WQ0001861_Monitoring - 02-2022_20220328

S& Soil & Environmental Consultants, PA
EC 8412 fells of Neuse Road,Suite 1U4,Raleigh,NC 27615•Phone: [phone]• lax: [phone]
sandec.com
March 18, 2022
S&EC Project # 1061
NC Department of Environmental Quality
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
To Whom it May Concern:
Soil &Environmental Consultants, PA has completed the groundwater monitoring well sampling
process for Gregory Poole Equipment Company, Leland facility. The enclosed information is in
reference to permit number WQ0001861.
Enclosed are the completed GW-59 groundwater monitoring compliance report forms for each
monitoring well, plus the laboratory data.
If you have any questions or require additional information then please call.
Sincerely y>
Soil & Environmental Consultants, PA
O /J � o0
Donald L. Wells, Hydrologist =yJ v
NC Licensed Soil Scientist ,
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GW-59A COMPLIANCE REPORT FORM Permit# hJ G2 000 Ifni
•
(Submit one each monitoring period with GFV.59 forms.)
1 Enter date monitoring results were due.( 3-zL ) Will this monitoring report(GW-59 and GW-59A) YES NO
be submitted after the established due date?
2 Was any required information missing on the GW-59 report forms? YES NO
iF the answer to question 1 or 2 is"YES",list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?If the answer is "Yes",contact the Regional Office for guidance.
4 Are any monitored constituents equal to or above the established standards? YES NO
If the answer to question 4 is"NO", skip to section 8.
If the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below: /r
5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO
same constituent(s)in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES';list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years).
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO
if the answer is "YES';a groundwater quality problem may be occurring.CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is"NO'; monitoring wells maybe improperly
located;contact the Regional Office.
7 Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem?
if the answer to question 7 is"YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines,and/or penalties.
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above Information was evaluated and the Informationvsubmitted this'
report(Compliance Report GW-59A)is true and complete to''the.beat my.knowledge
3-/g-z z
Signature of Permittee(or Authorized Agent) Date
GW-59A 12/8/2003

•
SUBMIT FORM ON YELLOW PAPER ONLY
Mail original bEPA01ENNT"OFii yy,12,NMENi,&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy to• VS1PNpF)wAT,I;R;nauAl"IT,);ikFORMATION°PftOcf=SSINCf UNIT, ;,
COMPLIANCE REPORT FORM : 1 N7gJN/11';SiR, d—E-ilCENTER iRALEIGHr Nc.27698.1817. Phone..(919)'733.=3221 -
FACILITY INFORMATIONPlease Print Clearly or Type PERMIT Number: Expiration Date:
Facility Name: Grey/ P,�(e EiIw�p..4- t, s%p.v.�/ Non-Discharge W a 000 /86/ UIC
Permit Name(if different): ✓ // r NPDES Other
Facility Address: FSl 8tve X A , toot I TYPE OF PERMITTED OPERATION BEING MONITORED
Lela«d (StheOt) NC 711gs/ County 8rrsosw..•tX ei(Lagoon ❑Remediation: Infiltration Gallery
tc+rl ',AA (Satre) (zip) El Spray Field El Remediation:
Contact Person: /v1 r. 14vi- 4(.. tk 7Li- Telephone#: 2 Q-•/41/-ill/ ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: ? ❑ Water Source Heat Pump El Other.
(from Permit)
SAMPLING INFORMATION A/���W� If WELL
WELL ID NUMBER(from Permit): 'Z Date sample collected: 2- tt- tZ FIELD ANALYSES: • WAS •
• Well Depth: 21.1 ft. Well Diameter: 2 In, pH y-6 units Temp. Z 3.5 °C DRY at
Depth to Water Level: 8•I ft.below measuring point Screened Interval: 8 ft. to PI ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 1.8 ft.above land surface Relative M.P.Elevation: ft. Odor check
Volume of water pumped/balled before sampling: 6 gallons Appearance here:pi
Samples for metals were collected unfiltered: DYES 0 NO and field acidified: OYES ❑NO l
LABORATORY INFORM.VIO '�� '
Date sample analyzed: 1-2 4 Z.L, 4 f 2-25 f 3-d/-ZZ, Laboratory Name: Part eta Certification No. &,1' 373
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/I
Coliform:MF Total /100m1 Phosphorus:Total as P mg/I
J
(Note: Use MPN method for highly turbid samples)) Orthophosphate i1/1b mg/I Other(Specify Compounds and Concentration Units): •
Dissolved Solids:Total IS) mg/I Al-Aluminum mg/I
pH(when analyzed) units Ba-Barium mg/I M 645 r ND
TOO mg/I Ca-Calcium mg/I
Chloride my/I Cd-Cadmium mg/I
Arsenic mg/I Chromium:Total mg/I
Grease and Oils mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? Yes(1) CI No(0)
Specific Conductance µMhos K-Potassium mg/I VOC— ND ,method# g2cv P.
Total Ammonia mg/I Mg-Magnesium mg/I ,method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn-Manganese mg/I ,method# •
9
. TKN as N mg/I Ni-Nickel mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWO•certified laboreto . I am aware that there are significant.enalties for submitting false information,including the.ossibilit of fines and im.risonment for knowing violations.
Don well4, NCL5C Do" (iv / 3-/-n
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.72007

•
SUBMIT FORM ON YFLI OW PAPER ONLY
Mail original bER,MMNI Nj'OFt)g VIRONMENTrB NATURAL.RESOuRCES r •
COMPLIANCE EPORTGROUNDWATER ITY FORM MONITORING: and 1 copy to: taMi maA` Eity coC ENTER„IRALE GH,ANC.27.699 1 17'NPho e.,(919).733=3221
FACILITY INFORMATIQNlease Print Clearly or Type PERMIT Number: Expiration Date:
Facility Name: . / Poole r(/ r.,,} �Gp ./y.n%/ Non-Discharge IJa OW al/ UIC
Permit Name(if different): NPDES Other
Facility Address: /S/ &telC/we eom d TYPE OF PERMITTED OPERATION BEING MONITORED
Lt/aw J (slum') NC
7 County 7�Irti«f�tvlcX Lagoon El Infiltration Gallery
ICiiY) (Male) (zip)Zip)
❑
'.AA Spray Field ElRemediatlon:
1V1
Contact Person: r. go►v.4c t t%alb -- Telephone#: Bb0—'Y/•ill: ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: ? ❑ Water Source Heat Pump 0 Other.
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): M W'3 Date sample collected: 2-22'12 FIELD ANALYSES: • WAS •
• Well Depth: _7ft. Well Diameter: 1In. pH s.J units Temp. 2 2.8 eC DRY at
Depth to Water Level: 7./ ft.below measuring point Screened Interval: 7 ft. to 17 ft. Spec,.Cond. gMhos time Of
sampling,
Measuring Point is Z. I ,ft.above land surface Relative M.P.Elevation: ft. Odor check
Volume of water pumped/bailed before sampling: S gallons Appearance here:n
Samples for metals were collected unfiltered: OYES 0 NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: Z•23, Z•2I I 2-25 , 2-27 3%2t Laboratory Name: aft As..1141riil Certification No. FLi. 1 7 S'
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal /100mI Nitrate(NO3)as N mg/I Zn-Zinc mg/I
Coliform:MF Total • /100m1 Phosphorus:Total as P mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate
ND mg/I Other(Specify Compounds and Concentra finits): •
Dissolved Solids:Total 6 S mg/I Al-Aluminum mg/I •
pH(when analyzed) units Ba-Barium mg/I MAAS= NO
TOO mg/I Ca-Calcium mg/I
Chloride me/I Cd-Cadmium mg/1
Arsenic mg/I Chromium:Total mg/I
Grease and 011s mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? A Yes(1) ❑ No(0)
Specific Conductance µMhos K-Potassium mg/I VOC : ND ,method# (tprt)
Total Ammonia mg/I Mg-Magnesium mg/I ,method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese mg/I ,method# •
. TKN as N mg/I Ni-Nickel mg/I ,method#
For Remediatlon Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWO-certified laborato . I am aware that there are significant.enalties for submitting false Information,including the.ossibilit of fines and im.risonment for knowing violations.
D2 Mt" ticLcc o>r, Wrl� �i►
3iz
Permittee(or Authorized�paM)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.1/2007

SUBMIT FORM ON YFLLOW PAPER ONLY
Mail original bERARnMENjTOkiig.t vIRONMENTrB NAT:p.w:RESDURCES .
GROUNDWATER QUALITY COMPLIANCE REPORT FORM MONITORING: and 1 copy to: bviv,knAjois,-,Nii C�c NTER iL4t E GHpNG27699 16,•-vNPhonalT".'• "--,''' 1 -
FACILITY INFORMATION ✓ Please Print Clearly or Type
PERMIT Number: Expiration Date:
Facility Name: Gt-i e•7 Pie i. L
f/ p„ 0.14- £ 7.ip.i.i/ Non-Discharge W a Dou /l6/ UIC
Permit Name(if different): NPDES Other
Facility Address: /S/ 8raC/rAe f otw f TYPE OF PERMITTED OPERATION BEING MONITORED
Lela"1 litr„eti NC 29 If/ County Rrwrs«r►,•ex 'Lagoon ❑Remediation: Infiltration Gallery
(City) (atekr) (ZIP) ❑ Spray Field ❑Remediation:
Contact Person: A tt• QoiM►+:c IA ltf�La► Telephone#: PM—Y/-7 L78 ❑ Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: 3 ❑ Water Source Heat Pump ❑Other.
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW—If Date sample collected: 2 Z7-22 FIELD ANALYSES: • WAS •
• Well Depth: 22. G ft. Well Diameter; 2' in, pH 4./units Temp. 7 Y• 56 DRY at
Depth to Water Level: 7. 5 ft.below measuring point Screened Interval: ff ft. toll 6 ft. Speo.Cond. Mhos time of
sampling,
Measuring Point is 7•1 ft.above land surface Relative M.P.Elevation: ft. Odor check
Volume of water pumped/balled before sampling: 8 gallons Appearance here:ri
Samples for metals were collected unfiltered: DYES ❑NO and field acidified: DYES ❑NO
LABORATORY INFORMATION
Date sample analyzed: Z•ZYi 2.23/ Z..ZS. 7-77. 3/-rt Laboratory Name: pQ(pr 4.h 5 Certification No. Et,lu ,75
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal /100m1 Nitrate(NO3)as N mg/I Zn-Zinc mg/I
Coliform:MF Total • /100m1 Phosphorus:Total as P N f mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Uni •
Dissolved Solids:Total I ?I mg/i Al-Aluminum mg/I ��
pH(when analyzed) units Ba-Barium mg/I m845- NO
TOC mg/I Ca-Calcium mg/
' Chloride mu/1 Cd-Cedmlum mg/I
Arsenic mg/I Chromium:Total mg/I
Grease and oils mg/I Cu-Copper mg/I ORGANICS:(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? tcl Yes(1) ❑ No(0
Specific Conductance µMhos K-Potassium mg/I VOC' /VD ,method# 6 OO
Total Ammonia mg/I Mg-Magnesium •mg/I ,method#
(Ammonia Nitrogen;NHsas N;Ammonia Nitrogen,Total)
Mn-Manganese mg/I ,method# . '
. TKN as N mg/I NI-Nickel mg/I ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWO•certifled laborato . I am aware that there are significant,enalties for submitting false information,including the.ossibilil of fines and im.risonment for knowing violations.
17" wef15e N( L55 : 4v -/P-21
Permlttee(or Authorized Anwnt)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.1/2007

