NC0004375_More Information (Received)_20020806

NPDES DOCU ENT ! CANNINO COVER SHEET
NPDES Permit:
NC0004375
Clariant Corporation
Document Type:
Permit Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Engineering Alternatives (EAA)
Correspondence
Owner Name Change
(Additional
Information Received ..f
Instream Assessment (67b)
Speculative Limits
Environmental Assessment (EA)
Document Date:
August 6, 2002
This document is printed on reuse paper - more any
content on the reirerse side

iin
1.4
NE► APPLICATION SUPPORT DOCUMENT
PERMIT RENEWAL AND MODIFICATION
NPDES PERMIT NO. NC004375
..' CLARIANT CORPORATION -MT. HOLLY EAST PLANT
1.1
mil
rug
MI
Pmq
Prepared for:
Clariant Corporation
PO Box 669246
Charlotte, NC 28266-9244
Prepared by:
AWARE Environmental® Inc.
9305-J Monroe Road
Charlotte, NC 28270-1490
AEI Job No. N130-20
AEI Document No. 13020r001
August, 2002

Firt
TABLE OF CONTENTS
Section No. Description Page No.
TABLE OF CONTENTS i
LIST OF TABLES ii
LIST OF FIGURES ii
LIST OF APPENDICES iii
1.0 BACKGROUND 1
1.1 GENERAL 1
1.2 EXISTING WASTEWATER SYSTEM 3
1.3 FACILITY CHANGES 5
1.3.1 Shutdown of Dye Manufacturing 6
1.3.2 SCR -Tech 6
1.3.3 Seaboard Container Cleaning Corporation 6
Fisi
2.0 WASTEWATER CHARACTERISTICS AND SOURCES 8
2.1 DISCHARGE CHARACTERISTICS 8
,., 2.2 WASTEWATER SOURCES 8
2.2.1 General 8
2.2.2 OCPSF Category 13
0.+ 2.2.3 Centralized Waste Treatment (CWT) Category 16
2.2.4 Non -Categorical Wastewaters 19
3.0 EFFLUENT GUIDELINES AND STANDARDS 24
3.1 GENERAL 24
3.2 CONVENTIONAL PARAMETERS 24
3.3 NON -CONVENTIONAL PARAMETERS 30
3.4 TOTAL NITROGEN, TOTAL PHOSPHORUS, PHENOLICS 31
i FINAL, 8/21/02

Pal
Table No.
LIST OF TABLES
Description Page No.
1-1 Production Data for the Last Three Years 2
2-1 Effluent Flow Data Summary 9
2-2 Wastewater Flow 14
2-3 Seaboard Container Cleaning (SCC) Process Wastewater Stream 18
2-4 Projected Daily Wastewater Flow From Seaboard
Container Cleaning (SCC) Operations 18
�► 2-5 SCR -Tech Process Wastewater Stream 22
2-6 Projected Daily Wastewater Flow From SCR -Tech Operations 23
3-1 US EPA Effluent Guidelines and Standards 25
PPIA 3-2 Current and Proposed Limits - Conventional Parameters 27
3-3(a) Tier 1 Wasteload Allocations, Conventional Parameters By
Industrial Category 28
3-3(b) Tier 2 Wasteload Allocations, Conventional Parameters by
Industrial Category 29
3-4(a) Tier 1 OCPSF Proposed Limits - Non -Conventional Parameters 32
PIM
3-4(b) Tier 2 OCPSF Proposed Limits - Non -Conventional Parameters 34
3-5(a) Tier 1 CWT Proposed Limits - Non -Conventional Parameters 36
3-5(b) Tier 2 CWT Proposed Limits - Non -Conventional Parameters 37
3-6(a) Tier 1 OCPSF & CWT Proposed Limits - Non -Conventional
Parameters 38
3-6(b) Tier 2 OCPSF & CWT Proposed Limits -
Non -Conventional Parameters 39
PEI
Figure No.
LIST OF FIGURES
Description Page No.
1 Average Effluent Total Nitrogen (June 2001-May 2002) 10
2 Average Effluent Total Phosphorus (June 2001 - May 2002) 11
3 Wastewater Flow Schematic 12
4 Probability Plot of Effluent NH3-N (June 2001-May 2002) 30
ii FINAL, 8/21/02

PrI
LIST OF APPENDICES
A June 2001-May 2002 Effluent Data Clariant WWTP
B Priority Pollutant Analysis Clariant WWTP Effluent
C Norflurazon Production Schematic
D stormwater determinations Clariant-Mt. Holly East Facility
0' 3RD Party Solicited Wastewaters 2001-2002 Clariant-Mt. Holly East Facility
F Section 14.8.3.3.1 USEPA Development Document For The CWT Point Source
Category
G Statistical Analysis of Effluent NH3-N
mai
H Proposed Effluent Limits for Non -Conventional Parameters
iii FINAL, 8/21/02

0111
SECTION 1.0
BACKGROUND
0,1 1.1 GENERAL
Clariant operates a specialty chemical and dye manufacturing facility in Mount Holly, North
"'' Carolina (Clariant-Mt. Holly East Plant). Wastewater from the facility is treated in an on -site
wastewater treatment plant (WWTP) and discharged to the Catawba River under NPDES
Permit No. NC004375. The current NPDES permit, which became effective in 1991, was
issued by the North Carolina Department of Environment and Natural Resources (NCDENR)
and is based on the US EPA OCPSF effluent guidelines.
1.4
based dyes, specialty organic chemicals and a pesticide (norflurazon). Clariant-Mt. Holly East
production amounts for the years 1999, 2000 and 2001 are shown in Table 1-1. The
fm,
forecasted OCPSF organic chemical manufacturing volume for 2002 is 33,000,000 to
mg,38,000,000 pounds.
The facility has been a specialty chemical and dye manufacturing site since 1937. In recent
years the primary products produced by the Clariant-Mt. Holly East facility have been sulfur-
Due to the recent decline in the US textile industry, dye manufacturing operations are currently
being substantially reduced at the Clariant-Mt. Holly East facility. Clariant plans to
pal discontinue textile dye manufacturing at the facility after 2002. However, OCPSF activities
related to on -site dye bulk storage/warehousing operations, batch specialty chemical production
and pesticide intermediates production are remaining active and will continue to generate
wastewater which will be treated in the on -site WWTP. Wastewater from norflurazon
`.R production is currently collected and hauled off -site for disposal through incineration and is not
discharged to the Clariant WWTP.
As a result of historical OCPSF operations, the facility is included on the National Priorities
List due to organic contaminants contained in surface water and groundwater from the site.
Stormwater from the facility is therefore treated in the on -site WWTP in addition to the
1 FINAL, 8/21/02

Pawl
Fori
torl
fori
004
TABLE 1-1
PRODUCTION DATA FOR THE LAST THREE YEARS
' r $ ` :
z {
Y f
Year
.}a 2 `F' ,
-� . 'Y
.,.. ,f�8_ �� ,.,
'tt' . SS ' ri gani " `Y
fF rf.' 'YT�y+ �'"RY t< h III.
�')s t"S C"' ' `�" �
x Chenueal Ifgg.. r, ,
;rPesticide Active
S" f •5y ?µ{�,.' tr . 41s, ran: d f5 ' 'S 1r
hf �j ` "�
Ingre°'d en- Mfg.. z
�. "T ,y' ,,t„4-C�ti i f
�� �'t�r4 �� s ����!;;f♦.e 7t ±"
C , 1'ij , Volum!•es 1 4
k0 CRS. ° ° s
.... :,I f.i ... �.. r { S'� -st. v+
) 6`'� - 9E" eY ",,,,%I 4 +¢�+^r i �~ f
jl a2Yy a4a i' �Sk S "t
ese.4 ,1:Yak- '±.2.
ce.(: t Y ,
�f�j
Z�4:,Sn`��1�F.=��Sv-.—��"��� �:.. ��....
1999
78,733,900 pounds
1,045,835 pounds
2000
65,135,700 pounds
1,670,455 pounds
2001
50,873,800 pounds
1,323,139 pounds
2 FINAL, 8/21/02

Pal
OCPSF process wastewater and domestic wastewater from current on -site manufacturing
ran, operations. The WWTP receives groundwater from a groundwater pump and treat system and
leachate from an active on -site landfill cell. Treatment in the on -site WWTP of leachate,
MEI groundwater and stormwater from the facility are continuing. Beginning in 2001, additional
wastewaters from off -site OCPSF and related textile operations are also, with prior approval
from NCDWQ, being hauled to the Clariant facility for treatment in the on -site WWTP.
Cal
As dye manufacturing portions of the facility become inactive, Clariant is developing the
facility as an industrial park for compatible industrial operations. The following two (2) new
tenant operations are planned for immediate location at the facility with the treatment of the
resulting process wastewaters in the on -site WWTP:
• SCR -Tech - A non -categorical operation that regenerates NOx air pollution control catalyst;
and
• Seaboard Container Cleaning - A categorical operation (transportation equipment cleaning
point source category) that cleans railcars used in the transportation of petroleum cargo.
Clariant also plans to add other additional compatible industrial tenant operations as dye
manufacturing operations are eliminated and on -site areas become available. Wastewater from
the additional tenants will also be treated in the on -site WWTP. It is expected that most of the
tenants will be OCPSF categorized operations.
With the changes in dye manufacturing and inclusion of the new wastewaters described above,
Clariant is requesting permit modifications which will result in a significant net reduction in
the currently allowed wasteload discharge from the Clariant-Mt. Holly East facility.
1.2 EXISTING WASTEWATER SYSTEM
The Clariant Mt. Holly East site has two separate sewer systems, an alkaline and an acid.
Both carry stormwater to the on -site WWTP for treatment in addition to carrying wastewater
from site buildings.
3 FINAL, 8/21/02

The acid sewer is a gravity system that terminates in a lift station at the WWTP. The lift
station pumps acidic wastewater to a primary treatment process. It can also pump water into
two lined impoundments for storage. The lined storage impoundments have a capacity of 2.5
MG. The acid sewer system has a capacity of 500,000 gallons per day.
The primary treatment process includes two neutralization tanks that operate in series. Lime
slurry is pumped into each neutralization tank in a continuous manner for neutralization of
acidic wastewater. The neutralization process can accept up to 750,000 gallons per day of
acidic wastewater at pH 0.5.
The alkaline sewer is a gravity system that terminates in a lift station at the WWTP. The lift
station pumps alkaline wastewater to a mixing chamber downstream of the two neutralization
tanks where the acid and alkaline sewer streams are mixed together. The lift station can also
pump water into two impoundments. These storage impoundments have a capacity of 3.5 MG.
The alkaline sewer system has a capacity of 4,500,000 gallons per day.
The combined and neutralized sewer streams flow into two primary clarifiers that operate in
parallel. Primary solids and calcium sulfate, from the neutralization process, settle out and are
pumped to two sludge holding tanks. Clarified wastewater flows by gravity from the primary
clarifiers to a 4.5 MG equalization basin. The two clarifiers are designed to handle a total
1.1 wastewater flow of 5,200,000 gallons per day.
The primary sludge is pumped from the sludge holding tanks to one of two continuous belt
filter presses for dewatering. Dewatered sludge is accumulated in dump trucks and is hauled
to a lined landfill on the site.
The 4.5 MG equalization basin has several mixers and aerators in it. Wastewater flows from it
by gravity to a 2.5 MG activated sludge aeration basin. The aeration basin has jet mixers that
pim
4 FINAL, 8/21/02
maintain a homogeneous mixture of sludge and water. Four aerators provide dissolved oxygen
for the mixed liquor bacterial population.
1.1

Mixed liquor from the aeration basin flows by gravity into two secondary clarifiers. Settled
biological sludge is returned to the aeration basin. Waste activated sludge is pumped to the
primary clarifiers where it mixes with primary sludge and is settled out for dewatering and
landfilling. The secondary clarifiers are designed to handle 5,000,000 gallons per day of flow.
Treated effluent exiting the secondary clarifiers flows through an exit canal paralleling the
WWTP. The canal flows to a small final exit pond that has an aerator in it to provide positive
dissolved oxygen prior to release into the Catawba River. The exit pond has an effluent lift
station in it and an exit valve that can shut off flow to the river.
The effluent lift station can deliver the entire flow of the exiting effluent to a lined 360 MG
effluent holding basin for storage and re -treatment through the WWTP. If any of the permitted
effluent parameters are expected to be impacted by a process upset or spill in the complex, all
of the WWTP throughput is pumped into the effluent holding basin. Based on the WWTP flow
rates treated in 2001, the effluent holding basin can store up to 225 days of plant wastewater
throughput. Water that is diverted into the effluent holding basin is eventually released back
to the WWTP equalization basin and re -treated through the activated sludge system prior to
discharge.
1.3 FACILITY CHANGES
Clariant has no plans to modify any of the on -site WWTP processes or components. Although
changes are planned for the site manufacturing and warehousing operations, the wastewater
they produce is compatible with existing WWTP design. Clariant is converting the
underutilized portions of the Clariant-Mt. Holly East facility into an industrial park, as space
becomes available. A brief discussion of the planned initial site utilization changes is presented
below.
5 FINAL, 8/21/02

t�1
1.3.1 Shutdown of Dye Manufacturing
(=I Clariant operates one remaining textile chemical and dyestuff plant within the complex.
This plant will be shut down prior to January 1, 2003. It will be cleaned and
mothballed shortly thereafter.
''°g 1.3.2 SCR -Tech
SCR -Tech regenerates NO. catalyst used for air pollution control in the fossil fuel
co` burning electrical power generation industry. Clariant is currently negotiating a lease
agreement with SCR -Tech for location of their operation at the Clariant-Mt. Holly East
awl
facility. Plans are to have a signed lease in August 2002. The lease will allow SCR -
Tech to occupy Building 48 within the Clariant facility (one of our mothballed
production plants) for their catalyst regeneration process and begin operations in late
2002. SCR -Tech will also occupy warehouse, laboratory, and office space at the site.
SCR -Tech will begin demolition and re -construction of the plant in late August. Their
current plans are to begin catalyst regeneration operations in November 2002.
1.3.3 Seaboard Container Cleaning Corporation
Seaboard Container Cleaning Corporation (SCC) is a railroad tank car cleaning firm
PIA currently located in Hamlet, North Carolina. Their primary customers send tank cars
that have been used to haul petroleum products. Clariant has been negotiating a lease
F°+ agreement with SCC for several months. The agreement has not yet been finalized.
oft' SCC will lease track spurs and several acres of ground within the Clariant Mt. Holly
East facility. Their process will include an oil/water separation process that utilizes
both phase separation and membrane filtration to lower the oil & grease content of their
effluent to less than 100 mg/1.
Clariant has currently been receiving truck shipments of SCC wastewater for over
pc,
seven (7) months as a trial of their quality control and process reproducibility and
f
6 FINAL, 8/21/02

confirmation that the SCC wastewater is compatible with the on -site WWTP. Their
process has generated a very good quality effluent during this period.
7 FINAL, 8/21/02

SECTION 2.0
WASTEWATER CHARACTERISTICS AND SOURCES
2.1 DISCHARGE CHARACTERISTICS
Effluent data from the Clariant-Mt. Holly East facility discharge monitoring reports (DMR)
''q submitted to NCDWQ for the period of June 2001 through May 2002 are summarized in
Appendix A. Average daily flows for the latest 12 months of available data are also presented
At\ in Table 2-1. As shown in Table 2-1, the average effluent flow for the 12-month period of
June 2001 through May 2002 is 0.61 MGD.
As required by the current NPDES permit, Clariant has collected one (1) effluent sample per
FRI
month and analyzed for total nitrogen (TN) and total phosphorus (TP). For the period of June
2001 through May 2002, TN and TP effluent monitoring results are shown respectively on
Figures 1 and 2.
A summary of priority pollutant analytical testing performed over the past 12 months is
included in Appendix B.
2.2 WASTEWATER SOURCES
2.2.1 General
RA, A water flow schematic for the Clariant-Mt. Holly East facility is presented in Figure
3. Wastewater present or planned for immediate inclusion are from the following
'a.1 industrial categories of the US EPA Effluent Guidelines and Standards:
• OCPSF (40 CFR Part 414);
• Centralized Waste Treatment Point Source (40 CFR Part 437); and
• Non -categorical industrial wastewaters.
8 FINAL, 8/21/02

f�1
AEI
PEI
Ott
Prl
TABLE 2-1
EFFLUENT FLOW DATA SUMMARY
Year �t
-s Months : ;
le P. D•ailyx ov. (tYtD
r
2001
June
0.930
2001
July
0.770
2001
August
0.780
2001
September
0.630
2001
October
0.410
2001
November
0.640
2001
December
0.590
2002
January
0.610
2002
February
0.330
2002
March
0.490
2002
April
0.590
2002
May
0.560
12-month Average Flow (MGD) 0.611
9 FINAL, 8/21/02

JIM l 1 I ] 3 J J! 1 1 1 ) ! 1 1 1
225
200
175
150
J
Y 125
o c
0
f
L.
it 100
c
0
75
50
25
0
Figure 1. Average Effluent Total Nitrogen (June 2001-May 2002)
Jun-01 Jul-01 Aug-01 Sep-01 Oct-01 Nov-01 Dec-01 Jan-02 Feb-02 Mar-02 Apr-02 May-02
• TN mg/L
BAT Eff TN
Final 13020s003
8/21/02 Fig1

111 J 1 1 1 1 1 I I 1 3 3 ] ] $ i
5.5
5.0
4.5
4.0
. 3.5
E
r 0
3.0
E
c 2.5
0
c
0
U 2.0
1.5
1.0
0.5
0.0
Figure 2. Average Effluent Total Phosphorus (June 2001-May 2002)
10C Xi 30I IOC IOC X0 XI X11 101 >X 301 3a xc pa ca\to co co co co
Jun-01 JuI-01 Aug-01 Sep-01 Oct-01 Nov-01 Dec-01 Jan-02 Feb-02 Mar-02 Apr-02 May-02
--®— TP mg/L
a. - BAT Eff TP
Final 13020s003
8/21/02 Fig2

ALKALINE ACID
SEWER SEWER
TRUCKS 34
TRUCKS
TRUCKS
O
O
co
40
50
THIRD PARTY OCPSF
34
SEMIWORKS &
WAREHOUSING
40
THIRD PARTY
NON—OCPSF
(FUTURE)
60
THIRD PARTY
OILY WATER PROCESSING
(PLANNED & FUTURE)
115
AIR FILTER
REGENERATION
(PLANNED)
GROUND WATER
REMEDIATION
55
RCRA 120
CERCLA 30
FUTURE
TENANT EXPANSION
(OCPSF & NON —CATEGORICAL)
HERBICIDE INTERMEDIATE
(SPECIAL CHEMICAL)
UTILMES
(NON —CONTACT COOLING)
200
115
EVAPORATION 25
50
UTILmES
(STEAM GENERATION)
50
STORM
WATER
283
GENERAL NOTES;
1. ALL FLOWS ARE IN 1,000 gpd AND ARE AVERAGE DAILY FLOWS.
2. FLOWS ARE BASED ON EXISTING OPERATION AND FUTURE (PLANNED)
ACTIVITIES. DYE MANUFACTURING OPERATIONS ARE SCHEDULED TO BE
SHUT —DOWN IN DECEMBER 2002 AND ARE NOT INCLUDED IN FLOW DIAGRAM.
3. NO LOSS OF WATER TO PRODUCT OCCURS DURING MANUFACTURING.
4. STORMWATER IS BASED ON A 0.118—INCH RAIN.
POTABLE WATER
CITY OF CHARLOTTE
SANITARY WASTE 28
NEUTRALIZATION
STORM FLOW
STORAGE
STORM FLOW
STORAGE
PRIMARY
CLARIFIERS
SLUDGE
FILTRATION
SLUDGE
LANDFILL
EQUALIZATION
STORM FLOW
STORAGE
WATER [ FILTER PLANT BACKWASH 70 I SETTLING
TREATMENT , CANAL
670 WATER INTAKE
STORAGE
70
CATAWBA RIVER FLOW--�
8/20/02
K.S.
AWARE ENVIRONMENTAL INC. — DOC No. 13020p02.DWG
3 7/30/02
K.S.
AWARE ENVIRONMENTAL INC. — DOC No. 13020p02.DWG
2
7/18/02
DH
REVISED STREAM FLOW RATES. ADDED SEMIWORKS .1c WAREHOUSING
1
8/21/02
DH
REVISED STREAM FLOW RATES
THIS OR'WCIC IS A MATE AND OONFTENTOL COWUNCATgN ADD TIE PROPERTY OF ammo CORPORATIII.
lit HOTLY PLANT. IT KIST NOT BE COPIED OR LQAIED WITHOUT THE CONSENT OF CLAMANT CORPORATION. AND
INST BE PR01EILY RETURNED ON REQUEST OR CCIPLEHON OF ORDER. TABS DRAWING HAS EEEN CREATED WITH
'WIDOW CO NOT NNVUILLY DRAFT ON THIS COPY.
APPn PRoJEcr ENGREER DUE APPn RAN WT'L/WHSE DUE APPROVED BY DATE
1MODENNICE
AAPn MIRES
APPROVED BY
.aNv. PROOUCIION
APie0. SVETIERARO.
FILE NNE
83420102
73
EVAPORATION
ACTIVATED
SLUDGE
SECONDARY
CLARIFIERS
i
POLISHING
POND
POLISHING
POND
POST
AERATION
i
EFFLUENT
METERING
1177
�Clariant
Mt. Holly Plant. P.O. Box 869248, Charlotte, North Carolina 28268
FIGURE 3
DEPARTMENT 50
PROCESS FLOW DIAGRAM
WATER FLOW SCHEMATIC
NPDES PERMIT NC0004375
0
1/19/01
DH
ISSUED FOR RECORD
REV.
DATE
PROJECT NO.
DRAWN
CHECKED
APP.')
REVISION DCScRIPTION
APPROVED NY
APPRO.ED B!
PLOT BOLE RATIO
1-1
"lux 1 S*W No.
NONE , 1 OF 1
790.53.050.01.8342
REV. No.

