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NC0004375_Permit (Issuance)_20030127
NPDES DOCUMENT SCANNING: COVER SHEET NPDES Permit: NC0004375 Clariant Corporation Document Type: Permit Issuance Wasteload Allocation Authorization to Construct (AtC) Permit Modification Complete File - Historical Engineering Alternatives (EAA) Correspondence Owner Name Change Additional Information Received Instream Assessment (67b) Speculative Limits Environmental Assessment (EA) Document Date: January 27, 2003 This document is printed on reuse paper - ignore any content on the rezrerae side State of North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross, Jr., Secretary Alan W. Klimek, P.E., Director January 27, 2003 Mr. Gary Sanderson Clariant Corporation P.O. Box 669246 Charlotte, North Carolina 28266 WA NCDENR Subject: Issuance of NPDES Permit NC0004375 Mt. Holly East Plant Mecklenburg County Dear Mr. Sanderson: Division personnel have reviewed and approved your application for renewal of the subject permit. Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency dated May 9,1994 (or as subsequently amended.) Clariant Corporation should be aware that the Division will re-evaluate the justification for the entire 3.9 MGD flow requirement upon the next renewal of this permit in 2005. The following modifications from the draft permit previously sent to you have been included in this final permit: • Facility information on the map has been corrected to show the U.S.G.S. Quad # as F14SE and the stream classification as WS-IV CA. • There is a modification in the footnotes of Section A. (6) Effluent Pollutant Scan. Two copies of the test result report, DMR-PPA1, shall be submitted along with the DMR forms to the Division's Central Files. A copy of the form is attached to the permit. These conditions from the draft permit remain in the final permit. • Effluent limitations for BOD and Total Suspended Solids have been modified based on the revision of waste flows used for development of the allocations for OCPSF, non -categorical and centralized waste treatment waste streams. Effluent limitations have been reduced due to a smaller flow (not design capacity) being used for allocation development. The application support document submitted by Clariant describes the allocation process. • Tiered limitations have been placed in the permit. Tier 1 limits are effective for existing wastewater sources. Tier 2 limits become effective when any additional wastewater sources are added. Special condition A. (7) requires that Clariant notify the Division at least fourteen days prior to the addition of any new wastewater sources. • The effluent limitation for NH3 as N has been revised slightly downward to a mass -based limit of 618 pounds/day (monthly average) and 927 pounds/day (daily maximum). In the past, the NH3 limit has been allocated based on secondary treatment of the effluent discharge. 1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617 - TELEPHONE 919-733-5083/FAX 919-733-0719 AN EQUAL OPPORTUNITY AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/ 1 0% POST -CONSUMER PAPER VISIT US ON THE INTERNET @ http://h2o.enr.state.nc.us/NPDES Permit NC0004375 • Monthly monitoring for manganese, sulfates, chlorides, MBAS and iron has been reduced to quarterly monitoring. The reduction was based on the results of reasonable potential analyses that indicated that the relevant NC water quality standards would not be violated by the effluent discharge. A limitation is not required for these parameters but due to the nature of the discharge, effluent monitoring is still required. • Monthly monitoring for chromium and zinc has been added to the permit based on new wastewater streams from Seaboard Container Cleaning and SCR -Tech. • Effluent limitations for total nitrogen and total phosphorus have been added to the permit based on the Catawba River Basin Management Plan for nutrient protection in the Lake Wylie watershed. These are interim limits based on current information from the facility. A nutrient worksheet is attached for recording the monthly average total nitrogen and total phosphorus data to be submitted to DWQ. • A special condition has been added to the permit that will require Clariant to conduct a BAT study for the development of more accurate nutrient limits in 2003. • Mercury continues to be a water quality concern throughout North Carolina. NPDES permittees have worked with the State to reduce potential risks from this pollutant, including tasks associated with collecting and reporting more accurate data. The most commonly used laboratory analysis (EPA Method 245.1) has a detection limit of 0.2 µg/L while the current water quality standard is an order of magnitude lower at 0.012 µg/L. A more recently approved analytical test (EPA Method 1631) should produce a detection limit below the level of the standard. This will allow the Division to assess potential water quality impacts from discharges more accurately. Therefore, beginning on or before September 1. 2003, you will be required to begin using EPA Method 1631 when analyzing for mercury. Please note that mercury shall be measured as a grab sample. • Instream monitoring for BODS and NH3 have been deleted based on review of data, showing no impact on water quality in the Catawba River. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the office of Administrative Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699- 6714. Unless such a demand is made, this permit shall be final and binding. This permit is not transferable. The Division may require modification or revocation and reissuance of the permit. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act, or any other Federal or Local governmental permits may be required. If you have any questions or need additional information, please contact Ms. Jacquelyn Nowell at telephone number (919) 733-5083, extension 512. Sincerely, Avai an W. Klimek, P.E. cc: Mooresville Regional Office/Water Quality Section EPA Region IV/Roosevelt Childress Ned Fiss/Aware Environmental, Inc. (9305 J Monroe Road, Charlotte NC 28270-1490) DEH Aquatic Toxicology Point Source Compliance and Enforcement Unit Central Files NPDES File Permit NC0004375 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY PERMIT TO DISCHARGE WASTEWATER UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Clariant Corporation is hereby authorized to discharge wastewater from a facility located at the Mt. Holly East Facility NC Highway 27 northwest of Charlotte Mecklenburg County to receiving waters designated as the Catawba River in the Catawba River Basin in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV hereof. This permit shall become effective March 1, 2003 This permit and authorization to discharge shall expire at midnight on June 30, 2005. Signed this day January 27, 2003. ?-7an W. Klimek, P.E.,UDirector Division of Water Quality By Authority of the Environmental Management Commission 1 Permit NC0004375' SUPPLEMENT TO PERMIT COVER SHEET Clariant Corporation is hereby authorized to: 1. Continue operation of a 3.9 MGD wastewater treatment plant consisting of the following treatment units: • Two. stormwater equalization basins for non -alkaline wastewater; • Two stormwater equalization basins for alkaline wastewater; • Two acid neutralization tanks; • One lime slurry tank; • Two primary clarifiers; • One wastewater equalization basin; • One aeration basin with mechanical aeration; • Two secondary clarifiers; • Two polishing ponds; • Staged discharge facility including effluent holding basin and post aeration; • Two sludge holding tanks; and • Two sludge dewatering belt presses. This facility is located at the Mt. Holly East facility off NC Highway 27 northwest of Charlotte in Mecklenburg County. 2. Discharge treated OCPSF, centralized waste treatment (CWT) and non -categorical industrial process wastewaters from said facility at the location specified on the attached map through outfall 001 into the Catawba River, classified WS-IV CA waters in the Catawba River Basin. 1 e • t / Pie 121 • • 1: • N V. 4. law 1411— • 4 1 k. 1 -r Facility Information Latitude: Longitude: Quad #: Stream Class: Receiving Stream: Permitted Flow: 35°16'46" Sub -Basin: 81°00'32" Fl4SE WS-1V CA Catawba River 3.9 MGD 03-08-34 Facility Location • • • no ,t4 Clanant Corporation' . NC0004375 Mecklenburg County Permit NC0004375 A. (1) a TIER 1 EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS During the period beginning on the effective date of the permit and lasting until the addition of future wastewater sources or expiration, the Permittee is authorized to discharge treated OCPSF, CWT and non -categorical industrial process wastewater from outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below: EFFLUENT LIMITATIONS MONITORING REQUIREMENTS EFFLUENT CHARACTERISTICS Monthly Average Daily Maximum Measurement Sample Sample Location Frequency Tie Flow 3.9 MGD Continuous Recording Influent or Effluent BOD, 5-day, 20°C4 329.0 pounds/day 810.0 pounds/day Daily Composite Effluent Total Suspended Solids 410.0 pounds/day 1115.0 pounds/day Daily Composite Effluent Dissolved Oxygen Daily Grab Effluent, U' & D' Fecal Coliform (geometric mean) Monthly Grab Effluent pH2 Daily Grab Effluent, Ul & Di NH3 as N4 618.0 pounds/day 927.0 pounds/day Daily Composite Effluent Temperature °C Daily Grab Effluent, U' & D1 Conductivity Daily Grab Effluent, Ul & D' COD Monthly Grab Effluent Total Nitrogen5 (NO2+NO3+TKN) See below for Annual Average Monthly Composite Effluent Total Phosphorus5 See below for Annual Average Monthly Composite Effluent Total Mercury6 Monthly Grab Effluent Total Phenols? Monthly Grab Effluent MBAS Quarterly Composite Effluent Total Iron Quarterly Composite Effluent Sulfates Quarterly Composite Effluent Chlorides Quarterly Composite Effluent Total Manganese Quarterly Composite Effluent Chronic Toxicity3 Quarterly Composite Effluent Total Chromium? Monthly Composite Effluent Total Zinc7 Monthly Composite _ Effluent Notes: 1. U= upstream at NC Highway 27. D = downstream at I-85. Upstream and downstream samples for dissolved oxygen, temperature, conductivity and pH shall be collected three times per week during June, July, August and September and once per week during the remaining months of the year. 2. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units. 3. Chronic Toxicity, refer to Section A. (3). 4. Staging requirements (applicable April 1-October 31) — Refer to Section A. (5). 5. The Total Nitrogen limitation is 444.1 pounds/day and Total Phosphorus limitation is 32.5 pounds/day based on a 12- month rolling average. Refer to Section A. (4). b. See Sections A. (2) b and A. (2) e. 7. See Sections A. (2) c and A. (2) f. There shall be no discharge of floating solids or visible foam in other than trace amounts. When an approved analytical protocol with the appropriate minimum detection level is followed and a result of "non -detectable" or "below quantitation limit" is obtained, the permittee will be considered to be in compliance with the numerical permit limit for that pollutant. 3 Permit NC0004375 A. (1) b TIER 2 EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS During the period beginning upon addition of future wastewater sources and lasting until expiration, the Permittee is authorized to discharge treated OCPSF, CWT and non -categorical industrial process wastewater from outfall 001. Such discharges shall be limited and monitored by the Permittee as saecified below: LIMITATIONS MONITORING REQUIREMENTS EFFLUENT EFFLUENT CHARACTERISTICS Monthly Average Daily Maximum, Measurement Sample Sample Locations Frequency Type Flow 3.9 MGD Continuous Recording Influent or Effluent BOD, 5-day, 20°C4 485.0 pounds/day 1215.0 pounds/day Daily Composite Effluent Total Suspended Solids 543.0 pounds/day 1437.0 pounds/day Daily Composite Effluent Dissolved Oxygen Daily Grab Effluent, U', Di Fecal Coliform (geometric mean) Monthly Grab Effluent pH2 Daily Grab Effluent, U', Di NH3 as N4 618.0 pounds/day 927.0 pounds/day Daily Composite Effluent Temperature °C Daily Grab Effluent, Ul, DI Conductivity Daily Grab Effluent, U', D1 COD Monthly Grab Effluent Total Nitrogen5 (NO2+NO3+TKN) • See below for Annual Average Monthly Composite Effluent Total Phosphorus5 See below for Annual Average Monthly Composite Effluent Total Mercury6 Monthly Grab Effluent Total Phenols? Monthly Grab Effluent MBAS Quarterly Composite Effluent Total Iron Quarterly _ Composite Effluent Sulfates Quarterly Composite Effluent Chlorides Quarterly Composite Effluent Total Manganese Quarterly Composite Effluent Chronic Toxicity3 Quarterly Composite Effluent Total Chromium? Monthly Composite Effluent Total Zinc7 Monthly Composite Effluent Notes: 1. U = upstream at NC Highway 27. D = downstream at I-85. Upstream and downstream samples for dissolved oxygen, temperature, conductivity and pH shall be collected three times per week during June, July, August and September and once per week during the remaining months of the year. 2. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units. 3. Chronic Toxicity, refer to Section A. (3). 4. Staging requirements (applicable April 1-October 31) — Refer to Section A. (5). 5. The Total Nitrogen limitation is 444.1 pounds/day and Total Phosphorus limitation is 32.5 pounds/day based on a 12- month rolling average. Refer to Section A. (4). 6. See Sections A. (2) b and A. (2) e. 7. See Sections A. (2) c and A. (2) f. There shall be no discharge of floating solids or visible foam in other than trace amounts. When an approved analytical protocol with the appropriate minimum detection level is followed and a result of "non -detectable" or "below quantitation limit" is obtained, the permittee will be considered to be in compliance with the numerical permit limit for that pollutant. 4 Permit NC0004375 A. (2) a EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 1 OCPSF Parameters During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge OCPSF and Centralized Waste Treatment (CW1) related process wastewater from outfall serial number 001. Such discharges shall be limited and monitored by the Permittee as specified below: "tn.t ".."• - �„„MVntChaacterWi 4.x,-7.r/- .:a..t -, -- ... �t.. . _t,: DailMiAimuni alMon b1p' A/v' erage ' (t ti . S!y% . k.} "MJeagures ent }y 2F :'vC c +-7/1e - .. ...... .. ib. s ,,Location );':. .. -r.. ... .. d , . 4,....t.44--.w e'_..3al Acenaphthene 0.50 0.11 Annually Grab Effluent Acenaphthylene 0.50 0.11 Annually Grab Effluent Acrylonitrile 1.19 0.47 Annually Grab Effluent Anthracene 0.50 0.11 Annually Grab Effluent Benzene 0.67 0.18 Annually Grab Effluent Benzo(a)anthracene 0.50 0.11 Annually Grab Effluent 3,4-Benzofluoranthene 0.50 0.11 Annually Grab 'Effluent Benzo(k)fluorantherie 0.50 0.11 Annually , Grab Effluent Benzo(a)pyrene 0.50 0.11 Annually Grab Effluent Carbon Tetrachloride 0.19 0.09 Annually Grab Effluent Chlorobenzene 0.14 0.07 Annually Grab Effluent Chloroethane 1.32 0.51 Annually Grab Effluent Chloroform 0.23 0.10 Annually Grab Effluent 2-Chlorophenol 0.48 0.15 Annually ' Grab Effluent Chrysene 0.50 0.11 Annually Grab Effluent Di-n-butyl phthalate 0.28 0.13 Annually Grab Effluent 1,2-Dichlorobenzene 0.80 0.38 Annually Grab Effluent 1,3-Dichlorobenzene 0.22 0.15 Annually Grab Effluent 1,4-Dichlorobenzene 0.14 0.07 Annually Grab Effluent 1,1-Dichloroethane 0.29 0.11 Annually Grab Effluent 1,2-Dichloroethane 1.04 0.33 Annually Grab Effluent 1,1-Dichloroethylene 0.12 0.08 Annually Grab Effluent 1,2-trans-Dichloroethylene 0.27 0.10 Annually Grab Effluent 2,4-Dichlorophenol 0.55 0.19 Annually Grab Effluent 1,2-Dichloropropane 1.13 0.75 Annually Grab Effluent 1,3-Dichloropropylene 0.22 0.14 Annually Grab Effluent Diethyl phthalate 1.00 0.40 Annually Grab Effluent 2,4-Dimethylphenol 0.18 0.09 Annually Grab Effluent Dimethyl phthalate 0.23 0.09 Annually Grab Effluent 4,6-Dinitro-o-cresol 1.36 0.38 Annually Grab Effluent 2,4-Dinitrophenol 0.61 0.35 Annually Grab Effluent 2,4-Dinitrotoluene 1.40 0.56 Annually Grab Effluent 2,6-Dinitrotoluene 3.15 1.25 Annually Grab Effluent Ethylbenzene 0.53 0.16 Annually Grab Effluent Fluorene 0.50 0.11 Annually Grab Effluent Hexachlorobenzene 0.14 0.07 Annually Grab Effluent Hexachlorobutadiene 0.24 0.10 Annually Grab Effluent Hexachloroethane 0.27 0.10 Annually Grab Effluent Methyl Chloride 0.93 0.42 Annually Grab Effluent Methylene Chloride 0.44 0.20 Annually Grab Effluent Naphthalene 0.50 0.11 Annually Grab Effluent Nitrobenzene 0.33 0.13 Annually Grab Effluent 5 Permit NC0004375 A. (2) a EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 1 OCPSF Parameters (continued) <s.� _ Effiunt e.Characteristic •... . w. _ .. ...�'... _. .. - Daily Ma$imum . - poundsfdayYr � Y:... w _.,._. ._ •.... .w.. .. Monthly Average:. r, pounds/day, } �. .• Lti , s. i:G.Y . ,ti. •,. ,J,: : P, Measurement,'. , Frequency r, .,.Y'.•'t:t w... __1. Sample -.MType .... ... .. .... _ Sample:,..; A Locations .. - _ .. 2-Nitrophenol 0.34 0.20 Annually Grab Effluent 4-Nitrophenol 0.61 0.35 Annually Grab Effluent Phenanthrene 0.50 0.11 Annually Grab Effluent Pyrene 0.50 0.12 Annually Grab Effluent Tetrachloroethylene 0.28 . 0.11 Annually Grab Effluent Toluene 0.39 0.13 Annually Grab Effluent Total Cyanide 2.52 2.07 Annually Grab Effluent 1,2,4-Trichlorobenzene 0.69 0.33 Annually Grab Effluent 1,1,1-Trichloroethane 0.27 0.10 Annually Grab Effluent 1,1,2-Trichloroethane 0.27 0.10 Annually Grab Effluent Trichloroethylene 0.27 0.10 Annually Grab Effluent Vinyl Chloride 1.32 0.51 Annually Grab Effluent A. (2) b EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 1 CWT Parameters ; ,F, .'. _ . Elfiuent Characteristic •: Daily:Maaiadunk , pounds/day* x MonthlyAgerage:. pounds/dalr , • 1 • Measurement. Frequcnc3r L t%' _. Saiaple- : Sampler Location Total Antimony 0.166 0.099 Annually Composite Effluent Total Arsenic 0.113 0.073 Annually Composite Effluent Total Barium 0.299 0.197 - Annually Composite Effluent Total Cadmium 0.012 0.007 Annually Composite Effluent Total Cobalt 0.135 0.087 Annually Composite Effluent Total Mercury 0.0016 0.0005 Monthly Grab Effluent Total Molybdenum 0.708 0.676 Annually Composite Effluent Total Selenium 1.149 0.286 Annually Composite Effluent Total Silver 0.084 0.025 Annually Composite Effluent Total Tin 0.287 0.084 Annually Composite Effluent Total Titanium 0.036 0.021 Annually Composite Effluent Total Vanadium 0.153 0.046 Annually Composite Effluent Acetone 21.157 5.583 Annually Grab Effluent Acetophenone 0.080 0.039 Annually Grab Effluent Aniline 0.023 0.011 Annually Grab Effluent 2-Butanone 3.370 1.296 Annually Grab Effluent Butylbenzyl phthalate 0.132 0.062 Annually Grab Effluent Carbazole 0.419 0.193 Annually Grab Effluent o-Cresol 1.345 0.393 Annually Grab Effluent p-Cresol 0.489 0.144 Annually Grab Effluent n-Decane 0.664 0.306 Annually Grab Effluent 2,3-Dischloroaniline 0.051 0.025 Annually Grab Effluent n-Octadecane 0.413 0.212 Annually Grab Effluent Pyridine 0.259 0.128 Annually Grab Effluent 2,4,6-Trichlorophenol 0.109 0.074 Annually Grab Effluent 6 Permit NC0004375 A. (2) c EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 1 Combined OCPSF and CWT Parameters ;" r _ _ = , Effiuent.Characteristic- Daily Mazianu h1 poumda/da Monthly Average: poudapnds/ M'easufemen Frequency- T - �` '.Sample`` ,fir =Type. -, Sample' Location ..:-. Bis(2-ethylhexyl) phthalate 1.52 0.58 Annually Grab Effluent Total Chromium 14.15 5.69 Monthly Composite Effluent Total Copper 16.98 7.30 Annually Composite Effluent Fluoranthene 0.37 0.14 Annually Grab Effluent Total Lead 3.64 1.69 Annually Composite Effluent Total Nickel 22.35 9.33 Annually Composite Effluent Total Phenol 2.68 0.83 Annually Grab Effluent Total Zinc 13.19 5.46 Monthly Composite Effluent 7 Permit NC0004375 A. (2) d EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 2 OCPSF Parameters r r.