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HomeMy WebLinkAboutWQ0034775_Monitoring - 03-2022_20220420 wood. 30 March 2022 cNv N North Carolina Department of Environmental Quality !0 Division of Water Resources cr Information Processing Unit Q 1617 Mail Service Center • -' N Raleigh, North Carolina 27699-1617 • o 0 cq Subject: March 2022 Monitoring Well Sampling and Analysis Results Bakelite LLC Closed-Loop Recyde System Permit(WQ0034775) 333 Neils Eddy Road Riegelwood, North Carolina 28456 Wood E&IS Project No.6228220017 To Whom it May Concern: On behalf of Bakelite LLC., Wood Environment & Infrastructure Solutions, Inc (Wood E&IS) is pleased to provide the Division of Water Resources(DWR)of the North Carolina Department of Environmental Quality (DEQ) with the results of the March 2022 monitoring well sampling event at the referenced site in Riegelwood, North Carolina. If you have questions regarding this report or need additional information, please contact Mr. Ben Moore at (910)452-1185. Sincerely, Wood Environment& Infrastructure Solutions, Inc. `I Vr - atAl* /l�✓�d/W� W. Ben Moore Carolyn Smillie Project Manager Technical Reviewer Attachments: A)Compliance Monitoring Forms(GW-59 and GW-59A) B) Laboratory Analytical Reports Cc: Mr. Ronald Bazinet, Bakelite Ms. Emily Thompson, Bakelite Correspondence: Wood Environment&Infrastructure Solutions,Inc. 5710 Oleander Drive,Suite 110 Wilmington,North Carolina 28403 Tel (910)452-1185 Fax (910)791-1338 Licensure:NC Enaineerino F-1253 NC Geoloov C-247 11� SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: and copy t0: DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:(919)733-3221 - , FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0034775 Expiration Date: January 31,2028 Facility Name: Bakelite LLC Non-Discharge UIC Permit Name(if different): Permit No.W00034775 Bakelite Synthetics—Riegelwood CLRS Closed-Loop Recycle System Columbus County NPDES Other Facility Address: 333 Neils Eddy Road TYPE OF PERMITTED OPERATION BEING MONITORED Riegelwood (Street) NC 28456 County Columbus Lagoon ❑Remediation: Infiltration Gallery Sta p' (Zip) ❑ Spray Field ❑ Remediation: Contact Person: Mr.Ronald Bazinet Telephone#: (910)655-2263 ext 5257 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name:WWMW-1 No.of wells to be sampled: 2 ❑ Water Source Heat Pump ❑■ Other: CLRS (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): WWMW-1 Date sample collected: March 09,2022 FIELD ANALYSES: WAS Well Depth: 17.80 ft. Well Diameter: 2 in. pH 00400: 7.59 units Temp.00010: 16.27 °C DRY at Depth to Water Level 82546:10.85 ft.below measuring point Screened Interval: 7.8 ft. to 17.8 ft. Spec.Cond.00094: 3995 µMhos time of sampling, Measuring Point is 2.45 ft.above land surface Relative M.P. Elevation: 23.29 ft. Odor 00085: odor check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance black/cloudy here:® Samples for metals were collected unfiltered: 10 YES LI NO and field acidified: ®YES ❑NO LABORATORY INFORMATION ' Date sample analyzed:March 10-21,2022 Laboratory Name: Environmental Chemists,Inc. Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N oo615 mg/L Pb-Lead 01051 ug/L Coliform:MF Fecal 31616 /100mL Nitrate(NO3)as N 0062o <0.02 mg/L Zn-Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 2.46 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 1260 mg/L Al-Aluminum 01105 mg/L Formaldehyde(8315A): 270 ug/L pH(Lab)00403 units Ba-Barium 01007 DJ ug/L Naphthalene(8260):6.02 ug/L TOC o0680 69.7 mg/L Ca-Calcium 00916 mg/L Carbon Disulfide(8260):874 ug/L Chloride o094o mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 807 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑� Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC(GWVOC) method# 8260 low concentration Total Ammonia o0s10 580 mg/L Mg-Magnesium 00927 mg/L , method# - (Ammonia Nitrogen;NH as N;Ammonia Nitrogen,Total g NH, g Mn-Manganese 01055 ug/L , method# TKN as N oos25 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a 1 DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.Ronald Bazinet-Bakelite Site Leader _67'I4-ti' ��" f 'y/I /l 2 Z Permittee(or Authorized Agent)Name and Title-Please print or type Signature of"ermittee(or Authoriz•d A1nt) (Date)!!! GW-59 Rev.2/2010 GW-59A COMPLIANCE REPORT FORM Permit#WQ0034775 (Submit one each monitoring period with GW-59 forms.) Enter date monitoring results were due.