WasteServices 650251h Straet,NW, Suite 100 Cievelend, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 A. Generator. t'�� wa•/F %... f..�r rll7t�,"�° .� B. Address: 7 � 9.?r Jar • �/,o.� C r��'l� ,Q�� G��y.�« �.�/�� N4 aft'7f�� C. Phone: (�'�-'�)� S4C" '"�1.i of �� D. Profile Number: !7 /ai / q E. Generating Location: S A M t F G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name:__ I. Owner's Phone: ( ) J. Description of Waste: K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units 0- Other _ 0- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDI710N FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature 66620 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: !.� tl0 �r s� .� � /.�/� C. Phone: (Y..��' e�`/9 - t%✓J 6 D. Truck No./Type: �i8 E. Vehicle License No./State: /ice W �, r� <%� � �% � F. Driver (Please Prinl) AcknowledgementofRecelptMate►IaIa:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR S17E LISTED IN THE OENEF%� pORTIF THIS MANIFEST. G. ��1��/ oment Date / ��. `7 -" (Driver Signature) � �� A. Transporter Name: B. Address: C, Phone: ( ) D. Truck No.Ifype: E. Vehicle License No./State: F. Driver Name: (Please Pdnt) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION�MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G• Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. Authorized Signature Date ' O D r iWA tv-` V In 0 o S 6 Q 6 0 O p n n fD C7 y " RE 'AN 1 6 2020 L Bl� w' � a�0 m Z o O Dz n = z N N < rn m Oz 3 m m N m D Z O = m r G m z m M '-" v -I Z Z m z n rm O RI z O mi 2 0 w m m N Z O O � N m m O m N OI r --I0 0 m c rn ~O -I m o in m 3 z N m � m V O C 3 Z 3 Z O n c O < D z z n m m m D O = D < n � O 3 � y z m O O � O O �n SANTE K T , WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 G B. Address: =Z IML C ree L4�co� D. Pro"le Number: f71 1 E. Generating Location: F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: K. Containers: � TYPE UNITS Type D- Drum P- Pounds Quantity _)0 B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 66627 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: to.16) D. Truck No./Type: a G E. Vehicle License No./State: MW it L�A AJL _l F. Driver Name: (Please Print) AcknowledgementofReceipt Materials: IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST, G•IFShipment Date (Driver Signature) A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No.rfype: E. Vehicle License NoJState: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. i G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m i Receipt Date � i , Authorized Signature � c� 70 m J A J tD W �p O O 6 6 6 D m 0 D r S � 6 O p C n N Q 0 NTERE JAN 2 8 2020 Bl� > �3� ZON z;�h m �I O z. ,T 1z n 2 z N CA rnmz mUl m z O O = Z m m 2 � ZW n w Z 3 N i z z n O T Z O X 8 M O P * o � w _ N z O O r mrri m O -n N C r m o + m CO CD C m Ln m o � w m -o z 3 r o m 3 0 m G� S D m SANTE K VA WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 G B.Address: 2dd4L J6ng�ytc, , Crce IN lAlat1A, s v, Ile . NC 28785' C. Phone: D. Profile Number: 4019 E. Generating Location: nA e F G. Phone: 66626 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: (f?de) �yg • �ss� D. TruuckNoJType: �6 E. Vehicle License No./State: /bfW i4g69 F. Driver Name: (Please Print) AcknowledgementofReceipt Materials: IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE L RAR D IN THE GENEPORTION.DF THIS MANIFEST. P- G.= mentDate (Driver ignature) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: - I. Owner's Phone: ( ) J. Description of Waste: A. Transporter K. Containers: Type CS TYPE UNITS D- Drum P- Pounds Quantity /0 B- Bag TN- Tons X- Box CY- Cubic Yards Units TAI O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. rAll i Generator Aytho zed Agent (Please Print) Signature Shipment Date m m C. Phone: ( ) D: Truck No.lType: E. Vehicle License No./State: 14 F. Driver Na (Please Pdnt) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill i State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. ,i 1-A of ,t 0 r L Receipt Date Q ,4'uthorized Signature T Z m �A� Z � 2020 �� ��,� N p �O1ON tD _ Z O D �OC� (n �o � o�� � � N � ztnD ,T �` zyz n m-t � rn,p=z v�i` � ��� ��z c�mo�v� —I z �m cn rnmz m C o a z � 3 m � N "Z'� rn m ,twit rn z � O � 7C a o to y z 0= m (/� o 0 o r � � z C 6 6 O" Z m O < rn V -I z m � w z 3 z r � z � � a � r o � O C O T 7 � z Q. 0 � � 0 n � M ;O m z u � -I O � � y o cn Z N -i �-' � w m m N z O o � � N m m � O m N C m o � � � � m o � z , ., w � m m N � w -� o � �-. m z � � � N � � m to O a � � C Z 3 c� m Z O 00 n Z � O � � z � G m .Z7 � x m y m � r 3 m ,ZOj fill � G� m D C f�Tl O n D � � O 3 m D z � o r � r OT O O Tt O S�NTE K WasteServices 650251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 478-1952 F B.Address: `7J �lS f4n�'�han f�rc',- k /�C', C. Phone: D. Profile Number: ��) �' -/ 1 E. Generating Location: sVMe f� G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: fo�� Ma-�-:�,o/ K. Containers: Type (1 TYPE UNITS D- Drum P- Pounds Quantity � �) B- Bag TN- Tons X- Box CY- Cubic Yards Units i /`� O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REpU1REMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. is Generator Authorized�Agent (Please Print)` 65E25 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B.Address: /7�v rr3n�L /Ir• Cq, C. Phone: �,� E. Vehicle F. Driver Truck No.lType: ��' ACknowledgementofRecelptMaterlalls:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIS IN THE GENERATOR PORTION OF THIS MANIFEST. • � . •.. G• $hipmentDate i / .�_ .,/ '�_I 1,-' r r Si ` aturo) A. Transporter Name: %` C. Phone: ( ) D;'Truck No.Ifype: E. Vehicle License No./State: % F. Driver Name: i (Pleeae�Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT .INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date / / (Driver Siflnature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Q Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. Shipment Date m m i� ' I „� . li � ` I j i red Signature i i Date i , fV p r� n v w < z _ � m o r -ml D O ;10 Cf) m co 0 0 0 > j 6 < 0 0 c c Fi a (D n ➢ Z o c o�z n r m N � H rn m zz Z m D r U) m n U) z n m C o Z N N m Z p S m c Z z m o V -I Z W m N � a r O r Z O M S n a X O r O O U) O � m w m N z O O 0 N m mLOo TczF O O n m G z c� 07 -1 LIJ w m m W m z 3 m o o O d 3 1 Z O c z < z n m m m D < = O n c D O Z � � m m z A O r0 n ' T SANTE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 4764160 Fax (423) 479-1952 I: B. Address: MZ 7 Z �OnRm7hAA lr r e Y k �t -�• /j. hj. i0 s,,Il e /VC tgR7gf C�J?7i--Ti D. Profile Number: E. Generating Location: SOM e F. If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste:) n 201;4tt±Ed �.t�AS7�r;/.JG±-Cr /�P_Pn'frdn AAA K. Containers: Type 6%EDrum E UNITS D. P- Pounds Quantity 0 TN- Tons CY- Cubic Yards Units 7LO- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. J r .# Authorized Agent (Please Print) Signature NON=HAZARDOUS SPECIAL AND ASBESTOS i WASTE MANIFEST ! C. Phone: (pj �� la 41 - sf3` D. Truck No./type: LI E. Vehicle License No./State: M W `i y G 8 N L. F. Driver Name: (Please Prinl) Acknow ledgementofRecelptMaterlals:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIST IN THE GENE"' R PORTIO, F THIS MANIFEST. ent Date I 1 :3 (Driver Signature) A. Transporter C. Phone: ( ) D. Truck�No./fype: E. Vehicle License No./Slate: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. �r (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Lj Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 �) Haywood County Landfill State Road 1338 Waynesville, NC 28786 Date ! / Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials \ Shipment Date .'U� A��A.�� Receipt Date f 3 40 � U Authorized Signature O i1 D c Z z D m 0 D r z c� a o rl � m cn W W V N 00 0 Q 6 6 0 0 (0). a m p � Z Z y z n=m X rn m z0 z m D r m n m z n ENTERED JAN 2 n 2010 11; Z 2 � rm M m C c z m m w m 5 0 � x z o = m v m z z m O w z 3 z 0 r O 97 z O C) Nco zi i a D m O C O W n w T V m L i m z G x � � � m D n 3 Im -i m SANTE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 4764160 Fax (423) 479.,1952 S C. Phone: D. Profile Number: E. Generating Location: 56(4 C F G. Phone: It owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: Sod d� Fl r d dile *-.Ajamt A eirn7f%,� a4 er d K. Containers: Type d TYPE UNITS ,� D- Drum P- Pounds v Quantity / B. Bag TN- Tons X- Box CY- Cubic Yards Units TN 0- Other O- Other L. Special Handling InsWctions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m ss623 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address:_ �S�b Pf S 0 e i► Df . CaIA V-LA _ �NL af�7l G C. Phone: (���) % �i ^ sSsG D. Truck No,fType: 1400 E. Vehicle License No./State: MW q q WC F. Driver (Please Print) AcknowledgementofReceiptMaIsrlais: IHER EBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. - 561prtlent Date i (Driver Signature) A. Transporter Name: r 8. Address: C. Phone: ( ) D. Truck No.rfype: i E. Vehicle License No./State: F. Driver (Pleaae Print) Acknowledgement of RecelptMaterlala: I HEREBYACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. r G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0" Haywood County Landfill ' State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. `tI,'t,( L<^, 'I o_\ 1( Receipt Date L LUZU Authorized Signature ƒ k \ \ \ \ % �TIERI jA428 20� � » ©) 7o > 0\z C \ z /°2 2�\ \ z c z m /\ \\\ \ƒ\ 2�§> 2 < n 2 ƒ� \ §k§ ± / m \ R § ° § / -EE \ \ Mk n q 2 / INA I �§ ^ 2 CT / _ & / 0 q § m ± / yCD S ~ � \ \ NJ\ » \ NJ m � \ z \ k � 0 0 / \ Lrl \ k § � c / / J / / _ / < j 2 / n \ > z ® > 0 m o q c \ \ / @ = w > a § \ / / o P / o o SANTE K WasteServices 650251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 /� B. Address: _ ys �'� Ti,n �';`{i c,n I`�t k /2c! c. Phone: (� j� S!!GI ,- 9 SG y D. Profile Number: /7 I a i 9 E. Generating Location: 5 orh c- F. Address: G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: J. Description of Waste: / l �G ���r>Ce G {N4� I�.JG?-tr %�c�f�-a<.ov1 PUn d n� a���r u � K. Containers: Type (J TYPE UNITS D- Drum P- Pounds ouantity /6 B- Bag TN- Tons X- Box CY- Cubic Yards units TN O- Other o- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. GeneratorAuthorized Agent (Please Print) ��� � � � �� .. .sssz� NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B,Address: 15L0 PisQA% Qom. /� C. Phone: (g,2B) �n � � - 5S5G D. Truck No./Type: yG E. Vehicle License No.lState: M�1/ �JL � � NG F. Driver Name: 1��t' ! n �J (Please Print) Acknowledgement ofRecelptMateriala:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. �r l_ .� _, �)/�_� G•—I' /� ,� _��Itament Date i / c?{ � / L� D � � , r( river 31Dnaluro) A. Transporter f C. Phone: i Truck No.lType: E. Vehicle License No./State: F. Driver Name: (Plaaee Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT 7HE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. / G. Shipment Date / / (Odver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m (�� ( ''r1 !.f ,�.g (�,-c (.; � �,_ Receipt Date � � ( ) Authorized Signature z G� D O m cNi) w co 0 0 0 0 6 O" Q 0 0 c r) n (D NT ERE BAN 2 2020 SY 01 Z cD z z Pit n=m Uri` z v A A !A p r C�y Lq > N a rn rn Z <rn ~ NLTI m z a 7C D Z O S m r p LO Z W NMI Z U) INA W Z m z r z C) a � O O O N L-A p m T N Z O O —i N m m m a' O m N �I —i c) z �A m m c)� N m m z m m O Z Z _ m Z O0 A D m Gzi m n z n m > rn m D z = F m O p D O A O Z CO --A = c� m D z O O n O o r O O (j T O 0 S/ NTE K T V Waste Services 65025th Straet,NW, Suite 100 Cleveland, TN 37311 (800) 467.9160 (423) 476.9160 Fax (423) 479-1952 E B. Address: 7S%� �o, , k=cr ja�r'E C LN ;!¢L4, D. Profile Number:��I�I 9 E. Generating Location: S6me F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: ( ) J. Description of Waste: soti�1414L C a t,)n s4t 1;d6N=f-(r �i Po„ d m alwer, a K. Containers: Type EDrum E UNITS P- Pounds Quantity 0 0 TN- Tons ACY- Cubic Yards Units C LO- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 66628 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: (LOW) G D. TruckNo.lfype: E. Vehicle License No./State: MW j4q 6j? NG F. Driver �� � (Please Print) AcknowledgementofRecelptmaterials:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date (Ddver Signature) A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./State: F. Driver Name: (Please Print) Acknowledgement of Receipt Materlal8: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley Couniy Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Lj Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evensville, TN 37332 Ranger, GA 30734 Loudon County Landfill L] Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill E3 Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 I hereby acknowledge receipt of the above described materials. •/� r�)I >>�.,� �" f) Receipt Date Authorized Signature N7ERE JAN2ba2UI 9r� N D z z G� A ➢ O co Zz C` m Cl) -A W w V O 00 io N O) co cn o 0 0 C Q Q 6 rn m z --I > :30 O <0 c - rD n o 0 2 O r+ �oC.Np Ova Z D z n = m N � Z SAS rnrn0 m z D m rn m rn z n O � m m 70 Z n m C z z Z D z 0' D O Ti m r O 70 D m O O � 2 � D z :10O O � (7 O rm m C p a Z m m N -1 F+ r� m Z O = m v m z z m O V -I z w z 3 F+ z a r O m z O S D O r N zco 0 N � m m o z o D m 0 N O -A O co n Lo m o -A 0w t3ow�'3 3 O C z D rn m D G) 2 n 3 m SAI�TE K WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 r,• B. Address: A%�L S JOM7kat„ jWL ec 11 ld u, lip ^/c C. Phone:Lpl D. Profile Number: hl 102 E. Generating Location: ja^ e F. G. Phone: If owner of the generating facility differs from the generator, please provide H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: C_1t J,r^ _ r . _ K. Containers: Type 'EDrum E UNITS P- Pounds Quantity TN- Tons CY- Cubic Yards Units "� O- Other. L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m 66629 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST / fa C. Phone: (6,, j G �i�- �sfG D. Tru/ck No./Type: L E. Vehicle License No./State: %�W y`i !ok A)L F. Driver Name: ? ' (Please Print) AcknowledgementofReC011ptMaterlala:IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date (Driver Signature) A. Transporter B. Address: Cy Phone: ( ) D. Truck No E. Vehicle License No./State F. Driver Name: (Please Print) Acknowledgement of Receipt Materfala: 1 HERfBYACKNOWLEDGE THA7 THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED( WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evensville, TN 37332 Ranger, GA 30734 Loudon County Landfill Lj Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill El Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 Haywood County Landfill State Road 1338 Waynesville, NC 28786 I hereby acknowledge receipt of the above described materials. ' Receipt Date :' Authorized Signature NTERE AO fffs�- o O x O LO W U a' O O J J O O 4--I 0 � TCOID z Q O O o WU_W CD 2 H d 00 w Q > z Of LU O O U < 0 Z_ Z Z) H E 0 d O W (+') 2E m F- M Z E d LU LO 00 �_ 7 W fV U Y LO Z U CO W H I- O K � N W O LU W FW- \ x O O Z N W W I� tn o < Qom., � O a Of Z U H Cf) mi W O y� N_ 0 ma U = H of Z C (D 0 0 U fl z F_ W 3 ri LU w Fm Z ts > LULU M w W Z � a a Z Q N o 0 N W H O � N M 7 H N W zW�O .c-> �ily iii CO ��cnczoN LUz z z<W za0 CDZ �z � Q rj FAA� �1-Pzsol- IG' ono N o a o +b O O 0 < Q ~ w O U F- Z Q z LU U U +G to I Ce Phone: (� NOV OlSfiL/ D. Profile Number: P E. Generating Locatlon: 5®wtiE F. If owner of 4h@ generating facility difrers from the generator, please provide: 11. Owner's Name: 1. Owner's Phone: J. Description of DF6Z3F 1MMIM ,EA, G"uoug �M3UHAL A�® ASSEV`dC�� '000. u E Goon NIFESi I E. Vehicle License NoJState: IV I� K DPIV2P A. Yransporter Nat ®.Address: _ _ C. Phone: E. Vehicle License F. ®river Name:_ Truck No.lry�e: IC. Containers: - - (Plaoaa F'rinq Type ® �YPF UNITS Aekn®wled®ement a4 �30 (31N�k �9akerl()fn: I PfEREBY ACKNOWLk;®GE THAT THE ©- ®rdm P- YN• Tons o ABOVE• DESCRIPTION M ERIALS WERE RECEIVED FROM YNE GENERATOR SITE )(- Box CY Cubic Yards Quantity ®- BoAND WERE TRANSNO ED WITHOUT INCIDENT TO THE DESTINATION LISTED x Units O• Other O- Other BELOW. G. Shipment Date 1, I L. Special Handling Instructions: ' (®dvarSlonsture) M. Generator's Certification; I HEREBY CERY(FY THAT YHE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 269 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS, AND, IF Y"11 WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 Generator Authorized Agent (Please Print) Signatureno Disposal Site: (Check One) Bradley County Landfill 282 Landfill an McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 � Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® PolkCounty Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1336 Waynesville, NC 28786 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 ® Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledgereceiptof the above described materials. (}t� LAJAUL Receipt Date � Psi°' ' c LL , O p J O C7 Q ? O _ Z Q C7 Q W W d z O U H a > O Z U 0 O Z Z 7 a O N W O N F- Z_ O_ W n W w m _ z W y 00 W U_ O LU a:~ ON LL 7 U W ^ or: W N Q C) � O O Z ` W n Fn o Q 0 Z N J 0 Cd Q U 0 Z W 0 J Q H � W Z M Z F- M FZ- Z = Z F- N IY LLI Q N 7 J to N U uni N U Z H U u w z w x z W �o 0^0 Z Q N zaz Q N Z z° 00 O N V C 7 C � � H H LU m00 M � K � w � � z S/ N` E WasteServices 65025th Stmet,NW, Suite 100 Cleveland, TN 37311 (800) 467=9160 (423) 476%9160 • Fax (423) 4794962 i I--- DProfile fri If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) K. Containers: ® TYPE UNITS Type D- Drum P- Pounds QuantityB- Bag TN- Tons X- Box CY Cubic Yards Units O- Other 0- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PAF3T 289 OR ANY APPLICABLE STATE LAW AND ARE NOT SUS,1€CT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE SEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 291. Generator Authorized Agent (Please Print) ah�1 �� aRLU ©u9 Truck No./Type: �O !:. Vehicle License�No.IState: /�Wt! yr'ila Q � � F. Driver Name: I1RR.0 WMISM111 A. Transporter Name; B. Address: C. Phone: ( ) Truck No,rrype: E. Vehicle Ucanse No./State: F. Driver Name: (Please Print) AeknowfQdpealent oy Re alpt 119aterlals: l HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION 110A 7RRIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPO� ED WITHOUT INCIDENT TO THE DESTINATION LISTED ®€LOW. G. Shipment Date / / (Driver Sipnetura) Disposal Site: (Check One) Bradley County Landfill 284 Landfill Road McDonald, TN 37353 ® Rhea County Landfill 207 Sanitary Drive €vensville, TN 37332 ® Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 © PolkCounty Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 20788 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 ® Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date Receipt Date z c� D O m (N/,) Ovl N W 0 0 0 Q 6 6 S 0 0 c o D iN N_ O CD z�z ( rm m D n = z rn rn m m ,� N m � 5 p 7C D Z o S m m p U) Z W -mi Z mw Z cn m z '+ n n V m m N Z O O � N m m m o T O -1 r0 .Zm7 n m m m z C7 N cn -4 m w m z 3 r � N � Lri m w O a 3 C Z 3 z Z O m C7 _ Z ;7 D m 0O m0 m z n (� m m D > z = A m o � c N O 3 S m D z m o p a O � � r O O ,n 0 SANHTE K VIV lk A& AAA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476.9160 Fax (423) 479A 952 G B.Address: "15 12 J1 ^raJ.EAA Lree Mo D. Profile Number: NI 1 E. Generating Location: *Ve If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: S6Ill cis+ I etl LnjQ51e %,A)6 '' L LL�lf/fttr#I PeA 1A-%. , r K. Containers: Type EDrum E UNITS P- Pounds Quantity TN- Tons CY- Cubic Yards Units %/1/ O- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m J) 66636 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B.Aduress: C. Phone: tp Aji it 7Y_SS3G D. Truck No./Type: E. Vehicle License NOJState: M\oV qq 4h 164 F. Driver (Please Prnf) AcknowiedgementofRec iptMaterlal6:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTfp IN THE GENERATQO PORTION OF_THIS MANIFEST. -P, foment Date / 7 (Driver Signature) A. Transporter fa C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./State: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Ej Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1336 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. � �-jtA r� )(-F� - Receipt Date 1 "2 Authorized Signature WERE JAN 2 6 2020 s� z c) O D m u..) w w rn to w � 