-► t rt7 ;_. .`.:I t,-- *,;.- '.3 '` *matCharaet t L f Maximum. i' . you dOtda Monthly: Average • pounds/day;'lr -Measurement. p y inmn ., . Sample i 'ripe 1 . Sample y, Loca flow; _ Acenaphthene 0.50 0.13 Annually Grab Effluent Acenaphthylene 0.50 0.13 Annually Grab Effluent Acrylonitrile 1.39 0.55 Annually Grab Effluent Anthracene 0.50 0.13 Annually Grab Effluent Benzene 0.78 0.21 Annually Grab Effluent Benzo(a)anthracene 0.50 0.13 Annually Grab Effluent 3,4-Benzofluoranthene 0.50 0.13 Annually Grab Effluent Benzo(k)fluoranthene 0.50 0.13 Annually Grab Effluent Benzo(a)pyrene 0.50 0.13 Annually Grab Effluent Carbon Tetrachloride 0.22 0.10 Annually Grab Effluent Chlorobenzene 0.16 0.09 Annually Grab Effluent Chloroethane 1.54 0.60 Annually Grab Effluent Chloroform 0.26 0.12 Annually Grab Effluent 2-Chlorophenol 0.56 0.18 Annually Grab Effluent Chrysene 0.50 0.13 Annually Grab Effluent Di-n-butyl phthalate 0.33 0.16 Annually Grab Effluent 1,2-Dichlorobenzene 0.94 0.44 Annually Grab Effluent 1,3-Dichlorobenzene 0.25 0.18 Annually ' Grab Effluent 1,4-Dichlorobenzene 0.16 0.09 Annually Grab Effluent 1,1-Dichloroethane 0.34 0.13 Annually Grab Effluent 1,2-Dichloroethane 1.21 0.39 Annually Grab Effluent 1,1-Dichloroethylene 0.14 0.09 Annually Grab Effluent 1,2-trans-Dichloroethylene 0.31 0.12 Annually Grab Effluent - 2,4-Dichlorophenol 0.64 0.22 Annually Grab Effluent 1,2-Dichloropropane 1.32 0.88 Annually Grab Effluent 1,3-Dichloropropylene 0.25 0.17 Annually Grab Effluent Diethyl phthalate 1.17 0.47 Annually Grab Effluent 2,4-Dimethylphenol 0.21 0.10 Annually Grab Effluent Dimethyl phthalate 0.27 0.11 Annually Grab Effluent 4,6-Dinitro-o-cresol 1.59 0.45 Annually Grab Effluent 2,4-Dinitrophenol 0.71 0.41 Annually Grab Effluent 2,4-Dinitrotoluene 1.64 0.65 Annually Grab Effluent 2,6-Dinitrotoluene 3.69 1.47 Annually Grab Effluent Ethylbenzene 0.62 0.18 Annually Grab Effluent Fluorene 0.50 0.13 Annually Grab Effluent Hexachlorobenzene 0.16 0.09 Annually Grab Effluent Hexachlorobutadiene 0.28 0.12 Annually Grab Effluent Hexachloroethane 0.31 • 0.12 Annually Grab . Effluent Methyl Chloride 1.09 0.49 Annually Grab Effluent Methylene Chloride 0.51 0.23 Annually Grab Effluent Naphthalene 0.50 - 0.13 Annually Grab Effluent Nitrobenzene 0.39 0.16 Annually Grab Effluent 2-Nitrophenol 0.40 0.24 Annually Grab Effluent 4-Nitrophenol 0.71 0.41 Annually Grab Effluent Phenanthrene _ 0.50 0.13 Annually Grab Effluent 8 Permit NC0004375 A. (2) d EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 2 OCPSF Parameters (continued) , s �.. � �•` � > � ,'R �,t � n Effiuent Charactesistic.. _ .1....._.•.. ..,, -7 ...... ?:fi i ��Dailp 11da�aimttm f 1 h' ilia/days' :•, ♦ _ ..v' , ,4t.- -, -. ">•. Moatlly Average:, . i. • lbs/da►g- • -_ • H . r. a ,.. _ ' Measurement' f y '. Frequency +.:r ... . -� .z _ . -' :... Sample i� - .. Y NType : ` Sample , Y 'Location ,, ___ Pyrene 0.50 0.14 Annually Grab Effluent Tetrachloroethylene 0.32 0.13 Annually Grab Effluent Toluene 0.46 0.15 Annually Grab Effluent Total Cyanide 2.95 2.42 Annually Grab Effluent 1,2,4-Trichlorobenzene 0.81 0.39 Annually Grab Effluent 1,1,1-Trichloroethane 0.31 0.12 Annually Grab Effluent 1,1,2-Trichloroethane 0.31 0.12 Annually Grab Effluent Trichloroethylene 0.31 0.12 Annually Grab Effluent Vinyl Chloride 1.54 0.60 Annually Grab Effluent A. (2) e EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 2 CWT Parameters '"' - . + ,�� ^t Effluent Characteristic = ate •.. ... .... "-` _ ..'. .., .: = ..: Daily Maximum -.Monthly Average.: .�. pounds/day ,_ , .. .. ... :. .. .. •Measurement : Frequency i.'.... .. .. ,... 'r. . Saa�ple4 r , � -.� Type .... :>.t :: §gam ple, .Location -. :+`: ., _ . .•: _ ,pounds/day ..ti... ,.., a,. 5•_.,., .-.. Total Antimony 0.526 0.313 Annually Composite Effluent Total Arsenic 0.359 0.231 Annually Composite Effluent Total Barium 0.947 0.623 Annually Composite Effluent Total Cadmium 0.038 0.023 Annually Composite Effluent Total Cobalt 0.426 0.275 Annually Composite Effluent Total Mercury ' 0.0052 0.0016 Monthly Grab Effluent Total Molybdenum 2.241 2.141 Annually Composite Effluent Total Selenium 3.638 0.905 Annually Composite Effluent Total Silver 0.266 0.078 Annually Composite Effluent ' Total Tin 0.907 0.266 Annually Composite Effluent Total Titanium 0.113 0.066 Annually Composite Effluent Total Vanadium 0.484 0.147 Annually Composite Effluent Acetone 66.997 17.681 Annually Grab Effluent Acetophenone 0.253 0.125 Annually Grab Effluent Aniline 0.074 0.036 Annually Grab Effluent 2-Butanone 10.671 4.104 Annually Grab Effluent Butylbenzyl phthalate 0.417 0.197 Annually Grab Effluent Carbazole 1.327 0.612 Annually Grab Effluent o-Cresol 4.259 1.245 Annually Grab Effluent p-Cresol 1.548 0.455 Annually Grab Effluent n-Decane 2.103 0.969 Annually Grab Effluent 2,3-Dischloroaniline 0.162 0.080 Annually Grab Effluent n-Octadecane 1.307 0.670 Annually Grab Effluent Pyridine 0.821 0.404 Annually Grab Effluent 2,4,6-Trichlorophenol 0.344 0.235 i Annually Grab Effluent 9 Permit NC0004375 A. (2) f EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Tier 2 Combined OCPSF and CWT Parameters is -, n .1: ,4a, '. Effluent Characteristic Daily Maximum -.pounds/day. . , Monthly Average', -pounds/day . Measurement, Frequency Sample: r Typc ., Sample Locafioa Bis(2-ethylhexyl) phthalate 2.08 0.82 - Annually Grab Effluent Total Chromium 17.60 7.10 Monthly Composite Effluent Total Copper 20.56 8.88 Annually , Composite Effluent Fluoranthene 0.51 0.20 " Annually Grab Effluent Total Lead 4.75 2.20 Annually Composite Effluent Total Nickel 31.7 12.9 Annually Composite Effluent Total Phenol 8.25 2.48 Annually Grab Effluent Total Zinc 16.12 6.97 Monthly Composite Effluent Notes for OCPSF and CWT Parameters Should any annual monitoring result in detection of an OCPSF parameter contained in 40 CFR 414 Subpart I (excluding metals) or CWT parameter contained in 40 CFR 437 Subpart D, then quarterly monitoring will begin immediately for the detected parameter(s). After four consecutive quarterly samples resulting in non -detection are achieved, the monitoring frequency will revert to annually. When an approved analytical protocol with the appropriate minimum detection level is followed and a result of "non - detectable" or "below quantitation limit" is obtained, the permittee will be considered to be in compliance with the numerical permit limit for that pollutant. A. (3) CHRONIC TOXICITY PERMIT LIMIT (Quarterly) The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to Ceriodaphnia dubia at an effluent concentration of 1.8%. The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. The tests will be performed during the months of March June September and December. Effluent sampling for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes. If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. The chronic value for multiple concentration tests will be determined using the geometric mean of the highest concentration having no detectable impairment of reproduction or survival and the lowest concentration that does have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the following address: Attention: North Carolina Division of Water Quality Environmental Sciences Branch 1621 Mail Service Center Raleigh, North Carolina 27699-1621 Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30 days after the end of the reporting period for which the report is made. 10 Permit NC0004375 Test data shall be complete, accurate, include all supporting chemicaVphysical measurements and all concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Branch at the address cited above. Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be required during the following month. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control -organism survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an invalid test and will require immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring. A. (4) TOTAL PHOSPHORUS AND TOTAL NITROGEN MONITORING The Permittee shall calculate a 12-month rolling average mass loading as the sum of monthly loadings, according to the following equations: (1) Monthly Average (pounds/day) = TP x Qw x 8.34 where: TP = the arithmetic average of total phosphorus concentrations (mg/L) obtained via composite samples (either daily, weekly, or monthly average values) collected during the month Qw = the average daily waste flow (MGD) for the month 8.34 =conversion factor, from (mg/L x MGD) to pounds The 12-month rolling average mass loading is defined as the sum of the monthly average Loadings for the previous 12 months inclusive of the reporting month: 12 (2) 12-Month Mass Loading (pounds/day)= ETPma =12 (inclusive of reporting month) Where: TPma = the total phosphorus monthly average mass loading (calculated above). Total Nitrogen is to be calculated using the same method. The monthly average and 12-month average mass loadings shall be reported on the attached worksheet and submitted with the discharge monitoring report for Clariant Corporation. The first worksheet is due with the discharge monitoring report, 12 months from the effective date of the total phosphorus and total nitrogen limits. In the interim period between the effective date and the requirement to submit the attached worksheet, the total phosphorus and total nitrogen monthly average mass loadings should be reported on the discharge monitoring report for the respective facility. The Permittee shall report the total phosphorus and total nitrogen concentrations for each sample on the discharge monitoring report. Reporting of and compliance with the phosphorus and nitrogen limits shall be done on a monthly basis. 11 ti Permit NC0004375 A. (4) TOTAL PHOSPHORUS AND TOTAL NITROGEN MONITORING (continued) The permittee shall be required to perform a study which determines monthly average limits for total phosphorus (TP) and total nitrogen (TN) which can be met through the application of best available technology (BAT) that is economically achievable. The study shall be based on 12 months of effluent monitoring data collected from January 1, 2003 to December 31, 2003. The BAT study report shall be submitted to the NCDWQ for approval by July 1, 2004 and the division will apply BAT limits for TP and TN to the permittee's discharge based on the results of this study and the performance of other similar plants. The TP and TN limitations shown in A. (1) are interim limits which shall remain in effect until the BAT study is completed and BAT limits for TP and TN are established by the Division. A. (5) STAGING REQUIREMENTS (APPLICABLE APRIL 1— OCTOBER 31) The operating day runs from 7:00 am to 7:00 am. Each day, the permittee will calculate a running daily average stream flow as determined by turbine operation at Mountain Island Dam, leakage at the dam (80 cfs), and the 7Q10 flow of Dutchman's Creek (15 cfs). Effluent release is to be controlled such that projected release of BOD and ammonia, using the most recent analytical values for these parameters, will not exceed the value given in the following formulas: (1) When the daily river flow is calculated to be < or = 175 cfs: BOD5 + 0.54(NH3-N) <=566.4 pounds/day (2) When daily average river flow is calculated to be >175 cfs but < or = 250 cfs: BOD5 + 0.54(NH3-N) <=1044 pounds/day The attached additional DMR sheet (see next page) shall be used to monitor compliance with BOD and NH3 staging requirements during the summer (April 1— October 31) 12 Permit NC0004375 Additional DMR Sheet for Clariant-Mt. Holly East EFFLUENT NPDES Permit NC0004375 Discharge Month Year Clariant Class 4 Mecklenburg County Operator in Responsible Charge (ORC): Certified Laboratory: Person(s) Collecting Samples: Check if ORC has changed Qw T River Flow BOD5 I certify that this report is accurate and complete to the best of my knowledge. X Allowable Actual NH3 BOD+.54NH3 BOD+.54NH3 ends/day) (pounds/day) (pounds/day) Case Comp? (Y/N) LJ4LG 1 1'me v,,a -',../ v-..,/ kt- -----• ---;, ..- - - _ 2 3 4 5 _ 6 7 8 9 10 11 12 13 14 15 16 17 18 19 _ 20 21 22 23 - 24 25 26 27 28 29 30 31 Average Case 1: River Flow <= 175 cfs, BOD5 + 0.54NH3 <= 566.4 pounds/day Case 2:175 cfs < River Flow <= 250 cfs, BODs + 0.54NH3 <=1044 pounds/day Case 3: River Flow > 250 cfs, BODs<= 329.0 pounds/day (monthly average), BODs<= 810 pounds/day (daily maximum), NH3<= 618.0 pounds/day (monthly average), BODs<= 927 pounds/day (daily maximum) 13 Permit NC0004375 A. (6) Effluent Pollutant Scan The permittee shall perform an annual pollutant scan of its treated effluent for the following parameters: Ammonia (as N) Trans-1,2-dichloroethylene Bis (2-chloroethyl) ether Chlorine (total residual, TRC) 1,1-dichloroethylene Bis (2-chloroisopropyl) ether Dissolved oxygen 1,2-dichloropropane Bis (2-ethylhexyl) phthalate Nitrate/Nitrite 1,3-dich oropropylene 4-bromophenyl phenyl ether K(eldahl nitrogen Ethylbenzene Butyl benzyi phthalate Oil and grease Methyl bromide 2-chloronaphthalene Phosphorus Methyl chloride 4-chlorophenyl phenyl ether Total dissolved solids Methylene chloride Chrysene Hardness 1,1,2,2-tetrachloroethane Di-n-butyl phthalate Antimony Tetrachloroethytene Di-n-octyl phthalate Arsenic Toluene Dibenzo(a,h)anthracene Beryllium 1,1,1-trichloroethane 1,2-dichlorobenzene Cadmium 1,1,2-trichloroethane 1,3-dichlorobenzene Chromium Trichloroethylene 1,4-dichlorobenzene Copper Vinyl chloride 3,3-dichlorobenzidine Lead Acid -extractable compounds: Diethyl phthalate Mercury P-chioro-m-creso Dimethyl phthalate Nickel 2-chlorophenol 2,4-dinitrotoluene Selenium 2,4-dichlorophenol 2,6-d€nitrotoluene Silver 2,4-dimethylphenol 1,2-d€phenylhydrazine Thallium 4,6-dinitro-a-cresol Fluoranthene Zinc 2,4-dinitrophenol Fluorene Cyanide 2-nitrophenol Hexachlorobenzene Total phenolic compounds 4-nitrophenol Hexachlorobutadiene Volatile organic compounds: Pentachlorophenol Hexachtorocydo-pentadiene Acrolein Phenol Hexachloroethane Aaylonitrile 2,4,6-trichlorophenol lndeno(1,2,3-cd)pyrene Benzene Base -neutral compounds: Isophorone Bromoform Acenaphthene Naphthalene Carbon tetrachloride Acenaphthytene Nitrobenzene Chlorobenzene Anthracene N-nitrosodi-n-propylamine Chlorodibromomethane Benzidine N-nitrosodimethylamine Chloroethane Benzo(a)anthracene N-nitrosodiphenylam€ne 2-chloroethylvinyl ether Benzo(a)pyrene Phenanthrene Chloroform 3,4 benzofluoranthene Pyrene Dichlorobromomethane Benzo(ghi)perylene 1,2,4-trichlorobenzene 1,1-dichloroethane Benzo(k)fluoranthene 1,2-d€chloroethane Bis (2-chEoroethoxy) methane > The total set of samples analyzed during the current term of the permit must be representative of seasonal variations. ➢ Samples shall be collected and analyzed in accordance with analytical methods approved under 40 CFR Part 136. ➢ Unless indicated otherwise, metals must be analyzed and reported as total recoverable. ➢ Test results shall be reported to the Division on DWQ Form- DMR-PPA1 or in a form approved by the Director, within 90 days of sampling. Two copies of the report shall be submitted along with the DMR forms to the following address: NC DENR / DWQ/ Central Files, 1617 Mail Service Center, Raleigh, North Carolina 27699-1617. 14 Permit NC0004375 A. (7) NOTIFICATION OF NEW WASTE SOURCE Clariant Corporation will notify the Division of Water Quality's Mooresville Regional Office and the Point Source Compliance/Enforcement Unit at least fourteen (14) days prior to the addition of any new waste source to the treatment facility. The addition of any new waste source will trigger Clariant's compliance with Tier 2 effluent limitations and monitoring requirements. 15 DEC 12 2002 09:15 FR CLT DESERVER AD TO 9191973307190653 P.02/02 DEC 12 2002 09:15 FR CLT OBSEvEP AD TO 9191973307198653 P.01/02 ww512.1.1.4r ZNItb rain . 4 d agpaagabarmlallru.q roPIN e7 4111 Nato. r'1w`i2.: er�a ,T,eeeor.°F:6�v:'mw acb" ° Ver''`".w+ kaArrAS2.7 SIt.11 r o.V:i wee Vs'rry wwv ..rands a.noumr k} f rt 14.401 areray.,r 11.12 Y p� T16 Yb.61.I.,cn�r. 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"""'1%ii a wi w Kgt:'rn°"°�yr" . ai ITrW/FM,I. a._(r..raY^• �laaee "r.• na]. w"'"""°.�bcr";,y,' $a=iRiairl !!du ti8i •euglitr=""°l.1.pa t.tt�1aM ....- Gel -Great k Results' +gp��..�o.er:a"t.. ,', wrnr +gYlaq,sl.ao rlde.rMtllgl•ip•tESE Ya0 tTMGNUGIYTXq aN �iiwioa OY.eM �� OItMr FrI'tl. ,Aa a,aMl. r. Oats C Wclun an.l„ aaa.eerrww 11 pet buro lP NRra.11otaarhia.2.6r�"uourt wuel ynw c l' PALM 1 M�pn�Cwr"r` 61«I, r,rr rri��. a'r: PP" SIrWOLa � r6at Ya N� n ror .O'".t. N ( fir di MP"' ..ntl MV eer y'byry A tlrindj. P r� l L gM Notices reel IOryarpXyfA hbarRW I( 6� 9 uAX aeAm cNi6u'OY Waes/Mr ,j bN ChWda6lt O..tldM.RYaMr.d N" eIC rat aaetrb �'fvr R.Y,IOX, XC ittq-lair Ip 10. ebNf• p.ri ice rawlrw aCe�Nr. =.' bIYW+MuafoKl ANN eve "n'Yl,„_ EIYr"~+nrrn�*�+bn I u^I a"ODYr llam kr.y. .. angrla Aram I �M.//6 Yl►readYb Re•.s Ow+,:A R.W, rw,, td'i•ftylam M+rYe tie��Yirhm awl YYmowi.4 �aaq+aa.vtwtlo nu?? bl.w1 •b. n« gzar�em""raar"'{ry =w'�w yqb Wtera'e47rrahN ~IW'p 9«rnl :?0 Z.N.Y. Mbvltlenb0a e++WI.d CArYlaas Olga "IS .�.1rWr.�ar,H41YT n]faAO M..wn w.ti ow.. e.� rah tlegr b rW r latlq I"^ P VYO M rrna N ll,mMr/ IACaW �7Y,.NOf• 37a•/OOo'•I RGTIretAllegKI, lU1 RArrIr A X.NJ a .40a l brat.,. r4176 t.rr gpa,,y� A M16f�, r�rlAl Y,a.s or OW�apt�. d.dNwWr a•rRl'OW.Y YA Boge ]R r Vp. 11f..Yw9Y,bur r ..2s4110.4. 'ftr"`.+r�e°�' NM: Ml•mlo tM PKrralAWu, Cowl rem* eatrr .aOSWlaY,er ps P errd •aRu.7-UYiiWWI m ann , c pa peyn w ** TOTAL PFlGE.02 ** Phone: 704-358-5322 Fax: 704-358-5340 Fax To: Christy Taylor raxt 919-733-0719 The Charlotte Observer From: Olivia Bachman Pagus: 2 Phone: Re: Gate: 12/12102 0 Urgent 0 For Review 0 Please Comment 0 Please Reply 0 Please Rocycle Christy, I have faxed you a copy of the ad that appeared in today's paper, Thursday. December 12, 2002. Please let me know if for any reason it was printed Incorrectly. I have also aged out vouchers for both EIS that ran incorrectly on September 10, 2002 and December 1, 2002. NCDENR should reaciva these credal as anon as at the paperwork is processed; within a month If you need any further assistance. please let me know. Thank you. OInas Bachman - County Mecklenburg NPDES Permit Number NC0004375, Mount Holly East (MHE) Facility, PO Box 669246, Charlotte, NC 28266 has applied for a for a facility located in Mecklenburg County discharging treated wastewater into CATAWBA RIVER in the CATAWBA River Basin. Currently are water quality limited. This discharge may affect future allocations in this portion of the receiving stream. Wednesday, November 27, 2002 1617 Mail Service Center, Raliegh, North Carolina 27699-1617 - Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer - 50% Recycled / 10% post -consumer paper DEC 12 2002 09:15 FR CLT OBSERVER AD TO 9191973307198653 P.02/02 UNDER AND Ef' VIFTTIIF d��the 1.,,,.f anal eutha,kn contat,gq m rim we canon Deed of 7Kmt eaa0tltbded detvettld byy'7DMMIE MILTON de 9L J0341Y AND KAREN J. 111/ NSY HU98AND AM] WI dater: t,ln era Sgeptember 24. 