NC0021253_Permit (Modification)_20171215

NPDES DOCUMENT SCANNIN`: COVER SHEET
NC0021253
Havelock WWTP
NPDES Permit:
Document Type:
Permit Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Engineering Alternatives (EAA)
Correspondence
Owner Name Change
(RenewalApplication
,k-,,,,,,s,r„ao;i✓^.'?nv7�'4n'"-"nN'r'
Instream Assessment (67b)
Speculative Limits
Environmental Assessment (EA)
Document Date:
December 15, 2017
This document is printed on reuse paper - ignore any
content on the revrerse side

CITY OF HAVELOCK
Post Office Box 368
1 Governmental Ave.
Havelock, NC 28532
December 15, 2017
Water Quality Permitting Section — NPDES
Division of Water Resources
North Carolina Department of Environmental Quality
1617 Mail Service Center Raleigh, NC, 27699-1617
Re: NPDES Permit Renewal Application (NC0021253)
City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
To whom it may concern:
DIDEN�DR
R,�D�tiV�
DEC VI 2011
Water Resgeton
ces
Permitting
The City of Havelock Public Services Department is permitted to discharge 2.25 million gallons per day (mgd) of
treated effluent from the City of Havelock Wastewater Treatment Plant (WWTP) to the Neuse River under North
Carolina NPDES Permit NC0021253. This NPDES permit is scheduled to expire on June 30, 2018. The enclosed
application is for the renewal of this permit. In accordance with the requirements of federal (40 CFR 122) and state
(15A NCAC 2H .0105(3)) regulations, we are submitting three signed copies of the completed application package
and associated attachments and figures. The application package includes the following information:
• NPDES Permit Application — EPA Form 2A
• EPA Form 2A Additional Information (Process Narrative, Topographic Map, and Process Flow Diagrams)
• City of Havelock WWTP Sludge Management Plan
• First Species Effluent Toxicity Testing, 2015-2017
• Annual Priority Pollutant Analysis Results, 2014-2017
• Technical Memorandum in support of the Reduction of Monitoring Frequency for Exceptionally Performing
Facilities
At the time of this application submittal, the required second species toxicity testing events have not yet been
completed. The four second species effluent toxicity tests are currently scheduled to be completed in December 2017,
January 2018, March 2018, and May 2018. When the toxicity test results become available, they will be forwarded to
the Division of Water Resources (DWR) along with revisions to Part E of EPA Form 2A to include these results. All
second species toxicity tests will be submitted prior to the current permit expiration date of June 30, 2018.
A sample for the annual priority pollutant analysis was not taken in 2016. In it's place, a second sample was taken in
early December 2017. The annual priority pollutant analysis section is currently based on data collected in 2014, 2015,
and 2017. Part D of form 2A as well as Tab E will be updated to replace the 2014 data with the additional 2017 data
when that data becomes available.
Phone [phone]
www.havelocknc.us Fax [phone]

In accordance with ISA NCAC 2B .0508(b)(I) and the October 2012 DWR Guidance Document for the Reduction of
Monitoring Frequency for Exceptionally Performing Facilities, the City of Havelock respectfully requests a reduction
in frequency monitoring for total suspended solids (TSS), ammonia (NH3-N), and fecal coliform. Effluent sampling
results from the past three years demonstrate that all state and regulatory and guidance requirements have been met in
support of this request. A complete summary of the sampling data and analysis for the reduction of monitoring
frequency is attached in Tab G of this application.
If you have any questions regarding anyof the NPDES permit renewal application materials, please contact me at (252)
444-6409 or msavaer(&havelocknc.us.
Sincerely,
Mark Sayger
Public Services Director
Attachments
cc:
Raymond Burgos, City of Havelock
Mary Sadler, Hazen and Sawyer
Todd Davis, Hazen and Sawyer
Ted Elshof, Hazen and Sawyer
Phone [phone]
www.havelocknc.us Fax [phone]

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
EPA Form 2A, NPDES Renewal Application December 2017

