WQ0001817_Monitoring - 11-2021_20220113 (3)

GW-59A COMPLIANCE REPORT FORM Permit # v114 00018/'7
(Submit one each monitoring period with GW-59 forms.)
1 Enter date monitoring results were due.(iA-31'Ai ) Will this monitoring report(GW-59 and GW-59A) YES ; 0
be submitted after the established due date?
2 Was any required information missing on the GW-59 report forms? YES NOI
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3 Arc and of the monitor wells in need of repair or maintenance(damaged easing,unlocked or missing cap, missing YES O )
identification plate,area overgrown,etc.)?If the answer is -Yes-, contact the Regional Office Jur guidance.
4 Are any monitored constituents equal to or above the established standards? , YES,/ NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below:
A 'I u1•c 1/i / file a, 10
nn
5 For the constituents identified in question 4 above, have standards been exceeded previously for the 4 YES NO
same constituent(s) in the same well(s)in the last two years?
r,
i If the answer to question 5 is "NO'; skip to section 8. cm
' If the answer to question 5 is "YES", list in the space provided below, each well with con, uent(s)exceeding
standards, concentration(s)reported, and sample collection date for each occurrence(for thelast two years). ,
>C.0 / Y/ CIC.I c CC' '
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YF.S 6 -44161
if the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is "NO", monitoring wells may be improperly
located;contact the Regional Office.
7 Is the permittee implementing previously approved actions required by the Division involving this I YES
groundwater quality problem?
If the answer to question 7 is "YES". describe those actions in the space provided below.
if the answer to question 7 is "NO", contact the Regional Office within 90 clays;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject thepermittee to a Notice of Violation,
fines, and/or penalties.
c
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this i
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report(Compliance Report GW1-59A)is true and complete to the best of my know dge.
•U‘ !
(A , z 2112 I
ao Pe ee(or Authorized Agent) Date
I 1
GW-59A I2/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES
and I Copy to: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Comapany Non-Discharge W00001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford N.0 27944 County Pergimans © Lagoon El Remediation: Infiltration Gallery
LI Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#:[phone] El Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: North of Holding Lagoon No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-1 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 20 ft. Well Diameter: 2 in. pH 00400:5.0 units Temp.00o10: 15.7 °c DRY at
time of
Depth to Water Level 82546: 13-3 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec.Cond.00094: µMhos sampling,
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check
Volume of water pumped/bailed before sampling: 4.0 gallons Appearance Tan/Turb here:
Samples for metals were collected unfiltered: 0 YES ® NO and field acidified: ❑YES ®NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.17 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 360 mg/L Al-Aluminum 01105 mg/L
pH(Lab)00403 5.0 units Ba-Barium 01007 ug/L
TOC 00680 3.9 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 10 mg/L Cd-Cadmium 01027 ug!L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) El No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method#
Total Ammonia 00610 1 mg/L Mg-Magnesium 00927 mg/L .method# 1
{Armarua estrogen.NH,as N.Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L . method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete and that the laboratory analytical data was produced using approved methods of analysis by a
C1ti'R-certified laboratory. I am aware that there are s;grit cant peralnes for s.ibmifting false information,.includirg the puscibaity of`roes and imprisonment for know ng viotat;ons..
Shayne Lamb Corporate Secretary �� it<,,,
( L . 2 I
aC- .- {1t/, jt
Permittee(or Authorized Agent)Name and Title-Please print or type Sign-tore• P€rmett4•(or Authorized Agent) (Oates}
GW-59 Rev.06-07-2018 •
I

Environmental Chemists, Inc.
envirocl em
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,:n RnwScrtr,wn It„:.a,Ntin'r•t,, NC 27t)i4 • 1-'' ').''':. i ;,t'
)`,`, ;\ Wilmingti . Hi};ftu:dt, lack,,,,nv illy, "(_ 2.h5•;t` • •r } ;r : . .i!, ,
ANALYTICAL&CONSULTING CHEMISTS info 4r.cm.it,i^r,nk ntAICI•ini:!, , 1I
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51662 Site: MW-1 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Tan/Turbid 11/19/2021
Depth to water, ft. Depth to Water,Ft. 13.3 feet 11/19/2021
Ammonia Nitrogen EPA 350.1.Rev.2.0,1993 1 pg/L 11/29/2021
Gallons bailed before sampling Gallons Bailed before sampling 4 (dry)gallons 11/19/2021
Odor Qualitative None 11/19/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 360 mg/L 11/23/2021
Temperature SM 2550 B-2010 15.7 C 11/19/2021
pH SM 4500 H B-2011 5.0 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 B-2014 3.9 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5.g/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichioroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 IJg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 ug/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report k. 2021-20623 Page 1 of 30

Environmental Chemists, Inc.
1! nvjrobe,u , 6602 Windmill Way,Wilmington,Ni,„ 2h40 • 910.3992 0223 1.ab • 9)0 392.4I, 1 I
"1
710 I3owsertown Road, Manico, NC 27954 • 252.473,5702 Ltif }at
255-A Wilmington Highway,Jacksonville,NC 28540 • 910 347.5843 Lai-i 1
ANALYTICAL&CONSULTING CHEMISTS info ii environrnentslchemists com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer Pa#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene sM 6200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 6200 8.2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromochioromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromoform SM 8200 8-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 13-2011 <0.5 pg/L 11/24/2021
Chioromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichioroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dibromochioromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Ethylbenzene sM 6200 B•2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 6200 8-2011 <0.5 pg/L 11/24/2021
lsopropylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butyibenzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene sM 6200 8-2011 <0.5 pg/L 11/24/2021
Report#:: 2021-20823 Page 2 of 30

Environmental Chemists, Inc.
4:7'envirochem (602 Windmill Way,Wilmington,NC 28405 4 910.392.0223 lab 9l !t'2-444:'4I l ax
710 Bowsertown Road,Manteo,NC:27954 + 252.47 -3702 Lah11,
—.. 255-A Wilmington Highway,Jacksonville,NC 28540 • 91U347-584-, Lao i=.ix
ANALYTICAL&CONSULTING CHEMISTS infiOenvirnnrnentalchentists.corn
Albemarle UtilityDate of Report: Dec 06, 2021
P
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 B-2011 <0.5 ug/L 11/24/2021
p-lsopropyltoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Styrene SM 6200 8.2011 <0.5 Ug/L 11/24/2021
tert-B utyl benzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 8200 B-2011 <0.5 Ng/L 11/24/2021
Toluene SM 8200 B-2011 4.15 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 8200 8.2011 <0.5 pg/L 11/24/2021
Vinyl chloride 5M 6200 8-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride 5M45oo CI E•2011 10 mg/L 11/24/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev 2 0, 1993 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353 2,Rev 2 0 1993 0.19 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.17 mg/L 12/03/2021
Report# 2021-20623 Page 3 of 30 .A.>.