A breakdown of the flows from each source, by industrial category is shown in Table
2-2. Flow components included in each category are discussed in the following
subsections.
2.2.2 OCPSF Category
ram, The following wastestreams from the Clariant-Mt. Holly East facility are included
under the OCPSF category activities:
• Specialty Chemicals (115,000 gpd) - Clariant manufactures the herbicide
Norflurazon at the Clariant-Mt. Holly East facility. A simplified flow diagram of
the Norflurazon process is included in Appendix C. The first three reaction vessels
`m' in the system produce organic chemical intermediates. OCPSF wastewater is
generated from the aqueous phase separation following these reactions. The organic
MET
phase of the produced intermediates is then sent to the next production stage for the
Norflurazon reaction.
Wastewaters generated from Norflurazon manufacturing are currently hauled off -
site for disposal by incineration and are not discharged to the on -site WWTP.
rim These wastewaters, if discharged, would be subject to regulation under the US EPA
Effluent Guidelines for Pesticide Chemicals (40 CFR Part 455).
Pin
• Semiworks & Warehousing (40,000 gpd) — Clariant will continue to perform the
Semiworks and Warehousing activities on -site. The warehousing operation involves
bulk storage and blending of organic chemicals and dyes. Prepared batches are
stored in bulk storage tanks in the warehouse building. OCPSF wastewaters are
generated by rinsing of tanks and piping between batch changes. The Semiworks
""‘ operation involves custom batch production of small volume organic chemicals.
Wastewater from the production is classified as OCPSF.
13 FINAL, 8/21/02

1 } 1 I 1 1 1 1 1 1 1 1
TABLE 2-2
WASTEWATER FLOWS
Wastewater Source
Existing and Planned Flows
Existing, Planned and Future Flows
Average
Daily Flow
(MGD)
Category
Avera e
g
Daily Flow
(MGD)
Category
Max Monthly
(MGD)(2)
Average
Daily Flow
(MGD)Daily
Category
Average
Flow
(MGD)
Category
Max Monthly
(MGD )(2)
OCPSF(3)
Specialty Chemicals (Herbicide Intermediate)
0.115
0.115
Semiworks and Warehousing
0.040
0.040
Groundwater
0.150
0.150
Stormwater .
0.251
0.251
3rd Party OCPSF WW
0.034
0.034
Future Tenant Expansion
--
0.100
0.590
0.897
0.690
1.05
Centralized Waste Treatment
Future 3rd Party Non-OCPSF WW
--
0.060
0.091
Planned On -site Oily WW (Seaboard Container)
0.055
0.055
0.084
Future 3rd Party Oily WW
--
0.060
0.091
0.055
0.084
0.175
0.266
Non -categorical
Sanitary
0.028
0.043
0.028
0.043
Filter Plant Backwash
0.070
0.106
0.070
0.106
Non -process Area Stormwater
0.032
0.049
0.032
0.049
Planned Air Filter Regeneration WW (SCR -Tech)
0.055
0.084
0.055
0.084
Utilities WW
0.100
0.152
0.100
0.152
Future Tenant Expansion
--
0.100
0.152
0.285
0.433
0.385
0.585
Total Average Daily Flow
0.930
1.250
Notes•
(I) Tier 1 Flow does not include future flows.
(2) Based on historical data (June 2001 - May 2002), max monthly flow is 1.52 times greater than the average daily flow.
(3) OCPSF does not include current wastewater discharge from dye manufacturing operations, which are scheduled to be shut -down by January
1, 2003.
14
FINAL, 8/21/02

• Groundwater (150,000 gpd) — The Clariant-Mt. Holly East site is included on the
National Priority List (NPL) due to organic contaminants contained in groundwater
and surface water. Groundwater is extracted from the site, treated and discharged
to the on -site WWTP for further treatment.
• Stormwater (251,000 gpd) — As discussed above, the Clariant-Mt. Holly East site
is included on the NPL due to organic contaminants contained in groundwater and
surface water. These contaminants resulted from historical OCPSF activities
previously performed at the facility. OCPSF stormwaters include only those
generated due to runoff from areas currently known or suspected of surface and soil
contamination by residual organic contamination or on -going OCPSF activities.
These stormwaters, which are treated in the on -site WWTP for removal of
contaminants prior to discharge, are generated from the following areas of the site:
• Effluent holding basin;
• Landfill Cell 3;
• Production buildings area;
• Former dinitrophenol (DNP) production area; and
• WWTP area.
A detailed description of the OCPSF stormwaters and the basis of average flow
determinations are presented in Appendix D.
• 3rd Party Solicited Wastewaters (34,000 gpd) — Clariant has been accepting 3`d
party OCPSF wastewaters trucked to the Clariant-Mt. Holly East facility since 2001
for treatment in the on -site WWTP. An inventory of the 3`d party wastewaters that
have been treated on -site is included as Appendix E. The 3`d party wastewaters
treated on -site have also included some wastewaters from non-OCPSF operations
with wastewater similar to the Clariant wastewater and compatible with the Clariant
WWTP. These non-OCPSF 3rd party wastes are discussed further in Section 2.2.3.
15 FINAL, 8/21/02

far
Pal
Pat
01114
2.2.3 Centralized Waste Treatment (CWT) Category
Under the modified permit, Clariant will be receiving oily wastes and organic -bearing
wastes from both on -site and off -site sources which are included under the Centralized
Waste Treatment category. Clariant will not receive metal -bearing wastewaters
included under Subpart A - Metals Treatment and Recovery (40 CFR Part 437.10) of
the CWT Effluent Guidelines and Standards. CWT wastes that will be received by
Clariant are described below:
Oily Wastes (115,000 epd)
Oily wastewaters will be generated by the on -site operations of Seaboard Container
Cleaning Corporation (SCC). SCC currently has a rail tank car cleaning operation in
Hamlet, North Carolina. Wastewater from their Hamlet, NC operation is currently
regulated under the Transportation Equipment Cleaning Point Source Category, 40
CFR 442.20 as an industrial discharge to the Town of Hamlet WWTP. SCC primarily
cleans rail cars used in the transportation of petroleum cargo. Clariant and SCC are
negotiating to relocate their operation to the Clariant-Mt. Holly East Site. Their
process uses high pressure water blasting to remove residue from the walls of rail cars.
The material exiting the rail cars is treated with surfactants and other chemicals and
phase -separated in a series of tanks. Recovered oils from the process are sold for fuel
value.
Water from the phase -separation process is then further processed for additional
removal of oils through membrane filtration technology. The settling and membrane
fact filtration provides pretreatment of the SCC wastewater as a part of their rail car
cleaning and oil recovery process. This process wastewater will then be discharged to
my, the Clariant on -site WWTP for biological treatment. The SCC process wastewater
consistently contains very low concentrations of oils and greases. The remaining O&G
components are water soluble varieties and are highly treatable in the activated sludge
16 FINAL, 8/21/02
rgai

PEI
Tarl
fogl
fan
sag
tatt
lei
process included in the Clariant WWTP. SCC process wastewater characteristics are
presented in Table 2-3. Projected SCC wastewater flows are presented in Table 2-4.
At the Clariant-Mt. Holly East facility, SCC will also receive oily wastewater from off -
site sources for processing. These wastewaters will be commingled with in-house oil
bearing waters and processed through the phase separation/membrane filtration portions
of the railcar cleaning operation. The commingled SCC process wastewater will then
be discharged to the Clariant WWTP for biological treatment.
The SCC wastewater would normally be included under the Transportation Equipment
Cleaning (TEC) category. However, based on Section 14.8.3.3.1 of the US EPA
Development Document for the CWT Point Source Category (see Appendix F),
inclusion of the commingled off -site oily wastewaters makes the SCC wastewaters
subject to the CWT standards, Subpart B, regarding oils treatment and recovery.
Organic -Bearing Wastes (60,000 gpd)
Clariant will receive organic -bearing wastewaters from off -site sources. These will be
solicited 3'' party wastewaters from non-OCPSF sources and will include wastewaters,
compatible with the on -site WWTP, from the following categories:
Textile Mills (Part 410)
• Subpart D - Woven Fabric Finishing;
• Subpart E - Knit Fabric Finishing;
• Subpart F - Carpet Finishing;
• Subpart G - Stock and Yarn Finishing; and
• Subpart H - Non -woven Manufacturing.
17 FINAL, 8/21/02

P4
Pin
PIM
Aw
Pim
TABLE 2-3
SEABOARD CONTAINER CLEANING (SCC) PROCESS WASTEWATER STREAM
BOD
TSS
pH
Oil & Grease
Antimony
Barium
Chromium
Cobalt
Copper
Lead
Molybdenum
Tin
Zinc
7,000 - 10,000
20 - 100
9.0 - 9.5
1 - 25
0.11
0.009
0.026
0.053
<0.01
<0.005
2.0
0.006
0.46
Note: Process wastewater parameters shown are following the phase -
separation and membrane filtration portions of process.
TABLE 2-4
PROJECTED DAILY WASTEWATER FLOW FROM
SEABOARD CONTAINER CLEANING (SCC) OPERATIONS
er�od i 'k� t w P ojected era
ar
November 2002 - March 2003
April 2003 - August 2003
September 2003 - January 2004
February 2004 - July 2004
August 2004 - January 2005
February 2005 & Thereafter
10,000
17,000
38,500
50,000
80,000
115,000
18
FINAL, 8/21/02
PEI

Soap and Detergent Manufacturing (Part 417)
• Subpart F - Soap Flakes and Powders
• Subpart H - Liquid Soaps; and
• Subpart P - Liquid Detergents.
Steam Electric Power Generating (Part 423)
• Wastewater generated by contract firms providing start-up and/or
turnaround boiler tube cleaning. This will not include cooling tower
sludges or other metal bearing wastes.
Landfills Point Sources (Part 445)
• Leachate from landfills; and
• Groundwater from RCRA/CERCLA groundwater extraction systems.
Plastics Molding and Forming (Part 463)
• Subpart A - Contact cooling and heating water;
• Subpart B - Cleaning water; and
• Subpart C - Finishing water.
Clariant has been accepting 3rd party non-OCPSF wastewaters from most of the
categories listed above since 2001 for treatment in the on -site WWTP as a trial for
continuing operations. The Clariant WWTP performance has been very good during
the 11-month trial period.
2.2.4 Non -Categorical Wastewaters
Under the modified permit, Clariant will continue to treat the following existing non -
categorical wastewaters in the on -site WWTP:
• Sanitary wastewater;
• Filter plant backwash;
19 FINAL, 8/21/02

• Non -process area stormwater; and
• Utilities wastewater including cooling tower blowdown, boiler blowdown
and condensate.
The following new non -categorical wastewaters will also be treated through the on -site
WWTP:
SCR -Tech
SCR -Tech regenerates NO„ reduction catalyst used for air pollution control in the fossil
fuel burning electrical power generation industry. Clariant is currently negotiating a
lease agreement with SCR -Tech for location of their operation at the Clariant-Mt. Holly
East facility. Plans are to have a signed lease in August 2002. The lease will allow
SCR -Tech to occupy Building 48 within the Clariant facility (one of our mothballed
production plants) for their catalyst regeneration process and begin operations in late
2002. SCR -Tech will also occupy warehouse, laboratory, and office space at the site.
SCR -Tech will begin demolition and re -construction of the plant in late August. Their
current plans are to begin catalyst regeneration operations in November 2002.
SCR operates under SIC 3564. SCR's regeneration process is not covered by any of
the categorical standards in the US EPA Subchapter N Effluent Guidelines and
Standards.
The catalyst regeneration process removes metallic and fly ash contaminants from the
ceramic substrate and re -deposits new catalyst on the substrate. Ultrasonic baths
containing hydrochloric acid solutions are used to dissolve contaminants, and clean
deposits from the substrate. Lime slurry is then added to precipitate the soluble
metallic contaminants.
The company's regeneration process includes pretreatment of the spent regeneration
solutions by addition of lime slurry to the regeneration solution for precipitation of
20 FINAL, 8/21/02

farl
metals. The lime solids and metals are then removed from the spent solutions through
filtration along with significant amounts of fly ash contained in the solutions. The
filtered solutions will then be discharged as process wastewater to the Clariant WWTP
for further treatment. SCR -Tech process wastewater characteristics are presented in
Table 2-5. Projected SCR -Tech wastewater flows are presented in Table 2-6.
The sludge from the SCR regeneration operations will be collected in roll -off containers
and hauled to the BFI landfill in Concord, North Carolina for disposal. The Hazardous
Waste Section has determined the sludge to be non -hazardous.
tpIMA
21 FINAL, 8/21/02
tom

f=1
r=1
F=1
ran
Fmn
nma
Fon
114
TABLE 2-5
SCR -TECH PROCESS WASTEWATER STREAM
BOD5
TSS
Aluminum
Ammonia
Antimony
Arsenic
Beryllium
Barium
Cadmium
Chromium
Chloride
Copper
Lead
Mercury
Molybdenum
Nickel
Selenium
Silver
Thallium
Zinc
�ncentrationlin°r
Ocess frea ii
None
6,300 — 10,000
<0.01
25
Not detectable
<0.2
Not detectable
<0.01
<0.05
<0.05
15-30
<0.05
<0.01
<0.003
<0.2
<0.05
<0.1
<0.005
<0.01
0.05
Note: Concentrations based on operations at other SCR -Tech facilities
22 FINAL, 8/21/02

TABLE 2-6
PROJECTED DAILY WASTEWATER FLOW FROM
SCR -TECH OPERATIONS
October 2002 - February 2003
March 2003 - September 2003
October 2003 - February 2004
March 2004 - September 2004
October 2004 - February 2005
March 2005 & Thereafter
8,000
16,500
26,500
36,000
47,000
55,000
23 FINAL, 8/21/02

SECTION 3.0
EFFLUENT GUIDELINES AND STANDARDS
own 3.1 GENERAL
There have been changes in facility production and wastewater flows at the facility over the
past several years. Additional changes are planned for the latter half of 2002. These changes
in wastewater sources, flows, and character affect the current NPDES effluent limits. As
discussed in Section 2.2.1, there are three (3) industrial categories of wastewater to be
considered, OCPSF, Centralized Waste Treatment (CWT) and Non -Categorical. The US EPA
has developed the Effluent Guidelines and Standards for each industrial category. The
proposed limits for conventional and non -conventional parameters based on these guidelines
are presented in the following sections.
Since Clariant is developing the facility as an industrial park for compatible industrial
operations, future wastewater sources will occur. In order to account for these future
wastewater sources in the proposed permit effluent limits, a tiered approach to developing the
limits was used. The proposed limits for both conventional and non -conventional parameters
are presented in two tiers, Tier 1 and Tier 2. The Tier 1 limits are based on wastewater flow
from existing and planned wastewater sources. Planned wastewater sources include
wastewater from Seaboard Container and SCR -Tech. The Tier 2 limits are based on
wastewater flow not only from existing and planned wastewater sources, but also from future
wastewater sources. The existing, planned and future wastewater sources and flow are shown
in Table 2-2. Tier 2 limits become effective when any new wastewater source, in addition to
the planned wastewater sources, is added.
3.2 CONVENTIONAL PARAMETERS
'm' The US EPA Effluent Standards and Guidelines for conventional parameters for the three
industrial categories are summarized in Table 3-1 along with the previous allocations allowed
permitted by NCDENR for the specific non -categorical discharges. Ammonia -nitrogen (NH3-
N) is included in the current Clariant NPDES permit, but is not included in the EPA
24 FINAL, 8/21/02

MEI
PEI
Antl
FIR
TABLE 3-1
US EPA EFFLUENT GUIDELINES AND STANDARDS
R _
Industrial{.,'Category an Parameters,
hly Avg.
Effluent�Limits
Max Dy
Effluena
t `Limit
OCPSF
BOD5
45
120
TSS
57
183
Non -categorical: Sanitary, Planned Air Filter
Regeneration, Utilities, Future Tenant
Expansion
BOD5
30
45
TSS
30
45
Non -categorical: Non -Process Stormwater a)
BOD5
1
1
TSS
30
45
Non -categorical: Filter Plant Backwash")
BOD5
0
0
TSS
30
45
Non -categorical: Utilities"
BOD5
0
0
TSS
0
0
Centralized Waste Treatment
BOD5
53
163
TSS
30.6
74.1
O&G
38
127
Notes:
(1) Based on previous allocations allowed by NCDENR for the Clariant facility.
25 FINAL, 8/21/02

rati
guidelines. Oil and grease (O&G) is not included in the current permit, but will need to be
added due to wastewater from centralized waste treatment operations.
mci Proposed limits for conventional parameters were determined based on the past 12 months
(June 2001 - May 2002) of flow data and the EPA limitations. A summary of the existing
limits for the current permit and proposed limits for the new permit are presented in Table 3-2.
Break -downs of the BOD5, TSS and O&G allocations by industrial category are presented in
'°'' Tables 3-3(a) and 3-3(b). For the OCPSF wastewater, the one-year average daily flow (long
term average) which was presented in Table 2-2, was used to calculate the effluent loads. For
the CWT and Non -Categorical wastewater, the maximum monthly flow was used to calculate
the proposed limits. The maximum monthly flow was determined based on the historical ratio
PPM
of average daily flow to maximum monthly flow, as noted in Tables 3-3(a) and 3-3(b).
The EPA effluent guidelines do not include limitations for NH3-N. The 1995 Catawba River
Basinwide Water Quality Management Plan (Catawba Plan), prepared by NCDENR, indicates
that no water quality problems have been identified in the Catawba River at Monitoring Station
No. 02142938 (near S. Belmont), downstream of the Clariant discharge. Since ammonia has
not been identified in the Catawba Plan as a water quality problem in the discharge stream,
,r, proposed limits were calculated based on historical effluent data. The Clariant WWTP
includes biological nitrification in the activated sludge process for oxidation of ammonia
,moo nitrogen. This process is considered to be BAT by US EPA guidelines.
A statistical plot of the daily effluent NH3 N load (June 2001-May 2002) was prepared and the
95 percentile effluent load was determined to be 618 lb/d NH3-N. This plot is presented in
Figure 4. The statistical analysis of the effluent data is included in Appendix G. Based on the
methodology used in the USEPA OCPSF development documents, the 95 percentile level is
utilized as the basis for the monthly average limitation. The max day limit of 927 lb/d was
determined by using the ratio of the current max day limit (977 lb/d) to the current monthly
average limit (651 lb/d) for ammonia (ratio = 1.50).
26 FINAL, 8/21/02

rMrk
PEI
001
TABLE 3-2
CURRENT AND PROPOSED LIMITS - CONVENTIONAL PARAMETERS
..Parameter -
_:
.
Current
,.
Limns
Proposed Limits.
Tfee-1
Tier`2 (s)
Monthly
rX
Avg.....
x Daily . t
Ma i = t
thiy
Mon r4'i`
D � �
_ 'b ail y�F
M
�, � hly .-
�z
' tin `
Av
,D Y.
ail
��Max
: =Av �►�
Flow
BOD5
TSS
NH3-N
O&G
Total Nitrogen)
Total Phosphorus°)
3.9 MGD
852 lb/d
976 lb/d
651 lb/d
none
none
none
none
2236 lb/d
2928 lb/d
977 lb/d
none
none
none
3.9 MGD
329 lb/d
410 lb/d
618 lb/d
26.6 lb/d
444.1 lb/d
32.5 lb/d
none
810 lb/d
1115 lb/d
927 lb/d
89 lb/d
none
none
3.9 MGD
485 lb/d
543 lb/d
618 lb/d
84.3 lb/d
444.1 lb/d
32.5 lb/d
none
1215 lb/d
1437 lb/d
927 lb/d
282 lb/d
none
none
Notes:
(1) Tier 1 proposed limits based on existing and planned flow only as shown in Table 2-2.
Does not include future flows.
(2) Tier 2 proposed limits based on existing, planned and future flow as shown in Table 2-2.
0.4 (3) Total Nitrogen and Total Phosphorus limits based on a 12-year rolling average beginning
after 12 months of data collection under the new permit. The limits are to be interim
limits until the establishment of new BAT limits as discussed in Section 3.4.
FIR
27 FINAL, 8/21/02

Pin
OKI
PER
Alq
TABLE 3-3(a)
TIER 1 WASTE LOAD ALLOCATIONS - EXISTING AND PLANNED FLOWS ONLY
CONVENTIONAL PARAMETERS BY INDUSTRIAL CATEGORY
BASED ON US EPA EFFLUENT GUIDELINES AND LIMITATIONS
1. OCPSF, Average Daily Flow = 0.590 MGD
Month Avg. Max Day Month Avg. Max Day
(mg/LL (mg/L) (lb/d) (lb/d)
BOD5 45 120 221.4 590.5
TSS 57 183 280.5 900.5
2a. Non -categorical, Max Monthly Flow = 0.279 MGD (1,2)
Includes: Sanitary (0.043 MGD), Planned Air Filter Regeneration (0.084 MGD), and Utilities
(0.152 MGD)
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d) (lb/d)
BOD5 30 45 69.8 104.7
TSS 30 45 69.8 104.7
2b. Non -categorical, Max Monthly Flow = 0.049 MGD (2)
Includes: Non -Process Stormwater
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d), (lb/d),
BOD5 1 1.5 0.4 0.6
TSS 30 45 12.3 18.4
2c. Non -categorical, Max Monthly Flow = 0.106 MGD (2)
Includes: Filter Plant Backwash
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d) (lb/d)
BOD5 0 0 0 0
TSS 30 45 26.5 39.8
3. Centralized Waste Treatment, Max Monthly Flow = 0.084 MGD (2)
Includes: Planned On -Site Oily WW
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d) (lb/d)
BOD5 53 163 37.1 114.2
TSS 30.6 74.1 21.4 51.9
O&G 38 127 26.6 89.0
TOTAL
Month Avg. Max Day
(lb/d) (Ib/d)
BOD5 329 810
TSS 410 1115
O&G 26.6 89.0
Notes:
(1) Max monthly flow was calculated based on ratio of Max Monthly Flow to Average Daily Flow for
June 2001 - May 2002. Ratio of max monthly flow to Average Daily Flow is 1.52.
(2) No BOD or TSS allocation for Utilities (0.050 MGD steam generation and 0.050 MGD non -contact
cooling.)
28
FINAL, 8/21/02

Fmi
Min
FINN
fain
104
PIM
Awl
TABLE 3-3(b)
TIER 2 WASTE LOAD ALLOCATIONS - INCLUDES FUTURE FLOWS
CONVENTIONAL PARAMETERS BY INDUSTRIAL CATEGORY
BASED ON US EPA EFFLUENT GUIDELINES AND LIMITATIONS
1. OCPSF, Average Daily Flow = 0.690 MGD
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (1b/d) (lb/d)
BOD5 45 120 259.0 690.6
TSS 57 183 328.0 1053.1
2a. Non -categorical, Max Monthly Flow = 0.431 MGD (1,2)
Includes: Sanitary (0.043 MGD), Planned Air Filter Regeneration (0.084 MGD), Utilities (0.152
MGD) and Future Tenant Expansion (0.152 MGD)
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d) (lb/d)
BOD5 30 45 107.8 161.8
TSS 30 45 107.8 161.8
2b. Non -categorical, Max Monthly Flow = 0.049 MGD a)
Includes: Non -Process Stormwater
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d) (lb/d)
BOD5 1 1.5 0.4 0.6
TSS 30 45 12.3 18.4
2c. Non -categorical, Max Monthly Flow = 0.106 MGD ca)
Includes: Filter Plant Backwash
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (Ib/d), (lb/d)
BOD5 0 0 0 0
TSS 30 45 26.5 39.8
3. Centralized Waste Treatment, Max Monthly Flow = 0.266 MGD (2)
Includes: Planned On -Site Oily WW and Future 3' Party Oily and Non-OCPSF WW
Month Avg. Max Day Month Avg. Max Day
(mg/L) (mg/L) (lb/d) (lb/d)
BOD5 53 163 117.6 361.6
TSS 30.6 74.1 67.9 164.4
O&G 38 127 84.3 281.7
TOTAL
Month Avg. Max Day
(lb/d) (lb/d)
BOD5 485 1215
TSS 543 1437
O&G 84.3 282
Notes:
(1) Max monthly flow was calculated based on ratio of Max Monthly Flow to Average Daily Flow for
June 2001 - May 2002. Ratio of max monthly flow to Average Daily Flow is 1.52.
(2) No BOD or TSS allocation for Utilities (0.050 MGD steam generation and 0.050 MGD
non -contact cooling.)
29
FINAL, 8/21/02

Kotg PROBABILITY X 90 DIVISIONS
46 8000
=IZMIZilb d'
99.99
qo0 -
Soo
7o0
GOO
500
1100
99.9 99.8
Figure 4. Probability Plot of Effluent NH3—N (June 2001—May 2002)
99 98 95 90 80 70 60• 50 40 30 20 10 5 2 1 0.5 0.2 0.1 0.05 0.01
{
1
1
1
V.
i
L
1
r
1 . .
Ir
•
•
1,
r
1
1
�00
Zoo
boo
Lrt
-111
-4
•
1J
_
t
�a.
1
--r
r
rt
i
1
•
r � r
•
f
--
if/
_ Tl
0.01 0.05 0.1 0.2 0.5 1 2 5 10 20 30 40 50 60 70 80 90 51.5 98 99 99.8 99.9 99.99
% Probability CIS f s (Q I g

PRI
3.3 NON -CONVENTIONAL PARAMETERS
1.1 The EPA guidelines also include non -conventional parameters for wastewater discharged from
OCPSF and CWT categorical operations. The current NPDES permit already includes limits
,am for OCPSF non -conventional parameters. With the historical and planned changes in
wastewater flow and character, the OCPSF effluent permit limits need to be modified and
►-F, additional parameters need to be added to the permit for CWT wastewater. A summary of the
current and proposed limits for non -conventional parameters are presented in Tables 3-4(a), 3-
4(b), 3-5(a), 3-5(b), 3-6(a) and 3-6(b). Tables 3-6(a) and 3-6(b) include those parameters
which appear in both the OCPSF and CWT effluent guidelines. The OCPSF parameters were
calculated using the 12-month average daily flow and the CWT parameters were calculated
using the max monthly flow. Appendix H contains a more detailed data analysis of current and
proposed limits for the non -conventional parameters. As shown in the tables in Appendix H,
many of the effluent limits are very low and either at or below the analytical detection limit.
For the OCPSF parameters, it should be noted that 1,1,1-trichloroethane appears twice in
Clariant's current NPDES permit. However, 1,1,2-trichloroethane is not included in the
current NPDES permit, but is included in the OCPSF guidelines. Therefore, 1,1,2-
trichloroethane is included in Tables 3-4(a) and 3-4(b) in the proposed limits.
3.4 TOTAL NITROGEN, TOTAL PHOSPHORUS, PHENOLICS
In October 1999, a study was performed by AWARE Environmental® Inc. at the request of
Clariant and submitted to the NCDENR to evaluate the best available technology economically
achievable (BAT) for control of total nitrogen (TN) and total phosphorus (TP) in the effluent
, discharge. The 1999 BAT study proposed monthly average effluent TN and TP limits of 37.5
mg/L and 2.6 mg/L, respectively. Since the study was performed in 1999, there have been
�► significant changes in Clariant-Mt. Holly East production which have affected the wastewater
flows and characteristics. These changes in production and wastewater characteristics are
0.1 expected to continue through the remainder of 2002.
4.4 Clariant has performed monitoring once per month of effluent TN and TP as required as part
of the current Clariant NPDES permit. Graphical summaries of the effluent TN and TP over
31 FINAL, 8/21/02

