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Facility Name- PERMIT it: EXPIRATION DAT 9.
Name (if dip..arent): i"v
Facility Address: t. `1- (k c"rk l',6 ,� i NPDES
�-'E 2xr,\A ttiiy) �• slot _ ) 42} Zia 4 County ��C'�4 TYPE OF PERMUTED OPERATION BEING MOTORED
Contact Person: a �•Y> c'}xr�_ Telephone#: -gel
Lagoon Rernedatlorr Infiltration Gallery
_
--Vtiesi- to tion Site-Na '�o_ofWells o -Sar,tpr Field- Rerr lar_ —
' Rotary Distributor Land Applicationof Sludge
Welt l:ertifidatiorn Number(Worn Permit): M\KYO I For Groundwater Treatment Systems I - Other:
Well Depth- ' (o K ft- Well Diameter: [�h„ it rr: I
S>a-ee, ed n ar.. -- Zit-- NOTE lues s -- - of --d -
�,^ �_j[tfiuent_(98 . "� � _�hourdretlect dtss veo an _
Depth to Water tc,v61: - -mac:ieI& .T:..asur1 :wait. a - -.
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Et ; i ri.IIue33r (`u9) colloidal concentrations_
Measuring Point is c�2 ft_above land surface. / r
Gallons ofwaterpurnped/bailed_before_sam ---- j_-Date�ampfe-collected l 2 - Date sam 112a z `�'/
sampling: - 1 ' .,�, -�11►�1 nl5 ,
Field analysis: pH , Specific Conductance uMhos ! LaboratoryName: __lfrV\CClYiY�r�4.X1 ,Temp. 'C,Odor Appearance I Certification No._ 31(129---
PARAMETERS(Samples for metals were collected unfiltered YES NO end field acIdified YES NO)
COD mg/I Nitrite (NO2) as N mg/1 Ni-Nickel mg/i
Coliiorm: MF Fecal /100m1 Nitrate (NO3) as N ma/I __- -I earl' ;print_
colrrorm-MF-rotai- --1100m osphorus: Total as P mg/ Zn-Zinc mg/I
(Note:Use MPH method for highly turbid samples) Orthophosphate KI'd mg/I Ammonia Nitrogen fng/i
Dissolved_Solids:Total mg/I Al-Aluminum mg/l Other(Specify Compounds and Concentration Units)
pH (when analyzed) units Ba-Barium MAR 2 3 2022 mg/1
TOG mail Ca-Calcium mg/I —MIN NI!'j
hbi ide mg/i Cci-Cadmium mg/I i 7 r/W 7/'1'/ T'
Arsenic mn Chromium:Total �r
y/l v..rv....u....Tvt�i, Il lg/,
G ease and Oils mg/I Cu-Copper �` m jil t/'��T=��
Phenol
mnA G n-Irnny. - larstf r' rigs/. OF•GAN v : (GC.GC/MS,H
r_S Iif:te rigA, rI -Mercury
MO (Specify test and method tech lab repori-i
Specific Conductance
Total uMhos K-Potassium 1:� f:i ,i mg/I ¢2annr:A:' 4aor1? Yes (I} n
r otal Ammonia mn i Mg Magnesium m 2:;1,i-;r 2, .w_ •• c 1 all
z•�� �,. w,, �- Mn -a~,.ag.resLir r, g/i 1/tJC : method#>;
K3- :- mg/i M -Manganese mg/I : method#>Q
method#
certify tftt�to the best cf—my knowledge andbelief,the information submitted In_this report is true,accurate,and complete,and that the laboratory analytical datawas-produced
sin a••loved methods of Gnat s sby&No fhC4Niaa.-OJAtQ-(fotzerly,DE }teri+f laborata - _ - r• 1 I -- is_1i nt-i T„ .. fq4n off-- 0-.44
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- ' Environmental Chemists, inc.
\l 4' 5� 4: c em •' 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
' ' I 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax •
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L s 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan F•-•' Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-52253 Site: MW-3 11/23/2021 9:25 AM Water Kevin Stanley
Test Method Results Date Analyzed
- ��
Ammonia Nitrogen EPA350.1,Rev.2.0,1993 < 0.2 mg/L 12/01/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 193 mg/L 11/24/2021
Total Phosphorus SM 4500 P(F-H)-2011 1.48 mg/L 12/01/2021
Total Organic Carbon (TOC) SM 5310 B-2014 2.6 mg/L 11/29/2021
1,1,1,2 Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichlorobenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloroethane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2,2-Dichloropropane SM 6200 C-2011 E-MAILED DEC 0 6 2021 < 0.50 pg/L 11/30/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
.---_
Report#.. 2021-20833 Page 1 of 12

I Environmental Chemists, Inc.
1 , `� f � 1 i
1 5Qc1iem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
fir', r sM 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
k 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroethane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
M+P Xylene sM 6200 C-2011 < 1.00 pg/L 11/30/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
n-Butylbenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
p-lsopropyltoluene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Report#.. 2021-20833 Page 2 of 12

re• Environmental Chemists, Inc.
CiL1 yvi `*chen , 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
• 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
h , 1'
255-A Wilmington Highway,lmin Hi Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
g g
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Toluene SM 6200 C-2011 < 0.50 ug/L 11/30/2021
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,3-dichloropropene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Vinyl chloride SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/23/2021
Chloride SM4500 CI E-2011 19 mg/L 11/26/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 11/24/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0, 1993 0.13 mg/L 11/29/2021
Nitrate Nitrogen Subtraction Method 0.08 mg/L 12/03/2021
--
Report#.. 2021-20833 Page 3 of 12

