NC0031038_Analytical Results_20200622

Colonial Pipeline Company
John Culbreath
PO Box 87
Charlotte, NC 28130
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Charlotte CRT Remediation
Lab Submittal Date: 06/08/2020
Work Order: 0060878
Case Narrative
6/22/20 12:58
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
BRL
MDL
RPD
Below Reporting Limit
Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 10

Sample Receipt Summary
06/22/2020
Work Order: 0060878
Client Sample ID
Lab Sample ID Matrix Date/Time Sampled Date/Time Received
EFF
INF
0060878-01
0060878-02
Water
Water
06/08/20 13:00
06/08/20 13:10
06/08/20 13:45
06/08/20 13:45
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
Field Data
Project: Charlotte CRT Remediation
Laboratory Report
06/22/2020
Work Order: 0060878
Laboratory ID
0060878-01
Client ID
EFF
Field Parameter Result
pH
Temperature (C)
0060878-02 INF
7.15
28.3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road • P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
Project: Charlotte CRT Remediation
Sample Matrix: Water
Laboratory Report
06/22/2020
Client Sample ID: EFF
Sample ID: 0060878-01
Work Order: 0060878
Time Collected: 06/08/20 13:00
Time Submitted: 06/08/20 13:45
Parameter
Result
Units
Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
General Chemistry Parameters
Total Suspended Solids
Total Metals
BRL
mg/L
2.5 0.75 1 *SM2540 D 6/10/20 10:41 ENM P0F0885
Lead
BRL
Volatile Organic 601/602 Compounds by GC/MS
mg/L 0.010 0.0025 1 *200.7 6/11/20 17:39 JAB P0F0857
1,2-Dichforoethane
Benzene
Ethylbenzene
m,p-Xylenes
Methyl-tert-Butyl Ether
o-Xylene
Toluene
Xylenes, total
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ug/L 1.0 0.066 1 *SM6200 B 6/9/20 15:42 JLB
ug/L 0.50 0.048 1 *SM6200 B 6/9/20 15:42 JLB
ug/L 1.0 0.061 1 *SM6200 B 6/9/20 15:42 JLB
ug/L 2.0 0.12 1 *SM6200 B 6/9/20 15:42 JLB
ug/L 5.0 0.042 1 *SM6200 8 6/9/20 15:42 JLB
ug/L 1.0 0.044 1 *SM6200 B 6/9/20 15:42 JLB
ug/L 1.0 0.044 1 *SM6200 B 6/9/20 15:42 JLB
ug/L 3.0 0.15 1 *SM6200 B 6/9/20 15:42 JLB
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
Surrogate
Recovery
Control Limits
4-8romofluorobenzene
Dibromofluoromethane
Toluene-d8
91 %
92 %
95 %
70-130
70-130
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
Project: Charlotte CRT Remediation
Sample Matrix: Water
Laboratory Report
06/22/2020
Client Sample ID: INF
Sample ID: 0060878-02
Work Order: 0060878
Time Collected: 06/08/20 13:10
Time Submitted: 06/08/20 13:45
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
Volatile Organic 601/602 Compounds by GC/MS
1,2-Dichloroethane
Benzene
Ethylbenzene
m,p-Xylenes
Methyl-tert-Butyl Ether
o-Xylene
Toluene
Xylenes, total
BRL ug/L 1.0 0.066 1 *SM6200 B 6/9/20 16:06 JLB
19 ug/L 0.50 0.048 1 *SM6200 B 6/9/20 16:06 JLB
BRL ug/L 1.0 0.061 1 *SM6200 B 6/9/20 16:06 JLB
44 ug/L 2.0 0.12 1 *SM6200 B 6/9/20 16:06 JLB
170 ug/L 50 0.42 10 *SM6200 B 6/10/20 18:53 JLB
12 ug/L 1.0 0.044 1 'SM6200 B 6/9/20 16:06 JLB
1.6 ug/L 1.0 0.044 1 *SM6200 B 6/9/20 16:06 JLB
56 ug/L 3.0 0.15 1 *SM6200 B 6/9/20 16:06 JLB
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
P0F0878
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8
92 %
94 %
93 %
70-130
70-130
70-130
This report should not be reproduced, except in Its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
Level II QC Report
6/22/20
Project: Charlotte CRT Remediation Work Order: 0060878
Time Submitted: 6/8/2020 1:45:OOPM
Volatile Organic 601/602 Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0878 - SM6200 B
Blank (P0F0878-BLK1) Prepared & Analyzed: 06/09/20
1,2-Dichloroethane BRL 1.0 ug/L
Benzene BRL 0.50 ug/L
Ethylbenzene BRL 1.0 ug/L
m,p-Xylenes BRL 2.0 ug/L
Methyl-tert-butyl Ether BRL 5.0 ug/L
o-Xylene BRL 1.0 ug/L
Toluene BRL 1.0 ug/L
Xylenes, total BRL 3.0 ug/L
Surrogate: 4-Bromofluorobenzene 46.4 ug/L 50.00 93 70-130
Surrogate: Dibromofluoromethane 46.4 ug/L 50.00 93 70-130