TABLE 3-4(a)
OCPSF PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
TIER 1 WASTE LOAD ALLOCATIONS
Proposed Average Daily Flow = 0.590 MGD
r Cf
Effluent�Char"a ens
5 (':t 3 i�
rj,t£,»F
... �,.. . .; f5 +
�
Proposed :,iniits @ 0 590:
A.Y ,a$g "i .. i fi, srJ •p`�
.v.'Y'r E14 u- 93""7s6 s "1%iy„ i Y 4
�� • 1V�GD F w Y
` % Reduction
.:. 6'w^
i. ,p .
; ;r�
in Current
• -. f
ut
�i NN
�Si:t ��Ht 7y YM G�;F3.[ ?
l onth �, g. f
_.:`�_ �
R i y f { "eft } MMC
11�ax Day
�'m'
` .(lb/ ;r i
�4
`!f .R/'g � Ti 3t.._ y;
z Month:.Aog.•Max
• t
j Limitr "
L,.
Day
TTr,
Acenaphthene
*
0.11
0.50
72 %
0%
Acenaphthylene
*
0.11
0.50
72 %
0%
Acrylonitrile
0.47
1.19
72%
72%
Anthracene
*
0.11
0.50
72%
0%
Benzene
0.18
0.67
76%
75%
Benzo(a)anthracene
*
0.11
0.50
65 %
0%
3,4-Benzofluoranthene
*
0.11
0.50
72%
0%
Benzo(k)fluoranthene
*
0.11
0.50
72 %
0%
Benzo(a)pyrene
*
0.11
0.50
72 %
0%
Carbon Tetrachloride
0.09
0.19
72 %
72 %
Chlorobenzene (2)
0.07
0.14
76 %
76 %
Chloroethane
0.51
1.32
72 %
72 %
Chloroform
0.10
0.23
72 %
72 %
2-Chlorophenol
0.15
0.48
75 %
75 %
Chrysene
*
0.11
0.50
72 %
0%
Di-n-butyl phthalate
0.13
0.28
72%
72%
1,2-Dichlorobenzene
0.38
0.80
76%
76%
1,3-Dichlorobenzene
0.15
0.22
75 %
76 %
1,4-Dichlorobenzene
0.07
0.14
76 %
76 %
1,1-Dichloroethane
0.11
0.29
72 %
72 %
1,2-Dichloroethane
0.33
1.04
72%
72%
1,1-Dichloroethylene
0.08
0.12
72 %
72 %
1,2-trans-Dichloroethylene
0.10
0.27
72 %
72 %
2,4-Dichlorophenol
0.19
0.55
75 %
75 %
1,2-Dichloropropane
0.75
1.13
72 %
72 %
1,3-Dichloropropylene
0.14
0.22
72%
72%
Diethyl phthalate
0.40
1.00
72 %
72 %
2,4-Dimethylphenol
0.09
0.18
75 %
75 %
Dimethyl phthalate
0.09
0.23
72%
72%
4,6-Dinitro-o-cresol
0.38
1.36
75%
75%
2,4-Dinitrophenol
0.35
0.61
84%
84%
2,4-Dinitrotoluene
0.56
1.40
72%
72%
32
FINAL, 8/21/02

Pik
PPR
PIR
flat
Fol
TABLE 3-4(a) (continued)
A 4 ,; r s
EffluentCh- aa..Fra.xcercz :.✓. i c y#
- � .
a ars
Proposed Li
� S r
nits Cg?s 0 590 :
' % Reduction. in Current
Ya z•+ t • • ^' . S
T3P •g, a {
isM*...ZK
si
g,.7• ,{,C.b�,� b j ,v:
kDPAj"
"
on.tYd
*h_.M
�t
.bd
a?bS` zikaxt E{a'tS4a
fa
.Z..x.D3Vd
id', ,,'
-a
.YAv`3
Month
• nv�
aL
r+w
La
itan�,•ii.i:
l �rD
r39 :T
2,6-Dinitrotoluene
1.25
3.15
71 %
72%
Ethylbenzene
0.16
0.53
76%
76%
Fluorene
*
0.11
0.50
72%
0%
Hexachlorobenzene
0.07
0.14
72%
72%
Hexachlorobutadiene
0.10
0.24
72%
72%
Hexachloroethane
0.10
0.27
74%
72%
Methyl Chloride
0.42
0.93
72%
72%
Methylene Chloride
0.20
0.44
72%
72%
Naphthalene
*
0.11
0.50
76%
0%
Nitrobenzene
0.13
0.33
72 %
72 %
2-Nitrophenol
0.20
0.34
84%
84%
4-Nitrophenol
0.35
0.61
84%
84%
Phenanthrene
*
0.11
0.50
72 %
0%
Pyrene
*
0.12
0.50
72%
0%
Tetrachloroethylene
0.11
0.28
72 %
72 %
Toluene
0.13
0.39
76%
76%
Total Cyanide
2.07
2.52
72%
72%
1,2,4-Trichlorobenzene
0.33
0.69
72%
72%
1,1,1-Trichloroethane
0.10
0.27
72%
72 %
1,1,2-Trichloroethane
0.10
0.27
72 %
72 %
Trichloroethylene
0.10
0.27
72%
72%
Vinyl Chloride
0.51
1.32
72 %
72 %
* These parameters are water quality limited.(WQL)
NA - no limit established in current NPDES permit
Pal
folil
Fart
33
FINAL, 8/21/02

TABLE 3-4(b)
OCPSF PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
TIER 2 WASTE LOAD ALLOCATIONS
Proposed Average Daily Flow = 0.690 MGD
.:
Effluent Characteristic
�_ ,-
' F
a�MGD
- .
Proposed Limifsi 0.690K• a
.% Reduction in Current
' 'F` t Limit.
=.
` ' `
.,,:.
o .
Month A g
(lb/d)..
• -
IViaDay
bl d): ,,.
; y7Vlonth Avg.;
Limit
Max Day
Limit . ,
Acenaphthene
*
0.13
0.50
68%
0%
Acenaphthylene
*
0.13
0.50
68%
0%
Acrylonitrile
0.55
1.39
67 %
68 %
Anthracene
*
0.13
0.50
68%
0%
Benzene
0.21
0.78
72%
71%
Benzo(a)anthracene
*
0.13
0.50
59%
0%
3,4-Benzofluoranthene
*
0.13
0.50
67%
0%
Benzo(k)fluoranthene
*
0.13
0.50
68%
0%
Benzo(a)pyrene
*
0.13
0.50
67%
0%
Carbon Tetrachloride
0.10
0.22
68 %
67 %
Chlorobenzene (2)
0.09
0.16
72%
72%
Chloroethane
0.60
1.54
67 %
67 %
Chloroform
0.12
0.26
67%
67%
2-Chlorophenol
0.18
0.56
71%
71 %
Chrysene
*
0.13
0.50
68%
0%
Di-n-butyl phthalate
0.16
0.33
68 %
67 %
1,2-Dichlorobenzene
0.44
0.94
72%
72%
1,3-Dichlorobenzene
0.18
0.25
71%
72%
1,4-Dichlorobenzene
0.09
0.16
72%
72%
1,1-Dichloroethane
0.13
0.34
68%
67 %
1,2-Dichloroethane
0.39
1.21
67%
67%
1,1-Dichloroethylene
0.09
0.14
67 %
67 %
1,2-trans-Dichloroethylene
0.12
0.31
67%
67%
2,4-Dichlorophenol
0.22
0.64
71 %
71 %
1,2-Dichloropropane
0.88
1.32
67%
67%
1,3-Dichloropropylene
0.17
0.25
67%
67%
Diethyl phthalate
0.47
1.17
67 %
67 %
2,4-Dimethylphenol
0.10
0.21
71%
71%
Dimethyl phthalate
0.11
0.27
67 %
67 %
4,6-Dinitro-o-cresol
0.45
1.59
71%
71 %
2,4-Dinitrophenol
0.41
0.71
81%
81%
2,4-Dinitrotoluene
0.65
1.64
67%
67%
34
FINAL, 8/21/02

"`' TABLE 3-4(b) (continued)
MIA
PRIN
Met
ANN
fag
PEA
{ a s xxF 3 ..
Effluent~Charac er• '
} i >} tpp 'R a m
x 46r tS�� fEt 7x.^' � � �"
t 1:} I {.+..3£ 4 i
t �
a ::,
}
i
l
O�
'� ;
r
•Proposed Limits 690
:,.,j L; : t MGDt .} is, rt }
'_ rat Y j7 Y a
% Reduction in Current
. •.
Limit
gt ?
Month
S 1 �'
,,�:o
.Avg.- (Yb7d)
s. �Y r 1
lMiair�a•ri i
�
nbld J
11 a
Month tA� •
� g�
fiLin it
4
�MaX Da
:L t
2,6-Dinitrotoluene
1.47
3.69
67%
67%
Ethylbenzene
0.18
0.62
72%
72%
Fluorene
*
0.13
0.50
68%
0%
Hexachlorobenzene
0.09
0.16
67 %
67 %
Hexachlorobutadiene
0.12
0.28
67%
67%
Hexachloroethane
0.12
0.31
69%
67%
Methyl Chloride
0.49
1.09
67%
67%
Methylene Chloride
0.23
0.51
67%
67%
Naphthalene
*
0.13
0.50
72 %
0%
Nitrobenzene
0.16
0.39
68%
67%
2-Nitrophenol
0.24
0.40
81 %
81 %
4-Nitrophenol
0.41
0.71
81 %
81 %
Phenanthrene
*
0.13
0.50
68 %
0%
Pyrene
*
0.14
0.50
67%
0%
Tetrachloroethylene
0.13
0.32
68 %
67 %
Toluene
0.15
0.46
72%
72%
Total Cyanide
2.42
2.95
67 %
67 %
1,2,4-Trichlorobenzene
0.39
0.81
67%
67%
1,1,1-Trichloroethane
0.12
0.31
67 %
67 %
1,1,2-Trichloroethane
0.12
0.31
NA
NA
Trichloroethylene
0.12
0.31
67%
67%
Vinyl Chloride
0.60
1.54
67 %
67 %
* These parameters are water quality limited.(WQL)
NA - no limit established in current NPDES permit
35 FINAL, 8/21/02

faxl
razt
IMP
6111
tan
IMP
Plat
TABLE 3-5(a)
CWT PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
TIER 1 WASTE LOAD ALLOCATIONS
Proposed Max Monthly Flow = 0.084 MGD
'''
Effluent ` Characteristic
_ : _ .. P
Proposed� Li ts,@ 0.084:MGD'`
, Month Avg. -
(111d) ' .
Max ; Da .
(ib/d)
Antimony
0.099
0.166
Arsenic
0.073
0.113
Barium
0.197
0.299
Cadmium
0.007
0.012
Cobalt
0.087
0.135
Mercury (1)
0.0005
0.0016
Molybdenum
0.676
0.708
Selenium
0.286
1.149
Silver
0.025
0.084
Tin
0.084
0.287
Titanium
0.021
0.036
Vanadium
0.046
0.153
Acetone
5.583
21.157
Acetophenone
0.039
0.080
Aniline
0.011
0.023
2-Butanone
1.296
3.370
Butylbenzyl phthalate
0.062
0.132
Carbazole
0.193
0.419
o-Cresol .
0.393
1.345
p-Cresol
0.144
0.489
n-Decane
0.306
0.664
2,3-Dischloroaniline
0.025
0.051
n-Octadecane
0.212
0.413
Pyridine
0.128
0.259
2,4,6-Trichlorophenol
0.074
0.109
Notes:
(1) Mercury monitoring required on current NPDES limit, but no limit
established.
36 FINAL, 8/21/02

Cal
GINA
ales
TABLE 3-5(b)
CWT PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
TIER 2 WASTE LOAD ALLOCATIONS
Proposed Max Monthly Flow = 0.266 MGD
z
r x'
Effluent- Characteristic
:,.. _
Proposed;Limits :a,0.266 ;MGD
Mon A
� Y�-��,
` '. Max Day s
Antimony
0.313
0.526
Arsenic
0.231
0.359
Barium
0.623
0.947
Cadmium
0.023
0.038
Cobalt
0.275
0.426
Mercury (1)
0.0016
0.0052
Molybdenum
2.141
2.241
Selenium
0.905
3.638
Silver
0.078
0.266
Tin
0.266
0.907
Titanium
0.066
0.113
Vanadium
0.147
0.484
Acetone
17.681
66.997
Acetophenone
0.125
0.253
Aniline
0.036
0.074
2-Butanone
4.104
10.671
Butylbenzyl phthalate
0.197
0.417
Carbazole
0.612
1.327
o-Cresol
1.245
4.259
p-Cresol
0.455
1.548
n-Decane
0.969
2.103
2,3-Dischloroaniline
0.080
0.162
n-Octadecane
0.670
1.307
Pyridine
0.404
0.821
2,4,6-Trichlorophenol
0.235
0.344
Notes:
(1) Mercury monitoring required on current NPDES limit, but no limit
established.
37 FINAL, 8/21/02

1214
lark
gift
Plah
OEN
Ptgl
TABLE 3-6(a)
OCPSF & CWT PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
TIER 1 WASTE LOAD ALLOCATIONS
Note: List of parameters which appear in both OCPSF and CWT Effluent Guidelines. Final
proposed limit is the sum of OCPSF and CWT allocation
a f'j
» s
OCPSF Allocation a
., J P `f SFa'^'b �4"\t c",.��
x« 3.,.:::�
�g C �4liocatIo �x
a+r«O ;.,°�°f��
�k5?,�T
D..f
.i+n ... !
;k K' ,
.f. ;f,.:
Efluenl�..�
a w� � .�� .��� �
:.:.'.�nt�"F+i Xa :}a,Y�`fi
d
_ .-0 0:5901VI ; t
:�� ..� �.. �,,.� �.�
., ' E">. S
..� >s,_
.......�O.Q8�4�MGI�F� �x.
Proposed Limut
..r��.�w.:� �
v�aK. •�`'`-.b�`s..'>�•L�`
,j ,yc
Gh aced
4, � ..� ��
� E.jmtd�����{Y.. T T.S.F'F�1w
i^' t&
dk;#
d... ,.
r�N «r; Y'.$i_�v.-
�. "'�
on ,:v .
Fes, �... g
-•+�T,ySG'-0.D•.z. C8.
Ln
, Y,'
<
.._«
A tl .+ 3� a=<,r5,,,
MaxDaZ
.�. 3
,t . "�` �'i:
.. ` k : Fri
.>K.n, i „,.
;1Y'f '
.«� (� �:
.'?'^:w.•Ti:
e ....,<S«.
On
onth Av .
� .�.
A `� w �
»'�°
«i %�: aof+ra:^
&'?:
�t�bf ��
,� .fin.
Max
M Y$
.z Rfi.,�
... 4. >,
3F_ :'
4v ,ih.. i -F.
ff C��f� �rt ��
,. :... n ' `$ 'znb`ix'$' '
on =h�H°
>:KK t -
n ys: ,�. «�Rs�'Gsx t.'e:�
i^l`,1� :;g `�. q
...2 .t.
��a) ����/r
64,' 3 Z:.....< V
MaxDa
i. - .E. » �s
,�' •y^� t .
�i a,e ,Kq �, t� t
Bis(2-ethylhexyl)
phthalate
0.51
1.37
0.071
0.151
0.58
1.52
Chromium
5.46
13.63
0.226
0.523
5.69
14.15
Copper
7.13
16.63
0.170
0.350
7.30
16.98
Fluoranthene
0.12
0.33
0.019
0.038
0.14
0.37
Lead
1.57
3.40
0.112
0.245
1.69
3.64
Nickel
8.32
19.58
1.016
2.767
9.33
22.35
Phenol
0.07
0.13
0.757
2.557
0.83
2.68
Zinc
5.17
12.84
0.294
0.348
5.46
13.19
38 FINAL, 8/21/02
fftl

Pak
rao
MKS
Aft
01111
Oft
fsDk
WEN
PIO
TABLE 3-6(b)
OCPSF & CWT PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
TIER 2 WASTE LOAD ALLOCATIONS
Note: List of parameters which appear in both OCPSF and CWT Effluent Guidelines. Final
proposed limit is the sum of OCPSF and CWT allocation
Effluent ` ...
Characteristic
y .
. _ T
OCPSF tAllo"cation'•
'r"_ r, a
�40IV,iIzD:} .�.
' LCW, ] ' Allocation
,i--:-
^ sr-�0 26
�� 6.PM
Proposed Limit
Month Avg.
(lb/d) .
M;a .Day #Mon
_ (lb%d)
r ,
!v
`� Max Dayrroj
... (lb/d)
Month: -Avg
i..(lbld) _
Max Day
(lb/d)-_
Bis(2-ethylhexyl)
phthalate
0.59
1.61
0.224
0.477
0.82
2.08
Chromium
6.39
15.94
0.717
1.655
7.10
17.60
Copper
8.34
19.45
0.537
1.109
8.88
20.56
Fluoranthene
0.14
0.39
0.059
0.119
0.20
0.51
Lead
1.84
3.97
0.355
0.776
2.20
4.75
Nickel
9.73
22.90
3.217
8.763
12.9
31.7
Phenol
0.09
0.15
2.396
8.097
2.48
8.25
Zinc
6.04
15.02
0.932
1.103
6.97
16.12
39 FINAL, 8/21/02

flog
C�1
rogl
the past 12-months (June 2001 - May 2002) are presented in Figures 1 and 2 in Section 2.0.
These figures show that the effluent nutrient levels have at times exceeded the BAT limits
determined in 1999.
Because of the changes at the facility and the resulting change in the wastewater character since
Mot 1999, Clariant is proposing that the new permit include interim limits for TN and TP, and
conditions be included in the permit to require that a new BAT study be conducted based on 12
months of data, representative of current wastewater characteristics, to evaluate currently
attainable effluent TN and TP levels on a weekly basis to determine new BAT limits. The
'kt BAT study will primarily involve increased data collection and continued WWTP optimization
for TN and TP reduction. Following completion of the study, the data collected will be used
for determining new BAT limits for TN and TP. The interim and final TN and TP limits will
be annual average limits based on a 12-month rolling average.
cal
014
PEA
/04
raKt
Monitoring of total phenols and other phenolic compounds (4-chloro-3-methylphenol, 2-
methylphenol, 4,6-dimethylphenol, 2-methylphenol, pentachlorophenol, 2,4,5-trichlorophenol)
are required under the current NPDES permit. However, monitoring and/or limitations for
total phenols and the other phenolic compounds are not required as part of the EPA effluent
guidelines for the types of industrial wastewaters treated at the facility. Dye manufacturing is
scheduled to shut -down by January 1, 2003. Over the past 21/2 years dye manufacturing has
been decreasing and consequently phenol levels in the wastewater have also decreased.:,Nye are
requesting that the limits and monitoring requirements for total phenol and the phenolic
compounds mentioned above be discontinued with the new permit.
13020r001
40 FINAL, 8/21/02
rmv

APPENDIX A
JUNE 2001-MAY 2002 EFFLUENT DATA
CLARIANT WWTP

1 1 3 ,01 9 9 3
Effluent Monitoring Data
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
SUMMARY
12-month
Average
Max 30-day
Average
Max Day
Total No.
Analyses
Effluent Flow
MGD
0.61
0.93
2.01
365
Temperature
deg C
20
29
32
365
pH
SU
7.8
7.9
8.5
365
Min pH
SU
7.5
7.2
Fecal Coliform
#/100 ml
418
NA (1)
>1200
13
12-month
Average
(mg/L)
12-month
Average
(Ib/d)
Max 30-Day
Avg. (mg/L)
Max 30-Day
Avg. (Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
Total No.
Analyses
250
BOD
Ibs/d
49
248
277
763
438
1642
Ammonia
Ibs/d
60
305
155
427
253
717
250
TSS
Ibs/d
18
93
86
400
88
812
249
TN
mg/L
59
303
NA (1)
NA (1)
202
1633
12
TP
mglL
1.3
6.7
NA (1)
NA (1)
4.9
12.3
12
Total Phenols
Ibs/d
0.25
1.2
0.8
2.80
1.2
5.11
49
Total Sulfate
mg/L
1342
6835
1931
5314
2256
5080
51
COD
mg/L
230
1172
567
2648
775
3102
250
MBAS
mg/L
0.2
1.2
NA (1)
NA (1)
0.5
1.4
12
Manganese
mg/L
1.0
5.0
NA (1)
NA (1'
1.9
5.4
12
Iron
mg/L
0.35
1.8
NA (1)
NA (1)
1.6
12.0
12
Chlorides
mg/L
403
2054
NA (1)
NA (1)
930
2327
12
Mercury
mg/L
0.0004
NA (1)
0.0012
12
Mercury
Ibs/d
0.0019
NA (1)
0.0034
12
Nitrate-N
7
36
NA (1)
NA (1)
30
80
12
Nitrite-N
9
47
NA (1)
NA (1)
45
402
12
NO2+NO3 - N
16
84
NA (1)
NA (1)
50
204
12
TKN
43
219
NA (1)
NA (1)
200
1618
12
(1) Parameters only measured once per month are TN, TP, MBAS, Manganese, Iron,
Chlorides, Mercury and Fecal Coliform. Monthly average not applicable.
(2) Nitrate and TKN not reported on DMR, but needed for permit application
Final, 8/16/02
1 of 5
13020s003
DMR Data

Effluent Monitoring Data
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
June 2001
July 2001
August 2001
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
31
Effluent Flow
MGD
0.93
2.01
30
0.77
1.88
31
0.78
1.21
Temperature
deg C
27
30
30
28
31
31
29
32
31
pH
SU
7.7
8.1
30
7.8
8.5
31
7.7
8.0
31
Min pH
SU
7.3
30
7.3
7.3
Fecal Coliform
#/100 ml
310
310
1
150
150
1
220
220
1
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mglL)
Max Day
(Ibld)
No.
Analyses
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
_
No.
Analyses
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
19
Max Day
(Ibld)
147
No.
Analyses
21
B O D
Ibs/d
1.3
10
4.0
32
21
7
44
20
131
21
8
50
Ammonia
Ibs/d
0.5
4
1.5
12
21
8
49
19
170
21
4
27
14
105
21
TSS
Ibs/d
1.4
11
2.0
19
21
2
16
4
33
21
11
69
14
109
21
TN
mg/L
3.5
26
3.5
26
1
7.1
37.9
7.1
37.9
1
36
267
36
267
1
TP
mg/L
0.26
2.0
0.26
2.0
1
0.51
2.7
0.51
2.7
1
0.21
1.6
0.21
1.6
1
Total Phenols
Ibs/d
0.06
0.47
0.06
0.58
4
0.17
1.09
0.4
3.24
4
0.30
1.92
0.4
3.12
4
Total Sulfate
mg/L
910
7058
1120
7659
4
1046
6717
1480
12096
4
1351
8789
2018
13632
4
COD
mg/L
38
295
88
484
21
72
462
174
1146
21
121
787
194
1100
21
MBAS
mg/L
0.3
2.3
0.3
2.3
1
<0.1
0.5
<0.1
0.5
1
0.2
1.5
0.2
1.5
1
Manganese
mg/L
0.4
3.0
0.4
3.0
1
0.92
4.9
0.92
4.9
1
0.86
6.4
0.86
6.4
1
Iron
mg/L
1.6
12.0
1.6
12.0
1
0.3
1.6
0.3
1.6
1
0.1
0.7
0.1
0.7
1
Chlorides
mg/L
160
1201
160
1201
1
120
641
120
641
1
44.0
327
44.0
327
1
Mercury
mg/L
<0.0002
<0.0002
1
<0.0002
<0.0002
1
<0.0002
<0.0002
1
Mercury
Ibs/d
<0.0015
<0.0015
1
<0.0011
<0.0011
1
<0.0015
<0.0015
1
Nitrate-N
1.8
14
1.8
14
1
5.3
28
5.3
28
1
14
104
14
104
1
Nitrite-N
0.47
4
0.47
4
1
0.1
0.5
0.1
0.5
1
11
82
11
82
1
NO2+NO3 - N
2.3
17
2.3
17
1
5.4
29
5.4
29
1
25
186
25
186
1
TIN
1.2
9
1.2
9
1
1.7
9
1.7
9
1
11.0
82
11.0
82
1
Final, 8/16/02
2 of 5
13020s003
DMR Data

