Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
NCG030130_Monitoring Report_20210830
SHIELD ENGINEERING August 10, 2021 Mr. Ryan Pennington Gastonia Components and Logistics Daimler Trucks North America, LLC 1400 Tulip Drive Gastonia, NC 28052 Subject: Stormwater Sampling — July 2021 NPDES General Permit No. NCGO30000 - CoC No. NCGO30130 Daimler Trucks, Gastonia Components and Logistics, LLC 1400 Tulip Drive Gastonia, North Carolina Shield Project No. 1140099-09 Dear Mr. Pennington: Shield Engineering, Inc. (Shield) successfully collected the 3' Quarter 2021 stormwater samples for Stormwater Discharge Outfall (SDO) #001 at the Daimler Trucks Gastonia facility during the month of July 2021. During the July 8t6 sampling event, Shield's measurement for pH was 8.00 at SDO #001. Some foam was observed in the stormwater discharge at SDO #001 on July 81. The Qualitative Monitoring Report and a partially completed Discharge Monitoring Report (DMR) form are attached to this cover letter. In addition, the analytical results for the stormwater samples collected during the qualifying storm events are attached to this cover letter. Results from the July 81 sampling event show an exceedance of Copper at SDO #001. The rain event on July 8th did not produce enough rain in order to collect the stormwater samples for Stormwater Discharge Outfalls (SDO) #002 & #003. Shield will continue to monitor daily weather conditions and continue coordination of appropriate staff and resources to collect stormwater samples at these outfalls, for the 3'" quarter 2021 (July — September 2021). Shield greatly appreciates the opportunity to provide environmental services to Daimler Trucks of North America. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIE EN INEERING, INC. Magdaline Tzannis Senior Project Manager Melinda M. Greene, EIT Senior Engineer Robert L. Griffin, PE President/CEO Attachments: Stormwater DMR, Qualitative Monitoring Report, Analytical Results 4301 Taggart Creek Road www.shieldenglneering.com Telephone 704.394.6913 Charlotte, NC 28208 License No. F-0856 NCOEQ Division of Energy, Mineral and Land Resources AUG 3 0 2021 Stormwater Discharge Monitoring Report (DMR) Form for NCG030000 Metal Fabrication Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permh iota MPnitorinR Report fDMRI Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Reeional Olfice Certificate of Coverage No. N0303 0130 Person Collecting Samples: TJ Gladden Facility Name: Daimler Trucks - Gastonia Laboratory Name: Pace Analytical Facility County: Gaston Laboratory Cert. No.: 329 Discharge during this period; + Yes No (7f no, skip to signature and date) Has your facility Implemented mandatory Tier response actions this sample Period for any benchmark exceedances7 Yes + No If so, which Tier (I, 11, or III)? A copy of this DMR has been uploaded electronically via httasl/edocs deo.nc,aw/Forms/SW-DMR Ld Yes 12 No Date Uploaded: 8 aG aDa- Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in fno,it Parameter Code Parameter Outfall 001 Outfa11002 Outfall 003 Outfall Outfall N/A Receiving Stream Class C C C N/A Date Sample Collected MM/DD/YYYY 07/08/2021 No Flow No Flow 46529 24-Hour Rainfall in Inches 0.23 C0530 TSS In mg/L (100 w So*) 31 00400 PH in standard units (6.0 — 9.0 FIN, 8.0 6.8-8.5 SW) 01119 Copper, total