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Home My WebLink AboutWQ0033677_Monitoring - 03-2022_20220420 (2) • 'FORM: NDMR 08-11 NON-DISCHARGE MONITORING REPORT (NDMR) Page / of Permit No.: WQ0033677 Facility Name: CASE FARMS HATCHERY County: Burke Month: March Year: 2022 PPI: 001 Flow Measuring Point: 0 Influent ❑Effluent ❑No flow generated Parameter Monitoring Point: ❑influent 0 Effluent ❑Groundwater Lowering ❑Surface Water c0 ' ' 00625 00665 - 00610 00530 31616 00940 00094 '' 70300 00620 Parameter Code ---► 50050 00400 00310 b,. - > O m a) m > y �, v _ ' E E 3 ,e o m � o'o mQ' ° .0 m ? -No mat � o) i = a ¢ E E � o = O E o a o m . o = 8 0 - ._ Z 2 o 2 o a 0 U F' U iz LL CO E I- to u) I' . L C N_ti) In Z �6 :'_' F- At E- NO CC Q. 7 " U O 0 .. Z :, Z L �' 24-hr hrs GPD su mg/L ttng/L mg/L #/100 mL mg/L p02 mg/L mg/L mg/L mglL mg/L i,: 1 5:00 10.5 7,700 2 6:00 7 7,700 3 5:00 10 7.700 1.______� 4 5:00 9 7.700 ( i 5 ,7,700 , 6 7,700 I I _ 7 5:00 9.5 7,700 7.2 8 5:00 10 7,700 C 9 6:00 6 7,700 I - - - 10 5:00 13 I 7.700 AiL 11 5:00 10.5 7,700 i 12 5:30 5 7,700_ ,,. 13 77 14 5:00 11.5 7,71 d'!`= 7.2 15 5:00 11.5 7,700 16 5:30 9 7,700 .'; I- - 17 5:00 11.5 7,700 ' O _ 18 5:00 10.5 7.700 `' QV• 19 7,700 20 7.700 21 5:00 11 7,700 7.2 ._,.. 22 5:00 11 7,700 '' .• 23 5:00 7 7,700 €: -- - 24 5:00 10.5 7,700 'i f 25 5:00 11.5 0, 7,700 26 7,700 L 27 7,700 `` ,' 28 5:00 4 7,700 6 8 1167 34.52 390 >5600 62 9 1188 844 1.56_ 71 72 10.1 29 5:00 11.5 7,700 " _ 30 5:00 9 7,700 ii 31 5:00 12 7,700 Average: 7,700 1,167.00 '34.52 390.00 62.90 1,188.00 844.00 1.56 71.00 72.56 ' 10.10 Daily Maximum: 7,700 720 1,167.00 34.52 390.00 62.90 1.188.00 844.00 1.56 71.00 72.56 I 10.10 Daily Minimum: 7,700 6 80 1,167.00 ,:.:13. 52 390.00 62.90 1,188.00,:r 844.00 - 71.00 72„5,,6., 10.10 Sampling Type y Monthly Limit: 3000 u Daily Limit: - _ -raga,_ Sample Frequency: j 4,.. ":� FORM: NDMR 08-11 NON-DISCHARGE MONITORING REPORT(NDMR) Page of Sampling Person(s) Certified Laboratories Name: James Edwards Name: Water Tech Labs Inc Name: Cindy McGinnis Name: Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? 0 Compliant ❑ Non-Compliant If the facility is non-compliant,please explain in the space below the reason(s)the facility was not in compliance. Provide in your explanation the date(s)of the non-compliance and describe the corrective action(s)taken.Attach additional sheets if necessary. Operator in Responsible Charge(ORC)Certification Permittee Certification ORC: Cindy McGinnis Permittee: Case Farms Hatchery Certification No.: 992943 Signing Official: Cindy McGinnis Grade: SI Phone Number: 808-438-6900 Signing Official's Title: Hatchery Supervisor Has the ORC changed since the previous NDMR? ❑Yes RI No Phone Number: 828-438-6900 Permit Expiration: 12/31/2021 