WQ0018087_Monitoring - 01-2022_20220420

DA IC A ran er cots
January 19, 2022
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
Subject: Permit No. WQ001087
Cape Fear Manufacturing Facility
Surface Disposal of Class B Residuals (Dedicated)
Brunswick County
Dear Division of Water Resources:
Enclosed please find:
1. Two copies of Compliance and Monitoring Form (GW-59) for the 6 wells
associated with the Sludge Disposal Unit.
2. Laboratory analysis for these same wells.
3. Compliance Report Form GW-59a
4. Summary of the Groundwater Monitoring Results
As shown in the summary, some of the results in the monitoring wells are above the
permit limits. However, these results remain consistent with previous results and most
results show decreases in concentration. The regional office has received this data.
No additional actions are planned at this time.
If additional information is needed, please feel free to contact either myself on 910-371-
5232 or Larry Young on 910-264-2564.
Sincerely yours,
P. . (7 /7_
Penny C. Mahoney
Sustainability Director
DAK Americas LLC
DAK Americas LLC • 1205 Culbreth Drive, Suite 100 • Wilmington, NC 28405
910-371-4863(Phone) • 910-371-4456(Fax)
www.dakamericas.com

GW-59A COMPLIANCE REPORT FORA/ Permit# i(1900/zoo
(Submit one each monitoring period with GlV-59 forms.)
j Enter date monitoring results were due. V/3//.22) Will this monitoring report(GW-59 and GW-59A) YES NO
be submitted after the established due date?
2 Was any required information missing on the GW-59 report forms? YES N
IF the answer to question I or 2 is"YES", list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3 Arc any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?If the answer is "Yes",contact the Regional Office for guidance. /
4 Are any monitored constituents equal to or above the established standards? 1E, NO
If the answer to question 4 is"NO, skip to section 8.
If the answer to question 4 is"YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below: „5
exceeding �€ .7_ -eD, *,,f(
5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES ,NO
same constituent(s) in the same well(s) in the last two years? l✓/
If the answer to question 5 is"NO", skip to section 8.
If the answer to question 5 is"YES", list in the space provided below, each well with constituent(s)exceeding
standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years).
-,e e 49 �C c-fc.,,,,,,
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES- NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL I/
OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is "NO",monitoring wells may be improperly
located;contact the Regional Office.
/J G � 4 I.s 4.., J. ."I C G?ti./ Í Gti
L" j C
7 Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem? '
,
U
If the answer to question 7 is"YES", describe those actions in the space provided below.
If the answer to question 7 is"NO", contact the Regional Office within 90 days;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines,and/or penalties.
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby ack owledge that the above information was evaluated and the information submitted in this
report(Cp lance i3e órt GW-59A) is true and complete to the best of my knowledge.
/� `! ,,./ » ,, ,. /,..„, / /
°' Sin re of Permittee or Aut o iz /g atii ( h n ed'A ént) Date
J
i
GWV-59 1 12/8/2003

Permit MW-2A M W-2B MW-2C
Parameter Limit Units Dec-16 Dec-19 Dec-21 Dec-16 12/16 Rspl Jun-17 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21 Dec-16 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21
Ammonia Nitrogen 1.5 mg/I 12.0 82.5 83.5 47.9 84.3 37.9 53.5 32.9 18.0
Total Dissolved Solids 500 mg/I 827 509 632 673 727 800 692 753 588 597 568 504 744
Nitrate 10 mg/I 14.3 10.8 21.2 15.5
Arsenic 0.01 mg/I 0.017 0.02 0.02 0.02
Cobalt' 0.001 mg/I 0.002 0.022 0.021
pH 5.5
5.13
Permit MW-2D MW-2E
Parameter Limit Units Dec-16 12/16 Rspl Jun-17 Dec-17 Dec-18 Dec-19 Jun-21 Dec-16 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21 Dec-21
Ammonia Nitrogen 1.5 mg/I 157 12.8 96.4 142 80.5 45.8 57.3 9.5 11.0 8.5 5.5 3.3 8.4
Total Dissolved Solids 500 mg/I 678 846 532
Arsenic 0.01 mg/I 0.02
Cobalt' 0.001 mg/I 0.003 0.005 0.004
fi New limit in 2020 permit
V..1-"M028
r - WQ, �.,.0 M - i�
t i' i� .
l ri h
i MW-O2A
; MW-2EÍ••% _ '
Restricted Internal Use