{
JitMJJJJ
$
Effluent Monitoring Data
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
September 2001
October 2001
November 2001
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
30
Effluent Flow
MGD
0.63
1.30
30
0.41
0.87
31
0.64
0.89
Temperature
deg C
24
28
30
20
24
31
16
21
30
pH
SU
7.7
8.0
30
7.9
8.1
31
7.9
8.1
30
Min pH
SU
7.2
7.3
7.6
Fecal Coiiform
#/100 mi
380
380
1
>1200
>1200
2
530
530
1
Month
Avg.
(mglL)
Month
Avg.
(Ibld)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
Month
Avg.
(mglL)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
23
Month
Avg.
(mg/L)
11
Month
Avg.
(Ib/d)
61
Max Day
(mglL)
21
Max Day
(Ib/d)
129
No.
Analyses
BOD
Ibs/d
16
83
13
141
19
35
119
69
486
20
Ammonia
Ibs/d
3
15
8
51
19
67
228
205
651
23
77
412
105
612
20 _
TSS
Ibs/d
14
73
12
130
19
14
47
13
94
23
11
60
15
89
20
TN
mg/L
52.0
213
52.0
213
1
46.7
125
46.7
125
1
83.7
489
83.7
489
1
TP
mg/L
0.22
0.9
0.22
0.9
1
0.99
2.6
0.99
2.6
1
1.40
8.2
1.40
8.2
1
Total Phenols
Ibs/d
0.5
2.62
0.9
3.77
4
0.82
2.80
1.2
5.11
6
0.10
0.54
0.1
0.75
4 _
Total Sulfate
mg/L
1584
8323
1866
9649
4
876
2995
1501
4006
5
944
5039
1055
6159
4
COD
mg/L
148
778
210
963
19
177
605
307
2228
23
176
939
345
1669
20
MBAS
mg/L
0.4
1.6
0.4
1.6
1
0.3
0.80
0.3
0.80
1
0.3
1.8
0.3
1.8
1 _
Manganese
mg/L
1.20
4.9
1.20
4.9
1
1.40
3.7
1.40
3.7
1
1.00
5.8
1.00
5.8
1
Iron
mg/L
0.1
0.4
0.1
0.4
1
0.1
0.27
0.1
0.27
1
0.1
0.6
0.1
0.6
1
Chlorides
mg/L
470
1921
470
1921
1
540
1441
540
1441
1
140
817
140
817
1
Mercury
mg/L
<0.0002
1
<0.0002
<0.0002
1
<0.0002
<0.0002
1
Mercury
lbs/d
<0.0008
1
<0.0005
<0.0005
1
<0.0012
<0.0012
1
Nitrate-N
14
57
14
57
1
30
80
30
80
1
0.62
4
0.62
4
1 _
Nitrite-N
36
147
36
147
1
3.7
10
3.7
10
1
1.1
6
1.1
6
1
NO2+NO3 - N
50
204
50
204
1
33.7
90
33.7
90
1
1.72
10
1.72
10
1
TKN
2.0 _
8
2.0
8
1
13.0
35
13.0
35
1
82.0
479
82.0
479
1
Final, 8/16/02
3 of 5
13020s003
DMR Data

Ji13! ill
Effluent Monitoring Data
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
December 2001
January 2002
February 2002
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
28
Effluent Flow
MGD
0.59
1.10
31
0.61
1.07
31
0.33
0.64
Temperature
deg C
13
17
31
11
19
31
13
18
28
pH
SU
7.7
7.9
31
7.5
7.8
31
7.9
8.2
28
Min pH
SU
7.2
7.2
7.7
Fecal Coliform
#/100 m!
310
310
1
36
36
1
290
290
1
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
Month
Avg.
(mg/L)
Month
Avg.
(IbId)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
20
BOD
Ibs/d
17
85
40
328
19
28
140
55
267
22
277
763
438
1642
Ammonia
Ibs/d
99
488
77
625
19
80
407
70
625
22
155
427
253
717
20
TSS
Ibs/d
12
57
14
111
19
13
67
25
184
21
14
39
24
129
20
TN
mglL
201.9
1633
201.9
1633
1
98.8
882
98.8
882
1
46.4
132
46.4
132
1
TP
mg/L
3.80
31
3.80
31
1
1.20
11
1.20
11
1
1.10
3.1
1.10
3.1
1
Total Phenols
Ibs/d
0.09
0.43
0.1
0.69
4
0.2
0.86
0.3
1.53
1
0.25
0.69
0.4
0.99
5
Total Sulfate
mg/L
1246
6131
1574
12471
4
1317
6700
1964
4750
5
1931
5314
2256
5080
4
COD
mg/L
153
753
226
792
19
140
712
267
1292
22
473
1302
694
1563
20
MBAS
mg/L
0.2
1.6
0.2
1.6
1
0.2
1.8
0.2
1.8
1
0.5
1.4
0.5
1.4
1
Manganese
mg/L
1.30
10.5
1.30
10.5
1
1.60
14
1.60
14
1
1.90
5.4
1.90
5.4
1
Iron
mg/L
0.2
1.6
0.2
1.6
1
0.1
0.9
0.1
0.9
1
0.3
0.9
0.3
0.9
1
Chlorides
mg/L
450
3640
450
3640
1
430
3837
430
3837
1
800
2268
800
2268
1
Mercury
mg/L
<0.0002
<0.0002
1
<0.0002
<0.0002
1
0.0012
0.0012
1
Mercury
Ibs/d
<0.0016
<0.0016
1
<0.0018
<0.0018
1
0.0034
0.0034
1
Nitrate-N
0.58
5
0.58
5
1
4.8
43
4.8
43
1
3.1
9
3.1
9
1
Nitrite-N
1.3
11
1.3
11
1
45
402
45
402
1
3.3
9
3.3
9
1
NO2+NO3 - N
1.88
15
1.88
15
1
49.8
444
49.8
444
1
6.4
18
6.4
18
1
TKN
200
1618
200
1618
1
49
437 _
49
437
1
40
113
40
113
1
Final, 8/16/02
4 of 5
13020s003
DMR Data

i
Pi 3
Effluent Monitoring Data
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
March 2002
April 2002
• May 2002
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
Month
Avg.
Max Day
No.
Analyses
31
Effluent Flow
MGD
0.49
0.96
31
0.59
0.99
30
0.56
1.11
Temperature
deg C
16
21
_ 31
23
29
30
24
29
31
pH
SU
7.8
8.1
31
7.9
8.1
30
7.9
8.1
31
Min pH
SU
7.5
7.7
7.7
Fecal Coliform
#/100 ml
13
13
1
393
393
1
1180
1180
1
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
Month
Avg.
(mg/L)
Month
Avg.
(Ib/d)
Max Day
(mg/L)
Max Day
(Ib/d)
No.
Analyses
Month
Avg.
(mg/L)
39
Month
Avg.
(Ib/d)
182
Max Day
(mg/L)
165
Max Day
(Ib/d)
1002
No.
Analyses
22
BOD
Ibs/d
104
423
332
831
20
43
210
93
560
22
Ammonia
Ibs/d
32
130
70
469
20
99
488
238
715
22
94
440
111
613
22
TSS
Ibs/d
13
_ 54
17
119
20
28
136
42
297
_
22
86
400
88
812
22
TN
mg/L
35.2
88
35.2
88
1
38.3
192
38.3
192
1
64.3
391
64.3
391
1
TP
mg/L
4.90
12
4.90
12
1
0.48
2.4
0.48
2.4
1
0.74
4.5
0.74
4.5
1
Total Phenols
Ibs/d
0.29
1.17
0.3
1.66
4
0.14
0.67
0.13
0.92
5
0.07
0.33
0.1
0.58
4
Total Sulfate
mg/L
1520
6212
1856
12074
4
1639
8065
1878
11904
4
1736
8108
2172
11593
5
COD
mg/L
236
964
461
1192
20
460
2263
687
4354
22
567
2648
775
3102
22
MBAS
mg/L
<0.1
<0.25
<0.1
<0.25
1
<0.1
<0.5
<0.1
<0.5
1
<0.1
<0.6
<0.1
<0.6
1
Manganese
mg/L
0.47
1.18
0.47
1.18
1
0.4
2.0
0.4
2.0
1
0.26
1.6
0.26
1.6
1
Iron
mg/L
0.5
1.25
0.5
1.25
1
0.3
1.5
0.3
1.5
1
0.5
3.0
0.5
3.0
1
Chlorides
mg/L
930
2327
930
2327
1
4.1
21
4.1
21
1
750
4566
750
4566
1
Mercury
mg/L
0.0004
0.0004
1
0.0002
0.0002
1
0.0010
0.0010
1
Mercury
Ibs/d
0.0010
0.0010
1
0.0010
0.0010
1
0.0061
0.0061
1
Nitrate-N
<2
<5
<2
<5
1
9.2
46
9.2
46
1
0.15
0.91
0.15
0.91
1
Nitrite-N
9.2
23
9.2
23
1
<0.1
0.5
<0.1
0.5
1
<0.1
0.61
<0.1
0.61
1 _
NO2+NO3 - N
11.2
28
11.2
28
1
9.3
46.5
9.3
46.5
1
0.25
1.5
0.25
1.5
1
TKN
24
60 _
24
60
1
29 _
145
29
145
1
64
390
64
390
1
Final, 8/16/02
5 of 5
13020s003
DMR Data

i
1
Effluent Data - Quarterly Monitoring of OCPSF Parameters
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
08/01/01
11/07/01
02/06/02
05/01/02
Long -Term
Average
Max Day
Avg
(ug/L)
Avg
(lb/d)
Avg
(ug/L)
Avg
(Ib/d)
Avg
(ug/L)
Avg
(lb/d)
Avg
(ug/L)
Avg
(Ib/d) .
Avg
(ug/L)
(Ib/d)
Avg
(ug/L)
(Ib/d)
Effluent Flow for Sample
MGD
0.89
0.7
0.34
0.73
1,3-Dichlorobenzene
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
4-Chloro-3-methylphenol
lb/d
<51
<0.379
11
0.064
<5.2
<0.015
13
0.079
20
0.134
<51
<0.379
2-Methylphenol
lb/d
<51
<0.379
<5.0
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
4,6-Dimethyphenol
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Pentachlorophenol
lb/d
<260
<1.933
<25
<0.145
<26
<0.073
<25
<0.152
<84
<0.576
<260
<1.933
2,4,5-Trichlorophenol
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Acenaphthene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Acrylonitrile
lb/d
<100
<0.744
<100
<0.582
<100
<0.280
<100
<0.607
<100
<0.553
<104
<0.744
Benzene
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Carbon Tetrachloride
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Chlorobenzene
lb/d
9.4
0.07
<5
<0.029
12
0.034
<5
<0.030
8
0.041
12
0.034
1,4-Dichlorobenzene
lb/d
7.4
0.055
<5
<0.029
<5
<0.014
<5
<0.030
6
0.032
7.4
0.055
1,2,4-Trichlorobenzene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Hexachlorobenzene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
1,2-Dichloroethane
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
1,1,1-Trichloroethane
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Hexachloroethane
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
1,1-Dichloroethane
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Chloroethane
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Chloroform
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
2-Chlorophenol
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
1,2-Dichlorobenzene
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
1,1- Dichloroethylene
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
1,2-trans-Dichloroethylene
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
2,4-Dichlorophenol
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
1,2-Dichloropropane
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
1,3-Dichloropropylene
lb/d
<10
<0.074
<10
<0.058
<9.9
<0.028
<10
<0.061
<10
<0.055
<10
<0.074
2,4-Dimethylphenol
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
2,4-Dinitrotoluene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
2,6-Dinitrotoluene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Ethylbenzene
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Fluoranthene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Methylene Chloride
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Methyl Chloride
lb/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Hexachlorobutadiene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Naphthalene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Nitrobenzene
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
2-Nitrophenol
lb/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
4-Nitrophenoi
lb/d
<260
<1.933
<25
<0.145
<26 ,
<0.073
<25
<0.152
<84
<0.576
<260
<1.933
Final, 8/16/02
1 of 2
13020s003
DMR OCPSF

I
Effluent Data - Quarterly Monitoring of OCPSF Parameters
Clariant Corporation - Mt. Holly
Parameter
DMR
Units
08/01/01
11/07/01
02/06/02
05101/02
Long -Term
Average
Max Day
Avg
(ug/L)
Avg
(Ib/d)
Avg
(ug!L)
Avg
(Ib/d)
Avg
(ug/L)
Avg
(Ib/d)
Avg
(ug/L)
Avg
(Ib/d)
Avg
(ug/L)
<84
(Ib/d)
<0.576
Avg
(ug/L)
<260
(Ib/d)
<1.933
2,4-Dinitrophenol
Ib/d
<260
<1.933
<25
<0.145
<26
<0.073
<25
<0.152
4,6-Dinitro-o-cresol
Ib/d
<260
<1.933
<25
<0.145
<26
<0.073
<25
<0.152
<84
<0.576
<260
<1.933
Phenol
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Bis(2-ethylhexyl)phthalate
Ib/d
<51
_ <0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Di-n-butyl phthalate
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Diethyl phthalate
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379 ,
Dimethyl phthalate
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Benzo(a)anthracene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Benzo(a)pyrene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
3,4-Benzofluoranthene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379 -
Benzo(k)fluoranthene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Chrysene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
_
<0.379
Acenaphthylene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Anthracene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Fluorene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Phenanthrene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379 ,
Pyrene
Ib/d
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<17
<0.113
<51
<0.379
Tetrachloroethylene
Ib/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Toluene
Ib/d
<5
<0.037
<5
<0.029
8.1
0.023
<5
<0.030
5.7
0.030
8.1
0.023
Trichloroethylene
Ib/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
_
<0.037
Vinyl Chloride
Ib/d
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.028
<5
<0.037
Total Cyanide
Ib/d
9
0.0669
<2
<0.0116
2.6
0.0073
4.7
0.0285
4.6
0.029
9
_
0.0669
Final, 8/16/02
2 of 2
13020s003
DMR OCPSF

APPENDIX B
PRIORITY POLLUTANT ANALYSIS
CLARIANT WWTP EFFLUENT

1
1
Clariant Corporation - Effluent Data
EPA I.D. Number. NCD001810365
Duffel!: 001
Compound
Sample Date.
Sample Date.6126/02
Sample Date. 8/1/01
Sample Date.
Sample Date. 2/6/02
Sample Date. 5/1/02
Max Day
Long -Term Average
No. of
9/19/01
11/7/01
Flow. 0.62 MGD
Flow, 0.54 MGD
Flow. 0.89 MGD
Flow. 0,70 MGD
Flow. 0.34 MGD
Flow. 0.73 MGD
Concen-
tration
(ug1L)
Mass
(Ibld)
Concen-
tration
(uglL)
Mass
(Ib/d)
Concen-
tration
(uglL)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(lb/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(mg/L)
Mass
(lb/d)
Concen-
tration
(ug/L)
Mass
(Ibld)
Concen-
tration
(ug/L)
Mass
(Ibld)
Analyses
Volatile Organics
Acrolein
<100
<0.52
<100
<0.45
<100
<0.52
<100
<0.484
2
Acryl
<
<0.52
<100
<0.45
<100
<0.744
<100
<0.582
<100
<0.280
<100
<0.607
<100
<0.744
<100
<0.530
6
a>
9.7
0.050
<5
<0.02
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
9.7
0.050
6
0.030
6
- • Alchloromethane
<
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
Bromoform
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2 _
Bromomethane
<10
, <0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Carbon etr-chloride
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.037
<5
<0.026
6
_thlorobenzne_.-
4rni.
<0.051
<6
<0.027
944
0.07
<5
<0.029
(12
0.034
<5
<0.030
12
0.034
8
0.040
6
Chloroethane
<10
<0.052
<10
<0.045
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.034
6
2-Chloroethyl vinyl ether
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Chloroform
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.037
<5
<0.026
6
Chforomethane
<10
<0.052
<10
<0.045
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.034
6 -
Dibromochloromethane
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
1,1-Dichloroethane
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.037
<5
<0.026
6
1,2-Dichloroethane
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.037
<5
<0.026
6
1,1-Dichloroethylene
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
trans-1,2-Dichloroethylene
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
1,2-Dichloropropane
<6
<0.031
<6
<0.027
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<6
<0.031
<5
<0.028
6
cis-1,3-Dichloropropene
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
trans-1,3-Dichloropropene
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
Ethylbenzene
<8
<0.041
<8
<0.036
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<8
<0.041
<6
<0.031
6 -
Methylene chloride
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.037
<5
<0.026
6
1,1,2,2-Tetrachloroethane
<7
<0.036
<7
<0.032
<7
<0.036
<7
<0.034
2 _
Tet thylene
'
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<5
<0.037
<5
<0.026
6
oluene
�72
<0.040
<6
<0.027
<5
<0.037
<5
<0.029
8.1 j
0.023
<5
<0.030
8.1
0.023
6.1
0.03 '
6
, , - richloroethane
<5
<0.026
<5
<0.023
<5
<0.037
<5
<0.029
-<5
<0.014
<5
<0.030
<5
<0.037
<5..
\i
_
6
1,1,2-Trcchloroethane
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
Trichloroethylene
<5
<0.026
<5
<0.023
<5
<0.026
<5
<0.024
2
Trichlorofluoromethane
<10
<0.052
<10
<0.045
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.034
6
Vinyl chloride
<10
<0.052
<10
<0.045
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.034
6
Acid Extractables
4-Chloro-3-methylphenol
<10
<0.052
<10
<0.045
<51
<0.379
11
0.064
<5.2
<0.015
13
0.079
<51
<0.379
<17
<0.106
6
2-Chlorophenol
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
2,4-Dichlorophenol
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
2,4-Dimethylphenol
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
ni rophtno
�,6-dinitrophenol
<50
<0.259
<50
<0.225
<260
<1.933
<25
<0.145
<26
<0.073
<25
<0.152
<260
<1.933
<73
<0.464
6
<50
<0.259
<50
<0.225
<50
<0.259
<50
<0.242
2
2-Nitrophenol
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
c A -NI rf hnol?
<50
<0.259
<50
<0.225
<260'_
<1.933
<25
<0.145
<26
<0.073
<25
<0.152
<260
<1.933
<73
<0.464
6
Final, 8/16/02
Page 1 of 4
13020s003
P. Pollut

3
1
Clariant Corporation - Effluent Data
EPA I.D. Number. NCD001810365
Duffel!: 001
Compound
Sample Date,
9/19/01
Flow. 0.62 MGD
Sample Date.6/26/02
Sample Date. 8/1/01
Sample Date.
Sample Date. 216/0Z
Sample Date, 5/1/02
Max Day
Long -Term Average
No. of
11/7/01
Flow. 0.54 MGD
Flow. 0.89 MGD
Flow. 0.70 MGD
Flow. 0.34 MGD
Flow. 0.73 MGD
Concen-
tration
(uglL)
Mass
(Ib/d)
Concen-
tration
(ug!L)
Mass
(Ibld)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(mg/L)
Mass
(Ib/d)
Concen-
tration
(uglL)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Pentachlorophenol
<50
<0.259
<50
<0.225
<260
<1.933
<25
<0.145
<26
<0.073
<25
<0.152
<260
<1.933
<73
<0.464
6
Phenol
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
2,4,6-Trichlorophenol
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Base Neutrals
Acenaphthene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Acenaphthylene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
_
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Anthracene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Benzidine
<50
<0.259
<50
<0.225
<50
<0.259
<50
<0.242
2
Benzo (a) anthracene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Benzo (a) pyrene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Benzo(b)fluoranthene
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2 .
Benzo (ghi) perylene
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Benzo (k)fluoranthene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379_
<14
<0.092
6
Bis(2-chloroethoxy) methane
<10
<0.052
<10
<0.045
_
-
<10
<0.052
<10
<0.048
2
Bis(2-chforoethyi) ether
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048 -
2
Bis(2-chloroisopropyl) ether
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Bis(2-ethylhexyl) phthalate
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
4-Bromophenyl phenyl ether
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Butyl benzyl phthalate
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
2-Chtoronaphthalene
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
4-Chlorophenyl phenyl ether
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Chrysene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Dibenzo (a,h) anthracene
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
1,2-Dichlorobenzene
<10
<0.052
<10
<0.045
<5
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.034
6
1,3-Dichlorobenzene
<10
<0.052
<10
<0.045
<
<0.037
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.034
6
1,4-Dichlorobenzene
<10
<0.052
<10
<0.045
7.4 `
0.055
<5
<0.029
<5
<0.014
<5
<0.030
<10
<0.052
<7
<0.037
6
3,3-Dichtorobenzidine
<20
<0.103
<20
<0.090
<20
<0.103
<20
<0.097
2
Diethyl phthalate
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Dimethyl phthalate
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Di-n-butyl phthalate
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
2,4-Dinitrotoluene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
2,6-Dinitrototuene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Di-n-octyl phthalate
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
1,2-Diphenylhydrazine
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Fluoranthene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Fluorene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Hexachlorobenzene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Hexachlorobutadiene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Hexachtorocyclopentadlene
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Hexachloroethane
<10
<0.052
<10 _
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Final, 8/16/02
Page 2 of 4
13020s003
P. Pollut

l 1 )
1
9
Clariant Corporation - Effluent Data
EPA I.D. Number. NCD001810365
Outfall: 001
Compound
Sample Date.
Sample Date.6/26102
Flow. 0.54 MGD
Sample Date. 8/1/01
Sample Date.
Sample Date. 2/6/02
Sample Date. 5/1/02
Max Day
Long -Term Average
No. of
9/19/01
11/7/01
Flow. 0.62 MGD
Flow. 0.89 MGD
Flow. 0.70 MGD
Flow. 0.34 MGD
Flow. 0.73 MGD
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ibld)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(mg/L)
• Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Indeno (1,2,3-cd) pyrene
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Isophorone
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Naphthalene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Nitrobenzene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6 t
N-nitrosodimenthylamine
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
N-nitroso-di-n-propylamine
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
N-nitrosodiphenylamine
<10
<0.052
<10
<0.045
<10
<0.052
<10
<0.048
2
Phenanthrene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Pyrene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
1,2,4-Trichlorobenzene
<10
<0.052
<10
<0.045
<51
<0.379
<5
<0.029
<5.2
<0.015
<5
<0.030
<51
<0.379
<14
<0.092
6
Pesticides and PCBs
Aldrin
<0.05
<0.0003
<0.05
<0.0002
<0.05
<0.0003
<0.05
<0.0002
2
Alpha-BHC
<0.05
<0.0003
<0.05
<0.0002
<0.05
<0.0003
<0.05
<0.0002
2
Beta-BHC
<0.05
<0.0003
<0.05
<0.0002
<0.05
<0.0003
<0.05
<0.0002
2
Delta-BHC
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
2
Gamma-BHC (Lindane)
<0.05
<0.0003
<0.05
<0.0002
<0.05
<0.0003
<0.05
<0.0002
2 _
Chlordane
<0.2
<0.0010
<0.2
<0.0009
<0.2
<0.001
<0.2
<0.001
2
4,4'-ODD
<0.1
<0.0005
0.28
0.0013
0.28
0.0013
0.19
0.0009
2
4,4'-DDE
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
2
4,4'-DDT
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
2
Dieldrin
<0.02
<0.0001
<0.02
<0.0001
<0.02
<0.0001
<0.02
<0.0001
2
Endosulfan I (alpha)
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
<0.1
<0.0005
2
Endosulfan II (beta)
<0.1
<0.0005
0.26
0.0012
0.26
0.0012
0.18
0.0008
2
Endosulfan sulfate
<0.7
<0.0036
<0.7
<0.0032
<0.7
<0.004
<0.7
<0.003
2
Endrin
<0.06
<0.0003
<0.06
<0.0003
<0.06
<0.0003
<0.06
<0.0003
2
Endrin aldehyde
<0.2
<0.0010
<0.2
<0.0009
<0.2
<0.001
<0.2
<0.001
2
Heptaehr� le__
<0.05
<0.0003
<0 •
<0.0002
<0.05
<0.000
<0.05
<0.000
2 _
Heptachlor epoxy
<0.8
<0.0041
a
0.0039
0.86
0.0039
0.83
0.0040
2
or
<0.5
<0.0026
1 .
<0.0023
<0.5
<0.003
<0.5
<0.002
2
Mirex
<0.2
<0.0010
<0.2
<0.0009
<0.2
<0.001
<0.2
<0.001
2 _
Toxaphene
<2.4
<0.0124
<2.4
<0.0108
<2.4
<0.012
<2.4
<0.012
2
PCB 1016
<1.0
<0.0052
<1.0
_ <0.0045
<1.0
<0.005
<1.0
<0.005
2
PCB 1221
<1.0
<0.0052
<1.0
<0.0045
<1.0
<0.005
<1.0
<0.005
2
PCB 1232
<1.0
<0.0052
<1.0
<0.0045
<1.0
<0.005
<1.0
<0.005
2
PCB 1242
<1.0
<0.0052
<1.0
<0.0045
<1.0
<0.005
<1.0
<0.005
2
PCB 1248
<1.0
<0.0052
<1.0
<0.0045
<1.0
<0.005
<1.0
<0.005
2
PCB 1254
<1.0
<0.0052
<1.0
<0.0045
<1.0
<0.005
<1.0
<0.005
_
2
PCB 1260
<1.0
<0.0052
<1.0
<0.0045
<1.0
<0.005
<1.0
<0.005
2
Demeton
<2.5
<0.0129
<2.5
<0.0113
<2.5
<0.013
<2.5
<0.012
2
Parathion (ethyl)
<0.6
<0.0031
<0.6 _
<0.0027
<0.6
<0.003
<0.6
<0.003
2
Final, 8/16/02
Page 3 of 4
13020s003
P. Pollut