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENNFORMATIONTAL QUALITY-PROCE SING UNIT
OF WATER RESOURCES
COMPLIANCE REPORT FORM and 1 copy to:
1617 MAIL SERVICE CENTER,RALElGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans ® Lagoon ❑Remediation: Infiltration Gallery
Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:East of Baffle Lagoon No.of wells to be sampled: 10 ❑ Water Source Heat Pump 0 Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-2 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp.00010: 15.9 °C DRY at
time of
Depth to Water Level 82546: 7.6 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.00004. µMhos sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085. Sulfur check
Volume of water pumped/bailed before sampling: 3.0 gallons Appearance Tan/Turbid here: 1
Samples for metals were collected unfiltered: ❑YES ® NO and field acidified: ❑YES ®NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environment Chemists, Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead o1051 ug/L
Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.14 mg/L Zn-Zinc o1092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 263 mg/L Al-Aluminum 01105 mg/L
pH(Lab)00403 5.8 units Ba-Barium 01007 ug/L
TOC o0680 19.0 mg/L Ca-Calcium 00916 mg/L
Chloride oo94o 12 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method#
Total Ammonia 00610 1 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L .method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
certify that to the best of my knowledge and belief the nformation st.bmitted in this report is true.accurate.and complete,and that the laboratory analytical data was produced awng.approved methods of analyse by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information.mr,clt,dmg the possibility o'fires and imprisonment for knowing violations j
Shayne Lamb Corporate Secretary` • r or ` f y
Permitter,:(or Authonzed Agent)Name and Title-Please print or type Sig e• ••r Mee it Authorized Agent) (Date) r
GW-59 Rev.06-07-2018

. Environmental Chemists, Inc.
'' envirochem 6602 Windmill Way,Wilmington,NC 28405 + 910.392,0223 Lab • y I G 192 4424 I,,,,
710 Bowsertown Road, Manteca,NC 27954 + 252,473.5702 l.abi Faa
255-A Wilmington Highway,Jacksonville,NC 28540 • 910 347 3 4; I • 0,; 10,_
ANALYTICAL&CONSULTING CHEMISTS in ._ .e•nvfrnnmentaicherms:c corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51663 Site: MW-2 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Tan/Turbid 11/19/2021
Depth to water, ft. Depth to Water,Ft 7.6 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 1 pg/L 11/29/2021
Gallons bailed before sampling Gallons Balled before sampling 3 (dry)gallons 11/19/2021
Odor Qualitative Sulfur 11/19/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 263 mg/L 11/23/2021
Temperature SM 2550 B-2010 15.9 C 11/19/2021
pH SM 4500 H 8-2011 5.8 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 B-2014 19.0 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 iig/L 11/24/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5►ag/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 ig/L 11/24/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dich loropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report# 2021-20623 Page 4 of 30

Environmental Chemists, Inc.
virochetn 6602 Windmill Way,Wilmington,NC 28405 • 910._392.0223 Lab • 9:1.392 44.?4 Fa>
710 Bowsertown Road,Manteo, NC 27954 • 252.471 5702 E ab`I a>
255-A Wilmington I Iighway,Jacksonville,NC 28540 • 910 347.5811 iab<1;ax
ANALYTICAL 8 CONSULTING CHEMISTS info(a;cnvironmentalchcmists.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 8200 B-2011 <0,5 i1g/L 11/24/2021
Bromochloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromoform SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 8200 B-2011 <0.5 itg/L 11/24/2021
Carbon tetrachloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chiorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 B-2011 <0.5 ug/L 11/24/2021
Chloromethane sM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichioroethene SM 6200 13-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 B-2011 <Q.5 pg/L 11/24/2021
Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 8200 B-2011 <0.5 pg/L 11/24/2021
isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 8200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM6200B-2011 <0.5iJg/L 11/24/2021
n-Butylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 6200 B-2011 <0.5 i.Ig/L 11/24/2021
Report#:: 2021-20623 Page 5 of 30

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392 0223 Lab • 910_3`42.4424 1-Fa.
710 Bows>rtown Road, Manteo,NC 27954 • 252.473.57(12 Lab;1'as
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 l_ab I.,),.
ANALYTICAL&CONSULTING CHEMISTS info{a!environmentalehemists.coln
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 8200 8-2011 <0.5 pg/L 11/24/2021
p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Styrene SM 6200 B-2011 <0.5 pg/L 11/24/2021
tert-Butylbenzene SM 8200 13-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Toluene SM 8200 B-2011 6.78 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trich loroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 6200 13-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 8-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 12 mg/L 11/24/2021
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2 0,1993 0.14 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.14 mg/L 12/03/2021
Report#:• 2021-20823 Ndye