C c� ti—)Li-a� C A/ � 1-09 �- Signature Date Signature Date By this signature,I certify that this report is accurrate and complete to the best of my knowledge. I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 08-11 NON-DISCHARGE APPLICATION REPORT(NDAR-1) Page / of U` Permit No.: WQ0033677 Facility Name: Case Farms Hatchery County: Burke Month: March Year: 2022 Field Name: 2 i,'-Old Name: 3 Field Name: 4 Did irrigation occur ~,. . -- - 'Area(acres): 1 Area(acres): 1.13 'Area(acres): 1.12 r Area(acres): 0.96 at this facility? +' Cover Crop: FESCUE y Cover Crop: FESCUE Cover Crop: FESCU Z. Cover Crop: FESCUE p P p YES ]Noi El ', Hourly Rate(in): 0.23 , Hourly Rate(in): 0.27 ?,Hourly Rate(in): 0.24 „ Hourly Rate(in): 0.2 ''Annual Rate(in): 29.18k; Annual Rate(in): 29.18 '•nnual Rate(in): 29.18 y, Annual Rate(in): 29.18 Weather Freeboard Field Irrigated? ,YES;: ■ Field Irrigated? E YES ❑NO b:Field Irrigated? __,YES No..i Field Irrigated? 0 YES ❑NO y a y 1 ' .c 2 a, w .n m •c .c • , c a; -o Is rn E , I•d a •o c> E arb mof >. ° E :° m a. as E .d a; Q; >, E c E E . a -% ?' E c c I,:E v m > E c > cl. E m w m > E E >` c coa c E • -c EN c E - o E c .c E ca • o EE 0 y a a o >, a j a 2' m in - a m in .% o w °-- `i (a x o ca c a - co •f0 m E o o L ,, a ° a i= o o m =�., o a i= •c o p m I 0 o a F. .` D o c s o o a 1- - o 0 m N E co a7 �iyl�� Q _ J > < _ -J 2 -J •,.� Q _. J J.:� Q J 2 = J a H a w °F in ft ft ^'' gal min in in a,I gal min in in ',¢,gal min in in F._ gal min in in 1 C 55 2 C 56 r. 3 C 58 8.8 Mi.' fr 4 C 57 5 C 55 6 PC 56 7 R 56 0.2 `' 8 PC 59 9 R 50 1.25 , 10 C 50 8 F: 11 R 47 0.5 12 PC 42 , 13 C 55 14 C 54 " ..._1 15 C 55 _ 16 R 51 0.6 ��i o" 17 C 55 7.6 18 PC 55 ,11 19 C 60 Y 20 C 57 .4,2,100 22 0.08 0 iJ' 2,500 26 0.08 0.08 9,500 26 0.08 0.08 i;, 2,100 31 0.08 0.08 21 C 60 'i 2,100 22 0.08 0.08('i 2,500 26 0.08 0.08 9,500 26 0.08 0 08 M' 2,100 31 0.08 0.08 22 C 60 ""2.100 22 0.08 0.08?' 2,500 26 0.08 0.08 "-0,500 26 0.08 0.08.' 2,100 31 0.08 0.08 23 R 58 2 24 CL 57 7 (2.100 22 0.08 0 08 2,500 26 0.08 0.08 9;500 26 0.08 0.r:. 2,100 31 0.08 0.08 25 C 55 „,2,100 22 0.08 0.0810 2,500 26 0.08 0.08 9,500 26 0.08 0.08 +9 2,100 31 0.08 0.08 26 PC 60 `.:,2,100 22 0.08 0.08",I 2,500 26 0.08 0.08 +,500 26 0.08 0.08 --. 2,100 31 0.08 0.08 27 C 58 04.2,100 22 0.08 0.08; 2,500 26 0.08 0.08 -'''2,500 26 008 0.08 01 2,100 31 0.08 0.08 28 C 59 12.100 22 0.08 0 08'.,. 2,500 26 0.08 0.08 2,500 26 0.08 0 08 a 2,100 31 0.08 0.08 29 C 59 2,100 22 0.08 0 08;' 2,500 26 0.08 0.08 ,500 26 0.08 0,08 2,100 31 0.08 0.08 30 C 60 .(2.100 22 0.08 008y, 2,500 26 0.08 0.08 ' 9,500 26 0.08 0.08 „(1 2,100 31 0.08 0.08 31 R 62 0.75 7.3 Monthly Loading: '21 000 �/:'<X/` 0.77 r� ?