$ D ) 1 } B
0
Clariant Corporation - Effluent Data
EPA I.D. Number: NCD001810365
Outfall: 001
Compound
Sample Date.
Sample Date.6/26/02
Sample Date. 8/1/01
Sample Date.
Sample Date. 2/6/0Z
Sample Date. 5/1/02
Max Day
Long -Term Average
No. of
9/19/01
11/7/01
Flow. 0.62 MGD
Flow. 0.54 MGD
Flow. 0.89 MGD
Flow. 0.70 MGD
Flow.9.34 MGD
Flow. 0.73 MGD
Concen-
tration
(ug/L)
Mass
(Ibld)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ibld)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(uglL)
Mass
(Ib/d)
Concen-
tration
(p(g/
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
Concen-
tration
(ug/L)
Mass
(Ib/d)
_
Herbicides
2,4-D
<12.0
<0.062
<12.0
<0.05
<12
<0.062
<12
<0.058
2
Silvex
<2.0
<0.010
<2.0
<0.01
<2.0
<0.010
<2.0
<0.010
2
2,4,5-T
<2.0
<0.010
<2.0
<0.01
<2.0
<0.010
<2.0
<0.010
2 _
Metals
_
Aluminum
<100
<0.52
300
1.35
300
1.35
200
0.93
2
Antimony
<50
<0.26
< 0
<0.23
<50
<0.26
<50
<0.242
2
Arsenic
<10
<0.05
<10
<0.05
<10
<0.052
<10
<0.048
2
Beryllium
<25
<0.13
<25
<0.11
<25
<0.13
<25
<0.121
2
Cadmium
<2
<0.01
<2
<0.01
<2
<0.010
<2
<0.010
2
Ch um
<5
<0.03
<5
<0.02
<5
<0.03
<5
<0.024
2
opper)
4�
0.12
29
0.13
29
0.13
27
0.13
2
Lead.._
<10
<0.05
<10
<0.05
<10
<0.052
<10
<0.048
2
ercury)
C1
<0.00
<0.2
<0.001
0.2
0.001
0.2
0.001
2
<
<10
<0.052
(2)
0.054
12
0.054
11
0.053
2
Selenium
-
<5
<0.03
<5
<0.02
<5
<0.026
<5
<0.024
2
Silver
<5
<0.03
<5
<0.02
<5
<0.026
<5
<0.024
2
-
Zinc
<10
<0.05
34
0.15
34
0.15
22
0.10
2
Other Inorganics
-
-
<500
<2.59
< 0
<2.3
<500
<2.59
<500
<2.42
2
�•�•
44001
2275
8000'
1261
�-
440000
2275
360000
1768
2
Cyanid
0
<0.10
0
<0.09
9
0.0669
<2j
<0.0116
2.q
0.0073
j4
0.0285
<20
<0.103
<10
<0.051
6
.. on • ='
1300
11.9
82o
3.7
2300
11.9
1560
7.8
2
Final, 8/16/02
Page 4 of 4
13020s003
P. Pollut

APPENDIX C
NORFLURAZON PRODUCTION SCHEMATIC

1
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s
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i
pt. :c.lit'aATl014 ! ; tZecht•.lc-r tom ! .
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zsq. i�1ao H
fil i S pt.. (,R)
1.PR'
IYEN I
: G0041E.1JSE(2.S
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I
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4 I
SS
I .
I
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NORFLuRRION
1
•
R‘v4C�'
1 1
- i -
1 L H. 1
tv o a . Na L.tsea of _
P;lA . 1 czi LUog� a.TNY AN! tL'L'
i 1 I
MUGS - i`nUCro4ltt ot2.. I Rc v8 _...
n - I:soirRisoc4:(...1 II t-IL
(.iMfA - ME to _.'G1r,ti I ..1 !.._
t-4xOL - - TR% I ei /L3EN�t* .
( iR)! - RccYc..,L-c-i 1
( Lr) - LA,)',,c)-1L:L— I - .. __
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1—
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TIti o1 wauD j-L.ntloadS
ry
0
0
1
rge

APPENDIX D
, STORMWATER DETERMINATIONS
CLARIANT-MT. HOLLY EAST FACILITY

Fm1
1p
ago
ran
APPENDIX D
OCPSF STORMWATER DISCHARGES DRAINED TO WWTP -
BASIS FOR CATEGORY
A portion of the stormwater from the Clariant property is treated with process wastewater in
the on -site WWTP. The total stormwater area drained to the WWTP is 4,574,000 ft2. The
average precipitation in Charlotte, NC as provided by NOAA is 43.09 inches/yr. This is
equivalent to approximately 0.118 inches/day. Based on the average annual rainfall, the
various areas of drainage and the degree of imperviousness in each area, the average daily
stormwater runoff was calculated to be 283,000 gpd. Of the total stormwater runoff, 251,000
gallons is considered to be OCPSF and 32,000 gallons is considered to be non -categorical.
Stormwater drainage areas and associated runoff are summarized in Table D-1. Stormwater
drainage areas are shown on the stormwater site plan included with the permit application.
The OCPSF stormwater sources include the following:
• Effluent Holding Basin
• Landfill Ce11 3
• Production Buildings Area
• Former Dinitrophenol Production Area
• WWTP Area
These sources are discussed below.
Effluent Holding Basin
The effluent holding basin is typically not used during the summer when the WWTP is
operating most effectively. The basin captures precipitation and some stormwater which
comes into contact with the basin walls, process wastewater sludges and settled material
contained in the basin, which is then treated in the WWTP.
Landfill Cell 3
All stormwater that falls on the landfill is collected as leachate and treated in the WWTP. The
landfill is designed so that none of the stormwater runs off and none of the stormwater
infiltrates the groundwater.
Production Building Area
This area comprises the chemical and dye manufacturing production area.
Former Dinitrophenol Production Area
Dinitrophenol (DNP) was formerly produced in an area near the Production Building Area.
The DNP production facility was shut -down and demolished and replaced with lawn.
However, the soil in this location is visibly contaminated with DNP which leaches to the
surface of the ground from subsurface sources. All stormwater drainage from this area is
considered to be contaminated with dinitrophenol.
WWTP Area
The area of the WWTP captures precipitation and stormwater from the immediate surrounding
impervious area, which combines with the process wastewater and is treated in the WWTP.

I 1 I 1 .1 / I 1 1 I $ 1, I 1 1
t
I I 1
TABLE D-1
SUMMARY OF STORMWATER DRAINAGE TO WWTP
Clariant Corporation - Mt. Holly East Plant
NPDES Permit No. NC0004375
Category
g ry
Stormwater Drainage Area DescriptionRun-off
g p
Surface Area
Impervious Area
Pervious
Area .Stormwater
Run-off
Coefficient
(C)
Runoff
(9Pd)(1)
Stormwater
Infiltration
(9Pd)(1)
acres
ft2
%
Coefficient
(C)
%
OCPSF
Wastewater Impoundment (Eff. Holding
34.14
1,487,138
100%
1.00
0%
109,384
0
Basin)
Landfill Cell 3
4.06
176,854
100%
1.00
0%
13,008
0
Production Buildings Area
34.14
1,487,138
100%
0.90
0%
98,446
10,938
Former Dinitrophenol Production Area
1.03
44,867
0%
100%
0.35
1,155
2,145
WVVTP Area
9.89
430.808
100%
0.90
0%
28.519
3,169
Total OCPSF =
83.26
3,627,000
251,000
16,000
Non -Categorical
All other areas that drain to WWTP
21.74
947,000
20%
0.90
80%
0.35
32,000
38,000
Total Stormwater Drainage =
105.00
4,574,000
283,000
54,000
Notes:
(1) Stormwater flow is based on NOAA Average Charlotte, NC rainfall of 43.09" per year. Average daily rainfall
based on 365 days is 0.118".

APPENDIX E
3'D PARTY SOLICITED WASTEWATERS
2001-2002
CLARIANT-MT. HOLLY EAST FACILITY

fmt
Third Party OCPSF Wastewater
2001 Summary
Clariant Corporation - Mt. Holly
August 2001
September 2001
October 2001
November 2001
December 2001
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
08.28.01
4635
09.05.01
2983
10.01.01
4018
11.01.01
4668
12.03.01
5284
08.29.01
4479
09.06.01
5417
10.02.01
2905
11.01.01
2979
12.04.01
2516
08.30.01
4639
09.06.01
4221
10.02.01
2960
11.05.01
5239
12.04.01
4516
09.07.01
5198
10.02.01
4054
11.06.01
4496
12.04.01
5258
09.07.01
5078
10.03.01
5486
11.07.01
2770
12.04.01
4534
09.07.01
4315
10.03.01
3700
11.07.01
2327
12.05.01
5094
09.11.01
4357
10.03.01
5474
11.07.01
3978
12.05.01
4564
09.12.01
4762
10.04.01
4113
' 11.08.01
2550
12.06.01
2413
09.12.01
3477
10.04.01
5975
' 11.09.01
2461
12.06.01
4113
09.13.01
4108
10.05.01
5425
11.09.01
4383
12.06.01
3936
09.17.01
4992
10.05.01
4136
11.13.01
2265
12.06.01
5001
09.17.01
3548
10.05.01
3801
11.13.01
2938
12.06.01
3887
09.19.01
4516
10.08.01
4142
11.13.01
5037
12.10.01
4295
09.19.01
3866
10.09.01
3828
11.14.01
2948
12.10.01
5332
09.20.01
3782
10.09.01
5658
11.15.01
4864
12.10.01
4183
09.21.01
4649
10.09.01
3497
11.19.01
4637
12.10.01
5439
09.21.01
4212
10.10.01
4249
11.20.01
5256
12.11.01
4934
09.24.01
3868
10.10.01
2272
11.20.01
3581
12.11.01
4437
09.25.01
4791
10.11.01
4817
11.21.01
5217
12.11.01
5206
09.26.01
3952
10.11.01
4179
11.27.01
4946
12.11.01
5072
09.26.01
3616
10.12.01
2981
11.27.01
4902
12.11.01
2591
09.27.01
3024
10.12.01
2968
11.28.01
5049
12.12.01
5314
09.28.01
3048
10.12.01
5431
11.28.01
5444
12.12.01
3894
09.28.01
3068
10.15.01
4189
11.29.01
5067
12.13.01
5162
09.28.01
4671
10.15.01
5536
11.30.01
4304
12.14.01
4752
10.16.01
4088
11.30.01
2147
12.14.01
5307
10.16.01
5850
11.30.01
4618
12.17.01
2049
10.16.01
3983
11.30.01
5337
12.17.01
5318
10.17.01
3034
12.17.01
4707
10.17.01
5718
12.18.01
4243
10.18.01
2976
12.18.01
5212
10.18.01
5905
12.18.01
5158
10.19.01
5603
12.19.01
4513
10.22.01
4721
12.19.01
5,275
10.22.01
5789
12.19.01
5102
10.23.01
4318
12.20.01
5061
10.23.01
5693
12.21.01
4635
10.24.01
5876
12.21.01
3075
10.25.01
4764
12.27.01
1452
10.25.01
4226
12.28.01
3556
10.26.10
4438
12.28.01
4455
10.29.01
4810
12.28.01
4635
10.29.01
1078
12.28.01
5455
Final, Page 1 of 2
8/16/02
13020s004
2001

,a Third Party OCPSF Wastewater
2001 Summary
Clariant Corporation - Mt. Holly
Mil
Pa,
AM
Ail
OM
Pal
PRI
1I
r=1
OKI
PM
MI
rwf
Mal
MEI
August 2001
September 2001
October 2001
November 2001
December 2001
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
10.30.01
4371
12.28.01
3954
10.31.01
3604
12.28.01
4882
12.31.01
1,531
12.31.01
1,520
12.31.01
3,583
12.31.01
4,226
12.31.01
4,714
12.31.01
4,235
12.31.01
4,860
12.31.01
5,100
12.31.01
4,446
12.31.01
5,402
Final, Page 2 of 2
8/16/02
13020s004
2001

r�
furl
PIM
REIM
Pan
rArs
Port
Pin
Fan
Third Party OCPSF Wastewater
2002 Summary
Clariant Corporation - Mt. Holly
January 2002
February 2002
March 2002
April 2002
May 2002
June 2002
July 2002
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
01.02.02
1,642
02.01.02
4,380
03.01.02
5,562
04.01.02
4,653
05.01.02
5,994
06.03.02
5,934
07.01.02
5,701
01.07.02
5,600
02.01.02
4,949
03.01.02
4,949
04.01.02
4,234
05.01.02
5,944
06.03.02
3,832
07.01.02
5,785
01.07.02
1,424
02.01.02
3,059
03.01.02
5,494
04.01.02
5,785
05.01.02
5,898
06.03.02
4,809
07.01.02
5,615
01.07.02
2,676
02.01.02
4,259
03.01.02
4,440
04.01.02
5,958
05.01.02
5,565
06.04.02
5,886
07.01.02
5,939
01.08.02
5,150
02.01.02
2,706
03.01.02
4,957
04.02.02
5,159
05.01.02
5,709
06.04.02
5,804
07.01.02
3,942
01.09.02
4,594
02.01.02
3,007
03.01.02
3,368
04.02.02
5,752
05.01.02
5,806
06.04.02
5,932
07.01.02
3,762
01.09.02
5,512
02.04.02
5,483
03.01.02
5,919
04.02.02
5,900
05.02.02
5,910
06.04.02
5,831
07.01.02
1,985
01.10.02
5,651
02.04.02
5,115
03.01.02
6,020
04.03.02
5,728
05.02.02
5,759
06.04.02
5,178
07.01.02
3,311
01.10.02
4,624
02.04.02
5,328
03.01.02
5,850
04.04.02
4,027
05.02.02
5,948
06.04.02
4,972
07.02.02
5,615
01.10.02
5,151
02.04.02
5,037
03.01.02
6,006
04.04.02
3,772
05.02.02
5,783
06.05.02
5,864
07.02.02
5,891
01.10.02
3,113
02.04.02
4,880
03.01.02
5,591
04.04.02
5,617
05.02.02
5,629
06.05.02
5,807
07.02.02
5,689
01.11.02
4,548
02.04.02
3,951
03.01.02
3,440
04.05.02
4,559
05.02.02
5,496
06.05.02
6,054
07.02.02
5,828
01.11.02
5,499
02.05.02
4,377
03.02.02
5,584
04.05.02
929
05.02.02
391
06.05.02
324
07.02.02
3,153
01.14.02
4,667
02.05.02
4,857
03.04.02
3,518
04.05.02
5,640
05.03.02
5,807
06.06.02
5,891
07.03.02
4,568
01.14.02
5,160
02.05.02
5,533
03.04.02
5,728
04.05.02
394
05.03.02
5,730
06.06.02
5,944
07.03.02
5,641
01.15.02
5,368
02.05.02
5,680
03.04.02
4,470
04.08.02
5,761
05.03.02
5,917
06.06.02
6,188
07.03.02
5,910
01.15.02
5,553
02.05.02
5,073
03.04.02
5,469
04.08.02
5,900
05.03.02
5,692
06.06.02
5,860
07.03.02
5,581
01.16.02
5,156
02.05.02
2,841
03.04.02
6,037
04.08.02
5,843
05.03.02
7,220
06.06.02
5,402
07.03.02
5,924
01.17.02
4,753
02.05.02
3,104
03.04.02
5,638
04.09.02
4,278
05.04.02
5,821
06.07.02
6,138
07.03.02
3,390
01.17.02
5,538
02.06.02
4,155
03.04.02
5,887
04.09.02
5,864
05.04.02
5,824
06.07.02
5,804
07.03.02
2,272
01.18.02
2,248
02.06.02
4,238
03.04.02
5,756
04.10.02
4,275
05.04.02
5,711
06.07.02
5,912
07.05.02
5,493
01.18.02
5,056
02.06.02
4,753
03.05.02
5,495
04.11.02
4,329
05.06.02
5,687
06.07.02
4,411
07.05.02
5,590
01.21.02
4,531
02.06.02
3,984
03.05.02
4,486
04.11.02
2,517
05.06.02
5,716
06.07.02
1,581
07.05.02
5,464
01.21.02
5,106
02.06.02
5,331
03.05.02
4,670
04.12.02
4,336
05.06.02
5,869
06.10.02
5,903
07.05.02
3,804
01.22.02
5,077
02.06.02
3,621 -
03.05.02
4,545
04.12.02
3,653
05.06.02
5,581
06.10.02
5,804
07.05.02
2,127
01.22.02
5,324
02.06.02
5,020
03.05.02
5,547
04.12.02
3,373
05.06.02
2,872
06.10.02
4,401
07.05.02
3,768
01.22.02
2,808
02.07.02
5,221
03.05.02
3,571
04.12.02
1,986
05.06.02
2,155
06.10.02
4,337
07.05.02
3,746
01.23.02
5,397
02.07.02
4,218
03.05.02
6,064
04.12.02
3,260
05.07.02
5,845
06.10.02
5,371
07.05.02
338
01.23.02'
5,117
02.07.02
3,701
03.05.02
5,901
04.12.02
4,400
05.07.02
5,886
06.11.02
5,788
07.08.02
5,588
01.23.02
3,602
02.07.02
4,136
03.05.02
6,054
04.12.02
401
05.07.02
550
06.11.02
3,574
07.08.02
5,647
01.25.02
4,252
02.07.02
3,858
03.05.02
5,927
04.15.02
4,263
05.07.02
1,454
06.13.02
5,891
07.08.02
5,584
01.25.02
5,123
02.07.02
5,190
03.06.02
5,604
04.15.02
5,984
05.08.02
5,944
06.13.02
5,848
07.08.02
5,915
01.28.02
4,461
02.07.02
3,950
03.06.02
5,538
04.15.02
5,651
05.08.02
5,740
06.13.02
3,203
07.08.02
2,009
01.28.02
5,205
02.08.02
4,780
03.06.02
5,486
04.15.02
5,651
05.09.02
5,761
06.13.02
3,501
07.08.02
4,561
01.28.02
2,871
02.08.02
5,574
03.06.02
5,958
04.16.02
4,368
05.09.02
5,759
06.13.02
2,628
07.09.02
5,874
01.29.02
3,779
02.08.02
2,730
03.06.02
5,813
04.16.02
3,734
05.09.02
365
06.14.02
5,807
07.09.02
5,485
01.29.02
3,918
02.08.02
5,069
' 03.06.02
5,939
04.16.02
5,730
05.10.02
5,680
06.14.02
5,941
07.09.02
5,728
01.29.02
5,104
02.08.02
1,092
03.06.02
5,901
04.16.02
3,630
05.10.02
5,831
06.14.02
3,208
07.09.02
5,972
01.30.02
5,044
02.08.02
413
03.07.02
5,630
04.17.02
5,783
05.13.02
4,864
06.14.02
355
07.09.02
3,690
01.30.02
4,441
02.11.02
5,586
03.07.02
5,574
04.17.02
5,824 '
05.13.02
5,672
06.17.02
4,096
07.10.02
5,900
01.30.02
5,389
02.11.02
4,791
03.07.02
5,426
04.18.02
4,353
05.13.02 '
5,629
06.17.02
5,927
07.10.02
5,893
01.30.02
5,233
02.11.02
4,696
'
03.07.02
5,505
04.18.02
5,828
05.13.02
5,744
06.17.02
6,076
07.10.02
4,321
01.30.02
3,754
02.11.02
5,662
03.07.02
4,430
04.18.02
5,848
05.13.02
5,932
06.17.02
5,850
07.10.02
358
01.31.02
4,340
02.11.02
5,486
03.07.02
6,006
04.19.02
4,369
05.14.02
5,980
06.17.02
5,891
07.11.02
5,812
01.31.02
5,067
02.11.02
5,097
03.07.02
5,840
04.19.02
5,816
05.14.02
5,718
06.17.02
919
07.11.02
5,776
01.31.02
2,791
02.11.02
4,115
03.07.02
5,949
04.19.02
5,800
05.14.02
5,869
06.18.02
5,936
07.11.02
4,811
02.12.02
4,435
03.07.02
5,871
04.19.02
4,400
05.14.02
5,852
06.18.02
5,927
07.11.02
5,603
02.12.02
5,688
03.07.02
5,364
04.20.02
5,726
05.15.02
5,718
06.18.02
5,187
07.12.02
5,927
02.12.02
5,853
03.08.02
4,629
04.20.02
5,716
05.15.02
5,838
06.19.02
5,879
07.12.02
5,884
02.12.02
5,076
03.08.02
5,540
04.20.02
5,785
05.15.02
5,682
06.19.02
5,836
07.12.02
` 5,311
02.12.02
4,452
03.08.02
5,654
04.20.02
5,982
05.15.02
5,761
06.19.02
3,611
07.15.02
5,790
02.13.02
5,850
03.08.02
5,248
04.22.02
5,312
05.15.02
3,808
06.19.02
3,990
07.15.02
5,783
02.13.02
4,668
03.08.02
5,970
04.22.02
5,838
05.15.02
3,086
06.20.02
3,678
07.15.02
4,963
02.13.02
4,645
03.08.02
5,847
04.22.02
5,555
05.16.02
5,771
06.20.02
5,905
07.16.02
4,185
02.13.02
5,342
03.08.02
5,863
04.22.02
5,819
05.16.02
5,680
06.20.02
5,951
07.16.02
5,614
02.13.02
5,552
03.08.02
396
04.22.02
403
05.16.02
5,862
06.21.02
5,696
07.16.02
5,617
02.13.02
5,338
03.11.02
4,581
04.23.02
4,583
05.16.02
5,680
06.21.02
5,924
07.17.02
2,636
Final, Page 1 of 3
8/16/02
13020s004
2002

Fml
MCI
MEI
gni
FIR
Pal
PRI
Plet
PPM
Third Party OCPSF Wastewater
2002 Summary
Clariant Corporation - Mt. Holly
January 2002
February 2002
March 2002
April 2002
May 2002
June 2002
July 2002
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
02.13.02
5,138
03.11.02
5,517
04.23.02
4,784
05.16.02
245
06.21.02
5,764
07.18.02
4,350
02.13.02
2,777
03.11.02
5,218
04.23.02
5,495
05.17.02
5,747
06.21.02
5,816
07.18.02
5,960
02.14.02
5,493
03.11.02
5,453
04.23.02
5,924
05.17.02
5,836
06.21.02
3,877
07.18.02
3,273
02.14.02
5,458
03.11.02
5,298
04.23.02
5,584
05.17.02
283
06.21.02
3,028
07.18.02
367
02.14.02
5,080
03.11.02
5,966
04.23.02
5,696
05.17.02
341
06.21.02
322
07.19.02
5,905
02.14.02
1,688
03.11.02
5,813
04.24.02
4,930
05.20.02
5,612
06.24.02
5,963
07.19.02
5,869
02.15.02
4,960
03.11.02
6,008
04.24.02
4,706
05.20.02
5,682
06.24.02
5,788
07.22.02
5,912
02.15.02
5,017
03.11.02
5,932
04.24.02
5,608
05.20.02
5,989
06.24.02
5,922
07.22.02
5,771
02.15.02
5,495
03.12.02
5,549
04.24.02
5,862
05.20.02
5,561
06.24.02
5,941
07.22.02
4,479
02.15.02
5,677
03.12.02
5,637
04.24.02
5,809
05.20.02
5,927
06.24.02
3,991
07.23.02
4,129
02.15.02
5,361
03.12.02
5,398
04.24.02
4,863
05.21.02
5,879
06.24.02
4,259
07.23.02
4,613
02.15.02
5,140
03.12.02
5,575
04.25.02
4,313
05.21.02
5,764
06.24.02
3,470
02.15.02
3,301
03.12.02
5,835
04.25.02
4,646
05.21.02
5,975
06.25.02
5,920
02.15.02
374
03.12.02
5,963
04.25.02
5,617
05.21.02
5,881
06.25.02
5,807
02.18.02
4,741
03.12.02
5,923
04.25.02
5,800
05.21.02
3,186
06.25.02
5,725
02.18.02
5,483
03.12.02
5,802
04.25.02
5,540
05.22.02
5,857
06.25.02
5,807
02.18.02
5,324
03.12.02
3,830
04.25.02
5,833
05.22.02
5,735
06.25.02
4,505
02.18.02
5,127
03.13.02
2,308
04.26.02
2,695
05.22.02
5,922
06.25.02
5,438
02.18.02
5,188
03.13.02
2,229
04.26.02
5,548
05.22.02
5,636
06.26.02
6,011
02.19.02
4,797
03.13.02
5,604
04.26.02
5,852
05.23.02
5,852
06.26.02
5,809
02.19.02
4,720
03.13.02
4,862
04.26.02
5,730
05.23.02
5,711
06.26.02
5,884
02.19.02
4,509
03.13.02
5,961
04.26.02
4,393
05.23.02
5,872
06.26.02
5,790
02.19.02
5,352
03.13.02
5,825
04.26.02
3,939
05.23.02
5,696
06.26.02
2,771
02.19.02
5,517
03.13.02
5,925
04.26.02
4,881
05.23.02
391
06.26.02
5,370
02.19.02
5,341
03.13.02
5,875
04.27.02
5,744
05.24.02
5,821
06.27.02
5,900
02.19.02
5,203
03.13.02
3,298
04.27.02
5,800
05.24.02
5,706
06.27.02
5,790
02.19.02
5,189
03.14.02
5,581
04.27.02
5,764
05.24.02
5,992
06.27.02
5,912
02.19.02
4,072
03.14.02
5,348
04.27.02
5,898
05.24.02
5,732
06.27.02
5,588
02.19.02
2,999
03.14.02
6,016
04.29.02
4,553
05.24.02
2,575
06.28.02
5,831
02.20.02
5,060
03.14.02
5,740
04.29.02
5,948
05.28.02
5,872
06.28.02
5,692
02.20.02
5,507
03.14.02
5,980
04.29.02
5,749
05.28.02
_
5,684
06.28.02
5,838
02.20.02
5,269
03.14.02
5,917
04.29.02
5,972
05.28.02
4,873
06.28.02
3,434
02.20.02
5,308
03.15.02
5,185
04.29.02
5,694
05.29.02
3,882
06.28.02
336
02.20.02
4,944
03.15.02
5,576
04.29.02
4,996
05.29.02
3,717
02.20.02
5,097
03.15.02
5,932
04.30.02
5,944
05.29.02
5,692
02.20.02
4,514
03.15.02
5,797
04.30.02
5,461
05.29.02
5,980
02.21.02
5,623
03.15.02
5,879
04.30.02
6,004
05.29.02
5,744
02.21.02
5,711
03.15.02
5,265
04.30.02
3,614
05.29.02
3,103
02.21.02
4,813
03.15.02
382
04.30.02
5,671
05.29.02
5,376
02.21.02
5,507
03.18.02
5,987
05.29.02
5,704
02.21.02
5,201
03.18.02
5,761
05.29.02
5,319
02.21.02
4,450
03.18.02
6,004
05.29.02
5,255
02.22.02
4,590
03.19.02
4,957
05.30.02
5,912
02.22.02
4,756
03.19.02
5,670
05.30.02
5,718
02.22.02
5,303
03.19.02
5,804
05.30.02
5,869
02.22.02
4,991
03.20.02
4,432
05.30.02
5,735
02.22.02
4,331
03.20.02_
5,833
05.30.02
4,785
02.22.02
4,528
03.20.02
5,910
05.30.02
2,898
02.22.02
3,823
03.20.02
3,011
05.30.02
1,359
02.22.02
418
03.21.02
4,523
05.30.02
5,427
02.23.02
5,597
03.21.02
4,557
05.30.02
5,711
02.23.02
6,137
03.21.02
5,716
05.31.02
4,480
02.23.02
4,474
03.21.02
5,879
05.31.02
5,790
02.25.02
4,643
03.22.02
5,557
05.31.02
_
5,658
02.25.02
5,485
03.22.02
4,944
05.31.02
5,948
02.25.02
4,120
03.22.02
5,863
05.31.02
5,720
02.25.02
5,360
03.22.02
5,735
05.31.02
394
Final, Page 2 of 3
8/16/02
13020s004
2002