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Man original DEPARTMENT OF OF WATER RESOURCES
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and 1 Copy 10. 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge W00001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans 0 Lagoon ❑Remediation: Infiltration Gallery
❑ti Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: South East of Spray field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Permn)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-3 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.0 units Temp.Qom: 16.0 °C DRY at
time of
Depth to Water Level 82546: 7.9 ft.below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.0oos4. µMhos sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check
Volume of water pumped/bailed before sampling: 2 gallons Appearance Brown here:
Samples for metals were collected unfiltered: ❑YES It NO and field acidified: 0 YES It NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.03 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.03 mg/L Zn-Zinc otos2 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 m /L Other(Specify Compounds
g ( p ty and Concentration Units):
Dissolved Solids:Total 70300 845 mg/L Al-Aluminum 01105 mg/L
pH(Lab)00403 6.0 units Ba-Barium 01007 ug/L
TOC 00680 47.2 mg/L Ca-Calcium 00916 mg/L
Chloride oos4o " 15 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method#
Total Ammonia 00610 15 mg/L Mg-Magnesium 00927 mg/L .method#
(Ammonia Nitrogen,NH,as N,Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L . method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L . method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief,the information submitted in:his report is true.accurate,and complete.and that the laboratory analytical data was produced using approved methods of analysts by a
041WR-certified laboratory. I am aware that there are significant penalties for submitting false adormation,including the possibility of fines and-mprisonment for know ng vio)atrons.
Shayne Byrum- Corporate Secretary 12
Permittee for Authorized Agent)Name and Title-Please print or type Sign re -ermitte.(or Authorized Agent) Date)
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910 392 4424 F ,x
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/lax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910 347 5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS :nto(d)environrnentaichcmists.com
I emarl A b e Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51664 Site: MW-3 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color • Brown 11/19/2021
Depth to water, ft. Depth to water,Ft. 7.9 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev 2 0,1993 15 pg/L 11/30/2021
Gallons bailed before sampling Gallons Bailed before sampling 2 (dry)gallons 11/19/2021
Odor Qualitative Sulfur 11/19/2021
Total Dissolved Solids(IDS) SM 2540 C-2015 845 mg/L 11/23/2021
Temperature SM 2550 8-2010 16.0 C 11/19/2021
pH SM 4500 H 8.2011 6.0 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 8-2014 47.2 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 8.2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 8200 8.2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 8.2011 <0.5 pg/L 11/24/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 8.2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trich lorobenzene SM 6200 B-2011 <0.5 lg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 8-2011 <0.5.g/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloropropane SM 6200 8-2011 <0.5.ig/L 11/24/2021
1,3,5-Trimethylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Report# 2021-20623 Page 7 of 30

Environmental Chemists, I -tc
s(I;2 4\ t,ci tli'\ay 1N'i r1 ngt n, ''C ftES ,(:' 11:_ i.,i
7th 3e »�,c'rti>.4'Il kud,i, A!'_? ' ' '. : 4 r`+i-i _ �i%
�4 ". 1 .I 7:nn:;t +i�; ,, I:, ;- ,sir,�.( v�� .t f.
ANALYTICAL&CONSULTING CHEMISTS
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 6200 B.2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 8.2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 8.2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Benzene sM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Ch loromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/24/2021
lsopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 6200 8-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 8-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 8-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 8.2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report#:. 2021-20823 Page 8 of 30 fi

Environmental Chemists, Inc.
envirochein 6602 Wmdmili Way,Wilmington,NC 28405 • 910.39.2 0223 I_ab 9 91(1c/ ;1.'; I r,.
710 Bowsertown Road,'vlanten,NC 27954 • 252.473- 702 Lal.,11,r>.
--- - :, '" 255-A Wilmington Highway,Ia.ksonville,NC 28540 * 9I0.347'. 443 IAt,/Fo,
ANALYTICAL&CONSULTING CHEMISTS intoqem'uorimentalchermsts.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 8200 8-2011 <0.5 pg/L 11/24/2021
p-isopropyitoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
sec-Butyibenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Styrene SM 6200 B-2011 <0.5 ig/L 11/24/2021
tert-Butyibenzene SM 6200 8.2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Toluene SM 8200 8-2011 1360 Iig/L 11/24/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 15 mg/L 11/24/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 0.03 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0.1993 0.06 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/03/2021
Report# 2021-20623 Page 9 at 30 -.

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF TION PROCESSING SI G UNITF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: INFORMATION
COMPLIANCE REPORT FORM and 1 copy to:
1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans El Lagoon ❑Remediation: Infiltration Gallery
0 Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: South West of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-4 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 12 ft. Well Diameter: 2 in. pH 00400:5.8 units Temp.0o010: 17.5 °C DRY at
1Mhos time of
Depth to Water Level 82546: 8.2 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.00094. t sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check
Volume of water pumped/bailed before sampling: 3.0 gallons Appearance Tan/Clear here:r ,
Samples for metals were collected unfiltered: CI YES in NO and field acidified: ❑YES ®NO u 1
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mgfL Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.10 mg/L Zn-Zinc 01092 mg/L
Coliform:ME Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 202 mgfL Al-Aluminum o1105 mg/L
pH(Lab)00403 5.8 units Ba-Barium 01007 ug/L
TOC 00680 23.9 mg/L Ca-Calcium o0916 mg/L
Chloride o0940 - 6 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 iMhos K-Potassium 00937 mg/L VOC 7873 ,method#
Total Ammonia 00610 1 mg/L Mg-Magnesium 00927 mg/L ,method#
i Ammonia Nitrogen,NH,as N.Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L . method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L . method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief.the information submitted in this report is true.accurate.and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
OSha nef ied laboratory.
a Lamb raCOr l am a,.yare
athere are significant penalties for submitting falseinformatron-including tie possibility of fines and:mpr�sormen'for know np violations.
1 2. Zf
YP SecretaryriFf
r T
Permittee for Authorized Agent)Name and Title-Please print or type Sig-a P- te- r Authorized Agent) ft" to
GW-59 Rev.06 07-2018

Environmental Chemists, Inca
i `ir the . 6602 Windmill Way,Wilmington, NC 28405 • 910.392.0223 : it . 91(a 99 .4;:; i z,.
710 Bowsertown Road,Manic n,N.C.27954 • 252.4/3.57(}2 Lab /Fay.
. ' 255-A Wilmington Highway,Jacksonville, NC28540 • 910 347.58 .3 I an'i'ay
ANALYTICAL&CONSULTING CHEMISTS into%rgeraiironmentalchemists.Coin
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51665 Site: MW-4 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Tan/Clear 11/19/2021
Depth to water, ft. Depth to water,Ft. 8.2 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 1 .ig/L 11/29/2021
Gallons bailed before sampling Gallons Balled before sampling 3 (dry)gallons 11/19/2021
Odor Qualitative None 11/19/2021
Total Dissolved Solids (IDS) SM 2540 C-2015 202 mg/L 11/23/2021
Temperature SM 2550 B-2010 17.5 C 11/19/2021
pH SM 4500 tt 8-2011 5.8 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 B-2014 23.9 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichooroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2-Trichioroethane SM 6200 13-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichioropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene sM 6200 B-2011 <0 51Jg/L 11/24/2021
Report it:: 2021.20623 Page 10 of 30