1
IMIIII611-111, 400i itmnuonurpmquc
4'
ace Analytical A \ A L Y T CAL R T D O R T
March 07, 2022 iiiiiiil
1
Ss
Soil & Env. Consultants - Raleigh, NC
4
Sample Delivery Group: L1464280 Cn
Samples Received: 02/23/2022 Sr
Project Number: GW-1 1061-200
Description: Groundwater Job#1061 :�c
7
GI
Report To: Mr. Don Wells
8412 Falls of Neuse Road,Suite 104 Al
Raleigh, NC 27615-3543
L.
Sc
Entire Report Reviewed By:
Jason Romer
N. Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and :;.
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the Information provided.
and as the samples are received4 it
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Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh.NC GW-11061-200 L1464280 03/07/22 09:24 1 of 30

TABLE OF CONTENTS
Ss:Sample Summary 3 2Te
Cn: Case Narrative 4
Sr:Sample Results 5 Ss
MW-2A L1464280-01 5 4
Cn
MW-3 L1464280-02 7
MW-4A L1464280-03 9 Sr
TRIP BLANK L1464280-04 11
Qc: Quality Control Summary 13
Gravimetric Analysis by Method 2540 C-2011
Wet Chemistry by Method 4500P E-2011 I GI
Wet Chemistry by Method 5540 C-2011 17
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 18
GI:Glossary of Terms 28
Al:Accreditations & Locations 29
Sc:Sample Chain of Custody 30
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 2 of 30

SAMPLE SUMMARY
Collected by Collected dateftime Received date+time
MW-2A L1464280-01 GW Don Welk 0222/221045 02/23;2209.00
I
1
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
1
Gravimetric Analysis by Method 2540 C-2011 WG1825498 1 03/01/22 13:43 03/01/2216:28 MMF Mt.Juliet,TN I
Wet Chemistry by Method 4500P E-2011 WG1822490 1 02/23/2215:52 02/23/22 15:52 SDE Mt.Juliet,TN
Wet Chemistry by Method 5540 C-2011 WG1822723 1 02/24/22 08:00 02/24/22 12:28 BMD Mt.Juliet,TN 55
Volatile Organic Compounds(GC/MS)by Method 6200B-2011 WG1823129 1 02/24/22 17:08 02/24/22 17:08 BMB Mt.Juliet,TN
Volatile Organic Compounds(GC/MS)by Method 6200E-2011 WG1823716 1 02/25/22 14:19 02/25/22 14:19 JHH Mt.Juliet,TN 4Cn
Cn
Volatile Organic Compounds(GC/MS)by Method 6200B-2011 WG1824738 1 03/01/22 13:53 03/01/22 13:53 BMB Mt.Juliet,TN
Collected by Collected dateftime Received date/time Sr
MW-3 L1464280-02 GW Don Wells 02 22 22 115 02/23/22 09 00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1824470 1 02/27/22 14:58 02/27/2217:13 MMF Mt.Juliet,TN G
Wet Chemistry by Method 4500P E-2011 WG1822490 1 02/23/22 16:09 02/23/2216:09 SDE Mt.Juliet,TN
Wet Chemistry by Method 5540 C-2011 WG1822723 1 02/24/22 08:00 02/24/2212:29 BMD Mt.Juliet,TN
Volatile Organic Compounds(GC/MS)by Method 6200E-2011 WG1823129 1 02/24/2217:29 02/24/22 17:29 BMB Mt.Juliet,TN
Volatile Organic Compounds(GUMS)by Method 6200E-2011 WG1823716 1 02/25/22 14:41 02/25/2214:41 JHH Mt.Juliet,TN
Volatile Organic Compounds(GUMS)by Method 6200E-2011 WG1824738 1 03/01/2214:14 03/01/22 14:14 BMB Mt.Juliet,TN SC
Collected by Collected dateftime Received date/time
MW-4A L1464280-03 GW Don'Welk 02;/22/2211.45 02-2322 0900
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1824470 1 02/27/2214:58 02/27/2217:13 MMF Mt.Juliet,TN
Wet Chemistry by Method 4500P E-2011 WG1822490 1 02/23/2216:11 02/23/2216:11 SDE Mt.Juliet,TN
Wet Chemistry by Method 5540 C-2011 WG1822723 1 02/24/22 08:00 02/24/22 12:30 BMD Mt.Juliet,TN
Volatile Organic Compounds(GUMS)by Method 6200B-2011 WG1823129 1 02/24/2217:50 02/24/22 17:50 BMB Mt.Juliet,TN
Volatile Organic Compounds(GUMS)by Method 6200E-2011 WG1823716 1 02/25/22 15:04 02/25/2215:04 JHH Mt.Juliet,TN
Volatile Organic Compounds(GUMS)by Method 6200E-2011 WG1824738 1 03/01/22 14:34 03/01/2214:34 BMB Mt.Juliet,TN
Collected by Collected datetime Received date/time
TRIP BLANK L1464280-04 GW Don Wells 02/22/22 00 00 0223/220900
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds(GUMS)by Method 6200B-2011 WG1823129 1 02/24/2212:14 02/24/22 12:14 ACG Mt.Juliet,TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 3 of 30

f(IQU glll/II�IUngr}11111111(F
` CASE NARRATIVE
All sample aliquots were received at the correct temperature,in the proper containers,with the
appropriate preservatives,and within method specified holding times, unless qualified or notated within
the report. Where applicable,all MDL(LOD)and RDL(LOQ)values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative,a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge,all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory,and no information or data have been
knowingly withheld that would affect the quality of the data.
Sr
7GI
Jason Romer
Project Manager
SC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 4 of 30

` MW-2A SAMPLE RESULTS - 01
Collected date/time. 02/22/22 10:45 L1464280
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch I--
Analyte mg/I mg/I date/time
Dissolved Solids 78.0 10.0 1 03/01/2022 16:28 WG1325490
Wet Chemistry by Method 4500P E-2011 Ss
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time 4
Cn
Phosphate,Ortho ND 0.0300 1 02/23/2022 15:52 WGi822490
Wet Chemistry by Method 5540 C-2011 Sr
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time , -
MBAS ND 0.100 1 02/24/202212:28 W01822723
.GI
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/1 mg/I date/time
Acetone ND 0.0500 1 02/25/2022 14:19 WG1823716
Acrolein ND 0.0500 1 0225/202214:19 WG1823716 SC
Acrylonitrile ND 0.0100 1 02/25/2022 14:19 WG1823716
Benzene ND 0.00100 1 02/25202214:19 WG1823716
Bromobenzene ND J4 0.00100 1 0224202217:08 WG1823129
Bromodichloromethane ND 0.00100 1 0225202214:19 WG1823716
Bromoform ND 0.00100 1 02/24/2022 17:08 WG1823129
Bromomethane ND 0.00500 1 03/01/202213:53 WG1824738
n-Butylbenzene ND J4 0.00100 1 0224202217:08 W61823129
sec-Butylbenzene ND 0.00100 1 02/24/202217:08 WG1823129
tert-Butylbenzene ND 0.00100 1 0224202217:08 W61823129
Carbon tetrachloride ND 0.00100 1 0225202214:19 WG1823716
Chlorobenzene ND 0.00100 1 0224202217:08 WG1823129
Chlorodibromomethane ND 0.00100 1 0224202217:08 WG1823129
Chloroethane ND 0.00500 1 0225202214:19 WG1823716
Chloroform ND 0.00500 1 0225/202214:19 WG1823716
Chloromethane ND 0.00250 1 0225202214:19 WG1823716
2-Chlorotoluene ND 0.00100 1 02/24/202217:08 WG1823129
4-Chlorotoluene ND J4 0.00100 1 0224202217:08 WG1823129
1,2-Dibromo-3-Chloropropane ND 0.00500 1 0224202217:08 WG1823129
1,2-Dibromoethane ND 0.00100 1 0224202217:08 WG1823129
Dibromomethane ND 0.00100 1 0225202214:19 WG1823716
1,2-Dichlorobenzene ND 0.00100 1 0224202217:08 WG1823129
1,3-Dichlorobenzene ND 0.00100 1 0224202217:08 WG1823129
1,4-Dichlorobenzene ND 0.00100 1 0224202217:08 WG1823129
Dichlorodifluoromethane ND 0.00500 1 0225202214:19 WG1823716
1,1-Dichloroethane ND 0.00100 1 0225202214:19 W61823716
1,2-Dichloroethane ND 0.00100 1 0225202214:19 WG1823716
1,1-Dichioroethene ND 0.00100 1 0225202214:19 WG1823716
cis-1,2-Dichloroethene ND 0.00100 1 02/25/202214:19 WG1823716
trans-1,2-Dichloroethene ND 0.00100 1 0225202214:19 WG1323716
1,2-Dichloropropane ND 0.00100 1 0225202214:19 WG1823716
1,1-Dichloropropene ND 0.00100 1 0225202214:19 WG1S23716
1,3-Dichloropropane ND 0.00100 1 02/24/202217:08 WG1823129
2,2-Dichloropropane ND 0.00100 1 0225202214:19 0VG1623716
Di-isopropyl ether ND 0.00100 1 0225202214:19 WG1823716
Ethylbenzene ND 0.00100 1 0224202217:08 WG1823129
Hexachloro-1,3-butadiene ND 0.00100 1 0224202217:08 WG1823129
Isopropylbenzene ND 0.00100 1 0224202217:08 WG1823129
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 5 of 30