�020 0.81 25,000 `79"./ifii2 0.82 -'�d7s i ' 0.81 12 Month Floating Total(in): , . � ,, 16.73 ',r�. y 17.60 '/ i4.?.:j��"',t��i 1, , 16.42 (, (,;(°s i 19.49 y/'� FORM: NDAR-1 08-11 NON-DISCHARGE APPLICATION REPORT (NDAR-1) Page of Did the application rates exceed the limits in Attachment B of your permit? 0 Compliant ❑Non-Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Q Compliant ❑Non-Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? 2 Compliant ❑Non-Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? ❑� Compliant ❑Non-Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? E Compliant ❑Non-Compliant If the facility is non-compliant, please explain in the space below the reason(s)the facility was not in compliance. Provide in your explanation the date(s)of the non-compliance and describe the corrective action(s)taken.Attach additional sheets if necessary. Operator in Responsible Charge(ORC)Certification Permittee Certification ORC: Cindy McGinnis Permittee: Case Farms Hatchery Certification No.: 992943 Signing Official: Cindy McGinnis Grade: SI Phone Number: 828-438-6900 Signing Officials Title: Hatchey Supervisor Has the ORC changed since the previous NDAR-1? ❑Yes 0 No Phone Number: 828-438-6900 Permit Exp.: 12/31/21 Pf 2&/ ...V.AVAlti-4 141-29- Signature Date Signature Date is signature,I certify that this report is accurrate and complete to the best of my knowledge. I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ifIRTER4Tggiut Lartivar.inc. POT OFFICE BOX 1056 ^ /15 PINEWOOD PLAZA DR. GRANITE FALL,NO8) 6 C44L O NP 28630 (8 SAMPLE: Case Farms-Hatchery COLLECTION DATE: 3/28/2022 COLLECTION TIME: 14:30 PERMIT#: ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/28/2022 RECEIVED TIME: 14:50 REPORTED: 4/7/2022 ANALYSIS ANALYSIS EFFLUENT UNITS DATE ANALYST BOD 1,167 mg/L 3/30/22 jdg TSS 390 mg/L 3/30/22 jrg NH3 34.52 mg/L 3/31/22 jrg >5600 /100mL 3/28/22 Th Fecal Coliform 4/1/22 Th 1,188 umhos/cm Conductivity 4/1/22 lag �n c � 1.56 mg/L NO3-N 0 � � � 4/1/22 jdg 71.00 mg/L TKN 4/1/22 jdg 72.56 mg/L T.Nitrogen 3/31/22 jdg 10.1 mg/L T.Phosphorus 4/4/22 62.9 mg/L Chloride 3/30/22 TDS 844 mg/L i II LOG ID: 2203-443 REPORTED BY: NC CERTIFIED LAB#50 4t* WATEFVTLGts ionsym.111C. POST OFFICE BOX 4056 ° #5 PINEWOOD PLAZA'YR. GRANITE FALLS,NORTH CA44.OLINA 28630 (828) SAMPLE: Case Farms-Hatchery-MW#3 COLLECTION DATE: 3/28/2022 COLLECTION TIME: 13:00 PERMIT#: ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/28/2022 RECEIVED TIME: 14:50 REPORTED: 4/7/2022 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST 108 mg/L 3/30/22 TDS 4/1/22 Th 140 umhos/cm Conductivity mg/L 3/31/22 jrg <1.0 Chloride J 12.9 mg/L 4/4/22 Metals pace lag mg/L 4/1/22 NO3-N N; 41 J 2.60 jdg mg/L vJ <1.0 4/1/22 jdg T.Nitrogen 2.60 mg/L 4/1/22 0.31 mg/L 3/31/22 jdg T.Phosphorus �l REPORTED BY: NC CERTIFIED LAB#50 LOG ID' 