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Home My WebLink AboutNC0031038_Analytical Results_20200420ANALYTICAL Colonial Pipeline Company John Culbreath PO Box 87 Charlotte, NC 28130 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Charlotte CRT Remediation Lab Submittal Date: 03/24/2020 Work Order: 0030327 Case Narrative 4/2/20 16:26 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: BRL MDL RPD Below Reporting Limit Method Detection Limit Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 9 Sample Receipt Summary 04/02/2020 Work Order: 0030327 ANALYTICAL Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received EFF INF 0030327-01 0030327-02 Water 03/24/20 11:25 03/24/20 16:35 Water 03/24/20 11:30 03/24/20 16:35 Samples were received in good condition at 2.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525.0409 Page 2 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Field Data Project: Charlotte CRT Remediation Laboratory Report 04/02/2020 Work Order: 0030327 Laboratory ID Client ID Field Parameter Result 0030327-01 EFF pH Temperature (C) 0030327-02 INF 7.10 15.8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical . 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 704/525-0409 Page 3 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Charlotte CRT Remediation Sample Matrix: Water Laboratory Report 04/02/2020 Client Sample ID: EFF Sample ID: 0030327-01 Work Order: 0030327 Time Collected: 03/24/20 11:25 Time Submitted: 03/24/20 16:35 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/Time Batch ID General Chemistry Parameters Total Suspended Solids Total Metals BRL mg/L 2.5 0.70 1 *SM2540 D 3/26/20 9:51 ENM P000517 Lead BRL Volatile Organic 601/602 Compounds by GC/MS mg/L 0.010 0.0030 1 *200.7 3/27/20 16:16 JAB P000531 1,2-Dichloroethane Benzene Ethylbenzene m,p-Xylenes Methyl-tert-Butyl Ether o-Xylene Toluene Xylenes, total BRL BRL BRL BRL BRL BRL BRL BRL ug/L 1.0 0.066 1 *SM6200 B 3/26/20 17:10 JLB ug/L 0.50 0.048 1 *SM6200 B 3/26/20 17:10 JLB ug/L 1.0 0.061 1 *SM6200 B 3/26/20 17:10 JLB ug/L 2.0 0.12 1 *SM6200 B 3/26/20 17:10 JLB ug/L 5.0 0.042 1 *SM6200 B 3/26120 17:10 JLB ug/L 1.0 0.044 1 *SM6200 B 3/26/20 17:10 JIB ug/L 1.0 0.044 1 *SM6200 B 3/26/20 17:10 JLB ug/L 3.0 0.15 1 *SM6200 B 3/26/20 17:10 JLB P000538 P000538 P000538 P000538 P000538 P000538 P000538 P000538 Surrogate Recovery Control Limits 4-Bromofluorobenzene Dibromofluoromethane Toluene-d8 102 % 101 % 99 % 70-130 70-130 70-130 This report should riot be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 9 Ethylbenzene m,p-Xylenes Methyl-tert-Butyl Ether o-Xylene Toluene Xylenes, total ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Charlotte CRT Remediation Sample Matrix: Water Laboratory Report 04/02/2020 Client Sample ID: INF Sample ID: 0030327-02 Work Order: 0030327 Time Collected: 03/24/20 11:30 Time Submitted: 03/24/20 16:35 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/Time Batch ID Volatile Organic 601/602 Compounds by GC/MS 1,2-Dichloroethane BRL Benzene 61 4.3 16 97 3.7 1.6 20 ug/L 1.0 0.066 1 *SM6200 B 3/26/20 17:35 JLB uglL 0.50 0.048 1 *SM6200 B 3/26/20 17:35 JLB ug/L 1.0 0.061 1 *SM6200 B 3/26/20 17:35 JLB ug/L 2.0 0.12 1 *SM6200 B 3/26/20 17:35 JLB ug/L 5.0 0.042 1 *SM6200 B 3/26/20 17:35 JLB ug/L 1.0 0.044 1 *SM6200 B 3/26/20 17:35 JLB uglL 1.0 0.044 1 *SM6200 B 3/26/20 17:35 JLB ug!L 3.0 0.15 1 *SM6200 B 3/26/20 17:35 JLB P000538 P000538 P000538 P000538 P000538 P000538 P000538 P000538 Surrogate Recovery Control Limits 4-Bromofluorobenzene Dibromofluoromethane Toluene-d8 103 % 101 % 99 % 70-130 70-130 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1.800/529.6364 - Fax: 704/525-0409 Page 5 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Level II QC Report 4/2/20 Project: Charlotte CRT Remediation Work Order: 0030327 Time Submitted: 3/24/2020 4:35:OOPM Volatile Organic 601/602 Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P000538 - 5030B Blank (P0C0538-BLK1) Prepared & Analyzed: 03/26/20 1,2-Dichloroethane BRL 1.0 ug/L Benzene BRL 0.50 ug/L Ethylbenzene BRL 1.0 ug/L m,p-Xylenes BRL 2.0 ug/L Methyl-tert-Butyl Ether BRL 5.0 ug/L o-Xylene BRL 1.0 ug/L Toluene BRL 1.0 ug/L Xylenes, total BRL 3.0 ug/L Surrogate: 4-Bromofluorobenzene 51.2 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 51.0 ug/L 50.00 102 70-130 Surrogate: Toluene-d8 49.5 ug/L 