' •",',Illllillllllll111111 it_[_I I11.411_
r MW-2A SAMPLE RESULTS - 01
Collected date/time: 02/22/22 10:45 L1464280
Volatile Organic Compounds (••✓__ ✓"',11') uy ✓:.AI.:1:-._:, -2011
Result Qualifier. RDL Dilution Analysis Batch
Analyte mg/i mg/I date/time
p-Isopropyttoluene ND 0.00100 1 02/24/2022 17:08 WG1823129 7
2-Butanone(MEK) ND 0.0100 1 02/25/2022 14:19 WG1823716 I
Methylene Chloride ND 0.00500 1 0225202214:19 WG1823716
4-Methyl-2-pentanone(MIBK) ND 0.0100 1 02/24/2022 17:08 WG1323129 SS
Methyl ten-butyl ether ND 0.00100 1 02/25/2022 14:19 WG1823716
Naphthalene ND 0.00500 1 02/24/2022 17:08 WG1823129 4
Cn
n-Propylbenzene ND 0.00100 1 02/24/2022 17:08 WG1823129
Styrene ND 0.00100 1 02/24/2022 17:08 WG1823129
1,1,1,2-Tetrachloroethene ND 0.00100 1 0224202217:08 WG1823129 S
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/24/2022 17:08 WG1623129
Tetrachloroethene ND 0.00100 1 0224/202217:08 WG1823129 ,
Toluene ND 0.00100 1 0224202217:08 WG1823129
1,2,3-Trichlorobenzene ND 0.00100 1 0224202217:08 WG1823129 7
1,2,4-Trichlorobenzene ND 0.00100 1 0224202217:08 WG1823129 GI
1,1,1-Trichloroethane ND 0.00100 1 0225/202214:19 WG1823716
1,1,2-Trichloroethane ND 0.00100 1 0224202217:08 WG1823129 Al
Trichloroethene ND 0.00100 1 02/25/2022 14:19 WG1823716
Trichlorofluoromethane ND 0.00500 1 0225202214:19 WG1823716 '
1,2,3-Trichloropropane ND 0.00250 1 0224202217:08 WG1823129 SC
1,2,4-Trimethylbenzene ND 0.00100 1 0224202217:08 WG1323129
1,3,5-Trimethylbenzene ND 0.00100 1 0224202217:08 WG1823129
Vinyl chloride ND 0.00100 1 02/25/2022 14:19 WG1823716
o-Xylene ND 0.00100 1 0224202217:08 WG1823129
m&p-Xylenes ND 0.00200 1 02/24/2022 17:08 WG1823129
0 Toluene-d8 95.1 80.0-120 02/24/202217..08 WG1823129
(S)Toluene-d8 103 80.0-120 02/25/202214:19 WG1823716
(S)Toluene-d8 108 80.0-120 03/01/202213:53 WG1824738
(S)4-Bromofluorobenzene 103 77.0-126 02/24/20221708 WG1823129
(S)4-Bromoiluorobenzene 83.0 77.0-126 02/25/202214:19 WG1823716
(S)4-Bromofluorobenzene 107 770-126 03/0V202213:53 WG1824738
(S)1,2-Dichloroethane-d4 107 70.0-130 02/24/202217.:08 WG1823129
(S)1,2-Dichloroethone-d4 108 70.0-130 02/25/2022 14:19 WG1823716
(S)1,2-Dichloroethane d4 98.8 70.0-130 03/01/202213:53 WG1824738
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 6 of 30

•
i MW-3 SAMPLE RESULTS - 02
Collected date/time: 02/22/22 11:15 L1464280
Gravimetric Analysis by Method 2540 C-2011 1
Result Qualifier RDL Dilution Analysis Batch i
Analyte mg/I mg/I date/time
Dissolved Solids 65.0 10.0 1 02/27/202217:13 WG1324470
Wet Chemistr', '.' ~Dd 4500P E-2011
Ss
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/1 mg/I date/time 4
Cn
Phosphate,Ortho ND 0.0300 1 02/23/2022 16:09 WG1822490
Wet Chemistry by Method 5540 C-2011 Sr
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time ID
MBAS ND 0.100 1 02/24/202212:29 W61322723
GI
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
AI
Analyte mg/1 mg/I date/time
Acetone ND 0.0500 1 02/25/202214:41 WG1823716
Acrolein ND 0.0500 1 02/25/202214:41 WG1823716 Sc
Acrylonitrile ND 0.0100 1 02/25/202214:41 WG1823716
Benzene ND 0.00100 1 02/25/202214:41 WG1823716
Bromobenzene ND J4 0.00100 1 02/24/202217:29 W61823129
Bromodichloromethane ND 0.00100 1 02/25/202214:41 WG1823716
Bromoform ND 0.00100 1 02/25/202214:41 WG1323716
Bromomethane ND 0.00500 1 03/01/202214:14 WG1824738
n-Butylbenzene ND J4 0.00100 1 02/24/2022 17:29 WG1823129
sec-Butylbenzene ND 0.00100 1 02/24/202217:29 WG1823129
tert-Butylbenzene ND 0.00100 1 02/24/202217:29 WG1823129
Carbon tetrachloride ND 0.00100 1 02R5/202214:41 WG1823716
Chlorobenzene ND 0.00100 1 0225/202214:41 WG1823716
Chlorodibromomethane ND 0.00100 1 0225/202214:41 WG182 3716
Chloroethane ND 0.00500 1 0225202214:41 WG1823716
Chloroform ND 0.00500 1 0225202214:41 WG1823716
Chloromethane ND 0.00250 1 0225202214:41 WG1823716
2-Chlorotoluene ND 0.00100 1 0224202217:29 WG1823129
4-Chlorotoluene ND J4 0.00100 1 0224202217:29 WG1823129
1,2-Dibromo-3-Chloropropane ND 0.00500 1 0224202217:29 WG1823129
1,2-Dibromoethane ND 0.00100 1 0225202214:41 WG1823716
Dibromomethane ND 0.00100 1 0225/202214:41 WG1823716
1,2-Dichlorobenzene ND 0.00100 1 02/24/2022 17:29 WG1323129
1,3-Dichlorobenzene ND 0.00100 1 0224202217:29 WG1823129
1,4-Dichlorobenzene ND 0.00100 1 02/24/2022 17:29 WG1323129
Dichlorodifluoromethane ND 0.00500 1 0225/202214:41 WG1823716
1,1-Dichloroethane ND 0.00100 1 0225202214:41 WG1823716
1,2-Dichloroethane ND 0.00100 1 0225/202214:41 WG1823716
1,1-Dichloroethene ND 0.00100 1 0225202214:41 WG1823716
cis-1,2-Dichloroethene ND 0.00100 1 0225202214:41 WG1823716
trans-1,2-Dichloroethene ND 0.00100 1 0225202214:41 WG1323716
1,2-Dichloropropane ND 0.00100 1 0225202214:41 WG1823716
1,1-Dichloropropene ND 0.00100 1 0225202214:41 W61323716
1,3-Dichloropropane ND 0.00100 1 0225/202214:41 WG1823716
2,2-Dichloropropane ND 0.00100 1 0225202214:41 WG1323716
Di-isopropyl ether ND 0.00100 1 0225202214:41 WG1823716
Ethylbenzene ND 0.00100 1 0225202214:41 WG1823716
Hexachloro-1,3-butadiene 'ND 0.00100 1 0224202217:29 WG1823129
Isopropylbenzene ND 0.00100 1 0225202214:41 W61823716
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-11061-200 L1464280 03/07/22 09:24 7 of 30

4
MW-3 SAMPLE RESULTS - 02
Collected date/time: 02/22/22 11:15 L1464280
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time `-"""-'
p-Isopropyttoluene ND 0.00100 1 02/24/2022 17:29 WG1823129
2-Butanone(MEK) ND 0.0100 1 02/25/2022 14:41 WG1823716
Methylene Chloride ND 0.00500 1 02/25/2022 14:41 WG1823716
4-Methyl-2-pentanone(MIBK) ND 0.0100 1 02/25/2022 14:41 WG1S23716 Ss
Methyl tert-butyl ether ND 0.00100 1 02/25/2022 14:41 WG1823716
Naphthalene ND 0.00500 1 02/24/202217:29 W01823129 4Cn
Cn
n-Propylbenzene ND 0.00100 1 02/24/202217:29 WG1823129
Styrene ND 0.00100 1 02/25/2022 14:41 WG1823716
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/25/2022 14:41 WG1823716 i
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/24/202217:29 WG1823129
Tetrachloroethene ND 0.00100 1 02/25/202214:41 WG1823716
Toluene ND 0.00100 1 02/25/202214:41 WG1823716
1,2,3-Trichlorobenzene ND 0.00100 1 02/24/202217:29 WG1823129
1,2,4-Trichlorobenzene ND 0.00100 1 02/24/202217:29 WG1823129 GI
1,1,1-Trichloroethane ND 0.00100 1 02/25/2022 14:41 WG1823716
1,1,2-Trichloroethane ND 0.00100 1 02/25/202214:41 WG1823716 A
Trichloroethene ND 0.00100 1 02/25/2022 14:41 WG1823716
Trichlorofluoromethane ND 0.00500 1 02/25/202214:41 WG1823716
1,2,3-Trichloropropane ND 0.00250 1 02/24/202217:29 WG1823129 SC
1,2,4-Trimethylbenzene ND 0.00100 1 02/24/202217:29 WG1323129
1,3,5-Trimethylbenzene ND 0.00100 1 02/24202217:29 WG1823129
Vinyl chloride ND 0.00100 1 02/25/202214:41 WG1823716
o-Xylene ND 0.00100 1 02/25202214:41 WG1823716
m&p-Xylenes ND 0.00200 1 02/25/202214:41 WG1823716
(S)Toluene-d8 96.8 80.0-120 02/24/202217.29 WG1823129
(S)Toluene-d8 100 80.0-120 02/25/2022 14:41 WG1323716
(S)Toluene-d8 102 80.0-120 03/01/202214:14 WG1824738
(S)4-Bromofluorobenzene 102 770-126 02/24/20221729 WG1S23129
(S)4-Bromof1uorobenzene 79.8 77.0-126 02/25/2022 14:41 WG1823716
(S)4-Bromofluorobenzene 98.1 77.0-126 03/01202214:14 WG1S24736
(5)1,2-Dichloroethone-d4 102 70.0-130 02/24/202217..29 W61823129
(5)12-Dichloroethane-d4 109 70.0-130 02/25/2022 14:41 WG1823716
(S)1,2-Dichloroethone-d4 94.4 70.0-130 03/01/202214:14 WG1824738
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 8 of 30