Environmental Chemists, Inc,
oc '' 66()2 Windmill Way,'vVilmington,NC 28=105 • 910.39?0227 i.at; 91i �,'i.?--i,. ' ? .1
. 710 Bowsertown Road,Manteo, NC 27954 • 252.473.5702 Lab, l,ix
255-A Wilmington Highway,Jacksonville,NC 28540 * Y1().3-17 5843 1 ab'f`a>.
ANALYTICAL&CONSULTING CHEMISTS infor,environmentalchemists coin
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
• Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane sM 6200 B-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1 2,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane sM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichloroethene SM 6200 6.2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane sM 6200 8-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Ethylbenzene sM 6200 B-2011 <0.5 pg/L 11/24/2021
Hexachlorobutad iene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 8200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM6200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report# 2021-20623 Page 11 of 30

Environmental Chemists, Inc.
envirochein 6602 Windmill Way,Wilnungton,NC 28405 • 910,392.0223 L<1h . 910.392.4 12 I ,,y
710 Bowsertown Road,Manteo, NC 27954 • 252.473 5702 Lab/Fax
" 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347 5843 I.ab/}*,1y
ANALYTICAL&CONSULTING CHEMISTS int-4-0environnlentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/24/2021
p-lsopropyltoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 6-2011 <0.5 pg/L 11/24/2021
Styrene SM 8200 B-2011 <0.5 pg/L 11/24/2021
tert-Butylbenzene SM 6200 B•2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Toluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichioropropene SM 6200 6-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Fecal Coliforrn SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 6 mg/L 11/24/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0.1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.10 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.10 mg/L 12/03/2021
Repot# 2021-20623 Page 12 of 30

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
and 1 copy to: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge W00001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans IN Lagoon ❑Remediation: Infiltration Gallery
IN Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: South West of Sprayfield No.of wells to be sampled: 10 0 Water Source Heat Pump ❑Other:
(from Permit) _
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-5 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 5.9 units Temp.000to: 1 8.1 °C DRY at
!Mhos time of
Depth to Water Level 82846: 8.5 ft. below measuring point Screened Interval: 12 ft. to 2 ft. Spec.Cond.00094: f sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfar check
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here:I f
Samples for metals were collected unfiltered: CI YES IN NO and field acidified: ❑YES MI NO u
LABORATORY INFORMATION
Date sample analyzed:1l/19/2021 Laboratory Name: Environmental Chemists,Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L• Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01a51 ug/L
Coliform:MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.03 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Oissotved Solids:Total 70300 312 mg/L Al-Aluminum 01105 mg/L
pH(Lab)00403 5.9 units Ba-Barium 01007 ug/L
TOC 00680 4.6 mg/L Ca-Calcium owls mg/L
Chloride o0940 64 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC GC/MS, HPLC)
Phenol 32730 ugiL Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method#
Total Ammonia o0610 0 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen,NH,as N:Ammonia Nitrogen.Total) Mn-Manganese 01o55 ug/L ,method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L . method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that.to the best of my knowledge and belief.the reformation submitted in this report is true.accurate.and complete.and that the laboratory analytical data was produced using approved methods of analysis bya
DWR-certified laboratory. I am aware that there are significant penalties for submittng false information.including the poss h5lity of fines and imprisonment for know:na violations.
Shayne Lamb - Corporate Secretary
1 �} fJ
Agent)Name and Title-Please print or t Sig.ure of Permdte: or Authorized Agent) I (Date f
Permittee(or Authorized Aa ) n yPe
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
:Tien _ __ � 6602 Windmill Way,Wilmington,NC 2fi405 • -)10.�3��2.0223 Lab • �rl� �_ t. `. i
710 Bowsertown Road,Manteo,►*JC 2795# 2.52.E 73a5-r't,2 t ab, t ax
��� 255-A Wilmington Highway,Jacksonville,NC 2R940 • 91�3 347,58.33 Lail
ANALYTICAL&CONSULTING CHEMISTS tnfora?environment alchemists.corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51666 Site: MW-5 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Tan/Clear 11/19/2021
Depth to water, ft. Depth to Water,Ft. 8.5 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0.1993 0 pg/L 11/29/2021
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2021
Odor Qualitative Sulfur 11/19/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 312 mg/L 11/23/2021
Temperature SM 2550 8-2010 18.1 C 11/19/2021
pH SM 4500 H B-2011 5.9 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 B-2014 4.6 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1.1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 8.2011 <0.5 pg/L 11/24/2021
1,1-Dichioropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichioropropane SM 6200 8-2011 <0 5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report S': 2021-20623 Page 13 of 30

Environmental Chemists, Inc.
envirocheni 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910192.44Z4 1,,,
710 Bowsertown Road,Manteo,NC 27954 • 252 473 5702 1.ab/1'ax 5
255-A Wilmington Highway,Jacksonville, NC 28540 • 910_;347.5843 1,ah,I d).
ANALYTICAL&CONSULTING CHEMISTS into(d)cnvironmentalchcmists.corrt
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
1 Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
2-Chtorotoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 6200 a-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromochioromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromoform SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chlorobenzene sM 6200 8-2011 <0.5 pg/L 11/24/2021
Chioroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloromethane SM 6200 B-2011 <0.5 pgfL 11/24/2021
cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromochioromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 8200 8-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 6200 8.2011 <0.5 pg/L 11/24/2021
isopropyIbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 8.2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Report tt:: 2021-20623 Page 14 of 30

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab 4 910 392.142-4 Fa'.
710 13owsertown Road,Manteo,NC 27954 • 252.473.5702 Labi hay
w 255-A Wilmington Highway,Jacksonville, NC 28540 • 910.3475E+43 LaI,"Fax
ANALYTICAL&CONSULTING CHEMISTS infocOenvrronmentalchemtsts.cont
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/24/2021
p-lsopropyltoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Styrene SM 8200 8-2011 <0.5 pg/L 11/24/2021
tert-Butylbenzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Tetrachioroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Toluene SM 8200 B-2011 <0.5 i g/L 11/24/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 620D B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 64 mg/L 11/24/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2.Rev.2.0.1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0, 1993 0.03 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/03/2021
Report p- 2021.20623 Page'5 or 3C