2203 444 #10,464, # E .,T 'few/rzc. POST O'FICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS,N 6 ORT CAROLINA 28630 (828) -4444 SAMPLE: Case Farms-Hatchery-MW#4 COLLECTION DATE: 3/28/2022 COLLECTION TIME: 14:00 PERMIT#: ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/28/2022 RECEIVED TIME: 14:50 REPORTED: 4/7/2022 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST 107 mg/L 3/30/22 TDS Conductivity 138 umhos/cm 4/1/22 Th jrg NH3 ;P(10/�� 6\ �/ <1.0 mg/L 3/31/22 Chloride ?/ 13.2 mg/L 4/4/22 Metals / pace lag 2.76 4/1/22 f ,'' mg/L NO3-N ;' 4/1/22 jdg <1.0 mg/L TKN mg/L Nitrogen i 2.76 4/1/22 jdg3/31/22 jdg T.Phosphorus 0.16 mg/L 1 REPORTED BY: NC CERTIFIED LAB#50 LOG ID: 2203-445 ftlill* L POST OF ICE 30X 1056 ^ :15 'NEVJOOD PLAZA DR. GRANITE FALLS, '"ORTN CAROLINA 28630 (828)396-4444 SAMPLE: Case Farms-Hatchery-MW#5 COLLECTION DATE: 3/28/2022 PERMIT#: COLLECTION TIME: 13:30 ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/28/2022 RECEIVED TIME: 14:50 REPORTED: 4/7/2022 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST TDS ` 111 mg/I 3/30/22 4/1/22 Th Conductivity / 136 umhos/cm NH3 r', i,,, ,, <1.0 mg/L 3/31/22 jrg Chloride 12.9 mg/L 4/4/22 Metals pace NO3-N 2.64 mg/L 4/1/22 lag TKN sl <1.0 mg/L 4/1/22 jdg 1 T.Nitrogen 2.64 mg/L 4/1/22 Jdg r T.Phosphorus „ <0.16 mg/L 3/31/22 jdg 1 i E6 LOG ID: 2203-446 REPORTED BY: NC CERTIFIED LAB#50 Kernersville,NC 27284 www.pacelabs.com a�yfiica� (704)977-0981 ANALYTICAL RESULTS Project: CASE FARMS Pace Project No.: 92595832 sample: CASE FARMS MW3 Lab ID: 92595832001 Collected: 03/28/22 00:00 Received: 03/29/22 09:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville ND 1mg/L 0.010 1 03/30/22 16:14 03/30/22 22:47 7440-38-2 Arsenic Copper 0.0081 mg/L 0.0050 1 03/30/22 16:14 03/30/22 22:47 7440-50-8 ND mg/L 5.0 1 03/30/22 16:14 03/30/22 22:47 7440-09-7 Sodium Sotausium 5.0 1 03/30/22 16:14 03/30/22 22:47 7440-23-5 n0.03 8.4,� mg/L 4 \' mg/L 0.010 1 03/30/22 16:14 03/30/22 22:47 7440-66-6 Zinc 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Asheville 108 mg/L 25.0 1 03/30/22 15:15 Total Dissolved Solids 4500 Chloride Analytical Method:SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 12.9 mg/L 1.0 1 04/04/22 18:17 16887-00-6 5310B TOC Analytical Method:SM 5310B-2014 Pace Analytical Services-Asheville 1.7 mg/L 1.0 1 03/31/22 16:10 7440 44 0 Total Organic Carbon REPORT OP LABORATORY ANALYSIS Analytical Environmental services, III Client: Pace Analytical Services, Inc. Client Sample ID: CASE FARMS MW3 - Project Name: 92595832 Collection Date: 3/28/2022 12:01:00 AM Matrix: Aqueous Lab ID: 2203Z24-001 Reporting Dilution Result Qual Units BatchlD Date Analyzed Analyst Analyses Limit Factor Formaldehyde by SW8315A BRL 50 ug/L 333521 1 03/30/2022 16:08 TO Formaldehyde