1007 rend moonr,d Indio Ccied of the Este( 61 Indebt Deed, of MECIq. N[61AB County Nadi carotins. n Book 7 a mew end became. of dofwil In the Deynaoit Qt yto rnyt6�- beds fb w *live 100eoml o(n Wad pen0 ride lain, .towtaenlltgdq taw e" lace M seed Deed vt, Dare tlreaan, to the N heel b �btle tell praob 76r see, et CUM ' Darold he cram contained encl. pthduael Imp demander j bidder id web el der treUnt pteca of =eat Ow sting IDOM 10l OF E ono =limo cvitowo, coo Bur 4TH ero'MEET..c VW TTE, Fa 11100 NEIJRO Cum1 Catinhltm, In / b.eso oath Oct *Meese, ld�Ovl le tl a4n of Fdd�y She 13dt der LINO n, al ,deaf, ykfp end being In the dry vl Chance IrnIXOYenuilla din- S67 EN8UREL Rea* or North G rdirw, end barns nest Dank ,env tNMb.el M lehoe'0: • vino el Oi Lot 21 in Frock 4 0f Papier Spina Mrbdiyhton Be care b etyrvntitwr/r acRep Ire Lisp pool zl at P.m re to Ohs tell dime d property: 6120 t� Soho r, r3henne. NO 20 e0 exesed a 5 r, o the rain to 0)1 pronely ore awrarb0e may a serves kl luau leered bid* Tate &thet as Tut. 2 Le oe6tl th, right M.ro a or writhed dxxk net to a08 (el leant Record thie te: Tberrny Morton slakes. and Koran J. Old ono term, d the radiate that the real Iwr,In stet erq raq uital LP pay rid Tier iq yr u end the reetapo bytamps v3.C.pdie .R Sb°edlon 7M �� 9 Eunnlee.a$D{*yNYet dk/ Cute fool:tared BBe p I 1- Airedale P201 AKC Cho 1 ' Behind Hots pe gnle2 Why 8 Drowns. 704 SJ2-Dill tins. ! 0 ee. le4_�gg. T� yy Asia rtce vakea e i [�RISTryIAS 04-542 ES a farmed plan bloodline, $460, Cd seiX1. ,f5 P -5 8 erg@, Our 91h VBar sllrvtnD the HCHRIST AS' i Euet o28-d4o•2677orB29-584.gg6Z C7v"-233•tm88 communtly pe naive lnami FREQ To ti ustrol, 704405• 07.1 riles, grant cers. pl-�e•34er ion, I F. /b,(ol595.l803 aAK yks Akitapups,1 female. S6 ureherd Perri AU4!reh Ilan Fred to owl h et Rr-+ceetl aui �2•'Oi fa - � Mather of & 4ICJIlens. oAKC Alai an Metemt+fe ITC Basel No4in f pypole; Ca 1704-537-6256 CI frl , specs IaSrpetlSfC ' 9 7 -rrto9 I n k111eng eFA, fate re. or936-J92 4 �5 ZY4- 1 Persle �� Sims . Val Can l earn . I sh �� • e a Wkand fbt+, 64-J20- 516 Au■.2M' vup RBatlY .wl Rog. Pers4ntend Him. meant Rev Ialnledt eeebe877791 emai hooka/aforedeed txe 60d exceed eater of vo m' (S a e Sovvnd D Fl8y noon (s7sono%. NM( a‘roe° "1.11,2124 Bole inn/ Noto, 19 rexempt hem plylnp the seas, the eUrceaSM bidder io� may aim be hid ID pay revenue slam on the Tueter9 Deed, mar Land hwWor. Ttr. anal the eat r q,*q by N.C,tia. Svevvn 7a NI pp�� wteryyaapYrnlltbiegeri n SDOve 4b dam,/, Inxn the Pu917lh dose of Vie rw (N Itatad b61OWr ei- Wrtt'a7 comments rmoar:Ms the pperrt,b 'mil De eccgpted ra . U 39 Wye afar the pu01bh date of ice. AL rbmmerea tecdv@d prior 10Iris* Date me oor>t*dared in the and determk,ellprte roe. 03Ioo tM propaard plank_ The Rpr,10( 01 t0 Nc DM1i0lpn 01 W01ef °le ty men decide to hold a pLt,irg reeding for the propp0 porn.* should GUit D pionof receive a etprrtfica tt decree a Wino In4nnL to delermkts oentlnl presentM de �gmaij 4sDle upon raoua!n and Mrment 01114 ooei bt m n,2.201D0, Mel 00mrninm °nd)w',quests lea Information t0191 NC 0Mllon of Wear Quality at the above address or pee Ms. *Env Stppl y at RIM t e-sor1, mr• tonere". woo. Ple.re brltafe me NPV5tj permit number (°trathgSQ In any aammunrarelen, frrLOrsamd person*r��iy�el�se Wall the I)11 on of Wafer Quality 94 812 N, 9ariabury Straw. aalai0N Ne 7l11041148 be- tween th, IMMIx, 010 0, tm. and 6:00 p.m. 0? raylaw rrd5rtlleucn 02 NOTIFICATION OF TO issisr A raw, wweTEwA78)i PE.RMr7 On the bests d ttevouui ,lee'wl w and a teerbn cf NO ()dr,arar CD pEite rteolea.2t. Ptluro taw a'Js0oMdeverlawtufetarlgnaend ree- ( PnE l0 leads a om, he North o ref PoA OmI Mprlea n i Connngylpl P The .x of Lai re to Bropt 16 d Patti Ridge, en same le shown Thereof recorded a ME* Book 1B, at Pepe 125. Madden Only Public amity. Addreee of pioperbo 11203 ranglbher b�, Cremona, NC 28220 wet 'loID,be Caenetor to the "'greet a�Tnc 9u6Nlule Tn tto C manse the meat to u4o ■ aPftMkd 2 Fvmare jQ permit dub all (17 Tha TM!jho 22nd dal of Novenae; 200 . WWI & Pitt, PA M: Subedarg metro larked: AaelolanWeFyty Clark of Suprxlor (lots* IP4ea98p/ • 1gx at the eels. e Bala wit he ante o nts wig armours. ag by low reglered, 'ten for tin (E0l dare for upset mv@ RKCD /U few woe T.rT l•I Y� Lady Gould: n FInches all C0iori 3125•3 Oe. %Hatfield II Chrtalmo.. 4-2t3-ea01 Ler Umbrella C Rehm NPOFA Ps h N,rmber N00004Xre, mute TM East (5l4 Peony PDa! In PO Box 18024ss,, chaarrllotte, NC T50 Ida Noodled for a }ler:11It totaled k1 IncMG co/AMA Ftref d " yern2e hr Into CATAwt3A luv5sl Ugtin, ere we; quality Wood. This dKneeledws in nup erect k4Ory eke -icon' M teal POMon dire. ncc. tine FHA neat VA/ 16.t9-0-Og3ODg. UN Nom10E OF CuoaIT►UTO Trehinc 9 FORECLOSURE Vial ' �OF RFAL 1ROPEf77Y ,Cou ire t.amorio•rog •NOTICE OF SU98TTTUTE TRUSTEE'S FORECLOSURE SALE or nett mummy car �n 0iioND dY 1 VIRTUE 4E 00 last anetr endauthorityby EDW*iod Ours, A MAP11°IE4 F N, Mod 86plentbgt 20 89 nr:1 rvcDMad In the OMw of tag Re( of peed, Of MECKLENBUR fall - North Garonne. k. Book MOO et roir, Moe; anti eapeur8 U ratioD to mot payment d the 114 0ledmae secured thereby and tau of erf.ony cee o pe orrttthg dlpt48VOne and Bargemen.* ono woman W demuroo(unt owner tarp hadar of the ;Owe Poaurtd by saki Deed of Tale* the undo 9tbdtlMa Tharee MII phaa lax al1B. el t9 eYrnrm M the under for cue m uwuerrdplgpa dsetr Id FIJOM 101 OFTHE CIVIL RTB BUILDINI0, 1199 EAST 4TH STREET CHARLOTTE. ECi0.EN6UA0 Caurrtv CaurFMxile In C1,MO , Nora, C....a.>a O'clock �d,.hdQn_. rig s 25each (02B)6 i AKC eaeyte�rupra, lit tdtol Fie aim pa rl-celareds 704-87p_2D34, elterS150 Dealt. AKC Bkhon pups, 4 mom 7rL ill 6heti, 3408. 028-753.40m caw?, hats, small. 744 624. Opp ps' aeol bDslpIts,JeekRun,Beeple keel. RolTet,AmHelrls i,Fties{ N. Cblhuihu.- pan by svl Oster 80r, leeh.lJ36)9S7-J60981000o Bta 16d, WKKWW,Heellhypt6�cam °"'m olld. tell 1edoekcd, lea i CTOD n 1 ■N d w/ el en corner, .7a4-277-6492 burg CKC Box puppies vow a Rent stet w/hlk race, D 9t Ia tl �le, Tgady iD a2DE4-�76-itim bed ForS°Ie:AK Boxer Rues. a• 4-792. e. 6 4111uI Christmas Boxer AK J91-2B0Tt 536 ep00011 laths 70/-C25 40p0i, pi114-793-4274j ewpOWeal( g. vat rtrr g Id rfnahY. i250, 704.545,76i6 dry viers, 2 luv, PoM9r9nlerte, 704.469.0140 ER p eprea 6 who o1 min3tar &c�glaoon ltg . 7b+-Dzs-6632, AKC Bvxgr Pu chentdan btnoa,ne, rich 7 -y9T-7B999t9i - AKnnGdd81u11Wyg��pu1 t gee, 9 W1,�k , 3B5-9Iy0 F�n9fleh Bulldog. pups. AKC; c,entp 010In. ve, record short & wrinkled, 2 Utters. 315C0 act, & W. 6/-244.3635 AKC rep. Ens', 8utld exc. bldlIn 8wk Whl9,g79rl9dlo F!1k3a6 m lila'4u 64a•335-8R}S En I eh Bu1d62 Pope [KG, 91 , Wrinkled 19Yeabq, bo,3II!UL freei lamas pro - sent Reidy now, BO-Jae-2037 Ar si7E II6h9471I 20 mo!@, 1 e 101jt day of December, 20D2 that EnCDrr- rOmBMI ORfgOf1 ousted tying sn� 0l 000 Present Rexed Ownero ECMaM A $*eggs et to MIchgke That TI ie Ci�pLRI.C7TTE OBSERVER 1 9V,Charhlottc-co)n era Mortgage Services Li cats -- Legal Service $100 DIVORCE 124 brs/d■ 7ppp-522-)}71 $1 oS`parationAo°reem,N Our ttorneys o11 Alt 15 : Pets' and Livestock coon �•.,w- .,, �1 25 125 kralealechles/5ervice`is- to Ll+ee ppltes./ `15-TIE /t nllfornu q 'Zits 3950 rail nl bk1,3150704-289.3941. ipfn, 010.704-846-> i CArilii5mes N@w oktn> peps. - neeple IwDDlos plus seer k- email: Whiskeqf/of061r0ya 0Om Hiring? led 4. bk a Mn. iO4-52g-SiiO4 SUN CONURE, S70D 6r 70/-677.1226- Ohe.rvvr Clasalhed, Oee,le tree to Good Hamel I04•e46 oils Rep RapAdolti ready 704-377-66S6 10 MOD1f1 old rf16k free to e XmeS$65070d 485 6a79 paDd owner wHlt a amend for �� Nam. Adorable Rescued KII- 24)223 ens/cers, vet_-Currenl, 02- 70/-J91• eaalah- StaM6ie mum,. 70 -992.1a9i. FOUND white lemala'mynQ Catr-hunk Iles war, ht.eit beaCy,nbtacl lierloll 5cp( ln_ Ianal Ehn S1. 704-044-6fi0o • Get•Grest Results: r,_i _ Call CMssined 7174-377.5555 , . Notices L(eg�1 Nopces~- STAtEMAUD Nome NORM CAROL/NA 20 ENVIRONMENTAL MANAGEMENT COMMI881QWMPOES Ukrr a • - let? HAh4.rAV1C6 COMA RALEIOH, NC 7Met1.1612 lnl www.eharlolre,com Yard. ry0e ell snots and been neutered Cell Lon al (704)660-925L Cairns BChIhu hued, Mel 090iilor i rtiri Age `5hlh zue, To r P0Ddallei fie,, rcc � kucsei errterb elegies, Pekeartomt, Blchon BAAl65, Pomcr.onlarrs UKC 81 Terriers. Credlr Cards S200-3800 Ctegpldd. 8-397.4891 ar-�41 1n the DIY M t=l,arl, y d MCC NauRin, Blalh Garotte, aril being mare perLet4arlY OraCrIbed as !pions ALL OFLOT38 NBLOCK in0KF0000TPAW'NCi0:T7rra.,l sA1E la SHOWN ON MAP THEREOF iN MAP 1300K 15, PAOE MECKLENBURG FUSUC RE0ISTRy Adrhne Mwropwhy; ?214 grammes, Road, Cr1N16ea, NC 28218 ati,.olmesole we0,adwred n L,Stabod t 9 add la sash 10 the P °eO�gle Toon" rg,9lyre the tight to reouira g� alb, o o �ibs* cheek 9 Toon" to Htheu yr of w I aA tthu amount c the not to Flap 0oeere rc7m ) n� hetherodth of he bid er Older le axe i from ayloo 1... In the arm(* w the Gamer rev AP PwInO oho Sam.. the axoahaM Wrld,r die Oros PorpW. vein ) e1 the °mann of O e do or e rn Hrxfarad Flay Dollen 0750, , In On event Oral oho Owner Tire b h t from paying the ttem. the 111 bidder led, t71S 15 sy also t» J b Went.? ,landed Ott required y(N. D,gdh I"b y Lend Tart and Tar sod the tat tegtagd by N.Qti S. rase �1 tAr3pi (Al (I). n upset cos Legal Notions 7 Nt719DE OF atuesrnv TRUSTEES FCkiECU3suRE Littler And Ono. of the OF REAL PROP ,•Kits Litt o M al That me 9 per and authority contained In diet do Cogan eL,ADCI and Ceflyargd rN A. Byron Zallar, 9 And win windy Aan avker, detect Its Mey Id,1008 end recorded In the Ottce of me spieler a Deeds rx Mevkler ,n Saw,/,InBtrep887alpapaOa52,ra,..ora,atlor,Ma 1q Saw, 7O3T9 et recta lag; 0r,d twrauae altlglelAt In erg ktdebteetga iennee theist. and ral ,o to pot 81���yyTtpttttOf the selpululdar end wanementr eerie /non therein ono, put n to Derail♦ Of be owner end Moiler Wine Inivplednee6 eared b at lObOorauc .1119ion undgral3nod Subeftu1e Trualoe WI pica at 010 Room 101 Of o the hTT a Civlet bldder t8uI o t et it: u.l4 hortotte, MgMOenb Count,/ n0In cEeat41 8 Comae., .e 1:00 remote p.m oh Friday, Ina tout die/ d ' Oa MN pered of Mad, inceideno 1 mprovmrtefke ■hutron, MtJa nand being In the City of Charred tit County of Mock:a lbu Horne Ca ria, and 1100g more particularly dOIC,1 J m ksl� t0. Block to, Perk irdgb 91C, It46P Book la pp 128. net pppvrtY t reinebows deedbed ttl This Da�Ii00E�k�11►rterElft Is Prrd wAt be deal wWsd berg ^OI^ we , e d a etashe e19 b.,w conarEiorn melt ha Del blW ea by teYI 'red, Open fatal (1D) deyd for mead is the 151h awe! fecember. 2002. mean; Yei realpropertyaher o 000 01 oe c fa hdno one+nd for a.). • lama, and epagal ra ahel �r lb HI rlor Lrlgo Ovvnt CaneCorsopubples, Rao charm, b ltllns. 704.413-15d6 CKCig�R,�e,by,, ChIntrehuel,, long hoe lS2sg t �0°46-•rri s ere C chlhuahu & shin- u 370a. so3-vaS-soee flea Aden: Areiafrvoeputy Clerk 01$uperb: Court • • =�10i rfut, 1.57s^ 4185-70e certain, l iiet NOTICE OF 8Ua$Tii11tE TRUS1F tOREC1DSURe Sane OP will h red proehvlelnebOV9 oeaar1bed b alto Oared for ado . WHERE Jr1 and will be add euHact to al rler 11 tees, war Spacial eeeemmenn. Other 0cnd a MI be MOW at be sale. The Me will be held open for ten (tat d9ye for bids ea by law rot 0!,,d. the 1550i dry of Wm:robe; 200s. Knlem a P.nit. PA. $50etWre lhi6,ae i b3U.IgmU 8 Rego CK DUDDilt i(e11 h Path P.A. LAVAS gybathae mew. • Adakrur VDdooly Clerk d Superior Coln 193 • Chibuehua eke Toy female 7w1ss ell shots,Via0.00 �. 794-711Y-6 Call 0 Teo Cup & Toy e M 6 F iioe&upee20-657•aon AKA Sher• Pa Nee, 701-91t3-247,er -784 20i p9 p6her=Pelrs. AKC reg., kit si57`1'77 6 2498rrterr, ordSpar-iioNNel, bISUIIi 1, 1u wk 885850f ,call 704-sgx46-�107 Ines AKCC cd11a Pups, 2 Nners, wlllge 6 L 7 wad old Dn 12725, treble, Mid merle, tr1•color. tell hove 1snoro,°� rl000 ube(to; 3oenorolIl9nsar o��. 70f431-8875 It Border GasslliCCe pc, ,,(ready for o1df - o- 76det nci . : TOTHL PRGE.02 ** County Mecklenburg NPDES Permit Number NC0004375, Mount Holly East (MHE) Facility, PO Box 669246, Charlotte, NC 28266 has applied for a for a facility located in Mecklenburg County discharging treated wastewater into CATAWBA RIVER in the CATAWBA River Basin. Currently are water quality limited. This discharge may affect future allocations in this portion of the receiving stream. TIMEScI�g 1 Charlotte, N.C. AFFIDAVIT OF PUBLICATION NORTH CAROLINA MECKLENBURG COUNTY Before the undersigned, allotary Public of Mecklenburg County, North Carolina, duly commissioned, qualified, and authorized by law to administer oaths, personally appeared Shelby J. Cumming: THE Mecklenburg TIMES, a newspape entered as second-class mail inihe City of and State; that he/she is authorized to make statement; that the notice or other legal ad PUBLIC NOTICE STATE OF NORTH CAROLI ENVIRONMENTAL MANAGEN NOTIFICATION OF INTER WASTEWATER PERMIT atrue copy of which is attached hereto, was lenburg TIMES on the following dates: DEc. 17, 2002 and that the said newspaper in which such or legal advertisement was published was every such publication, a newspaper meetu and qualifications of Section 1-597 of the t Carolina and was a qualified newspaper wi lion 1-597 of the General Statutes ofNort This (Signed) 17th day of Dec. Sworn to and subscribe -c PUBLIC NOTICE STATE OF NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION/NPDES UNIT 1617 MAIL SERVICE CENTER RALEIGH, NC 27699-1617 NOTIFICATION OF INTENTTO ISSUEA NPDES WASTEWATER PERMIT On the basis of thorough staff review and application of NC General Statute 143.21, Public law 92. 500 and other lawful standards and regulations, the North Carolina Environmental Management Com• mission proposes to issue a National Pollutant Discharge Elimination System (NPDES) wastewater discharge permit to the person(s) listed below effective 45 days from the publish date of this notice. Written comments regarding the proposed permit will be accepted until 30 days after the publish date of this notice. All comments received prior to that date are considered in the final determinations regarding the proposed permit. The Director of the NC Division of Water Quality may decide to hold public meeting for the proposed permit should the Division receive a significant degree of publi interest. Copies of the draft permit and other supporting information on file used to determine condition present in the draft permit are available upon request and payment of the costs of reproduction. Mai comments and/or requests for information to the NC Division of Water Quality at the above address o call Ms. Valery Stephens at (919) 733-5083, extension 520. Please include the NPDES permit numbe (attached) in any communication. Interested persons may also visit the Division of Water Quality at 51 N. Salisbury Street, Raleigh, NC 27604-1148 between the hours of 8:00 a.m. and 5:00 p.m. to revie information on file. NPDES Permit Number NC0004375, Mount Holly East (MHE) Facility, PO Box 669246, Charlotte, N 28266 has applied for a facility located in Mecklenburg County discharging wastewater into CATAWBA RIVER in the CATAWBA River Basin. Currently are water quality limited. This discharge may affec future allocations in this portion of the receiving stream. 104100 Dec 17 efoteine, this-- . - -- -- 7th day of Dec. 20p2 CA r Notary Public ommission Expires: 7 17 / 2004 41 a c s 2 w C Re: NC0004375 Clariant - Factsheet Amendment Subject: Re: NC0004375 Clariant - Factsheet Amendment Date: Thu, 21 Nov 2002 08:19:44 -0500 From: Hyatt.Marshall@epamail.epa.gov To: jackie.nowell@ncmail.net thanks for sending. have no problems with this. know you'll be glad to issue this one soon. Marshall 1 of 1 11/21/02 10:07 AM NC0004375 — Clariant Corporation Factsheet Amendment 11/20/02 Upon additional review by the NPDES Unit, the following items have been addressed and modified in the final Clariant permit. 1. The sentence: "The Division will need to assess the necessity for the entire 3.9 MGD flow requirement upon the next renewal of the Clariant permit on June 30, 2005. " will be added to the text of the permit cover letter. 2. The new DWQ DMR form for sampling PPA data will be attached to the cover letter. The sentence at the bottom of the PPA condition Section A.(6.) has been modified to say that "two copies of the report will be sent to DWQ Central Files...." This replaces having the PPA form sent to the NPDES Unit and the Compliance Enforcement Unit. Central Files retains all permit effluent data, therefore information should be sent directly there. 3. The nutrient worksheet will also be attached to the letter instead of being included as a page in the permit. 4. An email was sent to Bob Sledge and Shannon Langley in the Compliance Unit addressing the issue of their notification about the addition of the new wastestream. He indicated that the Unit had no problem with the condition being included in the permit. Updating the Tier 2 effluent limitations in the information database will be addressed upon receipt. 11/20/2002 Notes to Clariant File: 1. The special staging requirement for discharge. A research of the Clariant file found a 12/5/96 memo from the DWQ Instream Assessment Unit (IAU) addressing Clariant's 1998 challenge of several conditions found in the permit. IAU concurred that the staging requirement was not consistent with the BOD5 and NH3 effluent limits in the permit, and that because of the lower BOD5 limit there should be a modification. The response memo states that "The case scenario where the river flow is greater than 175 cfs and less than 250 cfs is no longer necessary because the combination of the revised BOD5 and NH3 limits would be much lower than the allowable 1044 lb/day. Since the new guidelines or limits are low, the equation is only needed when the river flow is less than or equal to 175 cfs." The only scenario needed is as follows: River flow < 175 cfs, BOD5 + 0.54 NH3 < 566.41b/day Explanation for BOD5 + 0.54 NH3 < 566.41b/day Permitted BOD5 limits, Tier 1 - 329.0 #/d (mo. avg.) 810 #/d (da. max.); Tier 2 - 485.0 #/d (mo. avg.) 1215 #/d (da. max.) Permitted NH3 limits, Tier 1 & 2 - 618 #/d (mo. avg.) 927 #/d (da. max.) Using monthly averages 1) 329 + 0.54 (618) = 329 + 333.72 = 662.72 is not < 566.4 2) 485 + 0.54 (618) = 485 + 333.72 = 818.72 is not <566.4 Using daily maximums 1) 810 + 0.54 (927) = 810 + 500.58 = 1310.58 is not < 1044 #/d 2) 1215 + 0.54 (927) = 1215 + 500.58 = 1715.58 is not < 1044 #/d DAG would like to remove this requirement. However, further research needs to be done on the staging requirement, its history and whether it should remain a part of the permit. This should be reviewed more thoroughly upon next permit renewal. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION 4 ATLANTA FEDERAL CENTER 61 FORSYTH STREET ATLANTA, GEORGIA 30303-8960 OCT 0 9 'W'IJI Ms. Jackie Nowell North Carolina Department of Environment and Natural Resources Division of Water Quality NPDES Unit 1617 Mail Service Center Raleigh, NC 27699-1617 OCT 1 1 2Cn2 SUBJ: Draft NPDES Permit for Clariant Corp. NC0004375 Dear Ms. Nowell: In accordance with the EPA/NCDENR MOA, we have completed review of the draft permit specified above and have no comments or objections to its conditions. We request that we be afforded an additional review opportunity only if significant changes are made to the draft permit prior to issuance or if significant comments regarding the draft permit are received. Otherwise, please send us one copy of the final permit when issued. If you have any questions, please call me at (404) 562-9304. Sincerely, Marshall Hyatt, Environmental Scientist Permits, Grants and Technical Assistance Branch Water Management Division Internet Address (URL) • http://www.epa.gov Recycled/Recyclable • Printed with Vegetable Oil Based Inks on Recycled Paper (Minimum 30% Postconsumer) Re: comments on NC0004375 - Clariant Y Subject: Re: comments on NC0004375 - Clariant Date: Tue, 08 Oct 2002 16:44:22 -0400 From: Hyatt.Marshall@epamail.epa.gov To: Jackie Nowell <jackie.nowell@ncmail.net> thanks for getting back to me and for your responses. I will send you a no comment letter. Marshall 1 of 1 10/9/02 7:43 AM Re: comments on NC0004375 - Clariant Subject: Re: comments on NC0004375 - Clariant Date: Tue, 08 Oct 2002 16:39:30 -0400 From: Jackie Nowell <jackie.nowell@ncmail.net> Organization: NC DENR DWQ To: Hyatt.Marshall@epamail.epa.gov CC: Dave Goodrich <Dave.Goodrich@ncmail.net> Hello Marshall, thanks for your comments. The typographical errors that you submitted will be corrected.: a. In Section A(1)a, in footnote 5, "Section A(5)" should be Section A(6). ( Your note said footnote 4 but I think the staging requirement is footnote 5) . b. In Section A(1)b, in the Effluent Characteristics column for BOD, the footnote will be corrected to 5. c. In Section A(1)b, in footnote 5, "Section A(5)" should be Section A(6). see (a) . d. Regarding the DO monitoring requirement. This is a renewal of the existing monitoring requirement for DO for the last permit issued in 1996. The 1991 factsheet indicated that a DO limit with a minimum of 5 mg/1 was a part of the permit, but the 1991 permit issued did not have DO limited. With the current renewal, a review of instream DO data for the past three years showed no violations of the 5 mg/1 DO standard downstream of the Clariant facility. It would not appear that an effluent DO limit is necessary. e. You are correct that Hg should be sampled as a grab instead of composite. A letter to the facility about the new method 1631 will clarify this and it will be corrected in the final permit. f. According to 15A NCAC 2B. 0505(c)(3)(C), chlorides is not one of the parameters listed that should be grab sample. It is not a volatile and should be sampled as composite. g. Clariant has agreed to the addition of a condition/permit language that they will notify DWQ at least 14 days prior to the addition of any new waste source to the treatment facility. Please contact me if there are any additional comments or questions. Thank you. Hyatt,Marshall@epamail.epa.gov wrote: > hope these are useful. will you be able to respond to these by Oct 9, > so I have time to prepare a comment letter if needed? thanks Marshall > Section A(1)a: > - In footnote 5, "Section A(5)" should be "Section A(6) ". > - the previous draft permit had an effluent DO limit of 5.0 mg/1; this > draft does not. It seems strange that ammonia and BOD5 limits here are > water quality -based to protect DO, but there is no effluent DO limit. > Pis explain. > - re Hg, if/when the facility begins using Method 1631, shouldn't the > sample type be grab, rather than composite? this applies to Hg in other 1 of 2 10/9/02 8:28 AM Re: comments on NC0004375 - Clariant > parts of the permit also. > > - shouldn't chlorides sampling be grab, rather than composite? this > applies to chlorides in other parts of the permit. > > Section A (1) b: > > - in the effluent characteristics column for BOD, it should be footnote > "4„ not "5". > > - In footnote 5, "Section A (5) " should be "Section A(6) ". > > re any Tier 2 limits, is there a need to add language to the permit that > says the permittee must notify the Division 30? 14? _ days before a > new wastewater discharge begins? 2 of 10/9/02 8:28 AM NCDENR MRO NCDENR'DWO Fax:7046636040 Fax:919-733-0719 Oct 10 2002 14:03 P.02 Oct 9 '02 9:16 P.31/31 Regional Office Comment veS (fit 0-r,f0 sTEI s11?fi�w�� At'i�� °i� BfrS � �'S 'f'�(� fJvJJ.� l�L.���! G✓1'9"1�7� _ PLO iiz,g 4/ 2,4 /Jo n1 �► _ �/ LU4E1 TIN l- fit: I -Tao /� � a /fir a G ::7;i1( W-°,1(7),44/ 649g .57-8&0 D/54.mie6E-- F./9-6/6/7y /Afczo9b,./6 aw.9 f '. 'Al c-T-V 0 -5-646-&- 171-PZ-0/A/6 7;9)4)/<5 LUG/ SG� �Rzssr�s' NAME tf 4 B��-C-K4 ,CRATE: Fuel. SViaec 4'T ES 1Lcncwa1 ragG 10 NCDENR riR0 Fax:7046636040 Oct 10 2002 14:03 P.01 .Date.: /ro --i o - ° ,� r' K [ Aio G r ax Number 9 iq 3 -3 —Or/ I R Message: 5 4/, k�. c CQ /ou AVA NCDENR North •Carolina .Department of Environment :and 'Natural Resources Mooresville :Regional Office 919 North Main Street Mooresville, .North Carolina .28115 Phone; 7D4/6e3-1 699 Fax; 704/663-6O4O From: c5i1-011 ' ° t, lDiv! Section: CDC '._ !'umber of pages (Intl_ c:vr) Department of Environment and Natural Resources Division of Water Quality Fact Sheet For NPDES Permit NC0004375 Facility Information Applicant/Facility Namel: Applicant Address': Facility Address': Permitted Flow': Type of Waste': Facility/Permit Status': County': Miscellaneous Receiving Stream': Stream Classification: 303(d) Listed?2: Subbasin2: Drainage Area (mi2): [calculated] Summer 7Q 10 (cfs): 30Q2 (cfs): Average Flow (cfs): IWC (%): Primary SIC Code: Regional Office: USGS Topo Quad: Permit Writer: Date: Summary Clariant Corporation - Mt. Holly P.O. Box 669246, Charlotte, NC 28266 11701 Mount Holly Road, Charlotte, NC 28214 3.9 MGD (Grade IV - Biological) Industrial Renewal Mecklenburg 03-08-34 40.8 mi2 329 cfs 716 cfs 3016 cfs 1.8% 2865 Mooresville Mountain Island Lake & Mount Holly Jackie Nowell September 4, 2002 Clariant operates a specialty chemical and dye manufacturing facility in Mount Holly, North Carolina (Clariant-Mt. Holly East Plant) in the Northwest portion of Mecklenburg County. Wastewater from the facility is treated in an on -site wastewater treatment plant (WWTP) and discharged to the Catawba River under NPDES Permit No. NC0004375. The permit allows a discharge of up to 3.9 MGD of treated industrial wastewater through one outfall (001). Clariant has submitted an application for renewal of this NPDES permit. The NPDES Unit has reviewed the application, correspondence files, discharge monitoring reports, permit files, instream data and other pertinent data in developing this permit. This fact sheet summarizes the rationale used to determine permit limits and conditions. Wastewater from the Clariant Corporation facility is treated in the on -site WWTP. The treatment plant is comprised of the following treatment units: • Two separate sewer systems, acid sewer and alkaline sewer. • Acid sewer lift station pumps. • Alkaline sewer lift station pumps. • 2.5 MG lined equalization basins for non -alkaline wastewater. • 3.5 MG lined equalization basins for alkaline sewer wastewater. • Two pH neutralization tanks with lime slurry addition. • Two primary clarifiers. • One 4.5 MG equalization basin with mixers and aerators. • One 2.5 MG activated sludge aeration basin with jet mixing and aerators. • Two secondary clarifiers. Fact Sheet NPDES Renewal Page 1 c • Two sludge holding tanks for primary and secondary sludge. • Two belt filter presses. • Effluent polishing canal that flows to a small final exit pond that has an aerator in it to provide positive dissolved oxygen prior to release into the Catawba River. • Staged discharge facility that includes an effluent lift station can deliver the entire effluent flow of the WWTP to a lined 360 MG effluent holding basin for storage and pretreatment. The last wasteload allocation was conducted in 1991. Since that time, there have been changes that would dictate a reevaluation of the wasteload allocation. The facility's existing permit incorporates water quality based limits for ammonia, acenaphthene, acenaphthylene, anthracene, benzo(a)anthracene, 3,4-benzofluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, chrysene, fluorene, naphthalene, phenanthrene and pyrene. Monitoring is also performed on various other parameters including dissolved oxygen, fecal coliform, total nitrogen, total phosphorus, total phenols, total sulfate, chemical oxygen demand, methylene blue active substances, iron, chlorides and mercury. The existing permit also includes limits for a variety of organic chemicals as required by the US EPA for OCPSF categorical dischargers. These chemicals are: acrylonitrile, benzene, bis(2-ethylhexyl)phthalate, carbon tetrachloride, chlorobenzene, chloroethane, chloroform, 2-chlorophenol, di-n-butyl phthalate, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, 1,1-dichloroethane, 1,2-dichloroethane, 1,1-dichloroethylene, 1,2-trans-dichloroethylene, 2,4-dichlorophenol, 1,2- dichloropropane, 1,3-dichloropropylene, diethyl phthalate, 2,4-dimethylphenol, dimethyl phthalate, 4,6-dinitro-o-cresol, 2,4-dinitrophenol, 2,4-dinitrotoluene, 2,6-dinitrotoluene, ethylbenzene, fluoranthene, hexachlorobenzene, hexachlorobutadiene, hexachloroethane, methyl Chloride, methylene chloride, nitrobenzene, 2-nitrophenol, 4-nitrophenol, phenol, tetrachloroethylene, toluene, total cyanide, 1,2,4-trichlorobenzene, 1,1,1-trichloroethane, 1,1,2- trichloroethane, trichloroethylene, vinyl chloride. Facility Description Clariant operates one remaining textile chemical and dyestuff plant within the complex. This plant will be shut down prior to January 1, 2003. Other OCPSF activities are continuing. Clariant has no plans to modify any of the on -site WWTP processes or components. Although changes are planned for the site manufacturing and warehousing operations, the wastewater to be produced is compatible with existing WWTP design. Clariant is converting the underutilized portions of the Clariant-Mt. Holly East facility into an industrial park, as space becomes available. Wastewater present or planned for immediate inclusion are from the following industrial categories of the US EPA Effluent Guidelines and Standards: • Organic Chemicals, Plastics and Synthetic Fibers (OCPSF) (40 CFR Part 414); • Centralized Waste Treatment (CWT) Point Source (40 CFR Part 437); and • Non -categorical industrial wastewaters. Discharge Monitoring Report Data Review According to the self -monitoring data, the facility is achieving compliance with the current permit limits. Current Stream Conditions The Catawba River flows from western North Carolina into Lake Wylie. The Catawba River is in the Catawba River drainage area. The Catawba River is classified as a class WS-IV CA water in the Catawba River Basin (North Carolina's classification system), which means it is a protected water supply and is designated for drinking water. The Catawba River is not listed as an impaired water according to North Carolina's draft 2000 303(d) list. Fact Sheet NPDES Renewal Page 2 G Instream Monitoring Clariant conducts monitoring of the Catawba River, both upstream and downstream of the WWTP discharge. Analysis of approximately 3 years of instream data (1989 - 2002), shows no violations of North Carolina's dissolved oxygen standard. Fact Sheet NPDES Renewal Page 3 Compliance Summary Staff Reports indicate that the facility is well maintained and operated. The Clariant Corporation WWTP has a very good compliance record. Over the past three years, the facility had no violations of monthly average limits. Toxicity Testing Current Requirement: Chronic toxicity limit monitored quarterly @ 1.8%. The facility has a good toxicity compliance record over the past six years. Recommended Requirement: Chronic toxicity limit monitored quarterly @ 1.8%. Toxicant Analysis Using the self monitoring data required per the NPDES permit and the approved Long Term Monitoring Plan, reasonable potential analysis' were conducted on the following toxicants: iron, manganese, chloride, mercury, total phenols and total sulfate. The standards used for the analysis are consistent with the standards for a class WS-IV stream. Refer to the proposed changes section to see results. PROPOSED WATER QUALITY BASED LIMITS This permit contains water quality based limits for ammonia, dissolved oxygen, benzo(a)anthracene, benzo(a)pyrene, 3,4-benzofluoranthene, benzo(k)fluoranthene, chrysene, acenaphthylene, acenaphthene, anthracene, fluorene, phenanthrene, pyrene, naphthalene and toxicity. PROPOSED TECHNOLOGY BASED LIMITS This permit contains technology based limits for pH, oxygen demand, total suspended solids, acrylonitrile, benzene, carbon tetrachloride, chlorobenzene, chloroethane, chloroform, 2- chlorophenol, di-n-butyl phthalate, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4- dichlorobenzene, 1,1-dichloroethane, 1,2-dichloroethane, 1,1-dichloroethylene, 1,2-trans- dichloroethylene, 2,4-dichlorophenol, 1,2-dichloropropane, 1,3-dichloropropylene, diethyl phthalate, 2,4-dimethylphenol, dimethyl phthalate, 4,6-dinitro-o-cresol, 2,4-dinitrophenol, 2,4- dinitrotoluene, 2,6-dinitrotoluene, ethylbenzene, hexachlorobenzene, hexachlorobutadiene, hexachloroethane, methyl chloride, methylene chloride, nitrobenzene, 2-nitrophenol, 4- nitrophenol, tetrachloroethylene, toluene, total cyanide, 1,2,4-trichlorobenzene, 1,1,1- trichloroethane, 1,1,2-trichloroethane, trichloroethylene, vinyl chloride, total antimony, total arsenic, total barium, total cadmium, total cobalt, total mercury, total molybdenum, total selenium, total silver, total tin, total titanium, total vanadium, acetone, acetophenone, aniline, 2-butanone, butylbenzyl phthalate, carbazole, o-cresol, p-cresol, n-decane, 2,3- dischloroaniline, n-octadecane, pyridine, 2,4,6-trichlorophenol, bis(2-ethylhexyl)phthalate, total chromium, total copper, fluoranthene, total lead, total nickel, total phenol and total zinc. Fact Sheet NPDES Renewal Page 4 tr Proposed Changes Since Clariant is developing the facility as an industrial park for compatible industrial operations, future wastewater sources will occur. In order to account for these future wastewater sources in the permit effluent limits, a tiered approach to developing the limits was used. The proposed limits for both conventional and non -conventional parameters are presented in two tiers, Tier 1 and Tier 2. The Tier 1 limits are based on wastewater flow from existing and planned wastewater sources. The Tier 2 limits are based on wastewater flow not only from existing and planned wastewater sources, but also from future wastewater sources. Tier 2 limits become effective when any new wastewater source, beyond the existing and planned wastewater sources, is added. Most of the NPDES permit limits for the facility have been significantly reduced compared to current limits due to the planned changes at the Clariant facility. The daily maximum limits and monthly maximum limits for the following parameters have been significantly reduced: 5-day biochemical oxygen demand (43% reduction), total suspended solids (44% reduction), ammonia -nitrogen (5% reduction) and fifty-three (53) OCPSF parameters (59 to 81% reduction). The monitoring frequency for total iron, MBAS, manganese, sulfates and chlorides have been reduced from monthly to quarterly based on results of the reasonable potential analysis that indicated that no violation of the water quality standard should occur from the discharge.. Daily maximum limits and monthly average limits for twenty-five (25) CWT parameters have been added. These include limits for the following: total antimony, total arsenic, total barium, total cadmium, total chromium, total cobalt, total copper, total lead, total mercury, total molybdenum, total nickel, total selenium, total silver, total tin, total titanium, total vanadium, total zinc, acetone, acetophenone, aniline, bis(2-ethylhexyl)phthalate, 2-butanone, butylbenzyl phthalate, carbazole, o-cresol, p-cresol, n-decane, 2,3-dschloroaniline, fluoranthene, n- octadecane, phenol, pyridine and 2,4,6-trichlorophenol. The monitoring frequency for OCPSF parameters has been reduced from quarterly to annually. However, should any annual monitoring result in detection of an OCPSF parameter, then quarterly monitoring must be performed until four consecutive quarterly samples result in non - detection. Monthly monitoring for chromium and zinc have been added to the permit based on new wastewater streams from Seaboard Container Cleaning and SCR -Tech that indicate their presence. Annual average effluent limitations for total nitrogen and total phosphorus have added to the permit based on the Catawba River Basin Management Plan for nutrient protection in the Lake Wylie watershed. These are interim limits based on current information from the facility. A special condition has been added to the permit that will require that Clariant will conduct a BAT study for the development of more accurate nutrient limits in 2003. Mercury continues to be a water quality concern throughout North Carolina. Holders of NPDES permits have worked with the state to reduce potential risks from this pollutant, including tasks associated with collecting and reporting more accurate data. The most commonly used laboratory analysis (EPA Method 245.1) has a detection limit of 0.2 ug/L while the current water quality standard is an order of magnitude lower at 0.012 ug/L. A more recently approved analytical test (EPA Method 1631) should produce a detection limit below the level of the standard. This will allow the Division to assess potential water quality impacts from discharges more accurately. Therefore, beginning on or before September 1, 2003, you will be reciuired to begin using EPA Method 1631 when analyzing for mercury. Instream monitoring for GODS and NH3 have been deleted based on review of data, showing no impact on water quality in the Catawba River. Fact Sheet NPDES Renewal Page 5 ADMINISTRATIVE PROCEDURES 15A NCAC 02H .0109 PUBLIC NOTICE (a) Notice of Application (1) Public notice of each complete individual NPDES permit application and each general NPDES permit shall be circulated in the geographical areas of the proposed discharge by the Director at least 45 days prior to any proposed fmal action: (A) by publishing the notice one time in a newspaper having general circulation in said county; and (B) by mailing the notice to all persons or agencies listed in Subsection (c) of this Rule. (2) The notice shall set forth at least the following: (A) name, address, and phone number of the agency issuing the public notice; (B) name and address of each applicant; (C) brief description of each applicant's activities or operations which result in the discharge described in the NPDES application; (D) name of waterway to which each discharge is made and a short description of the location of each discharge on the waterway indicating whether such discharge is a new or an existing discharge; (E) a statement of the tentative determination to issue or deny an NPDES permit for the discharge described in the NPDES application; (F) a brief description of the procedures for the formulation of final determinations, including a 30-day comment period and any other means by which interested persons may influence or comment upon the determinations; and (G) address and phone number of state agency premises at which interested persons may obtain further information, request a copy of the draft permit, request a copy of the fact sheet, and inspect and copy NPDES application forms and related documents. Copies of the fact sheet shall be made available free upon request. Copies of the information on file, other than fact sheets, will be made available upon request and payment of the cost of reproduction. (3) Public notice for those activities covered by Certificates of Coverage issued pursuant to a general permit and Authorizations to Construct shall not be required. (b) Notice of Public Meeting (1) Notice of public meeting on any NPDES permit application shall be circulated in the geographical areas of the proposed discharge by the Director at least 30 days