MW-4A SAMPLE RESULTS - 03
Collected date/time: 02/22/22 11:45 L1464280 ,
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch r
Analyte mg/I mg/I date/time
Dissolved Solids 171 10.0 1 02/27/202217:13 WG1024470
Wet Chemistry by Method 4500P E-2011 'Ss
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/ mg/ date/time 4
Cn
Phosphate,Ortho ND 0.0300 1 02/23/202216:11 WG1822490
Wet Chemistry by Method 5540 C-2011 ``
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time
MBAS ND 0.100 1 02/24/202212:30 WG1022723
GI
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
,I
Analyte m gil mg/I date/time
Acetone ND 0.0500 1 02/25/202215:04 W61823716
Acrolein ND 0.0500 1 0225202215:04 WG1823716 SC
Acrylonitrile ND 0.0100 1 02/25/202215:04 WG1823716
Benzene ND 0.00100 1 0225202215:04 WG1823716
Bromobenzene ND J4 0.00100 1 02/24/202217:50 WG1823129
Bromodichloromethane ND 0.00100 1 0225202215:04 WG1823716
Bromoform ND 0.00100 1 02/24/202217:50 W01323129
Bromomethane ND 0.00500 1 03/01202214:34 WG1824738
n-Butylbenzene ND _Hi 0.00100 1 02/24/202217:50 WGI823129
sec-Butylbenzene ND 0.00100 1 0224/202217:50 WG1823129
tert-Butylbenzene ND 0.00100 1 02/24/202217:50 W61823129
Carbon tetrachloride ND 0.00100 1 0225202215:04 WG1823716
Chlorobenzene ND 0.00100 1 02/24/202217:50 WG1323129
Chlorodibromomethane ND 0.00100 1 0224202217:50 WG1823129
Chloroethane ND 0.00500 1 02/25/202215:04 WG1823716
Chloroform ND 0.00500 1 02/25/202215:04 WG1823716
Chloromethane ND 0.00250 1 02/25/202215:04 WG1823716
2-Chlorotoluene ND 0.00100 1 0224202217:50 WG1823129
4-Chlorotoluene ND J4 0.00100 1 02/24/202217:50 WG1823129
1,2-Dibromo-3-Chloropropane ND 0.00500 1 0224202217:50 WG1823129
1,2-Dibromoethane ND 0.00100 1 0224202217:50 WG1323129
Dibromomethane ND 0.00100 1 0225202215:04 WG1823716
1,2-Dichlorobenzene ND 0.00100 1 02/24/202217:50 WG1323129
1,3-Dichlorobenzene ND 0.00100 1 0224202217:50 WG1823129
1,4-Dichlorobenzene ND 0.00100 1 02/24/202217:50 WG1823129
Dichlorodifluoromethane ND 0.00500 1 0225202215:04 WG1823716
1,1-Dichloroethane ND 0.00100 1 0225202215:04 W01823716
1,2-Dihloroethane ND 0.00100 1 0225/202215:04 WG1823716
1,1-Dichloroethene ND 0.00100 1 02/25/202215:04 WG1823716
cis-1,2-Dichloroethene ND 0.00100 1 0225/202215:04 WG1823716
trans-1,2-Dichloroethene ND 0.00100 1 02/25/202215:04 WG1823716
1,2-Dichloropropane ND 0.00100 1 0225202215:04 WG1823716
1,1-Dichloropropene ND 0.00100 1 0225202215:04 W01823716
1,3-Dichloropropane ND 0.00100 1 0224202217:50 WG1823129
2,2-Dichloropropane ND 0.00100 1 0225202215:04 WG1323716
Di-isopropyl ether ND 0.00100 1 0225202215:04 WG1823716
Ethylbenzene ND 0.00100 1 02/24/202217:50 W01823129
Hexachloro-1,3-butadiene ND 0.00100 1 0224202217:50 WG1823129
Isopropylbenzene ND 0.00100 1 02/24/202217:50 VJ61823129
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-11061-200 L1464280 03/07/22 09:24 9 of 30

MW-4A SAMPLE RESULTS - 03
Collected date/time: 02/22/22 11:45 L1464280
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mgA date/time
p-Isopropyitoluene ND 0.00100 1 02/24202217:50 WG1823129 I l
2-Butanone(MEK) ND 0.0100 1 02/25/202215:04 WG1S23716 1
Methylene Chloride ND 0.00500 1 02/25/202215:04 WG1823716
4-Methyl-2-pentanone(MIBK) ND 0.0100 1 02/24/202217:50 WG1023129 SS
Methyl tent-butyl ether ND 0.00100 1 02/25202215:04 WG1823716
Naphthalene ND 0.00500 1 02/24/202217:50 WGI323129 4Cn
Cn
n-Propylbenzene ND 0.00100 1 02/24/202217:50 WG1823129
Styrene ND 0.00100 1 02/24/202217:50 WG1823129
1,1,1,2-Tetrachloroethane ND 0.00100 1 02/24202217:50 WG1823129 S r
1,1,2,2-Tetrachloroethane ND 0.00100 1 02/24/202217:50 W01023129
Tetrachloroethene ND 0.00100 1 0224202217:50 WG1823129 ;j,.
Toluene ND 0.00100 1 0224202217:50 WG1823129
1,2,3-Trichlorobenzene ND 0.00100 1 02/24/202217:50 WG1823129
1,2,4-Trichlorobenzene ND 0.00100 1 02/24/202217:50 W01023129 GI
1,1,1-Trichloroethane ND 0.00100 1 0225/202215:04 WG1823716
1,1,2-Trichloroethane ND 0.00100 1 02/24/202217:50 WG1823129 AI
Trichloroethene ND 0.00100 1 02/25202215:04 WG1823716
Trichlorofluoromethane ND 0.00500 1 0225202215:04 WG1023716
1,2,3-Trichloropropane ND 0.00250 1 0224202217:50 WG1823129 SC
1,2,4-Trimethylbenzene ND 0.00100 1 0224202217:50 WG1823129
1,3,5-Trimethylbenzene ND 0.00100 1 0224202217:50 WG1823129
Vinyl chloride ND 0.00100 1 0225202215:04 WG1823716
o-Xylene ND 0.00100 1 0224202217:50 WG1823129
m&p-Xylenes ND 0.00200 1 02/24/202217:50 WG1823129
(S)Toluene-0 963 80.0-120 02/24/20221750 WG1823129
(S)Toluene-d8 104 80.0-120 02/25/2022 15:04 WG1023716
(5)Toluene-dB 105 80.0-120 03/01/202214:34 WG1824738
(S)4-Bromofluorobenzene 103 77.0-126 02/24/20221750 WG1S23129
(5)4-Bromofluorobenzene 85.5 77.0-126 02/25/2022 15:04 WG1823716
(5)4-Bromofluorobenzene 98.2 770-126 03/01/202214:34 WG1S2473S
(5)1,2-Dichloroethane-d4 108 70.0-130 02/24/20221750 WG1823129
(S)1,2-Dichloroethone-d4 112 70.0-130 02/25/2022 15:04 WGI323716
(S)1,2-Dichloroethane d4 99.1 70.0-130 03/01/202214:34 WG1824738
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh,NC GW-1 1061-200 L1464280 03/07/22 09:24 10 of 30