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL
PROCESSINGI UNIT
WATER RESOURCES
GROUNDWATER QUALITY MONITORING: INFORMATION
COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025
Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans 0 Lagoon ❑Remediation: Infiltration Gallery
0 Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] 0 Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: West Of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW - 6 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp. 00010' 17.9 T. DRY at
time of
Depth to Water Level 82546: 11.7 ft.below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.00094. µMhos sampling,
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Grey/Turbid here:
Samples for metals were collected unfiltered: ❑YES IN NO and field acidified: ❑YES It NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N oasts <0.02 mg/L Pb-Lead 01051 ug/L
Coliform.MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.03 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
dissolved Solids:Total 70300 562 mg/L Al-Aluminum 01105 mg/L
pH(Lab)00403 5.8 units Ba-Barium 01007 ug/L
TOC 00680 3.6 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 - 132 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 }(Mhos K-Potassium 00937 mg/L VOC 7873 ,method# 1
Total Ammonia 00610 0 mg/L Mg-Magnesium 00927 mg/L method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Totali Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief.the information submitted in this report is true.accurate.and complete.and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory I am aware that there are significant penalties for submitting false information.including the poss bitity of fines and imprisonment for know'ng vio'ations. d
Shayne Lamb - Corporate Secretary 4 1 ���' 1 2,,,- 2-1 Z .I{
19!
Permittee(or Authorized Agent)Name and Title-Please print or type Signa ure of P• mitten r uthoriz-d Anent) (Date)
I
GW-59 Rev.06-07-2018 G
J

Environmental Chemists, Inc.
enviy�rAla
ochein r,b(!< vv,..,nufl lb,,, A\ rrringtun. "( 2K41_,, `01( _-' 2 ,.`', I.:ih . i .
7 1 L[iow sr rugs it RI,ri, ,tit,i::',• ', A 2''C, • . ,.' 171 : .ir. I
215-A 41yiimint;tur Hi£thwav, la(ks,,t)v;.IN. `.( '>1y111 • 91,' i 17 `i"1 ,
ANALYTICAL&CONSULTING CHEMISTS ntl.,:,t•1. I,':l;f I,'.+ic I•,'n.,,!>
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51667 Site: MW-6 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Grey/Turbid 11/19/2021
Depth to water, ft. Depth to Water.Ft 11.7 feet 11/19/2021
Ammonia Nitrogen EPA 350.1 Rev.2.0.1993 0 pg/L 11/30/2021
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2021
Odor Qualitative None 11/19/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 562 mg/L 11/23/2021
Temperature SM 2550 8-2010 17.9 C 11/19/2021
pH SM 4500 H B-2011 5.8 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 13-2014 3.6 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 8200 13-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM6200B-2011 <0.5 pg/L 11/24/2021
1,1,2-Trichloroethane SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane sM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane sM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene sM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichloropropane sM 8200 8.2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 8200 8.2011 <0.5 Ng/L 11/24/2021
Report# 2021-20623 Page 16 of 30

Environmental Chemists, Inc.
r ,' tr ,oche 6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab ° 91t, iy:'.1424 C
710 Bowsertown Road,Manteo,NC 27954 • 252.473 5702 Lily Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910 3475g43 I„ill,'/o
ANALYTICAL&CONSULTING CHEMISTS enfonenvironmentaIchemists.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 5200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane sM 8200 B-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chlorornethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 6200 8.2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Isopropylbenzene sM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report* 2021-20623 Page 17 of 30

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910 392 ;.}- 1 I-,,\
710 Bowsertown Road,Manteo,NC 27954 • 252.471 5702 Lab/Fax
255-A Wilmington Highway,Jacksonville, NC 28540 • 910347.543I al,,F<n
ANALYTICAL 8 CONSULTING CHEMISTS info(Li nvironmentalchemtsts corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/24/2021
p-lsopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 8200 9-2011 <0.5 pg/L 11/24/2021
Styrene SM 8200 B-2011 <0.5 ig/L 11/24/2021
tert-Butylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Toluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 132 mg/L 11/24/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev,2.0. 1993 0.03 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/03/2021
Report a 2021-20623 Page 18 of 3C

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENINFORMATION TAL QUALITY-DIV.OF WATER RESOURCES
PROCESSING NIT
COMPLIANCE REPORT FORM and 'I copy to:
1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge W00001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans Ei Lagoon El Remediation: Infiltration Gallery
© Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: West of Baffle lagoon No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Perm!)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW -7 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 16.9 ft. Well Diameter: 2 in. pH 00400: 5.3 units Temp.00010 17.0 °C DRY at
11.9 ft. to 16.9 ft. Spec. tMhos time of
Depth to Water Level e2546: 5.1 ft. below measuring point Screened Interval: Cond. 000sa i sampling,
Measuring Point is 2.5 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Reddish/Tan here:
Samples for metals were collected unfiltered: ❑YES ® NO and field acidified: ❑YES it NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists, Inc Certification No.94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead Pto51 ug/L
Coliform MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.02 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
5issolved Solids:Total 70300 247 mg/L Al-Aluminum o11o5 mg/L
pH(Lab)00403 5.3 units Ba-Barium 01007 ug/L
TOC 00680 9.3 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 29 mgiL Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mgiL ORGANICS:(by GC.GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 uMhos K-Potassium 00937 mg/L VOC 7873 .method#
Total Ammonia o0610 1 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen:NH3 as N.Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L .method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief,the information submitted in this report is true.accurate and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are s.gn.ficant penalties for submdfog false information.inducing the possibility of fines and imprisonment for kno,,ing violations.
WAP
�Shayne Lamb - Corporate Secretary : t 7Dle
r
Permittee(or Authorized Agent)Name andTitle-Please rnt or type Signet( e o :r !flee r Authorized Agent) ( at
GW-59 Rev.06-07-2018
J