Qualifiers: ` Value exceeds maximum contaminant level E Estimated(value above quantitation range) S Spike Recovery outside limits due to matrix BRL Below reporting limit H Holding times for preparation or analysis exceeded Narr See case narrative F Analyzed in the lab which is a deviation from the method N Analyze not NELAC certified c t...ess than Result value ��r,alyi,� -.. di t .;ort Pt ene�tbod alauk -;' . 7tn 0 Kernersville,NC 27284 _ PaceAnalytteaf (704)977-0981 �aoww.pacelabs.com ANALYTICAL RESULTS Project: CASE FARMS Pace Project No.: 92595832 Sample: CASE FARMS MW4 Lab ID: 92595832002 Collected: 03/28/22 00:00 Received: 03/29/22 09:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual ------- 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville ND mg/L 0.010 1 03/30/22 16:14 03/30/22 22:50 7440-38-2 Copper 0.0 ' mg/L Arsenic ND 0.0050 1 03/30/22 16:14 03/30/22 22:50 7440-50-8 ND': mg/L 5.0 1 03/30/22 16:14 03/30/22 22:50 7440-09-7 Potassium 5.0 1 03/30/22 16:14 03/30/22 22:50 7440-23-5 Sodiumn8'5 1 mg/L 0.025 / Zinc mg/L 0.010 1 03/30/22 16:14 03/30/22 22:50 7440-66-6 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Asheville Total Dissolved Solids 107 mg/L 25.0 1 03/30122 15:15 4500 Chloride Analytical Method:SM 4500-CI-E-2011 Pace Analytical Services Asheville Chloride 13.2 mg/L 1.0 1 04/04/22 18:18 16887-00-6 5310B TOC Analytical Method:SM 5310B-2014 Pace Analytical Services-Asheville Total Organic Carbon ND mg/L 1.0 1 03/31/22 17:12 7440-44-0 1r I A Ft CRATORYANAL\'SIS •Analytical Environmental Services,Inc Date: 31-Mar-22 Client: Pace Analytical Services, Inc. Client Sample ID: CASE FARMS MW4 Project Name: 92595832 Collection Date: 3/28/2022 12:01:00 AM • Lab ID: 2203Z24-002 Matrix: Aqueous Reporting Dilution Analyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Formaldehyde by SW8315A Formaldehyde BRL 50 ug/L 333521 1 03/30/2022 16:19 TO Qeulifiers: Value exceeds maximum contaminant level E Estimated(value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank a Less than Result value Citrates Mau Result value J Estimated value detected below Reporting Limit Page 21 of 26 ca aca nalyaica` NC Kernersville, 27284 +aww.pacela6s.cam NC(704)977-0981 ANALYTICAL RESULTS 'roject: CASE FARMS 'ace Project No.: 92595832 ample: CASE FARMS MW5 Lab ID: 92595832003 Collected: 03/28/22 00:00 Received: 03/29/22 09:20 Matrix: Water Report Limit DF Prepared Analyzed CAS No. O�_ Results Units ._------ ____ Parameters �_ --- -- '00.