' TRIP BLANK SAMPLE RESULTS - 04
Collected date/time: 02/22/22 00:00 L1464280
Volatile Organic Compounds (GC/MS) by Metnoa t 200B '1
Result Qualifier RDL Dilution Analysis Batch
Analyte m g/1 mg/I date/time
i
Acetone ND 0.0500 1 0224/202212:14 W611323129
Acrolein ND 0.0500 1 0224202212:14 WG1823129
Acrylonitrile ND 0.0100 1 0224202212:14 WG1323129 Ss
Benzene ND 0.00100 1 0224202212:14 WG1823129
Bromobenzene ND J4 0.00100 1 0224202212:14 WG1323129
4
Bromodichloromethane ND 0.00100 1 0224202212:14 WG1823129 Cn
Bromoform ND 0.00100 1 0224202212:14 WG1323129
Bromomethane ND 0.00500 1 0224202212:14 WG1823129 r
n-Butylbenzene ND J4 0.00100 1 02/24/202212:14 WG1823129
sec-8utylbenzene ND 0.00100 1 02/24/202212:14 WG1823129
tert-Butylbenzene ND 0.00100 1 0224202212:14 WG1823129 ,
Carbon tetrachloride ND 0.00100 1 02/24/202212:14 WG1823129
Chlorobenzene ND 0.00100 1 02/24/202212:14 WG1823129 GI
Chlorodibromomethane ND 0.00100 1 0224202212:14 WG1823129
Chloroethane ND 0.00500 1 02/24/202212:14 WG1S23129
Chloroform ND 0.00500 1 0224202212:14 WG1823129
Chloromethane ND 0.00250 1 02/24/2022 12:14 WG1S23129
2-Chlorotoluene ND 0.00100 1 02/24202212:14 WG1823129
4-Chlorotoluene ND J4 0.00100 1 0224202212:14 WG1823129
1,2-Dibromo-3-Chloropropane ND 0.00500 1 0224202212:14 WG1823129
1,2-Dibromoethane ND 0.00100 1 0224202212:14 WG1323129
Dibromomethane ND 0.00100 1 0224202212:14 WG1823129
1,2-Dichlorobenzene ND 0.00100 1 02/24/202212:14 WG1823129
1,3-Dichlorobenzene ND 0.00100 1 02/24202212:14 WG1823129
1,4-Dichlorobenzene ND 0.00100 1 0224202212:14 WG1823129
Dichiorodifiuoromethane ND 0.00500 1 0224/202212:14 WG1823129
1,1-Dichloroethane ND 0.00100 1 02/24/202212:14 WG1623129
1,2-Dihloroethane ND 0.00100 1 02/24/202212:14 WG1823129
1,1-Dichloroethene ND 0.00100 1 02/24/202212:14 WG1823129
cis-1,2-Dichloroethene ND 0.00100 1 02/24/202212:14 WG1823129
trans-1,2-Dichloroethene ND 0.00100 1 0224202212.14 WG1323129
1,2-Dichloropropane ND 0.00100 1 0224202212:14 WG1823129
1,1-Dichloropropene ND 0.00100 1 0224202212:14 WG1323129
1,3-Dichloropropane ND 0.00100 1 0224202212:14 WG1823129
2,2-Dichloropropane ND 0.00100 1 0224202212:14 WG1823129
Di-isopropyl ether ND 0.00100 1 0224202212:14 WG1823129
Ethylbenzene ND 0.00100 1 0224202212:14 WG1823129
Hexachloro-1,3-butadiene ND 0.00100 1 02/24202212:14 WG1823129
Isopropylbenzene ND 0.00100 1 0224202212:14 WG1823129
p-Isopropyttoluene ND 0.00100 1 02/24/202212:14 WG1823129
2-Butanone(MEK) ND 0.0100 1 02/24/202212:14 WG1S23129
Methylene Chloride ND 0.00500 1 0224202212:14 WG1823129
4-Methyl-2-perdanone(MIBK) ND 0.0100 1 0224202212:14 WG1S23129
Methyl tert-butyl ether ND 0.00100 1 0224202212:14 WG1823129
Naphthalene ND 0.00500 1 02/24/202212:14 WG1S23129
n-Propylbenzene ND 0.00100 1 0224202212:14 WG1823129
Styrene ND 0.00100 1 0224202212:14 W01823129
1,1,1,2-Tetrachloroethane ND 0.00100 1 0224202212:14 WG1823129
1,1,2,2-Tetrachloroethane ND 0.00100 1 0224202212:14 WG1823129
Tetrachloroethene ND 0.00100 1 0224202212:14 WG1823129
Toluene ND 0.00100 1 0224202212:14 WG1S23129
1,2,3-Trichlorobenzene ND 0.00100 1 0224202212:14 WG1823129
1,2,4-Trichlorobenzene ND 0.00100 1 0224202212:14 :1323129
1,1,1-Trichloroethane ND 0.00100 1 0224202212:14 .. ;'?129
1,1,2-Trichloroethane ND 0.00100 1 0224202212:14 _.,. ::29
Trichloroethene ND 0.00100 1 0224202212:14 WG1S23129
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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TRIP BLANK SAMPLE RES
ULTS - 04
Collected date/time: 02/22/22 00:00 L1464280
Volatile Organic Compounds (GC/MS) L., _ _ __ _ -2011
Result Qualifier RDL Dilution Analysis Batch
Analyte m g/1 mg/I date/time 1
Trichlorofluoromethane ND 0.00500 1 02/24/2022 12:14 vVG1323129
1,2,3-Trichloropropane ND 0.00250 1 02/24/2022 12:14 WG1823129
1,2,4-Trimethylbenzene ND 0.00100 1 02/24/202212:14 WG1323129
1,3,5-Trimethylbenzene ND 0.00100 1 02/24/202212:14 WG1823129
Vinyl chloride ND 0.00100 1 02/24/2022 12:14 WG1323129
o-Xylene ND 0.00100 1 02/24/202212:14 WG1823129 Cis
m&p-Xylenes ND 0.00200 1 0224202212:14 WG1323129
(s)Toluene-d8 95.6 80.0-120 02/24/20221214 WG1823129
(S)4-Bromofluorobenzene 105 77.0-126 02/24/202212::14 WG182 3129 Sr
(5)1,2-Dichloroethone-d4 10S 70.0-130 02/24/202212:14 WG1823129 r_
I 1
GI
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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•
WG182447O QUALITY CONTROL SUMMARY
Gravlmetric Analysis by Method 2540 C-2011
(MB)R3764991-1 0227/22 1713
MB Result MB Qualifier MB MDL MR RDL
Analyte mg/I mg/I mg/I
Dissolved Solids U 10.0 10.0
•
Cn
(OS)L1464858-03 02/27/22 1713•(DUP)R3764991-3 02/27/22 1713
Original Result DUP Result Dilution DUP RPD DUP Qualifier OUP RPD
mits
'Sr
Analyte mg/I mg/1 % %
Dissolved Solids 184 194 1 5.29 _ 5
Oc
• GI
(OS)L1465103-01 02/27/2217:13•(DUP)R3764991-4 02/27/22 17:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyse mg/I mgI % %
Dissolved Solids 1530 1610 1 5.10 _ 5 SC
(LCS)R3764991-2 02/2722 1713
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I
Dissolved Solids 8800 8430 95.8 77.4-123
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE
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k
WG1825498 QUALITY CONTROL SUMMARY
Gravirnetric Analysis by Method 2 54 0 C-2011
(MB)R3766137-1 03/01/22 16:28
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mgil
Dissolved Solids U 10.0 10 0 Pi
Sti
(OS)L1464280-01 03/01/22 16:28•(DUP)R3766137-3 03/01/22 16:28 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD _
Limits
Sr
Analyte mg/I mg/ % %
Dissolved Solids 78.0 81.0 1 3.77 5
QC
GI
(OS)L1464858-01 03/01/22 16:28•(DUP)R3766137-4 03/01/22 16:28
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPmit RsPD
Li
Analyte mg/I mg/ % %
Dissolved Solids 2400 2410 1 0.208 5 Sc
(OS)L1464858-02 03/01/22 16:28•(DUB)R3766137-5 03/01/22 16:28
Original Result DUP Result Dilution DUP RPD DUP Qualifier LiDUP RPD
mits
Analyte mg/I mg/ % %
Dissolved Solids 658 672 1 2.11 5
(OS)L1464858-03 03/01/22 16:28•(DUP)R3766137-6 03/01/22 16:28
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUmPits RPD
Li
Analyte mg/I mg/ % %
Dissolved Solids 206 215 1 4.28 5
ACCOUNT: PROJECT: SDGc DATE/TIME PAGE
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4-
WG1825498 QUALITY CONTROL SUMMARY
Grevimetric Analysis by Method 2540 C-2011 -
(LCS)R3766137-2 03/01/2216:28 _ _._
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 1
Anakyte mg/I �g' [ %
Dissolved Solids 8800 8620 'a8_ 77.4-123
•
S,
'Co
Sr
Qc
GI
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE
Soil&Env Consultants-Raleigh.NC GW-11061-200 L1464280 03/07/22 0924 15 of 30
it

4
WG1822490 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 4500P E-2011 L1464280 .
1
(MB)R3763113-1 02/23/2215:S1 ,__
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Phosphate,Ortho U 0.0140 0.0300
SS
•
Cn
(OS)L1464280-02 02/23/2216:09•(OUP)83763113-5 02/23/221610
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
L mits
Sr
Analyte mg/I mg7 % %
Phosphate,Ortho ND ND 1 0.000 20
'Oc
GI
(LCS)P3763113-2 02/23/2215:51
Spike Amount LCS Resuk LCS Rec. Rec.Limits LCS Qualifier •
Analyte mg/I mgn % %
Phosphate,Ortho 0.245 0.271 111 85.0-115
Sc
(OS)L1464280-01 02/23/22 15:52•(MS)P3763113-3 02/23/22 16:08•(MSD)R3763113-4 02/23/22 16:08
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limns
Analyte mg/I mg/I mg/I mg/I % % % % %
Phosphate,Ortho 0.500 ND 0.537 0.554 107 111 1 800-120 3,12 20
ACCOUNT: PROJECT: SOO: DATE/TIME PAGE
Soil&Env.Consultants-Raleigh.NC GW-11061-200 L1464280 03/07/22 09 24 16 C1'.r.

k
WG1822723 QUALITY CONTROL SUMMARY
Wet Chemi,try by Method 5540 C-2011 -
(MB)R3763484-1 02/24/2212:24 — --------__ -__,
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/i mg/I mg/I
MBAS U 0.0190 0.100
S5
4Cn
(OS)L1464280-01 02/24/2212:28•(DUP)R3763484-3 02/24/22 12:28
Original Result DUP Result Dilution DUP RPD DUP Qualifier DU R
LimnPsPD
3r
Analyte mg/I mgA % %
MBAS ND ND 1 0.000 20
Q
GIc
(LCS)93763484-2 02/24/2212:24
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I m57 % %
MBAS 1.00 0929 92.9 85.0-115
SC
•
(OS)L1464280-03 02/24/22 12 30•(MS)93763484-4 02/24/221230•(MSD)R3763484-5 02/24/2212:32
Spike Amount 0rginal Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mgA mg/I mg/I % % % % %
MBAS 100 ND 0.980 0.971 98.0 97.1 1 85.0-115 0923 20
ACCOUNT: PROJECT: SOG: DATE/TIME PAGE
Soil 8 Env Consultants-Relegh.NC GW-1 10 61-2 0 0 L1464280 03/07/22 0924 17 of 30