SUBMIT FORM ON YFLLOW PAPER ONLY
Mail original'"EPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
[GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and 1 copy to. 617 MAIL SERVICE CENTER,RALEIGH,NC 27699.1617 Phone:[phone]
FACIL.ITYINFORMATION Please Print Clearly orType PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site 'Non-Discharge UIC
Permit Name(if different): ,NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
I Wilmington "`r`' NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
"`a
te' I ❑ Spray Field ❑Remediation:
'Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor E Land Application of Sludge
'Well Location/Site Name:Down gradient/Monitoring Well#2A No.of wells to be sampled: 6 ❑ Water Source Heat Pump ®Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2A Date sample collected: 12/02/21 FIELD ANALYSES: WAS
!Well Depth: 13.0 ft. Well Diameter: 2.0 in. pH 6.85 units Temp. 19.3 °C DRY at
Depth to Water Level: 7.6 ft. below measuring point Screened Interval: 3.0 ft. to 13.0 ft. Spec. Cond. µMhos time of
sampling,
Measuring Point is 1.92 ft.above land surface Relative M.P. Elevation: 20.39 ft. Odor None check
Volume of water pumped/bailed before sampling: 10 gallons Appearance Clear here:
,Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: kJ YES ❑NO
;LABORATORY INFORMATION
(Date sample analyzed: 12/03/21- 12/08/21 Laboratory Name: Envirochem Certification No. 37729
(PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N <0.02 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0.22 mg/I Zn-Zinc <0.01 m9/I
Coliform: MF Total /100m1 Phosphorus:Total as P <0.04 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 273 mg/I Al-Aluminum mg/I Cobalt-0.002mg/I
pH (when analyzed) 6.8 units Ba-Barium mg/I Selenium -<0.01 mg/I
TOC mg/1 Ca-Calcium mg/I
Chloride 9 mg/1 Cd-Cadmium <0.001 mg/l
Arsenic <0.01 mg/I Chromium:Total <0.01 mg/1
Grease and Oils mg/I Cu-Copper <0.01 mg/I ORGANICS:(by GC, GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I HgMercury <0.0002 m /I Report E Yes ® No
9 - 9 p (1) (0)
Specific Conductance µMhos K-Potassium _ mg/I VOC , method#
Total Ammonia 0.4 mg/I Mg-Magnesium 3.16 mg/I , method#
(Ammonia Nitrogen:NH3as N;Ammonia Nitrogen.Total)
Mn-Manganese mg/1 , method#
TKN as N mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
:Dt(VQ„Ee tithd;aboratory. I am awareahátthere.,areslgnifieantspenaltte,lorsúbmitting false,iinformation including,tbz,,possiblhty,d;fines•an+J.impnsonr lent for hnpwing violations
Penny C. Mahoney Director of Sustainability and Operations Supp A� �: -��6, / /l
Permittee(or Authorized Agent)Name and Title-Please print or type Signattfr9of Permitte ( r Authorized Ag / ;Date)
GW-59 Rev. 1/2007

SUBMIT FORM ON YFLLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original,§EPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
and Copy t0: 'IVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 276 99-1 61 7 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Dr, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick E Lagoon E Remediation: Infiltration Gallery
E Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] E Rotary Distributor E Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2B No. of wells to be sampled: 6 E Water Source Heat Pump ❑?c Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2B Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH units Temp. °C DRY at
Depth to Water Level: 8.7 ft.below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. µMhos time of
sampling,
Measuring Point is 2.9 ft.above land surface Relative M.P. Elevation: 24 ft. Odor check
Volume of water pumped/bailed before sampling: gallons Appearance here: K 1
Samples for metals were collected unfiltered: EYES E NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: Laboratory Name: Certification No.
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total mg/I Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/I
TOC mg/I Ca-Calcium mg/I _
Chloride mg/I Cd-Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC. GC/MS, HPLC)
Phenol mg/I Fe-Iron _ mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance EtMhos K-Potassium mg/I VOC , method#
Total Ammonia mg/I Mg-Magnesium mg/I , method#
(Ammonia Nitrogen:NH3as N:Ammonia Nitrogen,Total) Mn-Manganese mg/1 , method#
TKN as N mg/I Ni-Nickel mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief.the information submitted in this report is true.accurate.and complete.and That the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information.including the possibility of fines and impdaonment for knowing vinrations.
Penny C. Mahoney - Director of Sustainability and Operations Supp ,7. y� // /
777 •
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Perna e-(or A/ori•ed Agent — (Date)
GW-59 Rev.1/2007 /