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville ND mg/L 0.010 1 03/30/22 16:14 03/30/22 23:00 7440-38-2 copy er c ND mg/L mg/L 0.0050 1 03/30/22 16:14 03/30/22 23:00 7440-50-8 ND 5.0 1 03/30/22 16:14 03/30/22 23:00 7440-09-7 copper Potassium 8.1 mg/L 5.0 1 03/30/22 16:14 03/30/22 23:00 7440-23-5 Sonc ND mg/L 0.010 1 03/30/22 16:14 03/30/22 23:00 7440-66-6 Zinc 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Asheville 03/30/22 15:15 Total Dissolved Solids 111 mg/L 25.0 1 4500 Chloride Analytical Method:SM 4500-CI-E-2011 Pace Analytical Services-Asheville 04/04/22 18:18 16887 00 6 12.9 mg/L 1.0 1 Chloride 53106 TOC Analytical Method:SM 5310B-2014 Pace Analytical Services-Asheville 03/31/22 17:28 7440 44-0 Total Organic Carbon ND mg/L 1.0 1 REPORT OF (.A O ATORY ANALYSIS ' Analytical Environmental Services,Inc Client Sample ID: CASE FARMS MWS Client: Pace Analytical Services, Inc. Collection Date: 3/28/2022 12:01:00 AM Project Name: 92595832 Matrix: Aqueous Lab ID: 2203Z24-003 Dilution Reporting Qual Units BatchID Date Analyzed Analyst Result Factor Analyses Limit Formaldehyde by SW8315A ug/L333521 1 03/30/2022 16:29 TO Formaldehyde Btu, 50 E Estimated(value above quantitatimt range) 1 Qualifiers: ' Value exceeds maximumcontaminant level S Spike Recovery outside limits due to matrix I BRL Below reporting limit Alarr See case narrative H Holding times for preparation or analysis exceeded F Analyzed in the lab which is a deviation from the method -lnal to uo�PJ t3LA certified - Less than Result value • • ivieritecli 1zi Inc Environmental Laboratory Laboratory Certification No. 165 14.0 Report Date: 4/5/2022 Contact: Cathy Gragg Client: Water Tech Labs;Inc 5 Pinewood Plaza Drive Granite Falls,NC 28630 Date Sample Rcvd: 3/29/2022 Meritech Work Order# 03292237 Sample: Case Farms-MW3 Grab 3/28/22 Parameters Result Analysis Date Reporting Limit Method MBAS (as LAS 340) <0.10 mg/L 3/29/22 0.10 mg/L SM 5540 C Meritech Work Order# 03292238 Sample: Case Farms-MW4 Grab 3/28/22 Parameters Result Analysis Date Reporting Limit Method MBAS(as LAS 340) <0.10 mg/L 3/29/22 0.10 mg/L SM 5540 C Meritech Work Order# 03292239 Sample: Case Farms-MW5 Grab 3/2$/22 Parameters Result Analysis Date Reporting Limit Method 3/29 22 0.1.0g/ham SM 5540 C MBAS(as LAS 3 0) <0.1.0 mg/L / I hereby certify that I nave reviewed and approve these se data_ta_ Laboratory Representative ve 1 , (°s (Tt 4:4 Road. Reidsville,North Carolina 27320 • f ace /�na( U ocal Kernersville,NC 27284 i�w vnv.pacelabs.com (704)977-0981 ANALYTICAL RESULTS Project: CASE FARMS Pace Project No.: 92595832 Sample: CASE FARMS EFFLUENT Lab ID: 92595832004 Collected: 03/28/22 00:00 Received: 03/29/22 09:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Asheville Total Dissolved Solids 844 mg/L 50.0 1 03/30/22 15:15 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services-Asheville Chloride 62.9 mg/L 2.0 2 04/04/22 18:19 16887-00-6 REPORT OF LABORATORY ANALYSIS �,µxtxpt ii rtik pH WORKSHEET Analysis Collection • Date Time Sample ID Date Time Results SU's