•
WG1823129 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS) by Method 6200E-2011
(MB)R3753524-5 02/24/2211:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/1 mg/1 mg/I
Acetone U 0.0113 0.0500
Acrolem U 0.00254 0.0500 -S5
Acrylomtr/e U 0.000671 0.0100
Benzene U 0.0000941 0.00100 4
Bromobenzene U 0.000118 0.00100 Cn
Bromodichlorornethane U 0.000136 0.60100
Bromoform U 0.000129 0.00100
Sr
Bromornethene U 0.000605 0.00500
n-Butylbenzene U 0.000157 0.00100
sec-eutylbenzene U 0.000125 0.00100 Oc
ten-Butylbenzene U 0.000127 0.00100
Carbon tetrachloride U 0.000128 0.00100 -GI
Chlorobenzene U 0.000116 0.00100
Chloroddbromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500
Chloroform U 0.000111 0.00500 '
Chloromethane U 0.000960 0.00250 SC
2-Chbrotoluene U 0.000106 0.00100
4-Chbrotoluene U 0.000114 0.00100
1,2-Dibromo-3-Chloropropane U 0.000276 0.00500
1,2-Dibromoethane U 0.000126 0.00100 !!
Dibrorrarnetharle U 0.000122 0.00100
1.2-Dchlorobenzene U 0.000107 0.00100
1,3-Dichbrobenzene U 0.000110 0.00100
1,4-Dehlorabenzene U 0.000120 0.00100
Dlchbrod8luoromethane U 0.000374 0.00500
1,1-Drchbroethane U 0.000100 0.00100
1,2-Dlchloroethane U 0.0000819 0.00100
• 1,1-Drchloroethene U 0.000188 0.00100
cis-1,2-0ichbrcethene U 0.000126 0.00100
trans-1,2-Drchloroethene U 0.000149 0.00100
1,2-0ichloropropane U 0.000149 0.00100
1,1-Dichbropropene U 0.000142 0.00100
13-Dichbropropane U 0.000110 0.00100
•
2,2-Dichloropropane U 0.000161 0.00100
• UI-Isopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Helmchloro-1,3-butadiene U 0.000337 0.00100 I
Isopropylbenzene U 0.000105 0.00100 •
p-sopropyltoluene U 0.000120 0.00100
ACCOUNT: PROJECT: SD& DATE/TIME PAGE
Sod&Env Consuttents-Relegh,NC GW-1 1061-2 0 0 L1464280 03/07/22 09 24 18 of 30

WG1823129 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 62008-2011 ,J4
(MB)R3763524-5 02/24/2211:32
M8 Result MB Qualifier M8 MDL MB RDL
Analyte mg/I mg/I mg/I
2-Butanone(MEK) U 0.00119 0.0100
MethyleneChbnde U 0.000430 0.00500 Ss
4-Methyl-2-pentanone(MIRK) U 0.000478 0.0100
Methyl tent-butyl ether U 0.000101 0.00100 4 Cn
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.0000993 0.00100
Styrene U 0.000118 0.00100 Sr
1,1,1,2-Tetrachbroethane U 0.000147 0.00100
1,1,2,2-Tetrachloroethane U 0.000133 0.00100 ^
-
Ietrachloroethene U 0.000300 0.00100 Qc
Toluene U 0.000278 0.00100
1,2,3-Trichlorobenzene U 0.000230 0.00100 GI
1,2,4-Inchlorobenzene U 0.000481 0.00100
1,1,1-Trlchloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Irichbroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500 Sc.
1,2,3-Trichloropropane U 0.000237 0.00250
1,2.4-Tnmethylbenzene U 0.000322 0.00100
1,35-Trimethylbenzene U 0.000104 0.00100
Vinyl chloride U 0.000234 0.00100
o-Xylene U 0.000174 0.00100
m&p-Xylenes U 0.000430 0.00200
(S)Toluene-ae 95.9 80.0-120
(5)4Bromolluorobenzene 106 77.0-126
(5)1,2-0xhlo/oethaned4 105 70.0-170
(LCS)93763524-1 02/24/22 09:47•(LCSD)93763524-2 02/24/22 10:07
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/l mg/I % % % % %
Acetone 0.0250 0.0279 0.0256 112 102 19.0-160 8.60 27
Acrolein 0.0250 0.0227 0.0221 90.8 88.4 10.0-160 2.68 26
Acrylomtnle 0.0250 0.0248 0.0239 99.2 95.6 55.0-149 3.70 20
Benzene 0.00500 0.00488 0.00489 97.6 972 70.0-123 0.205 20
Bromobenzene 0.00500 0.00376 0.00363 75.2 72.6 73.0-121 _ 3.52 20
Bromodkhloromethane 0.00500 0.00481 0.00494 96.2 98.8 75.0-120 2.67 20
Bromoform 0.00500 0.00384 0.00386 76.8 77.2 68.0-132 0.519 20
ACCOUNT: PROJECT: SD& DATE/TIME PAGE
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L
WG1823129 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 62008-2011 -
(LCS)R3763524-1 02/24/22 09 47•(LCSD)R3763524-2 02/24/22 10:07 _.._ _,
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/1 mg/I % % % % %
Bromomethane 0.00500 0.00462 0.00471 92.4 94.2 10.0-160 1.93 25
n-Butylbenzene 0.00500 0.00375 0.00356 75.0 71.2 73.0-125 _ 5.20 20 •SS
sec-eutylbentene 0.00500 0.00416 0.00405 83.2 81.0 75.0-125 2.68 20
tert-Butylbenzene 0.00500 0.00443 0.00411 88.6 82.2 76.0-124 7.49 20 4
Carbon tetrachloride 0.00500 0.00480 0.00514 96.0 103 68.0-126 6.84 20 Cn
Chlorobenzene 0.00500 0.00455 0.00470 91.0 94.0 80.0-121 3.24 20
Chlorodbromomethane 0.00500 0.00454 0.00439 90.8 872 77.0-125 3.36 20 Sr
Chloroethane 0.00500 0.00435 0.00431 87.0 86.2 47.0-150 0924 20
Chloroform 0.00500 0.00510 0.00510 102 102 73.0-120 0.000 20
Chloromethane 0.00500 0.00413 0.00406 82.6 81.2 41.0-142 1./1 20
III
2-Chbrbtoluene 0.00500 0.00412 0.00394 82.4 78.8 76.0-123 4.47 20
4-Chlorotoluene 0.00500 0.00409 0.00373 81.8 74.6 75.0-122 - 9.21 20 'GI
1,2-0bromo-3-Chloropropane 0.00500 0.00392 0.00372 78.4 74.4 58.0-134 5.24 20
1,2-Dibromoethane 0.00500 0.00479 0.00462 95.8 92.4 80.0-122 3.61 20
Drbromomathane 0.00500 0.00524 0.00494 105 98.8 80.0-120 5.89 20
1,2-Dlchlorobenzene 0.00500 0.00453 0.00439 90.6 87.8 79.0-121 3.14 20
1,3-0rchbrobentene 0.00500 0.00441 0.00423 88.2 84.6 79.0-120 4.17 20 Sc
14-0rchlorobenzene 0.00500 0.00430 0.00412 86.0 82.4 79.0-120 4.28 20
Drchbrodrtuoromethane 0.00500 0.00561 0.00526 112 105 51.0-149 6.44 20
11-0rchdroethane 0.00500 0.00470 0.00453 94.0 90.6 70.0-126 3.68 20
1,2-0Ihloroethane 0.00500 0.00500 0.00495 100 99.0 70.0-128 1.01 20
11-Dlchloroethene 0.00500 0.00480 0.00431 96.0 86.2 71.0-124 10.8 20
cis-1,2-Drchbroethene 0.00500 0.00492 0.00478 98.4 95.6 73.0-120 229 20
trans-1,2-0Ichloroethene 0.00500 0.00478 0.00465 95.6 93.0 73.0-120 2.76 20
1,2-Dchloropropane 0.00500 0.00454 0.00468 90.8 93.6 77.0-125 3.04 20•
1,1-Dlchloropropene 0.00500 0.00467 0.00467 93.4 93.4 74.0-126 0.000 20
1,3-Drchbropropane 0.00500 0.00438 0.00444 87.6 88.8 80.0-120 1.36 20
2,2-0lchloropropane 0.00500 0.00485 0.00463 97.0 92.6 58.0-130 4.64 20
Di-isopropyl ether 0.00500 0.00492 0.00456 98.4 91.2 58.0-138 7.59 20
Ethylbenzene 0.00500 0.00453 0.00450 90.6 90.0 79.0-123 0.664 20
Henachloro-1,3-butadiene 0.00500 0.00396 0.00398 79.2 79.6 54.0.138 0504 20
Isopropylbenzene 0.00500 000481 0.00461 96.2 92.2 76.0-127 4.25 20
p-Isopropyttoluene 0.00500 0.00423 0.00405 84.6 81.0 76.0-125 4.35 20
2-8utanone(MEK) 0.0250 0.0247 0.0239 98.8 95.6 44.0-160 3.29 20
MethyleneChbnde 0.00500 0.00516 0.00510 103 102 67.0-120 1.17 20
4-Methy1-2-pentanone(MIBKJ 0.0250 0.0238 0.0230 95.2 92.0 68.0-142 3.42 20
Methyl tert-butyl ether 0.00500 0.00532 0.00528 106 106 68.0-125 0.755 20
Naphthalene 0.00500 0.00356 0.00383 71.2 76.6 54.0-135 7.31 20
n-Propylbenzene 0.00500 0.00421 0.00393 84.2 78.6 77.0-124 6.88 20
Styrene 0.00500 0.00423 0.00415 84.6 83.0 73.0-130 1.91 20
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE
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l
WG1823129 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 62008-2011 ' 12,f13,U4
(LCS)R3763524-1 02/24/22 09:47•(L050)R3763524-2 02/24/22 10:07
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/1 mg/I % % % % % 1
1,1,1,2-Tetrachbroethane 0.00500 0.00470 0.00493 94.0 98.6 75.0-125 4.78 20
11,2,2-Tetrachloroethane 0.00500 0.00384 0.00360 76.8 72.0 65.0-130 6.45 20 SS
letrachloroethene 0.00500 0.00482 0.00466 96.4 93.2 72.0-132 3.38 20
Toluene 0.00500 0.00463 0.00444 92.6 88.8 79.0.120 4.19 20
,
1,2,3-Trichlorobenzene 0.00500 0.00360 0.00391 72.0 78.2 50.0-138 826 20 Cn
1.24-Trrchlorobenzene 0.00500 0.00381 0.00386 76.2 77.2 57.0-137 1.30 20
1,1,1-Tnchloroethane 0.00500 0.00526 0.00518 105 104 73.0-124 1.53 20 Sr
1,1,2-Tric hloroethane 0.00500 0.00443 0.00433 :•:.6 86.6 80.0-120 2.28 20
Trichbroethene 0.00500 0.00523 0.00526 105 105 78.0-124 0572 •20
Tnchbrofluoromethane 0.00500 0.00541 0.00505 108 101 59.0-147 6.:: 20 Oc
1,2,3-Trichloropropane 0.00500 0.00436 0.00421 87.2 84.2 73.0-130 3.50 20
1,24-Trimethylbenzene 0.00500 0.00414 0.00403 82.8 80.6 16.0-121 2.69 20 'GI
1,35-Trimethylbenzene 0.00500 0.00429 0.003139 858 77.8 76.0-122 9.78 20
Vinyl chloride 0.00500 0.00446 0.00424 89.2 84.8 67.0-131 5.06 20
o-X94ene 0.00500 0.00439 0.00451 87.8 90.2 80.0-122 2.70 20 _.
m8p-Xy4enes 0.0100 0.00951 0.00913 95.1 91.3 80.0-122 4.08 20
51Toluene-d8 96.3 94.5 80.0-120 SC
($)4Bromofluorobenzene 104 107 77.0-126
(5)1.2-Drchloroethoned4 105 105 70.0-130
(OS)L1464401-02 02/24/22 18:11.(MS)R3763524-6 02/24/22 2018•(MSD)R3763524-7 02/24/22 20:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Oualifer MSD Qualifier RPD RPD Limits
Analyte mg/I mg/l mg/I Nil % % % % %
Acetone 0.0250 ND ND ND 133 172 1 10.0-160 _ 26.0 35
Acrolein 0.0250 ND ND ND 0.000 0.000 1 10.0-160 _ _ 0.000 39
Acrylonitnle 0.0250 ND 0.0216 0.0281 86.4 112 1 21.0-160 26.2 32
Benzene 0.00500 NO 0.00534 0.00625 107 125 1 17.0-158 15.7 27
Bromobenzene 0.00500 ND 0.00342 0.00440 68.4 :4.0 1 30.0-149 25.1 28
Bromodchloromethane 0.00500 ND 0.00487 0.00606 97.4 121 1 31.0-150 21.8 27
Bromoform 0.00500 ND 0.00357 0.00463 71.4 92.6 1 29.0-150 25.9 29
8ronamethane 0.00500 ND ND ND 54.6 69.6 1 10.0-160 24.2 38 1
n-Butylbenzene 0.00500 ND 0.00430 0.00515 86.0 103 1 31.0-150 18.0 30
sec-8utylbenzene 0.00500 ND 0.00387 0.00513 77.4 103 1 33.0-155 28.0 29 •
tert-Butylbenzene 0.00500 ND 0.00371 0.00529 74.2 106 1 34.0-153 _ 35.1 28
Carbon tetrachloride 0.00500 ND 0.00530 0.00638 106 128 1 23.0-159 18.5 28
Chlorobenzene 0.00500 NU 0.00418 0.00555 83.6 111 1 33.0-152 _ 28.2 27
Chlorodrbromomethane 0.00500 ND 0.00415 0.00526 83.0 105 1 37.0-149 23.6 27
ACCOUNT: PROJECT: SDG: DATE ME PAGE
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k
WG1823129 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 62008.2011
- - I
(OS)L1464401-02 02/24/221811•(MO)R3763524-6 02/24/22 20:18•(MSD)R3 763 52 4-7 0 2/24/22 2 20:39
Spike Amount Original Result MS Result MSD Resuk MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits i
Analyte mg/I mg7 mg/I mg71 % % % % %
Chloroethane 0.00500 ND 0.00517 0.00618 103 124 1 10.0-160 17.8 30 1
Chloroform 0.00500 ND 0.00514 0.00639 103 128 1 29.0-154 212 28 Ss
Chloromethane 0.00500 NU 0.00394 0.00478 78.8 95.6 1 10.0-160 19.3 29
2-Chbrotoluene 0.00500 ND 0.00362 0.00484 72.4 96.8 1 32.0-153 28.8 28 • 4
4-Chbrotoluene 0.00500 ND 0.00348 0.00468 69.6 93.6 1 32.0-150 _ 29.4 28 Cn
1,2-Dibromo-3d3doropropane 0.00500 ND ND 0.00500 84.0 100 1 22.0-151 17.4 34
1,2-Dlbromoethane 0.00500 ND 0.00426 0.00542 85.2 108 1 34.0-147 24.0 27 Sr
Dibrorr omethane 0.00500 ND 0.00494 0.00575 98.8 115 1 30.0-151 15.2 27
1,2-0-chlorobenzene 0.00500 ND 0.00419 0.00562 83.8 112 1 34.0-149 - 29.2 28
1,3-Dichlorobenzene 0.00500 NU 0.00369 0.00510 73.8 102 1 36.0-146 _ 32.1 27 Cc
1,4-Dchlorobenzene 0.00500 ND 0.00372 0.00497 74.4 99.4 1 35.0-142 - 28.8 27
Dichbrodifluoromethane 0.00500 ND 0.00585 0.00743 117 149 1 10.0-160 23.8 29 'G(
1,1-Dichloroethane 0.00500 ND 0.00456 0.00582 91.2 116 1 25.0-158 24.3 27
1,2-Dchbroethane 0.00500 ND 0.00472 0.00590 94,4 118 1 29.0-151 22.2 27 •
1,1-Dichloroethene 0.00500 ND 0.00474 0.00577 94.8 115 1 11.0-160 19.6 29 -
cis-1,2-0Ichbroethene 0.00500 NU 0.00477 0.00604 95.4 121 1 10.0-160 23.5 27
trans-1,2-Drchloroethene 0.00500 ND 0.00444 0.00587 88.8 117 1 17.0-153 - 27.7 27 SC
1,2-Dchloropropane 0.00500 ND 0.00464 0.00571 92.8 114 1 30.0-156 20.7 27
1,1-0rchbropropene 0.00500 ND 0.00469 0.00599 93.8 120 1 25.0-158 24.3 27
1,3-Dichbropropane 0.00500 ND 0.00422 0.00516 84.4 103 1 38.0-147 20.0 27
2,2-Dichloropropane 0.00500 ND 0.00476 0.00614 95.2 123 1 24.0-152 25.3 29
Dr-isopropyl ether 0.00500 ND 0.00492 0.00615 98.4 123 1 21.0-160 22.2 28
6thylbenzene 0.00500 NO 0.00578 0.00623 116 125 1 30.0-155 7.49 27
Neuechloro-1,3-butadrene 0.00500 ND 0.00430 0.00554 86.0 111 1 20.0-154 25.2 34
Isopropylbenzene 0.00500 ND 0.00447 0.00581 89.4 116 1 28.0-157 26.1 27
pasopropykoluene 0.00500 ND 0.00405 0.00537 81.0 107 1 30.0-154 28.0 29
2-Butanone(MEK) 0.0250 ND 0.0309 0.0330 119 127 1 10.0-160 6.57 32
Methylene Chloride 0.00500 ND ND 0.00590 97.0 118 1 23.0-144 19.5 28
4-Methyl-2-pentanone(MI5K) 0.0250 ND 0.0230 0.0294 92.0 118 1 29.0-160 24.4 29
Methyl tert-butyl ether 0.00500 ND 000505 0.00669 101 134 1 28.0-150 27.9 29
Naphthalene 0.00500 ND 0.0144 0.00780 288 156 1 12.0-156 _ _ 59.5 35
n-Propylbenzene 0.00500 ND 0.00429 0.00523 85.8 105 1 31.0-154 19.7 28
Styrene 0.00500 ND 0.00392 0.00507 78.4 101 1 33.0-155 25.6 28
1,1,1,2-Tetrachloroethane 0.00500 ND 0.00472 0.00585 94.4 117 1 36.0-151 21.4 29
11,2,2-Tetrachloroethane 0.00500 ND 0.00210 0.00241 42.0 48.2 1 33.0-150 13.7 28
letrachloroethene 0.00500 NU 0.00426 0.00560 85.2 112 1 10.0-160 _ 27.2 27
Toluene 0.00500 ND 0.00713 0.00705 155 141 1 26.0-154 _ 9.20 28
1,2,3-Trrchlorobenzene 0.00500 ND 0.00355 0.00492 71.0 98.4 1 17.0-150 32.3 36
1.24-Trrchlorobenzene 0.00500 ND 0.00372 0.00504 74.4 101 1 24.0-150 301 33
1,1,1-Trrchloroethane 0.00500 ND 0.00559 0.00695 112 139 1 23.0-160 21.7 28
ACCOUNT: PROJECT: SOS DATE/TIME PAGE
Sod 8 Env Consultants-Raleigh.NC GW-11061-200 L1464280 03/07/22 09 24 22 of 30