(4/30/2022 ) Will this monitoring report(GW-59 and GW-59A) YES CO) be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES `NO) IF the answer to•question 1 or 2 Is"YES",list In the space provided below the well identification number(s)and explain the problems encountered in obtaining the required information. • 3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO identification plate,area overgrown,etc.)?If the answer is "Yes",contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? NO If the answer to question 4 is"NO",skip to section 8. If the answer to question 4 Is"YES"list the affected wells individually with constituent(s)and concentration(s) exceeding standards In the space provided below: WWMW-1: Total Dissolved Solids(1260 mg/L);Total Ammonia Nitrogen(580 mg/L);Sulfate(807 mg/L);Naphthalene(6.02 ug/L);Carbon Disulfide(874 ug/L) WWMW-2: Total Dissolved Solids(500 mg/L);Total Ammonia Nitrogen(26.1 mg/L);pH(5.92 su) 5 For the constituents Identified in question 4 above,have standards been exceeded previously for the YES NO same constituent(s)In the same well(s)In the last two years? If the answer to question 5 is"NO",skip to section 8. If the answer to question 5 Is"YES",list in the space provided below, each well with constituent(s)exceeding standards, concentration(s)reported,and sample collection date for each occurrence(for the last two years). W WMW-1:Total Ammonia Nitrogen 783 mg/L(3/10/20),916 mg/L(7/16/20),610 mg/L(11/24/20),748 mg/L(3/17/21),890 mg/L(7/08/21),760 mg/L(11/10/21);TDS 1160 mg/L(3/10/20);1090 mg/L(7/16/20);1380 mg/L(11/24/20),1840 mg/L(3/17/21),2520 mg/L(7/08/21),2410 mg/L(11/10/21);Sulfate 779 mg/L(3/10/20),1470 mg/L(7/16/20),772 mg/L(11/24/20),761 mg/L (3/17/21),315 mg/L(7/08/21),1590 mg/L(11/10/21);Carbon Disulfide 1950 ug/L(3/17/21)W WMW-2:Total Ammonia Nitrogen 34.3 mg/L(3/10/20),48 mg/L(7/16/20),28.5 mg/L(11/24/20),45.4 mg/L(3/17/21),54.1 mg/L(7/08/21),64.2 mg/L(11/10/21);T05 758 mg/L(7/16/20),679 mg/L(11/24/20),950 mg/L(3/17/21),623 mg/L(7/08/21),513 mg/L(11/10/21);pf 6.15 su(3/10/20),5.25 su(7/16/20),4.88 su(11/24/20),4.73 su(3/17/21),5.58 su(7/08/21),5.56 su(11/10/21) 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer Is "YES",a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is"NO",monitoring wells may be improperly located;contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is"YES", describe those actions in the space provided below. If the answer.to question 7 Is"NO",contact the Regional Office within 90 days;an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. The Lined Pond has been permanently removed from closed-loop recycle service. 8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the fop ofthe current GW-59 form. 1 (i �� (1r(aret,'A ( dtI t tl'il ;Y c�t=:t19 iiiJ')1 Xs itr•1 pe^ ii kc li it7t +�t9it li+ a ! 1 t ati��a i ly . AY •( 1= i e�f i k _ \ y * s,y 9 [� �,fa�i.l.i IgLi -,t a.�_ i'/,,:�el ��.d. _i4'd.('_I ��i°i•V _.. . ei"`),i.i.•1t�o1�, i air�1.