recoverable in mg/L 0.010 FIN, 0.0058 SW) 0.016 01051 Lead, total recoverable In mg/ L 0.07S FIN, 0.22 S 0.0011 01094 Zinc, total recoverable in mg/ L (0.126 FIN, 0.095 SIN) 0.0046 00340 Chemical Oxygen Demand (COD) in m L(120) 45 00552 r Non -Polar Oil &Grease in mg/L(15) s5.o Outtalk to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) haves benchmark TS5 limit of 50 mg/L. All other water classlficadom have a benchmark of 100 mg/L FIN (Freshwater) SIN (Saltwater) Notes (optional): Benchmark exceedance for Copper (Outfall Dail. "I certify by my signature below, under penalty of law, thatthis document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based an my Inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Informyn, including the possibility of fines and Imprisonment for knowing violations." of Permittee or Delegated Authorized Individual scott.sabatini@daimier.com Email Address 210 2 Date 704-868-5760 Phone Number Z^ E'nvfronmCental Quality 411, t � Stormwater Discharge Outfall (SDO) 19 <� O�� Qualitative Monitoring Report For guidance on filling out thisform, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resoui2es/ nudes-stomiwater-gps Permit No.: N/C/ / / / / / / /1, or Certificate of Coverage No.: N/C/G/ Facility Name: Va,"mike - 6466M.f,, County: 6-25 kit Phone No. Inspector: Date of Inspection: ima l Time of Inspection: UT 00 Total Event Precipitation (inches): 0. 23 ;L4, All permits require qualitative monitoring to be performed during a "measurable storm event." I A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the penmittee obtains approval from the local DEMLR LRegional office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Pemtittee or Designee) 1. Outfall Description: Outfall No. 601 Structure (pipe, ditch, etc.): PiiEs Receiving Stream: Describe the industrial activities that occur within the outtall drainage area: Page] of 2 SWU-242. Last mudificd 06 01rOI8 2. Color: Describe the color of the c�arge using basic colors (red, brown, blue, etc.) and tint _ (light, medium, dark) as descriptors: Ar f#* R 3. Odor: Describe ny distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): a 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (?� 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 6 �7 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. 8. 9. Is there any foam in the stormwater discharge? )P Yes Q No. Is there an oil sheen in the stormwater discharge? QYes #No. Is there evidence of erosion or deposition at the outfall? Q Yes A(No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-342. Last modified 00-01/2018 (� aceAnalytical" Report of Analysis Shield Engineering 4301 Taggart Creek Road Charlotte, NC 28208--5483 Attention: Melinda Greene Project Name: Daimler Gastonia SW Lot Number:WG09056 Date Completed:08/06/2021 H'9'h/ X 08/09/2021 4:23 PM Approved and released by: Project Manager I: Hannah K. Lucas The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel 803-791-9700 Fax:803-791-9111 www.parelabs.com Page I of20 PACE ANALYTICAL SERVICES, LLC SC DHEC No. 