Environmental Chemists, Inc.
r
r u l irochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
• .; s"' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-522 Site: MW-5 11/23/2021 9:15 AM Water Kevin Stanley
Test Method Results Date Analyzed
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.7 mg/L 12/01/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 504 mg/L 11/24/2021
Total Phosphorus SM 4500 P(F-H)-2011 6.48 mg/L 12/02/2021
Total Organic Carbon (TOC) SM 5310 B-2014 23.0 mg/L 11/29/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1.1,2,2-Tetrachloroethane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trichlorobenzene SM 5200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dibromoethane SM 6200 c-2011 < 0.50 jg/L 11/30/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichloropropane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Report# 2021-20833
Page 4 of 12

Environmental Chemists, Inc.
L1 115s oehem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax -
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
," SM' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromochloromethane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 11/30/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Styrene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
E2epoit# 2021-20833 Page 5 of 12

,
i, ,
:l3 Environmental Chemists, Inc.
'
1 i1 n. 1r`; bchem i"; 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
4 I sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,3-dichloropropene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichloroethene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Fecal Coliform SM9222D-2015MF <1 Colonies/100mL 11/23/2021
Chloride SM4500 CI E-2011 122 mg/L 11/26/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/24/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.07 mg/L 11/29/2021
Nitrate Nitrogen Subtraction Method 0.07 mg/L 12/03/2021
Report# 2021-20833 Page 6 of 12

- } ,' Environmental Chemists, Inc.
6602 Windmill Way,Wilmington,ton,NC 28405 • 910.392.0223 Lab o 910.392.4424 Fax •
(`�+ � � "I��`OC�1e111 �
s`:P 3 i 1 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
.: SM,
= , 1 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Lab ID mple ID: Collect Date/Time Matrix Sampled by
21-52255 Site: MW-6 11/23/2021 9:05 AM Water Kevin Stanley
T st _Method Results Date Analyzed
Ammonia Nitrogen EPA 350.1,Rev.2.0, 1993 1.2 mg/L 12/01/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 501 mg/L 11/24/2021
Total Phosphorus SM 4500 P(F-H)-2011 9.10 mg/L 12/02/2021
Total Organic Carbon (TOC) SM 5310 B-2014 28.4 mg/L 11/29/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichloropropane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1.2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
--
Report# 2021-20833 Page 7 of 12

Aa Environmental Chemists, Inc.
i rr ra
Q Iochem ; '' 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax •
' : ' 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
• sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromociichloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,2 Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromochloromethane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 11/30/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
n-Butylbenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
p-Isopropyltoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
sec-Butylbenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Styrene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
tert-Butylbenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Report# 2021-20833 Page 8 of 12

1 t, Environmental Chemists, Inc.
°1 r ii ochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax •
tip 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
2`� sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,3-dichloropropene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/23/2021
Chloride SM4500 CI E-2011 108 mg/L 11/26/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/24/2021
Nitrate+Nitrite-Nitrogen EPA353.2,Rev.2.0,1993 0.05 mg/L 11/29/2021
Nitrate Nitrogen Subtraction Method 0.05 mg/L 12/03/2021
-
1?er ort# 2021-20833 Page 9 of 12

�� Environmental Chemists, Inc.
at
r.
1. N if7 ,; of he it I 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
•
'11 !' 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
S_ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
Lab I Sample ID: Collect Date/Time Matrix Sampled by
21-5 256 Site: MW-7 11/23/2021 8:55 AM Water Kevin Stanley
Te Method Results Date Analyzed
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 < 0.2 mg/L 12/01/2021
Total Dissolved Solids (TDS) SM 2540 C-2015 180 mg/L 11/24/2021
Total Phosphorus SM 4500 P(F-H)-2011 2.39 mg/L 12/02/2021
Total Organic Carbon (TOC) SM 5310 B-2014 17.8 mg/L 11/29/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,1-Dichloropropene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichlorobenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trichlorobenzene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 ig/L 11/30/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
12-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
1.3-Dichloropropane SM 6200 c-2011 < 0.50 pg/L 11/30/2021
1 4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
2 Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Report# 2021-20833 Page 10 of 12

,
h_ Environmental Chemists, Inc.
t_}I ,� octieln 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax '
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
M' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Benzene SM 6200 C-2011 < 0.50 ug/L 11/30/2021
Bromobenzene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
lsopropylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 11/30/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
ortho-Xylene SM 6200 c-2011 < 0.50 pg/L 11/30/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Report# 2021-20833 ��- Page 11 of 12

ii, Environmental Chemists, Inc.
a£A �R
! _.aid � �{ 1
�.4EN:J4�o heir 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax •
' , 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
` '' �� _ - 0255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Dec 06, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20833
Project ID: Cape Royal Dolphin MW
T etrachloroethene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Toluene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,2-Dichloroethene sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trans-1,3-dichloropropene sM 6200 c-2011 < 0.50 pg/L 11/30/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 11/30/2021
Vinyl chloride sM 6200 C-2011 < 0.50 pg/L 11/30/2021
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/23/2021
Chloride SM4500 CI E-2011 24 mg/L 11/26/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/24/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0, 1993 0.03 mg/L 11/29/2021
Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/03/2021
Comment: ��
Reviewed by: � �IQ-.
Report#:, 2021-20833 Page 12 of 12