Mit
luirt
tml
FEDI
13114
Third Party OCPSF Wastewater
2002 Summary
Clariant Corporation - Mt. Holly
January 2002
February 2002
March 2002
April 2002
May 2002
June 2002
July 2002
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
Date
Volume
(gal)
02.25.02
5,856
03.22.02
2,708
02.25.02
5,977
03.23.02
5,341
02.25.02
5,792
03.23.02
4,518
02.25.02
5,844
03.25.02
5,970
02.25.02
5,600
03.25.02
5,867
02.25.02
5,678
03.25.02
5,927
02.25.02
3,095
03.25.02
5,862
02.26.02
5,298
03.25.02
1,769
02.26.02
4,669
03.26.02
2,318
02.26.02
4,575
03.26.02
4,007
02.26.02
5,155
03.26.02
4,695
02.26.02
6,042
03.26.02
6,059
02.26.02
6,025
03.26.02
5,908
02.26.02
5,920
03.26.02
5,965
02.26.02
5,913
03.26.02
5,783
02.27.02
5,564
03.26.02
3,877
02.27.02
5,357
03.26.02
5,580
02.27.02
4,357
03.27.02
4,530
02.27.02
5,094
03.27.02
6,020
02.27.02
4,340
03.27.02
5,780
02.27.02
5,973
03.27.02
5,471
02.27.02
5,790
03.27.02
5,778
02.27.02
5,958
03.27.02
4,950
02.27.02
5,917
03.28.02
5,180
02.27.02
3,903
03.28.02
4,592
02.28.02
5,411
03.28.02
6,013
02.28.02
4,053
03.28.02
5,888
02.28.02
4,197
03.28.02
5,795
02.28.02
4,606
03.28.02
408
02.28.02
4,416
02.28.02
5,621
02.28.02
4,409
02.28.02
5,944
02.28.02
5,823
02.28.02
5,911
02.28.02
2,464
02.28.02
3,431
02.28.02
5,435
Final, Page 3 of 3
8/16/02
13020s004
2002

2001 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
61N4 Broker: Four Seasons Environmental
Generator Profile No. Date Shipment
Size(gal)
Catawba Charlab MHE-2001-0003 08.28.01 4635
08.29.01 4479
08.30.01 4639
F.;09.05.01 2983
09.06.01 5417
09.07.01 5198
09.07.01 5078
09.12.01 4762
09.12.01 3477
09.17.01 4992
09.19.01 4516
09.21.01 4649
09.27.01 3024
09.28.01 3048
09.28.01 3068
10.02.01 2905
10.02.01 2960
10.03.01 5486
10.05.01 5425
10.11.01 4817
10.12.01 2981
10.12.01 2968
10.17.01 3034
10.18.01 2976
10.22.01 4721
igi, 10.25.01 4764
10.29.01 4810
10.29.01 1078
11.01.01 4668
11.01.01 2979
11.05.01 5239
11.06.01 4496
11.07.01 2770
11.07.01 2327
11.08.01 2550
11.09.01 2461
11.13.01 2265
11.13.01 2938
11.14.01 2948
11.19.01 4637
11.27.01 4946
11.28.01 5049
11.30.01 4304
11.30.01 2147
Pa, 11.30.01 4618
12.04.01 2516
12.06.01 2413
ma, 12.10.01 • 4295
12.11.01 4934
Final, Page 1 of 5 13020s006
8/16/02 Sheetl

2001 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
12.14.01 4752
12.17.01 2049
12.19.01 4513
Im, 12.21.01 4635
POI
ILI
PM
PR
Mal
Catawba Charlab Totals 204,339
Broker: Clariant-Mt. Holly East
Generator Profile No. Date Shipment
Size(gal)
Clariant-Elgin S.C. Plant MHE-2001-0002 09.06.01 4221
09.07.01 4315
09.11.01 4357
09.13.01 4108
MHE-2001-0004 09.17.01 3548
09.19.01 3866
09.21.01 4212
09.25.01 4791
09.26.01 3952
MHE-2001-0012 09.28.01 4671
tam 10.01.01 4018
10.02.01 4054
10.03.01 3700
rim10.04.01 4113
10.05.01 4136
10.08.01 4142
pm10.09.01 3828
10.10.01 4249
10.11.01 4179
10.15.01 4189
rAm
10.16.01 4088
M' MHE-2001-0021 10.23.01 4318
10.25.01 4226
10.26.10 4438
rim 10.30.01 4371
' M H E-2001-0033 12.04.01 4516
12.06.01 4113
12.11.01 4437
gm 12.18.01 4243
psi Clariant-Elgin S.C. Plant Totals 121,399
Final, Page 2 of 5
8/16/02
13020s006
Sheetl

2001 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
,e, Broker: Clariant-Mt. Holly East
Generator
Clariant-Coventry Plant MHE-2001-0017 11.09.01 4383
Clariant-Coventry Plant Totals 4383
Clariant - Leeds Plant MHE-2001-0010 09.24.01 3868
Clariant - Leeds Totals 3868
Broker: Clariant-Mt. Holly East
Generator Profile No. Date Shipment
Size(gal)
Clariant - Millington Plant MHE-2001-0011 09.26.01 3616
508
Clariant - Millington Totals 4124
Clariant - Gainesville Plant MHE-2001-0013 10.03.01 5474
10.04.01 5975
10.09.01 5658
10.12.01 5431
10.15.01 5536
10.16.01 5850
10.17.01 5718
fan 10.18.01 5905
10.19.01 5603
10.22.01 5789
10.23.01 5693
10.24.01 5876
11.13.01 5037
Pal11.15.01 4864
ram
11.28.01 5444
11.29.01 5067
11.30.01 5337
est' 12.03.01 5284
12.04.01 5258
12.05.01 5094
' 12.10.01 5332
12.11.01 5206
12.12.01 5314
F`' 12.13.01 5162
12.14.01 5307
12.17.01 5318
°`' 12.18.01 5212
12.19.01 5,275
a•a
Clariant - Gainesville Plant Totals 167,394
11.20.01 5256
11.21.01 5217
11.27.01 4902
ma► Broker: Four Seasons Environmental
Final,r aorPge 3 of 5 Profile No. Date Shipment
8/16/02
13020s006
Sheetl

IMP
2001 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Size(gal)
Wikoff Color MHE-2001-0005 09.20.01 3782
Wikoff Color Totals
Broker: Haz-Mat
Generator
AEA Technology Engr. Serv.
10.05.01 3801
10.16.01 3983
10.31.01 3604
11.07.01 3978
11.20.01 3581
12.06.01 3936
12.10.01 4183
30,848
Profile No. Date Shipment
Size(gal)
MHE-2001-0015 10.09.01 3497
10.10.01 2272
F■1' AEA Technology Engr. Serv. Totals
Mgt
Pin
Broker: Philips Services
Generator
Stockhausen - Greensboro
Profile No.
MHE-2001-0027
Stockhausen - Greensboro Totals
12.04.01
12.05.01
12.06.01
12.06.01
12.10.01
12.11.01
12.12.01
12.17.01
12.18.01
12.19.01
12.20.01
12.21.01
12.27.01
12.28.01
Broker: CTW Specialties
Generator Profile No.
Stockhausen - Greensboro MHE-2001-0023 12.11.01
Stockhausen - Greensboro Totals
Broker: Resource Management
Generator
CommScope-Catawba
Final, Page 4 of 5
8/16/02
Profile No.
MHE-2001-0034 12.28.01
12.28.01
5769
4534
4564
5001
3887
5439
5072
3894
4707
5158
5102
5061
3075
1452
3556
60,502
2591
2591
4455
4635
13020s006
Sheetl

OKI
2001 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Ac► 12.28.01 5455
12.28.01 3954
12.28.01 4882
1314
CommScope-Catawba Totals 23381
gig
owlTotal Annual Business Level 605,217
001
ram,
Mrs
MCI
Final, Page 5 of 5
8/16/02
13020s006
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Four Seasons Environmental
Generator Profile No.
Catawba Charlab
Catawba Charlab Totals
MHE-2001-0003
Broker: Four Seasons Environmental
Generator Profile No.
Filtration Group MHE-2001-0006
Final, Page 1 of 21
8/16/02
12.31.01
12.31.01
12.31.01
01.10.02
01.14.02
01.15.02
01.17.02
01.18.02
01.22.02
01.23.02
01.25.02
01.29.02
01.30.02
02.04.02
02.07.02
02.11.02
02.13.02
02.15.02
02.19.02
02.22.02
02.25.02
02.27.02
03.04.02
03.08.02
03.11.02
03.13.02
03.13.02
03.15.02
03.20.02
03.21.02
03.21.02
03.22.02
03.26.02
03.26.02
03.27.02
04.01.02
04.02.02
04.05.02
Date Shipment
Size(gal)
1531
1520
3583
5651
4667
5368
4753
2248
5077
5397
4252
3779
5044
5483
5221
5586
5850
4960
4797
4590
4643
5564
3518
4629
4581
2308
2229
5185
4432
4523
4557
5557
2318
4007
4530
4653
5159
4559
166,309
Date Shipment
Size(gal)
04.01.02 4,234
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
04.22.02 5,312
05.13.02 4,864
05.31.02 4,480
06.17.02 4,096
06.20.02 3,678
07.03.02 4,568
07.18.02 4,350
07.18.02 5,960
Broker: Clariant-Mt. Holly East
Generator Profile No. Date Shipment
Size(gal)
Clariant-Elgin S.C. Plant MHE-2001-0033 01.09.02 4594
01.10.02 4624
01.11.02 4548
01.21.02 4531
MHE-2001-0004 01.28.02 4461
01.29.02 3918
01.30.02 4441
02.11.02 4791
02.11.02 4696
02.12.02 4435
02.13.02 4668
02.13.02 4645
02.18.02 4741
02.19.02 4720
04.15.02 4263
04.18.02 4353
04.23.02 4583
04.24.02 4930
04.25.02 4313
04.26.02 2695
MHE-2001-0002 02.01.02 4380
02.05.02 4377
02.05.02 4857
02.06.02 4155
02.06.02 4238
02.06.02 4753
01.31.02 4340
02.07.02 4218
02.15.02 5017
02.19.02 4509
Final, Page 2 of 21
8/16/02
13020s007
Sheetl

figN
2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Final, Page 3 of 21
8/16/02
MHE-2002-0009
02.20.02 5060
04.09.02 4278
04.10.02 4275
04.11.02 4329
04.12.02 4336
04.16.02 4368
04.19.02 4369
04.23.02 4784
04.24.02 4706
04.25.02 4646
02.04.02 5115
02.04.02 5328
02.04.02 5037
02.05.02 5533
02.05.02 5680
02.06.02 3984
02.06.02 5331
02.06.02 3621
02.07.02 3701
02.07.02 4136
02.07.02 3858
02.08.02 4780
02.08.02 5574
02.08.02 2730
02.11.02 5662
02.11.02 5486
02.12.02 5688
02.12.02 5853
02.13.02 5342
02.13.02 5552
02.13.02 5338
02.14.02 5493
02.14.02 5458
02.15.02 5495
02.15.02 5677
02.15.02 5361
02.18.02 5483
02.18.02 5324
02.18.02 5127
02.19.02 5352
02.19.02 5517
02.19.02 5341
02.19.02 5203
02.20.02 5507
02.20.02 5269
02.20.02 5308
02.20.02 4944
02.21.02 5623
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
WI
02.21.02 5711
02.21.02 4813
'm' 02.21.02 5507
02.22.02 4756
02.22.02 5303
'ft' 02.25.02 5485
02.25.02 4120
02.25.02 5360
ra, 02.26.02 5298
02.26.02 4669
02.27.02 5357
mil 02.27.02 4357
02.27.02 5094
02.27.02 4340
02.28.02 5411
02.28.02 4053
02.28.02 4197
02.28.02 4606
02.28.02 4416
02.28.02 5621
03.01.02 5562
ma, 03.01.02 4949
03.01.02 5494
03.01.02 4440
03.01.02 4957
03.01.02 3368
03.02.02 5584
r"' 03.04.02 5728
03.04.02 4470
03.04.02 5469
1221 03.05.02 5495
03.05.02 4486
03.05.02 4670
r_ 03.05.02 4545
03.05.02 5547
03.06.02 5604
ri, 03.06.02 5538
03.06.02 5486
03.07.02 5630
,ag
, 03.07.02 5574
03.07.02 5426
03.07.02 5505
�, 03.08.02 5540
03.08.02 5654
03.08.02 5248
03.11.02 5517
FM
Final, Page 4 of 21
8/16/02
03.11.02 5218
03.11.02 5453
03.12.02 5549
13020s007
Sheetl

MI
2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
01101
egRI
MI
MA
03.12.02 5637
03.12.02 5398
03.12.02 5575
03.13.02 5604
03.14.02 5581
03.14.02 5348
03.15.02 5576
03.23.02 5341
03.23.02 4518
03.28.02 5180
MHE-2001-0033 04.29.02 4553
MHE-2001-0012 02.26.02 4575
pm
02.28.02 4409
- -- 03.01.02 5919
03.05.02 3571
pm 03.07.02 4430
03.11.02 5298
03.13.02 4,862
"z' 03.19.02 4957
03.22.02 4944
03.26.02 4695
izm 03.28.02 4592
iim Clariant-Elgin S.C. Plant Totals 734,499
Broker: Clariant-Mt. Holly East
„o, Generator
Clariant-Gainesville Plant MHE-2001-0013 01.07.02 5600
01.08.02 5150
,m 01.09.02 5512
01.10.02 5151
01.11.02 5499
01.14.02 5160
01.15.02 5553
01.16.02 5156
01.17.02 5538
CAI
01.18.02 5056
01.21.02 5106
01.22.02 5324
ta4 01.23.02 5117
01.25.02 5123
01.28.02 5205
MP
Final, Page 5 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Clariant - Gainesville Plant Totals
Broker: Clariant - Mt. Holly
Generator Profile No.
Clariant - Coventry Plant
Clariant-Coventry Plant Totals
MHE-2001-0017 02.04.02
02.11.02
05.29.02
Broker: Clariant-Mt. Holly
Generator Profile No.
Seaboard Container Cleaning MHE-2002-0019
Final, Page 6 of 21
8/16/02
01.29.02 5104
01.30.02 5389
01.31.02 5067
02.01.02 4949
02.04.02 4880
02.05.02 5073
02.06.02 5020
02.07.02 5190
02.08.02 5069
02.11.02 5097
02.12.02 5076
02.13.02 5138
02.14.02 5080
02.15.02 5140
02.18.02 5188
02.19.02 5189
02.20.02 5097
02.21.02 5201
02.22.02 4,991
02.26.02 5155
170,593
Date Shipment
Size(gal)
3,951
4,115
3,882
11,948
Date Shipment
Size(gal)
02.21.02 4,450
02.22.02 4,331
02.22.02 4,528
02.23.02 5,597
02.23.02 6,137
02.23.02 4,474
02.25.02 5,856
02.25.02 5,977
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
Am Size(gal)
02.25.02 5,792
02.25.02 5,844
a' 02.25.02 5,600
02.25.02 5,678
02.26.02 6,042
owl 02.26.02 6,025
02.26.02 5,920
02.26.02 5,913
"I 02.27.02 5,973
02.27.02 5,790
02.27.02 5,958
02.27.02 5,917
gm
02.28.02 5,944
02.28.02 5,823
02.28.02 5,911
03.01.02 6,020
03.01.02 5,850
03.01.02 6,006
`M 03.01.02 5,591
03.04.02 6,037
03.04.02 5,638
w" 03.04.02 5,887
03.04.02 5,756
03.05.02 6,064
j0C" 03.05.02 5,901
03.05.02 6,054
03.05.02 5,927
r� 03.06.02 5,958
03.06.02 5,813
03.06.02 5,939
pict 03.06.02 5,901
03.07.02 6,006
03.07.02 5,840
03.07.02 5,949
03.07.02 5,871
03.08.02 5,970
,�, 03.08.02 5,847
03.08.02 5,863
03.11.02 5,966
03.11.02 5,813
ac►
03.11.02 6,008
03.11.02 5,932
03.12.02 5,835
PIP
03.12.02 5,963
03.12.02 5,923
03.12.02 5,802
Final, Page 7 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
Size(gal)
03.13.02 5,961
03.13.02 5,825
03.13.02 5,925
03.13.02 5,875
03.14.02 6,016
03.14.02 5,740
03.14.02 5,980
03.14.02 5,917
03.15.02 5,932
03.15.02 5,797
03.15.02 5,879
03.18.02 5,987
03.18.02 5,761
03.18.02 6,004
03.19.02 5,670
03.19.02 5,804
03.20.02 5,833
03.20.02 5,910
03.21.02 5,716
03.21.02 5,879
03.22.02 5,863
03.22.02 5,735
03.25.02 5,970
03.25.02 5,867
03.25.02 5,927
03.25.02 5,862
03.26.02 6,059
03.26.02 5,908
03.26.02 5,965
03.26.02 5,783
03.27.02 6,020
03.27.02 5,780
03.27.02 5,471
03.27.02 5,778
03.28.02 6,013
03.28.02 5,888
03.28.02 5,795
04.01.02 5,785
04.01.02 5,958
04.02.02 5,752
04.02.02 5,900
04.03.02 5,728
04.08.02 5,761
04.08.02 5,900
04.08.02 5,843
04.09.02 5,864
Final, Page 8 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
1=' Size(gal)
04.15.02 5,984
04.15.02 5,651
at, 04.15.02 5,651
04.16.02 3,734
04.16.02 5,730
04.17.02 5,783
04.17.02 5,824
04.18.02 5,828
04.18.02 5,848
04.19.02 5,816
04.19.02 5,800
Pal
04.20.02 5,726
04.20.02 5,716
04.20.02 5,785
04.20.02 5,982
04.22.02 5,838
- - 04.22.02 5,555
04.22.02 5,819
f=, 04.23.02 5,495
04.23.02 5,924
04.23.02 5,584
�"' 04.23.02 5,696
04.24.02 5,608
04.24.02 5,862
'am 04.24.02 5,809
04.25.02 5,617
04.25.02 5,800
Ma+ 04.25.02 5,540
04.25.02 5,833
04.26.02 5,548
04.26.02 5,852
04.26.02 5,730
04.27.02 5,744
04.27.02 5,800
04.27.02 5,764
04.27.02 5,898
tap04.29.02 5,948
04.29.02 5,749
04.29.02 5,972
fam 04.29.02 5,694
04.30.02 5,944
04.30.02 5,461
04.30.02 6,004
anm
05.01.02 5,994
05.01.02 5,944
05.02.02 5,910
Final, Page 9 of 21
8/16/02
13020s007
Sheet1

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator
Final, Page 10 of 21
8/16/02
Profile No.
05.02.02
05.02.02
05.02.02
05.03.02
05.03.02
05.03.02
05.03.02
05.04.02
05.04.02
05.04.02
05.06.02
05.06.02
05.06.02
05.06.02
05.07.02
05.07.02
05.08.02
05.08.02
05.09.02
05.09.02
05.10.02
05.10.02
05.13.02
05.13.02
05.13.02
05.13.02
05.14.02
05.14.02
05.14.02
05.14.02
05.15.02
05.15.02
05.15.02
05.15.02
05.16.02
05.16.02
05.16.02
05.16.02
05.17.02
05.17.02
05.20.02
05.20.02
05.20.02
05.20.02
05.21.02
05.21.02
Date Shipment
Size(gal)
5,759
5,948
5,783
5,807
5,730
5,917
5,692
5,821
5,824
5,711
5,687
5,716
5,869
5,581
5,845
5,886
5,944
5,740
5,761
5,759
5,680
5,831
5,672
5,629
5,744
5,932
5,980
5,718
5,869
5,852
5,718
5,838
5,682
5,761
5,771
5,680
5,862
5,680
5,747
5,836
5,612
5,927
5,682
5,989
5,879
5,764
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
cladi
Broker: Clariant-Mt. Holly
Generator
Final, Page 11 of 21
8/16/02
Profile No.
05.21.02
05.21.02
05.22.02
05.22.02
05.22.02
05.22.02
05.23.02
05.23.02
05.23.02
05.23.02
05.24.02
05.24.02
05.24.02
05.24.02
05.28.02
05.28.02
05.29.02
05.29.02
05.29.02
05.29.02
05.30.02
05.30.02
05.30.02
05.30.02
05.31.02
05.31.02
05.31.02
05.31.02
06.03.02
06.03.02
06.03.02
06.04.02
06.04.02
06.04.02
06.04.02
06.05.02
06.05.02
06.05.02
06.06.02
06.06.02
06.06.02
06.06.02
06.07.02
06.07.02
06.07.02
06.10.02
Date Shipment
Size(gal)
5,975
5,881
5,857
5,735
5,922
5,636
5,852
5,711
5,872
5,696
5,821
5,706
5,992
5,732
5,872
5,684
3,717
5,692
5,980
5,744
5,912
5,718
5,869
5,735
5,790
5,658
5,948
5,720
5,934
3,832
4,809
5,886
5,804
5,932
5,831
5,864
5,807
6,054
5,891
5,944
6,188
5,860
6,138
5,804
5,912
5,903
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
Size(gal)
06.10.02 5,804
06.11.02 5,788
06.13.02 5,891
06.13.02 5,848
06.14.02 5,807
06.14.02 5,941
06.17.02 5,927
06.17.02 6,076
06.17.02 5,850
06.17.02 5,891
06.18.02 5,936
06.18.02 5,927
06.19.02 5,879
06.19.02 5,836
06.20.02 5,905
06.20.02 5,951
06.21.02 5,696
06.21.02 5,924
06.21.02 5,764
06.21.02 5,816
06.24.02 5,963
06.24.02 5,788
06.24.02 5,922
06.24.02 5,941
06.25.02 5,920
06.25.02 5,807
06.25.02 5,725
06.25.02 5,807
06.26.02 6,011
06.26.02 5,809
06.26.02 5,884
06.26.02 5,790
06.27.02 5,900
06.27.02 5,790
06.27.02 5,912
06.27.02 5,588
06.28.02 5,831
06.28.02 5,692
06.28.02 5,838
07.01.02 5,701
07.01.02 5,785
07.01.02 5,615
07.01.02 5,939
07.02.02 5,615
07.02.02 5,891
07.02.02 5,689
Final, Page 12 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator
Profile No.
Date Shipment
Size(gal)
07.02.02 5,828
07.03.02 5,641
07.03.02 5,910
07.03.02 5,581
07.03.02 5,924
07.05.02 5,493
07.05.02 5,590
07.05.02 5,464
07.08.02 5,588
07.08.02 5,647
07.08.02 5,584
07.08.02 5,915
07.09.02 5,874
07.09.02 5,485
07.09.02 5,728
07.09.02 5,972
07.10.02 5,900
07.10.02 5,893
07.11.02 5,812
07.11.02 5,776
07.12.02 5,927
07.12.02 5,884
07.15.02 5,790
07.15.02 5,783
07.19.02 5,905
07.19.02 5,869
07.22.02 5,912
07.22.02 5,771
Clariant-Seaboard Container Totals 1,805,781
Broker: Four Seasons Environmental
Generator Profile No. Date Shipment
Size(gal)
Wikoff Color MHE-2001-0005 01.10.02 3113
01.23.02 3602
01.31.02 2791
02.19.02 4072
03.01.02 3440
03.12.02 3830
03.22.02 2708
04.04.02 4027
04.16.02 3630
Final, Page 13 of 21
8/16/02
13020s007
Sheetl