� )�� -� '�., 4-H id l`'I%11•I V/Z/7,2 Signature • Permittee(or Auth izofi Agent) Date GW-59A 12/8/2003 i SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: and 1 copy to: DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:(919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0034775 Expiration Date: January 31,2028 - Facility Name: Bakelite LLC Non-Discharge UIC Permit Name(if different): Permit No.W00034775 Bakelite Synthetics—Riegelwood CLRS Closed-Loop Recycle System Columbus County NPDES Other . Facility Address: 333 Neils Eddy Road TYPE OF PERMITTED OPERATION BEING MONITORED Riegelwood (Street) NC 28456 Count y Columbus ❑ Lagoon ❑Remediation: Infiltration Gallery CCir,, Sheet p ❑ Spray Field ❑Remediation: Contact Person: Mr.Ronald Bazinet Telephone#: (910)655-2263 ext 5257 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name:WWMW-2 No. of wells to be sampled: 2 ❑ Water Source Heat Pump ❑U Other: CLRS (from Permit) SAMPLING INFORMATION If WELL • WELL ID NUMBER(from Permit): WWMW-2 Date sample collected: March 09,2022 FIELD ANALYSES: • WAS Well Depth: 13.21 ft. Well Diameter: 2 in. pH 00400: 5.92 units Temp.00010: 16.65 °C DRY at Depth to Water Level 82546:8.30 ft. below measuring point Screened Interval: 3.21 ft. to 13.21 ft. Spec.Cond.00094: 716 µMhos time of sampling, Measuring Point is 1.56 ft.above land surface Relative M.P. Elevation: 15.89 ft. Odor cocas: none check Volume of water pumped/bailed before sampling: 4.5 gallons Appearance cloudy here:® Samples for metals were collected unfiltered: YES ❑ NO and field acidified: ®YES ❑NO LABORATORY INFORMATION Date sample analyzed:Marchl0-22,2022 Laboratory Name: Environmental Chemists,Inc. Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N coals mg/L Pb-Lead oiosi ug/L i Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N oos20 32.6 mg/L Zn-Zinc o1os2 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P oosss 0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 500 mg/L Al-Aluminum o11os mg/L Formaldehyde(8315( q50 ug/L pH(Lab)00403 units Ba-Barium 01007 ug/L (J�J TOC ooseo 4.2 mg/L Ca-Calcium 00916 mg/L Chloride oo940 mg/L Cd-Cadmium 01027 ug/L Arsenic o1002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) i Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate oosas 197 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? • Yes(1) ❑ No(0) Specific Conductance moss µMhos K-Potassium 00937 mg/L VOC(GWVOC) , method# 8260 low concentration Total Ammonia ooseo 26.1 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese o1055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. [, Ronald Bazinet-Bakelite Site Leader 014/ /GI/ ) ' J /Z/ZZ Permittee(or Authorized Agent)Name and Title-Please print or type Signature or Permittee(orAuthori.ed gent) (late) GW-59 Rev.2/2010 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax ero 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS infow environmentalchemists.com Wood -AMEC Date of Report: Mar 25, 2022 5710 Oleander Drive , Suite 110 Customer PO#: 6228220017.6228.573000 Wilmington NC 28405 Customer ID: 11070019 Attention: Ben Moore Report#: 2022-04313 Project ID: Bakelite Acme CLRS Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-10326 Site: WWMW-02 3/9/2022 9:55 AM Water Client Test Method Results Date Analyzed Sulfate EPA 300.0,Rev.2.1, 1993 197 mg/L 03/10/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 26.1 mg/L 03/15/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 500 mg/L 03/10/2022 Total Phosphorus SM 4500 P(F-H)-2011 0.04 mg/L 03/17/2022 Total Organic Carbon (TOC) SM 5310 B-2014 4.2 mg/L 03/14/2022 1,1,1,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,1,1-Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,1,2-Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,1-Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,1-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,1-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2,3-Trichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2,4-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2-Dibromoethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2-Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,3,5-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,3-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 