WG1823129 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS) by Method 62008-2011 e0-01,02,n3,04
(OS)L1464401-02 02/24/22 18:11•(MS)R3763524-6 02/24/22 20:18•(MSD)43 763 524-7 02/24/22 20:39
Spike Amount original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits I
Anelyte mg/I mg/1 mg/I mg/1 % % % % % 1 I
1,1,2-Trichbroethane 0.0050.0 ND 0.00422 0.00539 84.4 108 1 35.0-147 24.3 27 I
Trtchbroethene 0.00500 ND 0.00705 0.00963 141 193 1 10D-160 30.9 25 SS
Trichbrofluoromethane 0.03500 ND 0.00583 0.00750 11/ 150 1 17.0-160 25.1 31
1,2,3-Trlchloropropane 0.00500 ND 0.00379 0.00524 75.8 105 1 34.0-151 _ 32.1 29 4
1,2,4-Tnmethylbenzene 0.00500 ND 0.00983 0.00694 197 139 1 26.0-154 _ _ 34.5 27 Cn
1,35-Tnmethylbenzene 0.00500 ND 0.00534 0.00564 107 113 1 28.0-153 5.46 27
Vinyl chloride 0.00500 ND 0.00463 0.00556 92.6 111 1 10.0-160 18.3 27 :Sr
o-Xylene 0.00500 ND 0.00675 0.00651 135 133 1 45.0-144 3.62 26
m&p-Xyfenes 0.0100 ND 0.0147 0.0136 147 136 1 43.0-146 _ 7.77 26
roh ene ae 93.7 930 e0.0-170 Cc
9)4Bromo1uorobenzene 103 102 770126
•
IS)12-De Nomethaned4 /05 107 700.130 GI
Sc
•
ACCOUNT: PROJECT: SOG DATE/TIME PAGE
Soil&Env Consultants-Raleigh.NC GW-1 1061-200 L1464280 03/07/22 09 24 23 of 30