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Shield Engineering Lot Number: WG09066 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Pace Analytical Services, LLC (formerly Shealy Envimnmetal Services, Ina) 106 vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 20 PACE ANALYTICAL SERVICES, LLC Sample Summary Shield Engineering Lot Number: WG09066 Project Name: Daimler Gastonia SW Project Number: Sample Number Sample ID Matrix Date Sampled Date Received 001 SDO-001 Aqueous 07/08/20210940 07/09/2021 (1 sample) Pace Analytical Services. LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 20 PACE ANALYTICAL SERVICES, LLC Detection Summary Shield Engineering Lot Number: WG09066 Project Name: Daimler Gastonia SW Project Number: Sample Sample ID Matrix Parameter Method Result Q Units Page 001 SDO-001 Aqueous COD SM 5220D- 45 mg/L 5 001 SDO-001 Aqueous TSS SM 254013- 31 mg/L 5 001 SDO-001 Aqueous Copper 200.8 16 ug/L 6 001 SDO-001 Aqueous Lead 200.8 1.1 ug/L 6 001 SDO-001 Aqueous Zinc 200.8 4.6 J ug/L 6 (5 detections) Pare Analytical Services, LLC (lorme►iy Shealy Envlronmentel Servkes, Inc.) 108 Vantage Point Drive West Columbla, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 20 Inorganic non-metals Client:Shield Engineering Laboratory ID:WG09056-001 Description: SDO-001 Matrix: Aqueous Date Sampled:07/08/2021 0940 Project Name: Daimler Gastonia SW Date Received:0710912021 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 (COD) SM 522OD-2011 1 07/16/2021 1501 DAK 99065 1 (TSS) SM 254OD-2011 1 07/14/2021 1725 MOM 98866 1 (SGT - HEM (n) 1664B 1 07/16/2021 1100 SAF 99101 CAS Analytical Parameter Number Method Result Q LOO DL Units Run COD SM 5220D-2011 45 20 20 mg1L 2 TSS SM 264OD-2011 31 7.1 1.0 mg1L 1 SGT - HEM (non -polar material) 1664E ND 5.0 1.6 mg/L 1 LOQ = Limit of Quantitation 8 = Detected in the method blank E = Quantitabon of compound exceeded the calibration range DL = Detection Limit Q = Sumvgate failure ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and a DL L = LCSILCSD failure H = Out of holding time W = Reported on wet weight basis S = MSIMSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.paosiabs.com Page 5 of 20 ICP-MS Client:Shield Engineering Laboratory ID: WG09056-001 Description: SDO-001 Matrix: Aqueous Date Sampled:07/08/2021 0940 Project Name: Daimler Gastonia SW Date Received:0710912021 Project Number. Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 08/06/2021 0929 BNW 07/12/2021 1129 98525 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Copper 7440-50-8 200.8 16 5.0 1.3 ug/L 1 Lead 7439-92-1 200.8 1.1 1.0 0.25 ug/L 1 Zinc 7440-66-6 200.8 4.6 J 10 2.5 ug/L 1 LOCI = Umtt of Quantitation 8 = Detected in the method blank E = Qusa tation of compound exceeded the calibration range DL = Detection Limit 0 = Surrogate failure ND = Not detected at or above the DL N = Recovery is out of criteria Pa The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL L = LCSA.CSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure Pace Analytical Services, LLC (formerly Shealy Enufronmentat Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacolabs.com Page 6 of 20 OZ3o L 099d woo-squisoud-mmm W6-W (Ea8) xed 0016-W (s08) ELM OS'Grgwnloo lsGM GnPp;ulod GBlRuen SU 990609M :aegwnN 401 ao; Lne0 Ob tcul 'saapuGS leluGwuwlnu3 AI8,DYS AIJDuuOJ) 011 'sw'/uGS IB*AAigud Goad A.jewwnS ot) OZ3o 8 098d woo'sgelooud*mmm M6-WL (£08) xuri 00M-WL (£OS) ZL16Z oS'etgwnjoo;seM snua;ulod 069JUDA 904 8g060JM :legwnN iol col e3ea ab {out 'seo�ueS le�ueeuua�nu3 �lesilS �tpaewa1) 011 'SWIJUaS WJ.4A{gW Good s:qnsai po;elnolea