1,4-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Report#:: 2022-04313 Page 1 of 6 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemists.com Wood -AMEC Date of Report: Mar 25, 2022 5710 Oleander Drive , Suite 110 Customer PO#: 6228220017.6228.573000 Wilmington NC 28405 Customer ID: 11070019 Attention: Ben Moore Report#: 2022-04313 Project ID: Bakelite Acme CLRS 2-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 2-Hexanone SW 846 Method 8260D/5030B <2.5 pg/L 03/21/2022 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Acetone SW 846 Method 8260D/5030B <2.5 pg/L 03/21/2022 Acrolein SW 846 Method 8260D/5030B <5 pg/L 03/21/2022 Acrylonitrile SW 846 Method 8260D/5030B <5 pg/L 03/21/2022 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Bromoform SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Bromomethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Carbon Disulfide SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Carbon tetrachloride SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Chlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Chloroethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Chloroform SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Chloromethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 cis-1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Dibromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Dibromomethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Ethylbenzene SW 846 Method 82600/5030B Y <0.5 pg/L 03/21/2022 Hexachlorobutadiene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 IPE SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Iso ro (benzene SW 846 Method 8260D/5030B P PY <0.5 pg/L 03/21/2022 M+P Xylene SW 846 Method 8260D/5030B <1.0 pg/L 03/21/2022 MEK SW 846 Method 8260D/5030B <2.5 pg/L 03/21/2022 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Report#:: 2022-04313 Page 2 of 6 • Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax r 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info(a'environmentalchemists.com Wood -AMEC Date of Report: Mar 25, 2022 5710 Oleander Drive , Suite 110 Customer PO#: 6228220017.6228.573000 Wilmington NC 28405 Customer ID: 11070019 Attention: Ben Moore Report#: 2022-04313 Project ID: Bakelite Acme CLRS MIBK SW 846 Method 8260D/5030B <2.5 pg/L 03/21/2022 MTBE SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 ortho-Xylene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 p-lsopropyltoluene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 sec-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 tert-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Toluene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Trans-1,3-dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Trichlorofluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Vinyl chloride SW 846 Method 8260D/5030B <0.5 pg/L 03/21/2022 Formaldehyde SW846 8315A <50 pg/L 03/14/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 Rev 2 0,1993 0.34 mg/L 03/10/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 32.9 mg/L 03/14/2022 Nitrate Nitrogen Subtraction Method 32.6 mg/L 03/21/2022 Total Nitrogen(Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2.0,1993 25.2 mg/L 03/18/2022 Total Nitrogen Total Nitrogen 58.1 mg/L 03/21/2022 Report#:: 2022-04313 Page 3 of 6 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info(i4environmentalchemists.com Wood -AMEC Date of Report: Mar 25, 2022 5710 Oleander Drive , Suite 110 Customer PO #: 6228220017.6228.573000 Wilmington NC 28405 Customer ID: 11070019 Attention: Ben Moore Report#: 2022-04313 Project ID: Bakelite Acme CLRS Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-10327 Site: WWMW-01 3/9/2022 10:15 AM Water Client Test Method Results Date Analyzed Sulfate EPA 300 0,Rev.2.1. 