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original"EPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy to uIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2C No.of wells to be sampled: 6 ❑ Water Source Heat Pump ©Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2C Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH units Temp. °C DRY at
Depth to Water Level: 8.1 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. µMhos time of
sampling,
Measuring Point is 3.05 ft. above land surface Relative M.P. Elevation: 25 ft. Odor check
Volume of water pumped/bailed before sampling: gallons Appearance here: ñ
Samples for metals were collected unfiltered: EYES ❑ NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: Laboratory Name: Certification No.
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P mg/I
(Note Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/I
TOC mg/I Ca-Calcium mg/I
Chloride mg/I Cd-Cadmium mg/I _
Arsenic _ mg/I Chromium:Total mg/I
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC, GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia mg/I Mg-Magnesium mg/I , method#
(Ammonia Nitrogen;NH3as N:Ammonia Nitrogen,Total) Mn-Manganese mg/I , method#
TKN as N mg/I Ni-Nickel mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment( r knowinu violations.
Penny C. Mahoney- Director of Sustainability and Operations Supp ' ... //� - ,_ `1�
Permittee(or Authorized Agent)Name and Title-Please print or type Signature:f ,er ittee(or Authorized Agent) .------ (Date)
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
WI álpia �.-i'1°EPARie^.ENTOFENVIRONMENT&NATURALRESOURCES
GROUNDWATER QUALITY OI I T ORING: 4., r am` !VISION OF UÚATERQUALITY-INFORMATION PROCESSING'UNIT
'.COIfIPLBANCE REPORT FORMIi CO �! l' 617 MAIL SERVICE CENTER,RALEIGHI,NC 27699-1617 Prone:[phone]
sv or Please Pont Clear Type
iFACIL�T Y INFORMATION.. IPERMIT Number:w120018087 Expiration Date: Jan. 31, 2027 h
11Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
¡Permit Name(if different): NPDES NC0000663 Other
.Facility Address: 1430 Commonwealth Drive, Suite 305 (TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon If Remediation:Infiltration Gallery
i Í ❑ Spray Field E Remediation:
I
Contact Person: Larry Young Telephone#: [phone] ElRotary Distributor E Land Application.of Sludge
Well Location/Site Name:Down gradient/Monitoring Well i 2D No.of wells to be sampled: 6 ❑ Water Source Heat Pump ®Other:Surface Disposal Res.Sol`�
hori Permit I
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2D Date sample collected: 12/02/21 FIELD ANALYSES: WAS
¡Well Depth: 13 ft. Well Diameter: 2.0 in. pH units Temp. °C DRY at
time of
!Depth to Water Level: 8.2 ft below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. ItMhos sampling,
'Measuring Point is 3.0 ft above land surface Relative M.P.Elevation: 22 ft. Odor check
Volume of water pumped/bailed before sampling: gallons Appearance here:
'Samples for metals were collected unfiltered: EYES E NO and field acidified: E YES E NO
;LABORATORY INFORMATION
,Date sample analyzed: Laboratory Name: Certification No.
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal /100m1 Nitrate(NO3)as Ni mg/I Zn-Zinc mg/I
Coliform:MF Total /100ml Phosphorus:Total as P mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total mg/I Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/1
TOO mg/I Ca-Calcium mg/I
Chloride mg/I Cd-Cadmium mg/I
Arsenic mg/1 Chromium:Total mg/I
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/1 Hg-Mercury mg/I Report Attached? E Yes(1) ® No(0)
Specific Conductance uMhos K-Potassium mg/i VOC , method#
Total Ammonia mg/I Mg-Magnesium mg/I ,method#
(Ammonia Nitrogen:NH,as N:Ammonia Nitrogen,Total)
Mn-Manganese mg/I ,method#
TKN as N mg/I Ni-Nickel mg/l ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
' ,.e. e'.'ofAmy .owl • e'l ` beU t.`r ."!*.k Mo m,11, ,o1,->4e W,:aa Ztlral.;p (1k-a)•t-cIiii `,bói:0 A..(fat..eI.,data ás: o red • : 4d aliód. ofáña1, 1, atay l' _.. ,' jV
1' °' Sri 4t '" át�M. `re,a 1 � "v.n +t n ,,,.' .,,,r, ��,,�++ 3- w e aL + k, rA s r: ��, �r�w „ kü� 0,SE !!
ire -a t-• - •nr� -rta�avlar.�ha eLe•ar6:§t•'�S r.�l sly._aloes A� ,rg - .- -.• �i�+ttAllt����t�é� .�Slbl it ofpes�rJmpns.4t. •�i1fo��r��f�atión: �>~•. •:I,,�M��. ���. �4,,,, „ `v1�.
Penny C. Mahoney-Director of Sustainability and Operations Supp /�je� ,�a`� ,/j�Q // j /7-'� O -z «�-
Pennittee(or Authorized Agent)Name and Title-Please print or type Signature of , ii ee Co horized Agent) r (Re.')
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
( Mail original..EPARTMENTOF ENVIRONMENT&NATURAL RESOURCES •
GROUNDWATER QUALITY MONITORING: and 1 cop"to: 'MSION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone] l{
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0 0 1 8 0 8 7 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC. Cape Fear Site Non-Discharge UIC
I,
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
(State) (Zip)
❑ Spray Field ❑Remediation:
Contact Person: Larry Young _ Telephone#: [phone] E Rotary Distributor ❑Land Application of Sludge
iWell Location/Site Name:Down gradient/Monitoring Well#2E No.of wells to be sampled: 6 E Water Source Heat Pump other:Surface Disposal Res.Sol
!from Permit)
SAMPLING INFORMATION If WELL
!WELL ID NUMBER(from Permit): MW#2E Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH 6.05 units Temp. 18.2 °C DRY at
,Depth to Water Level: 7.9 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 3•0 ft. above land surface Relative M.P. Elevation: 23 ft. Odor None check
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ®YES ❑NO
(LABORATORY INFORMATION
Date sample analyzed: 12/03/21 - 12/08/21 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
I COD _ mg/I Nitrite(NO2)as N 0.07 mg/I Pb-Lead <0.01 mg/I
1 Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0•24 mg/I Zn-Zinc <0.01 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P <0.04 mg/I
t (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 92 mg/I Al-Aluminum mg/I Cobalt-0.004 mg/I
pH(when analyzed) 6.6 units Ba-Barium mg/I Selenium -<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride _ 6 mg/l Cd-Cadmium <0.001 mg/I
Arsenic <0.01 mg/l Chromium:Total <0.01 mg/I
i Grease and Oils mg/I Cu-Copper <0.01 mg/I ORGANICS:(by GC,GC/MS, HPLC)
I Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
I Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) Id No(0)
1 Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 8.4 mg/I Mg-Magnesium 1.27 mg/I , method#
(Ammonia Nitrogen;NHuas N;Ammonia Nitrogen,Total) Mn-Manganese mg/I ,method#
TKN as N mg/I Ni-Nickel <0.01 mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: _ _mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knovaledge and belief,the information submitted in this report is true,accurate,and complete.and that the laborstrry analytical d.ia was produced using approved methods of analysis by a
DW -cérfi ied laborator cba aware that there,are,si nifica t, enaltiesforsubmittin :falsemformation-.jincludin .the possihility.of.fines-a,td im_risonme.nf:¿or.knowing:violatio.ris. - ..: '
Penny C. Mahoney- Director of Sustainability and Operations Supp , / / / /r.�,2
Permittee(or Authorized Agent)Name and Title-Please print or type Signature ermittee•or•utitorized Agen • • ' (Pate)
GW-59 Rev. 1/2007