prior to the date of the meeting: (A) by publishing the notice one time in a newspaper having general circulation in said county; (B) by mailing the notice to all persons and government agencies which received a copy of the notice or the fact sheet for the NPDES application; and (C) by mailing the notice to any person or group upon request. (2) The notice of any public meeting shall include at least the following: (A) name, address, and phone number of agency holding the public meeting; (B) name and address of each applicant whose application will be considered at the meeting; (C) name of waterway to which each discharge is made and a short description of the location of each discharge on the waterway; (D) a brief reference to the public notice issued for each NPDES application including identification number and date of issuance; (E) information regarding the time and location for the meeting; (F) the purpose of the meeting; (G) address and phone number of premises at which interested persons may obtain further information, request a copy of each draft NPDES permit, request a copy of each fact sheet, and inspect and copy NPDES forms and related documents; and Fact Sheet NPDES Renewal Page 6 (H) a brief description of the nature of the meeting including the rules and procedures to be followed; The notice shall also state that additional information is on file with the Division of Environmental Management, Department of Environment, Health, and Natural Resources at the Archdale Building at 512 North Salisbury Street, Raleigh, North Carolina, and may be inspected at any time during normal working hours. Copies of the information on file will be made available upon request and payment of cost of reproduction. (c) Mailing Lists. Any person may request to receive copies of all notices required under this Rule and the Director shall mail such notice to any such person. An annual charge of twenty- five dollars ($25.00) may be charged for any person desiring to be placed and maintained on the NPDES Permit mailing list. The Director shall also give notice to the following for NPDES permits: (1) State water pollution control agency for the States of Virginia, South Carolina, Tennessee, and Georgia; (2) Appropriate district engineer, U.S. Army Corps of Engineers; (3) Lead agency responsible for preparation of plan pursuant to Section 208(b) of the Clean Water Act, 33 U.S.C. Section 1251 et seq, in approved 208 areas; (4) State agency responsible for the preparation of plans pursuant to Section 303(e) of the Clean Water Act, 33 U.S.C. Section 1251 et seq; (5) North Carolina Department of Environment, Health, and Natural Resources, Division of Environmental Health; and (6) Any other federal, state, or local agency upon request. History Note: Authority G.S. 143-215.1(a) (1); 143-215.1(c); 143-215.4(a); 143-215.4(c); Eff. February 1, 1976; Amended Eff. March 1, 1993; August 1, 1988; October 1, 1987; December 1, 1984. 15A NCAC 02H .0111 MEETINGS AND HEARINGS (a) Public Meetings: (1) The Director shall provide an opportunity for the applicant, any affected state, any affected interstate agency, the regional administrator, or any interested agency, person, or group of persons to request or petition for a public meeting with respect to NPDES permit applications. Any person who desires a public meeting on any NPDES permit application shall so request in writing to the Director within 30 days following the publication date of the notice of application. Any such request or petition for public meeting shall indicate the interest of the party filing such request and the reasons why a meeting is warranted. (2) The Director is delegated authority to determine if a public meeting shall be held in accordance with G.S. 143-215.1(c) (3) and to issue public notice and conduct such meeting for the Commission. (3) All comments received within 30 days following the publication date of the notice of NPDES permit application shall be made part of the application file and shall be considered by the Director prior to taking final action on the application. (4) Any meeting brought pursuant to this Subsection shall be held in the geographical area of the proposed discharge or other appropriate area, in the discretion of the Director, and may, as appropriate, consider related groups of permit applications. (b) Adjudicatory Hearings and appeals shall be conducted in accordance with Article 3 of Chapter 150B of the General Statutes. History Note: Authority G.S. 143-215.3(a)(1); 143-215.1(c)(1); 143-215.3(a)(3); 143-215.3(a)(4); 143-215.5; 143-215.1(e); Eff. February 1, 1976; Amended Eff. March 1, 1993; November 1, 1987. 15A NCAC 02H .0112 FINAL ACTION ON PERMIT APPLICATIONS Fact Sheet NPDES Renewal Page 7 (a) The Director shall take final action on all NPDES applications not later than 60 days following notice of intent to issue or deny, or, if a public meeting is held, within 90 days following the closing of the record of the meeting or in the case of an Authorization to Construct permit 90 days after the receipt of a complete application or, if a public meeting is held concerning the Authorization to Construct, within 90 days following the closing of the record of the meeting. (b) The Director is authorized to: (1) issue a permit containing such conditions as are necessary to effectuate the purposes of G.S. 143-215.1 and G.S. 143-215.67; (2) issue a permit containing time schedules for achieving compliance with applicable effluent standards and limitations, water quality standards, and other legally applicable requirements; (3) modify or revoke any permit upon giving 60 days notice to the person affected pursuant to Rule .0114(a) of this Section; (4) suspend a permit pursuant to Rule .0114(a) of this Section; (5) rescind a permit upon request by the permittee; (6) deny a permit application: (A) where necessary to effectuate the purposes of Article 21 Chapter 143, (B) for a discharge prohibited by G.S. 143-214.2(a), (C) where the Secretary of the Army fmds the discharge would substantially impair anchorage and navigation, (D) for a discharge to which the regional administrator of EPA has objected as provided in Section 402(d) of the Clean Water Act as amended, 33 U.S.C. Section 1251 et seq, (E) for any point discharge which conflicts with a plan approved pursuant to Section 208(b) of the Clean Water Act as amended, 33 U.S.C. Section 1251 et seq, effective February 4, 1987. (c) The permit applicant has the burden of providing sufficient evidence to reasonably ensure that the proposed system will comply with all applicable water quality standards and requirements. No permit may be issued when the imposition of conditions cannot reasonably ensure compliance with applicable water quality standards and regulations of all affected states. (d) Permits shall be issued or renewed for a period of time deemed reasonable by the Director except in no case shall permits be issued for a period to exceed five years. History Note: Authority G.S. 143-215.3(a)(1); 143-215.1(c)(4); 143-215.1(b); 143-215.3(a)(3); 143-215.3(a)(4); 143-215.1(c)(5); 143-214.2(a); 143-215; 143-215.2(a); Eff. February 1, 1976; Amended Eff. March 1, 1993; October 1, 1987; September 1, 1986; December 1, 1984. Proposed Schedule for Permit Issuance Draft Permit to Public Notice: Permit Scheduled to Issue: References September 11, 2002 October 25, 2002 1. 2002. NPDES Permit Application Form 1, Clariant Corporation. 2. 2000. 303(d) List of North Carolina Impaired Waters - Draft. North Carolina Division of Water Quality, Water Quality Section. Copies obtained through Planning Branch, Archdale Building, 512 N. Salisbury St., Raleigh, North Carolina. Fact Sheet NPDES Renewal Page 8 4 State Contact If you have any questions on any of the above information or on the attached permit, please contact ckie Nowell at (919) 733-5038 ext. 512. NAM ) DATE: f/VO Z- NP I SU' RVISOR NAME: DATE: Fact Sheet NPDES Renewal Page 9 fate of North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross, Jr., Secretary Alan W. Klimek, P.E., Director MEMORANDUM Io: From: Subject: V1� SEP ? 5 nr September 4, 2002 Britt Setzer \C DENR / DEH / Regional Engineer Mooresville Regional Office Jackie Nowell NPDES Unit Review of Draft NPDES Permit NC0004375 Clariant Corporation — Mt. Holly East Plant Mecklenburg County NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES • RECEIVED -,, 1 7 2002 NCDENR Division of Environmental Health Public Water Supply Section Mooresville Regional Office Please indicate below your agency's position or viewpoint on the draft permit and return this form by October 4, 2002. If you have any questions on the draft permit, please contact me at the telephone number or e-mail address listed at the bottom of this page. w,v% wNY/Y w w w/VVNV v w wANAN w,^v^„ Y/VV w wA A w w VVi ' w w, V N V w wM/ N w RESPONSE: (Check one) Concur with the issuance of this permit provided the facility is operated and maintained properly. the stated effluent limits are met prior to discharge. and the discharge does not contravene the designated water quality standards. Signed Concurs with issuance of the above permit, provided the following conditions are met: Opposes the issuance of the above permit. based on reasons stated below. or attached: tcf: i; ON Date: q / .24 (` 2__ 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 919 733-5083, extension 512 (fax) 919 733-0719 Visrr us ON THE INTERNET @ httpJ/h2o.enr.state.nc.us/NPDES Jackie.nowell@ ncmail.net Draft lrmit Review-Clariant Corp.-NC0004375 Subject: Draft Permit Review-Clariant Corp: NC0004375 Date: Wed, 11 Sep 2002 15:52:05 -0400 From: Matt Matthews <matt.matthews@ncmail.net> Organization: NC DENR DWQ To: Jackie Nowell <jackie.nowell@ncmail.net> Jackie, I've reviewed the subject draft permit and have one minor comment. The receiving stream classification on the map (WS-III) does not agree with the fact sheet and supplement to permit cover sheet (WS-IV CA). Thanks for the opportunity to comment, Matt Matt Matthews NC DENR/Division of Water Quality Aquatic Toxicology Unit 1621 Mail Service Center Raleigh, North Carolina 27699-1621 v-(919) 733-2136 f-(919) 733-9959 MailTo:Matt.Matthews@ncmail.net A few observations and much reasoning lead to error; many observations and a little reasoning to truth. --Alexis Carrel 1 of 1 9/11/02 3:57 PM Re: Clagiant NC0004375 Subject: Re: Clariant NC0004375 Date: Fri, 15 Nov 2002 14:22:23 -0500 From: Bob Sledge <bob.sledge@ncmail.net> To: Jackie Nowell <jackie.nowell@ncmail.net> CC: Shannon Langley <Shannon.Langley@ncmail.net> Jackie, As we briefly discussed, I don't have any problem with the way this has been written. I just hope they will give us the update when they go ahead with the changes. In the wonderful world of BIMS, I don't know who will actually have the responsibility or authority to make the changes after we get their notification. Thank you, Bob 1 of 1 11/15/02 2:59 PM ti SUMMARY OF CMUD/DWQ/SCDHEC SETTLEMENT AGREEMENT INTRODUCTION In the summer of 2001, the South Carolina Department of Health and Environmental Control (SCDHEC) filed a Petition for a Contested Case in the North Carolina Office of Administrative Hearings regarding the renewal of NPDES Permit No. NC0024970, the Charlotte Mecklenburg Utilities Department (CMUD) McAlpine Creek Wastewater Treatment Plant. The primary complaint on the part of SCDHEC has been that the permit was renewed without a phosphorus limit. Nearly all of South Carolina's municipal dischargers to the mainstem Catawba (upstream of Lake Wateree) have been given phosphorus limits, generally equivalent to 1 mg/L. The McAlpine Creek WWTP permit had a phosphorus optimization study special condition that stipulated preparatory requirements for the facility to ready itself for the upcoming phosphorus Total Maximum Daily Load (TMD). Since the summer, SCDHEC, the North Carolina Division of Water Quality (NCDWQ) and CMUD have been working towards achieving consensus on an appropriate phosphorus limit for the McAlpine Creek WWTP. The understanding has been that this decision will also affect DWQ's permitting strategy for three additional municipal permits: CMUD - Irwin Creek WWTP, CMUD - Sugar Creek WWTP, and Union County - 12-Mile Creek WWTP. The final settlement agreement includes the terms of the limits for all three CMUD plants. A similar strategy will be used by DWQ to limit phosphorus in the Union County permit. SUMMARY OF SETTLEMENT AGREEMENT Limits at McAlpine Creek WWTP Based upon a construction schedule provided by CMUD during the settlement proceedings, the compliance date for the total phosphorus limit at the McAlpine Creek WWTP is set for February 28, 2006. At this time, the McAlpine Creek WWTP must meet a 534 lbs./day total phosphorus limit. This limit is to be calculated as a 12-month rolling average. It corresponds to a 1 mg/L limit at McAlpine Creek's permitted flow of 64 MGD. This limit, as well as the monthly mass cap described below, shall be incorporated into a major modification to NPDES Permit NC0024970 with special condition language to be included with reference to the Irwin and Sugar Creek WWTPs. Since SCDHEC's stipulation was that any limit come into effect prior to the expiration date of the permit, the permit expiration date will also be modified to February 28t, 2006 (instead of June 30, 2005). This puts the permit out of sync with the Basinwide schedule, but is within the five years allowable for a permit term under federal regulations. Bubble Limit A major point of the settlement agreement is the idea of a bubble limit. This refers to a mass limit for total phosphorus that applies to discharge at the three CMUD plants combined. This type of a limit would give CMUD more operational flexibility with regard to phosphorus removal. The bubble limit, to be calculated as a 12-month rolling average, is 826 lbs./day of total phosphorus from all three CMUD plants. This corresponds to a 1 mg/L phosphorus limit at permitted discharge for the three plants. If CMUD conducts construction activities at either the Sugar or Irwin Creek plants, the compliance date for this bubble limit will be February 28, 2007. If CMUD decides not to conduct construction activities at either plant in order to achieve compliance, the bubble limit will come into effect on February 28, 2006. This is identical to the compliance date at the McAlpine Creek plant. Special condition language will be included in the Irwin and Sugar Creek WWTP permits regarding the compliance date. Mass cap In order to be protective of the water quality at the downstream lakes in South Carolina, SCHEC requested that monthly mass caps also be included as part of the total phosphorus limits at the three CMUD plants. This would also ensure optimized operation of the plants at all times. The mass caps at the three plants take the form of a monthly average mass limit and correspond to a concentration limit of 2 mg/L at maximum permitted flow. At McAlpine Creek, this limit is 1,0671bs. /day of total phosphorus beginning February 29, 2006. At the Sugar and Irwin Creek plants, the mass caps only come into effect if construction activities are pursued at each plant. At Sugar Creek WWTP, the limit is 334 lbs./day with compliance commencing on February 28, 2007. At Irwin Creek WWTP, the limit is 250 lbs./day with compliance commencing on February 28, 2007. TMDL As part of the settlement agreement DWQ requested a provision for full inclusion in the TMDL process for both DWQ and all affected NC entities (to be provided in a list by DWQ). APPLICABILITY TO PERMITTING PROCESS The three CMUD permits will have the bubble limit included as a special condition. Monitoring for phosphorus will be included in the regular effluent limit pages. Mass caps will also be included in the effluent limit pages, with a footnote specifying applicability (for Sugar and Irwin Creek plants) and compliance dates. The Union County - 12 Mile Creek WWTP shall have a mass limit equivalent to 1 mg/L at the permitted flow. As with the three CMUD plants, compliance for this limit is to be judged as a rolling annual average. Special monitoring language is being developed for this situation. It is also recommended that the phosphorus optimization study special condition from the original McAlpine Creek WWTP permit be included in this permit to allow DWQ time to review the County's preparations for the impending phosphorus TMDL. NC DENR - DIVISON OF WATER QUALITY 2B .0300 .0308 CATAWBA RIVER BASIN Name of Stream Description Class Classification Date Index No. Johnson Creek CATAWBA RIVER (Mountain Island Lake below elevation 648) McDowell Creek McDowell Creek Caldwell Station Creek Caldwell Station Creek Torrence Creek McDowell Creek Gar Creek Gar Creek CATAWBA RIVER (Lake Wylie below elevation 570) Harwood Lakes and Brinkley Twin Lakes Dutchmans Creek Leepers Creek Sawmill Branch Lippard Creek Link Creek Ore Bank Branch Lick Run From a point 0.6 mile upstream of mouth to Mountain Island Lake, Catawba River WS-IV CA From Water Intake at River WS-IV&B CA Bend Steam Station to Mountain Island Dam (Town of Mount Holly water suppl intake) From source to U.S. Hwy. 2 C From U.S. Hwy. 21 to a WS-IV point 0.7 mile upstream of mouth From source to I-77 C From 1-77 to McDowell Cree From source to McDowell Creek From a point 0.7 mile upstream of mouth to Mountain Island Lake, Catawba River WS-IV WS-IV WS-IV CA From source to a point 0.6 WS-IV mile upstream of mouth From a point 0.6 mile upstream of mouth to Mountain Island Lake, Catawba River WS-IV CA From Mountain Island Dam t WS-IV CA Interstate Highway 85 Bridge at Belmont Entire lakes and connectin streams to Lake Wylie, Catawba River From source to a point 0.8 mile downstream of Taylors Creek From source to a point a point 0.8 mile upstream of mouth From From From From From source source source source source to Leepers to Leepers to Lippard to Leepers to Leepers Cre Cre Cre Cre Cre 29 WS-IV CA WS-IV C 08/03/92 11-113-(2) 08/03/92 11-(114) 09/01/74 11-115-(1) 08/03/92 11-115-(1.5) 09/01/74 11-115-2-(1) 08/03/92 11-115-2-(2) 08/03/92 11-115-4 08/03/92 11-115-(5) 08/03/92 11-116-(1) 08/03/92 11-116-(2) 08/03/92 11-(117) 08/03/92 11-116 08/03/92 11-119-(0.5) 08/03/92 11-119-1-(1) 08/03/92 08/03/92 08/03/92 03/01/62 03/01/62 Whole Effluent Toxicity Testing Self -Monitoring Summary August 16, 20 FACILITY REQUIREMENT YEAR JAN FEB MAR APR MAY JUN JUL AUG SEP OCT NOV DEC Cltgo Petroleum 9002 Perm: 24hr LC50 ac monil epis Mid (grab) 1998 — — — — -- — — — -- NRM NC0021954/002 Begin:7/1/1999 Frequency: 5OWD/A NonComp: 1999 — — — >100 >100 >100 >100 >100 — >700 — County: Johnston Region: RRO Subbasin: NEU02 2000 >100 >100 — — -- -- — — — — -- — PF: VAR Special 2001 — >100 — — — — — — -- — — 7Q10:0.0 IWC(%):100 order: 2002 >100 — — — — — Cltgo-Paw Crk Bulk Terminal Pent: 24hr LC50 ac monit epis 11191(grab) 1998 -- — — >100 — — — -- — — NC00219621001 Begin:9/1/2001 Frequency: A NonComp: 1999 --- — — — >100 — — --- — County: Mecklenburg Region: MRO Subbasin: CTB34 2000 >100 -- -- --- -- -- --- — PF: NA Special 2001 -.. >100 — -- — --- --- — 7Q10:0.0 IWC(%):100 Order: 2002 --- -- -• — Claremont North WWTP Penn chr lim: 13 % N00032662/00I Begin:4/I/2001 Frequency: Q Jan Apr Jul Oct County: Catawba Region: MRO Subbasin: CTB32 PF: 0.10 Special 7Q10: 1.0 IWC(%):13 Order: + NonComp:Single 1998 Pass 1999 Pass 2000 Pass 2001 Pass 2002 Pass,Pass — Pass — -- Pass --- --- Pass — Pass -- Pass — — Pass -- -- Pass -- Pass --- Pass — -• Pass Pass -- — Pass — -- Pass Claremont South WWTP Penn chr lim: 61% NC0026549/001 Begin:4/1/2001 Frequency: Q Jan Apr Jul Oct County: Catawba Region: MRO Subbasin: CTB32 PF: 0.10 Special 7Q10: 0.10 1 WC(%):60.78 Order: + NonComp:Single 1998 1 — — I — -- — — 1999 1 — — 1 — — 2000 I — I -- — — 2001 1 1 ... _. — 2002 N N — Claremont-MeUn Creek WWTP Pem1 chr lim: 9% NC0081370/001 Begin:6/I/2001 Frequency: Q Jan Apr Jul Oct County: Catawba Region: MRO Subbasin: CTB32 PF: 0.3 Special 7Q10: 5.0 IWC(%):9.0 Order: + NonComp:Single 1998 Pass Pass -- Pass — — Pass 1999 Pass -- Pass --- Pass -- — Pass 2000 Pass — -- Pass — Pass — — Pass 2001 pass Pass Pass Pass 2002 Pass -• Pass aeriant Corp: ML Holly Plant PERM CHR LIM: 1.8 % NC0004375/001 Begin:9/I/199I Frequency: Q P/F + Mar Jun Sep Dec County: Mecklenburg Region: MRO Subbasin: CTB34 PF: 3.9 Special 1( 7Q10: 95.0 IWC(%):5.98 , Order: Y 1998 — NonComp:Singk ' 1999 -• 2000 -- 2001 ... 