AlR
2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
pm Size(gal)
04.30.02 3614
05.06.02 2872
Ina 05.06.02 2155
05.15.02 3808
05.28.02 4873
p, 06.11.02 3574
06.24.02 3991
07.03.02 3390
pm07.15.02 4963
07.23.02 4129
too
Broker: Four Seasons Environmental
"m, Generator Profile No. Date Shipment
Size(gal)
Firestone Fibers & Textiles MHE-2002-0018 02.07.02 3950
*a 02.20.02 4514
_ 02.22.02 3823
03.07.02 5364
''°' 03.13.02 3298
03.20.02 3011
03.25.02 1,769
"" 03.26.02 3,877
_ 04.12.02 3,653
04.29.02 4,996
rosi 05.02.02 5,629
05.21.02 3,186
05.30.02 4,785
MN 06.10.02 4,401
06.19.02 3,611
06.21.02 3,877
_. 06.24.02 4,259
06.25.02 4,505
07.01.02 3,942
„p 07.03.02 2,272
07.05.02 3,804
07.05.02 2,127
07.05.02 3,768
07.08.02 2,009
07.10.02 4,321
07.16.02 4,185
cm
07.22.02 4,479
07.23.02 4,613
Final, Page 14 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
'" Size(gal)
fie
Broker: Four Seasons Environmental
Generator Profile No. Date Shipment
mi Size(gal)
Plastech MHE-2002-0061 07.01.02 3762
07.01.02 1985
,m 07.05.02 3746
Broker: Four Seasons Environmental
- Generator Profile No. Date Shipment
Size (gal)
Cardell Fabrics MHE-2002-0062 07.18.02 3273
w.
Broker: Haz-Mat
Generator Profile No. Date Shipment
'a Size(gal)
AEA Technology Engr. Serv. MHE-2001-0015 06.10.02 4,337
07.17.02 2,636
1214
fie
enl
Op
IZO
fali
Pe
AEA Technology Engr. Serv. Totals 6973
Broker: Haz-Mat
NICCA USA
Broker: Haz-Mat
Final, Page 15 of 21
8/16/02
MHE-2002-0007 01.30.02 5233
01.30.02 3754
02.01.02 3059
02.01.02 4259
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
im Size(gal)
Boral Materials Technologies MHE-2002-0010 02.01.02 2706
02.19.02 2999
02.25.02 3095
Broker: Haz-Mat
am Allied Die Casting MHE-2002-0015 02.01.02 3007
02.15.02 3301
02.28.02 2464
0. 02.28.02 3431
PM
04.12.02 3373
04.12.02 1986
07.11.02 4811
Broker: Haz-Mat
Eagle Mountain Finishing MHE-2002-0051 05.03.02 7220
05.15.02 3086
Broker: Haz-Mat
Haz-Mat MHE-2002-0056 05.29.02 3103
05.30.02 2898
"" 05.30.02 1359
06.13.02 3203
06.13.02 3501
114 06.14.02 3208
06.21.02 3028
06.26.02 2771
06.28.02 3434
07.01.02 3311
07.02.02 3153
Broker: Phillips Services
_ Generator Profile No.
Stockhausen - Greensboro MHE-2001-0027 12.31.01 4226
- 01.07.02 1424
PM
INI
Final, Page 16 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
AMR
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
Size(gal)
Stockhausen - Greensboro Totals 5,650
Broker: CTW Specialties
Generator Profile No.
Piedmont Chemicals MHE-2001-0019 01.07.02 2676
01.22.02 2808
01.28.02 2871
02.05.02 2841
02.14.02 1688
04.12.02 3260
06.19.02 3990
06.24.02 3470
Broker: CTW Specialties
Generator Profile No.
Piedmont Chemicals MHE-2002-0025 04.05.02 929
Broker: CTW Specialties
Generator Profile No.
Rotometrics MHE-2002-0002 02.13.02 2777
Broker: CTW Specialties
Generator Profile No.
Finetex, Inc. MHE-2001-0028 02.05.02 3104
02.08.02 1092
02.27.02 3903
Final, Page 17 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
"" Size(gal)
a► FineTex Totals
Broker: CTW Specialities
FM Generator Profile No. Date Shipment
Valspar Corporation MHE-2002-0037 Size(gal)
04.04.02 3772
rx► 05.02.02 5496
06.04.02 5178
06.10.02 5371
ai, 06.18.02 5187
Rug
06.26.02 5370
07.08.02 4561
07.12.02 5311
Broker: Resource Management
Generator Profile No.
"'� CommScope-Catawba MHE-2001-0034 12.31.01 4714
12.31.01 4235
12.31.01 4860
M" 12.31.01 5100
12.31.01 4446
12.31.01 5402
"" 01.02.02 1642
mri CommScope-Catawba Totals 23355
Broker: A&D Environmental
rw, Generator Profile No.
DEB SBS, Inc. MHE-2001-0025 02.12.02 4452
DEB SBS, Inc. Totals 4452
Broker: A&D Environmental
cm
Generator Profile No.
KAO Specialties Americas MHE-2002-0023 03.27.02 4950
04.19.02 4400
wa
Final, Page 18 of 21
8/16/02
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
m"" Size(gal)
04.12.02 4400
04.26.02 4393
oft 05.07.02 550
rairl
Broker: A&D Environmental Date Shipment
Generator Profile No. Size(gal)
KAO Specialties Americas MHE-2002-0045 04.26.02 3939
MA
ow
Broker: A&D Environmental
Mal Generator Profile No. Date Shipment
KAO Specialties Americas MHE-2002-0050 Size(gal)
05.07.02 1454
eilltl
WI
Broker: Clariant-Mt. Holly
rm., Generator Profile No. Date Shipment
Size(gal)
SPECIALTY POLYMERS, INC. MHE-2002-0021 02.28.02 5435
rAr, 03.15.02 5265
pm
04.30.02 5671
05.01.02 5898
05.01.02 5565
05.01.02 5709
05.01.02 5806
05.20.02 5561
rim 05.29.02 5376
05.29.02 5704
05.29.02 5319
mia
Final, Page 19 of 21
8/16/02
03.26.02 5580
04.04.02 5617
04.05.02 5640
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
"' Size(gal)
05.29.02 5255
05.30.02 5427
05.30.02 5711
06.04.02 4972
06.06.02 5402
MI 06.07.02 4411
raI
06.25.02 5438
07.11.02 5603
07.16.02 5614
07.16.02 5617
Broker: Clariant-Mt. Holly
FM
Generator Profile No. Date Shipment
Size(gal)
Piedmont Portable Toilets MHE-2002-0026 02.08.02 413
02.15.02 374
fam
02.22.02 418
03.08.02 396
03.15.02 382
mi 03.28.02 408
04.05.02 394
04.12.02 401
04.22.02 403
05.02.02 391
05.09.02 365
MEI 05.16.02 245
Broker: Clariant-Mt. Holly
Generator
Final, Page 20 of 21
8/16/02
05.17.02 283
05.17.02 341
05.23.02 391
05.31.02 394
06.05.02 324
06.07.02 1581
06.14.02 355
06.17.02 919
06.21.02 322
06.28.02 336
07.05.02 338
07.10.02 358
07.18.02 367
Profile No. Date Shipment
13020s007
Sheetl

2002 3rd Party OCPSF Wastewater Received: Business Volumes by Broker
Broker: Clariant-Mt. Holly
Generator Profile No. Date Shipment
Size(gal)
Size (gal)
Mt. Holly Plant -West MHE-2002-0040 04.11.02 2517
Broker: Clariant-Mt. Holly Profile No. Date Shipment
Generator Size (gal)
Cocoa -Cola Bottling Co. MHE-2002-0043 04.24.02 4863
04.26.02 4881
Broker: Solution IES Profile No. Date Shipment
pm Generator Size (gal)
Sun Chemical MHE-2002-0036 05.24.02 2575
07.09.02 3690
Broker: Prism Group Profile No. Date Shipment
Generator Size (gal)
Harrell Industries MHE-2002-0057 06.13.02 2628
Final, Page 21 of 21
8/16/02
13020s007
Sheetl

..-
APPENDIX F
SECTION 14.8.3.3.1
USEPA DEVELOPMENT DOCUMENT FOR
THE CWT POINT SOURCE CATEGORY

Chanter 14 lm • lementation Develo • ment Document or the CWT Point Source Cate • ory
Exceptions to Guidance Provided for
CWT Facilities Also Covered By
Another Point Source Category 14.8.3.3
The only exceptions to the guidance
provided in sections 14.8.4.1 and 14.8.4.2 are
for facilities also subject to effluent guidelines
and preatreatment standards for Transportation
Equipment Cleaning (40 CFR 442) and effluent
guidelines for Landfills (40 CFR 445). The
application of the CWT rule to each of these
types of facilities is discussed below.
TRANSPORTATION EQUIPMENT
CLEANING (TEC) 14.8.3.3.1
There are some facilities which are engaged
in both traditional CWT activities and traditional
TEC activities. If the wastewaters from the two
operations are commingled, under the approach
adopted for TEC, the commingled wastewater
flow from the transportation equipment cleaning
activities would be subject to CWT limits.
Therefore, a facility performing transportation
equipment cleaning as well as other CWT
services that commingles these wastes is a CWT
facility and all of the wastewater discharges are
subject to provisions of this rule. If, however, a
facility is performing both operations and the
waste streams are not commingled (that is,
transportation equipment cleaning process
wastewater is treated in one system and CWT
wastes are treated in a second, separate system),
both the TEC rule and CWT rule apply to the
respective wastewaters. If, however, the
wastewaters from the two separate treatment
systems are combined after treatment but prior
to discharge monitoring, discharge requirements
would be calculated by applying the "building
block approach" or the "combined waste stream
formula" as detailed in Sections 14.8.4.1 and
14.8.4.2.
14-28
LANDFILLS
14.8.3.3.2
In the CWT industry, there are some
facilities which are engaged both in CWT
activities and in operating landfills. For the CWT
final rule, EPA's approach to facilities which
treat mixtures of CWT wastewater and landfill
wastewater is consistent with that established for
the . landfill guideline. Therefore, a facility
performing landfill activities, as well as other
CWT services, and commingles the wastewater
is a CWT facility only, and all of the wastewater
discharges are subject to the provisions of this
rule. If a facility is performing both operations
and the waste streams are not commingled (that
is, landfill wastewater is treated in one treatment
system and CWT wastewater is treated in a
second, separate treatment system), the
provisions of the Landfill rule and CWT rule
apply to its respective wastewaters. If, however,
the wastewaters from the two separate treatment
systems are combined after treatment, but prior
to discharge monitoring, discharge requirements
would be calculated by applying the "building
block approach" or the "combined waste stream
formula" as detailed in Sections 14.8.4.1 and
14.8.4.2.

APPENDIX G
STATISTICAL ANALYSIS OF EFFLUENT NH3-N

Final, 8/16/02
Page 1 of 6
Statistical Analysis of Effluent Ammonia -Nitrogen
Daily Effluent Ammonia (June 2001 - May 2002)
Clariant Corporation - Mt. Holly
i Prob % Prob NH3 (lb/day)
1 0.004 0.4 0 Prob = i / (n+1)
2 0.008 0.8 1 % Prob = Prob * 100
3 0.012 1.2 1 n=252
4 0.016 1.6 1
5 0.020 2.0 1
6 0.024 2.4 2
7 0.028 2.8 2
8 0.032 3.2 2
9 0.036 3.6 2
10 0.040 4.0 2
11 0.043 4.3 2
12 0.047 4.7 2
13 0.051 5.1 2
14 0.055 5.5 3
15 0.059 5.9 3
16 0.063 6.3 3
17 0.067 6.7 3
18 0.071 7.1 3
19 0.075 7.5 3
20 0.079 7.9 3
21 0.083 8.3 3
22 0.087 8.7 3
23 0.091 9.1 3
24 0.095 9.5 4
25 0.099 9.9 4
26 0.103 10.3 4
27 0.107 10.7 4
28 0.111 11.1 4
29 0.115 11.5 4
30 0.119 11.9 5
31 0.123 12.3 5
32 0.126 12.6 5
33 0.130 13.0 5
34 0.134 13.4 5
35 0.138 13.8 5
36 0.142 14.2 5
37 0.146 14.6 6
38 0.150 15.0 6
39 0.154 15.4 6
40 0.158 15.8 6
41 0.162 16.2 7
42 0.166 16.6 7
43 0.170 17.0 7
44 0.174 17.4 7
13020s008
Daily Ammonia Data

Statistical Analysis of Effluent Ammonia -Nitrogen
Daily Effluent Ammonia (June 2001 - May 2002)
Clariant Corporation - Mt. Holly
i Prob % Prob NH3 (Ib/day)
45 0.178 17.8 8
46 0.182 18.2 8
47 0.186 18.6 8
48 0.190 19.0 8
49 0.194 19.4 9
50 0.198 19.8 9
51 0.202 20.2 10
52 0.206 20.6 10
53 0.209 20.9 10
54 0.213 21.3 10
55 0.217 21.7 12
56 0.221 22.1 13
57 0.225 22.5 13
58 0.229 22.9 14
59 0.233 23.3 14
60 0.237 23.7 14
61 0.241 24.1 15
62 0.245 24.5 18
63 0.249 24.9 20
64 0.253 25.3 25
65 0.257 25.7 26
66 0.261 26.1 27
67 0.265 26.5 28
68 0.269 26.9 28
69 0.273 27.3 28
70 0.277 27.7 31
71 0.281 28.1 32
72 0.285 28.5 34
73 0.289 28.9 39
74 0.292 29.2 43
75 0.296 29.6 45
76 0.300 30.0 47
77 0.304 30.4 48
78 0.308 30.8 48
79 0.312 31.2 49
80 0.316 31.6 51
81 0.320 32.0 51
82 0.324 32.4 52
83 0.328 32.8 56
84 0.332 33.2 57
85 0.336 33.6 58
86 0.340 34.0 59
87 0.344 34.4 60
88 0.348 34.8 61
Final, 8/16/02
Page 2 of 6
13020s008
Daily Ammonia Data

MI
Statistical Analysis of Effluent Ammonia -Nitrogen
Daily Effluent Ammonia (June 2001 - May 2002)
Clariant Corporation - Mt. Holly
i Prob % Prob NH3 (lb/clay)
FM 89 0.352 35.2 62
90 0.356 35.6 64
91 0.360 36.0 64
_, 92 0.364 36.4 70
93 0.368 36.8 76
94 0.372 37.2 80
95 0.375 37.5 81
96 0.379 37.9 86
97 0.383 38.3 87
98 0.387 38.7 88
044
99 0.391 39.1 92
100 0.395 39.5 98
101 0.399 39.9 105
lami
102 0.403 40.3 105
103 0.407 40.7 105
104 0.411 41.1 107
0." 105 0.415 41.5 109
106 0.419 41.9 112
107 0.423 42.3 117
am 108 0.427 42.7 117
109 0.431 43.1 121
110 0.435 43.5 126
wo 111 0.439 43.9 129
112 0.443 44.3 134
113 0.447 44.7 136
ow 114 0.451 45.1 137
115 0.455 45.5 140
116 0.458 45.8 147
am 117 0.462 46.2 150
118 0.466 46.6 156
119 0.470 47.0 157
ow120 0.474 47.4 163
121 0.478 47.8 167
122 0.482 48.2 167
123 0.486 48.6 170
wo
124 0.490 49.0 178
125 0.494 49.4 190
126 0.498 49.8 191
awl
127 0.502 50.2 195
128 0.506 50.6 195
129 0.510 51.0 197
`o` 130 0.514 51.4 199
131 0.518 51.8 206
132 0.522 52.2 208
rami
Final, 8/16/02
Page 3 of 6
13020s008
Daily Ammonia Data

FIR
Statistical Analysis of Effluent Ammonia -Nitrogen
Daily Effluent Ammonia (June 2001 - May 2002)
Clariant Corporation - Mt. Holly
1 Prob % Prob NH3 (Ib/day)
AM 133 0.526 52.6 212
134 0.530 53.0 214
135 0.534 53.4 219
136 0.538 53.8 232
137 0.542 54.2 242
138 0.545 54.5 249
mil139 0.549 54.9 250
140 0.553 55.3 258
141 0.557 55.7 258
142 0.561 56.1 264
ant
143 0.565 56.5 276
144 0.569 56.9 284
145 0.573 57.3 284
Fs, 146 0.577 57.7 285
147 0.581 58.1 285
148 0.585 58.5 298
"a 149 0.589 58.9 300
150 0.593 59.3 302
151 0.597 59.7 302
°" 152 0.601 60.1 304
153 0.605 60.5 316
154 0.609 60.9 325
agg 155 0.613 61.3 325
156 0.617 61.7 326
157 0.621 62.1 333
OM 158 0.625 62.5 336
159 0.628 62.8 338
160 0.632 63.2 347
,M 161 0.636 63.6 349
162 0.640 64.0 368
163 0.644 64.4 371
„n% 164 0.648 64.8 392
165 0.652 65.2 392
166 0.656 65.6 393
ma167 0.660 66.0 393
168 0.664 66.4 400
169 0.668 66.8 401
170 0.672 67.2 401
cot
171 0.676 67.6 402
172 0.680 68.0 405
173 0.684 68.4 412
FRI
174 0.688 68.8 413
175 0.692 69.2 430
176 0.696 69.6 441
sal
Final, 8/16/02
Page 4 of 6
13020s008
Daily Ammonia Data

PM
Statistical Analysis of Effluent Ammonia -Nitrogen
Daily Effluent Ammonia (June 2001 - May 2002)
Clariant Corporation - Mt. Holly
! Prob % Prob NH3 (lb/clay)
00 177 0.700 70.0 459
178 0.704 70.4 459
179 0.708 70.8 460
am 180 0.711 71.1 461
181 0.715 71.5 463
182 0.719 71.9 469
„i, 183 0.723 72.3 477
184 0.727 72.7 487
185 0.731 73.1 489
186 0.735 73.5 495
187 0.739 73.9 496
188 0.743 74.3 498
189 0.747 74.7 499
tall
190 0.751 75.1 501
191 0.755 75.5 504
192 0.759 75.9 506
a"°' 193 0.763 76.3 515
194 0.767 76.7 515
195 0.771 77.1 533
"i' 196 0.775 77.5 542
197 0.779 77.9 543
198 0.783 78.3 564
199 0.787 78.7 573
200 0.791 79.1 574
201 0.794 79.4 574
m+ 202 0.798 79.8 576
203 0.802 80.2 577
204 0.806 80.6 580
Sall 205 0.810 81.0 585
206 0.814 81.4 586
207 0.818 81.8 588
,� 208 0.822 82.2 588
209 0.826 82.6 589
210 0.830 83.0 589
rap211 0.834 83.4 589
212 0.838 83.8 591
213 0.842 84.2 592
214 0.846 84.6 592
aigR
215 0.850 85.0 593
216 0.854 85.4 593
217 0.858 85.8 593
218 0.862 86.2 595
219 0.866 86.6 596
220 0.870 87.0 596
gml
Final, 8/16/02
Page 5 of 6
13020s008
Daily Ammonia Data

Statistical Analysis of Effluent Ammonia -Nitrogen
Daily Effluent Ammonia (June 2001 - May 2002)
Clariant Corporation - Mt. Holly
01114
nal
Final, 8/16/02
Page 6 of 6
i Prob % Prob NH3 (Ib/day)
221 0.874 87.4 596
222 0.877 87.7 599
223 0.881 88.1 600
224 0.885 88.5 601
225 0.889 88.9 603
226 0.893 89.3 603
227 0.897 89.7 604
228 0.901 90.1 605
229 0.905 90.5 606
230 0.909 90.9 608
231 0.913 91.3 609
232 0.917 91.7 610
233 0.921 92.1 610
234 0.925 92.5 611
235 0.929 92.9 612
236 0.933 93.3 613
237 0.937 93.7 613
238 0.941 94.1 616
239 0.945 94.5 616
240 0.949 94.9 618
241 0.953 95.3 618
242 0.957 95.7 620
243 0.960 96.0 623
244 0.964 96.4 623
245 0.968 96.8 624
246 0.972 97.2 625
247 0.976 97.6 625
248 0.980 98.0 650
249 0.984 98.4 651
250 0.988 98.8 715
251 0.992 99.2 717
252 0.996 99.6 823
13020s008
Daily Ammonia Data

APPENDIX H
DATA SUMMARY OF PROPOSED NON -CONVENTIONAL PARAMETERS

+ 1 I B I. 1 1+ I i 1 I I I I I I
TIER 1 LIMITS
OCPSF CURRENT AND PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Average Daily Flow (MGD) = 0.590
Effluent Characteristic
WQL
OCPSF Limits
Current Limits
Current Limits -
Calculated Flow
Proposed Limits
@ 0.590 MGD
% Limit
Reduction
Histor-
ical
Max Allowable
Effluent from
Conc.
Proposed
Month
Avg.
Conc. @
1.5 MGD
(ug/L)
9
in Final
Limits
Month
Avg.
Conc. @
1.0 MGD
(ug/L)
13
Month
Avg.
(ug/L)
Max
Day
(ug/L)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Flow
(MGD)
Max
Day
Flow
(MGD)
Month
Avg.
(Ib/d)
Max
Day
(lb/d)
Month
Avg.
Limit
Max
Day
Limit
Max
Conc.
(ug/L)(1)
<51
Month
Avg.
Conc. @
2.0 MGD
(ug/L)
6
Acenaphthene
*
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72%
0%
Acenaphthylene
*
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72%
0%
<51
6
9
13
Acrylonitrile
96
242
1.69
4.30
2.11
2.13
0.47
1.19
72%
72%
<100
28
38
57
Anthracene
*
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72%
0%
<51
6
9
13
Benzene
37
136
0.75
2.70
2.43
2.38
0.18
0.67
76%
75%
<5
11
15
22
Benzo(a)anthracene
*
22
59
0.31
0.50
1.69
1.02
0:11
0.50
65%
0%
<51
6
9
13
3,4-Benzofluoranthene
*
23
61
0.40
0.50
2.09
0.98
0.11
0.50
72%
0%
<51
7
9
14
Benzo(k)fluoranthene
*
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72°i°
0%
<51
6
9
13
Benzo(a)pyrene
*
23
61
0.40
0.50
2.09
0.98
0.11
0.50
72%
0%
<51
7
9
14
Bis(2-ethylhexyl) phthalate
103
279
1.81
4.91
2.11
2.11
0.51
1.37
72%
72%
<51
30
41
61
Carbon Tetrachloride
18
38
0.32
0.67
2.13
2.11
0.09
0.19
72%
72%
<5
5
7
_
11
Chlorobenzene (2)
15
28
0.31
0.57
2.48
2.44
0.07
0.14
76%
76%
12
4
6
9
Chloroethane
104
268
1.83
4.72
2.11
2.11
0.51
1.32
72%
72%
<5
31
41
61
Chloroform
21
46
0.37
0.81
2.11
2.11
0.10
0.23
72%
72%
<5
6
8
12
2-Chlorophenol
31
98
0.62
1.95
2.40
2.39
0.15
0.48
_
75%
75%
<51
9
12
18
Chrysene
*
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72%
0%
<51
6
9
13
Di-n-butyl phthalate
27
57
0.48
1.00
2.13
2.10
0.13
0.28
72%
72%
<51
8
11
16
1,2-Dichlorobenzene
77
163
1.57
3.32
2.44
2.44
0.38
0.80
76%
76%
<5
23
30
45
1,3-Dichlorobenzene
31
44
0.62
0.90
2.40
2.45
0.15
0.22
75%
76%
<5
9
12
18
1,4-Dichlorobenzene
15
28
0.31
0.57
2.48
2.44
0.07
0.14
76%
76%
7.4
4
6
9
1,1-Dichloroethane
22
59
0.39
1.04
2.13
2.11
0.11
0.29
72%
72%
<5
6
9
13
1,2-Dichloroethane
68
211
1.20
3.71
2.12
2.11
0.33
1.04
72%
72%
<5
20
27
40
1,1-Dichloroethylene
16
25
0.28
0.44
2.10
2.11
0.08
0.12
72%
72%
<5
5
6
9
1,2-trans-Dichloroethylene
21
54
0.37
0.95
2.11
2.11
0.10
0.27
72%
72%
<5
6
8
12
2,4-Dichlorophenol
39
112
0.77
2.22
2.37
2.38
0.19
0.55
75%
75%
<51
12
15
23
1,2-Dichloropropane
153
230
2.69
4.05
2.11
2.11
0.75
1.13
72%
72%
<5
45
60
90
1,3-Dichloropropylene
29
44
0.51
0.77
2.11
2.10
0.14
0.22
72%
72%
<10
9
11
17
Diethyl phthalate
81
203
1.43
3.57
2.12
2.11
0.40
1.00
72%
72%
<51
24
32
48
Final, Page 1 of 3
8/16/02
13020s002
OCPSF-Tier 1