00 0 C) C) 6 O' 6 0 0 C n Q V m T N Z O O � N m mo No mn � ro m 00 Z (On r �_ m o rn .p m a z r � N m Ln o N C c z 3 z Z O m n Fi O � z m = o T m z n ;az m D = I < n > m o D 0 O 3 m = z o O o 0 0 O 0 SANTE K IVA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800)467-9160 (423)476-9160 Fax (423) 479-1952 B. Address: N9 S Toe4di^a. G�erk Ra• C��T.LL-3 D. Profile P E. Generating Location: �j' = F. Address: G. Phone: ( If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: J. Description of Waste: K. Containers: � TYPE UNITS Type D- Drum P- Pounds Quantity 010 B- Bag TN -Tons X- Box CY- Cubic Yards Units TN 0- Other. O• Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature .666-34 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B.Address: /JVU r/7ggh IJr. G C�01.6^ -t _ NC o�6MLifto C. Phone: fW�) G yR s6� D. Truck No.mype: 4 E. Vehicle License No./mate: F. Driver Name: "• / (Please Pdnt) AcknowledgementofRecelptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISW IN THE GENERAJOA'PORTION OF THIS MANIFEST, G 1L �Ir ent Date F(D ver Signature) A. Transporter B. Address: r C. Phone: ( ) D. Truck No.lType: hicle License E. Ve F. Driver % (Pleeea Print) Acknowledgement of Recelp{Materials: I HEREBYACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver SigAature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Q' Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m { Y % �1 �l. / j ^1 Receipt Date! Authorized Signature CJ � C z Z O D n G� 0 O m N � N N �w 00 000 6 6 6 0 D r H Q Q c D fl. J O N N zl�z� fD Oz cn 2• �T zn n2rn t�°n` UOI a m m z c O = Z < W -I z n w z 3 rn cn I z n ra- 0 91 z O w4 S n a 0 CD o � 2 r O G) ` m = N Z n O U CD O m v O N C: r - m o O m 00 N m 3 z r O rn m r O v C: 3 z 3 Z O n C Z < MT v z c) m O m m D J. D < n n O c n O 3 m D z 0 o O o O (7 Tn O SANTE K Waste Services 650 25th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 B. Address:_ a 5 ya M 7h a L / CA IT 1A)arintty, hP Ale A2A*0I A01 if C. Phone: (116) �19/��UjL4j D. Profile Number: d4lor / '7- E. Generating Location: 5 XA o F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: ( ) J. Description of Waste: A4d K. Containers: Type D TYPE UNITS D- Drum P- Pounds Quantity �b B- Bag TN- Tons X- Box CY- Cubic Yards Units T/� 0- Other. O- Other. L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature ��►�� Hcr?S 66632 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: �✓ �U 1r7s31A 4 )✓ar• 7i G Truck No./Type: �y E. Vehicle License No./State: AI%Awlg46, NIL F. Driver Name: r, jr, %fI L? �° +fir. rot if (Please Print) AcknowiedgementofReceiptMaterials:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. d:x : ' ;, . Shipment Date /, /at ) (Driver Signature) A. Transporter B. Address: C. Phone: ( ) D. Truck No.,'fype: E. Vehicle License No./State: F. Driver Name: �� (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G• Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evensville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m Authorized Signature Date T F� D W �G D m O D r rni O D m N N In 0 0 0 0 Q 6 6 6 < O p c c n a 0 NTERE JAN M, o�z CD \a ? cn D_ rm Z D Z N n=m N N < p r C OM D o m z m O z 3 m Nm Ilk m Z $ x m � o � z S rn z V z z m `m" r `� z r z z n n � O UM z O P MrmnI _cnG)mD70 cn m � w z 3 CD Ln ZnO mO CD 3 Zca I rn n m O A DOa:m � n D o 0 3 m D z 0 o O O O SANTE K T VA L A& WasteServices 65025th Slreet,NW, Suite 100 Cleveland, TN 37311 (800) 467.9160 (423) 476-9160 Fax (423) 479-1952 B.Address:_ 45 15 1eA61JUTA l!ec / . 015AUAe s,1.11 P 7 R 5' C. Phone: t jd D. Profile Number: 41 f2i OF ' 11 E. Generating Location: Sd/Va F. If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of IIWaste: p K. Containers: Type 49EDrum E UNITS P- Pounds Quantity a b TN- Tons CY- CubicYards Units "rA/ O- Other. L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, Generator Authorized Agent (Please Print) Signature Shipment Date m m ``. 66633 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: 5G d =150ka 13 LaT _Cap.-f„� __f_ r✓c a8�r� C. Phone: (�,1�j la bS- S"f f<o D. Truck No./Type: yS E. Vehicle License F. Driver Na � (Please Print) AcknowledgementofReceiptMateriala:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTE IN THE GENERATOR PORTION OF THIS MANIFEST. G• Q)Shipment Date OL/ Z% / �d (Driver Sipnatu A. Transporter C. Phone: ( ) D. Truck E. Vehicle License F. Driver (Please Pdnq Acknowledgement of Receipt Miterlals: I HEREBYACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 �t Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. t i 1r r 1- �' Y Receipt Date Authorized Signature PJT b\-(C NTEF E JAN 2 8 202U / �� � 4 B: � c \ M \ CD % z / E i \ \ n�\ rm CD F % < a & \ \ \ / \ 0 p c @ > \ % » m k 2 2 ® * > E k) § @ v z ƒ \\\ \ z mk < n � �z / k § n j 0 ; / � 0 q § / ± § e z z \ x ? a CD fQ _ \ \ 2 » \ / 3 e / / j ) 2 \ k % 0 / ? / z 0 \ / m \ > < 0 z \ \ \ j o < \ \ ( \ \ > z 2 8 / z « 0 o / 0 0 2 0 SANTE K WasteServices 65025th Street,NW, Sufte 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 B. Address: 4�'�S J4nA71�Gv� Cree l�' !��• C. Phone: D. Profile Number: �I ar � / " I E. Generating Location: �M L F. G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: p� s6 � i ci ��' e d ii� w5'�e_ I,�a"f-(/ /`�c+{��•o�v K. Containers: Type b TYPE UNITS D- Drum P- Pounds Quantity �ZQ B- Bag TN- Tons .� X- Box CY- Cubic Yards Units � O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature sss�� NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: /�is0 /- � 74w %. !J f • _ C. Phone: (�,�o) GyB•.�S,�G D. Tr/uck No./Type: 4� E. Vehicle License No./State: /1+1W NyV � NL F. Driver ' "� � � �' / (Please Print) Acknowledgement of Receiptl(Aateriala:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR ��1'ION OF TH�NIFEST. r A. Transporter C. Phone: ( ) D. Truck No.ffype: E. Vehicle License No./State:__ r F. Driver ;. �: / % (Please Print) Acknowledgement of Receipt Materials: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED ;WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. >lr Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Traii Elizabethtown, KY 42701 Crittenden Counly Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m Authorized Signature {-;�� � Receipt Date � �� Y°�' 0 �oz� Z y Z n=m N z rnrnz0 m rn D r m rn m z n a z m Z O z 3 m Z D r O rn Z O 2 n 0 r N Z 0 0 o � N m m V m m N Z 0 o n A N m %m O m N C m o � -A A m c z m mco II -i m v m 3 z o m m o 3 C Z 3 O o z n m m 3 m m D z = m O n n O O 3 m y z � O Or O r O O ,m, 0 SANTE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467.9160 (423) 476-9160 Fax (423) 479-1952 G f C. Phone: D. Profile Number: HIl!�I E. Generating Location: /i" C F If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description ofI Waste: Solt ; � e d L�t2 R `i tl f ,) GT P:161 Magi :/ft,,./ K. Containers: Type Quantity Units L. Special Handling ED-Drum Instructions: TYPE er P- TN- CY- O- UNITS Pounds Tons Cubic Yards Other M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature s s73a NON=HAZARDOUS SPECIAL AND ASBESTOS B. Address: / E. Vehicle license F. Driver WASTE MANIFEST Truck No./Type: �is / (Please Print) ACknOwledgementOfR@C@IptMeterials:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE!LJSYD IN THE GENERATOR PORTION AFT (tS MANIFEST. Shipment Date / river Signature) A. Transporter C. Phone: ( ) D. 'truck No.lType: E. Vehicle License No./State: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G• Shipment Date / ! (Driver Siflneture) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray Couniy Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. 1, y- k1 ,k . 'v y r ,) Receipt Date Authorized Signature � m � 61 z Z =i �C C m z n m --I C Orn t JAN J u 2020 ey r 3 r Az 'IoO' (D� o�D 0• �T z n=m N` < �Co+a x m w Na v z N Z Wo D 0 0 0 � Z m C �66 m W -I Z w Z 3 n F+ z vmi ~ a z � n p 73 O O M a � S n a o � M p c0 Z m O D O � O n V T ~ m Z = N Z no M p c o > p N m O mn N r m O O C� m CO Z r L m r w m Ul m m a) z 3 r N � o m in p -a c 3 -' c Z 3 �1 Z 0 n c m D m v z m m m r 3 G) z m D = 0 p 3 N = G� m D z 0 o o O D O O T o — SANTE K WasteServices 650251h Street,NW, Suite 100 Cleveland, TN 37311 (B00) 467-9180 (423) 476-9160 Fax (423) 479-1952 C. Phone: V� D. Profile Number: l!� I � � 1 ' i7 E. Generating Location: .Sr►rU e F. G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of VV<' �i]'1 /J I K. Containers: � TYPE UNITS Type D- Drum P- Pounds Quantity cZ0 B- Bag TN- Tons X- Box CY- Cubic Yards Units � 0- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 269 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART Z81. Generator Authorized Agent (Please Print) Signature Shipment Date m m L�.�L_L_.J �6635 NON -HAZARDOUS SPECIAL AND ASBESTOS C. Phone: (� E. Vehicle License F. Driver N WASTE MANIFEST Truck No./Type: 4� � / (Please Print) AcknowledgementofRecelptMaterlals:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTE� )N THE GENERATOR PORTION OF THIS MANIFEST. ,! ��' ' °' �� p �"ir,,��',d Shipment Date �` / � �/ Za (Driver Siptiature) A. Transporter Name: �� C. Phone: ( ) D. Truck No.ffype: E. Vehicle License F. Driver �' (Please Print) Acknowledgement of Recelpt�Materlals: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. � Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 ,< a Haywood County Landfill � State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. ipt Date � �� �� Authorized Signature O ha C < C� m o D m O D r m ➢ O m co o W 0 0 0 Q Q om > j a' < 0 0 c o D U r 3 r o o A O�zl Z � Z nim z V p r rn m 0 3 z D r m rn n m z n 1020 BY m C o Z mr N m D ~ A Z p S m v Z Z m o W Z m ~ � z 0 r O m Z O -�i S n n a O r ri Z y o N N m r V m fail N Z O O ri ➢ m N m m O m N C m o r - o c� m co C) N W m o m -a z r � N � in m 0 0 -a c 3 O C Z � m z n Cl m Z D = C O C D O 3 m z A O 0 O n TI C SANTE K WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 L B. Address: !1 -1 Tor A 07kir,,, 1, rc 0 /L�% C. Phone: D. Profile Number: E. Generating Location: 50M C F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: _ !Li ed / do a% /f'►a �rr.�, G� K. Containers: Type aEDrum E UNITS P- Pounds Quantity �� TN- Tons CY- Cubic Yards Units N O- Other. L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 66637 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: cBaB) G yd ' fG D. Truck Nod type: 76 E. Vehicle License No./State: M W 4/1/%8 /iC F. Driver (Please Print) AcknOwledgementofReceiptMaterials:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE &L LISTED IN TTHE GENERATOR PORTION OF THIS MANIFEST. G. �,f/ /n *�Shipment Dateg' 1 (Driver Signature) A. Transporter C. Phone: ( ) D. T(lick No.liy{5e: E. Vehicle License No./State: r' F. Driver `(Pleeee Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATEF(IALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. t' G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill El Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill � Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 Haywood County Landfill State Road 1338 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. Shipment Date (_ �9�- Receipt Date + � , ' i ' I Authorized Signature \ ) z $ \\\ \\\ ƒ e � § / ) 2 2 .� , E: /- (n z /d4 f om �rn \z §� X j \ z m @ § § _ M ) ° z ¥ v ° 2 § z § § w Mi 2 § d m z q n - ) \ _ n > m \ \ \ § j % § / 2 ] k \ \ 3 z } \ \ 2 \ } < 9 / j z n / & m § $ % < @ 2 C / / ) ) § ƒ 2 j / \ 0 o « 0 SANTE K VA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800)467-9160 (423)4764160 Fax (423) 479-1952 B.Address: y�IS %OgAA2te• v C. Phone: wdlr)�Il f — D. Profile Number: N� 01) 9 E. Generating Location: SOMC F. If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: K. Containers: Type Quantity Units 66638 NON=HAZARDOUS, �;; SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: (gotb) y - sSSG D. Truck No,frype: M E. Vehicle License No./State: /HW 41FIL V ?\j +-. F. Driver Na - i (Please Print) ACknow ledgementofRecelptmaterials:IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR,, PORTION OF THIS MANIFEST. Shipment Date dver Sip tune) A. Transporter Name: B. Address: C. Phone: ( ) E. Vehicle License No./State: F. Driver Name: Truck No./fype: � TYPE UNITS % (Pleaae Pdnq D- Drum P- Pounds Acknowledgement of Re�Ceipt Materials: 1 HEREBY ACKNOWLEDGE THAT THE 2b LB. Bag TN- Tons ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE - Box CY- Cubic Yards AND WERE TRANSP R, iD WITHOUT INCIDENT TO THE DESTINATION LISTED Tw - Other O- Other BELOW, G. ° Shipment Date L. Special Handling Instructions: (Driver Signature) M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, Generator Authorized Agent (Please Print) Signature Shipment Date m m Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Laudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 ,f 0 Haywood County Landfill ! State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 k 1 1 hereby acknowledge receipt of the above described materials. �( 14 , , Receipt Date! �(J Authorized Signature FNTERE JAN 3 0 2020 BY M G) p r-i - c c D m � � D O -I z m w Lriri tD o 0 0 G< m z > j 6 � O O a(D o II m n r 3 r �00� O�>1 Z � Z n 2 m N z A O 3 m D r m m In m z n (D ,rnT m c o z m m N m x Z O x m v z Z m O V �l Z w Z m m z a r O mn z O X x a a O z O O C) D z ;0 V m m m N Z O O ;;o N m m O m C x p r0 �_ m co z O N to rn m m Z w m r m z w m o O a 3 C z 3 z O n --i O z O < m m m0 m z n m D m < n D O m 0 3 _ m D z 0 0 o D 0 r O O O 0 Apr, WasteServices 65025th Straet,NW, Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 4764160 , Fax (423) 4794952 D. Prome Number: E. Generating Location:50MC F. If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: V UV �FEUVQL Ah 11[U A919LSYUS E. Vehicl F. Driver A, Yransporter Q V�O4dE GVW� \h 1HP1Z`�� Yruclt No./Type: y� C. Phone: ( ) .Truck No.ITy�e: E. Vehicle License No./State: F. Driver Name: K, Containers: — (Please nrinq Type ® TYPE UNITS Acknowledgement oi? R alpt P&IReVISls: I HEREBY ACKNOWLEDGE THAT THE FFOOther--- Drum P- Pounds p®®VE• DESCRIPTION P:7CUTA6S WERE RECEIVE® PR®RX THE GENERATOR SITE Quantity Beg TN- Pons AND WERE YDANSf��y ED WIYb®!1Y INUI®t NY Y® THE DESTINATION LISTED Box CV Cubic Yards /% Units �� O• Other ®E! ©w. L. Special Handling Instructions: Signature G• ° Shipment Date (0rivar Sipnetur®) Disposal Site: (Check One) ®radley County LandPlil ® 282 Landiill Road McDonald, TN 37353 ® Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 © Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® Polk County Landfill 3477 FM 942 Wes4 Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 ® Gordon County Landfill 1224 Pleasant HIII Road Ext, NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 Kuhn Road West Wes4 Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. � Receipt Date O N z Z O D cQ O > li cf) m CO Lj CO ul �L� �p o O 6 6 6 D m 6 � O p c c � a C o O z O N H z�z z W V H rn n 0 3 rn D r N rn n rn z n > m Z 2 TT. ©T r C u m m NLrj m Z 0 = Z XS wml Z w Z 3 N Z a r O -n Z O X 2 n a 0 N o � n0 m m CD z 0 o m A N m co o "T� N C �... ---I m o o 0 A 0 m Ln m o p rn w z m 0 y c 3 C Z 3 Z O C O < H v z n n m D rn z m p < n 0 L3 p0 3 --q = 0 rn D z 0 O o O r O O „ Cbwlend, TN 37311 (800) 4874160 (423) 476.9160 Fax (423) 479-1Q52 L B.Addnss:_9� JOna-i�.ar e t-e•e� ,r — D. Profile • F. G. Phone: It owner of the generattng facility dlfters from the generator, please provido: H. Owner's Naha: I. Owner's Phone: ( ) J. Description of Vvaste: K. Containers: Type Ouantfty units 6sasv:�■ NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST G. Phone: D. Trucl(No.rrypa: LAB E. Vehicle License No./Stato:_ M W �i� (e� �C. F Driver Name: (Pia■.■ PrnQ AcknowladganzaritoPGlocotptMam"JIM:IHEREBYACKNOWLEDOE RECEIPT OF THE ABOVE43ESCRIPTION MATERIALS FOR TRANSPORT FROM a HR GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date ! / (Driver alpnatun) A. Transporter Mai B. Address:-- C. Phone: E. Vehk:le License F. Driver Name: Truck No,rfype: d TYPE UNITS (P19ace Pr{nq D- Drum P- Pounds Acknowledgement of Re elpt Nfaterials: I HEREBY ACKNOWLEDGE THAT THE B- Beg TN- Tons ABOVE- DESCRIPTION ERIALS WERE RECEIVED FROM THE GENERATOR SITE X- Box CY Cubic Yards AND WERE TRANSPOR ED WITHOUT INCIDENT TO THE DESTINATION LISTED I N O- Other O- Other BELOW, / G• � Shipment Date= / ! L. Special Handling 1„structigns: (Driver SipnaNn) M. Generator's Ceriificatlon: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, Generator Authorized Agent (Planes Print) Signature Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 { Polk County Landfill 3477 FM 942 West Leggett, TX 77350 ® Murray Couniy Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext, NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabeihtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials, Receipt Date. l I oxtab Aut Ized Signature T � D � z n � � n m v m r O D r �YS. 3AN 30 2010 v a OE m �Ocp cn z CD zz zI � D z (D -�D O Npz r�m tj Om m <C Z o, m z0 m M m r z o = m 14 Ni n v S 0 0 0 r a Q Q m Z m < w z w z 3 � z -� z a � n r 00 O � Jp a � z O O = X 0 O rw U E ��► ..A Naste5ervices a50251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 476.9180 Fax (423) 479-1952 G B. Addreas: Zti> ai Jooh6i an _ i�emmm ® ni,npsvdl io NC aeq 795� C. Phone: D. Profile Number:_- E. Generating Location: :5drn o F. N )WHAZAKUOUS SPECIAL AND ASBESTOS WASTE MANIFEST _Cane= G. Phone: (&V) :15�0(�D. Truck No.C7ypa: 46 E. Vehicle License No./State: M I J YS OP 6�G F. Driver Name; (Po�zae Prnq ACkngwledgemento7i3ac©1piMIMor1at3:IHEREBYACKNOU&EDGE RECEiPTOF THE ABOVE•DESCRIPTION P:7ATERIALS FOR TRANSPORT FROM THE GENERA fOn SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST, G. Phone: ( I G. Shipment Date / / (Ddwr SlpMtura) If owner of the generating facility differs from the generator, please provide: H, Owner's Name: TRANSPORTER • I. Owner's Phone: ( } J. Description of Wee A. Transporter Name: S0 Wt12A Q a/ o er+c tA3 a+ex B.Address: Re+eA-lion iron d Mck±e r; o, C. Phone: ( ) Truck No,rrypw E. Vehicle License No./State: F. Driver Name: K. Containers: � tpla.ee ar4,tt Type 6 TYPE UNITS Acknowledgement of Re efpt Materials: I HEREBY ACKNOWLEDGE THAT THE D- Drum P- Pounds ABOVE• DESCRIPTION ERUILS WERE RECEIVED FROM THE GENERATOR SITE Quantity a0 B. Beg TN- Tons X- Box CY Cubic Yards AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED Units TN O- Other O- Other Y BELOW. G. . Shipment Date= / / L. Special Handling Instructions: (06verSignalun) M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WA8TE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Places Print) Signature Is Disposal Slte: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 { Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Murray County Landfill 5565 Highway 411 Scuih Chatsworth, GA 30705 2899 � Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1520 Audubon Trail Elizabeihtawn, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. . Receipt Date d� Aut razed Signature JAN 3 02020 ; > �`> CIO m� Z O�z (D �T zm co = ` X z c> In (n �v�o coi2< rn(Mccyll0 m � rnmO m 0 Z z m m N m rn cn r z Z O= m rn m � D Z 0 0 o r �p 0 6 am mw -i Z mW Z IML m U4) r z NMI n 0 0 MOP MM c Z o A `l� n a o co C z D 0 o J -A z co m m N z O m N m m m ODO T O ;;a CD C7 m OJ m z IQWP (In m m ,.- m a z 3 r N � w m rn oc 3 c z_ 3 z z O _ D 0 0 z z0 m 'i m m DO m Z n ll m D D z = n n ;IJ3 D z o � O D O r O (� m O 0 I Ef ' vAk A NasteServices 650251h Strs•t,NW, Bulls 100 Cleveland, TN 37311 (800) 487d>1180 (423) 476.018D Fax (423) 479A 062 G ®.Address: —t = C meek (L� - - ..- - C. Phone: �.i.0)�-_ •,� �a.