7
Environmental Chemists, Inc.
envlroch.ein 6h02 Windmill Way,Witm;ngton, NC 28405 • 910.392.0223 Lab • ()it) i92.4424 l.o,
710 Bowscrtown Road,Mantco,NC_27954 • 252.471.5702 t.ah/I-ax
cv
255-A Wilmington Highway,Jacksonville,NC 28540 • 910 347 5843 Lab't-ztti
ANALYTICAL&CONSULTING CHEMISTS inf (wcnvironntentatchenni5ts corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51668 Site: MW-7 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Reddish/Tan 11/19/2021
Depth to water, ft. Depth to Water,Ft. 5.1 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,ReV.2.0,1993 1 pg/L 11/30/2021
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2021
Odor Qualitative None 11/19/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 247 mg/L 11/23/2021
Temperature SM 2550 8-2010 17.0 C 11/19/2021
pH SM 4500 H B-2011 5.3 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 B-2014 9.3 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 8.2011 <0.5 ug/L 11/24/2021
1,1,2-Trichloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1-Dichioroethane SM 8290 8-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichiorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 8-2011 <0.5.g/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 8200 8-2011 <0.5 ig/L 11/24/2021
1,2-Dichiorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dich loroethane SM 6200 B-2011 <0.5 ig/L 11/24/2021
1,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Reporl# 2021-2 06 2 3 Page 19 of 30

Environmental Chemists, Inc.
28405 ° 910.392.0223l ah • 9l , 1:-, s t 1 /a,
?� ��j�'(,��,�"�� , �� 6602 Windmill Way,Wilmington,f�f_' t �_•,•�=
710 Bowsertown Road,Manteca,NC 27954 • 252.471 5702 Lai::"Fa.
255-A Wilmington highway,Jacksonville, NC 28540 • 910.347 5843 t_a l=„.
ANALYTICAL&CONSULTING CHEMISTS infot);environmentalcherntsts.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane sM 6200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 8200 8-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chloromethane sM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichloroethene SM 8200 B-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Dichiorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene sM 6200 B-2011 <0.5 pg/L 11/24/2021
lsopropylbenzene SM 6200 S-2011 <0.5 pg/L 11/24/2021
M+P Xylene sM 8200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene sM 8200 8-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene sM 8200 B-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Report k 2021-20623 Page 20 of 30

Environmental Chemists, Inc.
] ochenl 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 9'0 392.4424 fax
710 Bowsertown Road,Manten,NC 27954 • 2.52.473.5702 Lab Fax
255-A Wilmington Highway,Jacksonville,N(:28540 • 910.347.5843 Lib/Fax
ANALYTICAL&CONSULTING CHEMISTS rnfo,a envirnnmentalchenusis.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 8-2011 <0.5 pg/L 11/24/2021
p-isopropyltoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Styrene SM 6200 8-2011 <0.5 pg/L 11/24/2021
tert-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Toluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM8200B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 8200 8-2011 <0.5pg/L 11/24/2021
Trichioroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 29 mg/L 11/24/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.20. 1993 0.02 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.02 mg/L 12/03/2021
Report#. 2021-20623 Page 21 of 30

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
and Copy to: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge WQ001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans 0 Lagoon ❑Remediation: Infiltration Gallery
El Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: East of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW - 8 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.3 units Temp.00010: 1 7.2 °c DRY at
5 ft. to 15 ft. Spec.Cond.00094: 'Mhos time of
Depth to Water Level 82546: 6.7 ft.below measuring point Screened Interval: sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here: t
Samples for metals were collected unfiltered: ❑YES ® NO and field acidified: 0 YES ®NO J
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 12 colonies /100mL Nitrate(NO3)as N 00620 0.29 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 401 mg/L Al-Aluminum 01105 mg/L
pH(Lab)00403 6.3 units Ba-Barium 01007 uglL
TOC 00680 6.5 rng/L Ca-Calcium 00916 mg/L
Chloride 00940 129 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC. GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method#
Total Ammonia 00610 0 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen:NH,as.N:Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L _. method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that.to the best of my knowledge and belief.the information submitted in this report rs:rue.accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysts by a
DWR-certified laboratory. I am aware that there are s,gn(ficant penalties for submitting false information.including the poss.hil,ty of fires and imprisonment for knowing vinlatons.
Mr
Shayne Lamb - Corporate Secetary lit 4� /�F - n
Permittee(or Authorized Agent)Name and Title-Please print or type Si " of Permitter,/.r uthonzed Agent) (Date)
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
' nvirocheni 6602 Windmill Way,Wilmington,NC 28405 r. 910.392(i223 Lab • 910 392 4,424 1.0,
710[3nwsertown Road,Manteo,NC 27954 • 252.473 5702 Labi l'aa
255-A Wilmington Highway,Jacksonville,NC 28540 • 910 347 5843 l abi 1,ix
ANALYTICAL&CONSULTING CHEMISTS inb.(d;environmentalchernists.corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
..
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51669 Site: MW-8 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Color Tan/Clear 11/19/2021
Depth to water, ft. Depth to Water,Ft. 6.7 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0 Ng/L 11/30/2021
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2021
Odor Qualitative Sulfur 11/19/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 401 mg/L 11/23/2021
Temperature SM 2550 B-2010 17.2 C 11/19/2021
pH SM4500 H B-2011 6.3 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 B-2014 6.5 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 ig/L 11/24/2021
1,1,1-Trichioroethane SM 6200 B-2011 <0.5 p g/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,1,2-Trichloroethane SM 6200 0-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 8200 B•2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Report# 2021-20623 Page 22 of 30

Environmental Chemists, Inc.
vi[o h (.02 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910 392 4424 i ,.*
710 E3owsertown Road,Mante°.NC 27954 • 252.473.5702 1 ab/bak
255-A Wilmington highway,Jacksonville,NC 28540 • 910.347 5843 I,al'/I a‘.
ANALYTICAL&CONSULTING CHEMISTS inlofa,cnvironmcntakhemists.cow
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene sM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 8200 0-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
2-Chiorotoluene sM 6200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 0-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 8200 8-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chioroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chioromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichioroethene SM 8200 B-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropene SM 6200 6-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 8200 8-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Hexachiorobutadiene sM 6200 8-2011 <0.5 pg/L 11/24/2021
lsopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 8200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Report#:: 2021-20623 Page 23 0f 30