j 1 1 1 1 1 1 1 1 1 1 11 1 ➢
TIER 1 LIMITS
OCPSF CURRENT AND PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Average Daily Flow (MGD) = 0.590
Effluent Characteristic
WQL
OCPSF Limits
Current Limits
Current Limits -
Calculated Flow
Proposed Limits
@ 0.590 MGD
% Limit
Reduction
Histor-
ical
Max Allowable
Effluent from
Conc.
Proposed
Month
Avg.
Conc. @
1.5 MGD
(ug/L)
7
in Final
Limits
Month
Avg.
Conc. @
1.0 MGD
(ug/L)
11
Month
Avg.
(ug/L)
Max
Day
(ug/L)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Flow
(MGD)
Max
Day
Flow
(MGD)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Limit
Max
Day
Limit
Max
Conc.
(ug/L)t1
<51
Month
Avg.
Conc. @
2.0 MGD
(ug/L)
5
2,4-Dimethylphenol
18
36
0.36
0.71
2.40
2.36
0.09
0.18
75%
75%
Dimethyl phthalate
19
47
0.33
0.83
2.08
2.12
0.09
0.23
72%
72%
<51
6
7
_
11
4,6-Dinitro-o-cresol
78
277
1.55
5.50
2.38
2.38
0.38
1.36
75%
75%
<260
23
31
46
2,4-Dinitrophenol
71
123
2.15
3.71
3.63
3.62
0.35
0.61
84%
84%
<260
21
28
42
2,4-Dinitrotoluene
113
285
1.99
5.03
2.11
2.12
0.56
1.40
72%
72%
<51
33
44
67
2,6-Dinitrotoluene
255
641
4.40
11.28
2.07
2.11
1.25
3.15
71%
72%
<51
_
75
100
150
Ethylbenzene
32
108
0.65
2.20
2.44
2.44
0.16
0.53
76%
76%
<5
9
13
19
Fluoranthene
25
68
0.47
1.20
2.25
2.12
0.12
0.33
74%
72%
<51
7
10
15
Fluorene
* _
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72%
0%
<51
6
9
13
Hexachlorobenzene
15
28
0.26
0.49
2.08
2.10
0.07
0.14
72%
72%
<51
4
6
9 -
Hexachlorobutadiene
20
49
0.35
0.86
2.10
2.10
0.10
0.24
72%
72%
<51
6
8
12
Hexachloroethane
21
54
0.39
0.95
2.23
2.11
0.10
0.27
74%
72%
<51
6
8
12
Methyl Chloride
86
190
1.51
3.34
2.11
2.11
0.42
0.93
72%
72%
<5
25
34
51
Methylene Chloride
40
89
0.70
1.57
2.10
2.12
0.20
0.44
72%
72%
<5
12
16
24
Naphthalene
*
22
59
0.45
0.50
2.45
1.02
0.11
0.50
76%
0%
<51
6
9
13
Nitrobenzene
27
68
0.48
1.20
2.13
2.12
0.13
0.33
72%
72%
<51
8
11
16
2-Nitrophenol
41
69
1.23
2.08
3.60
3.61
0.20
0.34
84%
84%
<51
12
16
24
4-Nitrophenol
72
124
2.17
3.74
3.61
3.62
0.35
0.61
84%
84%
<260
21
28
42
Phenanthrene
*
22
59
0.39
0.50
2.13
1.02
0.11
0.50
72%
0%
<51
6
9
13
Phenol (3)
15
26
1.56
2.70
12.47
12.45
0.07
0.13
95%
95%
<51
4
6
9
Pyrene
*
25
67
0.44
0.50
2.11
0.89
0.12
0.50
72%
0%
<51
7
10
15
Tetrachloroethylene
22
56
0.39
0.99
2.13
2.12
0.11
0.28
72%
72%
<5
6
9
13
Toluene
26
80
0.53
1.63
2.44
2.44
0.13
0.39
76%
76%
8.1
8
10
15
Total Chromium
1110
2770
-
-
-
-
5.46
13.63
-
-
-
327
437
655
Total Copper
1450
3380
-
-
-
-
7.13
16.63
-
-
-
428
570
856
Total Cyanide
420
1200
7.39
9.01
2.11
0.90
2.07
2.52
72%
72%
9
124
165
248
Total Lead
320
690
-
-
-
-
1.57
3.40.
-
-
-
94
126
189
Total Nickel
1690 _
3980
-
-
-
-
8.32
19.58
-
-
-
499
665
_
997
Final, Page 2 of 3
8/16/02
13020s002
OCPSF-Tier 1

1 1 1 1 1 1 1 1 1 1 1+ 1 1 1 1 1 1 1
TIER 1 LIMITS
OCPSF CURRENT AND PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Average Daily Flow (MGD) = 0.590
Effluent Characteristic
WQL
OCPSF Limits
Current Limits
Current Limits -
Calculated Flow
Proposed Limits
@ 0.590 MGD
% Limit
Reduction
Histor-
ical
Max Allowable
Effluent from
Conc.
Proposed
Month
Avg.
Conc. @
1.5 MGD
(ug/L)
413
in Final
Limits
Month
Avg.
Conc. @
1.0 MGD
(ug/L)
620
Month
Avg.
(ug/L)
Max
Day
(ug/L)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Flow
(MGD)
Max
Day
Flow
(MGD)
Month
Avg.
(lb/d)
Max
Day
(lb/d)
Month
Avg.
Limit
Max
Day
Limit
Max
Conc.
(ug/L)(1)
-
Month
Avg.
Conc. @
2.0 MGD
(ug/L)
310
Total Zinc
1050
2610
-
-
-
-
5.17
12.84
-
-
1,2,4-Trichlorobenzene
68
140
1.20
2.46
2.12
2.11
0.33
0.69
72%
72%
<51
20
27
40
1,1,1-Trichloroethane
21
54
0.37
0.95
2.11
2.11
0.10
0.27
72%
72%
<5
6
8
12
1,1,1-Trichloroethane(repeat)
21
54
0.37
0.95
2.11
2.11
0.10
0.27
72%
72%
<5
6
8
12
Trichloroethylene
21
54
0.37
0.95
2.11
2.11
0.10
0.27
72%
72%
<5
6
8
12
Vinyl Chloride
104
268
1.82
4.70
2.10
2.10
0.51
1.32
72%
72%
<5
31
41
61
* These parameters are water quality Iimited.(WQL). Used current max day limit for proposed max day limit.
(1) Max detection limit observed in sampling from Jan 2001 - Jun 2002.
(2) Historical chlorobenzene results (2001 - 2002): 9.4, <5, <5, 12, <5, <5.
(3) Basis for proposed phenol limit inconsistent with current phenol limit. Current phenol limit much higher than proposed. Basis for limit should be evaluated.
Final, Page 3 of 3
8/16/02
13020s002
OCPSF-Tier 1

1 1 1 1 1 1 1 1 1 1 1 I 1 1 1 1 1 1 1
TIER 2 LIMITS
OCPSF CURRENT AND PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Average Daily Flow (MGD) = 0.690
Effluent Characteristic
-1
OCPSF Limits
Current Limits
Current Limits -
Calculated Flow
Proposed Limits
@ 0.690 MGD
% Limit
Reduction
Histor-
ical
Max Allowable
Effluent from
Conc.
Proposed
Month
Avg.
Conc. @
1.5 MGD
(ug/L)
10
in Final
Limits
Month
Avg.
Conc.
1.0 MGD
(ug/L)
15
Month
Avg.
(ug/L)
Max
Day
(ug/L)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Flow
JMGD)
Max
Day
Flow
(MGD)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Limit
Max
Day
Limit
Max
Conc.
(ug/L)(1)
<51
Month
Avg.
Conc. @
2.0 MGD
(ug/L)
8
Acenaphthene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
Acenaphthylene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
<51
8
10
15
Acrylonitrile
96
242
1.69
4.30
2.11
2.13
0.55
1.39
67%
68%
<100
33
44
66
Anthracene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
<51
8
10
15
Benzene
37
136
0.75
2.70
2.43
2.38
0.21
0.78
72%
71%
<5
13
17
26
Benzo(a)anthracene
*
22
59
0.31
0.50
1.69
1.02
0.13
0.50
59%
0%
<51
8
10
15
3,4-Benzofluoranthene
*
23
61
0.40
0.50
2.09
0.98
0.13
0.50
67%
0%
<51
8
11
16
Benzo(k)fluoranthene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
<51
8
10
15
Benzo(a)pyrene
*
23
61
0.40
0.50
2.09
0.98
0.13
0.50
67%
0%
<51
8
11
16
Bis(2-ethylhexyl) phthalate
103
279
1.81
4.91
2.11
2.11
0.59
1.61
67%
67%
<51
36
47
71
Carbon Tetrachloride
18
38
0.32
0.67
2.13
2.11
0.10
0.22
68%
67%
<5
6
8
12
Chlorobenzene (2)
15
28
0.31
0.57
2.48
2.44
0.09
0.16
72%
72%
12
5
7
10
Chloroethane
104
268
1.83
4.72
2.11
2.11
0.60
1.54
67%
67%
<5
36
48
72
Chloroform
21
46
0.37
0.81
2.11
2.11
_
0.12
0.26
67%
67%
<5
7
10
14
2-Chlorophenol
31
98
0.62
1.95
2.40
2.39
0.18
0.56
71%
71%
<51
11
14
21
Chrysene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
<51
8
10
15
Di-n-butyl phthalate
27
57
0.48
1.00
2.13
2.10
0.16
0.33
68%
67%
<51
9
12
19
1,2-Dichlorobenzene
77
163
1.57
3.32
2.44
2.44
0.44
0.94
72%
72%
<5
27
35
53
1,3-Dichlorobenzene
31
44
0.62
0.90
2.40
2.45
0.18
0.25
71%
72%
<5
11
14
21 .
1,4-Dichlorobenzene
15
28
0.31
0.57
2.48
2.44
0.09
0.16
72%
72%
7.4
5
7
10
1,1-Dichloroethane
22
59
0.39
1.04
2.13
2.11
0.13
0.34
68%
67%
<5
8
10
15
1,2-Dichloroethane
68
211
1.20
3.71
2.12
2.11
0.39
1.21
67%
67%
<5
23
31
47
1,1-Dichloroethylene
16
25
0.28
0.44
2.10
2.11
0.09
0.14
67%
67%
_
<5
6
7
11
1,2-trans-Dichloroethylene
21
54
0.37
0.95
2.11
2.11
0.12
0.31
67%
67%
<5
7
10
14
2,4-Dichlorophenol
39
112
0.77
2.22
2.37
2.38
0.22
0.64
71%
71%
<51
13
18
27 _
1,2-Dichloropropane
153
230
2.69
4.05
2.11
2.11
0.88
1.32
67%
67%
<5
53
70
106
1,3-Dichloropropylene
29
44
0.51
0.77
2.11
2.10
0.17
0.25
67%
67%
<10
10
13
20
Diethyl phthalate
81
203
1.43
3.57
2.12
2.11
_ 0.47
1.17
67%
67%
<51
28
37
56
Final, Page 1 of 3
8/16/02
13020s002
OCPSF-Tier 2

1 1 1 i 1 1 1 1 1 1 1
TIER 2 LIMITS
OCPSF CURRENT AND PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Average Daily Flow (MGD) = 0.690
Effluent Characteristic
WQL
OCPSF Limits
Current Limits
Current Limits -
Calculated Flow
Proposed Limits
@ 0.690 MGD
% Limit
Reduction
Histor-
ical
Max Allowable
Effluent from
Conc.
Proposed
Month
Avg.
Conc. @
1.5 MGD
(ug/L)
8
in Final
Limits
Month
Avg.
Conc. @
1.0 MGD
(ug/L)
12
Month
Avg.
_ (ug/L)
Max
Day
(ug/L)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Flow
(MGD)
Max
Day
Flow
(MGD)
Month
Avg.
(Ib/d)
Max
Day
(Ib/d)
Month
Avg.
Limit
Max
Day
Limit
Max
Conc.
(ug/L)(1)
<51
Month
Avg.
Conc. @
2.0 MGD
(ug/L)
6
2,4-Dimethylphenol
18
36
0.36
0.71
2.40
2.36
0.10
0.21
71%
71%
Dimethyl phthalate
19
47
0.33
0.83
2.08
2.12
0.11
0.27
67%
67%
<51
7
9
13
4,6-Dinitro-o-cresol
78
277
1.55
5.50
2.38
2.38
0.45
1.59
71%
71%
<260
27
36
54
2,4-Dinitrophenol
71
123
2.15
3.71
3.63
3.62
0.41
0.71
81%
81%
<260
24
33
49
2,4-Dinitrotoluene
113
285
1.99
5.03
2.11
2.12
0.65
1.64
67%
67%
<51
39
52
78
2,6-Dinitrotoluene
255
641
4.40
11.28
2.07
2.11
1.47
3.69
67%
67%
<51
88
117
176
Ethylbenzene
32
108
0.65
2.20
2.44
2.44
0.18
0.62
72%
72%
<5
11
15
22
Fluoranthene
25
68
0.47
1.20
2.25
2.12
0.14
0.39
69%
67%
<51
9
12
17
Fluorene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
<51
8
10
15
Hexachlorobenzene
15
28
0.26
0.49
2.08
2.10
0.09
0.16
67%
67%
<51
5
7
10
Hexachlorobutadiene
20
49
0.35
0.86
2.10
2.10
0.12
0.28
67%
67%
<51
7
9
14
Hexachloroethane
21
54
0.39
0.95
2.23
2.11
0.12
0.31
69%
67%
<51
7
10
14 _
Methyl Chloride
86
190
1.51
3.34
2.11
2.11
0.49
1.09
67%
67%
<5
30
40
59
Methylene Chloride
40
89
0.70
1.57
2.10
2.12
0.23
0.51
67%
67%
<5
14
18
28
Naphthalene
*
22
59
0.45
0.50
2.45
1.02
0.13
0.50
72%
0%
<51
8
10
15
Nitrobenzene
27
68
0.48
1.20
2.13
2.12
0.16
0.39
68%
67%
<51
9
12
19
2-Nitrophenol
41
69
1.23
2.08
3.60
3.61
_
0.24
0.40
81%
81%
<51
14
19
_
28
4-Nitrophenol
72
124
2.17
3.74
3.61
3.62
0.41
0.71
81%
81%
<260
25
33
50
Phenanthrene
*
22
59
0.39
0.50
2.13
1.02
0.13
0.50
68%
0%
<51
8
10
15
Phenol (3)
15
26
1.56
2.70
12.47
12.45
0.09
0.15
94%
94%
<51
5
7
_
10
Pyrene
*
25
67
0.44
0.50
2.11
0.89
0.14
0.50
67%
0%
<51
9
12
17 _
Tetrachloroethylene
22
56
0.39
0.99
2.13
2.12
0.13
0.32
68%
67%
<5
8
10
15
Toluene
26
80
0.53
1.63
2.44
2.44
0.15
0.46
72%
72%
8.1
9
12
18
Total Chromium
1110
2770
-
-
-
-
6.39
15.94
-
-
-
383
511
766
Total Copper
1450
3380
--
--
-
-
8.34
19.45
-
-
-
500
667
1001
Total Cyanide
420
1200
7.39
9.01
2.11
0.90
2.42
2.95
67%
67%
9
145
193
290
Total Lead
320
690
--
-
-
-
1.84
3.97
-
-
--
110
147
221
Total Nickel _
1690
3980
--
- _
-
- __
9.73
22.90
--
-
-
583
777
1166
Final, Page 2 of 3
8/16/02
13020s002
OCPSF-Tier 2

l l 1 1 1, 1 1 I 1 1 l l 1
TIER 2 LIMITS
OCPSF CURRENT AND PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Average Daily Flow (MGD) = 0.690
Effluent Characteristic
WQL
OCPSF Limits
Current Limits
Current Limits -
Calculated Flow
Proposed Limits
@ 0.690 MGD
% Limit
Reduction
Histor-
ical
Max Allowable Conc. in Final
Effluent from Proposed Limits
Month
Avg.
(ug/L)
Max
Day
(ug/L)
Month
Avg.
(Ibld)
Max
Day
(Ib/d)
'
Month
' Avg.
Flow
(MGD)
Max
Day
Flow
(MGD)
Month
Avg.
(ibld)
Max
Day
(Ib/d)
Month
Avg.
Limit
Max
Day
Limit
Max
Conc.
(ug/L)(1)
-
Month
Avg.
Conc. @
2.0 MGD
(ug/L)
362
Month
Avg.
Conc. @
1.5 MGD
(ug/L)
483
Month
Avg.
Conc. @
1.0 MGD
(ug/L)
725
Total Zinc
1050
2610
-
-
--
-
6.04
15.02
-
--
1,2,4-Trichlorobenzene
68
140
1.20
2.46
2.12
_ 2.11
0.39
0.81
67%
67%
<51
23
31
47
1,1,1-Trichloroethane
21
54
0.37
0.95
2.11
2.11
0.12
0.31
67%
67%
<5
7
10
14
1,1,1-Trichloroethane(repeat)
21
54
0.37
0.95
2.11
2.11
0.12
0.31
67%
67%
<5
7
10
14
Trichloroethylene
21
54
0.37
0.95
2.11 2.11
0.12
0.31
67%
67%
<5
7
10
14 -
Vinyl Chloride
104
_ 268
1.82
4.70
_
2.10 2.10
0.60
1.54
67%
67%
<5
36
48
72
* These parameters are water quality limited.(WQL). Used current max day limit for proposed max day limit.
(1) Max detection limit observed in sampling from Jan 2001 - Jun 2002.
(2) Historical chlorobenzene results (2001 - 2002): 9.4, <5, <5, 12, <5, <5.
(3) Basis for proposed phenol limit inconsistent with current phenol limit. Current phenol limit much higher than proposed. Basis for limit should be evaluated.
Final, Page 3 of 3
8/16/02
13020s002
OCPSF-Tier 2

TIER 1 LIMITS
CWT PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Max Monthly Flow (MGD) = 0.084
Effluent Characteristic
CWT Limits
Proposed Limits @
0.084 MGD
Max Allowable Conc. in Final Effluent
from Proposed Limits
Month Avg.
(mg/L)
Max Day
(mg/L)
Month
Avg. (Ib/d)
Max Day
(Ib/d)
Month Avg.
Conc. @ 2.0
MGD (mg/L)
0.006
Month Avg.
Conc. @ 1.5
MGD (mg/L)
0.008
Month Avg.
Conc. @ 1.0
MGD (mg/L)
0.012
Antimony
0.141
0.237
0.099
0.166
Arsenic
0.104
0.162
0.073
0.113
0.004
0.006
0.009
Barium
0.281
0.427
0.197
0.299
0.012
0.016
0.024
Cadmium
0.0102
0.0172
0.007
0.012
0.000
0.001
0.001
Chromium
0.323
0.746
0.226
0.523
0.014
0.018
0.027
Cobalt
0.124
0.192
0.087
0.135
0.005
0.007
0.010
Copper
0.242
0.500
0.170
0.350
0.010
0.014
0.020
Lead
0.160
0.350
0.112
0.245
0.007
0.009
0.013
Mercury
0.000739
0.00234
0.0005
0.0016
0.0000
0.0000
0.0001
Molybdenum
0.965
1.01
0.676
0.708
0.04
0.05
0.08
Nickel
1.45
3.95
1.016
2.767
0.06
0.08
0.12
Selenium
0.408
1.64
0.286
1.149
0.017
0.023
0.034
Silver
0.0351
0.12
0.025
0.084
0.001
0.002
0.003
Tin
0.120
0.409
0.084
0.287
0.005
0.007
0.010
Titanium
0.0299
0.051
0.021
0.036
0.001
0.002
0.003
Vanadium
0.0662
0.218
0.046
0.153
0.003
0.004
0.006
Zinc
0.420
0.497
0.294
0.348
0.018
0.024
0.04
Acetone
7.97
30.2
5.583
21.157
0.33
0.45
0.67
Acetophenone
0.0562
0.114
0.039
0.080
0.0024
0.0031
0.005
Aniline
0.0164
0.0333
0.011
0.023
0.0007
0.0009
0.0014
Bis(2-ethylhexyl)phthalate
0.101
0.215
0.071
0.151
0.004
0.006
0.008
2-Butanone
1.85
4.81
1.296
3.370
0.08
0.10
0.155
Butylbenzyl phthalate
0.0887
0.188
0.062
0.132
0.004
0.005
0.007
Carbazole
0.276
0.598
0.193
0.419
0.012
0.015
0.023
o-Cresol
0.561
1.92
0.393
1.345
0.024
0.031
0.05
p-Cresol
0.205
0.698
0.144
0.489
0.009
0.011
0.017
n-Decane
0.437
0.948
0.306
0.664
0.018
0.024
0.04
2,3-Dischloroaniline
0.0361
0.0731
0.025
0.051
0.0015
0.0020
0.0030
Fluoranthene
0.0268
0.0537
0.019
0.038
0.0011
0.0015
0.0023
n-Octadecane
0.302
0.589
0.212
0.413
0.0127
0.017
0.025
Phenol
1.08
3.65
0.757
2.557
0.045
0.060
0.09
Pyridine
0.182
0.37
0.128
0.259
0.008
0.010
0.015
2,4,6-Trichlorophenol
0.106
0.155
0.074
0.109
0.004
0.006
0.009
Final, Page 1 of 1
8/16/02
13020s002
CWT-Tier 1

TIER 2 LIMITS
CVYT PROPOSED LIMITS - NON -CONVENTIONAL PARAMETERS
Proposed Max Monthly Flow (MGD) = 0.266
Effluent Characteristic
CWT Limits
Proposed Limits (ad'
0.266 MGD
Max Allowable Conc. in Final Effluent
from Proposed Limits
Month Avg.
(mg/L)
Max Day
(mg/L)
Month
Avg. (Ib/d)
Max Day
(Ib/d)
Month Avg.
Conc. @ 2.0
MGD (mg/L)
Month Avg.
Conc. c@D 1.5
MGD (mg/L)
Month Avg.
Conc. @ 1.0
MGD (mg/L)
0.038
Antimony
0.141
0.237
0.313
0.526
0.019
0.025
Arsenic
0.104
0.162
0.231
0.359
0.014
0.018
0.028
Barium
0.281
0.427
0.623
0.947
0.037
0.050
0.075
Cadmium
0.0102
0.0172
0.023
0.038
0.001
0.002
0.003
Chromium
0.323
0.746
0.717
1.655
0.043
0.057
0.086
Cobalt
0.124
0.192
0.275
0.426
0.016
0.022
0.033
Copper
0.242
0.500
0.537
1.109
0.032
0.043
0.064
Lead
0.160
0.350
0.355
0.776
0.021
0.028
0.043
Mercury
0.000739
0.00234
0.0016
0.0052
0.0001
0.0001
0.0002
Molybdenum
0.965
1.01
2.141
2.241
0.13
0.17
0.26
Nickel
1.45
3.95
3.217
8.763
0.19
0.26
0.39
Selenium
0.408
1.64
0.905
3.638
0.054
0.072
0.109
Silver
0.0351
0.12
0.078
0.266
0.005
0.006
0.009
Tin
0.120
0.409
0.266
0.907
0.016
0.021
0.032
Titanium
0.0299
0.051
0.066
0.113
0.004
0.005
0.008
Vanadium
0.0662
0.218
0.147
0.484
0.009
0.012
0.018
Zinc
0.420
0.497
0.932
1.103
0.056
0.074
0.11
Acetone
7.97
30.2
17.681
66.997
1.06
1.41
2.12
Acetophenone
0.0562
0.114
0.125
0.253
0.0075
0.0100
0.015
Aniline
0.0164
0.0333
0.036
0.074
0.0022
0.0029
0.0044
Bis(2-ethylhexyl)phthalate
0.101
0.215
0.224
0.477
0.013
0.018
0.027
2-Butanone
1.85
4.81
4.104
10.671
0.25
0.33
0.492
Butylbenzyl phthalate
0.0887
0.188
0.197
0.417
0.012
0.016
0.024
Carbazole
0.276
0.598
0.612
1.327
0.037
0.049
0.073
o-Cresol
0.561
1.92
1.245
4.259
0.075
0.099
0.15
p-Cresol
0.205
0.698
0.455
1.548
0.027
0.036
0.055
n-Decane
0.437
0.948
0.969
2.103
0.058
0.077
0.12
2,3-Dischloroaniline
0.0361
0.0731
0.080
0.162
0.0048
0.0064
0.0096
Fluoranthene
0.0268
0.0537
0.059
0.119
0.0036
0.0048
0.0071
n-Octadecane
0.302
0.589
0.670
1.307
0.0402
0.054
0.080
Phenol
1.08
3.65
2.396
8.097
0.144
0.192
0.29
Pyridine
0.182
0.37
0.404
0.821
0.024
0.032
0.048
2,4,6-Trichlorophenol
0.106
0.155
0.235
0.344
0.014
0.019
0.028
Final, Page 1 of 1
8/16/02
13020s002
CWT-Tier 2