�� D. Profile Numbers E. Generating Locnilonw. F, G. Phone: If owner of lho gonerating fedlity dl}f®rs from the generator, pl®osg provfd®: Owner'sH. I. Owner's Phone: K. Containers: Type Quantity Units 00 C)Lj SPECIAL AND ASBEST WASTE MANIFEST r C. Phone: (&V to 48'" $$5( D. Truck No./Type:. �,(9_--- — E. Vehicle License No./State: M W L(4 (eA1 i�C F. Driver Name:_. (Plans P&O AoknowledgorewntofReco➢plMaterials: I HEREBYACKNOWLE080 UNCEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM 7HR QErdERAYOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date / 1 (DdwrSipnatun) A. Transporter Net B. Address:_ - _ C. Phone: E. Vehicle License F. Driver Name nowiadyenlent o t5 TYPE UNITS Ackf '—"� D- Drum P- Pounds ABOVE• DESCRIPTION 1 B• Beg TN• Tons X- Box CY Cubic Yards AND WERE TRANSPOq 1 N O• Other 0- Other BELOW. / L. Spertiel Handling InstNctions: M. Generator's CerUfcetlon; I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED,ANOARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature In Truck No;/type• (Pleaea Pdnq slpt MateAala: 1 HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. (DdSipnatun) Shipment Date= / / wr Disposal Slte: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Murray County Landfill 8565 Highway 411 South Chatsworth, GA 30705 2D99 � Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. L Receipt Date CtU Author d Signature T mi n o mcry w w rn w to m LtJ oro .A N 0 0 0 O U 6 i� 3 �oo�a O�>1 z�z n 2 m z V � H A r < O rn rn z 3 m m m z n 2020 E z (D T X c m a Z m m Lq m Z C = m v Z -� X p W mq Z w Z m N ? :O o w O N r m z 00 m N Z O NJ -mi NJm m m 00 O m O -i n m m C� N � � m o �+ w m z � N rn N m V O n 3 c Z 3 z -i O z m > p z n m m m D G� A AO n D O 3 D z � O 0 0 O c r O O O G F E L AL A NastOServdces 65025th Strset,NW, Sullo too Cleveland, TN 37311 (800) 467.9180 (423) 470.0160 Fax (423) 4794952 5 C.Phona:�) raLClfo g5t/y D. Profile Number: W 0?19 / E. Genorating Lonllon: 50m le F, G. Phone: ( IP owner ofIF the generating facility differs from the generator, please provide: N jN-HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Addroea: Ise � 1— !� O� nin mil'. C. Phone: (&V) Wii?e.5506 D. Truck No.nype: 'AtS E. Vehicle License No./State: M W� isG F. Driver Name: USTI t—> 1 QuL. (Please Print) AcknowindijorelantofRouolptMaterials:IHEREBYACKNOWLU030 PuuCRIPT OF THE ABOVELMESCRIPTION MATERIALS FOR TRANSPORT FROM 0'a GEN21 . WOR 517E STE® IN TN ENE TOR PORTION OF THIS MANIFEST. G• Shipment Date / _ / (D ver posture) — H. owner's Name: I. Owner's Phone: ( ) J. Description of Vilaste: A. Transporter Name: SOlr�tZ4 A)Qd:: W Q+6ir B.Address: Re.+enyion Pon Cy Q+tp r; al C. Phone: ( ) Truck No,/Types- E. Vehicle License No./State: F. Driver Name: K. Containers: (Pkxm Print) Type TYPE UNITS Acknowledgement of Re alpt Materials: I HEREBY ACKNOWLEDGE THAT THE b- Drum P- Pounds ABOVE• DESCRIPTION ERIALS WERE RECEIVED FROM THE GENERATOR SITE Quantity Ro B- Beg TN- Tons X- Box CY- Cubic Yards AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED Units I N O- Other 0- Other BELOW, G. A Shipment Data= L. Special Handling Instructions: (Driver Signature) M. Generator's CerOficatlon: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT 8UBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 208 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature No Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 �{ Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Murray County Landfill 8565 Highway 411 Soulh Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials, QAk Receipt Date uthorized Signature L �I3olau O c n N z �D =i D m O D r O D mco .co co O O Q 6 Q > S O p C�7 JAN 3 0 2o.2o Z Q�i oN (n� Z i"11 OzDz N` n = rn Z N O H n Ul Qf UI rn < rn o Z rn z m m N m m C -�{ m Z Z = X < v -1 Z n Imb m m r z � r �\ O �\ z Z Q A n v � o r M Z 2 D O CO m = m m m y N Z O 77 m O 0 � m mN m m coO m mm Noc o m m n z (n m c� -A � m m O o ko m a z 3 N m w m a O C Z_ 3 Z O (7 C O z > D m p z n m D 4 m C ; D 0 00 3 2 m D z 0 O 0 O O S T E L A& A vvast&Services 650251h Strsat,NW. Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 476.9160 Fax (423) 479,4952 B.Addreaa:•�� Jonglw&P Cree 2� e r C. Phone: D. Profile Number: E. Generating Locallon: F, G. Phone: If owner of tho generating facility dIR®rs from Ute generator, please provide: H. Owner's Nahia: • f eUp mmt K. Containers: � Type Quantity 0 Units I N �I tI i t>r hIJN-IiAAIAKWUS SPECIAL AND ASBESTUS WASTE MANIFEST Il,Addroso: �5%® Ps�.aa�. D% �0 C. Phone: ( ) qg >�Cg D. Twok No.11ype: E. Vehicle Licenoo No./Steta: F Driver Name;_ (Plana Print) llcknowtedgereLontor[douolpBMateriAll:IHEREBYACKNDVVLEUSE RUCEIPT OF Yt1E ABOVE -DESCRIPTION MAYERIALS FOR TRANSPORT FROM 7HU 6UVJ0 r0R SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date / / (Ddvar Signature) A. Transporter Nal B. Address: C. Phone: E. Vehcle License F. Driver Name: ^ TYPE UNITS Acknowledgement of D- Drum P- Pounds B Beg TN- Tons ABOVE- DESCRIPTION A X- Box CY Cubic Yards AND WERE TRANSPOR @- Other 0- Other BELOW, / L. Speaal Handling InstNctions: M. Generator's CerOfication: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT 8UBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 28B AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, Generator Authorized Agent (Please Print) Signature Truck No./•fype: (Plaa•a Prht) eipt MateNale: I HEREBY ACKNOWLEDGE THAT THE RUILS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. � Shipment Date_ / ! (Driver Signature) Disposal Site: (Check One) Bradley Couniy Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 { Polk County Landfill T = 3477 FM 942 West Leggett, TX 77350 Murray County Landfill fi565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials, Receipt DateI�V Aut ized Signature i co z (7 m m D O �70 m U) cn w � v CDC) 0 0 0 Q Q Q >j O p C 7 fi a O D `D Z MOMI rn <�oz m m N T Z o = m v � z Z rm� X V Z w Z 3 N Z rm 0 T Z 0 x A a X 0 M Z O �\\ O ~ m am com �J D N z n o d 70 rn C D r0 ;U N m m coO T NJ C ® O -i —I ,Zml m co M z v m m m F, � -A o m � z N 11 m O a x 3 C Z_ _ m Z O 0 c z O m m D D x m r O z n n A m m D z x A m o � c n O 0 3 = G) m D z rn o O D � O Ti O 0 O L L. L VAlk A Wastebervices 6025th $60,NW, Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 476&0100 Fax (423) 479-1952 5 D. Profile Number: E. Generating Locallow. 1=, NDWHAZARDOUS SPEILAAL AND ASBESTOS WASTE MANIFEST B.Address: �J%® P�SOralr. flIL G. Phone: (&) (041L D. `iruc!(NosrPOC E. Vehicle License No./Stele:,__ M!t_ li i28 �C F. Ddver Name; (Plaata Print) ACknOwl©dbornont of Rocolp$ (7nional6: I HEREBYAck%vg0WL00GE RECEIPT OF THE ABOVU�DESCRIPTION MATERIALS FOR TRANSPORT VnOP.1 70a OnNERATOR 517E LISTED IN THE GENERATOR PORTION OF THIS MANIFESTS G. Ph ( } / G. Shipment Date one: (Drivar 6lgnature) If owner of the generating facility differs from the generator, please provide: H, Owner's No e: TRANSPORTER I. Owner's Phone: ( ) J. Description of Waste: A. Transporter Name: 504leA (A)QnEh3,Wa+e,ir B•Address; Re+e ,j0Non Po a CYOot±f r a1 C, Phone: ( ) Truck Na;/rypa: E. Vehicle License No./State: F. Driver Name: K. Containers: (Plan" PMI) Type 6 TYPE UNITS Acknowledgemeny pt MateNala: I HEREBYACKNOWLEDGE THAT THE D- Drum P- Pcunds ABOVE- DESCRIPTIALS WERE RECEIVED FROM THE GENERATOR SITE Quantity �� B- Beg TN- TonsX- Box CY CubicYards AND WERE TRANSITHOUT INCIDENT TO THE DESTINATION LISTED Units 1 N O- Other. 0- Other BELOW, G. Shipment Date= L. Special Handling Instructions: (Driver signature) DESTINATION Disposal Site: (Check One) Bradley County Landfill ❑ Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED Rhea County Landfill E3 Gordon County Landfill MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY40 CFR PART 207 Sanitary Drive 1224 Pleasant HIII Road Ext. NE 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL Evansville, TN 37332 Ranger, GA 30734 REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, ANDARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING Loudon County Landfill L3 Hardin County Landfill TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE 21712 Highway 72 North 1620 Audubon Trail OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND Loudon, TN 37774.5837 Elizabethtown, KY 42701 DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 260 AND Polk County Landfill ❑ Crittenden County Landfill IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 723D1 Generator Authorized Agent (Please Print) Signature I hereby acknowledge receipt of the above described materials, Shipment Date m m �J�Jtlk, Receipt Date Aul brized Signature T O �p c z cn O� � 61 c z 0 D r D Ol U1 J D 07 o 0 S Q 6 ' IN 3 U 2020 r 3 r �00 O�z z � H z y Z n=m Z rn m z 3 m D m rn n m U) z n o � N aw _ m r m � m D N Z n O m CDC \ D N m m w o Tcmr m No m G Vm m i r m N p m v z 3 r -I tz m O c ZO G D m mp z n m_ x Z m D O 2 -{ < n y A O 3 m D z m 0 o O r O O " .ANTE Waste'5ervices W0251h SUGMINW, sun.100 Clevaland,TN 37311 (800) 467.9160 (423) 476%9180 Fax (423) 47SA052 L C. D. Profile Number:,. E. Generating Locatlow. F, G. Phone: If owner of the generating fac]lity dllT®rs from th® generator, please provide: H. Owner's Natn®: I. Owner's Phone: ( t=1 FORM wunrm�f I • NtJWHAZARDOUS SPECIAL AND ASBESTUS WASTE MANIFEST A. Transporter B, Address:_ C. Phone: (w "5J!� D. Trunk No.rfypo A8__ E. Vehicle License NodState: M \n1 i6 � L? c F. Driver Name: (Plate Print) AcknowledgemontofRocolpiP.T cir1ols:IHEREBYACKNOWLEDGE RECEtPTOF THE ABOVE40ESCRIPTION MATERIALS FOR TRANSPORT I;ROM •TF1E OENP ATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST: C. 'Shipment Date (Driver slpnaWn) A. Transporter C. Phone: E. Vehk:ie License No.lS F. Driver Narne: K. Containers: Type Dm d TYPE UNITS ACknowledgement of O B- Bag TN- Tons Pw Pounds Quantity ABOVE• DESCRIPTION 6 XM Box AND Unite I N O- Other OY Other Yards BE OWERE TRANSPOR L. Special Handling Instructions: M. Generator's Cerlificatlon: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature so Truck No,l7ype: olpt Materials: 1 HEREBY ACKNOWLEDGE THAT THE RU1LS WERE RECEIVED FROM THE GENERATOR 817E OUT INCIDENT TO THE DESTINATION LISTED G. ' Shipment Date / / (DriSipnatun) aer Disposal Slte: (Check One) Bradley County Landflll 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 3T332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 �{ Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Murray County Landflll 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. �' Receipt Date �0 Auth zed Signature k & \ � 5 j / / / < z |\ \ < \ \ \ \ � \ o \§% \ \ § \ m /PPV� � \\\\ \ mr \ > \ �4 § $� § 0 p c > % m \ < m 2 � \ E k) m � � S \ NMI z m / � 2 � � m yINA ^ R 0 z 0 X x \ e m C) / § m e § / 2 ! � 5.A.PTE K Wclsfeservices SM25thstrae,NW, 8u1I01*00 Cleveland, TN 37311 (800) 4874180 (423)478&9180 Fax (423) 479=1952 Ba Addraas: — Z! D JOr�n ��aan C rce k 2a i G. Phon®: IP owner of the generattnH facility differs from the generator, please provide: H. Owner's Natne:. I. Owner's Phone: ( ) J. Description of Waste: So l i�-'iec� t J Q5+1LA) O,+UU K. Contalnere: TYPE UNITS Type D- Drum P- Pounds Quantity i;?o B- Bag TN- Tons X- Box CY Cubic Yards Units 1 N 0- Other O• Other L. Special Handling Instructions: M. Generator's Cerdfication: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT 8UBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature N JWMAZARDQUS SPECIAL AND ASBESTOS WASTE MANIFEST r J I . Truck . E. Vehicle License F Driver (Ph•t• Print) Acknowled amanto RoeoipatOrlak:IHEREBYACKNOWLEDOePRCEIPTOF THE ABOVE40ESCRIPTION MATERIALS FOR TRANSPORT FROM THIN CRNERATOR SITE LIS DIN THE GEN ;ORPORTI F THIS MANIFE3S G ipment Date (Drkw Slpnefuro) 1' � A. Transporter Name• B. Address: C. Phone: ( ) Truck No,fType: E. Vehicle License No./State: F. Driver Name: .. (Phew Pdnl) m Acknowledgeent of Re aipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION WERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW, G. A ' Shipment Date= (Driver Sipnaturo) Disposal Slte: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 ® Murray County Landflll 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Troll Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials, Receipt Date Authorized Signature T � Z v < c� m O D m W W V V Ui N 000 6 a a 0 0 C 7 ("i fl. D U Arreli, JAN `� t+ 9020 ch > �� n� 3F' cD 7 OCP (D z H n T nz =rn (p < r CN a A m y O rnrnzz m tm+ m 3 O x Z Z O = Z r -I m X m Z m O m W -i Z w Z m Z IML z r n O m Z O n a M O r H Z � C) � m N Z O O N m m O m N c r m O —{ O m a m Z r Om r m m m 3 z r _I N � m �o c 3 - c Z_ 3 Z O n C O < D m _ m0 z D m m m O m O O cD) � p p0 0i n -i = c) O D z o O � O O -" FEK L VA& 6 VvVasteServlces a50 251h Slmel,NW, Sidle 100 Cleveland, TN 37311 (800) 4674160 (423) 476*9100 Fax (423) 479A 982 Nc a9''G4S- C. Phona: D. Profile Number: 4y a19 E. Generating Local)on: F G. Phone: If owner of lho gonorating fatality differs from the generator, please provide: H. Owner's NsMe: I. Owner's Phone: ( r Aov vwtnT W6 r A r r ter«_ 6o��ao NCINwHA%4AKL)VUS SPACIAL AND ASB :b I Ub 'WASTE MANIFEST ,��� G. Phone: (&V t'O 8 e D. T ruck No.ffype: a E. Vehicle License NoJState: M lA 'gg1QA_y G F. Driver Name: .. / (PNae PrinO AcknowledgementofRace 1ptI ab:IHEREBYACKNOWLEt)GE RECEIPTOF THE ABOVE40ESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIST4ffi IN THE GENgIqTOR POSV910OF THIS MANIFEST. ipment Date �r Ddwr Sipnatun) A. Transporter C. Phone: E. Vehk:le License F. Driver Name: K. Containers: Type D• Drum TYPE P- Pou dsITS Acknowledgement of Quantity oZ O B. Beg TN- Tons ABOVE• DESCRIPTION A X- Box CY- Cubic Yards AND WERE TRANSPOR Units I N O• Other. O• Other. BELOW, L. Special Handling lnStNCtiOns: M. Generator's CerOfication: I HEREBY CERTIFY THA7 THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE A3 DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 280 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Truck Na,lType: / (Pleew P�q alpt Materials: I HEREBY ACKNOWLEDGE THAT THE iIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. � Shipment Date= / / (Driver Sipnetun) Disposal Slte: (Check One) Bradley Couniy Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 j{ Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Murray County Landfill 6565 Highway 411 Souih Chatsworth, GA 30705.2099 � Gordon County Landfill 1224 Pleasant HIII Road Ext, NE Aanger, GA 30734 Hardin County Lend1111 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 723D1 I hereby acknowledge receipt of the above described materials. M& r.)K-' k—' Q Receipt Date � j!�;� v Authorized Signature \ \ \\\ /D \\\ \� \ NTERF ]AN ] § � > \� Z �• rn \ � � r § E k) � � § m M m 2 z z - k a 0 § ) k z CQ m - a / z 2 _ \ m » / § m _ / ) 2 m 2 3 \ m @ 3 $ 2 \ > / m $ 4 / § * / a % } \ \ y \ ) S 2 ƒ z / 2 \ § > \ \ o « 0 � T 1E K Wj 7 L�� A Nasfes'ervices 65025th Stnst,NW, Suite 100 Clevdmnd, TN 37311 (800) 487-9180 (423) 470&9160 Fax (423) 479-1952 G B.Addreas; `tun an reek C. Phone: Q�g) r ti�0 � 9 J(9 y D. Profile Number:_ E. Generating Location: F. G. Phone: If owner of the generating fatality dlPfere from tho Generator, please prov(de: 00 013 N MasHAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B, Address: I�� ® 1— 15 CA nor. flC. CQl1T�n- G. Phone: (") �Q Li8 �� D. Truck No.ilypo: E. Vehicle License F, Driver Name:,r��' (ftus Pint) AcknowledgemontogRocelptMatarlala:IHEREDYACI(NrJNJVR®GE RECEIFTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM 711E GENERATOR SITE LISIV IN THE GENE t+'D TOR PORTIO THIS MANIFEST. G/ pr6ent Date 2atwdwr 86811n) I. Owner's Phone: ( ) � J. Description of Mste: A. Transporter Sr'[k-le,4 I A) A PVJrPr ., 014V Cr S.Address:_ (Z C,+er%-brio n ` o CYI. a :%.a r � n,.( K. Containers: - Type TYPE UNITS D- Drum P- Pounds Quantity .010 9- Beg TN- Tons X- Box CY Cubic Yards Units 1 N O• Other. O- Other L. Special Handling Instructions*Instructions*s: M. Generator's Certification; I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WA8TE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOt 8UBJECT TD FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Pdnt) Signature C. Phone: E. Vehk:le License iver Tuck No,lType: Acknowledgement of Re alpt MateNals: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION EAIALS WERE RECEIVED FROM THE tENERATOR SITE AND WERE TRANSP0 ED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW, Shipment Date= (Driver SipuNn) Disposal Site: (Check One) 282 Landfill Road 9radley County Landfill ❑ Murray County Landfill 6555 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill Ll Gordon County Landfill 207 Sanitary Drive 1224 Pleasant HIII Road Ext. NE Evensvllle, TN 37332 Ranger, GA 30734 Loudon County Landfill ❑ Hardin County Landfill 21712 Highway 72 North 1620 Audubon Troll Loudon, TN 37774.5837 Elizabethtown, KY 42701 Polk County Landfill L3 Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. ^Receipt Date �0 thorized Signature � p 00 D (J7 m T�J - D O -I z m z V Ll N o 0 0 C 6 Q 6 m z > j 0'< O p c DrD N_ 0 m 3 r r �o0-P z�z n=m O z A rn m Oz m m D m m n m z n 'AN 30�.a� BY Z (D , r rri �cu01+a z m M N m O A z o = m o z z m O z w z 3 m a r O On z O EMI n a X O N z D o Cn O o N r —I Z m m N Z O D N m m w O T 0 O �_ � n z m m C� N -� mO rn m N m m mo z N I 9: Ln m w O o 3 C Z 3 z z O z � � O -i < O O m ;7 m0 H m = m Z n D m m D z _ m < _o O n0 n m D z o 0 o O C7 T O m O 65025th 369,NW, Suits 100 Cleveland, TN 37311 (SDO) 467-9180 (423) 47S-91S0 Fax (423) 479-1952 BA Address: �J= �Or�"l�ar Me ®A)n1ffAPSL1d1i0 r A)C �RT7R� D. Profile Number:i r��C E. Generating Location: �®� I; G. Phone: It owner of the generating facility d8fers from U10 generator, please provide: H, Owner's Nefie: • n OWHAZARDOUS SPECIAL AND ASBEST011, WASTE MANIFEST A,TranspoRer C Qf1 G. Phone: (&V) (fly a �� D. Truck No.nype: __ � E. Vehicle License F. Drver Name: (PNe■s Prim) 1lckngwkdgement of Recelp8 i47ag01 1111 : I MERESTACKNOWLE®GE RECEIPT OF i trE ABOVE -DESCRIPTION MATERIALSOFORAMBIP,ORTFROM THE GENERATOR L DIN THE GENE TOR POF THIS ANIFEST. Gp• htpmant Date,-�f (bri rSlpnaWn) A.TranspaRer C. Phone: Truck No./Type: E. Vehk:le License No./State: . ` F. Driver Name: K. Containers: (PI■■w Pdnt) Type b TYPE UNITS Acknowledgement of Re elpt Materials: I HEREBY ACKNOWLEDGE THAT THE D- Drum P- Pounds ABOVE• DESCRIPTION ERIALS WERE RECEIVED FROM THE GENERATOR SITE Quantity �� B- Beg TN- Tons X- Box CY Cubic Yards AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED Units 1 N O• Other O- Other BELOW, G. Shipment Date= ! ! L. Special Handling InstrucUons: (DrivuSign■tur■) D• Disposal Site: (Check One) Bradley County Landfill ® Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART Zee AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, Generator AuthoRzedAgent (Please Print) Signature Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date A t orized Signature O i1 c CJl ➢ sl c z u� V z m1 A D O m w w m pp 00 O p O 6 6 6 0 D r H O O Q 0 D r 3 H zoOC� .o Z z�z nim A rn m OZ z m r rn rn n m Z n w'AZ tD, (D , rm T (D ff (A 01 In r C L D m m � m Z O = Z v Z m w m r Z F+ � r O MM Z OJ Z � m N z O O H � r rn m O n N C F m o --i O n rn z m r O rj CDLil m w m v z 3 r � o m °` O w c 3 -1 Z 3 Z O O C O < U ➢ = D m O z m m z m = m O o no m D z o O � 0 O O �n bi 650251h Strs•t,NW, Suits 10c Cleveland, TN 37311 (800) 467-9160 (423) 47&916D Fax (423) 479-1952 L • Profile Number- � s G. Phone: If owner of the generating fnclliiy dlfforc from Oho generator, please provide: IN Owner's 1. J. Description of Whstwo� rEotmm L' �- NC iN-HAZAKDOUS S OLUTAL AND ASBESTOS WASTE MANIFEST - C. Phone: ( ) (o�� D. Ilvo9t No.