Surrogate: Toluene-d8 46.1 ug/L 50.00 92 70-130
LCS (P0F0878-BS1) Prepared & Analyzed: 06/09/20
1,2-Dichloroethane 19.6 1.0 ug/L 20.00 98 70-130
Benzene 21.9 0.50 ug/L 20.00 110 70-130
Ethylbenzene 20.4 1.0 ug/L 20.00 102 70-130
m,p-Xylenes 42.9 2.0 ug/L 40.00 107 70-130
Methyl-tert-butyl Ether 21.4 5.0 ug/L 20.00 107 70-130
o-Xylene 20.4 1.0 ug/L 20.00 102 70-130
Toluene 22.0 1.0 ug/L 20.00 110 70-130
Xylenes, total 63.3 3.0 ug/L 60.00 106 70-130
Surrogate: 4-Bromofluorobenzene 48.4 ug/L 50.00 97 70-130
Surrogate: Dibromofluoromethane 45.1 ug/L 50.00 90 70-130
Surrogate: Toluene-d8 47.9 ug/L 50.00 96 70-130
Matrix Spike (P0F0878-MS1)
Source: 0060878-01 Prepared & Analyzed: 06/09/20
1,2-Dichloroethane 199 10 ug/L 200.0 BRL 100 70-130
Benzene 226 5.0 ug/L 200.0 BRL 113 70-130
Ethylbenzene 208 10 ug/L 200.0 BRL 104 70-130
m,p-Xylenes 441 20 ug/L 400.0 BRL 110 70-130
Methyl-tert-Butyl Ether 220 50 ug/L 200.0 BRL 110 70-130
o-Xylene 204 10 ug/L 200.0 BRL 102 70-130
Toluene 226 10 ug/L 200.0 BRL 113 70-130
Xylenes, total 645 30 ug/L 600.0 BRL 108 70-130
Surrogate:4-Bromofluorobenzene 45.8 ug/L 50.00 92 70-130
Surrogate: Dibromofluoromethane 45.4 ug/L 50.00 91 70-130
Surrogate: Toluene -dB 47.9 ug/L 50.00 96 70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypolnt Analytical.
449 Springbrook Road • P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1.800/529-6364 - Fax: [phone]
Page 6 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
Level II QC Report
6/22/20
Project: Charlotte CRT Remediation Work Order: 0060878
Time Submitted: 6/8/2020 1:45:OOPM
Volatile Organic 601/602 Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0878 - SM6200 B
Matrix Spike Dup (P0F0878-MSD1) Source: 0060878-01 Prepared & Analyzed: 06/09/20
1,2-Dichloroethane 201 10 ug/L 200.0 BRL 101 70-130 1 20
Benzene 220 5.0 ug/L 200.0 BRL 110 70-130 3 20
Ethylbenzene 200 10 ug/L 200.0 BRL 100 70-130 4 20
m,p-Xylenes 425 20 ug/L 400.0 BRL 106 70-130 4 20
Methyl-tert-Butyl Ether 233 50 ug/L 200.0 BRL 116 70-130 6 20
o-Xylene 199 10 ug/L 200.0 BRL 99 70-130 3 20
Toluene 228 10 ug/L 200.0 BRL 114 70-130 0.8 20
Xylenes, total 624 30 ug/L 600.0 BRL 104 70-130 3 20
Surrogate:4-Bromof!uorobenzene 46.8 ug/L 50.00 94 70-130
Surrogate: Dibromofuoromethane 46.0 ug/L 50.00 92 70-130
Surrogate: Toluene-d8 48.2 ug/L 50.00 96 70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road • P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
Total Metals - Quality Control
Level II QC Report
6/22/20
Project: Charlotte CRT Remediation Work Order: 0060878
Time Submitted: 6/8/2020 1:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0857 - 200.7
Blank (P0F0857-BLK1)
Prepared: 06/09/20 Analyzed: 06/11/20
Lead
BRL 0.010 mg/L
Blank (P0F0857-BLK2) Prepared: 06/09/20 Analyzed: 06/10/20
Lead
BRL 0.010 mg/L
LCS (P0F0857-BS1) Prepared: 06/09/20 Analyzed: 06/11/20
Lead
0.519 0.010 mg/L 0.5001 104 85-115
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 10

ANALYTICAL
Colonial Pipeline Company
Attn: John Culbreath
PO Box 87
Charlotte, NC 28130
General Chemistry Parameters - Quality Control
Level II QC Report
6/22/20
Project: Charlotte CRT Remediation Work Order: 0060878
Time Submitted: 6/8/2020 1:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0885 - NO PREP
Blank (P0F0885-BLK1)
Prepared & Analyzed: 06/10/20
Total Suspended Solids BRL 5.0 mg/L
LCS (P0F0885-BSI)
Prepared & Analyzed: 06/10/20
Total Suspended Solids 490 5.0 mg/L 477.0 104 90-110
Sample Extraction Data
Prep Method: 200.7
Lab Number Batch Initial Final Date/Time
0060878-01
Prep Method: SM6200 B
Lab Number
P0F0857 50 mL 50 mL 06/09/20 7:48
Batch Initial Final Date/Time
0060878-01 P0F0878 10 mL 10 mL 06/09/20 10:00
0060878-02 P0F0878 10 mL 10 mL 06/09/20 10:00
0060878-02 P0F0878 10 mL 10 mL 06/09/20 10:00
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529.6364 - Fax: [phone]
Page 9 of 10

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