SUBMIT FORM ON YFLLOW PAPER ONLY
Mail original EPARTIVIENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy to:1.IVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORS 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Pent Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site I Non-Discharge UIC
Permit Name(if different): iINPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
i
Wilmington NC 28403 County Brunswick Í ❑ Lagoon ❑Remediation: Infiltration Gallery
(State) (Z.p)
E Spray Field E Remediation:
Contact Person: Larry Young Telephone#: [phone] I ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Background/Monitoring Well#3A No.of wells to be sampled: 6 ¡ ❑ Water Source Heat Pump lI Other:Surface Disposal Res.SoI
(frem Permit) j
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#3A Date sample collected: 12/02/21 FIELD ANALYSES: WAS
Well Depth: 13.25 ft. Well Diameter: 2.0 in. pH 5.95 units Temp. 17.9 °C DRY at
Depth to Water Level: 5.7 ft. below measuring point Screened Interval: 3.25 ft. to 13.3 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 1.76 ft.above land surface Relative M.P. Elevation: 24.78 ft. Odor None check i
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: EI YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: 12/03/21 - 12/08/21 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N 0.03 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0.04 mg/I Zn-Zinc 0.015 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P <0.04 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 107 mg/I Al-Aluminum mg/I Cobalt-<0.001 mg/I
pH(when analyzed) 6.2 units Ba-Barium mg/I Selenium -<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride 7 mg/I Cd-Cadmium <0.001 mg/1
Arsenic <0.01 mg/I Chromium:Total <0.01 mg/I
Grease and Oils mg/I Cu-Copper 0.010 mg/I ORGANICS:(by GC,GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 0.2 mg/I Mg-Magnesium 1.00 mg/I , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn-Manganese _ mg/I , method#
TKN as N mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge,and belief,.the information submitted in this report s'true accurate and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ ce t ed;taboratory. :.l am;aware thatHere;,are;;significant pe.nalties,for,submittibgfalse injoytnation,including the.possibility et fines apd,irlprisonment for knowing violations. .
C. MahoneyDirector of Sustainabilityand Operations Su pp //
- P pp •. % / � / / ��
Permittee(or Authorized Agent)Name and Title-Please print or type , Signature of fr rmittee(or-Authorized Agent ;Date)
GW-59 Rev.1/2007