2002 ' -- Pass — Pass — Pass — — Pass Pas§ -- -- Pa0$_, Pass -- Pass Pass — Pass , Pass -- Pass — --- Pass — NR Pass - - NRPass - Pass -- --- Pass Pass --- --- Pass Clarkson WWTP Penn chr lim: 90% NC0021610I001 Begin:12/1/1999 Frequency: Q Jan AprJul Oct County: Bladen Region: FRO Subbasin LUM58 PF: 0.24 Special 7Q10: 0.0 IWC(%):100 Order: + NonComp:Single 1998 Pass — -- Fall 1999 Pass -- — Pass 2000 Fail 94.9 >100 Pass 2001 >100 -• >100 2002 Pass Pass Pass — Pass — — Pass — Fail Pass -- Pass -- -- - Pass — Fail >100 >100 Pass --- Pass -- --- Clayton WWTP Perm chr lint: 1.6% 1998 — — Pass — -- Pass — — Pass -- Pass NC0025453/001 Begin:9/l/2000 Frequency: Q Mar Jun Sep Dec + NonCornp:Single 1999 — Pass — — Pass —• -- Pass -- Pass County: Johnston Region: RRO Subbasin: NEU02 2000 — Pass — — Fail >8.64 >6.64 Pass — --- Pass PF: 1.9 Special 2001 — Pass -- — Pass -• -- Pass -- --- Pass 7Q10: 186 IWC(%):1.6 order: 2002 — — Pass >100,>100 -- Pass Cleveland MIIW001 PERM CHR LIM: 2.4%; IF EXP>.78MGD ® 3A% 1998 — -- Late Pass — Pass — — Pass -- -- Pass NC0004120/00I Iiegin:9/1/1993 Frequency: Q P/F + Mar Jun Sep Dec NonComp:SINGLE 1999 -- Pass — — Pass -- — Pass -- Pass County: Cleveland Region: MRO Subbasin: BRD04 2000 -- Pass — Pass — Pass — Pass PF: 0.78 Spacial 2001 --. -- Pass Pass — NRIH -- --- 7Q10:49.40 IWC(%)2.4 Order: 2002 -- H -- H Cleveland WWII. Perm chr lim: 3.0% NC0049867/001 Begin:3/1/2000 Frequency: Q Mar Jun Sep Dec + NonComp:Single County: Rowan Region: MRO Subbasin: YADO6 PF: 0.27 special 7Q10: 14.0 IWC(%)3.0 Order: 1998 Pass — Pass — Pass 1999 — — Fail Pass — Late 2000 — — NR/Pass — — Pass,Pass 2001 -. — Pass -- Pass 2002 Pass Pass -- Pass Pass — Pass — — Pass — Pass — — Pass — Pass — Pass — Pass -- — Late Y Pre 1998 Data Available LEGEND: PERM = Permit Requirement LET = Administrative Letter - Target Frequency = Monitoring frequency: Q- Quarterly; M- Monthly; BM- Bimonthly, SA- Semiannually; A• Annually OWD• Only when discharging; D- Discontinued monitoring requirement Begin = First month required 7Q10 = Receiving dream low flow criterion (cis) + = quarterly monitoring increases to monthly upon failure or NR Months that testing must occur - ex. Jan, Apr. Jul, Oct NonComp = Current Compliance Requirement PF = Permitted Bow (MGD) IWCk = Instream waste concentration P/F = Pass/Fail test AC = Acute CHR - Chronic Data Notation: f • Fathead Minnow; • - Ceriodaphnia sp.; my - Myaid shrimp; ChV - Chronic value; P - Mortality of stated percentage at highest concentration; at • Performed by DWQ Aquatic Tox Unit; bl - Bad test Reporting Notation: -- = Data not required; NR • Not reported Facility Activity Status: 1- Inactive, N - Newly Issued(To construct); H - Active but not discharging; t-More data available for month in question; • = ORC signature needed 10 Clariant Clariant Corporation Mt. Holly East Plant P.O. Box 669246 Charlotte, NC 28266 Phone: 704.827.9651 September 5, 2002 Ms. Jacquelyn M. Nowell Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: NPDES Permit Number NC0004375; Trial Period Data for Treatment of Solicited 3rd Party Industrial Wastewater Customers Dear Ms. Nowell; This letter and enclosed data tables contain information from the treatment of 3rd party wastewater at the Mt. Holly East Site. My February 12, 2001 letter to Mr. David Goodrich, promised a quarterly report on operating and shipment data. I have been sending the reports to both Mr. Goodrich and Mr. Michael Myers. This letter and attached data tables contains all 2002 information through July. I am sending you the entire report to date rather than just the second quarter data. The 3rd party wastewater treatment trials continue to proceed smoothly and the wastewater treatment plant continues to perform well. I appreciate the Division's helpful assistance provided during the trial period. Sincerely; P76,xicp6aen Gary P. Sanderson, P.E. Plant Services Manager 1-] [ (II1II [1-T1 S E P 1 2 2002 - cc: David Goodrich-DENR, Nick Altman, Frank Rash, Erin Russell — Clariant �� i Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts for January 200: pagel of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10' Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 2 1 13700 1 7.06 3.00 8.92 234 78 625 7.2 7.0 80 3 6.08 723 81 264 7.1 79 4 7.66 7.66 5.17 6.17 5.00 523 531 270 86 86 54 195 86 105 7.1 7.0 7.1 7.5 7.6 117 80 60 5 6 7 8 9 10 11 12 3 1 2 4 2 89620 47280 98980 220100 97540 2895 78 1090 4189 1071 6.68 8.30 6.11 5.50 5.55 5.00 360 72 70 7.3 60 4.92 477 97 48 7.5 59 3.83 437 114 56 7.8 50 4.50 7.6 13 6.67 7.4 14 2 86640 465 7.56 4.83 1290 267 338 7.3 53 15 2 96120 529 7.67 5.42 981 181 401 7.2 60 16 17 1 2 47700 90860 78 478 7.70 8.23 5.58 1322 237 167 7.5 72 4.42 977 221 604 7.6 80 18 2 65940 264 8.18 7.33 1341 183 620 7.8 184 19 20 21 22 23 24 25 2 3 3 2 89920 117560 123240 83260 1049 3219 3640 431 8.43 7.62 8.78 8.17 7.50 7.5 7.42 7.7 3.00 420 140 589 7.6 45 2.83 2.42 2.59 620 552 350 219 228 135 591 585 580 7.5 7.5 7.7 31 29 28 6.25 606 97 616 7.8 132 26 4.75 7.7 27 5.42 7.8 28 29 30 31 Total 3 3 5 2 45 121180 118560 211220 70980 1890400 7238 4216 12992 2386 46309 6.72 7.38 7.23 8.59 3.33 443 133 596 7.4 40 4.17 471 113 603 7.3 46 4.75 4.33 160.92 513 693 14134 108 160 3090 611 606 8956 7,7 7.6 47 48 1480 Avg. 2 99495 2437 7.45 5.19 642 140 407 7.5 67 Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts for February 2002 page2 of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10'5 Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 6 201120 30421 7.47 3.93 656 185 593 7.8 43 2 3.92 7.7 3 4.00 7.7 4 6 255700 9486 9.44 3.25 468 261 595 7.9 39 5 7 246080 26091 7.22 2.42 465 160 576 7.9 34 6 8 334640 42925 6.73 2.83 1701 235 589 8.1 31 7 7 265420 27575 7.09 2.83 1675 488 717 7.9 34 8 5 166780 7163 6.62 2.08 1204 718 564 7.8 23 9 2.08 7.9 10 2.08 8.0 11 7 273040 26061 7.20 5.33 3107 1330 413 8.0 129 12 5 228400 15799 6.21 3.33 1822 1157 347 8.0 46 13 8 354760 30689 6.41 3.08 1937 1122 589 7.9 44 14 4 155720 7576 5.92 3.33 1762 1254 592 7.8 56 15 7 303760 31581 6.31 2.25 1562 688 650 8.1 29 16 1.92 7.9 17 1.92 8.0 18 5 230240 17785 7.33 2.08 899 738 92 7.9 27 19 10 417430 36508 6.21 2.00 1086 875 285 8.0 24 20 7 308840 34259 8.05 2.42 1193 514 325 8.1 37 21 6 267880 13192 8.39 2.42 825 686 232 8.1 29 22 7 275440 21322 8.26 2.42 791 805 197 8.2 27 23 3 136440 6563 8.01 2.42 8.2 24 2.42 8.0 25 11 484220 24946 8.52 3.75 1905 1642 489 7.9 41 26 8 374900 15743 7.08 2.75 1193 847 326 7.8 36 27 10 441380 20713 8.70 2.25 1242 837 206 7.7 25 28 13 526060 54180 7.63 2.25 1282 726 167 7.9 27 29 30 31 Total 150 6248250 500578 77.76 26775 15268 8544 781 Avg. 7 297542 23838 7.37 0.00 2.78 1339 763 427 7.9 39 Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts for March 200 page3 of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10' Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 2 12 1 520010 47940 28087 3020 6.76 11.80 2.25 2.33 1022 687 80 7.7 7.5 27 3 2.33 7.6 4 8 358320 18101 9.18 2.25 574 192 64 7.8 25 5 6 10 7 443100 338760 23090 18380 38746 8.49 8.28 10.50 2.33 631 348 49 7.9 26 2.50 1148 831 107 7.8 31 7 10 427310 2.58 1189 538 98 7.9 28 8 11 341020 16579 9.98 2.58 1120 746 178 7.9 28 9 2.50 7.9 10 2.50 7.8 11 12 13 14 15 9 9 9 6 7 423940 420100 357040 289620 285800 19202 24620 23683 15302 15481 8.72 9.10 8.22 8.82 8.65 2.58 315 338 45 8.0 28 3.75 829 410 117 7.7 41 2.58 537 155 109 7.8 36 2.58 658 219 64 7.8 29 2.58 630 301 62 7.9 31 16 2.58 2.58 8.00 7.00 688 1246 240 293 112 147 7.6 8.1 7.8 7.9 96 119 17 18 3 147960 7117 8.40 19 3 141500 4931 7.28 20 4 160060 14582 9.01 6.08 1125 367 150 7.9 67 21 22 23 24 4 5 2 172320 212020 82620 5401 7264 5205 8.62 7.34 9.72 6.42 982 690 136 7.8 71 3.33 563 409 129 8.1 40 3.58 7.9 3.33 8.0 25 5 211960 15067 8.86 6.67 1067 268 469 7.8 74 26 9 374220 28334 8.09 6.33 7.85 318 156 7.7 115 27 6 280133 25497 9.34 6.50 838 552 137 7.6 97 28 6 237420 10241 8.62 6.75 1080 550 190 7.7 82 29 6.42 7.6 30 6.67 7.8 31 6.75 7.9 Total Avg. 146 6 6273173 285116 367930 16722 8.81 0.00 127.21 4.10 16250 812 8452 423 2599 130 7.8 1091 55 Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts Data for April 2Gu. page4 of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10' Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 4 172660 10138 6.30 3.58 759 217 393 8.1 40 2 3 140600 5123 7.11 8.25 1939 413 463 7.9 124 3 1 47740 2296 6.50 5.00 820 154 349 8.0 80 4 3 113560 12308 7.62 6.08 918 244 214 8.0 79 5 4 97440 7020 7.55 4.75 556 76 249 8.1 62 6 5.08 7.9 7 8.34 7.9 8 3 145900 7018 8.74 6.00 1284 60 126 7.7 114 9 2 93100 15618 7.28 5.00 1150 189 610 7.8 75 10 1 44180 13254 5.80 6.33 2804 159 623 7.9 159 11 2 65720 13446 6.95 3.50 2320 251 618 7.8 78 12 6 155260 49504 6.84 3.00 2034 180 715 7.8 135 13 2.58 7.8 14 2.58 8.0 15 4 188140 7353 7.09 3.59 2466 108 618 7.8 108 16 4 154580 20368 7.38 5.17 3262 135 533 7.8 197 17 2 96470 4653 7.10 6.00 3198 560 460 7.9 247 18 3 141580 8930 6.85 5.33 5.00 3251 3235 247 275 459 504 7.8 7.8 209 200 19 4 185262 31906 8.51 20 4 193920 9328 6.60 5.00 7.9 21 5.00 7.8 22 5 191980 13292 6.34 5.58 3281 211 499 7.9 200 23 6 277440 26845 7.56 7.09 2786 155 616 8.1 297 24 7 321262 39272 8.68 4.67 2480 292 608 7.8 127 25 6 274340 26165 9.12 3.92 2215 323 610 7.9 154 26 6 249000 13651 6.27 5.00 3175 89 573 7.9 124 27 4 193420 9304 7.62 3.83 8.0 28 4.67 7.9 29 6 279640 25766 7.42 5.09 3202 148 302 7.7 76 30 5 223260 15759 7.68 5.67 3215 125 596 8.0 113 31 Total 95 4046454 388317 150.68 50350 4611 10738 2998 Avg. 6 252903 24270 10.93 0.00 5.02 2288 210 488 7.9 136 Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts May 2002 page5 of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10' Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 2 6 8 295320 338469 28421 46099 7.79 8.38 6.08 5.50 3.33 3.42 3229 2684 1875 1002 177 137 498 613 592 7.9 8.0 8.0 7.9 231 193 127 3 5 253100 21833 7.67 4 3 144660 6958 8.00 5 3.33 8.0 6 6 232380 13319 7.40 4.25 2461 154 601 7.9 334 7 4 115494 7684 7.33 4.83 3178 207 405 7.8 279 8 2 97380 4684 6.70 3.08 2199 134 588 7.8 236 9 3 99060 4677 7.43 4.00 3100 129 250 7.9 412 10 2 95940 4615 7.00 4.08 3138 173 400 7.8 329 11 4.08 7.8 12 4.08 8.1 13 5 232060 14892 6.38 4.17 3169 169 603 7.8 525 14 4 195200 9389 7.52 2.25 1314 57 574 7.8 230 15 6 249160 17735 7.81 2.67 1674 46 577 7.9 305 16 5 193680 9257 7.16 3.50 2292 126 593 7.8 359 17 2 96540 4643 8.01 3.08 1984 43 586 7.9 291 18 3.08 7.9 19 3.08 6.09 4.75 5.33 3222 3126 3166 212 191 182 298 302 300 7.9 7.8 8.0 7.8 631 536 579 20 21 22 23 5 5 4 6 241200 223740 15068 19793 6.47 6.24 192960 9281 5.80 198000 9374 6.23 6.00 3198 301 333 7.7 512 24 5 215260 9858 5.98 5.83 2408 235 392 7.9 417 25 7.33 7.7 26 5.17 7.7 27 4.00 8.1 28 3 137340 8702 6.83 6.17 2733 124 371 7.8 502 29 11 421340 33817 7.16 5.50 1837 93 304 7.7 328 30 9 363520 39101 7.37 9.25 5.92 143.23 4.62 2553 2072 56612 2573 55 65 4012 182 284 212 9676 440 8.0 7.9 7.9 812 640 8808 400 31 6 233300 14562 6.40 Total Avg. 115 4 4865103 162154 353762 11412 0.00 Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts Data for June 26, page6 of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10° Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 8.25 7.9 2 6.58 7.8 3 3 121480 5843 6.17 6.17 1635 62 113 7.6 460 4 5 240800 13908 6.31 7.08 2018 57 238 7.6 431 5 5 193540 12360 6.88 8.17 2639 73 205 7.7 569 6 5 47280 15281 5.59 12.00 3288 144 277 7.6 828 7 5 200600 12070 7.12 9.58 2232 48 229 7.6 624 8 9.17 7.6 9 7.00 7.6 10 5 221220 23383 6.85 10.58 1502 53 422 7.7 402 11 2 79220 5394 7.76 8.34 1051 33 251 7.7 267 12 No Shipments received on this date 6.42 725 57 143 7.7 153 13 5 176280 11316 6.70 5.83 1131 29 106 7.7 314 14 4 127620 7369 6.64 6.08 1137 37 68 7.7 146 15 6.00 7.5 16 5.42 8.0 17 6 240380 14544 6.81 5.92 811 30 221 7.9 143 18 3 198280 9484 6.77 7.25 1160 29 127 8.0 152 19 4 164920 19943 6.33 8.75 1496 35 159 7.9 228 20 3 129480 9049 6.53 8.00 1664 48 205 7.8 185 21 7 254260 24070 6.28 7.08 1083 28 119 7.8 163 22 5.50 7.8 23 6.50 8.2 24 7 299080 29758 6.04 7.25 928 29 142 7.8 296 25 6 279300 29262 6.37 1.92 265 10 54 8.2 49 26 6 267260 16472 5.82 11.17 1407 67 298 7.8 235 27 4 193300 9298 5.85 9.34 1943 28 254 8.2 344 28 5 176120 9799 6.17 5.42 504 22 122 8.2 115 29 8.84 8.1 30 5.33 8.1 31 Total 90 3610420 278603 220.94 28619 919 3753 6104 Avg. 5 190022 14663 6.47 7.36 1431 46 188 7.8 305 Mt. Holly East WWTP: Operating Data Relative to 3rd Party Receipts Data for July 2002 page7 of 7 Date Data on Received Shipments Effluent Data from Daily Monitoring Reports No. of Loads Received Pounds Received COD Pounds pH lb x 10° Discharged COD Pounds BOD Pounds NH3 Pounds pH TSS Pounds 1 8 301360 25451 7.71 5.42 721 27 123 8.1 125 2 5 218180 11787 7.47 7.83 987 55 199 8.1 173 3 7 279340 24726 8.39 6.50 968 52 195 7.8 155 4 HOLIDA` 7.25 7.8 5 8 257220 38142 8.64 9.92 7.8 6 7.17 7.8 7 8.42 7.7 8 6 253120 20048 8.80 8.58 1107 34 456 7.9 231 9 5 222960 10014 8.18 9.34 1364 75 335 8.0 600 10 4 140020 18491 8.41 10.58 1576 64 378 8.0 381 11 4 186380 29675 7.78 9.75 2155 283 376 8.0 391 12 3 145360 9399 7.43 8.50 1998 153 352 8.0 358 13 9.08 7.8 14 12.50 7.8 15 3 138240 8784 7.60 10.00 1060 40 392 7.7 220 16 3 129660 24591 8.96 3.25 520 20 85 7.7 94 17 1 28780 6 8.50 3.33 773 106 141 7.7 83 18 4 116280 13678 8.11 3.33 663 114 193 7.9 91 19 2 98140 4721 6.50 5.83 1090 105 291 7.8 193 20 4.50 8.0 21 3.92 8.0 22 3 135460 18850 7.20 6.25 1212 37 253 7.9 131 23 2 73980 18038 9.03 4.83 850 34 140 8.0 107 24 8 410826 29932 5.99 4.92 822 148 248 7.9 118 25 5 344076 17061 6.17 5.33 864 42 364 8.0 170 26 3 237946 18123 5.36 8.09 1440 211 512 7.9 179 27 1 49200 2366 5.00 8.75 8.0 28 5.25 7.9 29 7 463491 37756 5.70 4.25 451 8 121 8.1 89 30 6 264140 55198 7.00 4.33 749 13 79 7.9 117 31 3 53980 2464 5.37 4.58 838 119 315 7.9 101 Total 101 4548139 439301 211.58 22208 1740 5548 4107 Avg. 5 216582 20920 8.06 0.00 6.83 1058 83 264 7.9 196 ci-riC Cf:f (q9 i) = �3 1,„or X5 2. 4cQ . ev,i 223ca ,#klot S q 2 c ZLs --t-,,tie."5- bs ei-, .3i64-ta ' 17 0� Jo re i 7Q fit �f /!.5rt.0 lire, '� %e cam, °UST' •_ itt 41,1d 11 e-ifek, •Yib w N - G$TJ F< ill II , ITS- ,-0 4r h. i V3 g; e q✓lvf) A64s l ' J �- s/� ) Co a e'`Z-/-g 6 #401-55-1144-1(s fi-jitv“d 44,1o, 61^c--G-f c/i7/7-. G C-60 ,Evte,L,L �s� z z. Doc_ E e„.f, C. y' 9! ) v (1ML ' -,vrt p7 27e.,-5 .t4 9 ieriy ��. Facility Name = Qw (MGD) = WWTP Classification NPDES # = Receiving Stream IWC (%) = Final Results: clariant corp.. 3.9 4 nc0004375 Catawba River 1.80 Reasonable Potential Summary X° 2° 3° 4° Stream Classification 7Q10s (cfs)= 30Q2 (cfs) Qavg (cfs) wS-Iv NSW 329 716 3016 Arsenic Max. Pred Cw Allowable Cw #DIV/0! µg/1 2771.3 µg/l :Implementation !Are all reported values less than? 'Is the detection limit acceptable? No Yes Limit? Monitor? I #DIV/0! Monitoring #DIV/0!'Frequency #DIV/O! Aluminum Max. Pred Cw Allowable Cw Not a POC 41 Not a POC µg/1 jlmplementation !Are all reported values less than? !Is the detection limit acceptable? Yes Yes Limit? Monitor? i No Monitoring No !Frequency None Barium Max. Pred Cw Allowable Cw Not a POC µg/1 55425.1 µg/l 'Implementation 'Are all reported values less than? GIs the detection limit acceptable? Yes Yes Limit? Monitor? No No I i Monitoring 'Frequency None Benzene Max. Pred Cw Allowable Cw Not a POC µg/l 501.1 µg/1 !Implementation !Are all reported values less than? 'Is the detection limit acceptable? Yes Yes Limit? Monitor? No No I !Monitoring j Frequency None Beryllium Max. Pred Cw Allowable Cw Not a POC µg/1 499.9 mil jlmplementation .Are all reported values less than? !Is the detection limit acceptable? Yes Yes Limit? Monitor? No No i .Monitoring !Frequency None Carbon Tetrachloride Max. Pred Cw Allowable Cw Not a POC µg/l 500.15 µg/l 'Implementation jAre all reported values less than? 'Is the detection limit acceptable? Yes Yes Limit? Monitor? No No ! i Monitoring 'Frequency None Cadmium Max. Pred Cw Allowable Cw #DIV/0! µg/1 110.9 µg/l !Implementation lAre all reported values less than? jls the detection limit acceptable? No Yes Limit? Monitor? 1 #DIV/0! IMonitoring #DIV/0! jFrequency #DIV/0! 1 ! 1/2 FAV (non Trout) 15.0 µg/1 ' 1/2 FAV (Trout) 2.1 µg/1 ! 1/2 FAV 42 µg/1 ! loride Max. Pred Cw Allowable Cw 2466.3 mg/L 13856.3 mg/L Implementation 'Are all reported values less than? Its the detection limit acceptable? No Yes Limit? Monitor? Yes onitorin reque y 2/Month Chlorinated Benzenes Max. Pred Cw Allowable Cw Not a POC µg/l 987.9 µg/1 !Implementation 'Are all reported values less than? jls the detection limit acceptable? Yes Yes Limit? Monitor? I 'Monitoring i Frequency None No No Chloroform Max. Pred Cw Allowable Cw Not a POC µg/1 Not aPOC µg/l Implementation !Are all reported values less than? 'Is the detection limit acceptable? Yes Yes Limit? Monitor? No No 1 !Monitoring I Frequency None Facility Name = Qw (MGD) = IWC (%) = NPDES # = Receiving Stream Final Results: 4'-iiii.'3111 ^^ ij 71121 aeY AI as t• ypa - y[ 9efi.-. E 1 1 3 °:::. , ``k -F EEww x=. _.::�F.C� -Y .• o tir..'t�s.t .«.b: rv•i :41J:1iT „s.:> p� S=: •:Y wypqg}q{ .... It " Y7 _ri•�, :.,1.SL'4."=` ...4 V. Reasonable Potential Summary Stream Classification 7Q10s (cfs)= 30Q2 (cfs) Qavg (cfs) X° of i r I f 1,x: 2° 30 4° N'dh, Chromium Max. Pred Cw #DIV/0! µg/I Allowable Cw 2771.3 µg/1 :Implementation 'Are all reported values less than? !Is the detection limit acceptable? No Yes Limit? Monitor? : #DIV/0! sMonitoring #DIV/0! !Frequency #DIV/0! I 1/2 FAV' 10221µg/1 I Copper Max. Pred Cw #DIV/0! µg/l Allowable Cw 388.0 µg/1 :Implementation 'Are all reported values less than? !Is the detection limit acceptable? No Yes Limit? Monitor? No 'Monitoring #DIV/0! ! Frequency #DIV/0! I I 1/2 FAV 7.3 141 I 1/2 FAV 5.8 µg/1 1 Cyanide Max. Pred Cw #DIV/0! µg/l Allowable Cw 277.1 µg/1 'Implementation !Are all reported values less than? Its the detection limit acceptable? No Yes Limit? Monitor? #DIV/0! ! Monitoring #DIV/0! I Frequency #DIV/0! I 1 1/2 FAV 22.0 µg/1 I 1/2 FAV 1.0 µg/1 Dioxin Max. Pred Cw Not a POC pg/1 Allowable Cw 512.9 pg/l 'Implementation !Are all reported values less than? lIs the detection limit acceptable? Yes Yes Limit? Monitor? ' No !Monitoring No 'Frequency None Fluoride Max. Pred Cw #DIV/0! µg/1 Allowable Cw 99765.3 µg/1 :Implementation 'Are all reported values less than? !Is the detection limit acceptable? No Yes Limit? Monitor? : #DIV/0!'Monitoring #DIV/0! !Frequency #DIV/0! Hexachlorobutadiene Max. Pred Cw Not a POC µg/1 -- Allowable Cw 500.3 µg/1 !Implementation :Are all reported values less than? 