�Po: E. Vehtole License F. Driver Name• (PI•u• Pmf) AcknOwlotlHorronto9t3o alpiM&terlakl:IHEREBYACKN0WLUD0U WECSIPT OF THE ABOVEZESCRIPTION MATERIALS FOR TRANSPORT FROM THE eerjHRATOFt B'IaTE LI DIN THE C3ENERA OR PORTf P �N;IS 111ANIFE'5 A. Transporter ►` e�ntio n t"o n� C. Phone: ( ) . Truck No,rlype: E. Vehicle License No./Stela: F. Driver Name: K. Containers: (PI•■w Pdnt) Type TYPE UNITS Acknowledgement o40ER Re olpt Materials: I HEREBY ACKNOWLEDGE THAT THE D- Drum P- Pounds ABOVE* DESCRIPTIONIALS WERE RECEIVED FROM THE GENERATOR 817E Quantity �� B- Beg TN- Tons X- Box CY Cubic Yards AND WERE TRANSPOD WITHOUT INCIDENT TO THE DESTINATION LISTED Units 1 N 0- Other O• Other BELOW, L. Speael Handling Instructions: M. Generator's Cedificatlon: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE aTATE LAW AND ARE NOT 8UBJECT TO FEpERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 208 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature G• ' Shipment Date= (Driver Sipn•tun) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext, NE Evenavllle, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Troll Loudon, TN 37774-5837 Elizabethtown, KY 42701 �{ Polk County Landfill West Leggett, TX 77350 3477 FM 942 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 1 hereby acknowledge receipt of the above described materials. Date/ Authorized Signature 0 LL O O J O o O O z w p O Lli O w = U z O0. W E < z O Z) U O z z JO � w AD z `� w M w W ID ~ ° z Y W \ F o w O \ W O w � o � w o z N W 2 w N C7 z (n o o 0 2 o _ a o) Z U mi N O J w O = Q U S O U Z o V' C 9 O S J Q u z W Z Viol LU g Z n U W Z F- M Od, w Z w � a CO NN kO CO M he O 5 z L N N LU Fill N W> F. z Z Q IA O J 10> U) L 2 Ul t0 fA U > ^w O � w z N < 7 Z Y ! J w 2 O U z V)Z CO t� Q Z r Cl) 2 o Z O SON O Z W '� S.A TE L Wasteservic,es 65025th 860,NW, Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 47&9180 Fox (423) 479-1962 L C. Phone: D. Profile Number 4q o�E. Genera0ng Location: F. G. Phone: NON -HAZARDOUS SPLCIAL AND ASBESTOS WASTE MANIFEST B. dress: ® _ �IS.ot Ck DC . C. Phone: () {Q L{g m sr556 D. Truck No./iype: M E. Vehicle License No./State: M W b too F. Driver Name: {Plow PrinQ AcknowladgementoFt3Out) 1ptt1 atorlak:IHEREBYACKNOWLR®Cfa RaCEIPT ®r THE ABOVE -DESCRIPTION MATERIALU FOR TRANSPORT FROM THE 611ANERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date / / . (DriverSiynttun) If owner of the generating feGlity dlRera from the generator, please provide; H, Owner's Name; I. Owner's Phone: ( ) J. Description of Waste; A. Transporter Q C. Phone: E. Vehicle License No.lS K. Containers: F. Driver Nama: Type d TYPE o UNITS Acknowledgement of D- Drum P- Pounds Quantity';?ABOVE• DESCRIPTION 6O B- Bag TN- Tons AND WERE TRANSPOfj � X- Box CY Cubic Yards Units I N O- Other O- Other - BELOW, Truck No,lType: / (Pie.w Prtnt) olpt M�teNale: I HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. ' Shipment Date= / / L. Special Handling I„struCtions: (t7riversiprutun) M. Generator's Ce�cati0n: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY as CFR PART 281 OR ANY APPLIGABLE STATE LAW AND ARE NOT 8U8JECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLA881FIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WA87E HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 j� Polk County Landfill 3477 FM 942 West Leggett, TX 77350 ® Murray County Landfill 6565 Highway 411 Souih Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 reby acknowledge receipt of the above described materials. Receipt D e Authorized Signature o o p J O Z Q w OU O F p H O W = O w z Q U J W O w U Z = w > z O � U O z z O W Ln O H � Z M W r M F- N O U W r Z Y GoW U CDO' LL N LU O N W H � 4 ') � o 0 z w N o o 0 U C 7 C � H H � � o m a Lfl N N N ¢w O Z �I N raj NasteServgces 650251h StrsN,NW, Sullo 100 Ckvl.nd, TN 37311 (800) 4874180 (423) 470U0100 Fax (423) 479=1952 r d�.Addrngs:�,'"!LP ' `�"1 611% f 2� C. Phone:$) D. Profile Humber: P% gf 9.�Y E. Generating Lcepllon: A&VI t; F G. Phon®: Il owner of the generating facility dlfi'srs from the generator, please provide: H. Owner's Na1ne: I. Owner's Phone: ( ) K. Containers: Type Quantity Units Wz==_. •s.�metF nI UNwHAZARDOUS hLCIAL AND ASBESTOS WASTE MANIFEST B.Addroes:_ _JSCs® Nis-01a�n �C'. C. Phone: (w �Q D. Truck No.r7ype: LAis E. Vehicle License No,/State: M 1 v♦ LiL%C� F. Driver Name: (Pfesa• PrinQ AcknowtedgenaontofRocolplP.15900916:IHEREBYACKN©WLEDGE RECEIPTOF THE ABOVE•DESCtRIPTION MATERIALS FOR TRANSPORT PROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Data 1 / (Ddvsr Slgnalw•) A. Transporter Nei B. Address:_ C. Phone: E. Vehk;le License F. Driver Name: Tnrck No,IType: � - - - � TYPE UNITS (Piaaw Pdnq B- Drum P- Pcunds Acknowledpenlen! of Ra dpt NlateHala: I HEREBYACKNOWLEDGE THAT THE cZ O B� Beg TN- Tons ABOVE• DESCRIPTION ERIALS WERE RECEIVED FROM THE GENERATOR SITE X( Box CY- Cubic Yards AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED 1 N O- Other O- Other BELOW, G. Shipment Date= / 1 L. Special Handling Instructions: (DrivarStpnaNn) M. Generator's Ceriification; I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEpERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REpUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 { Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Murray County Landfill 6565 Htghwey 411 South Chatsworth, GA 30705-2099 ® Gordon County Landfill 1224 Pleasant HIII Road Ext, NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Troll Elizabeihiown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials, Date I /, l Authorized Signature 0 LL O O U J 0 O 0 Of O Z T Q w (C7 = O O w O O J W x = ¢ w ¢ d w > 0 O z OU = ~ _ O Z W U � z z H E a O w m � F- N E z n w �o Lu W I-U Ln F N U Y 1O Z co w _U o [If!~ N W O W W N K Q p y O Ln W tY Z CD N U Q N U O o ¢ p = O d WUWLn O�OLUNN Z W=U 6 Z UO D CD O� a: � ' i N '( n 0 0 0 rn � LiDn m N n N N (n lY ¢ � w (7 z p ~I Z Z H H N Z '-L 'ml O FE L V ►.. / wasfeServiees 65025th Suset,NW, Suae 100 Cleveland, TN 37311 (8130) 467-9180 (423) 47&01i10 Fax (423) 479-1952 Be Address: W 5q 5 Jor�a &f% C rte. k �� ®,)nt,npsv;ll� NC tQ9TIB" D. Profile— F. G. Phone: IF owner of the genorating facility dlfT®rs from tho generator, pleaso provido: DescriptionJ. NtJN-HA4AKVVU5 SPECIAL AND ASBESTOS 'WASTE MANIM15 I r-� G. Phone: ( } a 5(9 D. Twrk No.Mpe:. L'_ E. Vehicle License No./Steto:..- PA NA! _ -41 12 0 PG.. F Driver Name:- (FI�3se Print) AcEcHMOlo[fpOPrrantoRECEIPTOF 7F, a ABOVEwDESCRIPTION MATERIALS FOR TRANSPORT FROM a 14H ORNRRAi®ft ITf LISTED IN THE GENERATORS PORTION OF THIS MANIFES'6 G. Shiprnsnt Date 1 / (Ddwr SIOn•turo) A. Transporter Met B. Address: C, Phone: E. Vehk le License F. Driver Name: K. Containers: Type TYPE UNITS Acknowledgement of �' D- Drum P- Pounds Quantity Q0 B. Bag TN- Tons ABOVE* DESCRIPTION A X- Box CY- Cubic Yards AND WERE TRANSPOR Units 1 N O- Other O• Other BELOW. / L. Spsael Handling lnstntctions: M. Generator's CErtification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (please Print) Signatureon Truck NoaFype• _ , ` (Ple®ee Print) alpt Materials: I HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. � Shlpmont Salo= / / (Dr)�er Sipnatun) Disposal Site: (Check One) Bradley County Landflll 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5337 { Polk County Landfill T� 3477 FM 942 West Leggett, TX 77350 ® Murray County Landflll 65fi5 Highway 411 South Chatsworth, GA 30705 2899 ® Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date Authorised Signature \ / 2 \ / \ / \ I \ W) _ > \�� CD C k\m / m%% �oz \/ / /// p��§ \»& m MM % % In E k) m v z ® ® UP) i m 2 \ w q 2 m w z z \ ImA IRA �k a 0 = 2 z 0 } = k 0 ) \ m m 9 � ~ \ m [NJ \ / m g / \ m rn NJCD § 2 Lri \ / \ / 2 \ 0 / / < j m \ / $ \ o \ o ƒ o a 0 / / ƒ § 0 m 0 0 / 0 , m L' FE L V A waste'Services 550251h S1reeI,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 47&9160 Fax (423) 479A 952 PH am e .. r D. Profiin Number: E. Generating LoGnilon; SeMQ F G. Phone: If owner of the generatin8 facility dlRera from the rJenerato� please provide: H, Owner's Natrie: I. Owner's Phone: ( )' J. Descriptlon or Waste: Sod ,eci (A) Q&+11 .) O,+e f Re4v.A% ion Pond Cyl ode ri_Ii TWA er�>Qaaa, NO1V-MAZARoou3 SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter --- C. Phone: (&V) (. ` D. iruc!(No.Iiype: _ LA$ E. Vehicte License F. Driver Nam - r _ {Please Prinl) AcknowledgementofRoc loll nEc)rlals:IHEREBYACKNOI?JLEDGE RECEIPTOF THE ABOV&DESCRIPTIONJ MATERALS FOR TRANSPORT F11078 THE GENERATOR SITE LIS b IN THE GEJ v TOR PO ON F THIS PAAHIPUST, fpment Date r2�dpo (DrlverSipnaturo) A.Trensporter C. Phone: E. Vehk:le License F. Driver Name; Type TYPE UNITS ACknowfedgement of D- Drum P- Pounds Ouantity 010 B- Beg TN- Tons ABOVE* DESCRIPTION h X� Box Units I N O- Other. Oa Yards WERE TRANSPOR Other.- 8EL W L. Special Handling !its{nJCUons: M. Generator's Certification; I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT 8UBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, GenaratarAuthodzedAgant (please Pdnt) Signature Truck No,lTypa: (Pieaee Pr1n1) efpt MateHafa: I HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. ' Shipment Date= / (Driver Sipnatun) Disposal Site: (Check One) ® Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, T% 77350 ® Murray County Landfill 8585 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant HIII Road Ext, NE Ranger, GA 30734 Hardin County Landfill 1820 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above descr[bed materials, AJU)k� �CIw U t�ceipt Date Authorized Signature O i_s n mi O D mcn U) N W � W N � W 0 0 0 6 Q U D m O D r 6 G O O c c n n. (D 0 nr3�' z o p O N H zyz nxm Z v, Z 3 Z D r U) m A n m Ln z n N fD, Z A Mimi rm `K lD N. m mIML N m Z c 2 Z m �ml Z A)� m ML Z r � X 2 A a 0 P Z o o � Gl W m r m = o D No z n A � o � x w m o O T N m r o o n mco rn m Z r � -i m O m c. com m w z 1 O 3 r O m w m .A I` m O c z o z c Ozi < A D = S O z C) D m m r� c5 Z m x O 2 O O m D z O O � O n T O Lw� A WasteSerUices 650251h Street,NW, Sulte 100 Cleveland, TN 37311 (8D0) 467=9160 (423) 47&9160 Fax (423) 479=1952 G ®. Addreos: L Sd=Z1 JOaLki .c.r C. t- e F hlt)WHAZ#RDC)US SPACIAL AND ASBEST WASTE MANIFEST A. Transporter Z12�L l a G. Phone: (&V) (0 `0{9 e 5J�A D. Truc% No.rrype:. g __ E. Vehicle License No./Stets:.. F. Driver Name; (Pfau®Fong Acknow fotalia mant01130c01P2Mate1rlafa:IHEREDYAUK140tNLU9GERECEIPTOF YHE ABOVE•DESCRIPTFON MATERIALS FOR TRANSPORT G1710f.1 THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFHST. G. Phone: ( ) G• Shipment {bdwr Sipnawn) If owner of the generating facility differs from the generator, please provide: H, Owner's Nam TRANSPORTER • I. Owner's Phone: ( ) J. Description of Waste: J A. Transporter Name: 8, Addressi Re+r1-loon Poe d mo,+,o ri aI C. Phone: ( ) Truck No;rType: E. Vehicle License No./State: F. Driver Name: K. Containers: (Plan" Print) Type 6 TYPE UNITS Acknowledgement of Re alpt Materials: 1 HEREBY ACKNOWLEDGE THAT THE b- Drum P- Pounds ABOVE- DESCRIPTION ERULLS WERE RECEIVED FROM THE GENERATOR SITE Quantity �� B- Beg TN- Tons X- Box CY Cubic Yards AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED Unite I N O- Other O- Other BELOW, G. Shipment Date= L. Special Handling 111structions: (DriwrSpnatun) M. Generator's Certification; I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 4o CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT 8UBJEGT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 ® Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill s 3477 FM 942 West Leggett, TX 77350 Murray County Landoll 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizaheihtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 723D1 I hereby acknowledge receipt of the above described materials. �(XTU 1alni r*) �v lAeceipt Date I - Authorized Signature Lrl 0 t9 Z w', r > ��� (D _I W z D 2 { z D z N PEAIT1 n = m N z -- m A 0A< { z `� m o rn m 0 m C O z 3 rrrm M N m rn r m Lo w z p x m o0 0 m m M 6 ow Q p z S w -m{ z rn W z m rl ~ z n rm 6 < on O 0 O z � ^ O C � a � S D m m j N z o Or D O Cl) O O) W --1 r m z CD N Z O O co) r � w m 0 m N r m O -A O m Co 7N Z r -mi m W O m w m r.� m z o m r v OC 3 Z 3 Z O n c O < D �7 D m m O z n T.m A m m < O pA 0O n-Ii D z O O 0 0 y O r p O 0 L VAW.A WasteServices 650251h Streel,NW, Suite 100 CIevalmnd. TN 37311 (800) 4674160 (423) 4784160 Fru( (423) 479-1p62 D * Profile Number: F. G. Phone: IP owner of the peneratinp facilit)r differs from the generator, please provide: H, Owner's NaMe: I. Owner's Phone: is Wilms 4 e I e 00 Q 1Li N DWHAZARDOUS SPECIAL AND ASBESTUS WASTE MANIFEST • hone: (0 Lia - I: _ G E. Vehkle LlCenae F. Driver Nam . (Pious Print) AoknowledgementofRoca ptMilterlale:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT rROM THE GENERATOR SITE LIVYD IN THE GENE TOR PORTT F THIS MANIFEST. i mint Datq.2.Aa2/441P. DAver Slpn•W») A.Trensparter C. Phone: E. Vehicle License F. Driver Name; K. Containers: Type 6 TYPE UNITS ACknowledgentent of D- Drum P- Pounds Ouentity 01O B- Beg TN- Tons ABOVE* DESCRIPTION I X- Box CY Cubic Yards AND WERE TRANSP7 Units 1 N O- Other. O- Other BELOW, L. Speael Hanrill np lnstruCtions: M. Generator's CENficatlon: 1 HEREBY CERTIFY THAT 7HE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLA831FIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 11 Truck No,liypa; (Ple�u Print) alpt Meteriale: I HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G. � Shtprnent Date= / / (Driver Siynatun) Disposal Site: (Check One) Bradley Couniy Landfill ❑ Murray Couniy Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill L3 Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evensville, TN 37332 Ranger, GA 30734 Loudon County Landfill ❑ Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774.5837 Elizabethiown, KY 42701 Palk County Landfill Lj Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials, Aumonzec atgnaiure T z c� D O m w °a rn o o O O Q 6 Q 5 � O O c n n CD � 3 � O z z y z �=m N z rn rn Oz 3 m z D m rn G n U) z n (D 2 TT r C c0i1 a Z rm- N m Z o = m ® Z Z m O V -I Z W z 3 ~ z a r O on Z O m 2 n a X O Fri Z O O Cn G) w -Di � 2 p rn m D N z n O � n .Z7 w m m �o O T O -I -I 70 O n m 00 m z m rn m o .A m z 3 m w O c C z 3 z z O _ - O A m 4 m D D = x r O z n D m D z m x m oA o co O n O m D z O D r � O O O T 0 ®C� SANTE K WasteerWes 65025th Streal,NW, Suite 100 Ciitvaland, TN 37311 (800) 4874180 (423) 47&9160 Fax (423) 479=1952 �i�eMr. r N©N-HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: E. Vehicle License NoJStfl4o: _ G� C F. Driver Name: (Please Print) - AePsnp'ariedpamentofRocolptMoterlials:IHEREBYACKNOM&EDGE RECEIPT OF THE ABOVE• DESCRIPTION MATERIALS FOR TRANSPORT FROP41 THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MArj1FC8T. G. Ph�• Shipment Date / / one: ( ) - " (Driver signature) If owner of the generating facility differs from the generator, please provide: H, Owner's Name; r r.r r I. Owner's Phone: ( ) J. Description of Waste; A. Transporter Name: C. Phone: ( ) Truck No;liype: E. Vehicle License No./State: F. Driver Name; K. Containers: (ple■ae Print) Type TYPE UNITS Acknowledgement of Re elpt Materials: I HEREBY ACKNOWLEDGE THAT THE [0*6- - Drum P- Pounds ABOVE- DESCRIPTION ERIALS WERE RECEIVED FROM THE GENERATOR SITE Ouentity �� Beg TN- Tons Box CY Cubic Yards AND WERE TRANSPOR ED WITHOUT INCIDENT TO THE DESTINATION LISTED Units l N Other O- Other BELOW. G. Shipment Date= L. Special Handling Instructions: (IMMSignature) M. Generator's Ceriiticatlon; I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR AFIY APPLICABLE 87ATE LAW AND ARE NOT 8UBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261, Generator Authorized Agent (Please Print) Signature Disposal Slte: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 © Murray Couniy Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Lend1111 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Troll Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby ackn led a receipt f the above described materials, Receipt Date Authorized Signature \ \ \ > \\z� CD /\ƒ rn \ \=m $�X \ mc§ p eG0 < \ E k m > v qz 5 M z m o § z 2 \ PA ImA « k \ ro 0 on 0 ) k 0 zco m / 0 9 m k \ � C) / /co e m e ° m / / ! / m 3 @ i 2 $ / ( § E 3 G 0 \ 2 $ $ _ 0 2 > m _ \ / a \ � \ j ? > $ S 2 d 0 = / / / o / 0 � �_ 9�B���eService� 650251h Siraet,NW, Sufte 100 Cleveland, TN 37311 (800) 467-9160 (423) 476.9160 Fax (423) 479.1952 r B.Address: �159�' �„a.a�la� C�{e� ��. "1 : ' ' �• — - � -. - 'I� _ - � F. G. Phone: ( ) " If owner of the generat(ng facility dieters from the generator, please provide: H. Owner's Name:_ __ I. Owner's Phone: ( ) r - rr_ K. Containers: ® TyPE UNITS Type ©- ®rum P- Pounds Quantity F�I� ®- ®eg TN- Tons X- Box CY Cubic Yards Units � 6� 0- Other 0- Other L, Special Llandling Instructions: M. Generator's Certifica0on: 1 HEREBY CERTIFY THAT THE ABDVE DESCRIBED PAATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 2Ff9 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAV@ BEEN FU6LY, A66URAT€LY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER COND)TION FDR TRANSPORTATION ACCORDING YO APPLICABLE REGULATIONS; AND, IF THE d6'ASYE IS A TREAYMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAN® DISPOSAL RESTRICTIONS, I CERTIt1f AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART saa ANO IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 289. Generator Authorised Agen4 (Please Print) ►. i' ������ ;�Q� �� ��� �p����� Q��D ��C��ii0 V�Q��� G�r�Q�`�(lG���`I� Truck No.ffype: �� - - - - � A � , � C - ' `'� � ��� !� = A. Transporter Name; _ _ _ _ _ _ 6. Address: C. Phone: ( ) .Truck No.1Ty�e: E. Vehicle License No./state: F. Driver Name: __ (Pleew Prinl) Actsli©�vlQdpetmant oy Ed13:,oIPt t�4o@erlals: 1 HEREBY ACKNOWLEBGE TRAY TLlE ABDVE- ®ESCRIPTION G7t,,�ERIALS WERE FIECEIVED FROM THE GENERATOR SITE AND WERE TRANSt�OF���E© WITHOUT INI;I©ANT YO TH€ ®ESYINATION LISTEd ®FLOW. // G. � ° Shipment Date (odvar Sianeturo) Disposal Site: (Check One) 9radley County Landflll 282 Landfill Road McDonald, TN 37353 ® Rhea County Landfill 207 Sanitary Drive @vensville, TN 37332 ® Loudon County Landfill 2f712 Highway 72 North Loudon, TN 37774.5837 � Polk County Landflll 3477 FM 942 West Leggett, TX 77350 �,] Haywood County Landfill State Road 1338 Waynesville, NC 28788 ® Murray County Landfill 8565 Highway 411 South Chatsworth, GA 30705-2899 ® Gordon County Landfill 1224 Pleasant Hill Road Ext, NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 Kuhn Road Wes4 West Memphis, AR 72301 I hereby acicnowleiige receipt of the above described materials. Date ' � ' r N p -P D � Z N < C z z 0 D r z G) O D mU) N N U'I 0 0 0 6 6 6 n r 3 r i�o� >1 z�z n 2 m z V < A rnrnz 3 m D r m m n m U) z n Wi m, Z rm � T �l x rG�yy N Z m m N m 5 O A Z p 2 m G z z m O W -I z w z m a r O T z O 2 n D 0 Z 2 \ D O fn w m r = o m D N z n U) o 0 \ D A w m m o m mNJ o No CD �_ m 0 Z r v m C) ri -A O -m-I m 00 w m z 3 N � m N m O c 3 c z_ 3 z O n c m p Z n D _m m m < O n O n0 m y z O O (7 T O F 41 N U E K WasteServices 65026th Street,NW, Suite 100 Cleveland, TN 37311 (800) 4674180 (423) 4764160 Fax (423) 479-1962 f< — n M D. Profile Number. E. Generating LocaOon: �®c�� F. Address: It owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: 1604V �pR�=3UOQL P h'10 ASBESTOS UVIA� d (� f MANIMby L C. Phone: (ga't8) a SSG DEnam . Truck No.f1ype: yJ E. Vehicle License No.18tate: fiAVJ q14 MC f'. Driver Acl'craowfedgement®PV3o1;e1pEF�7r3toriafls:IHEREBYACIIN®WLEDGE RECEIPT®P THE ABOVE•OESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOr SITE LISTE HE GENERATOR PORTION OF THIS MANIFEST, v2 PA, G Shipment Date,_/` 0/ �Gt7 (Diver Sign ure) A, Transporter f C. Phone: ( ) . Yrucic No./Ty¢e: E. Vehicle license No./State: C Containers: F. Driver Name: Type 7DDrum PE UNITS ,y (Pleass Print) P- Pounds Acknowledgement oP G�e�ratpt NI®teriafs: I HEREBY ACKNOWLEDGE THAT THE Quantity TN- Tons ABOVE• DESCRIPTION CTERIALS WERE RECEIVED FROM THE GEN€RAZOR SITE Units �¢ CY Cubic Yards AND WERE TRANSPO ED WIT"= INCIDENT TO THE DESTINATION LISTED 0- Other. BELOW, 1,. Special Handling Instructions: M. Generator's Certification: 1 WERE®Y CERTIFY THAT THE A®OV@ DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 289 OR ANY APPLICABLE STATE LAW AND ARE NOT l�UBdECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUEMNCT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND iS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 289, Generator Authorised Agent (Please Print) G• � Shipment Date / / (Driver Signature) r�rsposar arse: (cnecic ®ne) Bradley County Landflli ® Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705.2899 ® Rhea County Landfill 207 Sanitary Drive Evensvilie, TN 37332 ® Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 © Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 ® Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 t hereby acknowledge receipt of the above described materials. n m !