Analyst Buffer 4.00 ***** ***** z a d iO3 2 Buffer 10.00 ***** ***** `0•ab l i3 7L Buffer 7.00 QC ***** ***** 7. ***** Slope Efficiency ***** ***** ✓ /3 o.s CASE- A lit/3 3 2$-2-2- /3 OD ep•3 /33.r '1 M In/5 y (33b lea (Q '3 � ifrvtkJLf ��ao �,�f 1 3� „� r✓FF If /`f3 G.7 " EFF - ! �� t Y30 --,,,.,,,* 5c3 7 cR oreQ-R. Q C 7,�1D 7,0 1 4 __ _ WATERS: ' tP1 LOT# 8i 13f 3 i,Kr NOV l.02; 7.00 LOT# 81.1.0554, EX"! NOV 2023 1O O0 LOT# 8109645 EXP OCT 2023 r,1, P 1 f4E.ff BRTA 3L`"_ J pH WORKSH EET Analysis Collection • Date Time Sample ID Date Time Results SU's Analyst Z 2 07 Up Buffer 4.00 ***** ***** i o76 2. Buffer 10.00 C>?off -Buffer 7.00 QC ***** ***** 7. (P ***** Slope Efficiency ***** ***** I./ /O (S CASE FARMS _7_zz /olc� 7• 2 0 17 " Duplicate K N 7•7-- / -r'is- 1 o l 9 Buffer 7.00 QC 7 0 f S Buffer 4.00 ***** ***** �' (lb C-Q'e‘%b C 0 Cn Z Buffer 10.00 ob(-)1. Buffer 7.00 QC ***** ***** ***** Slope Efficiency ***** ***** /0 .f D CASE FARMS �_( Z2- (0 7' Z "Duplicate Buffer N 7 L /4Zs/4SrJ /° �`� 7• d / SF �� Buffer 4.00 ***** ***** Y ` vi) d -4-6 i Buffer 10.00 l O ' Buffer 7.00 QC ***** ***** ***** — ° crib ***** Slope Efficiency ***** ***** ✓ /Z CASE FARMS 3 -2 1-2 �- P 2- P 7" Z "Duplicate A. H ?. z /' '`I s� P 2 1 g Buffer 7.00 QC , / Buffer 4.00 ***** ***** Buffer 10.00 ***** ***** Buffer 7.00 QC ***** ***** ***** Slope Efficiency ***** ***** CASE FARMS " "Duplicate Buffer 7.00 QC Buffer 4.00 ***** ***** Buffer 10.00 ***** ***** Buffer'7,00 QC ***** ***** ***** Slope Efficiency ***** ***** — — CASE FARMS - upiiu.Le Buffer 7.00 QC BtJFt+1 RS WATER TECH...� S 4.00 LOT# 8111363 EXP NOV 2023 WAT 7.00 LOT# 8110554 EXP NOV 2023 10.00 LOT# 8109645 EXP OCT 2023 • 5 Pinewood Plaza Drive -P.O. Box 1056 • Granite Falls, NC 28630 Phone (828) 396-4444 -Fax (828) 396-5761 CLIENT: Case Farms Hatchery PHONE NUMBER: 828-438-6900 ext.6975 c/o Cindy McGinnis TYPE SAMPLE: n/a Manager No. LOCATIONS: 4 -s6sl,�q Gr�� SAMPLER NAME: {3u-f-liI- . Ef i C Sample Collection Information TYPE CONTAINERS Sample Location Grab/ Plastic/ ANALYSIS REQUIRED Facility Name DATE TIME TEMP. No. Composite Glass Effluent 300 ►i+:30 Do Grab 8 Plastic Fecal Coliform, Chloride, TDS BOD-5, TSS, Conductivity NO3-N,TKN, NH3-N Monitoring Well#3 �.f 3 QC i D Grab 12 Plastic/ TDS, Chloride, MBAS, Glass Formaldehyde, Conductivity As, Cu, K, Zn, Na NH3-N. NO3-N, T.P., TKN TOC VOC(Annual Nov. only) { Grab 12 Plastic/ Same As#3 Monitoring Well#4 /) :®Q g Glass Monitoring Well#5 (9 Plastic/ Same As#3 Grab 12 f 1 3 3a Glass Relinquished By: Date: Time: Re ved3yg __Oat Time: /.19404.,„/ 3Ag Li' S-6 elinquished By: Date: Time: Re ved 6y Date: Time: d r/ PfFSERVATION: _ - '�# 9/4°C k1 i :SO4 p]NaOH HNO3 Dechlornating Agent CjOther_ r SAMPLE TEMP. @ LAB (°C) • b Chlorine Residual6 0 mg/I