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ANALYTICAL 8 CONSULTING CHEMISTS info,a'environmentalchemists.com
DAR Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53379 Site: 2A 12/2/2021 11:46 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/.10/2021
Magnesium EPA 200.7,Rev4.4,1994 3.16 mg/L 12/10/2021
Nickel EPA 200.7,Rev 4.4,1994 <0.01 rng/L 12/10/2021
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Zinc EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Arsenic EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L '12/10/2021
Cadmium EPA 200.8,Rev.5.4,1994 <0.001 rng/L 12/08/2021
Mercury EPA 245.1,Rev.3.0,1994 <0.0002 mg/L 12/10/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.4 mg/1 12/08/2021
Total Dissolved Solids(TDS) sM2540 C-2015 273 rng/L 12/03/2021
pH 5M,i 4500 I-I 8-2011 6.8 units 12/07/2021
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 12/09/2021
1,1,1,2-f•etrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,1-Trichloroethane 5M 6200 8-2011 <0.5 pg/L 12/03/2021
1,1,2,2-Tetrachloroethane SNI 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,2-Trichloroethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,1-Dich loroeth an a Srvl 6200 8-2011 <0.5 pg/L '12/03/2021
1,1-Dichloroethene SM6200B-2011 <0.5 pg/L 12/03/2021
1,1-Dichloropropene Sb16200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,3-frichloropropane SLI 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trirnethyl benzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
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ANALYTICAL&CONSULTING CHEMISTS info re environmentalchemists.corn
DAS{Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#l: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC - Cape Fear Manufacturing
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L '12/03/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroben.cene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichioropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/202'1
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L '12/03/2021
1,3-Dich loropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L *12/03/2021
Benzene SM 6200 B-2011 <0.5 pg/L. 12/03/2021
Brornobenzene SPA 6200 B-2011 <0.5 pg/L 12/03/2021
Bromochlorornethane SM 6200 B-2011 <0.5 pg/L '12/03/2021
Bromodichloromethane SPA 6200 B-2011 <0.5 pg/L 12/03/2021
Brornoform SPA 6200 B-2011 <0.5 pg/L '12/03/2021
Brornornethane SPA 6200 B-2011 <0.5 pg/L '12/03/2021
Carbon tetrachloride SNl 6200 B-2011 <0.5 pg/L 12/03/2021
Chlorobenzene sNi 8200 8-2011 <0.5 pg/L 12/03/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L '12/03/2021
Chloroform SM 6200 B-2011 <0,5 pg/L '12/03/2021
Ch lorom e th 7n e SM 6200 B-2011 <0.5 pg/L '12/03/2021
cis-1,2-Dichloroethene SPA 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,3-Dichloropropene SM 6200 B-2011 <0,5 pg/L 12/03/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromomethane SPA 6200 B-2011 <0.5 pg/L 12/03/202'1
DichlorodiPluoromettlanº siv16200 B-2011 <0.5 pg/L 12/03/2021
Ethylbenzene SPA 6200 B-2011 <Q,5 pg/L 12/03/2021
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envirocheni 6602 Windmill Way,Wilmington,NC 28405 C 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 6 252.473.5702 Lab/Fax
sr;)! 255-A Wilmington Highway,Jacksonville,NC 28540 4 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoa environmentalchemists.com
OAR Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC - Cape Fear Manufacturing
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 12/03/2021
lsopropylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
(VI+P Xylene SPA 6200 8-2011 <1,0 pg/L 12/03/2021
Methylene chloride SPA 6200 B-2011 <0.5 pg/L 12/03/2021
Naphthalene SM 6200 8-2011 <0.5 pg/L 12/03/2021
n-Elutylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
ortho-Xylene SM 6200 8-2011 <0.5 pg/L 12/03/2021
p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
sec-Butylbenzene SPA 6200 B-2011 <0.5 pg/L 12/03/2021
Styrene S,M 6200 B-2011 <0.51Jg/L 12/03/2021
tert-Butylbenzene SM 6200 8.2011 <0.5 pg/L 12/03/2021
Tetrachloroethene SM 6200 B-2011 <0.5 iig/L 12/03/2021
Toluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,3-clichloropropene SM 6200 B-2011 <0.5 pg/L '12/03/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L '12/03/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloride SM4500 CI E-2011 9 rng/L '12/03/2021
Nitrate Nitrogen (C11lc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 rng/L 12/02/2021
Nitrate-I-Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.22 rng/L 12/07/2021
Nitrate Nitrogen Subtraction Method 0.22 rng/L 12/.13/2021
Lab It) Sample 1D: Collect Dateflime Matrix Sampled by
21-53379A Site: 2A 12/2/2021 11:46 AM Water Young/Simmons
Test Method Resulta Dote Arialyfed
Cobalt EPA 200.8,Rev.5.4, 1994 0.002 mg/L 12/08/2021
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Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 1tCDl-IHS:DLS CERTIFICATION#37729
COLLECTION AND CHAIN OF CUSTODY
'CLIENT: DAK Americas PROJECT NAME: LLC-Cape Fear Manufacturing REPORT NO:á1— �L h 7
ADDRESS: ;`iJ£„, L�,7ainGil !•J.¿Dil;0/L Dr. CONTACT NAME: /:,G1rru / f.-,�.���` Work Order NO:
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Sampled By: /� ��.�.,7���•�'f,� ��!7;rn.,-�h, SAMPLE TYPE:I=Influent, E=Effluent,�1='�Veli,ST=Stream,SO=Soil,SL=Sludr�e, Other:
" , Collection = , PRESERVATION !
wI v °' óp = co á
Sample IdentificationE ~ aóE _ ó � rn � m � w á � z -
O m
ANALYSIS REQUESTED
co o ó a � m ó Mi á ~ E
Dat, Time Temp u 0 ' " , zJ = = _ �
�� � �
, /\ 1'9. .s/�i �r'•�� � � ` z�...---�,�j�
;
ivlW# �� /"`' . � 3 f�lúJ �Gr G rD, J,_.� � X I � �i�= Chloride, "nitrite, TDS
r, /i;}=e'� i ( C tt�.,� � l..� �,, I i
Depth to Water: J. � i i ! � G � .� 1 � ,•� I Ammonia, Nitrate, TP
, //: S�� ! � C ��� i �' �� I �.D
Gallons Bailed: I � I � r G; G � ¡ s j X ` As.Cd,Cr,Co,Cu.Pb,I:rg,Ni,Se,Zn,'rig
i
� C P � !
pH (field): LG , ,.5... o , G G
s � } 1 i C P + I�?,.;1
ColCr. L Jt�L't(! i � , L •
G yG� � � ( " .' � � X � — VOC's (December Only)
Odor: �!' [j P
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G G 1
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Transfer Relinquished Bv: � Date/Time I Received By: Dateffime
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Temperature when Received 'C: �, � Attie ted�-�� Rected: Resample Restj�.�es.ed: J
Delivered By: /— t-i3` Received By: _ ,.�`��— ��a(�- Date: 1 Time:
Comments: p N- Ptt1i e 1: 7D J�j elu�� Ía cS'. .5 �-f 1 1•.35 1�r►�f7 /y. .5 TURNAROUND:

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ANALYTICAL&CONSULTING CHEMISTS infaaenvironmentalchemists.com
DA}< Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report if: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
Lab ID Sample ID: Collect Dater Time Isilatrix Sampled by
21-53389 Site: 2E 12/2/202'1 12:26 PM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Magnesium EPA 200.7,Rev 4.4, 1994 1.27 mg/L 12/10/202'1
Nickel EPA 200.7,Rev 4.4,1994 <0.0.1 mg/L 12/10/2021
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mglL '12/10/202'I
Zinc EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Arsenic EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/'10/2021
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L '12/10/20211
Cadmium EPA 200.8,Rev.5.4,1994 <0.001 mg/L 12/08/2021
Mercury EPA 245.1,Rev.3.0,1994 <0.0002 mg/L 12/10/2021
Ammonia Nitrogen EPA350.1,Rev.2.0,1993 8.4 mg/L '12/08/2021
Total Dissolved Solids(TOS) SM 2540 C-2015 92 mg/L 12/03/202'1
oil SM 4500 H 8-2011 6.6 units 12/07/2021
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 < 0.04 mg/L '12/09/2021
1,1,1,2-Tetrachloroethane SM 6200 a-2011 <0.5 pg/L 12/03/2021
'I,'1,1-Trichloroethane Sfvl 6200 B-2011 <0.5 pg/L 12/03/202'1
'1,1,2,2-felrachioroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,1,2-Tnichloroethane SM 6200 0-2011 <0.5 l.lg/L 12/03/2021
1,'I-Dichloroethane sM 6200 B-2011 <0.5 pg/L 12/03/2021
1,'I-Dichloroethene SM 6200 B-2011 <0.5 pg/L '12/03/2021
1,1-Dichloropropene Sid 6200 8-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichlorobenzene SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,2,3-Trichloropropane SMv16200 B-2011 <0.5 pg/L '12/03/202'1
1,2,4-Trichlorobenzene Sivi 6200 B-2011 <0.5 pg/L 12/03/2021
1,2,4-Trirnethylbenzene Sivl 6200 B-2011 <0.5 pg/L 12/03/2021