ul siane };o-punoi ploAe o; Bulpunoi elo;eq peuuojiod eie suopelnolso :o;oN ePGIP w MO si ada = + evew w Mo el asa =. Gov speem suwnp* ae OAR use#4eq oda 811 = d la < PuB oo-i > unsw powwgs3 = r uwn uop oisa = la UPOUD to MO sl kGAODeb = N la eu3 enoge Jo is PeMep ION = ON uoitemuenD o uwn = Doi 9ZLL =Z/K/10 TBW 0• I 0• L l aN SSl a;ea slsl(leud smun T3 001 Ila b ;Insaa Ja;eweaed L M-aOv9Z WS :Po43eIN le*RAIBUV 99886:4aies snoonby :xlj;eW LOO-99886bM :al eldweS 8W - SIegaw-uou Diue6joul Inorganic non-metals - LCS Sample ID: WQ98866-002 Matrix: Aqueous Batch: 98866 Analytical Method: SM 254OD-2011 Spike Amount Result %Roe Parameter (mg/L.) (mg L) Q Oil % Roe Limit Analysis Date TSS 250 250 1 98 90-110 07/14120211725 LOQ = Umii of Quantitabon ND = Not detected at or above the DL N = Recovery Is out of criteria DL = Detection Umlt J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40% • = RSD is out of criteria + = RPD Is out of criteria Note: Calculations are performed before rounding to avoid round -off errors In calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number. WG09056 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 9 of 20 ozio 01 220d woo•sgejeoed*mmm b LL6-66L (£09) xeq OM-66L (£08) U.&W OS 'ejgwnjoo }soM anus sul d 9OKUBn SOS 99060SM :jegwnN 101 Jo; IMea 00 ('aul `660WaS lWustuuOJlnu3 AleayS Apeuuol) 0l'1 'seojnueS jeopAjeuy aped s;lnsai pe}elnoleo ul sioaae.4o-puna pEoae 01 Buipunoi ejo;oq pewlojjed eie suopelnoleo MON elretuo;o;no s! Oda = + epe11MA MO si 0SU =. %04F OPaeoxe suutnjoo OCJ avq uaeAqeq 0dH e41 = d l0 7 Pue bOl >;lnsiu Petewpa = P mwn uopmoQ = l0 Bpe34O;0 MO si tienooea = N 10 GtH anage Jo M Peep;oN = ON ummusnp !o 3l n = idol 0091,l,zoz19I,1co -I/sw oz oz i GN a00 e;ea slsAleud s;lun Ia 001 lla b 3lnsea Je;ewiued I, M-aozz9 wS :potRew leopAeud 99066:401e8 snoonby :xla;ew LOo-99066OM :al eldweS aw - SILW48 w-uou DIue6aoul OZ3o II 092d woo-sgolsoed-mmm t L W-W (£09) xsd OM-WL (£08) W6Z 0S 'elgwnjoo;soM eApa iuiod GBRUBA 90L 99G60JM :JegwnN ;o-1 Jol Re0 �D t0ul 'Se*WGS leiuewuoJInu31489 lS AP&UUQW 011 'MINES fMPAfewd easd s;lnsoj po;elnolea ul sioJJo go -puns Alone o; BulpunoJ ejo;oq peuuojied eJe suopeinole0 :e;oN OPOMm to ino s! (3da = + WOW* p 00 st asa = . %0q MGM suwnloa 00 ON uesMieq QdH 041= d la < Pue DOl > ilnsw peiewgsa : r ilwn uop*eioo = l0 epeiva Jo M 91 AsAMN = N la GtA enog8lo ie Pe)MeP ION = (IN uopuMueno jo uw!l = OOl O09 L LZOM MO 50 L-96 90 L L Zt 017 DOO O;eQ Sls/tleuv MWI7 DON % 110 D MAW) .. (-116w) Je;eWeJed oeay, Mnsea ;unowV eXIdS L LOZ-QOZZ9 WS :p04;OW ImP eUV 99066:40;e9 snoonbV :xp;ew ZOO-990660M :al eldweS SO'1- SIMGW-uou 01ueG.Ioul Inorganic non-metals - MS Sample ID: WG09056-001MS Matrix: Aqueous Batch: 99065 Analytical Method: SM 522OD-2011 Sample Spike Amount Amount Result %Rec Parameter (mg/L) (mg/L) (mg/L) a DII % Rec Limit Analysis Date COD 45 40 84 1 99 90-110 07/16/20211502 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery Is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40% ' = RSD Is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors In calculated results Passe Analytical Services, LLC (fonnedy Shealy Env►mnmental Services, Inc.) QC Data for Lot Number: WG09056 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 12 of 20 Inorganic non-metals - MSD Sample ID: WG09056-001 MD Batch: 