Environmental Chemists, Inc.
,F.:,
,„: envirochem
;.,:.
6602 Windmill Way,Wilmington,NC 28405 * 910.392 0223 Lab ' 1410292 14124 I a
-3
710 Howsertown Road,Monter.,NC 27954 • 252,473 5702 Lab 13,ix
3':
255-A Wilmington Flighl,vay,Jacksonville,NC 28540 * 910 147 3843 I abi bax
alto a env oonmentalchemistsatom
ANALYTICAL&CONSULTING CHEMISTS
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 8200 13-2011 <0.5 pg/L. 11/24/2021
p-Isopropyltoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Styrene SM 6200 8-2011 <0.5 pgit_ 11/24/2021
tert-Butylbenzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene Mil 8200 8-2011 <0.5 pg/L 11/24/2021
Toluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Trans-13-dichloropropene SM 8200 8-2011 <0.5 pg/L 11/24/2021
,
Trichloroethene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM6200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 8-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF 12 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 129 mg/L 11/24/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev,2 0 1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2 0 1993 0.29 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.29 mg/L 12/03/2021
Page 24 of 3
Report# 2021-20623 ;:
____

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy to: INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford NC 27944 County Perquimans Ell Lagoon ❑Remediation: Infiltration Gallery
El Spray Field ❑Remediation:
Contact Person: Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor El Land Application of Sludge
Well Location/Site Name. West of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
('rain Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW - 9 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 15 ft. Well Diameter: 2 in. pH 00400. 5.5 units Temp.00o1o: 17.8 °C DRY at
Depth to Water Level 82546: 8.2 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec.Cond.00094: µMhos time of
sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ❑YES ® NO and field acidified: ❑YES ®NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists,Inc Certification No.94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ugiL
Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.06 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units).
Dissolved Solids:Total 70300 64.0 mg/L Al-Aluminum o1105 mg/L
pH(Lab)00403 5.5 units Ba-Barium 01007 ugiL
TOC 00680 0.9 rng/L Ca-Calcium oasts mg/L
Chloride 00940 - 7 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS.HPLC)
Phenol 32730 ugiL Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 7190o ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 ltMhos K-Potassium o0937 mg/L VOC 7873 ,method#
Total Ammonia o0610 0 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen,NH;as N,Ammonia Nitrogen.Total) Mn-Manganese 01055 ugiL . method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L .method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief.the information submitted in this report is true accurate.and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false rnformation,including the possibility of fines aro imprisonment for know.og viointions
Shayne Lamb - Corporate Secretary grr,,, MI 1 0 2 Pe-mittee(or Autho•ized Agent)Name and Title-Please print or type Sig •e o Pe mittee it Authorized Agent) (Date/ 2"
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
envirochen . 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 f o x
71013owsertown Road,Manteo,NC 27954 • 252 471.5702 Lab/Fax
sm
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347 5843 Lab,i.ax
ANALYTICAL&CONSULTING CHEMISTS tnlora)environmentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention; Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51670 Site: MW-9 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color Cola Clear 11/19/2021
Depth to water, ft. Depth to Water,Ft. 8.2 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0 pg/L 11/30/2021
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2021
Odor Qualitative Sulfur 11/19/2021
Total Dissolved Solids(TDS) SM 2540 C-2015 64.0 mg/L 11/23/2021
Temperature SM 2550 8-2010 17.8 C 11/19/2021
pH SM 4500 H B-2011 5.5 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 8-2014 0.9 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane sM6200B-2011 <0.5 pgfL 11/24/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichioropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Report#.. 2021-20623 Page 25 of 30

Environmental Chemists, Inc.
envirochem. 6602 Windmill Way,Wilmington,NC 28405 ' 910.392.0223 Lab • 910.392.4424 },,x
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
,A 255-A Wilmington Highway,Jacksonville,NC 285411 • 910.347 5843 Lab%Fat
ANALYTICAL&CONSULTING CHEMISTS infoi/Ienvirmtmcntalchemists.com
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3-Dichioropropane SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,4-Dichiorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Benzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromodichloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Bromomethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloromethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichioroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichioropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/24/2021
lsopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 8200 8-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene sM 8200 8-2011 <0.5 pg/L 11/24/2021
Report# 2021-20623 Page 26 of 30

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223[at, ',Ile)392 4424 l.1•,
710 Bowsertown Road,Manteo,NC 27954 t 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville,NC 28540 s
ANALYTICAL&CONSULTING CHEMISTS info•9'environmentalchemists.cont
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/24/2021
p-I sopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Styrene SM 8200 B-2011 <0.5 pg/L 11/24/2021
tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Toluene SM 6200 8.2011 <0.5 pg/L 11/24/2021
Trans-1,2-Dichioroethene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-dichloropropene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichiorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 7 mg/L 11/24/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0.1993 0.06 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.06 mg/L 12/03/2021
Report# 2021.20623 Page 27 of 30

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF TION PROCESSING UNITTAL QUALITY-DIV.OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: NFORMA
COMPLIANCE REPORT FORM and 1 copy to:
1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company Non-Discharge WQ001817 UIC
Permit Name(if different): NPDES Other
Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford N.C. 27944 County Perquimans 0 Lagoon ❑Remediation: Infiltration Gallery
0 Spray Field LI Remediation:
Contact Person. Danny Shelton Perry ORC Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name. South of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-10 Date sample collected: 11/19/2021 FIELD ANALYSES: WAS
Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 5.7 units Temp.noon. 18.6 °c DRY at
time of
Depth to Water Level 82546: 12.1 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec.Cond.000sa µMhos sampling,
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ❑YES IE NO and field acidified: ❑YES ii NO
LABORATORY INFORMATION
Date sample analyzed:11/19/2021 Laboratory Name: Environmental Chemists„ Inc Certification No. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead most ug/L
Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.09 mg/L Zn-Zinc wow mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
f Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 255 mg/L Al-Aluminum 0110s mg/L
pH(Lab)00403 5.7 units Ba-Barium 01007 ug/L
TOC 0osso 1.3 mg/L Ca-Calcium 00916 mg/L
Chloride 0094o 107 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1o02 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71so0 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 00095 pMhos K-Potassium 00937 mg/L VOC 7873 ,method#
Total Ammonia 00s10 <0 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen.NH,as N Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 0062s mg/L Ni- Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that.to the best of my knowledge and belief the.nformation submitted in this report is true.accurate.and complete.and that the laboratory analytical data was produced usrng approved methods of analysts by a
0)NR-certified laboratory. I am aware that there are s.gnificant penalties for submit4ng false mtorrratior.Including the possibtlih'of fires and imprisonment for knowing violatirns.
Shayne Lamb Corporate Secretary 'V/ L I )/
Permittee Authonzed Agent)Name and Title-Please print or type Sign, I Perm ee(or A.ent) (sate)
i
e (ora )
GW-59 Rev 06-07-2018
f
1