1993 807 mg/L 03/10/2022 Ammonia Nitrogen EPA 350 1,Rev.2 0, 1993 580 mg/L 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 1260 mg/L 03/10/2022 Total Phosphorus SM 4500 P(F-H)-2011 2.46 mg/L 03/16/2022 Total Organic Carbon (TOC) SM 5310 B-2014 69.7 mg/L 03/15/2022 1,1,1,2-Tetrachloroethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,1,1-Trichloroethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,1,2-Trichloroethane SW 846 Method 8260D/5030B < 0.50pg/L 3/16/2022 1,1-Dichloroethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,1-Dichloroethene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,1-Dichloropropene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.50 pg/L 3/16/2022 1,2,3-Trichloropropane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2,4-Trimethylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2-Dibromoethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2-Dichlorobenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,2-Dichloroethane SW 846 Method 82600/5030B < 0.50 pg/L 3/16/2022 1,2-Dichloropropane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,3,5-Trimethylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,3-Dichlorobenzene SW 846 Method 82600/5030B < 0.50 pg/L 3/16/2022 1,3-Dichloropropane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 1,4-Dichlorobenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 2,2-Dichloropropane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Report#:: 2022-04313 Page 4 of 6 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sU 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info it environmentalchemists.com Wood -AMEC Date of Report: Mar 25, 2022 5710 Oleander Drive , Suite 110 Customer PO#: 6228220017.6228.573000 Wilmington NC 28405 Customer ID: 11070019 Attention: Ben Moore Report#: 2022-04313 Project ID: Bakelite Acme CLRS 2-Chlorotoluene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 2-Hexanone SW 846 Method 8260D/5030B <2.50 pg/L 3/16/2022 4-Chlorotoluene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Acetone SW 846 Method 8260D/5030B < 2.50 pg/L 3/16/2022 Acrolein SW 846 Method 8260D/5030B < 5.00 pg/L 3/16/2022 Acrylonitrile SW 846 Method 8260D/5030B < 5.00 pg/L 3/16/2022 Benzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Bromobenzene SW 846 Method 82600/5030B < 0.50 pg/L 3/16/2022 Bromochloromethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Bromodichloromethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Bromoform SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Bromomethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Carbon Disulfide SW 846 Method 8260D/5030B 874 pg/L 3/16/2022 Carbon tetrachloride SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Chlorobenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Chloroethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Chloroform SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Chloromethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 cis-1,3-Dichloropropene SW 846 Method 82600/5030B < 0.50 pg/L 3/16/2022 Dibromochloromethane SW 846 Method 8260D/50308 < 0.50 pg/L 3/16/2022 Dibromomethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Dichlorodifluoromethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Ethylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Hexachlorobutadiene SW 846 Method 8260D/5030B < 0.50 pg/L 3 /16/2022 IPE SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Isopropylbenzene SW 846 Method 82600/5030B < 0.50 pg/L 3/16/2022 M+P Xylene SW 846 Method 8260D/5030B < 1.00 pg/L 3/16/2022 MEK 5W 846 Method 8260D/5030B < 2.50 pg/L 3/16/2022 Methylene chloride SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Report#:: 2022-04313 Page 5 of 6 L Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sn 