-3 n C�7 z o D O ? m O 00 0 0 0 � F EF Q' O < C O . ( n 3 � z z � D Z D Z n=m ti �mO 0 3 Z D r m rn r) n rn n 2 0 co = W m H D v m m CD Z O p n T W m m CD N O H � Z CO n m O a °v m C m m � z C Z Z n O O D O 2 _0 O D z C� G O O p O O � m D Fri O O p TE K L`Am / WasteServices 65025Ih Stnrt,NW, Suite 100 CNveland, TN 37311 (8D0) 4674160 (423) 476%9160 Fox (423) 479A952 D. Profile Number: E. Generating Location; E? F C 00o /(p NOWHAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A, Transporter B, Address:_ IS "a flC. F. Driver Name: (Pi■we Print) AcknowledgamentofRocolpiVADa arlah:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE40ESCRIPTION MATERIALS FOR TRANSPORT FROM THE; OGRisRATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFESTO Shipment Data ! / If owner of the generating fadlity differs from the generator, please provide: H. Owner's Name: TRANSPn I. Owner's Phone: J. Description of Waste: A. Transporter Name: SoI;r 'iec� ( A)a&+e� w a+e.ir B.Aaarasw Re+e NwVkoo Pond ale r; al C. Phone: ( ) Truck NoX1ype: E. Vehicle License No./State: F. Driver Name; K. Containers: _- (PI■■er Pdnq Type TYPE UNITS i Acknowledgement of Re elpt Materials: 1 HEREBY ACKNOWLEDGE THAT THE D- Drum P- Pounds I ABOVE• DESCRIPTION ERIALS WERE RECEIVED FROM THE GENERATOR SITE Quantity �O xw, Box B- Beg TN- Tons AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED Units T N 0. Other Om Other Yards i BELOW. G. Shipment Date= L. Special Handling Instrucftis: Oyersipnstur■) M. Generator's Cetlification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACItAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATIONACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature ME Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensvllle, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill r 3477 FM 942 West Leggett, Tx 77350 Murray County Landfill 65fi5 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Exf, NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Troll Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. UV Receipt Date I �-� Authorized Signature ¢ co < O = O C7 W LU ¢LLJ _U 2 = J 1- w 1 d z W uj o w ^ I-- Y 00 _U O O LU 0 Z W f W CD F O - (n Q G d 6° h 6' lS d h v4 © v mi M � b � Y aLna w U Y �`� a W � H (1) Z �CO cri O 0 C) 0 O 0 z O O O W i F- z ¢ w O a Z 0 D O O O � z z E - a 00 rs U) W z W LU O LU \ W o w m � ti C7 o w N Q O = = U Z W U Ctf Li to J Z W 0 ti �o zof co Q N W = z<z ¢ U-)za0 N o k z Ln N � U C O > O � ^ N ti Qj E I¢ O H J W ¢ 0 0 r- Q z = N r � z Co U) WasteServoces 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 4764160 , Fax (423) 479-1952 C C. Phone: W.0j D. Profile Number: Iq/ at 9 �1 E. Generating Location: F. If owner of the generating facility differs from the generator, please provide: H, Owner's Name: I. Owner's Phone: ( ) J. Description of VUaste:� ilk i�b�GVA ZARDC)US �pL 'A,° L1� ���9 �-) A SESTOS E. Vehicle F. Driver A. TranspoRer C. Phone: ( ) Truck No./Type: E. Vehicle License No./State: F. Driver Name: _ IC. C©ntainers: ® (Please Print) Type TYPE UNITS Aclin©wledgement oP R elpt 1�9oterlale: I HEREBY ACKNOWLEDGE THAT THE B- Drum P- Pounds ABOVE- DESCRIPTION M ERIALS WERE RECEIVED FROM THE GENERAYOR SITE Quantity �� ®- Bag TN- Tons AND WERE TRANSPO ED WITHAUT INCIDENT TO THE DESTINATION LISTED X" Box CY Cubic Yards Units /� O- Other O- Other BEt.OW. L, Special Handling Instructions: M. Generator's CeRification: I HEREBY CI:RTII'Y TF�AT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 269 AR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT T@ FED€RA6 REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SU13JECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE NAS DEEM TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 200 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CPR PART 261. Generator Authorized Agent (Please Print) Signature G• ' Shipment Date (Driver Sianeturo) Disposal Site: (Check One) Bradley County Landfill © 282 Landfill Road McDonald, TN 37353 ® Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 � Loudon County landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 ® Gordon County Landfill 1224 Pleasant Hill Road Ext: NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date LL O 0 0 O 0 0 J o _ w U i` Q Q 0 w = O w w < Nw ¢ v z O LU > z O 0 Z_ Z v O �IT H Z_ p_ w UJ �_ W w N ~ ~ Z y n W U O Q' ~ ON LU 0 W O or w M F Q ) . O � Z ON C w w O 0 Q 0 Z N J 0 U 2 O Z O u J Z LLJ W Z M U O ~ M ce w ce Z Z z W = O Z w � � � � W in Q w M J OD VI t0 0 U Z a N `N zaz U_ C7 `W z a O NLZ Ln to FAA3 0 0 0 N N O 0p l0 N lfl Lij ~ z 0 �I z SANYL IV - WasteServices 65025th street,NW, Suite 100 Cleveland, TN 37311 (800) 4674160 (423) 4764160 Fax (423) 479.1952 L D. Profile Location:E. Generating F. IP owner of the gen®rating facility differs from 4he generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of VUaste:`- Elm A. Transporter CP Truck NU.ilypd: E. vehicle License No./State: MW ��7� fP NC A. Transporter B. Address: 1 C. Phone: ( ) .Truck No./Ty�e: E. Vehicle License No./State: F. Driver Name: It. Containers* (PlsassPAnt) Type ® TYPE UNITS Acknowied®ement oP VCn tpt Materials: i HEREBY ACKNOWLEDGE THAT THE ©- Drum P- Pounds Quantity _� f� - 9- Beg TN- Tons ABOVE- DESCRIPTION P61IALS WERE RECEIVED FROM THE GENERATOR SITE )(- Box CY Cubic Yards AND WERE TRANSf 07iED WITHOUT INCIDENT TO THE DESTINATION LISTED Units 4'f� O- Other. On Other BELOW. Date. L, Special Nandlin0 Instructions: M. Generator's CertiOcation: I HEREBY CERTIFY TRAY THE ABOV@ DESCRI®ED AAAYERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 201 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) G• ` Shipment I I (nAver St®nature) Disposal Site: (Check One) Bradley County Landfill ® 282 Landfill Road McDonald, TN 37353 ® Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 ® Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705IN ® Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 {Cohn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date [`v p ._ Jhmrivorl Sinnahvn O N D z cn � D O Z z ? m chit SNP w O N N O o 0 G rn m z � 3 6 0 O p c n C CD n x N irn Cn ' n O r O z ? zDz nxm N z rnrnz 3 m D r m rn p r) m z n O n w r m 2 O m _ D N Z n O m o n --I ;;a w m m O N C m O - ~O —I . . .. ;;a (7 m z c V z 0 Ni —i N T T N V m m z � m A m w O 3 1 C z Z 3 Z O I:� (� C z 0 O z m o m z = D n m r GO) m A ;a 0 co D O z M O 0 ;a O o n o n o O T O ® - TZt WasteServices 65025th Street,NW, Suite 10D Cleveland, TN 37311 (600)Falk(9160 423) 4794952 , C. Phone: a t), Profile Number: 1 E. Generating Location: �®�(?� F. Addre If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) .1. Descriotion of Waste: - - K. Containers: Type -- Cuantity Units jV TYPE UNITS @- ®rum P- Pounds ®• tjut9 TN• Tons )(• l3ox CY Cubic Yards @• Othee O• Other L. Special Handling Instructions: GUU MC=FAQeUaU ) o UU k H 9 C. Phone: (gal) �y�- SssG D. Truck No./Type, E. Vehicle License No../State: F. Driver Name; < w "r (Please Prtnt) fit[snowledgementofReceipt Materialts,IHEREBY ACKNOWLEDGE RECEIPT OF ARoVEwHESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SIYE LISTED I THE GENERATORPORTION OF THIS MANIFEST. ) �,rShipment Date 1 / 3e ! zy (Driver naturo) A. Transporter C. Phone; ( ) �. Truck No.ffype: E. Vehicle License F. Driver �eee Pdnq ®Ipt IlilBteP!>;t18: /HEREBY ACKNOWLEDGE THAT THE DIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED G, � Shipmen4 Date ! / (ndvar Signature) �. --_ —=— Disposal Site: (Check One) Bradley County Landflll -- 202 Landfill Road McDonald, TN 37353 M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 269 OR ANY APPLICA®LE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE ©F A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZAR13OUS WASTE AS DEFINED BY 40 CFR PART 269. Generator Authorised Agent (Please Print) ® Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 ® Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® Pollc County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1339 Waynesville, NC 20786 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 ® Gordon County Landfill 1224 Pleasant HIII Road Ext, NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acl(nowledge receipt of the above described materials. Un Receipt Date \ \ \ \ \ \ / 3 \ \ � \ %CD o / 2 co g z CD _ w m Yj\ rn n m NJ® y 0 x \ / moo/m m ° / / CD m \ m \ Cm c z j > \ \ < \ / / \ % < ® / § § 7 § / ƒ j S m \ / 3 \ 0 o R 0 SA!'�1T�EK WasteSe�vi�as sso 251h Street,NW, Su1te 100 Cleveland, TN 37311 ((f00) 407.9180 (423) 476.9180 Fax (423) 479-1952 G C. Phone: (�oco � JP0,(E1. e °1 ✓`"� �2 D. Profile Number: �� � � � �D E. Generating Location: SOienP_ F. G. i�hone; ( 1 ° ,� a���,� ��� ������� �G��9® z} ��� �1'C� 5 1������ �� �' �`������ If owner of 4he generatin8 facility dl�rers from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( )`_ J. Description of Waste: _____ . / E. Vehicle License A. Transporter 9. Address: Truck No./Type: �� C. Phone: ( ) . 5'ruc{< No./7y(Se: E. Vehicle License No./Slate: I<. Containers: F. Driver Name: Type � HYPE � UNITS golsn®wiled®errtent oY Re elpt hA®terl»Is� I HEREBYACItNOWLEDGE THAT THE 6- ©rum P- Pounds q®®VE• ®ESCRIPTION rn ERIALS WERE RECEIVED FROIW THE GENERAYOR SITE Quantify �.�� ®• ®ag TN• Tans AND WERE TRANSPO ED WITHOUT INCIDENT TO THE DESTINATION LISTED Units �� 0• Other OY Othe c Yards BELOW L. Special I-fandling Insiruetions: M. Generator's Certification: I HEREBY CERTIFY TRAY THE A®OVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 289 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FED€RAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACtyURAT6'6Y AND PROPERLY DESCRI®ED, CLASSIFIED ANf3 PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDINP.v YO APPLICABLE REGULATIONS; AND, IF THE Ilb'ASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICT€D HAZARDOUS WA�aYE SU®,IECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANY THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITW YHE RE®UIREMENTS OF 40 CFR PART atia AND IS Nd L®LAGER A HAZARDOUS WASTE AS DEFINED BY 48 CFR PART 261. Generator Authorized Agen4 (Please Print) G• ° Shipment Date / (Driver Sipneture) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® Poll( County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 ® Gordon County Landfill 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 I(uhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date ® ® L�LL.J �/� � �/-�, T ����y'-'�-7 \� Receipt Date '�J n„�a...t�e.� c,n..���,.e T N o D o � z c) D O � co —I z m cn w co 00 m m 0 m 0 rn m Ln o 0 0 FT Er Q m z > j < 0 0 c a m o x Z77 CO nma+cn m c o.Y m mLvj N m Z o = m p z z m O W z w z m r z a r O an z O aq 2 n a a O M z ~ m m \� N Z O O N � w m m o 1 T o � m -{ n m 00 m z m (� m o -i i 00 m 00 m a z 3 C o � m co 0)O 3 c z 3 z Z O > -ml C7 0 � A D m m 0 y mO D m z X m m c> x O m � w � o G> n O m D z O O r � O O O T 0 6 1j � \J L-tl� Imo- t1\� ����ese��oces 65025th Strest,NW, Sulle 10D Cleveland, TN 37311 (800) Fib (423) 479-1952.9160 r, C Phone: D. Profile Number: �D � � � J� E. Genorating Location: �®6utP_ _�— F. G. Phone: ( ) IP owner of the generating facility di�r®rs from the generator, please provide: H. Owner's Name: _ - I. Owner's Phone: ( ) — - J. Descriptien oP Waste: ---- -- _ — � ��� � �) � �o����� � ����o�f� ����� �, � la��D � � ��� o Truck No./Type:, y0 E. Vehicle License No.!$tate: ��� �� N C F. Driver Nam . - (Placae Pnnl) L�olteee��la€3gemen4ofR eipiP.`.uBarlali3:IFIEREBYACKNOWLE®GR F�RCEIPiD� THE ABDVE-DESCRIPTION tiAATERIALS FOF3 YRANSPORT FROM THE GENEfiAiflti SITE W ED IN THE OE It;F3ATOR PO N OF THIS MANIFEST. i �� , - G hipment Dates /_ �� . ( duet Signs ure r�, iranspoRer 5a ►i ��,�` � � p _ �� �a.� t a �l�i,�' %��'�s�i1d+ ®.Address: ®Gt Gj� � a1�0 d�Jl _ -- - - id. Phone: ( ) . Truel< No.Ci'ype: E. Vehiole License No./state: _ - - --- F. Driver Name: {L. Conlalners: ® TYPE- UNITS (Plooea Print) Type �i� D- Drum P- Pounds Qolrtt®avledpet�leat oP � ®Ipt ��4oteel�ln: i HEREBY ACKNOWLE®GE THAT THE Quantity .� ®- Bag TN- Tons A®®VE- 6ESCRIPTION r9 ERIALS WERE EIECEIVE® PROM THE ®ENERATOR SITE ?t- Sox CY Cubic Yards AND WERE TRANSPO E® WIYN®t)T INCI®ENY Ya TFiE 6ESTINATION LISTED Units �r� O- Other 0• Other BEL®W G. Shipment ®nl® / / L. Special Handling Instructions: (orivaeSlaneture) M. Generator's Certification: I HEREBY CERTII'Y Yt1AT YHE ABOV@ DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 3Ei9 OR ANV APP616ABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTINCs PROPER D19POSAL OF HAZARDOUS WASTE HAVE BEEN FU66Y, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE FPo'ASTE IS A TREATMIENT RESIDUE OF A PREVIOUSLY RESTRICYED HABARDOI�S WASYE SUBJECT TO THE LAND DISPOSAL RESTRlCT10N3, t CERTIFY AND WARRANT THAT THE WASTE 01AS BEEN TREATED ON ACCORDANCE WITH YHE REQUIREPdENTS OF 48 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASYE AS REFINED BV 40 CFR PART 2€31. Generator Authorised Agent (Please Print) Disposal Site: (Check One) 6radley County Landfill 282 Landfill Rcad McDonald, TN 37353 Q Rhea County Landfill 207 Sanitary Drive Evensvilie, TN 37332 0 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 © Pollc County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1331i Waynesville, NC 20766 ® Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 ® Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Ituhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. ■■■� nuehorized Signature 1 Date 'G`- `�.:��. / / 2 j / § j\\� ƒ e ¥ < §z rn jfm CD z o >�z z \ �\in \ /7z m\z m m Ul M @@ o --5/\ IML M j zz�m y m m m f q§ /FT Fre / / m o ® z $ \ § ƒ § \ k ~ } y 0 0 k / e m o q m ± ) Cl) } k \ \ m F j � 2 / m \ NJ m \ / e j \ § m ) / m CD 0 cm) § 2 / j m j 2 / { \ m 5 \ \ ( o { § J / 3 E { \ 0 WasteServices sso25ih Street,NW, Suite 100 Cleveland, TN 37311 (800) Fax (423) 1160 479*1952.9160 L u C Phone: • dam. D. Profile Number' I� J� E. Generating Location: .550PAe F If owner of the generating facility differs from the generator, please provide: H, Owner's Name: — -- I. Owner's Phone: ( J. Description of Waste: — - — ki CS D68 i lD) \ ]�VA " 74ARLUOUv g Truck No./Type: y� _ �ofcrtowledgementofRecelptlL9at®riaits:INEREBYACKNOtfi1LEDGE RECEIP?©f YWE ABOVE•DESCRIPTI®N MATERIALS FOR TRANSPORT FROM THE GENERATOR SIYE LIST N THE GENERATOR PORTION OF THIS I MANIFEST. G, _Shipment Date /. / (Drivar analurs) A. Transporter ,1A Ildi fiti` Q Q.� LaiAddress: ----------- - iqg&Ad MA t,. C. Phone: ( ) .Truck No./Type: E. Vehicle License No./State: F. Driver Name: K. Containers: ® TYPE UNITS (Please Print) Type Acknowledgement oil Re aipt Motarlals: I HEREBY ACKNOWLEDGE THAT THE D- Drum P- Pounds ABOVE• DESCRIPTION roERIALS WERE RECEIVE6 FROM THE GENERATOR SITE Quantity oav B- Beg TN• Tons X- Box CY Cubic Yards AND WERE TRANSPO E® WfTHOUT INCIDENT TO THE DESTINATION LISTED Units �� 0- Other O• Other BELOW G. . Shipment Date L, Special Handling Instructions: (Driver 8ionalure) DE STV • Disposal Site: (Check One) ® Bradley County Landfill ® Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 307054899 M. Generator's Certification: 1 HEREBY CERTIFY 7t1AY THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECY TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE WAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PAIN 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CPR MART 261. GeneretarAuthorized Agent (Please Print) Signature Shipment Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 � Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 ® Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1336 Waynesville, NC 28786 Gordon County Landfill ® 1224 Pleasant HIII Road Ext. NE Ranger, GA 30734 ® Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 ® Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. .E Receipt Date Date FT] � O N W D o -t < z o mi O D co .co w m O� cn r N 7� W O O O S O p n n' 0 w®,➢ z � o r1i CD Z o 2 ?�D n rfl n=m (ri)b z NoH n (n a+ m A m c o z rn m 0 m N m E � Ho ® S m r X m W Z A d W 3 m m z n � ii 2 =I P I- � o a o w O W m r m m m N Z O O O � w m m m mra3l ro —I m co Z rn mmm r N o m O -o c C Z_ 3 Z O n c Z G m D m O z m m o O D 0O m D z � o Om O SANTE K IL A& VA WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 C B.Address: L{�/S �Ona 11 a Lerec %X /A iin F A I7S'IIC N 1c dq r C. Phone: 1u�_ D. Profile Number: N j E. Generating Location: 5011AL F. Address: G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) II J. Description of Waste: S01 t Cj i L_Ci Wcs4p t .j4cs) K. Containers Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 66994 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter C. Phone: ) (�yR -.SSS� D. Truck No./Type: ��t� E. Vehicle License No./State: MW IWILACPA JUc. / (Please Print) Acknow ledgementofReceiptMaterials:IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTIO THIS MANIFEST. ement Date__ (Driver Signature) ' A. Transporter Na C. Phone: ( ) 'D. Truck No.lType: E. Vehicle License No./State: F. Driver Name: (Please Print) Acknowledgement of,iteceipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION- MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1336 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m L_L_L.�J '; �J t,I�o-�`i4� }l Ar Receipt Date Authorized Signature CD un 0 0 O LnO w O tti Lq vi o LL U M re) v� O O N M J O r1 N 0 O O ur w O c� co 0 o �w = 0 Q W z o (7 J W Q' 0 p U0 o6J 2 W Q 0- > W iA- o Z 2 O W En Z z U 0 Z U 7 F-- E p_ O W N o 11 ro n _. z W m re) 0 U_ F � 1 l I OLU W M C p O C j Z ON W W Z re) p O a U Z_ N w U LU W (n z Z W z QW lD Z C) co w 2 U Z < Z z a 0 N 0 to Z o Ln z � O 111 Ln Ol co mry � ~ Z v U 0 �I z Z � p N U SANTE IC WasteServices 650251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-8160 Fax (423) 479-1952 r• B. Address:_ U�gs T tAw '��i►. [rye k %�c1. D. Profile Number: H � a I ! — % E. Generating Location: s6�'"C G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name I. Owner's Phone: ( ) C J. Description of Waste: S� � I d.i C. � � l Jas'}¢IJa-i'--f� K. Containers: Type �/ Quantity � f� units ?�tJ TYPE UNITS D- Drum P- Pounds B- Bag TN- Tons X- Box CY- Cubic Yards O- Other 0- Other L. Special Handling Instructions: M. Generator's Certification: i HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFYAND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature Shipment Date m m (�� �._: .6 6 9 9 y NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: (a���) (,W �' S5�' D. Truck No./Type: �`al8 E. Vehicle License No./State: /u �► �i 4 tp �? AI r F Driver s (Please Print) AcknOwledgementofRecelptMaterlalts:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF_,THIS MANIFEST. G ,L�'s"- —.-<<�l"�Fiipment Date / % _ (Diiv� Signaturo) � -'' A. Transporter Nai 8. Address: C. Phone: E. Vehicle License F. Driver Name: Truck No.lTylSe: ' i ' (Please Print) Acknowledgement of Rec,elpt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW, � G• %' Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill ' State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill � i 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 � Hardin County Landfill 1620 Audubon Traii Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. ,i � �i �/ l i, ti"%���,,,� � �. ��.. (.f` Receipt Date "���`� �� A)thorized Signature \ \ \ % § \ � ■ > / \ \CD k Z < //j \ e� rn _-----� % C�\ CD / / \ \ / \ \ / § § § § ° ° 2 m m 2 � § z k) m ƒ -se r� )S ° m o 20 w z ./ m INA \ / 0 / q q ± § )rQ§ .\ \ - j - x 2 = ) \ \ ^ j ` CD w m 9 ® @ m R \ / ~ --Am / / CO § { ® \ m ) � / \ \ ® 2 % / 2 / ƒ m s / \ ~ \ / ƒ \ 7 2 ICD / 3 c r/ n SANTE K WasteServices 650 25th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 G B. Address: ��9J �n n G '��6i n �'rG e �t �� l.✓ r I NC � ' S C. Phone: (�.�� �U � 11' � y D. Profile Number: W 1 �) E. Generating Location: ��MC F. G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: ( ) J. Description of Waste: `7n1 its t�i e � l�J A'S�i�t,.i n-� NJ K. Containers: Type � TYPE UNITS D- Drum P- Pounds Quantity <� G B- Bag TN- Tons X- Box CY- Cubic Yards Units �TN O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN - TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 286 ANO IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature Shipment Date m 66.998 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST a C. Phone: (°�i lays• �-�� D. Truck No./Type: y� E. Vehicle License No.JSt te) /V1 W ��W�� F. Driver Name:��'f � P� 1. r 7 � '^'- (Please Pnnl) AcknowledgementofRecelptMaterlata:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTE LIN TTHE GENE�R�ATyO/R PORTION OF THIS MANIFEST. G. -�1`r ��-" - � Shipment Date � i ' � / ` . / (Dri Sgnature) A. Transporter C. Phone: ( ) �' D. Truck No.lType: E. Vehicle License No./StatQ: F. Driver j (Please Print) Acknowledgement pf Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. �' G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill ' State Road 1336 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. '� � � Receipt Date , .