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Home My WebLink AboutNC0031038_Analytical Results_20200914ANALYTICAL Colonial Pipeline Company John Culbreath PO Box 87 Charlotte, NC 28130 NC Certification No, 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Charlotte CRT Remediation Lab Submittal Date: 09/02/2020 Work Order: 0090048 Case Narrative 9/14/20 16:21 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: BRL MDL RPD Below Reporting Limit Method Detection Limit Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. Thls report should not be reproduced, except in Its entirety, without the written consent of WaypolntAnalytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number:1-800/529.6364 - Fax: 7041525.0409 Page 1 of 9 Sample Receipt Summary 09/14/2020 Work Order: 0090048 ANALYTICAL Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received INF EFF 0090048-01 Water 09/02/20 15:00 09/02/20 15:40 0090048-02 Water 09/02/20 15:10 09/02/20 15:40 Samples were received in good condition at 2.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical . 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Field Data Project: Charlotte CRT Remediation Laboratory Report 09/14/2020 Work Order: 0090048 Laboratory ID Client ID Field Parameter Result 0090048-01 INF 0090048-02 EFF pH Temperature (C) 6.89 28.5 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Charlotte CRT Remediation Sample Matrix: Water Laboratory Report 09/14/2020 Client Sample ID: INF Sample ID: 0090048-01 Work Order: 0090048 Time Collected: 09/02/20 15:00 Time Submitted: 09/02/20 15:40 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/7ime Batch ID Volatile Organic 601/602 Compounds by GC/MS 1,2-Dichloroethane Benzene Ethylbenzene m,p-Xylenes Methyl-tert-Butyl Ether o-Xylene Toluene Xylenes, total BRL 650 21 79 220 15 13 94 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1.0 5.0 1.0 2.0 50 1.0 1.0 3.0 0.066 0.48 0.061 0.12 0.42 0.044 0.044 0.15 10 1 10 1 *SM6200 B *SM6200 B *SM6200 B *SM6200 B *SM6200 B *SM6200 B *SM6200 B *SM6200 B 9/4/20 22:29 9/4/20 22:54 9/4/20 22:29 9/4120 22:29 9/4/20 22:54 9/4/20 22:29 9/4/20 22:29 9/4/20 22:29 JLB JLB JLB JLB JLB JLB JLB JLB P010648 P010648 P010648 P010648 P010648 P010648 P010648 P010648 Surrogate Recovery Control Limits 4-Bromofluorobenzene Dibromofluoromethane Toluene-d8 97 % 102 % 88 % 70-130 70-130 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Charlotte CRT Remediation Sample Matrix: Water Laboratory Report 09/14/2020 Client Sample ID: EFF Sample ID: 0090048-02 Work Order: 0090048 Time Collected: 09/02/20 15:10 Time Submitted: 09/02/20 15:40 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/Time Batch ID General Chemistry Parameters Total Suspended Solids Total Metals 20 mglL 2.5 0.75 1 *SM2540 D 9/8/20 15:28 ENM P010657 Lead BRL Volatile Organic 601/602 Compounds by GC/MS mg/L 0.010 0.0025 *200.7 9/3/20 14:53 JAB P010606 1,2-Dichloroethane Benzene Ethylbenzene m,p-Xylenes Methyl-tert-Butyl Ether o-Xylene Toluene Xylenes, total BRL BRL BRL BRL BRL BRL BRL BRL ug/L 1.0 0.066 1 *SM6200 B 9/4/20 14:38 JLB ug/L 0.50 0.048 1 *SM6200 B 9/4/20 14:38 JLB ug/L 1.0 0.061 1 *SM6200 B 9/4/20 14:38 JLB ug/L 2.0 0.12 1 *SM6200 B 9/4/20 14:38 JLB ug/L 5.0 0.042 1 *SM6200 B 9/4/20 14:38 JLB ug/L 1.0 0.044 1 *SM6200 B 9/4/20 14:38 JLB ug/L 1.0 