50.00 99 70-130 LCS (P000538-BS1) Prepared & Analyzed: 03/26/20 1,2-Dichloroethane 16.4 1.0 ug/L 20.00 82 70-130 Benzene 17.1 0.50 ug/L 20.00 86 70-130 Ethylbenzene 16.8 1.0 ug/L 20.00 84 70-130 m,p-Xylenes 34.4 2.0 ug/L 40.00 86 70-130 Methyl-tert-Butyl Ether 17.1 5.0 ug/L 20.00 85 70-130 o-Xylene 17.2 1.0 ug/L 20.00 86 70-130 Toluene 17.1 1.0 ug/L 20.00 86 70-130 Xylenes, total 51.6 3.0 ug/L 60.00 86 70-130 Surrogate: 4-Bromofluorobenzene 51.1 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 50.7 ug/L 50.00 101 70-130 Surrogate: Toluene-d8 49.6 ug/L 50.00 99 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Total Metals - Quality Control Level II QC Report 4/2/20 Project: Charlotte CRT Remediation Work Order: 0030327 Time Submitted: 3/24/2020 4:35:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P000531 - 200.7 Blank (P0C0531-BLK1) Prepared & Analyzed: 03/27/20 Lead BRL 0.010 mg/L Blank (P0C0531-BLK2) Prepared & Analyzed: 03/27/20 Lead BRL 0.010 mg/L LCS (P0C0531-BS1) Prepared & Analyzed: 03/27/20 Lead Matrix Spike (P0C0531-MS1) Lead Matrix Spike Dup (P0C0531-MSD1) 0.481 0.010 mg/L 0.5001 96 85-115 Source: 0030327-01 Prepared & Analyzed: 03/27/20 0.480 0.010 mglL 0.5001 0.00547 95 70-130 Source: 0030327-01 Prepared & Analyzed: 03/27/20 Lead 0.478 0.010 mg/L 0.5001 0.00547 94 70-130 0.3 20 This report should not be reproduced, except in Its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-800/529.6364 - Fax: 704/525-0409 Page 7 of 9 ANALYTICAL Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 General Chemistry Parameters - Quality Control Level II QC Report 4/2/20 Project: Charlotte CRT Remediation Work Order: 0030327 Time Submitted: 3/24/2020 4:35:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P000517 - NO PREP Blank (P0C0517-BLKI) Prepared & Analyzed: 03/26/20 Total Suspended Solids BRL 5.0 mg/L LCS (P0C0517-BSI) Prepared & Analyzed: 03/26/20 Total Suspended Solids 440 5.0 mg/L 477.0 93 90-110 Sample Extraction Data Prep Method: 200.7 Lab Number Batch Initial Final Date/Time 0030327-01 Prep Method: 5030B Lab Number P000531 50 mL 50 mL 03/27/20 7:53 Batch Initial Final Daternme 0030327-01 0030327-02 P000538 P000538 10 mL 10 mL 10 mL 10 mL 03/26/20 10:00 03/26/20 10:00 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529.6364 - Fax: 704/525-0409 Page 8 of 9 0 rn 0 m P' 0 - 0 0 0. 0 la I 0 I Fa- 0 tP) NPUES: 10 NC 0 SC method ot Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATIOt il TO THE LAI30 RY. COC Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. If 0 Fed Ex EJ UPS Q Hand,dellvered \aynoint Mnlytical Fieki S °Nice _ LI Other .............__ - -- — — - (iienletIBIR) :As reusinbudem . . . 6 Upon relinquishing, this dgain of Custody WITour authorization for Waypoint Analytical to proceed witg the analyses as requested above. Any changes m submitted in writing to the Waypoint Analytical Project Manager. There will be charges for any changes afteranalyses have been initialized. Sampler's Signature CLIENT SAMPLE DESCRIPTION I-110FM tax (TeS)(No): Purchase Order No./Billing Reference Email Address: Requested Due Date 0 1 Day 0 2 Days 0 3 Days 04 Days 0 5 Days EDD Type: PDF Excel Other "Working Days" 0 6-9 Days 0 Standard 10 days Ruth Work Must Be Pre Approved Site Location Name: Samples received after 14:00 will be processed next business day, Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) UST: 0 NC OSC _ III TIME DATE ; COLLECTED COLLECTED 1 MILITARY HOURS ORpONDWATER1 DRIP+, 0 NC C3 SC UN( Sampled By (Print Name) 7"))7-11 /476V, MATRIX SAMPLE CONTA (SOIL, WATER, OR *TYPE NO. SLUDGE) SEE BELOW [ Received For Waypoint Analytical EY: / (111 Date 10 iiui IUIL Ics2.) W i SOLID WASTE: 0 NC 0 SC O RCRA: BRWNFLD LANDFILL I 0 NC CI SC Ca NC 0 SC 0 NC 0 SC 0 ' n W d < m m m m 73 < l''' Affiliation 442 K#1 ANALYSIS REQUESTED / / r::/Y/‘), tr) REMARKS ID NO. OTHER: 0 NC 0 SC TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC FL NC SC OTHER NIA Water Chlorinated: YES NO Sample Iced Upon Collection: YES1.---1(10 fi -.g Additional Comments: Site Arrival Time: Site Departure Time: Field Tech Fae: Mileage: SEE RevERsE FOR TERMS a conorrioNs 73 73 0 RI . .0v o o 0 0 .03 z 2 z p 3 Po• ' cl° > * 0.< -I w m UEL: 0 0"D Sq, -I 7 > Z P tri -I Fa, --&- ca 3 m a E o sy °/ • 0.< -• a 0 al 0 •D .0 e c cf, fiT • CD z a g-9- n c 5 a) ua 0-' o s lrlr-1111--'-z--'4" Page 9 of 9 ,..z.