Environmental Chemists, Inc.
e virocJie ' , 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 I a b - 910 39:144.4 I,IN
710 Bowsertown Road,Manteo,NC 27954 • 252.473 5702 L_1b, fax
255-A Wilmington Highway,facksonvltle,NC 28540 • 910..347_S43 I aiC1=a-
ANALYTICAL&CONSULTING CHEMISTS infoldtenvironmcrtaichemists.corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-51671 Site: MW-10 11/19/2021 Water Jay Baker
Test Method Results Date Analyzed
Color color Clear 11/19/2021
Depth to water, ft. Depth to Water,Ft 12.1 feet 11/19/2021
Ammonia Nitrogen EPA 350.1,Rev 20,1993 <0 pg/L 11/30/2021
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2021
Odor Qualitative None 11/19/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 255 mg/L 11/23/2021
Temperature SM 2550 8-2010 18.6 C 11/19/2021
pH SM 4500 H 8-2011 5.7 units 11/19/2021
Total Organic Carbon (TOC) SM 5310 8-2014 1.3 mg/L 11/22/2021
1,1,1,2-Tetrachloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1,1-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1,2,2-Tetrachloroethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,1-Dichloroprope ne SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2,4-Trichlorobenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 i g/L 11/24/2021
1,2-Dibromo-3-Chloropropane SM 8200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,2-Dichiorobenzene SM 6200 8.2011 <0.5 pg/L 11/24/2021
1,2-Dichloroethane SM 8200 8-2011 <0.5 IJg/L 11/24/2021
1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
1,3,5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report# 2021-20623 Page 28 of 30

Environmental Chemists, Inc.
envirochejm 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 kac
710 Bowsertown Road,Mantro,NC 27954 • 252.471 5702 Lab?Fax
255-A Wilmington Highway,lacksonville,NC 28540 • 910 347.5843 Lab,'kr,
ANALYTICAL&CONSULTING CHEMISTS nlfoid rnvircmrnncntaichemists corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
1,3-Dichlorobenzene SM 8200 8-2011 <0.5 pg/L 11/24/2021
1,3-Dichloropropane SM 6200 B•2011 <0.5 pg/L 11/24/2021
1,4-Dichlorobenzene SM 6200 B.2011 <0.5 pg/L 11/24/2021
2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/24/2021
2-Chlorotoluene SM 8200 B-2011 <0.5 pg/L 11/24/2021
4-Chlorotoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Benzene SM 8200 B.2011 <0.5 pg/L 11/24/2021
Bromobenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromochloromethane SM 6200 B-2011 - <0.5 pg/L 11/24/2021
Bromodichloromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Bromoform SM 6200 8.2011 <0.5 pg/L 11/24/2021
Bromomethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Carbon tetrachloride SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Chloroethane SM 8200 B-2011 <0.5 pg/L 11/24/2021
Chloroform SM 6200 8-2011 <0.5 pg/L 11/24/2021
Chloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
cis-1,2-Dichloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
cis-1,3-Dichloropropane SM 8200 8.2011 <0.5 pg/L 11/24/2021
Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Dibromomethane SM 6200 8.2011 <0.5 pg/L 11/24/2021
Dichlorodifluoromethane SM 6200 8-2011 <0.5 pg/L 11/24/2021
Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Hexachlorobutadiene SM 8200 8-2011 <0.5 pg/L 11/24/2021
Isopropylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/24/2021
Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/24/2021
Naphthalene SM 6200 B-2011 <0.5 pg/L 11/24/2021
n-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/24/2021
n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Report* 2021-20623 Page 29 of 30

Environmental Chemists, Inc.
envirochern 6602 Windmill Way,Wilmington,NC 28405 • 910.392 0223 Lab • 910 392 4424 1 ix
710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/
,4
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347 5843 1...,012F,p,
ANALYTICAL&CONSULTING CHEMISTS info@envIronmentalchmists corn
Albemarle Utility Date of Report: Dec 06, 2021
862 Holiday Island Road Customer PO#:
Hertford NC 27944 Customer ID: 09110024
Attention: Report#: 2021-20623
Project ID: Monitoring Wells
ortho-Xylene SM 6200 8-2011 <0.5 pg/L 11/24/2021
p-lsopropyftoluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
sec-Butylbenzene SM 6200 9-2011 <0.5 pg/L 11/24/2021
Styrene SM 6200 8-2011 <0.5 pg/L 11/24/2021
tert-Butylbenzene SM 6200 9-2011 <0.5 pg/L 11/24/2021
Tetrachloroethene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Toluene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trans-1,2-Dichloroethene SM 8200 B-2011 <0.5 pg/L 11/24/2021
Trans-1,3-clichloropropene SM 6200 8-2011 <0.5 pg/L 11/24/2021
Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/24/2021
Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/24/2021
Vinyl chloride SM 6200 8-2011 <0.5 pg/L 11/24/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/19/2021
Chloride SM4500 CI E-2011 107 mg/L 11/24/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2 0 1993 < 0 02 mg/L 11/19/2021
Nitrate+Nitrite-Nitrogen EPA 353 2,Rev 2 0,1993 0.09 mg/L 11/24/2021
Nitrate Nitrogen Subtraction Method 0.09 mg/L 12/03/2021
Comment: I
Reviewed by: ' glUoCS0 \CibiC1/4,)
Report# 2021-20623 Page 30 of 30

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