� I �V Authorized Signature ' l O W O Q o O 0 O w O c7 U v~i Q 0 O O U` J W of W ¢ Z O 2LU a > ? O 0 Z z a O a L N z_ fu W �o 2 U) W LU n H 00 LU Y U H O W O LU 2' W Ln O W U Z_ NN Q C) Z M J O U F=- G' O Z w O J I-� W Z � M Z H M LU z Z � � W = 00 Y E" � W N W W Z O ; w Q w n J Uf tD Vf u ILJ Y U H W U K w J F- Z W z W W � W z Q N W 2 U Z Ca7Z z a O �=) C:)z O Ln Q �. a o NLIJ LNl1 N ¢ � W a 0 w a z � 'mq c=i SA�1TE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 G B. Address: Nirq S �p n n -i 1- o � C t'Q[ �� �� C. Phone: (�,�) " S�Fn •- � s� �� D. Profile Number: / / �a7 � 9 E. Generating Location: •�Me F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: ( ) ` J. Description of Waste: .5c�� � ci r � P � o.l C�S�r- i . ��,r -12L-�f,-,-rrU;, iur,d ma-� ;�I K. Containers: Type � TYPE UNITS �1 D- Drum P- Pounds Quantity a� B- Bag TN- Tons X- Box CY- Cubic Yards Units �� 0- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 2a8 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 2B1. Generator Authorized Agent (Please Print) Signature 66995 N0,�1-HAZARDOUS SPECIAL AND ASBESTOS E MANIFEST A. Transporter CQr.•�Gn__.r N�-�8�ll0 C. Phone: (�,� � y� - l�l r6 D. Truck No.lfype: �� E. Vehicle License No /State: M W �/N � E !t%(- F. Driver Name: �� �fl� � f.Ul A �'7` � (Please Print) AcknOwiedgementofRecelptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR S17E LISTED 1N THE GENERATORt PORTION OF THIS MANIFEST. r`.'�ij'-. , j' p -� i G.� 1 �.;-"�.� �. ' j _ Shipment Date ` l�l r. �. (DnferSipnature) ' A. Transporter Na �� C. Phone: ( ) f D. Truck No.lfype: E. Vehicle License No./Slate:_ F. Driver Name: �" ` (Pleaae Pdnq Acknowledgement of Recalpt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION,MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. f G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 262 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill � Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 I-1 Haywood County Landfill , ': State Road 1338 Waynesville, NC 28786 I hereby acknowledge receipt of the above described materials. Shipment Date m m �/ t' t n t( �� �� JLJ� .( !'` � 6� i7 !�� 1, ;'�C�' Receipt Date • � Authorized Signature k� p N ➢ N < o m m Z 0 � —➢1 O n m m � � a O 0 0 0 > N 0 0 0 o O 0 0 o O z D � O m cp ? N V W co o Ni i � 6 n O � 0 7 3 n L7 � 3 � o O A O�>1 z�z n=m z V � H �<A rn m Oz Z rn D r m m m rn z n o = G� w z j D N n o m O � r m o � z m N w 3 tD, Z (D , A T N m C o Z m � � m Z p S m Z v Z m O V -i Z wz ran F+ z D r 6 rl 8 o � N � m m z 0 O o n 0 Go m z � 2 D m m � _ O D o co o M m 0 0 SANTE K WasteServices 65025th Street, NW Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 B. Address: MI5 —1 5 ar. o.'t A r C, r e F� i< RC1%, D. Profile Number: 6997 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name: a C. Phone: ®•�6')-�N�''�O D. Truck No.lfype: yG E. Vehicle L E. Generating Location: SUM c F. Driver Na F. G. Phone: It owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: J. Description of Waste: SA' l d t t= 2 Ll I,J (151}c LJrx� Fl K. Containers: aEDrum E UNITS Type 1 P. Pounds Quantity orb TN- Tons CY- CubicYards Units �O- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m L_L_1�.J AcknowledgementofRecelptMaterlala:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIST N THE GENERATOR PORTION OF THIS MANIFEST. G. 4A Shipment Date / / (Drive ignalure) A. Transporter Name: B. Address: C. Phone: E. Vehicle License N F. Driver Acknowledgement of ABOVE- DESCRIPTION A AND WERE TRANSPOR BELOW. Truck No.lfype: (Pleeae Print) Bipt MetBflala: I HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE OUT INCIDENT TO THE DESTINATION LISTED (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext, NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. 1 I YV� ,f A (,,j,d4 Receipt Date Authorized Signature lid T z c� D O �Cl) �a m co Ln 0 0 0 6 6 Q �oo znz n=m rn rn Oz 3 m z D m m G m rn N z n m, z rm X C �m a z M N m z o = m o z z m O V � z W z 3 m µ z 7 'ZJ O D O CD �® w r z r m m N z �/\ O O \ ww m m m m \ No m ro m of m — C z r V T m c� Fj � � m11 w m 'o z 3 � r m N .06 m 0 .o 3ci c Z_ 3 z Z O _ -I D C) z Z m m o 2 m O z D m r c> m op O D cn O m > z O 0 o n O r O (7 m O 0 SANTEK V VA WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467.9160 (423) 4764160 Fax (423) 479-1952 G B. Address: J �OAf fjh aft � i£ G K L*�!f . D. Profile Number: E. Generating Location:.'��" F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) r 1 t J. Description of(VVaste: VD0 V L4 ; r: a 1W K. Containers: TYPE UNITS Type r1 LD�Drurn P- Pounds Quantity orb ag TN- Tons �.ox CY- Cubic Yards Units /N ther O- Other L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 66999 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: !S� G- PtsaA b Dr . C. Phone: (47) G y$ -fG D. Truck No./Type: E. Vehicle License No./State: AA%A) Q41 iD Q Ivc F. Driver Name:_ - /� (Please Print) AcknowledgementofReceipt Materials: IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION.OF THIS MANIFEST. J ' � -v! ✓ ! .• rnent Date (Driver Signature) A. Transporter E. Vehicle License No./State: F. Driver Acknowledgement of Rece ABOVE• DESCRIPTION MATEA AND WERE TRANSPORTED,1 BELOW. J (Driver Signature) (Please Print) let@riels: I HEREBY ACKNOWLEDGE THAT THE WERE RECEIVED FROM THE GENERATOR SITE )UT INCIDENT TO THE DESTINATION LISTED Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 ipment Date / / Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date?'' Authorized Signature r O O U O 0 J O Q a' O z T Q c7 = O ly Q� 0 Q p > C7 < w w U z O _ LU ~ Q LU > w 0 z O Q z 0o _ o zLU � Z U z E 0 O co w °J o � E z LU M o W LU M H CO U Y 00 UCD 00 W H — O oo� W Z) N O M W LU O O_' O p Z Cl N LU H O Z H ti O U 0 O fLLU U w LU w Z W O ;ID Go z N w = U Z < Z Z o. 0 N � 0 Z 000 � o � ti A CO M � O ¢ C7 Z U U SANTE !C WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 373tt (800) 467.9180 (423) 476-9160 Fax (423) 479-1952 G B. Address: �l5"�?ri jOnq'r hcn �, f"t � fr iC%`'. C. Phone: (I�.1 �} Sad 95G �/ D. Profile Number: N� of � 9 ' i E. Generating Location: SG,>w L F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: -� �jit: � 4 n �fA�(:�.r�� l�Cr� . r l-(Jib/_:d ./ "�ii`7 ;'rr F-f / K. Containers: Type Quantity Units L. Special Handling D- � B- X- O- Instructions: TYPE Drum Bag Box Other P- TN- CY- O- UNITS Pounds Tons Cubic Yards Other M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED ANp PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE 13 A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature �7o�n NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST r A. Transporter Name:. f I` )Ur,'n �"u, n %wn v, r'�,n.. •i-a �, C. Phone: (- "•') � ' : ' �� D. Truck No./Type: +-I � E. Vehicle License No./State:�� '-ICI �:� �. /1.IC F. Driver Name:. }�� f (Please Prinl) AcknowledgementofReeelptMaterlala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date / / (Driver Signature) A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./State: F. Driver (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Traii Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. ■■ ■ �■■� Authorized Signature Date Cr 0 W O W U O p O of Of O 0 O z 2 w o c� z O O LU O U J W Of LU z = z a W ¢ w L.Li > Of ¢ z z O o O Z W U z z E o w o ro _z w w N H Ln V E O W U W Y W U 0O fy Z N O re) w W O Q N p O Z C) N H ~O Q Z U No O p * U W U W LU N z W 0> zp co W = U Z (D � Z Za0 H N O Qz N V C O � O � H H LU af �D iD O �n in o co ui re) o� m in c� z U U W p �I z z � IN O N SANTE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 r• B. Address: LIS�7 S JOA< fou L ieC'c �d. .9%l .nFSvllle /iC n26 71f/`3� C. Phone: D. Profile Number: H% a I �1 E. Generating Location: '61A ik r G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: �Ss hj r Le Gt _ ( ,Aj&5ie (, L4fr _mac , ;� ,�;, ?6lei o/ /11 a7 rr, , / K. Containers Type TYPE UNITS D- Drum P- Pounds Quantity ' B- Bag TN- Tons X- Box CY- Cubic Yards Units TN 0- Other. 0- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m 011V NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST D. Truck No./Type: L! O E. Vehicle License No./State: /NA W L14(odool NC F. Driver / (Please Print) AcknOwledgementOtRecelptMateriais: IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LI ED IN THE GENERATOR PORTJON OF THIS MANIFEST. f ''ShipmentDate. /,:/ (Driver Signature) A. Transporter Name: 8. Address: C. Phone: ( ) D. Truck No.lfype: E. Vehicle License No./State: F. Driver Name: ' (Please Print) Acknowledgement oJJReceipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW, G. Shipment Date ! / (Dover Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 (] Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. t Receipt Date Autlorized Signature U. o o J 0 0 w g _ Q p 0 12 W LLJ w ly /\ w ¢ z O 41 LU > z O t O z � z H E p O w � H ti z m w in M LU W CO U Y W Z U O LU H LU O w p N Li O W W p a: H Q N p O Z N H•--� Fw- MO N O < N D O .mod O U 2 F- O z um O J U z 3 w W ro U z z Z H m � 5� ~ z V) c W y ® Z z O g w LLJ N W W z z > ow�O Q ll1 J > n (n i0 0 U z inr%j W `U UJ z<z N zao Z I- rq . 0 ° z r�A16U v � u c o � o � 9 c 0 0 0 >J Vl M LL L Y � z �I z z � � M N U SANTE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 I B.Address: �! � c%� TUnc.��,i^n C AFC/t i�['�• C. Phone: (�;15') SU C� - �� � !o `-� D. Profile Number: �I � ^�� � 1 E. Generating Location: �h1 c F. G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: � � L �'�Oi� u� ! 1'") C�1 * I , Gi I K. Containers Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units ' "` O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 26H AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature s�aa� NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name: / r )r7;i; r-t ry � n ���� '� � � ,• �. , 1 B. Address: i�:% (:, � rr �ticr +� ,()r . C. Phone: (s;�JLJ) ' °•lY - � 3 j (c D. Truck No./Type: �"�O`� E. Vehicle License No./slate: ��t ���_ `~I'J(� �' �bi� F. Driver ' ,,.' (Please Print) ACknOwledgementofRecelptMatertela:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR �ORTION OF:7F�18 MANIFEST. G. 5hiprrtenF Date / / (Dover Signature) A. Transporter Name: B. Address: C. Phone: ( ) D: Truck No./Type: E. Vehicle License No./State F. Driver Name: (Please Print) Acknowledgement of Receipt Materlala: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Palk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m Authorized Signature ceipt Date LL o o U J O O Q: O _Z Q o K O O � 2 O W z O � FQ z O O U � Z Z E 0 a O w "� � o z E fu w o I. O W Lys kp F- .-a U Y W Z U W F H O K W O LL LU W Q N O W K CD u z N Q HFW-- C) 2 U O Q N L_7 O = Z M ..I Q U F=- 99 O Z LL O 'i U a z H W 3 rq rl W $ Z M U ce y� W Z w W = O Z z Y�Ln �g W N ry 1W. W z Z O Fy z W �o W �� fA tNG !A U > 00 ci z 0 N W = LdAi CM)z < z aUO'z N z n. O .Z �=�z O Q a �Y N N ¢ W c� z 0 f- ~ z I � z N TMA O SANTE K V VA IL A& WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 4764160 Fax (423) 479-1952 L B.Address: ZII�1S Jona7I,F Lfee l't!a�n r 5v; // e . /uc �87e5 C. Phone: VJV-p9�j'` D. Profile Number: E. Generating Location: 50M e F. Address: G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name:_ _ I. Owner's Phone: ( ) J. Description of Waste: /Uii d /Yt Girt': i6, K. Containers: Type Quantity Units L. Special Handling Instructions: E EDrum P- TN- CY- O• UNITS Pounds Tons CubicYards Other M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature sty 6700t NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST Qt, SSG D. Truck No./Type: y� E. Vehict F. Driver AcknOwledgementofReceiptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED I THE GENERATOR PORTION OF THIS MANIFEST, G. Shipment Date r ` L / / (Dover Signature) A. Transporter Name: B. Address: ,r C. Phone: ( ) D. Truck NoJType: E. Vehicle License No./State:;/ F. Driver Name: (Please Print) Acknowledgement ofj(Receipt Materlals: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION4111ATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSF fbRTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G / Shipment Date / / (Driver signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill • State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date Authorized Signature o 0 U O J Q Of Z Q U) 0 O C7 O o � 0 > W 2 F LU W w _ = Z O LU a.> Q' O z z z 7 H E O ro w 00 Ln � o z E co w Ln g m �j � F O U Y COZ U C W ti H O [if N W O \ w LU W O O W Z � Q Fw- = FW- p i CD_7 N O Q \ N = O d Q U 2 I- Z LL O d b � Ud �i W Z M u K ua w > INNF n Z W Id1 = O Z Z ® 5 w W LO W {L z Z® InnW 0 W kp �ID(AL of ID (A U > in W W `v z<z Z U) N Q z �ELr)(] v a U C O � O C H 'O � � o 0 � N V- 1 Vl O J tD �p 1 N N F � � Z Q M O P-I O Q O z 5AN7E K WasteServices h50251h Street,NW, Suite 100 Cleveland, TN 37311 (B00) 467-9180 (423) 476-9160 Fax (423) 479-1952 /� B.Address: `I`795 Ju�oih;�� C�EEk �,cr %:i���rsv,l%c , _ N,� �87K5 J C. Phone: (. ';,� a 0�/' �SC 'i D. Profile Number: !'�� � � � ` � E. Generating Location: iun F. G. Phone: ( 1 � If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: i end n��;-J��r�,J K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons Units X- � 0- Box Other CY- 0- Cubic Yards Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 266 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature �■■ ■■ ■■u 6700� NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B.Address: I �w0 !"r 54a t, J�r C. Phone: (P,,��,) /e �l i� — � SSG D. Truck No./rype: yb' E. Vehice License No./State: MW �lyC�� n,1r;� ii' F Driver Name: ,%` +� .� (.t-�-✓.� it (Please Prini) AcknowledgementofRecelptMaterlala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN,THE GENERATO,�RtPORTION OF THIS MANIFEST. G, r' /-) /._G��,.�fi">'.� Shipment Date � z / O� / ?_ (� (Driver Sfpnaturo) A. Transporter Name: B. Address: /� / C. Phone: ( ) ;/�D. Truck No.lType: E. Vehicle License No./state: �• F. Driver Name: % f (Pleeee PrtnO Acknowledgement of Recelpt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION M 'TERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. / G• � Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Polk County Landfill � Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 I hereby acknowledge receipt of the above described materials. ' 9 r" i ' � � � ! '' Receipt Dat, (... Authorized Signature 0 U- o O U J J _Z Q fn Q O _ ; O W c� w w LU _ _ O LU Li a z O Z_ Z E ra O N w O o z E m w 2i Lo ui Y00U U O) W F" •--� �'" O W N O W \ W Fw \ co: 0 O W Z N Q Iw— .-a 1W- = CD Cn O < N H O = Z FI J O ce Q U s F- O Z LL O W ri W L^ Z M U � W Z K w cj W O Z Q s = W Y G F- W W W N � Z CW M fa t�C V of U zWco w _ X��C � W o z z *>CD zao Z N 0koQZ In U v� U C O � � C H H Lj � O � In N N � � w c� z 0 N � Ln � N Wit.' SANTE K 4l� V r VA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 G L• C. Phone: A( 5610 - `l5"62l D. Profile Number: N / o? 9 E. Generating Location: W5741m e If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) r J. Descriptioon of Waste: (w) Qh Ae. 4,J O±C'r /CT1C11 410, �O/1 d ^I1041il j K. Containers: Type UED�Drum YPE UNITS P- Pounds Quantity a6TN- Tons CY- CubicYards Units />/ O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m s�00? NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name: /)) ou6 ) c ,,„ e:nvt r"Q , I I .I fn. 8. Address:_ /> 60 _ - .Pf 5cxl)l 0 r. C Ar�Gn C. Phone: (8de D. Truck No.lfype: E. Vehicil F. Driver AcknowledgementofRecelptMaterlals:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. fol Shipment Date ' ' / L.L (Driver Signature) A. Transporter Nat B. Address: C. Phone: E. Vehicle License F. Driver Name: Truck No.lType: (Please Print) Acknowledgement of Receipt Materials: I HEREBYACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPQRTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 out McDonald, TN 37353 Chatsworth, GA 30705=2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evensville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774.5837 Elizabethtown, KY 42701 Polk County Landfill � Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. �W.A_d /t 1 1 /I it Receipt Date 4 Authorized Signature " _Z f0 W co d LO YM ~ W U W Z U W W — C) O LU :D N W O LL w L" o ¢ N 0 o O Z !:�i V FW- O .0 (n O ¢ N Ol o s z Fi .J Q U S F- OC O Z LL O U Z W �~i W Z M U 0 W M W z Uj z U) c w = O Z z LU W � H E I� N ~ Z W io U) � U co w Wv`v z<z ¢ cn N z a O �oLn v � V_ C O � � O C 'O 0 0 0 N N O N N O Ln N N LLi ' � ¢ w c� z O � z N O �i E¢- O H SANTE K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 r B.Address: �IS`iS JQirgMAn Cieek l Ec/. C. Phone: c9rvv) s6G • ^9Jr�o �% D. Profile Number: 141 E. Generating Location: 5(j'"` e 3 G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's J. Description of/Waste: Snit Ci rt1r NCB _ J,) as4e- 1. )n+kr r' �e-tt2n?ran /"bncl %)�Q7'-tr,Ga l K. Containers: Type � TYPE UNITS D- Drum P- Pounds B- Bag TN- Tons Quantity b X- Box CY- Cubic Yards Units / N O- Other. O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 67001 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: I ��O Pr5 aOR _Can- <,4%-- -1 n/c -Xal1w C. Phone: (?4) 6 N8 - SSr'G D. Truck No./Type: L1$ E. Vehicle License N /$tate: MW 44 (0do AX F. Driver Name:`' J�1 ' / (Please Print) ACknOwledgementofReceiptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G•d dShipment Date (DriSer Signature) A. Transporter C. Phone: Truck No.Ifype: E. Vehicle License No./Slate: F. Driver Name: : (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW, G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC Him Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. Receipt Date Authorized Signature � 1 � 1 C:r 0 a o \ # � \ / zLU g z / CO \ \ / L E } $ 7 ) i #LLJ ) o $ \ / \ \ } z § o 2 a e R \ $ } § \ a \ UJ $ \ d \ LU e o LU m j \ CD CD \ G § N / / § § X § 0 \ k ) z § z e LLJ m z � a k k § z o § § G 2 d _ \ \ 7\\ ®2# \�§ \ G \ \ SANTE K VA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476.9160 Fax (423) 479-1952 I B. Address: CftC /i:,ri Sv,l/e AJC �a 7ryS C. Phone: D. Profile Number: /'� C, % E. Generating Location: .Sdn- F. Address: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: J. Description of Waste K. Containers: Type TYPE UNITS ��, D- Drum P- Pounds Quantity aO B- Bag TN- Tons T N X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: t HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE- LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m L_L_LJ-J t_r,' s7oo7 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST an'�Gn n1G e7/ C. Phone: 0 )_LIV� SSS� D. Truck No.rrype: E. Vehicle License No./ We:_ M \wv L; 41 C Y PIC F. Driver Name: (Please Print) ACknOwladis it ofReCeiptMaterials:IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE•DESCRIPTION MATERIALS ,FOR TRANSPORT FROM THE GENERATOR SITE LISTED 1N THE GENERATOR PORTION OF. T IS MANIFEST. rIt 004t Date (Dover Signature) A. Transporter Name: + B. Address: C. Phone: D. Truck No.ffyl5e: E. Vehicle License No./State: F. Driver Name: ' ' (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. i G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705=2899 Rhea County Landfill Lj Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill ❑ Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill t State Road 1338 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. iff (r. � Receipt Date Authorized Signature 7 Ir 0 L o O U J 0 O O o w O z Q Qo o O O W 0O J Z Q of a 2 z O J > z o z O0 D U < O z �~ � z v z E d O u7 w � N p_ Z_ W CO n m W H N U .4 W Z U 2 co c5 W F O af lL N U. O M LU H \ p O W Z N Q F_w-- •--� Fw- O (D Z Cn O 0 OCL = Z J O U 2 O Z LL O J Q F W g Z Z �m M 5� ~ Z cn C w = oo Z F N W {L Z O ki W U) ID u U U W Z,W U Z w U K w z Z W E O j iO 00 z 0 N w = U z<z z a O N 0 lD Z �OLn � � a d� N N c� z U O ~I Z O � n N TMI cJ S.A N T E K WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (8D0) 467-9180 (423) 476-9160 Fax (423) 479-1952 G B.Address: y5g� Junc.