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ANALYTICAL&CONSULTING CHEMISTS info,v-environmentalchemists.com
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report if: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dibromoethane SM 6200 B-2011 <0,5 pg/L 12/03/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,2-Dichloropropane SPA 6200 B-2011 <0.5 pg/L 12/03/2021
1,3,5-Trirnethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichiorobenzene SM 6200 B-2011 <0.5 lag/L 12/03/2021
1,39Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,4-Dichlorobenzene SM 6200 8-2011 <0.5 pglL 12/03/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
2-Chlorotoluene SM 6200 B-2011 <0-5 pg/L 12/03/2021
4-Chlorotoluene ShA6200 B-2011 <0.5 pg/L 12/03/2021
Benzene SM 6200 B-2011 <0.5 pg/L 12/03/202'1
Bromobenzene SPA 6200 B-2011 <0.5 pg/L •12/03/2021
Bra mochlorornelhane SM 6200 B-2011 <0,5 pg/L 12/03/2021
Brornociichiorornethane SM 6200 B-2011 <0.5 pg/L 12/03/202'1
Bromoforrn SM 6200 B-2011 <0.5 pig/ 12/03/2021
Bromomethane SPA 6200 B-2011 <0.5 pglL 12/03/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L '12/03/2021
Chlorobenzene SPA 6200 B-2011 <0.5 pg/L '12/03/2021
Chloroethane SPA 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroform SM 6200 B-2011 <0,5 pg/L 12/03/2021
Chloromethane SM 6200 B-2011 <0.5 pg/L 12/03/202'1
cis-1,2-Dichloroethene sia16200 B-2011 0.5 pg/L 12/03/2021
cis-1,3-Dichloropropane SPA 6200 B-2011 <0.5 pg/L 12/03/202'1
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibrornomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dichforoctifluoromethane SPA 6200 B-2011 <0.5 pg/L 12/03/2021
Ethylbenzene SM 6200 B-2011 <0.5 pcP/L 12/03/2021
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envirochexn 6602 Windmill Way,Wilmington,NC 28405 e 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 0 252.473.5702 Lab/Fax
Sto 255-A Wilmington Highway,Jacksonville,NC 28540 4 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info:?environmentalchemists.com
------------
DAR Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report II: 2021-21307
Attention: Larry Young Customer 1D: 08100044
Project ID: LLC -Cape Fear Manufacturing
F-lexachlorobutadiene Sív16200 B-2011 <0.5 pg/L 12/03/2021
Isopropylben:zene SM 6200 8-2011 <0.5 pg/L 12/03/2021
M-i-P Xylene SM 6200 8-2011 <1.0 pg/L 12/03/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-F3utylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/L -12/03/2021
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 12/03/2021
p-lsopropyltoluene SM 6200 B-2011 <0.5 pg/L 12/03/2021
sec-E3utylbenzene SM 6200 B-2011 <0.5 VIg/L 12/03/2021
Styrene SM 6200 B-2011 <0.5 pg/L 12/03/202.1
tent-Bu tyl benzen e SM 6200 8-2011 <0.5 pg/L 12/03/2021
Tetrachioroethene SM 6200 8-2011 <0.5 pg/L 12/03/202'1
Toluene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Trans-1,2-Dichioroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,3-dichioropropene SM62008.2011 <0.5 pg/L 12/03/2021
Trichioroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
frichiorofluoromethane SM 6200 8-2011 <0.5 pg/L 12/03/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L '12/03/2021
Chloride St•M14500 Cl E-2011 6 mg/L 12/03/202'1
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 0.07 rng/L 12/02/2021
Nitrate-I-Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.31 rng/L 12/07/2021
Nitrate Nitrogen Subtraction Method 0.24i mg/L '12/13/2021
Lab ID Sample ID: Collect i?aterrirno Matrix. Sampled by
21-53389A Site: 2E 12/2/202'1 12:26 PM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5.4, 1994 0.004 mglL '12/08/2021
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ENVIRONMENTAL CLig EMISTS 5 NC 910.392.0223 252.473.5702
[e-mail]
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION 11 94 NCDHHS:OLS CERTIFICATION g 37729
COLLECTION AND CHAIN OF CUSTODY
CLIENT: DAK Americas PROJECT NAME: LLC -Cape Fear Manufacturing REPORT N 0:,--y>i — 2.307
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ADDRESS: ;4,23D L....brnrnon 1.,..)e0 ht-i-Zi(, CONTACT NAME: .1-,-,0-Lrni / •e..2...,' i.; c, Work Order NO:
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REPORT TO: L,4: r r L/ z_,, ,,,,/y,-. 1PHONE/FAX: (9/‘..,),>-:;,f::,- f-,,..',?,j
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email: iy,,,;,,,./5,j_ Ozi.)&L),,27•0_-,.sy'-er- , cf.,.:.7,()
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Sampled By.,(,4/7-7 4/2•,131 /,.-25 SIA-i/nOt) SAMPLE TYPE: I =Influent,E=Effluent,W=Well,ST=Stream,SO zr,Soil,SL=Sludge,Other:
Cotfection ' PRESERVATION
1
Sample identification 2. ,
D 1.1 1 -'21 5 II^ It- 1 ! - ¿ a á 2 i 1
o 0 a- "X _3 M 0
o {-3 ' . 2 i 2 X X I- • o ANALYSIS REQUESTED
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Date Time Temp I 13 ( I
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,...
/TO' ir'''' ) C '2) 1
I
MW# C.:; f-' " -t/ ' /57/G1 P9 i-/' (,f' 1 G .,-.j2ti-k5.33117X -»]-4 Chloride, Nitrite, TDS
6".? 1;91» ,
• • . C I 1...51 -
f I II J Depth to Water: ', 17/ ii ,_ ( C__G) G <H5 I
,.., ....1
1 x I Ammonia, Nitrate, TP
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Gallons Bailed: 4,--, G irio ' I X As,Cd,Cr,Co,Cu,Pb,ivig,Ni,Se,Zn,Hg
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C P
,
pH (field): (2 , 5. 1
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, G G I
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-
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; i \1, 11 fh , - ( ? , (---2.-..---- x j,so
Color: : t.„...:,., '--- / - , •'' .. ....i.„ ,.G,., 1./
C P 1' X
- _ VOC's (December Only)
-
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1 P
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Transfer Relinquished By: -- Date/Time Received By: Date/Time
1. --)., . l,..:4,...--z--,..,-- 42, ) /552/2
2. i ,---47 4 ( \\
r
Temperature whé ived '. ''''--- .ccepted: ,----F . ,ie ...tt..d: Resame/Requested:
Delivered ..., . , Received By: Date: i___ Time:
Comments: - LI- (P i--,L3 , 0_/— ir /Y o2— TURNAROU, D:
0 r