WG1823716 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 62008-2011
-1
(MB)R3764423-2 02/25/2213:41 ! __.,
MB Result MB Qualifier MB MDL MB RDL
Analyte mgrl mgll mg/I
Acetone U 0.0113 0.0500
Acrolein U 0.00254 0.0500 Sy
Acrylonnnle U 0.000671 0.0100
Benzene U 0.0000941 0.00100
'.
BronmdEhloromethane U 0.000136 0.00100 Cn
Bromofdrm U 0.000129 0.00100
Carbon tetrachloride U 0.000128 0.00100 Sr
Chlorobenzene U 0.000116 0.00100
Chlorodrbromomethane U 0.000140 0.00100
Chloroethane U 0.000192 0.00500 QC
Chloroform U 0.000111 0.00500
-
Chloromethane U 0.000960 0.00250 GI
1,2-Drbromoethane U 0.000126 0.00100
Dibromomethane U 0.000122 0.00100
Dichbroddluoromethane U 0.000374 0.00500
1,1-Urchbroethane U 0.000100 0.00100
1.2-DKhloroethane U 0.0000819 0.00100 Sc.
1,1-Dichbroethene U 0.000188 0.00100
crs-1,2-Drchbroethene U 0.000126 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Drchloropropane U 0.000149 0.00100
1,1-Dichbropropene U 0.000142 0.00100
1,3-DKhloropropane U 0.000110 0.00100
2,2-Dichloropropane U 0.000161 0.00100
D:-:sopropyl ether U 0.000105 0.00100
Ethylbenzene U 0.000137 0.00100
Isopropylbenzene U 0.000105 0.00100
2-Butanone(MEK) U 0.03119 0.0100
Methylene Chbrbe U 0.000430 0.00500
4-Methy1-2-pentanone(MIBK) U 0.000478 0.0100
Methyl tert-butyl ether U 0.000101 0.00100
Styrene U 0.000118 0.00100
111.2-Tetrachloroethane U 0.000147 0.00100
Tetrachloroethene U 0.000330 0.00100
Toluene U 0.000278 0.00100
1,1,1-Inchloroethane U 0.000149 0.00100
1,1,2-Trichlaroethane U 0.000158 0.00100
Trichbroethene U 0.000190 0.00100
Tnchbrofluoromethane U 0.000160 0.00500
Vinyl chloride U 0.000234 0.00100
ACCOUNT: PROJECT: SDG DATE-RIME PAGE
Sod&Env Consultants-Raleigh.NC GW-11061-200 L1464280 03/07/22 09 24 24 of 30

•
•
4.
WG1823716 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 6200B-2011
(MR)93764423-2 02/25/22 13:41
MB Result MB Qualifier MB MDL MB RDL
Anelyte mg/ mg/I mg11
o-Xylene U 0.000174 0.00100
m&p-Xylenes U 0.000430 0.00200
(S)roluene-d8 102 80.0-120
(S)4Bromoluorobenzene 833 77.0-II6
(S)12-DKhloroethone-d4 107 70.0-130 Cn
Sr
(LCS)R3764423-1 02/25/22 12:56
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Qc
Anelyte mg/I mg/ % %
Acetone 0.0250 0.0234 93.6 19.0-160 GI
Acrolein 0.0250 0.0255 102 10.0-160
Acrylomtnle 0.0250 0.0232 92.8 55.0-149
Benzene 0.00500 0.00449 898 70.0-123
Bromodrchloromethane 0.00500 0.00423 84.6 75.0-120
Bromoform 0.00500 0.00447 89.4 68.0-132 'Sc
Carbon tetrachlor4e 0.00500 0.00439 87.8 68.0-126
Chlorobenzene 0.00500 0.00468 93.6 80.0-121
Chlorod:bromomethane 0.00500 0.00464 92.8 77.0-125
Chloroethane 0.00500 0.00449 89.8 47.0-150
Chloroform 0.00500 0.00458 91.6 73.0-120
Chloromethane 0.00500 0.00345 69.0 41.0-142
1,2-Dibromoethane 0.00500 0.00487 97.4 80.0-122
Dibromomethane 0.03500 0.00453 90.6 80.0-120
Drchbrodrfluoromethane 0.00500 0.00473 94.6 51.0-149
1,1-0rchbroethane 0.00500 0.00439 872 70.0-126
1,2-Dchloroethane 0.00500 0.00439 87.8 70.0-128
1,1-Dichbrcethene 0.013500 0.00431 . 86.2 71.0-124
crs-1,2-Dichbroethene 0.00500 0.00421 84.2 73.0-120
turns-1,2-Dichloroethene 0.00500 0.00458 91.6 73.0-120
1,2-0¢hloropropane 0.00500 0.00452 90.4 77.0-125
1,1-0¢hbropropene 0.00500 0.00455 91.0 74.0-126
1,3-Dichbropropane 0.00500 0.00463 92.6 80.0-120
2,2-Dichloropropane 0.00500 0.00463 92.6 58.0-130
Dr-rsoprapyl ether 0.00500 0.00429 85.8 58.0-138
Ethylbenzene 0.00500 0.00449 89.8 79.0-123
Isopropylbenzene 0.00500 0.00427 85.4 76.0-127
2-Butanane(MEK) 0.0250 0.0220 88.0 44.0-160
ACCOUNT: PROJECT: SDG DATE/TIME: PAGE
Sod&Env Consultants-Relegh.NC GW-11061-200 L1464280 03/07/22 09 24 25 of 30

WG1823716 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 6200E-2011 /1464280 .
(i_CSI R3764423-1 02/25/22 12:56 L___ _
Spike Amount LCS Result 1CS Rec. Rec.Limits LCS Qualifier
Arlalyte M911 mg11 % %
Methylene Chbr0e 0.00500 0.00432 86.4 67.0-120
4Methy1-2-pentanone(MIBK) 0.0250 0.0254 102 68.0-142 Sti
Methyl tert-butyl ether 0.00500 0.00404 80.8 68.0-125
Styrene 0.00500 0.00425 85.0 730-130
4
1,1,1,2-Tetrachbroethane 0.00500 0.00473 94.6 75.0-125 Cn
Tetrachloroethene 0.00500 0.00485 97.0 72.0-132
Toluene 0.00500 0.00467 93.4 79.0-120 Sr-
1,1,1-Tnchkmoethane 0.013500 0.00475 95.0 73.0-124
1,1,2-Tnchbroethane 0.00500 0.00489 97.8 80.0-120
Inchbroethene 0.00500 0.00446 89.2 78.0-124 Oc
Trlchlorotluoromethane 0.00500 0.00503 101 59.0.147
Vinyl chloride 0.00500 0.00444 88.8 67.0-131 GI
o-Xylene 0.00500 0.00411 82.2 80.0-122
m&p.Xytenes 0.0100 0.00871 87.1 80.0-122
(S)Toluene-d8 98.4 80.0-120
(S)4Bromoluorobenzene 86.7 77.0-46
(5)12-Drchloroethone44 107 70.0-130 Sc-
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE
Sal&Env.Consultants-Raleigh,NC GW-t 1061-200 L1464260 03/07/22 0924 26 of 30

WG1824738 QUALITY CONTROL SUMMARY
Volatile Organic Compounds(GC/MS)by Method 6200E-2011
(MB)03765258-3 03/01/22 10:26 ,
MB Result MB Qualifier MB MDL MB RDL 1.--7
Anah/te mg/l mph mg/I
8romomethane 3 0.000605 0.00500
(5)Toluene-d8 103 80.0-120 S,;
(S)4-Bromofluorobenzene 94.8 77.0-126
(S)1.2-Dchloroethaned4 96.8 70.0-130
Cn
(LCS)R3765258-1 03/01/22 09:26•(LCSD)03765258-2 03/01/22 09:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mgh mph mg/I % % % - 7. OC
Bromornethane 0.00500 0.00623 0.00586 125 117 10.0-160 - 25
(5)Toluene-d8 99.4 VI 80.0-20 GI
(S)4-Bromofluorobenzene 99.4 95.9 77.0-126
(S)12-Dchloroethone44 98.8 98.7 1120-130
Sc
ACCOUNT: PROJECT: SDGi DATE/TIME PAGE
Soil&Env Consultants-Raleigh.NC GW-11061-200 L1464280 03/0722 0924 27 of 30
1

` annuuunnuuuuuauutunluw
GLOSSARY OF TERMS
Guide to Reading and Understanding You' ,]boratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name,
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
Abbreviations and Definitions Ss
MDL Method Detection Limit.
4
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference. Sr
SDG Sample Delivery Group.
Surrogate(Surrogate Standard)-Analyses added to every blank,sample,Laboratory Control Sample/Duplicate and
(S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit(or MDL where applicable).
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the A
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the
result reported has already been corrected for this factor.
These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal SC
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary Control
analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(exduding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Semple Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination;spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is low.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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ACCREDITATIONS & LOCATIONS
Alabama 40660 Nebraska NE-OS-15-05 i
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey-NELAP TNO02
California 2932 New Mexico' TN00003
Colorado TN00003 New York 11742 SS
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina' DW21704 4
Georgia NELAP North Carolina' 41 Cn
Georgia' 923 North Dakota R-140
Idaho TN00003 Ohio-VAP CL0069
Illinois 200008 Oklahoma 9915 Sr
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356
Kentucky'6 KY90010 South Carolina 84004002
Kentucky' 16 South Dakota n/a 7
Louisiana A130792 Tennessee'' 2006 GI
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas 5 LAB0152
Maryland 324 Utah TN000032021-11 Al
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847 SC
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA-ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA-ISO 17025 5 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA-Crypto TN00003
'Drinking Water 'Underground Storage Tanks 'Aquatic Toxicity 'Chemical/Microbiological 5 Mold °Wastewater n/a Accreditation not applicable
•Not all certifications held by the laboratory are applicable to the results reported in the attached report.
'Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil&Env.Consultants-Raleigh.NC GW-1 1061-200 L1464280 03/07/22 09:24 29 of 30

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Company Name/Address Boling informaton Ana'vsis r Container/Pr sematve '.ham of Custody Page_of_
Soil&Env.Consultants- Raleigh, NC attn:Don Wells efP5
8412 Falls of Neuse Road Chk (,11 aceAnalytical
8412 Falls of Neuse Road,Suite 104 Suite 104
Raleigh,NC 27615-3543 Raleigh,NC 27615-3543
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GW-Groundwater B Bioassay Flow Other Bottles arrive intact: - t_N
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OW-(Yoking Water Samples returned via. Suf.facoer.t volume sent: GY—S
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