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info6tenvironmentalchemists.com Wood -AMEC Date of Report: Mar 25, 2022 5710 Oleander Drive , Suite 110 Customer PO#: 6228220017.6228.573000 Wilmington NC 28405 Customer ID: 11070019 Attention: Ben Moore Report#: 2022-04313 Project ID: Bakelite Acme CLRS MIBK SW 846 Method 8260D/5030B < 2.50 pg/L 3/16/2022 MTBE SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Naphthalene SW 846 Method 8260D/5030B 6.02 pg/L 3/16/2022 n-Butylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 n-Propylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 ortho-Xylene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 p-Isopropyltoluene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 sec-Butylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Styrene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 tert-Butylbenzene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Tetrachloroethene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Toluene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Trans-1,3-dichloropropene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Trichloroethene SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Trichlorofluoromethane SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Vinyl chloride SW 846 Method 8260D/5030B < 0.50 pg/L 3/16/2022 Formaldehyde SW846 8315A 270 pg/L 03/14/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev 2.0,1993 0.08 mg/L 03/10/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.06 mg/L 03/14/2022 Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/21/2022 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2.0,1993 645 mg/L 03/18/2022 Total Nitrogen Total Nitrogen 645 mg/L 03/21/2022 Comment: fI Reviewed by: �. . 7 Report# 2022-04313 Page 6 of 6 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax smi 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@ environmentalchemists.com Wood-Amec QC - 2022-04313 LCS Parameter True Value Result %Recovery Limits mg%L mg/L % Ammonia 5.0 5.1 102 90-110 Ammonia 5.0 5.1 102 90-110 NO2 0.60 0.61 102 90-110 NO3 &NO2 1.00 1.01 101 90-110 Sulfate 50.0 47.4 95 90-110 TDS 600 583 97 90-1 10 TOC 10.0 10.8 108 90-110 TOC 10.0 10.8 108 90-110 TK.N 4.0 4.0 100 90-110 TP 1.60 1.60 100 90-110 TP 1.60 1.64 102 90-1 10 MS/MSD Parameter True Value Recovery % Limits % Limits % Recovery mg'L mg/L Difference Recovery Difference Ammonia 4.0 4.0/4.0 100/100 0 80-120 <20 Ammonia 4.0 3.9/3.9 98/98 0 80-120 <20 NO2 0.50 0.49/0.51 98/102 4 80-120 <20 NO3 &NO2 0.50 0.50/0.50 100/100 0 80-120 <20 Sulfate 10.0 9.3/9.3 93/93 0 80-120 <20 TDS N/A N/A N/A N/A 80-120 <20 TOC 10.0 10.0 100 N/A N/A <20 TOC 5.0 5.4 108 N/A N/A <20 TKN 5.0 4.7/4.9 94/98 4 N/A <20 TP 2.00 1.90/2.00 95/100 5 80-120 <20 TP 2.00 1.88/1.84 94/92 2 80-120 <20 • Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info'i environmentalchemists.com DUPLICATE SAMPLES Results Parameter m /L %Difference Limits % g Ammonia N/A N/A N/A < l0 Ammonia N/A N/A N/A WA NO2 N/A N/A WA < 10 NO3 &NO2 N/A N/A N/A <20 Sulfate <15 <15 0 < 10 TDS 489 511 4 < I0 TOC 5.1 5.1 0 <10 TOC 1.7 1.8 6 <10 TKN N/A NIA WA <10 TP N/A N/A N/A <10 TP WA N/A N'A <l0 BLANK Results Limit Parameter mg/L mg/L Ammonia <0.1 0.1 Ammonia <0.1 0.1 NO2 <0.01 0.01 NO3 &NO2 <0.01 0.01 Sulfate <2.5 2.5 TDS <2.5 2.5 TOC <0.25 0.25 TOC <0.25 0.25 TKN <0.25 0.25 TP <0.02 0.02 TP <0.02 0.02 LABORATORY CONTROL SAMPLE #1 Report#2022-04313 Page 1 of 3 Method Spike Blank Spike QC Limits Spike Compounds Blank Added (Mandatory) p Result Result Recovery ( ry� Recovery Range Dichlorodifluoromethane <0.5 10 8.94 89.4 33.3-150 Chloromethane <0.5 10 8.85 88.5 61.2-128 Vinyl chloride <0.5 10 8.68 86.8 54.3- 134 Bromomethane <0.5 10 10.26 103 64.6- 143 Chloroethane <0.5 10 9.07 90.7 55.8-153 Trichlorofluoromethane <0.5 10 9.03 90.3 52.9-153 1,1-Dichloroethene <0.5 