0.044 1 *SM6200 B 9/4/20 14:38 JLB ug/L 3.0 0.15 1 *SM6200 B 9/4/20 14:38 JLB P010648 P010648 P010648 P010648 P010648 P010648 P010648 P010648 Surrogate Recovery Control Limits 4-Bromofluorobenzene Dibromofluoromethane Toluene-d8 98 % 102 % 86 % 70-130 70-130 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/525.0409 Page 5 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Level II QC Report 9/14/20 Project: Charlotte CRT Remediation Work Order: 0090048 Time Submitted: 9/2/2020 3:40:OOPM Volatile Organic 601/602 Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010648 - SM6200 B Blank (P010648-BLK1) Prepared & Analyzed: 09/04/20 1,2-Dichloroethane BRL 1.0 ug/L Benzene BRL 0.50 ug/L Ethylbenzene BRL 1.0 ug/L m,p-Xylenes BRL 2.0 ug/L Methyl-tert-Butyl Ether BRL 5.0 ug/L o-Xylene BRL 1.0 ug/L Toluene BRL 1.0 ug/L Xylenes, total BRL 3.0 ug/L Surrogate:4-Bromofluorobenzene 48.0 ug/L 50.00 96 70-130 Surrogate: Dibromoftuoromefhane 51.1 ug/L 50.00 102 70-130 Surrogate: Toluene-d8 44.0 ug/L 50.00 88 70-130 LCS (P010648-BS1) Prepared & Analyzed: 09/04/20 1,2-Dichloroethane 24.9 1.0 ug/L 20.00 125 70-130 Benzene 20.8 0.50 ug/L 20.00 104 70-130 Ethylbenzene 18.8 1.0 ug/L 20.00 94 70-130 m,p-Xylenes 39.9 2.0 ug/L 40.00 100 70-130 Methyl-tert-Butyl Ether 23.7 5.0 ug/L 20.00 119 70-130 o-Xylene 19.6 1.0 ug/L 20.00 98 70-130 Toluene 21.8 1.0 ug/L 20.00 109 70-130 Xylenes, total 59.5 3.0 ug/L 60.00 99 70-130 Surrogate: 4-Bromofluorobenzene 49.8 ug/L 50.00 100 70-130 Surrogate: Dibromofluoromethane 52.1 ug/L 50.00 104 70-130 Surrogate: Toluene-d8 43.8 ug/L 50.00 88 70-130 This report should not be reproduced, except In its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Total Metals - Quality Control Level II QC Report 9/14/20 Project: Charlotte CRT Remediation Work Order: 0090048 Time Submitted: 9/2/2020 3:40:OOPM Reporting Spike Source %REC RPD Anaiyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010606 - 200.7 Blank (P010606-BLK1) Prepared & Analyzed: 09/03/20 Lead BRL 0.010 mg/L Blank (P010606-BLK2) Prepared & Analyzed: 09/03/20 Lead BRL 0.010 mg/L LCS (P010606-BS1) Prepared & Analyzed: 09/03/20 Lead Matrix Spike (P010606-MS1) Lead Matrix Spike Dup (P010606-MSD1) 0.510 0.010 mglL 0.5001 102 85-115 Source: 0090048-02 Prepared & Analyzed: 09/03/20 0.507 0.010 mg/L 0.5001 BRL 101 70-130 Source: 0090048-02 Prepared & Analyzed: 09/03/20 Lead 0.507 0.010 mg/L 0.5001 BRL 101 70-130 0.008 10 This report should not be reproduced, except In its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 9 Level II QC Report 9/14/20 ANALYTICAL Colonial Pipeline Company Project: Charlotte CRT Remediation Work Order: 0090048 Attn: John Culbreath Time Submitted: 9/2/2020 3:40:OOPM PO Box 87 Charlotte, NC 28130 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010657 - NO PREP Blank (P010657-BLK1) Prepared & Analyzed: 09/08/20 Total Suspended Solids Prep Method: 200.7 Lab Number BRL 5.0 mg/L Sample Extraction Data Batch Initial Final DatefTime 0090048-02 Prep Method: SM6200 B Lab Number P010606 50 mL 50 mL 09/03/20 7:24 Batch initial Final Date/Time 0090048-01 P010648 10 mL 10 mL 09/04/20 10:00 0090048-01 P010648 10 mL 10 mL 09/04/20 10:00 0090048-02 P010648 10 mL 10 mL 09/04/20 10:00 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. 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