99065 Analvtical Method: SM 522OD-2011 Matrix: Aqueous Sample Spike Amount Amount Result %Roe % RPD Parameter (mglL) (mg/L) (mg/L) Q Dil % Roe % RPD Limit Limit Analysis Date COD 45 40 84 1 98 0.39 90-110 20 07/16/20211503 LOQ = Limn of Quantitation ND = Not detected at or above the DL N = Recovery Is out of criteria DL = Detection Limit J = Estimated result < LOCI and > DL P = The RPD between two GC columns exceeds 40% • = RSD is out of criteria + = RPD Is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number. WG09056 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.paoelabs.com Page 13 of 20 Inorganic non-metals - MB Sample ID: WQ99101-001 Matrix: Aqueous Batch: 99101 Analytical Method: 1664E Parameter Result Q DII LOQ DL Units Analysis Date SGT - HEM (non -polar material) ND 1 5.0 1.4 mg/L 07/16/2021 1100 LOQ = Limit of Quentltation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC oolumns exceeds 40% = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc) QC Data for Lot Number: WG09056 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 14 of 20 OZ3o SI a9ed woo•sgeieaed•mmm L LL6-L6L (£08) xed 00L6-L6L (£09) UM OS letqumioo;soM snap sutod e663ueA 90L 99060JM :JegwnN 401 Joj %VC) 00 (oui 'seowes towerumou3 xiesys Apeuuoo o-n 'seowas imtAleuy owed s;lnseJ pewinalea ul sJoJJe j;o-punoJ P1oAe o; BulpunoJ eJojeq peuuopod one suopelnolec) :e;oN 9901PO jo MO SI adH a + euello m Zno sl asa =. %0b sPmxe suumtoo 00 ONq ueernleq adH e1U. = d la < Pue OOl > jInsw Pel wpq = P win uogoowa =1a eusllp p ino el kQAOMJ = N to etg enOge so Ze PelOeZep ION = aN uoplaueno ►o pwil = t>01 00 L L =Z/9WO Z£ L" Z6 L 8 L OZ (Japo)ew jelod-uou) W3H -1JS e;ea slsAleuV i1WIl oea % 110 D (-UBW) M/Bw) Je;eWeJed oeb% ;Inset ;unowV e)lldS St►M :PO4;9W Igoli FuV W M :4o;e8 snoenby :x1J;eW Z00-M660M :pI eldweS so-1 - sle;aw-uou oiuefiaoul ICP-MS - MB Sample ID: WQ98525-001 Matrix: Aqueous Batch: 98625 Prop Method: 200.2 Analytical Method: 200.8 Prep Date: 07/12/2021 1129 Parameter Result Q Dil LOQ DL Units Analysis Data Copper ND 1 5.0 1.3 ug/L 07/30/20211801 Lead ND 1 1.0 0.25 ug/L 08/06/20210010 Zinc ND 1 10 2.5 ug/L 07/30/20211801 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery Is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40% • = RSD Is out of criteria + = RPD Is out of criteria Note: Calculations are performed before rounding to avoid round -off errors In calculated results Pace Analytical Services, LLC (fonnedy Shealy Environmental Services, Inc) QC Data for Lot Number: WG09056 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 16 of 20 ICP-MS - LCS Sample ID: WQ98525-002 Matrix: Aqueous Batch: 98525 Prep Method: 200.2 Analytical Method: 200.8 Prep Date: 07/12/2021 1129 Spike Amount Result %Roe Parameter (ug/L) (ug/L) Q Dil % Roe Limit Analysis Date Copper 100 110 1 112 85-115 07/30/20211808 Lead 100 94 1 94 85-115 08/06/20210017 Zinc 100 94 1 94 85-115 07/30120211808 LOQ = Limn of Quantltation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40% = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number. WG09056 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 17 of 20 OZ3o 8i *Bud wowsquisood,mmm I I W-M (£09) xBd OOLS-M (£08) ELM OS 'Blgwnloo 19BM anus 3u4od GBMUVA SO& (Ou! `SGOWOS IB;uac OVIAu3 AjBGgS APauuOJ) 0-11 '960INGS 180.019uV Bald sluawnooa