10 9.38 93.8 59.1 -145 Acetone <2.5 50 50.09 100 50.3- 155 Methylene chloride <0.5 10 9.24 92.4 52.0- 141 trans-1,2-Dichloroethene <0.5 10 9 90 58.3- 145 MTBE <0.5 10 9.79 97.9 58.3-145 1,1-Dichloroethane <0.5 10 9.03 90.3 66.1 -140 IPE <0.5 10 10.35 104 52.5-147 2,2-Dichloropropane <0.5 10 8.87 88.7 59.9-137 cis-1,2-Dichloroethene <0.5 10 9.16 91.6 57.4-139 MEK <2.5 50 52.43 105 58.9-135 Bromochloromethane <0.5 10 10.53 105 63.5-130 Chloroform <0.5 10 9.15 91.5 54.2-153 1,1,1-Trichloroethane <0.5 10 9.09 90.9 60.6-130 Carbon tetrachloride <0.5 10 9.14 91.4 51.7-147 1,1-Dichloropropene <0.5 10 9.16 91.6 53.6- 134 Benzene <0.5 10 9.38 93.8 63.3- 133 1,2-Dichloroethane <0.5 10 10.41 104 62.6-150 Trichloroethene <0.5 10 9.17 91.7 73.1 -138 1,2-Dichloropropane <0.5 10 9.21 92.1 61.8- 138 Dibromomethane <0.5 10 10.47 105 56.4- 136 LABORATORY CONTROL SAMPLE #1 Report#2022-04313 Page 2 of 3 Method Spike Blank Spike QC Limits Spike Compounds Blank Added (Mandatory) p p Result Result Recovery ( ry) Recovery Range Bromodichloromethane <0.5 10 9.24 92.4 74.3-143 cis-1,3-Dichloropropene <0.5 10 8.99 89.9 63.9- 135 MIBK <2.5 50 52.2 104 58.7-145 Toluene <0.5 10 9.28 92.8 62.3- 143 trans-1,3-Dichloropropene <0.5 10 10.16 102 71.3-143 1,1,2-Trichloroethane <0.5 10 10.22 102 57.7- 147 Tetrachloroethee <0.5 10 10.27 103 58.1 - 139 1,3-Dichloropropane <0.5 10 9.57 95.7 61.5- 147 2-Hexanone <2.5 50 53.71 107 59.6- 148 Dibromochloromethane <0.5 10 10.07 101 69.5- 147 1,2-Dibromoethane <0.5 10 10.54 tos 69.2- 133 Chlorobenzene <0.5 10 9.11 91.1 76.5- 117 Ethyl benzene <0.5 10 9.36 93.6 62.9- 143 1,1,1,2-Tetrachloroethane <0.5 10 10.57 106 69.4-137 M+P Xylene <1 20 18.63 93.2 62.5-134 O-Xylene <0.5 10 9.16 91.6 62.3-140 Styrene <0.5 10 9.38 93.8 66.8-131 Bromoform <0.5 10 10.06 101 61.6-141 Isopropylbenzene <0.5 10 9.18 91.8 68.1 -130 Bromobenzene <0.5 10 9.78 97.8 64.9- 125 1,1,2,2-Tetrachloroethane <0.5 10 10.57 106 65.7-146 n-Propylbenzene <0.5 10 9.37 93.7 54.2- 149 1,2,3-Trichloropropane <0.5 10 10.06 101 68.5-145 2-Chlorotoluene <0.5 10 9.35 93.5 56.8- 147 1,3,5-Trimethylbenzene <0.5 10 9.48 94.8 63.8 - 137 Ol d0 4 p 14 N0 CM M rN N N ,;D N.-1 MQ, ern- Mrr M M 4:,-- NM IZCt . - — — — - — — — - — — .-y .-1 „i ---I I I I I I 1 I I I I 1 I 1 I C O ,D O ao O to O ooC in `O to k ) O QN lf) I \D,aCC) N M �M r'=; O 0o cit. 'tin' 0t tvoD O Mt` e 4' 00 to 'D 0 i ? 00 N 00 t� Ch 01 — C}' 00 N vO l� ^ N a :r 41c, `! Q\ O\ C cps ON U ON ON Ct ON 4. kr, M cn ti) co 'r cocl M M V1 M v1 Cr Ct N N O v1 O „,,a) D\ 0 U Q, a; O, Q� 0\ 0\ O 6 O . Nt1 p Ct a E, :--: Z � o n,� © © O O 0 O © © © © © © O O C N � o CQ II. O - to to to to to to to to to to to to to F °' c o O o co 0 0 0 0 0 0 0 0 0 0 Q � c' V V V V V V V V V V V V V V v v 0 a) d a a) o a a) a) a' 0 a >~ O � ° ate) a) ° c co 0 0) a) a) 0 u a) 4-) Oc'cl 0 V y v O — O N O cp. O C y O tu a) O U O a) 0qO , C c o E. 0) 0 �, 0 :-° E-H -_ E...., .a, = 4 W Q O s Q 4 aO ." r) O o U N U M .) 4 CO N N N N c� N U v 4 1) .— ' — - x 4 . Q d • Analytical Environmental Services,Inc Date: 21-Mar-22 Client: Environmental Chemists,Inc. Client Sample ID: 22-10326 Project Name: 2022.54393- dLI3 13 'VI Zz(zz Collection Date: 3/9/2022 9:55:00 AM Lab ID: 2203D12-017 Matrix: Aqueous Reporting Dilution Analyses Result Qual Units BatchlD Date Analyzed Analyst Limit Factor Formaldehyde by SW8315A Formaldehyde BRL 50 uglL 332416 I 03/14/2022 11:44 TO Qu•lifien: • Value exceeds maximum contaminant level E Estimated(value above quantization range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysts exceeded Narr See case narrative N Analyze not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value f Estinuted value detected below Reporting Lunn Page 20 of 25 � � — c�L\313 Analytical Environmental Services,Inc Date: 21-Mar-22 Client: Environmental Chemists,Inc. Client Sample ID: 22-10327 Project Name: 