•l�an C�FC � %lG�• G✓�,�.,,� 1 �-/lc N� ��7� C. Phone: �,�j 566 - �%$`(o �/ D. Profile Number: �� °1� E. Generating Location: '�dn"'� F. G. Phone: ( ) r If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: ( ) J. Description of Waste: �Sc,JI; d � � e � �f� :�`r'�e t� ca-�u i?c-{f•,-1,�„ l (fin L; i)� r�^7:`�`r�Gt ! K. Containers: Type � ' TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE 1h'ASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature s7oaa NON -HAZARDOUS SPECIALAND ASBESTOS WASTE MANIFEST L B. Address:___ /��O (J _ P .S4G h ,�/'• ��,�'�bn � -- Nc ,��7l� C. Phone: (?f,�� G Y�' $^S�6 D. Truck No./Type: �� E. Vehicle License No�/Sta)t1e: M W W�/ Ca � /� � F. Driver Name: ��•l /; .� %, )!.� 1 l� (Please Print) AcknowledgementofRecelptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. „ - .t- , , Shipment Date ;) ; '- / � � ' / (Driver Signature) A. Transporter Name: B. Address: ' C. Phone: ( )TD. Truck No./Type: E. Vehicle License No./State: f F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW, % G. a Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea Couniy Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 Souih Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Traii Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. Shipment Date m (t � I 1 r/ !'Y� ,,...(.�. l ;i..�. Receipt Date - Signature 0 LL o o J o O a' O z T ¢ LU co Q 0 O 2E C) > L. W af LU = z O _ d ¢ w > 0 ~O O z O � = W U � Z Z H E 0 0 a w o Ln E z_ n w Ln � m w W00 n U Y U CO W w r= o W � N M W W O ¢ O O W Z CD N U ¢ rn 0 (D O (n O ¢ 0 = 0 a U Z_ LU w U LU w H Z W 0 W �D Z Q N W = U Z ¢ Z ¢ � Z za0D O Z N lO 2: . Q Lfl N N � K � � w c7 z U 0 �O � M SANTE K VA WasteServices 650 25th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 4764160 Fax (423) 479-1952 A. Generator: B. Address:. ��j�9� T ^G��u� lee "VIlf 5v, PC C. Phone: D. Profile Number: t4cl` " E. Generating Location: F If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: tonrl �� )(:r 4-C4r , Cs K. Containers: Type UEBa E UNITS P- Pounds Quantity U TN• Tons CY- CubicYards Units TN O• Other L. Special Handling Instructions: M. Generator's CerOfication: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date s�®1s NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name: lYi,,,i Address: �S�G ?/=4c ar. C C.,e% 4c4.. C. Phone: Truck No./Type: y� E. Vehicle License No./State: / /I W q4 L P_' N L (Please Print) ACknowledgementofRecelptmaterials:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED )N THE GENERATOR PORTION OF THIS MANIFEST. G• '- Shipment Date r' (Driver, Signature) A. Transporter Name: i B. Address: / f, 0 C. Phone: ( ) DtTruck No.rrype: E. Vehicle License No./State: F. Driver Name: 1' (Please Print) Acknowledgement of Rece)t Materials: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. / G• Shipment Date (Ddver signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. n rs f -1 fit.! �� Receipt Date Authorized Signature O O U J O o O z a_ W o o c� < o o 0 0Lu 0 0 � J w � w a z O LU > z O O Z_ Z F E o_ O m w F= z n w co N W W Go z Y co W UCD H CDW O muj H O Q N O C) Z �N W M W i < 0 N � p NO 3F U Z_ ui w �U, LU w N z Z W E W i0 z� w=U z<z Ln z z a O O Ln v� u � o � c � a � O � N W Moj cl � O a z � z � � M N O O w Z SANTE K VA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 4764160 Fax (423) 479-1952 G B. Address: �✓ �J� SunG 7�� r-jn lt%GyrtC: U /C C. Phone: vwr) aid G - M4 D. Profile Number: 91a2) 9 ' +/ E. Generating Location: -Some, F. If owner of the generating facility differs from the generator, please provide: H. Owner's s�aaa NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter CQ r%'�Gn C. Phone: 04) 61,0. SS'SG D. Truck No./Type: r E. Vehicle License F. Driver Name (Please Print) AcKnowleuguent Or riftellpt materials:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIS IN THE GENERAT PORTION OF THIS MANIFEST. G. titent Dawai6 / D ' r SipnaWro) / I. Owner's Phone: ( ) J. Description of Waste: A. Transporter Name: -;U%a eci 6G�) LJ4c1 Cg+-ft /< 4En4,c.n B.Address: 1 / C. Phone: ( )�D. Truck No./Type: E. Vehicle License No./State: F. Driver Name: K. Containers: I(Please Print) Type TYPE UNITS Acknowledgement of Recelipt Materials: I HEREBY ACKNOWLEDGE THAT THE D- Drum P- Pounds ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE Quantity �V B. Beg TN- Tons X- Box CY- Cubic Yards AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED Units ?N 0- Other O- Other BELOW, G. Shipment Date L. Special Handling Instructions: (Driver Signature) M. Generator's Certification; 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature Shipment Date m m Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 El Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 y acknowledge receipt of the herebabove described materials y ( ""�rlAA � ) A lit Y Receipt Date Authorized Signature O O o U O < 0 W O _z Q cn p O W O > 0 J L11 � = w a °Lij ' LU o z o ams O Z w v g Z z F- E O a w "n 2E � M N E Z_ d W ~ Ol N W W Co F N U Y CO W U 07 K H O W � N O m w w o Q N O O Z NO — %D O * O IL Z J ce Q u S 0 Z w 0 .J W g Z Z 1- rs W SW ~ Z O W S 00 Z W Im N W LU Z O W (a/1 U Y W � •� a) Z !CO � U Z_ D7 w U LU W w Z n z p N W = U Z_ (D Q V)Z z a O N 0tDDZ O Ln �E� N W � M mry � z 0 U N H �ANTEK WasteServices 65025ih Slreet,NW, Sulte 100 Cleveland, TN 37311 (8D0) 467-9180 (423) 476-9160 Fax (423) 479-1952 B. Address: LISP `i _S �p � c. ��� n.s C r < < -<" Ic✓ S' C. Phone: �c.,,,� , j 6(0 — S 5�G `i D. Profile Number: f"%I �1 �/ ' ,< E. Generating Location: �O'""'� F. G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: ( ) J. Description of Waste: jt��<�r,�.•,al K. Containers: ; , Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. GeneretorAuthortzedAgent (Please Print) Signature Shipment Date m m �i� �,� �I �� ;� �, � , NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. Phone: (�'.='�`) � }r�, D. Truck No./Type: c/F:' E. Vehicle License F. Driver Name: (Please Prinl) ACknOwledgementofRBceiptMeterlels:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTEp IN THE GENERATOR PORTION OF THIS MANIFEST. r G. .'y. .��`�`:*� -:�;� �d' �Shi�rtle'P1t�Date / 7 � (DriysrSipnature) A. Transporter Name: � B. Address: C. Phone: ( ) i D. Truck No./Type: E. Vehicle License F. Driver Acknowledgement of ABOVE- DESCRIPTION P AND WERE TRANSPOF BELOW. i (Please Pdnt) alpt Materials: I HEREBY ACKNOWLEDGE THAT THE RIALS WERE RECEIVED FROM THE GENERATOR SITE WITHOUT INCIDENT TO THE DESTINATION LISTED G. Shipment Date / (Driver Sipneture) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Palk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 i Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials. � 1` ��� j; 3 � � (� i'„� ; , �'! .l,� � Receipt Date � ' orized Signature 0 o W U J J J O O Z W O C7 = U) O O O LU C7 J W of W Q U Z U J = LU W Q W O j O Z a O Z z U z ca. O W � I— N E Z_ W M m M 11 W w Oi H N U Y co Z U Go LU K 1— F C) N LL O re) W W o Q N LU p O W z � U Q zU C7 cn o No = a r Z J O U H O Z L m O J a z 3 � W g z N Z m LU z Z � W = 0Ln 0 J W N WF W Z O F; w a in n J Vf t0 VA U U) co Z, c) /3: m N 9 uj 9 � � i0 Ol lf7 N N � � w SAI�ITE K VA WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 A. 5 f �.� s B. Address: '�S5 5" �ary 'r� a„+ �/C .k i��✓ C. D. Profile Number: ,t-% CJ E. Generating Location: ' � F. If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: IA)GTC/o /�F.�a.,-},an K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature s�012 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name:_ / Yl ,, u n -f c , r - ARA , c <"/ C. Phone: 0) % `�1'. Truck No./Type: E. Vehicle License N9, State: A4 L/ Z)41(ve NC F. Driver Name: �' %rl/ [-)lul: �J T% (Please Print) Acknowledgement of Receipt Materlals: I HEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED,IM THE GENERATOR PORTION OF THIS MANIFEST. G.//� Shipment Date ' (Driver ature) A. Transporter C. Phone: ( ) D. Truck No.lType: E. Vehicle License No./State; F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggeit, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ezt, NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. G r,�!.!, ` �,;liJ' . Receipt Date Authorized Signature O O W O p O J Q o 0 � O H W U c� _ U)Q C O w O O w C7 W K W U J = Q 0. LU O O w F- Z > z O < Q U O Z z z E n O LU M U) 1- ~ E Z_ Q W t0 N W F- W tD F- U Y M Z U co LU U: H H O LU p N O WU W C ¢ N p O Z CD N O ¢ N O (n � O H T7 a Z J a U 2 O Z LLM W �g Z M Z 1- M W Z M w F t� IME Z (A O W 2 0 Z tN N W W Z O w Uf �0 0 U U Z !n W U K W N W Z aWtko >>Go z Q N W = U Z<Z z z a O F- N 0 to ZQ ~ 2:Ln rn N 9 9 � Ln M a O ¢ F- d' H W U Z SAN�iE K WasteServices ti50251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 B. Address: �S �� T .ar s'7��-�.,r � r'f� � ,� - C. Phone: ( ) ��L�J -�Q fir^-� y ..S 6 �ji D. Profile Number: / 7 �� �'7 '� E. Generating Location: _� S i9 n�t �- " F. G. Phone: If owner of the generating faciliiy differs from the generator, please provide: H. Owner's Name:_-_ _ �-- �' __ - __ - I. Owner's Phone: ( ) J. Description of Waste: r � ' 'r-�s � , , / i K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. r Generator Authorized Agent (Please Print) Signature �� s7o� NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name:- lZ7Tsr/ ,!-..�s�� .S-•-=�w � „� /` B. Address: .5 �" �+ _� �y . � � �- C. Phone: (� `���.h r'�"'•s'�tSO. Truck No./Type: �is E. Vehicle License No.LState: %'��'� � %` f' � �� . N F. Driver / (Please PrinQ AcknowledgementofRecelptMaterlals:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR S17E LIST IN THE GENERATORfPORTION O HIS MANIFEST. i . -' G. `. -�' ' - rit Dated //� � river Signature) A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No.ffype: E. Vehicle License No./state: F. Driver Name (Please Print) Acknowledgement of Receipt Materials: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRgNSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774-5837 Elizabethtown, KY 42701 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill ` State Road 1338 Waynesville, NC 28786 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the above described materials � ,, ipt Date ` � � �� } O- o O LLL L O O o 0 O � F- W U U 2 O Q OLIJ O O C7 J W J U a. Lli> aLU Q Z O 0O D U w C) p Z z z F E :D m O O w o z w m W LU re)H O U Y W U co — FN O W O Wu O H Q N 0 O W K O QZ cli LU (n O Q N 2 O F z cn H M ~ F � G =0 N A H LU 1�l1 J t0 VI U U Z W LU LU V) H Z W �Wio �CGW z Q N W = U Z < Z z a O O z �z�6 N � lJ C � O O � LU � N N � � w (� Z SANTEK VA WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800) 467.9160 (423) 476-9160 Fax (423) 479/,1952 A. Generator. B. Address: �%S �/� J prJto j�� I.0 : r C. Phone: ( ) Fri - �d D. Profile Number: E. Generaiing Location: S � �'i t F G. Phone: If owner of the generating facility diners from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other 0- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) re s7®1s NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter B. Address: '` -� LS 0 �r s< tv ✓� / C. Phone: ( C�5%;i;;' -17TKID. Truck No./Type: � r E. Vehicle Licet F Driver Name AcknowledgementofRecelptMaterials:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. Shipment Date (Driver Signature) A. Transporter C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./State: F. Driver Name (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Data. (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 hereby acknowledge receipt of the Signatu above described materials. Shipment DateIII Ik� ) ( ,(_ �J L! jl / }i.1 m m L�JV }t I Receipt Dater` i Authorized Signature W U O O LU _ _ > H � O W Y O U W O � d Z W N Z W W = 6 Q � O p �NTEREry FEB d 5 �17p U w w z W �wko C� 0:) Z p N W 2 U Z � Z Z a O AD oz O u�i Q Z O d O N U U LU 2 o � � U � O o � .. Z W w 9 a o � o kD O N W � z z L z �w U Z Fr_- C) a SANTE K WasteServices 65025th Street, NW, Sulte 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 L C. Phone: ( ) �' _ J�o cs qj. 6 ey% E. Generating Location: f t4 rz.1 e F. Address: G. Phone: If owner of the generating facility Iffers from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: �1 C.c1 L+J i7 er r Lam/ K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other. L. Special Handling Instructions: M. Generator's Certification: 1 HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) , Signature iC1V1 �1CVE_S .67024 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter B. Address: C. Phone: (���`�'`�C•-�-�t�D. Truck No.lType: f!`.-�. E. Vehicle License {1R. tate: %� lr LU `� F. Driver Name: I Ad �f o C�-�-i ,2 TT ' (Please Print) ACknowledgementofRecelptmate rlais: IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. G. �• Ji1,GAIV Shipment Date '� � l OY' l Zu (DriverJi aturs) A. Transporter Name: B. Add C. Phone: ( ) D. Truck E. Vehicle License No./State: F. Driver Name 'Please Print)Acknowledgement of Receipt Materials: 1 HEREBY ACKNOWLEDGE THAT 7HE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Ej Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705 2899 Gordon County Landfill 1224 Pleasant Hill Road Ext, NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m W� `..+�yllll ri,( V,�..�A ?.o,4. 1 Receipt Date � Authorized Signature a LL o 0 C o O Q O o 0 2..7 w 0 U 00 0 LU p L) z ¢ W 2 W Q LU O z > Z OU cc: W D U O z z z o 0 W o. z_ W m g m W Ln ~ r4 U Z Y W U00 F- O W N U W W o N � C) W K Co Q Z � --� ~ CD n p NO = H a U W U ce W N H z W ZO W �o > Z � W 2 U Z (< z a O oz O Ln U v � o � 9 rC-i H LU 0 0 0 CO N Ln J- � � w c7 z U N W F-I Z Z H H � w n '� z � SA�1TE K WasteServices 65025th Stree1,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 A. Generator: Pe wf. t / T, r.�� r `e B. Address: ly/ 'S/ r J O - f rf -, �/ C. Phone: ( Q Lp� - 4 sr� r eZ D. Profile Number: E. Generating Location: r,A✓s•t 4 F G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste K. Containers Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units 0- Other. O- Other. L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Signature 07022 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter B. Address = /ter c G �^ +✓t 7�4n VV 0t- I _1 Sr • r r� C. Phone: (:`�?'cS;�� _D. Truck No./Type: E. Vehicle License No./State: r 4'o 44�/ _ "" y��� A r F. Driver Name: ty'�! + it a (Plea4e Print) Acknowledgement of Receipt Materiels: I HEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. r �f Shipment Date t/ t' /jo (Driver Signature) A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No.frype: E. Vehicle License No./Slate: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Laudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I•hereby acknowledge receipt of the above described materials. Shipment Date m � 1__l__L� )I Receipt Date Authorized Signature 0 O Q J o O W C7 = U 0 0 O z Z < LU = w O Z j Z O U 0 W z Z x Z 7 H E n O n W M F- .N-i O Z_ _ W M N Lu in H N U Y W U W F= I O W N li O �uj W O Q N 0 Z � W W d' ON O co O p Yk o Cl. W U LU w N J F- Z W z W io � OD z p N W = U Z < Z za.0 ��o� O z r U v � V_ C � O O � H Lij ry 0 0 0 0�0 O CO ti Ln kD CO M a � w O Z U N W Fr- ch � N O Z 0 N 4? 020 SANTE K L A& VA WasteServices 65025th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 4764160 Fax (423) 479-1952 A. Generator: B. Address: yam`% JV . r• n .� / ✓<' r• C. Phone: ( D. Profile Number: E. Generating Location: � � i'N � F. Address: G. Phone: ( If owner of the generating faciliiy H. Owner's I. Owner's Phone: J. Description of Vµaste: from the generator, please provide: K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B. Bag TN- Tons X. Box CY- Cubic Yards Units A 0- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. r Generator Authorized Agent (Please!Print) Signature Shipment Date m m L_L_L�.J Filp s �021 NON=HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C. P�hone: ('7; '�'Truck No./Type;�.� E. Vehicle License No./State:&�,Af V ` . 4�.- f'" . i`.e;r� F Driver Name: (Please Print) AcknowledgementofReceipt Materlal6:IHEREBY ACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERAOR PORTIO .& THIS MANIFEST. fil6ment Date /7 (Driver Signature) A. Transporter Na B. Address: C. Phone: ( ) D. Truck No:lfype: E. Vehicle License No./state: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HER ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date (Driver signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill Lj Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774=5837 Elizabethtown, KY 42701 Polk County Landfill L3 Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. l l �i•(�' 1��%Y:It (% �)'_ 1; �;' Receipt Date_/`��) r Authorized Signature i o O LL O 0 o O Q 0 O � W O C7 = 0 o Li U) O LU O w w C=7 w z O ¢ LU 0 LU a a O U D U z O z Z E O O LUvn N Z_ LU O W LU F H U LUm Z U co LU F oN w O LUo N O O LU O Q Z \ ui S Fw- 00 (D ZO Q O a Z N J O w 94 2 cd O n LL Z 0 O J F W ZM 9 Z LU M � FZ- Z� C W O Z W N W W Z O W (A tp (A U U Li w LU w Ln z w z w io Q' W Z Q N LU z<z Ln Z z a O N 0 io Z a O .Ln U V) N n v � u � o � o � o M� In N N N � � � w � Z 'Nr SANTE K WasteServices 650251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 A. Generator: s�o2a . NON -HAZARDOUS ,` 1 SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: v' � �s TV�Jn t�,� ten.,., �-' r (1_ _ y2 _ C. Phone: ( ) �.slvsr r �) 6 — 7 ..ter � did D. Profile Number: rf� �ix� � �� _� i E. Generating Location: Sr/4 rt-�C F. Address: � G. Phone: ( ) If owner of the generaiing facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) �� J. Description of Waste: r � l Lu w 7 /"�L^ r�rJ K. Containers: Type �� TYPE UNITS D- Drum P- Pounds Quantity - � B- Bag TN- Tons X- Box CY- Cubic Yards Units � 0- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, 1 CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR T 281. /� /�,����,;ti._ ,��� �.�/l Generator Authorized Agent (Please Print) A. Transporter B, Address: % ✓ O �_ / �.rC�- c � .� �� a ;�� :� � yr� C. Phone: (�v�i' ����""�x.f D. Truck No./Type: � �f r E. Vehicle License No./State: fl7 �'� � e�- ` � ' - f� F. Driver Name: "I f ��r ,n ' (Please Print) AcknOwledgementofRecelptMaterlala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. ����'' � � � ` � ' ' "�' Shipment Dated �- / ��/ Z. �"� G. � i�'1, _ �, (DriveFSipnalure) A. Transporter B. Address: C. Phone: ( ) D. Truck No.ffype: E. Vehicle License No./State: F. Driver Name: (Please Pdnq Acknowledgement of Receipt Materials: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. i G. Shipment Date / / (Dnver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill Slate Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. ptDate' 'l �_ Authorized Signature T N D z � P O n r �S? ry � _v / pp a O v O Z z z Z 0" Arm n Z co o CNO) �S `L m p? <'3 A V) Of 0)rnz Z ,cwn z m ~ Enn M 0 D Z O = m 0 0 � p 1 C a v m 1 m Z m O h V -q 2 w ZIML 3 r z n 7 � P p C - T n m z 0 X =^I A 2 s� Cam] 0 � bi y O (n Om m NP O Z O D A m Im O T N C m o --I --i m C) 0 z c m ---i -Ph Fn m 3 z Lq m 0) O v 3 C Z O O -i < �) o z D m G Z) m r m = ` m o S o > o r 2 O n m D z O � O A O o O r O o SAI�JTE K WasteServices 850251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 L Q C. Phone: ( ) �,./2��s - -1'~C� � " � -����-% D. Profile Number: ("7 �.�/ �7 E. Generating Location: s't1 yyt � F. Address: G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: l H. Owner's Name: I. Owner's Phone: ( ) J. Description of Vtfaste: �'i K. Containers: , ; Type TYPE UNITS D- Drum P- Pounds Quantity � " B- Bag TN- Tons X- Box CY- Cubic Yards Units O- Other O- Other L. Special Handling M. Generator's Certification: I HEREBY CERTIFY THA7 7HE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. t Generator Authorized Agent Signature Shipment Date m m ase Print) 67019 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter B. Address: %Jr�2� �� � r r � 1a C. Phone: (��� /{ ✓� :Ss'`1- plTruck No.lfype": / 'i��s' E. Vehicle License No./Mate: �Yl Lv' _ ,_' T _��� � �� .