snoeuellaosiW pue Apoisno jo weyt) if OZ3o 61 afed woo-squieovd-mmm L L L6-L6L (£08) Xvd OOL6-W (£08) ZLL6Z OS 'e;gwnloO;saM GAM MOd GBEuen m ('aul 'SODWOS MuecuucuuAu3 AjeeyS APGuual) 011 '9001AIGS 1800Isuy GOud rip 0"11 S331AM3S IVOLLAWMV 3Odd PACE ANALYTICAL SERVICES, LLC IW Mwelpt Chmcldlst 15� (M 13) A� Issuing Autitaritp: Pace ENV - WCOL Sample Receipt C6eekibt (SRG) Cliqu: SItIT,i.t� Ctiolcr llfipe+cEDd ldate: JSM 10111t391 MI Lot . WCQ9Cs5 1MCM Of recelut tot l Phar I-1C`liPint I—i Y c..ar EYes ffifiid, �'E:to seals ont%coat+sr?Yes ifcuwseals wens VwMat. arar+e ft intact and unbroka:n? • mzrtia � Strip ID. . Chlorine Strip [D: H► _ 1lesied �' ttntzw Drwwlwe apetaeure upon receipt! Vwiwsd (Corrected) fWhPcrattu�a upotii Mmipt %Solid Snap -Cup ID: NA 1.0 . aC. NA /NA aC NA /NA CC i+lA N,l aC Vlediod: ©Taap mtwe Dltitink 'iginst Boltks iR Gun ID: S iR Curti Cwcction rawotr: 0 'C Method of stool t- N w [� an . et Sw lee RICKS 16 D lae None [] Yes ❑ No QNA 3. If tempareture of'atsy cooler w=cded &OOC, was ProjoCt Ma:tia Mori f ed? PM was Notified by: phone 1 entail / face-too-fhce (Circle one). v Irio A 4. b the cart timmeraiai amdar a pawns SAP attached to this form? 21 Yes UNQ S. Were opar cusped rorcxittr+cs (relittquiahtxGreoeived folbtvcd? Yes AI G, Wesv Sara Ic JIM listed on the COC. Yes Na V. Ware sample IN listed on all sans fe oontainars? EYMOS No R Wn collection dare & lime iisW on the f:OC? No 9. Woe collection date & time lig d on all satrt is contahms? Yes No 10. Did ap container Jabal information (ID, date, trine) age ,veil~ the (X IC? Yea No t 1. Were trsts to be perfomrad listed on the COfCr m Yes ❑ Wn 12. Did all samples:hive in the proper co staineh fnr each test midlor In good condition {unbrolun, :ids on. etc.)? Yes No 13. Was uafe Sam Iss volwma avallabic? Yes 9a lei. Were all Sam Ira mceived within :4 the hown time or 48 hours, whkhever comes first? Yea N 1S. Mere seat lee mitacittg%xcess(citalo onc) a nWas Not listed on COC? ❑Yeg N ©NA IG. ror VOA and RSK-175 samples, were lwbbl= present>"pea sbe, CI-0r bmm in diamete to of *e VOA vials? Yes td A 17. Werc all I Ulistetalshtitttrfwt sate cs received at a H of { 27 Ye t8. Wcre all samples receivaf at s eH > 12 and sulfide lrs racelved at a H > g:► ❑Yes ❑ No MNA : _ m all _ applicable a esto as. .3 { .Sm smnp ea me o ❑ Yes El -No ONA 20. Wem client remarks4 quesm (i.e. Nested dltuuons, .MWMSO designations. cotywly transctibed fivm the COC into the cmn)nent Mcdon in UMS? Yes 1. Was the ualc number listed on the container label? If M Quote # IM 'ample Preservadan (Must be OMP1et9d forany ssmpk(s) inavrecW p umved er with headspare.) ;ample($) MA were rtisaeived Incormaly preserved and were adjuaW acc,+otdil n sample reining with NA of circle one: ti7StJ4, iil�i43, HCI, NaOH using $R # MA l? 'p tiun NA If mote ihan ane FreSMative is needed, picas not in tk comments below. lample(s) NA were raccivcd with bub las>6 min la diamotcr. uunlleg-S) 'M _ were rcaeivcd with TKC > O.s avi. (If m is no) and were idjusted ecowdingly in sample receiving with sodium thlosutfste (ma.s2 3) with Shealy 1D: ImA Rk batrode labels applied 4-: JSM Qata 47t camn.f a . Pace Analytical Services, LLC (formedy Shealy Enwftnmental Services, Inc.) 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.paoelabs.com Page 1 of 1 • Page 20 of 20