'Is the detection limit acceptable? Yes Yes Limit? Monitor? I No :Monitoring No 'Frequency None on Max. Pred Cw 7.0 µg/I Allowable Cw 55.4 µg/1 Implementation 'Are all reported values less than? :Is the detection limit acceptable? No Yes Limit? Monitor? s I Monitorin Yes : Frequen y 2/Month Lead Max. Pred Cw #DIV/0! µg/1 Allowable Cw 1385.6 µg/1 'Implementation 'Are all reported values less than? !Is the detection limit acceptable? No Yes Limit? Monitor? ' #DIV/0!'Monitoring #DIV/0! !Frequency #DIV/0! I ' 1/2 Fay 33.8 µg/I I 1/2 FAV 221.0 µg/I ' anganese Max. Pred Cw 4383.1 µg/I 11085.0 µg/1 ±Implementation !Are all reported values less than? !Is the detection limit acceptable? No Yes Limit? Monitor? 1 'Monitoring Yes IFrequency /Month Allowable Cw Facility Name = Qw (MGD) = IWC(%) _ NPDES # = Receiving Stream Finafsults: L11.1ii[# 5i+ ��==`=max.= S • • .. r =r �F:, ..• . i is ::..e_` =ir-, j..,,L.�"t;r:x.,..-..._,.., , --J. i p l ���ti�i r „ :� r_�;"T`. i. r,` ..cz":_:?i:e :�-�+L: I.cS Ettr'. [!E:4 _'0x „h .. '':Tir'= Reasonable Potential Summary Stream Classification 7Q1Os (cfs)= 30Q2 (cfs) Qavg (cfs) 10 2° 30 4° IVPAr BISW 0 Ors LAM BAS Max. Pred Cw 1755.8 µ/l g llowable Cw 27712.6 µg/1 'Implementation 'Are all reported values less than? !Is the detection limit acceptable? No Yes Limit? Monitor. No , I Monitoring Yes Frequenc 2/Month Mercury ax. Pred Cw 5.9881 µg/1 Allowable Cw 0.6651 µg/l !Implementation :Are all reported values less than? •Is the detection limit acceptable? No Yes Limit? Monito . I Yes Monitorin Yes s Frequen Weekly Nicker Max. Pred Cw #DIV/0! µg/1 Allowable Cw 1385.6 µg/l !Implementation 'Are all reported values less than? jls the detection limit acceptable? Yes Yes Limit? Monitor? ! #DIV/0! I Monitoring #DIV/0! jFrequency #DIV/0! ' I 1/2 FAV 261.0 µg/1 ' 1/2 FAV 75.0 µg/1 Oil & Grease Max. Pred Cw Not a POC mg/L Allowable Cw 1662.8 mg/L !Implementation !Are all reported values less than? the detection limit acceptable? Yes Yes Limit? Monitor? I No 'Monitoring No Frequency None PCB Max. Pred Cw Not a POC µg/l --" Allowable Cw 54.5317 µg/l iIs 'Implementation !Are all reported values less than? Its the detection limit acceptable? Yes Yes Limit? Monitor? i i No !Monitoring No IFrequency None Phenol Max. Pred Cw 1047.2296 1 µPS Allowable Cw 55.4251 µg/1 :Implementation 'Are all reported values less than? P !Is the detection limit acceptable? No Yes Limit? Monitor? % j Yes 8 Monitoring 9 Yes ! Frequency Weekly Silver Max. Pred Cw #DIV/0! µg/1 Allowable Cw 3.3 µg/l Immplementation jAre all reported values less than? 'Is the detection limit acceptable? No Yes Limit? Monitor? �� I No i Monitoring #DIV/0!:Frequency #DIV/0! 1 I 1/2 FAV 1.2 µg/1 I 1/2 FAV 1.9 µg/1 I Selenium Max. Pred Cw Not a POC µg/1 Allowable Cw 277.1 µg/l !Implementation :Are all reported values less than? Is the detection limit acceptable? No Yes Limit? Monitor? I No :Monitoring No !Frequency None Tetrachloroethane Max Pred. Cw Not a POC µg/1 Allowable Cw 500.06 µg/1 !Implementation 'Are all reported values less than? iIs the detection limit acceptable? Yes Yes Limit? Monitor? I No I Monitoring No :Frequency None Tetrachloroethylene Max Pred. Cw Not a POC µg/1 Allowable Cw 500.69 µg/1 Implementation !Are all reported values less than? I Is the detection limit acceptable? Yes Yes Limit? Monitor? 1 No !Monitoring No I Frequency None Total Dissolved Solids iImplementation I Max Pred. Cw Allowable Cw Not a POC mg/L 'Are all reported values less than? 500.0 mg/L !Is the detection limit acceptable? Yes Limit? No 'Monitoring Yes Monitor? No !Frequency None Facility Name = Qw (MGD) = IWC (%) = NPDES # = Receiving Stream Final Results: T':'i ....._....". ....Gu=::.• = t.LJL6rx=:= -' i •:.ri:.. 1. � �„ (`` _`• r}it ,- -.... ti�;'e ls.'�tf '"^l1 .r ' •.x` yi FJ.�if_3P, x... '"' � ii4. ��'�� ��s +�• .''.. [�S j �F[� >, t..• . ...d " I n;1 : a, r •, h: Reasonable Potential Summary Stream Classification 7QIOs (cfs)= 30Q2 (cfs) Qavg (cfs) 1° 2° 30 4° Toluene Max. Pred Cw Allowable Cw Not a POC µg/l 0.2 µg/l 'Implementation iAre all reported values less than? 'Is the detection limit acceptable? Yes Yes Limit? Monitor? I No i Monitoring No 'Frequency None Triaklyltin Max. Pred Cw Allowable Cw Not a POC µg/I 0.4 µg/1 !Implementation 'Are all reported values less than? jIs the detection limit acceptable? Yes Yes Limit? Monitor? I No I Monitoring No j Frequency None Trichloroethylene Max. Pred Cw Allowable Cw Not a POC µg/1 503.0 µg/l :Implementation ,Are all reported values less than? Its the detection limit acceptable? Yes Yes Limit? Monitor? ' No Monitoring No !Frequency None Turbidity Max. Pred Cw Allowable Cw Not a POC NTU 2771.3 NTU 'Implementation jAre all reported values less than? GIs the detection limit acceptable? Yes Yes Limit? Monitor? I No i Monitoring No , Frequency None Vinyl Chloride Max. Pred Cw Allowable Cw Not a POC µg/1 501.9 µg/l Implementation lAre all reported values less than? jls the detection limit acceptable? Yes Yes Limit? Monitor? I No 'Monitoring No i Frequency None Zinc Max. Pred Cw Allowable Cw #DIV/0! µg/1 2771.3 µg/1 'Implementation !Are all reported values less than? lls the detection limit acceptable? No Yes Limit? Monitor? i No !Monitoring #DIV/0!'Frequency #DIV/0! I 1 1/2 FAV ' 67.0 µg/1 1 I 1/2 FAV 95.0 µg/l : Clariant Corporation, Mt. Holly - Data Summary 18-months data for Fact Sheet RP analysis N130-20 Date Manganese Iron Chlorides Mercury mg/L ug/L mg!L mg/L mg/L ug/L 1/3/01 0.71 710 0.1 370 <0.0002 <0.2 2/7/01 0.78 780 0.1 710 <0.0002 <0.2 3/7/01 0.04 40 0.1 630 0.0002 0.2 4/4/01 0.97 970 0.3 760 <0.0002 <0.2 5/2/01 0.38 380 0.1 870 <0.0002 <0.2 6/7/01 0.4 400 1.6 160 <0.0002 <0.2 7/11/01 0.92 920 0.3 120 <0.0002 <0.2 8/1/01 0.86 860 0.1 44.0 <0.0002 <0.2 9/5/01 1.20 1200 0.1 470 <0.0002 <0.2 10/3/01 1.40 1400 0.1 540 <0.0002 <0.2 11/7/01 1.00 1000 0.1 140 <0.0002 <0.2 12/5/01 1.30 1300 0.2 450 <0.0002 <0.2 1/2/01 1.60 1600 0.1 430 <0.0002 <Q,2 2/6/02 1.90 1900 0.3 800 0.0012 3/6/02 0.47 470 0.5 930 0.0004 4/3/02 0.4 400 0.3 4.1 0.0002 5/1/02 0.26 260 0.5 750 0.0010 6/5/02 1.3 1300 0.6 1000 <0.0002 8/27/02 1 of 3 13020s0091 RP Data _�, Clariant Corporation, Mt. Holly - Data Summary 18-months data for Fact Sheet RP analysis N130-20 Date Total Sulfate Date Flow Total Phenolics mg1L Ibs mg/L ug1L 1/3/01 675 1/2/01 1.21 0.51 0.051 50.5 1/10/01 1288 1/9/01 1.28 0.64 0.060 60.0 1/17/01 1998 1/16/01 1.26 0.53 0.050 50.4 1/24/01 1345 1/23/01 1.21 0.61 0.060 60.4 1 /31 /01 1247 1/30/01 1.35 0.56 0.050 49.7 2/7/01 1439 2/6/01 1.76 1.03 0.070 70.2 2/14/01 1251 2/13/01 1.04 0.69 0.080 79.6 2/21/01 1345 2/20/01 1.24 0.52 0.050 50.3 2/28/01 1156 2/27/01 2.37 0.99 0.050 50.1 3/7/01 1328 3/6/01 1.46 0.61 0.050 50.1 3/14/01 1299 3/13/01 1.34 0.56 0.050 50.1 3/21/01 1124 3/20/01 2.36 0.98 0.050 49.8 3/28/01 434 3/27/01 1.29 0.54 0.050 50.2 4/4/01 1192 4/3/01 1.05 0.44 0.050 50.2 4/11/01 1124 4/10/01 1.26 0.53 0.050 50.4 4/18/01 832 4/17/01 0.94 0.39 0.050 49.7 4/25/01 1012 4/24/01 1.10 1.66 0.181 180.9 5/2/01 1181 5/1/01 1.60 1.07 0.080 80.2 5/9/01 1751 5/8/01 0.92 0.39 0.051 50.8 5/16/01 1794 5/15/01 1.13 0.47 0.050 49.9 5/23/01 1350 5/22/01 1.25 0.52 0.050 49.9 5/30/01 1562 5/29/01 1.00 0.50 0.060 60.0 6/6/01 748 6/5/01 1.16 0.58 0.060 60.0 6/13/01 1046 6/12/01 1.20 0.50 0.050 50.0 6/20/01 725 6/19/01 1.00 0.42 0.050 50.4 6/27/01 1120 6/26/01 0.97 0.40 0.049 49.4 7/4/01 1013 7/3/01 0.37 0.19 0.062 61.6 7/11/01 821 7/10/01 0.85 0.35 0.049 49.4 7/18/01 869 7/17/01 0.83 0.34 0.049 49.1 7/25/01 1480 7/24/01 1.05 3.24 0.370 370.0 8/1/01 1701 7/31/01 0.91 1.33 0.175 175.2 8/8/01 1025 8/7/01 1.21 2.82 0.279 279.4 8/15/01 289 8/14/01 1.04 3.12 0.360 359.7 8/22/01 1722 8/21/01 0.62 0.78 0.151 150.8 8/29/01 2018 8/28/01 0.68 0.96 0.169 169.3 9/5/01 1690 9/4/01 0.48 3.77 0.942 941.7 9/12/01 1218 9/11/01 0.46 0.73 0.190 190.3 9/19/01 1866 9/18/01 0.84 2.44 0.348 348.3 9/26/01 1562 9/25/01 1.09 3.55 0.391 390.5 10/3/01 1501 10/2/01 0.51 5.11 1.201 1201.4 10/10/01 685 10/9/01 0.16 3.45 2.585 2585.4 10/17/01 642 10/10/01 0.16 2.31 1.731 1731.1 10/24/01 934 10/16/01 0.39 3.51 1.079 1079.1 10/31/01 617 10/23/01 0.79 1.13 0.172 171.5 11 /7/01 1055 10/30/01 0.87 1.3 0.179 179.2 11/14/01 916 11/6/01 0.58 0.48 0.099 99.2 11 /21 /01 1024 11/13/01 0.55 0.32 0.070 69.8 11/28/01 781 11/20/01 0.89 0.75 0.101 101.0 12/5/01 1190 11/27/01 0.73 0.61 0.100 100.2 12/12/01 1204 12/4/01 0.46 0.19 0.050 49.5 12/19/01 1574 12/11/01 0.91 0.69 0.091 90.9 12/26/01 1017 12/18/01 0.98 0.49 0.060 60.0 1/2/02 827 12/25/01 0.47 0.35 0.089 89.3 8/27/02 13020s0091 2 of 3 RP Data 1/9/02 s 3 1/16/02 1673 1/23/02 1964 1/30/02 1479 2/6/02 1962 2/13/02 1951 2/20/02 1553 2/27/02 2256 3/6/02 1801 3/13/02 1219 3/20/02 1202 3/27/02 1856 4/3/02 1528 4/10/02 1878 4/17/02 1400 4/24/02 1750 5/1/02 1571 5/8/02 1754 5/15/02 1726 5/22/02 2172 5/29/02 1455 6/5/02 2016 6/12/02 871 6/19/02 1163 6/26/02 789 8/27/02 3 of 3 1/1/02 1/8/02 1/15/02 1/22/02 1/29/02 2/5/02 2/12/02 2/13/02 2/19/02 2/26/02 3/5/02 3/12/02 3/19/02 3/26/02 4/2/02 4/9/02 4/16/02 4/23/02 4/30/02 5/7/02 5/14/02 5/21/02 5/28/02 6/4/02 6/11/02 6/18/02 6/25/02 1.07 0.60 0.65 0.34 0.50 0.29 0.40 0.37 0.24 0.33 0.28 0.45 0.84 0.76 0.99 0.60 0.62 0.85 0.68 0.58 0.27 0.57 0.74 0.85 1.00 0.87 0.23 0.45 0.30 1.53 1.29 0.71 0.99 0.46 0.53 0.58 0.90 0.74 0.82 1.46 1.66 0.74 0.65 0.52 0.92 0.51 0.58 0.14 0.29 0.31 0.35 0.92 0.58 0.10 0.050 0.060 0.282 0.455 0.170 0.409 0.138 0.172 0.290 0.327 0.317 0.218 0.208 0.262 0.090 0.130 0.101 0.130 0.090 0.120 0.062 0.061 0.050 0.049 0.110 0.080 0.052 50.4 60.0 282.2 454.9 170.3 409.3 137.9 171.8 289.8 327.0 316.9 218.5 208.4 261.9 89.6 129.9 100.6 129.8 89.9 119.9 62.2 61.0 50.2 49.4 110.3 79.9 52.1 13020s0091 RP Data TOXICANT ANALYSIS rameter = Sulfates tandard = 250000 pg/I n DL=1/2DLActual Data RESULTS 1 643000 643000 Std Dev. 420486.393 2 1673000 1673000 Mean 1585160 3 1964000 1964000 C.V. 0.265264322 4 1479000 1479000 5 1962000 1962000 6 1951000 1951000 Mutt Factor 7 1553000 1553000 Max. Value 8 2256000 2256000 Max. Pred C 9 1801000 1801000 Allowable C 10 1219000 1219000 11 1202000 1202000 12 1856000 1856000 13 1528000 1528000 14 1878000 1878000 15 1400000 1400000 16 1750000 1750000 17 1571000 1571000 18 1754000 1754000 19 1726000 1726000 20 2172000 2172000 21 1455000 1455000 22 2013000 2013000 23 871000 871000 24 1163000 1163000 25 789000 789000 26 27 1.3 2256000 pg/ 2932800 Pg/ 13856286 Ng! 8/27/02 PAGE 1 TOXICANT ANALYSIS acility Name Clariant Co • Parameter = Cd Parameter = Cn Parameter = Phenols PP pg/1 S Dat RESULTS 50.4 Std Dev. 116.4058 60.0 Mean 166.0778 282.2 C.V. 0.700912 454.9 170.3 NPDES # NC0004375 Standard = 2 pg/I Standard = 5 pg/1 Standard = 300 Qw (MGD) 3.9 30Q2 (cfs) 716 n BDL=1/2DL tual Data RESULTS n DL=1/2D ual Data RESULTS n DL=1/2DLctual /WC (%) 0.84 1 0.5 <1 Std Dev. 0.574120394 1 17 17 Std Dev. 38.438 1 50.4 eying Stream Catawba River 2 0.5 <1 Mean 0.58372093 2 35 35 Mean 27.578 2 60 Stream Class WS-IV CA 3 0.5 <1 C.V. 0.983552867 3 38 38 C.V. 1.3938 3 282.2 4 0.5 <1 4 74 74 4 454.9 FINAL RESULTS 5 0.5 <1 5 43 43 5 170.3 Cd 6 0.5 <1 1 Mull Facto 1.8 6 4 4 Mull Facto 1.9 6 409.3 409.3 Mutt Fact ri 2.31 ax. Pred Cw 10.08 ugll 7 0.5 <1 Max. Valu: 5.6 pg/ 7 1 <2 Max. Value 220 pgli 7 137.9 137.9 Max. Value 454.9 pg/i 171.8 Max. Pn3d C 1046.27 pg/l 289.8 Allowable C 35833.50 pg/l 327.0 316.9 218.5 208.4 261.9 89.6 129.9 100.6 129.8 89.9 119.9 62.2 61 50.2 49.4 110.3 79.9 52.1 Allowable Cw 238.9 ug/1 8 0.5 _ <1 <1 Max. Pred 10.08 Ng/ 8 10 10 Max. Pred 418 g/i 8 171.8 Max. Value 5.6 9 0.5 Allowable 238.89 pg 9 26 26 Allowable • 597.22 pg/1 9 289.8 Cn ax. Pred Cw 10 0.5 <1 10 15 15 10 327 418 ugll 11 0.5 <1 11 37 37 11 316.9 Allowable Cw 597.2 ugll 12 0.5 <1 <1 12 10 10 12 218.5 Max. Value Phenols ax. Pred Cw Allowable Cw Max. Value Sulfates 220 1046.27 35833.5 454.9 ugll ugll 13 0.5 13 1 <2 13 208.4 14 0.5 <1 14 56 56 14 261.9 15 0.5 <1 15 64 64 15 89.6 16 0.5 <1 16 7 7 16 129.9 17 5.6 5.61 17 25 25 17 100.6 18 0.5 <1 18 19 19 18 129.8 ax. Pred Cw 2932800 ugll 19 0.5 <1 • 19 11 11 19 89.9 • 29861249.0 ug/i 20 0.5 <1 20 150 150 20 119.9 2256000 21 0.5 <1 21 2 2 - 21 622 22 0.5 <1 22 47 47 22 61 306 ugll 23 0.5 <1 23 36 36 23 50.2 5972.2 ugll 24 0.5 <1 24 73 73 24 49.4 170 25 0.5 <1 25 9 9 25 110.3 26 0.5 <1 • 26 8 8 26 79.9 ax. Pred Cw 0 ug/i 27 0.5 <1 • 27 5 5 27 52.1 Allowable Cw #VALUEI ug/l 28 0.5 <1 28 35 35 28 Max. Value 0 29 0.5 _ <1 29 90 90 29 0 30 0.5 <1 30 14 14 30 ax. Pred Cw 0 ugll 31 0.5 <1 31 89 89 31 Allowable Cw 0.0 ug/l 32 1.1 1.1 32 88 88 32 Max. Value 0 - 33 0.5 <1 33 3 3 33 0 34 0.5 <1 I 34 4 4 34 ax. Pred Cw 0 ugll 35 0.5 <1 35 8 8 35 Allowable Cw 0.0 ug/I 36 0.5 <1 • 36 6 6 36s Max. Value 0 37 0.5 <1 37 2 2 37 0 _ 38 0.5 <1 38 5 5 38 ax. Pred Cw 0 ugll 39 0.5 <1 39 71 71 39 Allowable Cw 0.0 ugll 40 0.5 <1 40 97 97 40 Max. Value 0 41 0.5 <1 41 190 190 41 0 42 _ 0.5 <1 42 140 140 42 ax. Pred Cw 0 u . /1 43 0.5 <1 43 220 220 43 Allowable Cw 0.0 ugll 44 0.5 <1 44 71 71 44 Max. Value 0 45 0.5 <1 45 43 43 45 9/3/02 TOXICANT ANALYSIS arameter = Phenols Standard = 1 pg/l n DL=1/2DLctual DatIZESULTS 1 50.4 50.4 Std Dev. 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 60 282.2 454.9 170.3 409.3 137.9 171.8 289.8 327 316.9 218.5 208.4 261.9 89.6 129.9 100.6 129.8 89.9 119.9 62.2 61 50.2 49.4 110.3 79.9 52.1 60.0 282.2 454.9 170.3 409.3 137.9 171.8 289.8 327.0 316.9 218.5 208.4 261.9 89.6 129.9 100.6 129.8 89.9 119.9 62.2 61 50.2 49.4 110.3 79.9 52.1 Mean C.V. 116.41 166.08 0.7009 2.3 454.9 pg/I 1046.3 pg/I 119.44 pg/I MuIt Factor Max. Value Max. Pred C Allowable C Pa S 3,66 /bs/c r 8/27/02 PAGE 1 N 130-20, RP analysis Subject: N130-20, RP analysis Date: Fri, 23 Aug 2002 12:24:19 -0400 From: "Lili Gellner"<lili_gellner@awareenvironmental.com> To: "NCDENR - Mike Myers" <mike.myers@ncmail.net>, "NCDENR - Jackie Nowell" <jackie.nowell@ncmail.net> CC: "Ned Fiss" <ned_fiss@awareenvironmental.com>, "Clariant - Gary S." <Gary.Sanderson@clariant.com> Michael and Jackie, File 13020s009.xls is 18-months of Clariant data for the RP Analysis: Manganese, Iron, Chlorides, Mercury, Total Sulfate, Total Phenolics. I completed the RP Analysis spreadsheet as much as possible using this data. Please note/review the following: 1. Manganese, Mercury, Total Phenolics are entered into the RP analysis worksheet as ug/L. Please make sure this is correct. 2. Iron and Chlorides are entered into the RP analysis worksheet as mg/L. Please make sure this is correct. 3. Total Phenolics was entered into the worksheet labeled "Phenol" (on the RP Analysis). I'm not sure if this is correct, but there was no worksheet set up for "Total Phenolics". 4. I did not add the Total Sulfate data to the RP Analysis b/c there was no worksheet set up for it. I believe that I have given you enough information/data to complete your evaluation of the RP Analysis. Please let me know if you have any questions or if there is additional information that is needed. Thanks. Lili Lili Gellner, P.E. Sr. Project Engineer AWARE Environmental Inc. 9305-J Monroe Rd. Charlotte, NC 28270 P (704) 845-1697 F (704) 845-1759 D13020s009.xls Name: 13020s009.xls Type: Microsoft Excel Worksheet (application/vnd.ms-excel) Encoding: base64 Download Status: Not downloaded with message DRP Analysis.xls Name: RP Analysis.xls Type: Microsoft Excel Worksheet (application/vnd.ms-excel) Encoding: base64 Download Status: Not downloaded with message 1 of 1 8/27/02 9:04 AM Facility Name = NPDES # = Qw (MGD) = ;o91 (44= IWC(%) = clariant corp.. _ nc0004375 3.9 1.80 FINAL RESULTS Phenol Max. Pred Cw 1047.2 Allowable Cw RESULTS Std Dev. Mean C.V. Number of data points Mult Factor = Max. Value Max. Pred Cw Allowable Cw 116.4058 166.1 0.7009 27 2.30 454.9 µg/1 1047.2 µg/1 /II . µg/l Parameter = Standard = Phenol 1.0 Date n < Actual Data BDL=1/2DL Jan-02 1 50.4 50.4 Jan-02 2 60.0 60.0 Jan-02 3 282.2 282.2 Jan-02 4 454.9 454.9 Jan-02 5 170.3 170.3 Feb-02 6 409.3 409.3 Feb-02 7 137.9 137.9 Feb-02 8 171.8 171.8 Feb-02 9 289.8 289.8 Feb-02 10 327.0 327.0 Mar-02 11 316.9 316.9 Mar-02 12 218.5 218.5 Mar-02 13 208.4 208.4 Mar-02 14 261.9 261.9 Apr-02 15 89.6 89.6 Apr-02 16 129.9 129.9 Apr-02 17 100.6 100.6 Apr-02 18 129.8 129.8 Apr-02 19 89.9 89.9 May-02 20 119.9 119.9 5/14/02 21 62.2 62.2 5/21/02 22 61 61.0 5/28/02 23 50.2 50.2 6/4/02 24 49.4 49.4 6/11/02 25 110.3 110.3 6/18/02 26 79.9 79.9 6/25/02 27 52.1 52.1 SEP 03 2002 16:49 FR CLHRirNT CORP ENGINEE 8226529 TO 19197330719 P.02%05 Clariant Ms. Jacquelyn Nowell NC Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Cloriont Corporation Mt. Holly Plant August 26, 2002 Re: Company Officer Signature Pages Addendum to 1996 Permit Renewal Application NPDES Permit No. NC004375 Dear Ms. Nowell: P.O. Dux CCO240 Charintta, NC 28266 704,827.9651 Enclosed are the signature pages of Forms 1, 2C and 2F. I have enclosed three of each to match with the three permit application packages that were sent via FEDEX on Friday August 23`d. The FEDEX package was sent to Mr. Michael Myers. Since Mr. Myers may he husy with clean- up type work this week, I am sending then; documents to you. I hope this does not cause any extra work or problem for you. If there are other documents you need or if you require any other information, please do not hesitate to call me at (704) 822-2787 or email me at 7arv.sa.nrlersowai.clariant.cotr,_ Sincerely, Attomf 74-10Le-e-t Gary Sanderson, P.E. Plant Services Manager Clariant Corporation Attachments cc: Marshall Hyatt, EPA N. Fiss, AE SEP 03 2002 16:49 FR CLRRIANT CORP ENGINEE 8226529 TO 19197330719 P.01/07 Clariant Corporation Mt. Holly Plant P.O. Box 669246 Charlotte, North Carolina 28266-9246 Engineering Telefax Number: (704) 822-6529 11701 Mt. Holly Road Charlotte, NC 28214 TELEFAX TRANSMITTAL To: Jacquelyn M. Noewll Location/Company: NCDENR- Division of Water Ouality Telefax Number: (91 a) 733-0719 Number of Pages (including Cover Sheet): ,5 Subject: Signature Pages for NPDES Permit Renewal Application From; Gary Situderson Date: Septener 3, 20Q2 Phone Number: (704) 822-2787 Notes: The: ignaturpages and a cover letter were trailed on August 27, 2002. The package was supposcc to be sent via FEDEX. Since you have not received it, lam worried that ur mail goup may have sent the material via the postal service. I will heck thi. ut en T uesday Sept. 4t. o for the trou lc If you need to call me., my number is (704) 822-2787_ • NCDENR-DIJQ Fax =►=>t- Tr ansrri i t Conf _ Re?port >E->+- Sep 3 '02 15:04 NCDENR-DIJQ ---> 94670311 No. 0001 Mode NORMAL Time 0'46" Pages 1 Page(s) Result 0 K Continued from Page 2 EPA ID Number (copy from Item 1 of Form 1) NCD001810365 ,: .- 1 • 1I: •I Complete one set of tables for each outfall. Annotate the outfall number in the space provided. on separate sheets numbered VII-1 and VII-2. A,B,C, & D: See Instructions before proceeding. Tables VII-A, VII-B, and VII-C are included E: Potential discharges not covered by analysis - which you currently use or manufacture as an is any toxic pollutant listed in table 2F-2, 2F-3 or 2F-4, a substance intermediate or final product or byproduct? or a component of a substance (go to Section cc 1 1 Yes (list all such pollutants below) I 1 No See Form 1 and Form 2C - General 0utfall 001. Stormwater discharged to treatment. • •L. ' • . 