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envirochem 6602 Windmill Way,Wilmington,NC 28405 = 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 e 252.473.5702 Lab/Fax
sm
255-A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
DAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08'100044
Project ID: LLC -Cape Fear Manufacturing
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53390 Site: 3A 12/2/2021 11:11 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 0.0-10 mglL 12/10/2021
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L -12/10/2021
Magnesium EPA 200.7,Rev 4.4, 1994 1,000mg/L 12/10/2021
Nickel EPA 200.7,Rev 4.4,1994 <0.01 mg/L 12/10/2021
Selenium EPA 200.7,Rev 4.4,1994 <0.0'1 mg/L 12/10/2021
Zinc EPA 200.7,Rev 4.4, 1994 0.0'15 mg/L 12/10/2021
Arsenic EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 12/10/2021
Cadmium EPA 200.8,Rev.5,4,1994 <0.001 rng/L 12/08/202'1
Mercury EPA 2451,Rev.3.0,1994 <0.0002 mc1/L '12/10/202'1
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.2 r-ng/L 12/08/202'1
Total Dissolved Solids(TOS) SM 2540 C-2015 107 rng/L 12/03/2021
pH SM 45001-1 8-2011 6.2 units 12/07/2021
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM4500 P(F-H)-201 I < 0.04 mg/L 12/09/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 12/03/202'1
1,1,1 Trichloroethans SM 6200 B-2011 <0,5 pg/L 12/03/2021
'1,1,2,2-Tetrachloroelhane SM 8200 B-2011 <0.5 pg/L '12/03/2021
1,1,2-Trichioroethane SM 6200 B-2011 <0.511g/L 12/03/2021
1,1-Dichloroethane Sib16200 13-20.11 <0.5 pg/L '12/03/2021
'I,1-Dichloroethene Sabi 6200 B-2011 <0.5 pg/L 12/03/2021
1,'I-Dichloropropene SM 6200 B-2011 <0.5 pg/L '12/03/202,1
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.511g/L 12/03/2021
1,2,3-T richloropropane SM 6200 B-2011 <0.5 pg/L '12/03/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 ig/L '12/03/2021
1,2,4-Trirnethylbenzene S1;16200 8-2011 <0.5 pg/L '12/03/2021

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�fá£e't�4,;:,r.•; .� �'�cr 71013owsertown Road,Manteo,NC 27954 0 252.473.5702 Lab/Fax
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tt,CONSULTING CHEMISTS info•:u environmentalchemists.com
OAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
1,2-Dibromo-3-Chloropropane SM 6200 8-2011 <0.5 pg/L 12/03/2021
1,2-Dibromoethane srn 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dich lorobenzen e Sh16200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L •12/03/2021
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
1,3-Dichloropropane Sr,16200 B-2011 <0.5 pg/L '12/03/2021
1,4-Dichlorobenzene sm 6200 B-2011 <0.5 pg/L 12/03/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 12/03/2021
2-Chlorotoluene SM 6200 B-2011 <0,5 pg/L 12/03/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L '12/03/2021
Benzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Bromobenzene Sti16200 B-2011 <0.5 pg/L '12/03/2021
lkornochloromethane Srn6200 8-2011 <0.5 pg/L 12/03/2021
F3rornodichloromethane S1v18200 8-2011 <0.5 pg/L 12/03/2021
13romoforrn SM 6200 B-2011 <0.5 pg/L 12/03/2021
E3romornethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L -12/03/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Chloroform SM 6200 B-2011 <0.5 pc1/L 12/03/2021
Chloror'nsthane SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 12/03/2021
cis-1,3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dibrornomethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Dicñlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 12/03/2021
Ethylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
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envirochem 6602 Windmill Way,Wilmington,NC 28405 0 910.392.0223 Lab 0 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 b 252.473.5702 Lab/Fax
sr 255-A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info+r?environmentalchemists.com
OAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report''#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC-Cape Fear Manufacturing
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 12/03/2021
Isopropylbenzene sM 6200 B-2011 <0.5 pg/L 12/03/2021
M-t-P Xylene SM 6200 8-2011 <1.0 pg/L '12/03/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 12/03/2021
Naphthalene SM 6200 B-2011 <0.51.ig/L 12/03/20211
n-6utylbenzene SM 6200 B-2011 <0.5 pg/L 12/03/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/t. 12/03/2021
ortho-Xylene SM 6200 B-2011 <0.5 pglL 12/03/2021
p-Isopropyltoluene S141 6200 B-2011 <0.5 pglL 12/03/2021
sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 112/03/202'1
Styrene SM 6200 B-2011 <0.5 pglL '12/03/202'1
tort-Butylbenzene SM 6200 B-2011 <0.5 pglL '12/03/202.1
Tetrachloroethene SM 6200 8-2011 <0.5 pg/L 12/03/2021
Toluene SM 8200 B-2011 <0.5 pg/L 12/03/2021
Trans-1,2-Dichloroethene sM 6200 B-2011 <0.5 pu/L 12/03/2021
Trans-1,3-dichloropropene SM 6200 B-2011 <0.5 pg/L -12/03/2021
Trichloroethene Sivl 6200 B-2011 <0.5 pg/L 12/03/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L '12/03/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 12/03/202'1
Chloride Siv14500 CI E-2011 7 mg/L '12/03/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev 2 0.1993 0.03 mg/L 12/02/2021
Nitrate-Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.07 rng/L 12/07/2021
Nitrate Nitrogen Subtraction Method 0.04 mg/L '12/13/2021
Lab ID Semple ID: Collect DEttefTime Matrix 1-.31iiriplr i by
21-53390A Site: 3A '12/2/202.1 11:11 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5.4,1994 <0,001 mg/L '12/08/2021