� F. Driver ,/ (Please Print) AcknowiedgementofRecelptMaterials:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LIST DIN THE GENERATOR PORTION. OF THIS MANIFEST. r , G _�'' `z �- S � _ � .�hp�ent Date / .; / ,;( river Sipnalure) ' A. Transporter u C. Phone: ( ) D; Truck No.ffype: E. Vehicle License No./State: F. Driver Name: ' (Please Pdnt) Acknowledgement of R6Caipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. ' Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705.2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. / i _ /�' } �/ j /� �/ , " ! t' ! .��` t � � ��� 1..%W'� �, Receipt Date - 11 ��r�l � Authorized Signature 0 w O O U J O O O J O 0 O z Q co 0 O O = O > O H (D LLI z Q W U w Ir _ LLI < d 1¢ d w ::D < O z 1' Z ® E O I-1CD w M m w Ln 7=i M W M H p w co ~ W F ~ F O rkf N ui O w H O x O Z O rN Cn O Q \ D O Z _O Z I — a N U U = w 0 2 O � LL + N O B � J C U W 3 rq N ti �Ali Z Z n W W fj m U LU F ~ � W w p O Z LO) N J o o a Y ~ 0 < IQ N � CCp N Z ry W W � W� 00 M �J- tanL�mi zwto ~ z ix CO X Y zoo & Vw �`V w=U z W z¢z ~ aLi z a o Ln Z,U) �o�z Q Q, W 2:L� o N SA(�iTEK WasteServices 65025th Street,NW, Suite 100 Cleveland, TN 37311 (800)467-9180 (423)476.9160 Fax (423) 479-1952 G s�oi� `�� NON -HAZARDOUS »` SPECIAL AND ASBESTOS WASTE MANIFEST � ,:: B. Address: 'ii -'^`7�-� .l �., ,.i r' >`�t_.� ..+ � r / , ` Gt' f. C. Phone: ( } `s:.�' �- � _�; 6'" _ � :' 1-- � - ; f,• D. Profile Number: �� � �� f E. Generating Location: �'~� <t � C F. G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) J. Description of Waste: � r t. K. Containers: ,, Type +--� TYPE UNITS D- Drum P- Pounds Quantity �� B- Bag TN- Tons X- Box CY- Cubic Yards Units �J�►i O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REpUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) ' Signature A. Transporter Name: B. Address: ,` � � �� F7 / .r' ,� .• �� %� � Z . C. Phone: ('' (=) es'i �'`' YP if � ..f � ff D. Truck No./T e: / S� E. Vehice License No./$tote: �'',' '--tJ r% ,' f'' �'� iL`fC` F. Driver Name: - � r � (Please Prinq AcknowledgementofRecelptMateriala:IHEREBYACKNOWLEDGE RECEIPTOF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN��THE���•Gi..EN,,ERATOR PORTION; QF T}11S MANIFEST. G.�?l�t.%i� � 1pment Date "���- �. --J l: � �° �tunver Signature) A. Transporter f� C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./Slate: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date. / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705-2899 Rhea County Landfill � Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774.5837 Elizabethtown, KY 42701 Polk County Landfill � Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 Haywood Couhty Landfill State Road 1338 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. Shi ment Date �,% )) � P m m � + ` l� I �.,(�f � +j Recei tDate'��t ��� LJ Authorized Signature O 0 O J o O a 0 O � H W O c� _ U oO LU C7 J Lli 0.' w a v Z O ¢ w z a O O a U O Z z E Z I- E S O w UM) rn m z w in qT w LU W N H m U Y W W U F- CDuj N U- O q;r � LU O Q N 0 O W U z Q LLJ cn Q N S O o F- a i J O U S O z N. O 4 J J Q H O W 3 i Z M A Z I- M ZW z X M w F J� Z O W = 00 W N W W Z O W Q IA J U) W Uf U U w U LU W Z W 57 z0 w � 0 z� w = U Z Z z a 0 =z �oLn U_ C O O O � C r-i o d ul u1 N N N � � ~ c� z SANTE K VA WasteServices 650251h Street, NW Suite 100 Cleveland, TN 37311 (800) 467.9160 (423) 476-9160 Fax (423) 479.1952 r .Address: r C. Phone: D. Profile Number: ` 4, l E. Generating Location: S � ru C F If owner of the generating facility differs from the generator, please provide: H. Owner's I. Owner's Phone: J. Description of Waste: n I. CJ • -f ^ / r i . c/" �l K. Containers: Type D• TYPE Drum P- UNITS Pounds Quantity r,B- Bag TN• Tons X. Box CY- Cubic Yards Units O• Other O• Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) _ r Signature 670is NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter B. Address:__ C. Phone: ( '{'f ��/�'�"s"r� D. Truck No./Type: E. Vehicle License No./State: F. Driver Name: �� i%,� r ,� L<<•f_, ") =r; r (Please Print) AcknowledgementofReceiptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION OF THIS MANIFEST. Shipment Date (Driver Signature) A. Transporter Name: C. Phone: ( ) D:Truck No.IType: E. Vehicle License No./State: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE• DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Data. / / {Driver Signature) Disposal Site: (Check One) Bradley County Landfill � Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705.2899 Rhea County Landfill Ll Gordon County Landfill 207 Sanitary Drive 1224 Pleasant Hill Road Ext. NE Evansville, TN 37332 Ranger, GA 30734 Loudon County Landfill � Hardin County Landfill 21712 Highway 72 North 1620 Audubon Trail Loudon, TN 37774.5837 Elizabethtown, KY 42701 Polk County Landfill � Crittenden County Landfill 3477 FM 942 1299 Kuhn Road West West Leggett, TX 77350 West Memphis, AR 72301 0 Haywood County Landfill State Road 1338 Waynesville, NC 28786 hereby acknowledge receipt of the above described materials. Receipt Date Authorized Signature NTERE FEB gyp'" 0 o W O ❑ O J a O O H O _ W Q c� Q O � O i LLU O W (D w Of z O J LU 2 O Z LU Z O > Q U O z Z � Z H � O LU Ln o H � E z w m v' w � W � CC)U Y U 00 W LU H H O Wi N O W w o Q N O ❑ W Z (NN U Q N O ¢ N = O H Z J ce ce v x ce O z LL O J Q H z 3 Lu z M o Z LU m ®p LU z J Z O J O W N W W Z mii J (A �0 0 U U Z W U LU w J H Z W 57 zO w ko 0 z w = U Z < Z z z a aOO LU v� � o o � C c H r=-i OLU 11 N or:a � O � z SANTE K WasteServices 650 251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9160 (423) 476-9160 Fax (423) 479-1952 A. Generator: ��o�a ' � `� NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST B. Address: 11 -� 9 -S �% v +JI f�A �✓ Cr` `- k /e ice✓/} y N r 1 v .- /.�L � G � &' ��� e C. Phone: ( ) �� fi' - .S "U r' — 9,s" 6 � i D. Profile Number: 7'� / d? / `� � / E. Generating Location: .S �'•'+'+L. G. Phone: ( ) If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( ) f J. Description of IMaste: .sa �, ` e / � � �� �� f w ,r, r_ !�. f` K. Containers Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY- Cubic Yards Units f O- Other ��' ' '` O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REpUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. ,�..t/. .�� f �' GeneratorAuthodzed Agent (Please Print) 4 Signature r � A. Transporter Name: il'?r � r-%r�-P � r1 �`--,vier lQ O „f,y, � e� c_. r B. Address: i s- � �' r S r P -� tt-� 2 C. Phone: (%�^ ��}. � "�SS.'s�, Truck No./t°ype: tf � E. Vehicle License No./.State: /rl �`� `: � "/ �'� _ /✓C�, F. Driver Name: s7 n / / � ;, t i r /.' � � �'i (1 (Please Print) AcknowiedgementofReceiptMateriala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED�N THE GENERATOR PORTION OF THIS MANIFEST. G. �') Shipment Date � �. /y � / Z � (Driver Signature) A. Transporter C. Phone: ( ) D. Truck No./Type: E. Vehicle License No./Slate: F. Driver Name (Pleaee Print) Acknowledgement of Receipt Materials: I HEREBYACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evensville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774.5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 , Haywood County Landfill State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Shipment Date m m � \~�/��� � L�' �'� / l J�-'l 1 )�)��:�I Receipt Date ( Authorized Signature E NTERE F �as 2020p 0 O LL U Q J O O a W O (7 = U O O LU LU U Z Q Q W 2 W Q O Z > Z O K W 0 U z Z Z E fu O o w N m E z w r� ^� w N f m z LU U co LU O_ ~' N W 2 N L O %I- Of W O I N Q O Z NN p N *k U) O Z ce a / U O - Z a O J Z Z 3 '� W *'{ Z M ZO F M LU W F Z M C W = O Z Z O ~ a � UI �0 W UIle U w U LU w Ln 9 z w E zw LO > z Q N w 2 U Z Z Ln z z a O N 0 �D Z O Ln ��� u � o � S N M h am� W ci d' � ~ z O U Q �I Z z � r � Q � N O Z SA- T E K V VA IL A& WasteServices 650 25th Street, NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 r• B.Address: /i 4S Jc+.JF�t��.✓ C /� e�yQ. C. Phone:( ).7 Se 6" D. Profile Number: �a2 / E. Generating Location: �� +'u- � F. G. Phone: IF owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: ( } J. Description of IMaste: _ ,A . K. Containers: Type TYPE UNITS D- Drum P- Pounds Quantity B- Bag TN- Tons X- Box CY,. Cubic Yards Units O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: i HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAZARDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REQUIREMENTS OF 40 CFR PART 268 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 261. Generator Authorized Agent (Please Print) Shipment Date m m (TI—I� U701b NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST A. Transporter Name: %h'f�• � �v� R• Sr �' �•. `- •- � B. Address: r ID �= f r• �� t CIVn/ t0l�� NC ==7k %�f C. Phone: (n 6`r� �SS 6 D. Truck No./Type: Y E. Vehicle License NolState: y`'' " ' Y a a ^t C F. Driver Na / (Please Print) AcknowledgementofReceipt Materials: IHEREBY ACKNOWLEDGE RECEIPTOF THE ABOVE -DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE GENERATOR PORTION, OF THIS MANIFEST. � ; : ' ,•-'- o` �iipment Date '`r' ! ' i (Driver Signature) - A. Transporter Name: B. Address: C. Phone: ( ) D. Truck No.lType: E. Vehicle License No./State: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: 1 HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. G. Shipment Date / ! (Ortver Signature) DESTINATION Disposal Site: (Check One) Bradley County Landfill Murray County Landfill 282 Landfill Road 6565 Highway 411 South McDonald, TN 37353 Chatsworth, GA 30705.2899 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill State Road 1336 Waynesville, NC 28786 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. Receipt Date Authorized Signature K W O 2� > � p O z cs6 WJ W W Q U z > z 6- D O D m �'- o Ln F- co w w ro w m Y � U W P: ? O N O Ri- LU O O G N 0 O z N F W CDF N O N O Z F-I J c� 0 a u S O Z a O Z rol 3 �, W Z FM Z - M FM Z = O Z F O Z O �+ W U a) Y �a) r W U) Z U) as (A / 3: v z U u w Z w 7. z W O � N z� w x U zaz adz z a O 0 �o °� W Q u � o � c H H ui vi of rn m Ln � w � � z M � N J w O z W U z t a 020 SA(�ITE K WasteServices 650251h Street,NW, Suite 100 Cleveland, TN 37311 (800) 467-9180 (423) 476-9160 Fax (423) 479-1952 G B.Address: LIS%S ../ar.r��c,,, t�ree-rK' /?c✓. C. Phone: �_ �l� - y5"G,�! D. Profile Number: /tI/a�/�! E. Generating Location: S(JM e F G. Phone: If owner of the generating facility differs from the generator, please provide: H. Owner's Name: I. Owner's Phone: J. Description of Vµaste: K. Containers: �, TYPE UNITS Type D- Drum P- Pounds Quantity �� B- Bag TN- Tons X- Box CY- Cubic Yards Units TN O- Other O- Other L. Special Handling Instructions: M. Generator's Certification: I HEREBY CERTIFY THAT THE ABOVE DESCRIBED MATERIALS ARE NOT HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281 OR ANY APPLICABLE STATE LAW AND ARE NOT SUBJECT TO FEDERAL REGULATIONS FOR REPORTING PROPER DISPOSAL OF HAL4RDOUS WASTE HAVE BEEN FULLY, ACCURATELY AND PROPERLY DESCRIBED, CLASSIFIED AND PACKAGED, AND ARE IN PROPER CONDITION FOR TRANSPORTATION ACCORDING TO APPLICABLE REGULATIONS; AND, IF THE WASTE IS A TREATMENT RESIDUE OF A PREVIOUSLY RESTRICTED HAZARDOUS WASTE SUBJECT TO THE LAND DISPOSAL RESTRICTIONS, I CERTIFY AND WARRANT THAT THE WASTE HAS BEEN TREATED ON ACCORDANCE WITH THE REpUIREMENTS OF 40 CFR PART 288 AND IS NO LONGER A HAZARDOUS WASTE AS DEFINED BY 40 CFR PART 281. Generator Authorized Agent (Please Print) Signature 67013 NON -HAZARDOUS SPECIAL AND ASBESTOS WASTE MANIFEST C B, Address: I SCo G %�Sna /� Imo/ C. Phone: �,'��) t9 y�• �`ii6 D. Truck No./Type: L✓f: E. Vehice License F. Driver Name:�� (Please PrinQ AcknowledgementofReceiptMaterlala:IHEREBYACKNOWLEDGE RECEIPT OF THE ABOVE•DESCRIPTION MATERIALS FOR TRANSPORT FROM THE GENERATOR SITE LISTED IN THE OENERATOR;PORTION OF THIS MANIFEST. �_t �/ G• � � S��ment Date/ 5`"Jl,�� (Driver Signature) A. Transporter Name: B. Address: C. Phone: ( ) `b. Truck No.ffype: E. Vehicle License No.lState: F. Driver Name: (Please Print) Acknowledgement of Receipt Materials: I HEREBY ACKNOWLEDGE THAT THE ABOVE- DESCRIPTION MATERIALS WERE RECEIVED FROM THE GENERATOR SITE AND WERE TRANSPORTED WITHOUT INCIDENT TO THE DESTINATION LISTED BELOW. i� G. Shipment Date / / (Driver Signature) Disposal Site: (Check One) Bradley County Landfill 282 Landfill Road McDonald, TN 37353 Rhea County Landfill 207 Sanitary Drive Evansville, TN 37332 Loudon County Landfill 21712 Highway 72 North Loudon, TN 37774-5837 Polk County Landfill 3477 FM 942 West Leggett, TX 77350 0 Haywood County Landfill ' State Road 1338 Waynesville, NC 28786 Murray County Landfill 6565 Highway 411 South Chatsworth, GA 30705-2899 Gordon County Landfill 1224 Pleasant Hill Road Ext. NE Ranger, GA 30734 Hardin County Landfill 1620 Audubon Trail Elizabethtown, KY 42701 Crittenden County Landfill 1299 Kuhn Road West West Memphis, AR 72301 I hereby acknowledge receipt of the above described materials. I. Authorized Signature ', Receipt Date NON -HAZARDOUS 1, Generator ID Number 2. Page 1 of 3. Emergency Response Phone 4. Waste Tracking Number WASTE MANIFEST 1 11-800-261-0031 'I�MA 5. Generator's Name and Mailing Add Widison County Schools Generator's Site Address (if different than mailing address) 230 Dogwood Lane Brushy Creek Elementary School Marshall, NC 28753 Brush Creek Road Generator'82W. 9-9276 Marshall, NC 6, Transporter 1 Company Name U.S. EPA ID Number Mountain Environmental 7, Transporter 2 Company Name U.S. EPA ID Number 1 8, Designated Facility Name and Site Address U.S. EPA ID Number Mountain Environmental 1560 Pisgah Dr., Canton, NC 28716 Facili 's Phone: 828-648-5556 10, Containers 11. Total it 12. Unit 9. Waste Shipping Name and Description Quantity No. Type ' Non -Regulated Waste, Non -Hazardous Liquid, N.O.S. o 001 DM a (Petroleum Impacted Absorbent & Water) % W z W 2, c� 3. 4, 13. Special Handling Instructions and Additional Information dg:;Meoe� pro44 14, GENERATOR'S/OFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged, marked and labeled/placarded, and are in all respects in proper condition for transport according to applicable international and national governmental regulations. Generata• Offeror's Printed/Typed Name Sign Month Year .DDayy mi 15. Intema venal Shipments ❑ Import to U.S. ❑ Export from U.S. Port of entry/e z Transporter Signature for exports only): Date leavingU.S.: w 16. Transporter Acknowledgment of Receipt of Materials 2 Trans rter 1 Printed(ryped Signature Month Day Year O IL a nsporter 2 P ntedrryped Name lure Month Da Year F 17. Discrepancy 17a, Discrepancy Indication Space ❑ Type ❑ Quantity yp ❑ Residue ❑ Partial Rejection Full Rejection Manifest Reference Number: F 17b, Alternate Facility (or Generator) U.S. EPA ID Number J U Phone: rai Facility's w 17c. Signature of Alternate Facility (or Generator) Month Day Year z a V5 W 18, Designated Facility Owner or Operator: Certification of receipt of materials covered by the manifest except as noted in Item 17a Printed/Typed Name Sign Month Day Year r 169-BLC-O 5 1197?'Rev. 9/0e :TOR NON -HAZARDOUS 1 •Generator ID Number 2. Page 1 of 3. Emergency Fespopse Phone 4. Waste Tracking Number WASTE MANIFEST `f--�'I�p (�� j .- � �. 5. Generator's Name and Mailing Addr ss Generator's Site Address (if different than mailing address) ��� � C/� I��� Generator's �/ ' Phone: /� 6. Transporter 1 Company Name _ U.S. EPA ID Number Ir 7. Transporter 2 Company Name U.S. EPA ID Number 8. Designated Facility Name and Site Atldress /j�� �y�??7 'r--�y//`��U.S. EPA ID Number � — 's -,��%�� �'�'!�� v� v�J � •V Facilit Phone: / 9. Waste Shipping Name and Qescription 10. Containers 11. Total 12. Unit No. Type Quantity Wt.Nol. 2 1. I - - �;-,_� a w /� ���� ����.� � ���y� L� 3. 4. 13. Special Handling Instructions and Additional Information 14. GENERATOR'S/OFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged, marked and labeled/placarded, and are in all respects in proper condition for transport according to applicablein{te�rnational and national governmental regulations. Generato Offeror's Printed/Typed Name Sign(....w" Month Day Year � 15. International Shipments - ❑ ❑.Export Import to U.S. from U.S. Port of xit: z Trans orter Si nature for ex orts onl Date leavin U.S.: w 16. Transporter Acknowledgment of Receipt of Materials � Transporter 1 Printed/Typed Name Signat Month Day Year � a � ! -ri / a Transporter 2 rinted/Typed Name 'nature Month Day Year x ' F- 17. Discrepancy 17a. Discrepancy Indication Space ❑ Quantit ❑Type ❑Residue ❑Partial ❑Full y Rejection Rejection Manifest Reference Number: 17b. Alternate Facility (or Generator) U.S. EPA ID Number U LL Facility's Phone: w 17c. Signature of Alternate Facility (or Generator) Month Day Year a z N W 0 18. Designated Facility Owner or Operator: Certification of receipt of materials covered by the manifest except as noted in Item 17a Printed/Tyy�pe�d!�Name / Signatu� �/' Month Day Year �/` / /"" � %1/'� � / �'7�t' e � 169-BLC-O 5 11977 (Rev. 9/09) DESIGNATED FACILITY TO GENERA OR NON -HAZARDOUS 1, Generator ID Number 3. F.rgetgency RespWW Phone S y�a� T acgi�p Number cg WASTE MANIFEST T2,Pagelof MAU�i 05. Generator's Name and Mailing Ad n County SchnM Generator's Site Address (if different than mailing address) 230 Dogwood Lane Brushy Creek Elementary Schonl , Marshall, NC 28753 Brush Creek Road ^?8-644-9276 Marshall, NC Generator's Phone: 6. Transporter 1 Company Name Mountain Environmental U.S. EPA ID Number 7. Transporter 2 Company Name U.S. EPA ID Number 8. Designated Facility Name and Site Address, _ antain Environmental U.S. EPA ID Number ', 560 Pisgah Dr., Canton, NC.287A 828-648-5556 Facili 's Phone: 9, Waste Shipping Name and Description 10. Containers 11. Total 12. Unit No. Type Quantity Wt.Nol. 1. — (lrs' I)hJ cc (Petroleum Impacted Absorbent & Water) F a W ` w 2. 3. 4. 13. Special Handling Instructions and Additional Information Off y So 7S 14. GENERATOR'S/OFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged, marked and labeled/placarded, and are in all respects in proper condition for transport according to applicable international and national governmental regulations. Gener is/Offeror's Pri ted/Typed Name Signatu Month Day Year rl mi 15. International Shipments ❑ ❑ ' f- Import to U.. Export from U.S. Port of entry/. Transporter Signature for exports only): Date leaving U.S.: cc 16. Transporter Acknowledgment of Receipt of Materials w Transp er 1 Printed(Typed Nam SignaA Month Day Year . CL to ¢ Transport. d/Typed Name ignature Month Day Year cc 17. Discrepancy 17a. Discrepancy Indication Space ❑ Quantity ❑Type ❑Residue ❑ El Partial, Rejection Full Rejection Manifest Reference°Number: 17b. Alternate Facility (or Generator) U.S. EPA ID Nglnber LL Facility's Phone: w 17c. Signature of Alternate Facility (or Generator) Month Day Year z cs w w 0 18. Designated Facility Owner or Operator: Certification of receipt of materials covered by the manifest except as noted in Item 17a Printed/Typed Name Signa Month Day Year r � 169-113LC-0 5 11977 (Rev. 9/09) � APPENDIX D PHOTOGRAPHS Wastewater pond during water removal. Looking east. Wastewater pond during water removal. Looking east. Wastewater pond after water removal water removal. Looking north. Wastewater pond after water removal water removal. Looking southwest. MARTIN S LAG LE GEOSCIENCES, PA PREPARED FOR: DATE 3/20/20 SITE PHOTOGRAPHS Wastewater Pond Closure CHK: RLM PO Box 1023 Powell Industries, Inc. Powell Industries, Inc. Black Mountain INC 28711 Waynesville, NC DR: CES 828.669.3929 828.669.5289 MARTIN S LAG LE GEOSCIENCES, PA PREPARED FOR: DATE 3/20/20 SITE PHOTOGRAPHS Wastewater Pond Closure CHK: RLM PO Box 1023 Powell Industries, Inc. Powell Industries, Inc. Black Mountain INC 28711 Waynesville, NC DR: CES 828.669.3929 828.669.5289 Pond after removal of residuals. Looking southeast. Pond after removal of residuals. Looking northwest. Pond after removal of residuals. Looking northeast. MARTIN S LAG LE GEOSCIENCES, PA PREPARED FOR: DATE 3/20/20 SITE PHOTOGRAPHS Wastewater Pond Closure CHK: RLM PO Box 1023 Powell Industries, Inc. Powell Industries, Inc. Black Mountain NC 28711 Waynesville, NC DR: CES 828.669.3929 828.669.5289