1 - ' • • 1 : . Do you have any knowledge or reason to believe on a receiving water In relation fo your discharge information for pollutants in to the WWTP is not tested that any biological test for acute or chronic toxicity has been within the last 3 years? effluent separately made on at prior any of your discharges or (go to Section 1 Yes (list all such pollutants below) 1 1 No See Form 1 and Form 2C - All effluent at 0utfall 001 in discharged to the WWTP is not Were any of the analysis reported in item VII performed toxicity testing is performed on accordance with NPDES Permit No. NC0004375. tested for toxicity prior to treatment. by a contract laboratory or consulting firm? number of, and pollutants firm below the WWTP final Stormwater (go to Section X) nYes (list the name, .address, and telephone No analyzed by. each sych laboratooLor A. Name B. Address C. Area Code &Phone No. D. Pollutants Analyzed See Form 1 and Form 2C 1 certify under penalty. of law that super vision in accordance with a system the Information submitted. Based on directly responsible for gathering the belief, true, accurate, and complete. including the possibility of fine and imprisonment this document and all attachments designed to assure that qualified my Inquiry of the person or persons Information, the information submitted I am aware that there are significant for knowing violations. were prepared under personnel properly who manage the system is, to the best of penalties for submitting my direction or gather and evaluate or those persons my knowledge and false information, A. Name & Official Title (type orprint) B. Area Code and Phone No. C. Signature D. Date Signed EPA Form 3510-2F (Rev. 1-92) Page 3 of 3 SEP 03 2002 16:49 FR CLARIANT CORP ENGINEE 8226529 TO 19197330719 P.03/05 'EPA IDNumber (copy from Bum !of Form 1) Continues trom Page 2 NCD001810365 . VII, Dl ohargo lnform:Lilo o: See instructions baforo proceeding. Complete one set Of tables for each outfaL Annotate the outran number in the space provided. Table* VII A VH-t, told vll-C are Included on separate sheets numbered VII-1 and VII.2. E: Potential discharges not covered by analysis - is any toxic pollutant listed in table 2F-2, 2P-3 cr 2F-4_ a nubstanca nr a component of a substance which you currently use or manufacture as an intsrnedlate or final product or byproduct? r--t n Ye s�llst all such e2fIutantr below) I I No (Bo to 5ecilon DQ See Form 1. and Form 2C - General information for pollutants in effluent at 0utfall 001, Stormwater discharged to the WWTP is not tested separately prior to treatment. VII1. SIols1 Do you have any knowledge or reason to believe that tiny tifologIcaf testfor acute orchrontctoxtdty has been made on any of your discharges or on o rebsiving water In relation to your discharge within the last 3 yue's? 11 Yoe (IIst an avcrtJx)uuranrs blow) 7 No (go to Section Al See Form 1 and Form 2C - All toxicity testing is performed on the WWTP final effluent at Outta1i 001 in accordance with NFEIES Permit No. NCU004375, Stormwater discharged to the WWTP is not tested for toxicity prior to treatment. 1X. Contrast Analyslg]nformat14n We any of the analysis reported in item Vil performeid by a contract laboratory or consulting firm? Li You (lla7 OK, name, ,address, and tolaphone ftumber of, and pollutants cnajyzest by, a oh, Ig rah:st4raro/7rterm bslaw.) A Nam* See Form 1 and Form 2C D.Addro,s n Na (©o to Secdon a) C. Aroa Code & Ptronu No. D, Pollutant, Analyzed 1 certify under penalty_ of law that this document and all attachments were prepared under my direction nr supervision In accordance with.ri system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persona who manage the system or those greens directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, Imo, (Accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fine end Imprisonment for knowing vlolstians. A. Name & Official Trite (type ornnnr) L, G 0 LDa1C ?7► ,E 3 t 171si i i G. E16naturo M Z°- EPA Form 3510-2F (Rev, 1.92 s Page 3cif 3 %J, f1rv� Cvdo end Pm,une No. (.304() $ 1770. 1 0. Date Signed 97/01(144.2 SEP 03 2002 16:49 FR CLARIANT CORP ENGINEE 8226529 TO 19197330719 P.03/05 Continued from Page 2 EPA IQ Number (copyhom Mem i cf Form 1J NCD001810365 YII.DI2 harge lnliymallon_ A,B,C, & o: See instructions before proceeding. Complete one set of !tibias for each outfall. Annotate the outfall number in the space provided. Tables Vtl-A. VII-B, and V11-0 aro Included on sepaate shoats numborad VIl-1 and VII.2. E: Potential discharge? not covered by analysis Which you currently use or manufacture as an - is any toxic pollutant listed in table 2F-2. 2P-3 or 2F-4, a substance intermodlate or final product or byproduct? or a cornpnnant of a substanc (go to 5ectlon DQ n Yee (11st all such Eollutants below) l No See Form 1 and Form 2C - General Outfall 001. Stormwater discharged to treatment. information for pollutants to the WWTP is not tested that any biological teat tot acute or chronic toxicity has been within the last 3 year:? - in effluent separately made on at prior any of your discharges or (go In Sectfart 1X : • ... t -. .e 1. - Do you have any knowledge or reason to believe on a robDiving water In rotation to your discharge n Yea (Itst art accti pollutants below) NO . See Form 1 and Form 2C - All effluent at 0utfall 001 in discharged to the WWTP is toxicity testing is performed on accordance with NPDES Permit No. not tested for toxicity prior to treatment. by a contract laboratory or ocnsulting firm? Dumber or, and pollutants firm WOW) the NC0004375. 4 WWTP final Stormwater (go to Sect/on X) IX. Contract Analysts Informatio Werra any of the analysts reported in item VII per•fornted Yee (list the name, .address, and telephone erfutizadjay. ouch snot? 11300[7171 .n No A Name B. Address C. Aroa Code &'Phone No. D. Pollutants Analyzed See Form 1 and Form 2C this document and all attachments designed to assure that qualified my Inquiry of tho parson or poreons information, the Information submitted aware that there are significant for knowing violations, were prepared under personnel properly who manage the system is, to the best of penalties for submitting my direction or gather and evaluate or those persons my knowledge and false Information, X. Certifica .1 1 certify Under penalty. of law that supervision in accordance with.a system the Information submitted_ Based on directly responsible for gathering the belief, true, accurate, and complete. (ani including the possibility of fine and Imprisonment A. Name as Official Trtle (type orprfm) 1CeNas-1 vrtt L. G 0 CD Et ram% (? '►S b CZ" .D, a, Area code nna Phone No. 0o') 3 S t—?v3 ) G. Filgnaturo � X ✓j/ff� r - — — Q. Dote Signed �/ efeSCQ EPA Form 3514.2F (Rev. 1.921 Page 3of3 For Approved. OMB No. 2040-0086. Approval expires 5-31-92 Please print or type in the unshaded areas only rfill-in areas are spaced for elite type, i.e., 12 characters/inch). FORM I GENERAL U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER GENERAL INFORMATION TtA Ilia E PA Consolidated Permits Program F o NCD001810365 (Read the "General instructions" before starting.) 1 2 13 14 15 LABEL ITEMS GENERAL INSTRUCTIONS I. EPA I.D. NUMBER If a preprinted label has been provided, affix it in the designated space. Review the information carefully; if any of it is III. FACILITY NAME incorrect cross through it and enter the correct data in the appropriate fill-in area below. Also, if any of the preprinted data is absent (the area to the left of the label V. FACILITY MAILING LIST PLEASE PLACE LABEL IN THIS SPACE space lists the information that should appear) please provide it in the proper fill - in area(s)sbelow. If the label is complete and correct you need not complete Items I, III, V, and VI(except VI-B which must be VI. FACILITY LOCATION II. POLLUTANT CHARACTERISTICS completed regardless). Complete all items if no label has been proved. Refer to the instructions for detailed item descriptions and for the legal authorization under which this data is collected. INSTRUCTIONS: Complete A through J to determine whether you need to questions, you must submit this form and the supplemental from listed in the the supplemental form is attached. If you answer "no" to each question, you excluded from permit requirements; see Section C of the instructions. See a submit any permit application forms to the EPA. If you answer "yes" to any parenthesis following the question. Mark "X" in the box in the third column if need not submit any of these forms. You may answer "no" if your activity is so, Section D of the instructions for definitions of bold-faced terms. MARK "X" MARK "X" SPECIFIC QUESTIONS YES NO FORM ATTACHED SPECIFIC QUESTIONS YES NO FORM ATTACHED A. Is this facility a publicly owned treatment works which results in a discharge to waters of the U.S.? (FORM 2A) ❑ `T ' ❑ B. Does or will this facility (either existing or proposed) include a concentrated animal feeding operation or aquatic animal production facility which results in a discharge ❑ X ❑ 16 17 18 to waters of the U.S.? (FORM 2B) 19 20 21 C. Is this facility which currently results in discharges to waters of the U.S. other than Fi ❑ `s D. Is this proposal facility (other than those described in A or B above) which will result in a discharge ❑ VA ❑ those described in A or B above? (FORM 2C) 22 23 24 to waters of the U.S.? (FORM 2D) 25 26 27 E. Does or will this facility treat, store, or dispose of hazardous wastes? (FORM 3) (Alread �' submitted. Current RCRA X 0 ❑ F. Do you or will you inject at this facility industrial or municipal effluent below the lowermost stratum containing, within one quarter mile of the well bore, underground sources of drinking water? E]® ❑ permit expires 1 / 2 / 07) 28 29 30 (FORM 4) 31 32 33 G. Do you or will'you inject at this facility any produced water other fluids which are brought to the surface in connection with conventional oil or natural gas production, inject fluids used for enhanced recovery of oil or natural gas, or inject fluids for storage of liquid hydrocarbons? ❑ X ❑ H. Do you or will you inject at this facility fluids for special processes such as mining of suffer by the Frasch process, solution mining of minerals, in situ combustion of fossil fuel, or recovery of geothermal energy? (FORM 4) ❑ E ❑ (FORM 4) 34 35 36 37 38 39 I. Is this facility a proposed stationary source which is one of the 28 industrial categories listed in the instructions and which will potentially emit 100 tons per year of any air pollutant regulated under the Clean Air Act and may affect or be ❑ M ❑ J. Is this facility a proposed stationary source which is NOT one of the 28 industrial categories listed in the instructions and which will potentially emit 250 tons per year of any air pollutant regulated under the Clean Air Act and may affect ❑ ❑ located in an attainment area? FORM 5 III. NAME OF FACILITY 40 41 42 or be located in an attainment are? FORM 5 43 44 45 c SKIP 1 Clariant Corporation 15 IV. 16-29 FACILITY 30 - - CONTACT A. NAME & TITLE (last, first, & title) 69 B. PHONE (area code & no.) c 2 Gary P. Sanderson 704 822 2787 15 V. FACILITY 16 MAILING ADDRESS 45 46 48 49 51 52 55 A. STREET OR P.O. BOX c 3 IPO Box 669246 15 16 45 B. CITY OR TOWN C. STATE D. ZIP CODE c 4 Charlotte NC 28266 15 VI. 16 40 FACILITY LOCATION 41 42 47 51 A. STREET, ROUTE NO, OR OTHER SPECIFIC IDENTIFIER c 5 11701 Mount Holly Road 15 16 45 B. COUNTY NAME Mecklenburg 46 70 C. CITY OR TOWN D. STATE E. ZIP CODE F. COUNTY CODE c 6 ( Charlotte NC 28214 15 16 40 41 42 47 51 52 54 EI'A FOR\I 3510-1 (8-90) CONTINUED ON REVERSE SEP 03 2002 16:50 FR CLARIANT CORP ENGINEE tiulr i InuCu hKum I tIk r, yr l 8226529 TO 19197330719 P.04/05 VII.SIC'CODES:(44! it; In ottler.-.ofptio ty) `:.:-. .... , . . _ ..., . A. FIRST'S . ..?'`:= "• *!•�•;Y';':; . •....- .:_ _ -�B:.SECO .. ..: c 286S .1r isPacr�) Dyes and Organic Chemicals :7 " ?spociry) Purification Equipment 3564 15 t7:: ;ta; : 1g •Air _ :. •C. THIRD. . •.....::• ...:.• .'. • • ,• :. ry t.;;. , : • ;. 4 - ,' D. FOURTH ........ 7..: • (specify) 2879 [(specify) I gricultural Herbicide .�':. 4953 Materials Recovery ' 15 16 : -• 17 :, •15:4.4:hl6iex :. :•.:•,.t�19• : F.acilit ES y1II. QPEFti TPRiNF�ORMATION` L IIIIIIIIIIIIIMI . ; .; , ;,...;....•. ...-.. .._,._ r.r•: ..:..E.1•-•1'PLNAM . yr tt:1,• •. ruy.,,.. ... .,...;... .,R' •;"•'B. 1 � . ... - .. ::L . �??�.� : .. , ... .... .. .... Is► we•natne: nstect1• ltern c•111! �VIII-A also the rainier? g .ICLariant Corporation NO I. � •0,.8T/NGtIS;OE4PERAtc • .YES (altar priete,•lafter`nteixitenswerbox;•1Potheaspecify.) ':.:,: ''p'PHONEfereac de.&.no) . F.-T) . FS " ,°: M - PUBLIC (Mar Man rotlerdlorsfdle) "r O = OTHER (5pechyj ,_ pp I (specl4y) P -?�: A'; r..w 704 ". =� 822• 2787 • is uL_"1 F ::4,55v..I 11.;: - .F.i5:a:.18:"e I :r rill : 22' •• -•: r- . °."; i'81:' fir.:Fr.. 11.v1.«.•':? :e=... OR iMBQ%C-.:w `' Wiz,: t..:: -.r l:i:::. _ '.i:.. : �.: �: cr�:�" r i;: n'y "y`` :.: •'^= �.*.:..,�w ,.,.,,,� P0 Box 669246 r;xs :R.CIT'rOR'TOWN A.K.,. .,-4..`•� r:! t•:=1 G. STATE H. ZIP CODE 7.IL .. ' °n ' - Charlotte 4 NC 28266 y(1044:1111 i° . .+"'�•';4-' 15"• fit. :.'.�:�•1),. ..•:.• : -:::::.-r,.Guk'.:M1.iJ" ..7 a s 1�� AO:tt,i:ttNr _., - ,,, t eT ( 0 S r#friBS:t4• Sr1t+'Ii =r`Wdfe0;1i;: •' :u ;Ms. POM ERi15SIPrF6" . fir°I'ropaB:fL'SQ.. r•; t$? +"', _," •. '; q• N. N00004375 .,,:i _ ' 08542R05 P•• -• Ts o. .tr. to . .1 .... 1,4., •... c,•% _ v II.G•(Undargrnrmd lnjecdorr of p�uids.,.r. : n,;: a E y .OTEIE fa +(Y) (S v1 t, , 7.; 9::. i U_, ..,, N/A -s., -,"•a ' :-1, NC000037 Stormwater 15 •.16 �:ir r:j .-1:•-.• :_• ...J: F' . '' :.Y Y .... ,_ .14_ 1.70c..RCR C rs la:Wasfa)1;:3` x.u? eg: '-.: "t OT13eftt(specby) ..-. , (Spec► c - Col ':?I.::a ., , w•-• . II r Et.._ k a: ;r-ls NQDOO1$10365 'h :.r.'' 00537 Landfill 15 r71fi. ;(t7i+ ielera lOi 4,41A I.: e,; earls. Bw 3a ::xr'.:s:+rwt . ,30.:* :.ail - Att r tr p?). rr c_rid ses "'`' • t liw.pi: `efaeUity�;.•� . fl n lfs. e)t hazaidaus►Waste area ant; sto ,mar � oa', tl?#�a f tom: ,an rivers an�#othe[ sur.(ace� otee-';bo w' :(r higniap, earxitans.Erne. XII. NATURE OF BUSINESS. (A (iidkarlsF.l 10$0 p n1•i: ff�ss eah or`ias na u alf springs; The Clariant Corporation operates an integrated organic chemicals manufacturing facility on the Catawba River at Mount Holly, North Carolina. The site includes a batch organic chemical production facility which currently produces dyes for use in the textile industry a herbicide active ingredient and specialty chemials. The site also receives"3rd party wastewater from off -site OCPSF, textiles and soap and detergent manufacturers. The on -sit manufacturing of dyes will cease in December 2002. New wastewaters from on -site operations for regeneration of air pollution control catalysts and transporation equipment cleaning will be generated beginning in late 2002. All site wastewater is treated in an activated sludge wastewater treatment plant (WWTP) and discharged to the Catawba River. Additional information on future wastewater sources is attached. XIIV.CERT!FI.CATION_Gsee. insiticji049 I pe,rtis under.' enaltygf lalwrtfia lhave~' dr;¢o : ' art ritlachment Pa'nd that 6ased��t �" p i,�'"�,>�rnlne�e�. gin, 7n1 rf��Off(f:the`Tc r �� on"SYflSfiiife�Tif•ti7s'.�'ppl(Catioirsnai: (r' lhgtf�yri tliase: rsorts wit►ed slleljciesporis161e.�rco(jtarriltiq<the inforrnetfon;contained it the application,; t he)IAv t "that the11 ifarmahp %.0 tclie, aacurat ,egl ,d h,plete. -1 am alvare tiierthere`'are slgnlfcarit penalties. for submlttlng-fa)se.►nforrriation, incfl atirt-t�re, �0$stb►l .offffneandim•►fsonment A. NAME & OFFICIAL - 1 LE ( pe or pnn !;"• - 4„.e4 �.. i/%e. x, COMME,NTSi!oR OFFICIAL CI,SE :QNL 1., j 1. c. EPA 1 ORN1 3510-1 (8-90) 62 1. ■ 1000 0 y 1/2 • 1 i' • • x651 t i/ f SCALE: 1: 24000 0 INIII 11011 I y' .1 • rt oJL� H O OUTFALL 001 .: eM74); LATITUDE: 35°16' 45" LONGITUDE: 81°00' 35' 2000 4000 6000 CLARIANT CORPORA I iON PROPERTY CHARLOTTE, NORTH CAROLINA 8000 REFERENCE: BASE MAP TAKEN FROM USGS QUADRANGLE MAP MOUNTAIN ISLAND LAKE, NORTH CAROLINA, (DATED 1969) AND MOUNT HOLLY, NORTH CAROLINA, (DATED 1970). 1 MILE 10,000 FEET JULY 2002 LOCATION MAP AENVIRONMENTAL INC /IP21® D. AEI PROJECT No. N130-20 TRUCKS 34 40 THIRD PARTY OCPSF TRUCKS 50 10 SEMIWORKS & WAREHOUSING TRUCKS 60 0 0 co THIRD PARTY NON—OCPSF (FUTURE) 34 40 60 ALKALINE ACID SEWER SEWER 55 55 THIRD PARTY OILY WATER PROCESSING (PLANNED & FUTURE) 115 200 AIR FILTER REGENERATION (PLANNED) 55 GROUND WATER REMEDIATION RCRA 120 CERCLA 30 115 FUTURE TENANT EXPANSION (OCPSF & NON —CATEGORICAL) 75 HERBICIDE INTERMEDIATE (SPECIAL CHEMICAL) 200 115 50 UTILITIES (NON —CONTACT COOLING) EVAPORATION 25 50 UTILITIES (STEAM GENERATION) 50 STORM WATER 283 GENERAL NOTES; 1. ALL FLOWS ARE IN 1,000 gpd AND ARE AVERAGE DAILY FLOWS. 2. FLOWS ARE BASED ON EXISTING OPERATION AND FUTURE (PLANNED) ACTIVITIES. DYE MANUFACTURING OPERATIONS ARE SCHEDULED TO BE SHUT —DOWN IN DECEMBER 2002 AND ARE NOT INCLUDED IN FLOW DIAGRAM. 3. NO LOSS OF WATER TO PRODUCT OCCURS DURING MANUFACTURING. 4. STORMWATER IS BASED ON A 0.118—INCH RAIN. POTABLE WATER CITY OF CHARLOTTE SANITARY WASTE 28 WATER TREATMENT FILTER PLANT BACKWASH 70 NEUTRALIZATION 1 STORM FLOW STORAGE i STORM FLOW STORAGE PRIMARY CLARIFIERS SLUDGE FILTRATION SLUDGE LANDFILL 670 WATER INTAKE I EQUALIZATION STORM FLOW STORAGE SETTLING CANAL STORAGE 73 EVAPORATION ACTIVATED SLUDGE 70 CATAWBA RIVER FLOW SECONDARY CLARIFIERS POLISHING POND i POLISHING POND POST AERATION EFFLUENT METERING 1177 8/20/02 3 7/30/02 K.S. K.S. AWARE ENVIRONMENTAL INC. — DOC No. 13020p02.DWG TFIS CRANING IS A PRMAE AND C0f10041141. COMMUNICATION AND THE PROPERTY OF CLAMANT CORPORAION. MT. HOLLY PWRT. R mar NOT BE COPIED OR LOANED MAHOUT 1IE came OF CLAMANT CORPORATION. AO MST BE PROMPTLY RETURNED ON REQUEST OR COLIPLE110N OF ORDER. THIS ORMOND W1S BEEN CREATED W H NQ4I1r. CO NOT MIAOW DRAFT ON MATS COPY. Clariant Mt. Holly Plant. P.O. Box 669246, Charlotte, North Carolina 28288 AWARE ENVIRONMENTAL INC. — DOC No. 13020p02.DWG ARM. PROJECT MOWER DATE APPA. RAW JYT'L/IR6i APPROVED BY 2 7/18/02 DH REVISED STREAM FLOW RATES. ADDED SEMIWORKS & WAREHOUSING 1 8/21/02 DH REVISED STREAM FLOW RATES APP L MAINTENANCE A.P.D. MUMS APPROVED BY MP'0. PBGDUCIIQI APP'LL SAiETYA:mem FUME 83420102 FIGURE 3 DEPARTMENT 50 PROCESS FLOW DIAGRAM WATER FLOW SCHEMATIC NPDES PERMIT NC0004375 0 1/19/01 ON ISSUED FOR RECORD REV. DATE PROJECT NO. DRAWN CHECKED AR°P.D. REVISION DESCRLFIToN APPROVED BY APPROVED BY PLAT SCALE RAID 1 1 NONE SHEET NO. 11 OF 1 7N60.53.050.01.8342 REV. No. TABLE 1A (Attachment to Application Form 2C) Process Design Summary Clariant Corporation WWTP Clariant Corporation, Mt. Holly, NC EPA I.D. Number NCD001810365, NPDES No. NC0004375 Item Value pH Neutralization Tanks Total No. of Tanks(') Volume per Tank Tank Diameter Tank Height Detention Time per Tank @ 1.045 MGD Primary Clarifiers Total No. of Tanks Volume per Tank Diameter per Tank Side Water Depth per Tank Surface Area per Tank Surface Loading Rate @ 1.045 MGD Aeration Basin ZO3A Volume Depth Detention Time @ 1.045 MGD Aeration Basin Z04 Volume Depth Detention Time @ 1.045 MGD Secondary Clarifiers Total No. of Tanks Volume per Tank Diameter per Tank Side Water Depth per Tank Surface Area per Tank Surface Loading Rate Using 1 Clarifier @ 1.045 MGD (2) Effluent Storage Basin — ZO2C Volume Surface Area Depth Filter Press Number of Units Type Sludge Handling Capacity Average Cake Solids 2 20,000 gallons 14ft 19ft 28 min 2 146,800 gallons 50 ft 12ft 1963 ft2 266 gpd/ft2 4.5 MG 16ft 4.3 days 2.5 MG 15ft 2.4 days 2 500,000 gallons 80 ft 12ft 5026 ft2 208 gpd/ft2 360 MG 25 acres 40 ft 2 Belt 120 gpm 25-30% (1) Lime addition for neutralization is alternated between tanks. (i.e. lime is not added simultaneously to both tanks.) (2) Typically only 1 clarifier is used. 13020t002 Page 1 of 1