2022-A4349:t{3 13 '(I) 3(22-IZZ Collection Date: 3/9/2022 10:15:00AM Lab ID: 2203D12-018 Matrix: Aqueous Reporting Dilution Analyses Result Qual Units BatchlD Date Analyzed Analyst Limit Factor Formaldehyde by SW8315A Formaldehyde 270 250 ugt/L 332416 1 03/14/2022 12:05 TO Qualifier: • value exceeds maximum contaminant level E Estimated(value above quanuacon range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Hart See case narrative N Analyte not NELAC certified F Analyzed in die lab which is a deviation from the method B Analyze detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 21 of 25 Environmental Chemist, Inc.,Wilmington, NC Lab#94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client WOO Date: h olc) Report Number: a — V(13 13 Receipt of sample: ECHEM Pickup 0 Client Deliveryyl IUPS 0 FedEx 0 Other 0 ❑ YES 0 NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt 3. g °C Corrected temperature upon receipt 'C How temperature taken: 0 Temperature Blank 0 Against Bottles IR Gun ID:Thomas Traceable S/N 192511657 IR Gun Correction Factor'C:0.0 ❑ YES 0 NO 3. If temperature of cooler exceeded 6°C,was Project Mgr./QA notified? 0 YES 0 NO 4. Were proper custody procedures(relinquished/received)followed? jig YES ❑ NO 5. Were sample ID's listed on the COC? YES 0 NO 6. Were samples ID's listed on sample containers? YES 0 NO 7. Were collection date and time listed on the COC? kYES 0 NO 8. Were tests to be performed listed on the COC? YES 0 NO 9. Did samples arrive in proper containers for each test? 54 YES 0 NO 10. Did samples arrive in good condition for each test? YES 0 NO 11. Was adequate sample volume available?' Dit YES 0 NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of<2?* YES 0 NO 14. Were cyanide samples received at a pH>12? ❑ YES 0 NO 15. Were sulfide samples received at a pH>9? YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L?** ❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L? ❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatifes are pH checked at time of analysis and recorded on the benchsheet. ** bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s)incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding(circle one): H2504 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed,notate in comments below Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or notify the state lab if directed to analyzed by the customer.Who was notified,date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC.QA.002 Rev 1 envirochem ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington,NC 28406 Analytical&Consulting Chemists NCDENR: DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 O FFICE:910- 2-0223 FAX it nmenta chemists.com2-4424 COLLECTION AND CHAIN OF CUSTODY Client: p PROJECT NAME: -Ec, k ( CAA? -0 3/ ADDRESS: 1s � Q�G.`, � Dv-I, REPORT NO: a._ __ V CONTACT NAME: ' N, \\A6°.M REPORT TO: PO NO: (oL�,� _se �K��3c.hi , � ,'�3� i C .4• COPY TO: s PHONE/FAX: I a Z(S ( I S Sam led B : email: ...CAA , lrindZP-f WAG . C , G• SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge, Other: Collection d Sample Identification ti �; o PRESERVATION -• O J . O W a 4 '�' O D -eh a In m O E a g o a r E `o z v ro 0 0 0 ` w ANALYSIS REQUESTED Date Time Temp u - u a 2 z° = s i / t- g '1 1.Z. SS ` / ° AU-D2� W C P P G 3 -cps, SV e Nti ri • ��W�Ml1,l—a 3�lzz 1Z�� P �� .I.rb eh c 0 `-F ;20O LL i'MC, G IC)S i SO -CA' e, N‘, -r1°,-9 0 G �.S �2 .SG aY S, W.r.ab><, �S� iv) NOTICE•DECHLORINATION: Samples for Ammonia.TKN,Cyanide,Phenol and Bacteria must be dechlonnated(0.5I 4,c t ,_ rU CN., U Transfer Relinquished By: ppm or less)In the field at the time of collection. See reverse for Instructions Date/Time Received By: 2. 2,Z Date/Time Temperature when Received °C; f: r Delivered By: Accepted: eje Comments: Received By: Re Dattea eq ested: o Time* TUR AROUND: ti r v"