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ij-; ;I'' '- , `t: # '�a!?I 710 Bo�\�sertown Road,Manteo,NC 27954 252.473.5702 Lab/Fax
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ANALYTICAL£1 CONSULTING CHEMISTS into:irenvironmentaichemists.com
OAK Americas Revised Report: Jan 03, 2022
1205 Culbreth Drive Suite 200 Original Report Date: Dec 13, 2021
Wilmington NC 28405 Report/#: 2021-21307
Attention: Larry Young Customer ID: 08100044
Project ID: LLC -Cape Fear Manufacturing
Comment: Amended 01/03/2022 to amend Cobalt results
Reviewed by: � _`7 ,,,,ZI_,�._.l — -

C.:ToV�«`+"'•3Jy^_}"�ct. � ����� � � INC 990.392.0223 252.�í73.57D2
� ENVIRONMENTAL ���� ;
,/+ in:[e-mail]
Analytical 8 Consulting Chemists NCDENR:MVO CERTIFICATION#94 NCDNIiS:DLS CERTIFICATION#37729
COLLECTION AND CHAIN OF CUSTODY
I— .
'CLIENT: DAK Americas PROJECT NAME: LLC-Cape Fear Manufacturino REPORT NO: �{—óL,.)jQ—
ADDRESS: ' .1
�;�;� .in('r`I 0:! !k%" • 144 �� CONTACT NAME: jt •-,,-,1, , •r..fi - Work Order NO:
�1-1_ r�L-'s REPORT TO: 2,-,-, L./5,. ; ,-i;; i PHONE/FAX: C'i 1�1 -2� `r- %.i G 5` 1
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� 1 • i ;ll'?�1s!i�(t��/� L1L� -�1' L1 J COPYTO: reffinErlIMMINIMIII
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' " Co41•ctian � e o ° � PRESERVATION
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Sample Identification s T I 4o � � á � � m m W ó , � ANALYSIS REQUESTED
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.^'' i A . 1 C .¿: ,:
Gallons Bailed: /,;) i111_ • fir_G - : G As,Cd,Cr,Co,Cu,Pb,iVig,vi,Se,Zn,Hg
MII 11111E1111 P I I I 1
pH (field): r . r ,"_ � � ! 111 111
-; MIEWMA ; C P l � l �:Y�•tf. !
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Color: , (�,: Mall $�;r , I � � � x 1 r t VOC's (December Only)
Odor: ' ` J ��'
�� C P Ell.
'—_�■
G GIi I
� C Pf HNIII
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• r ?a�te/rs;e j Received By: Date/Time
IMP'
1. --X �" �..+- d !�rd;<7 r'S 3 í3C-}
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Temperature wte eceived °C: Z. epted: " Rejected: Resample Reci;s'rsted:
Delivered By:—''`��`' 7�-r - •----- ----_ Received By: �� - Date: ¡�`�`t/D-'t Time:
Comments: �1,` ?c, !(tjt �L`4�� �sr,0:= .�.-; ,/`, :1 ,`r-fr, ,r, , . . ,�, TURNAROUND:

n ..
DWR - NonDischarge Monitoring Report Submittal •4 ..
NORTH CAROLINA
Enrlr...1M Qua(ily
Monitoring Report Submittal
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Permit Number#* WQ0011087
Name of Facility:* DAK Americas LLC
Month:* January Year:* 2022
Report Information
Type* Upload Document*
GW-59 2021 Annual Monitoring Well 5.77MB
Report_04202022.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1,NDAR-2,NDMLR,GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter:* Phyllis H Simmons
Signature:
C9:ilelr }iaTaRTrTd
Date of submittal: 4/20/2022
This will be filled in automatically
Initial Review
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Reviewer: Gerald,Wanda

Is the project number correct?* WQ0011087
Is the monitoring report accepted?* - Yes No
Regional Office* Wilmington
Accepted Date: 5/23/2022