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
FORM
2A
NPDES
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
NPDES FORM 2A APPLICATION OVERVIEW
APPLICATION OVERVIEW
Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet
and a "Supplemental Application Information" packet. The Basic Application Information packet is divided
into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or
equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental
Application Information packet. The following items explain which parts of Form 2A you must complete.
BASIC APPLICATION INFORMATION:
Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works
that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12.
B. Additional Application Information for Applicants with a Design Flow 2 0.1 mgd. All treatment works that have design flows
greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6.
C. Certification. All applicants must complete Part C (Certification).
SUPPLEMENTAL APPLICATION INFORMATION:
D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets
one or more of the following criteria must complete Part D (Expanded Effluent Testing Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to provide the information.
Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing
Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to submit results of toxicity testing.
Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any
significant industrial users (SlUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges
and RCRA/CERCLA Wastes). Sills are defined as:
1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40
CFR Chapter I, Subchapter N (see instructions); and
2. Any other industrial user that:
a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain
exclusions); or
b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic
capacity of the treatment plant; or
c. Is designated as an SIU by the control authority.
. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer
Systems).
ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION)
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 1 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WVVTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
BASIC APPLICATION INFORMATION
PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS:
All treatment works must complete questions Al through A.8 of this Basic Application Information Packet.
A.1. Facility Information.
Facility Name City of Havelock Wastewater Treatment Plant
Mailing Address P.O. Box 368, Havelock NC 28532
Contact Person Raymond Burgos
Title Wastewater Treatment Plant B-ORC
Telephone Number j252) 444-6421
Facility Address 304 North Jackson Dr.
(not P.O. Box) Havelock, NC 28532
A.2. Applicant Information. If the applicant is different from the above, provide the following:
Applicant Name City of Havelock
Mailing Address P.O. Box 368
Havelock. NC 28532
Contact Person Mark Samar
Title Public Services Director
Telephone Number j252) 444-6409
Is the applicant the owner or operator (or both) of the treatment works?
0 owner 0 operator
Indicate whether correspondence regarding this permit should be directed to the facility or the applicant.
0 facility ® applicant
A3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works
(include state -issued permits).
NPDES NC0021253 PSD 09110G01 (General Air Permit)
UIC Other WQ0000702 (Land Application Permit)
RCRA Other WQCS00104 (Collection System Permit)
A4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each
entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.).
Name Population Served Type of Collection System Ownership
Havelock, NC 12,500 Separate Municipal
Total population served 12,500
EPA Fomi 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 2 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
A.5. Indian Country.
a. Is the treatment works located in Indian Country?
❑ Yes ®No
b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through)
Indian Country?
❑ Yes ®No
A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the
average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period
with the 12th month of "this year" occurring no more than three months prior to this application submittal.
a. Design flow rate 2.25 mgd
Two Years Alto
(10/1/2014 - 9/30/2015)
b. Annual average daily flow rate 1.377
Last Year This Year
(10/1/2015 - 9/30/2016) (10/1/2016 - 9/30/2017)
1.356 1.304
c. Maximum daily flow rate 2.810 3.161 3.233
A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent
contribution (by miles) of each.
® Separate sanitary sewer 100
❑ Combined storm and sanitary sewer N/A
A8. Discharges and Other Disposal Methods.
a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes ❑ No
If yes, list how many of each of the following types of discharge points the treatment works uses:
i. Discharges of treated effluent
1
ii. Discharges of untreated or partially treated effluent 0
iii. Combined sewer overflow points
iv. Constructed emergency overflows (prior to the headworks)
v. Other
b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments
that do not have outlets for discharge to waters of the U.S.? ❑ Yes
If yes, provide the following for each surface impoundment:
Location:
0
0
N/A
® No
Annual average daily volume discharge to surface impoundment(s) mgd
Is discharge ❑ continuous or 0 intermittent?
c. Does the treatment works land -apply treated wastewater? ❑ Yes ® No
If yes, provide the following for each land application site:
Location:
Number of acres:
Annual average daily volume applied to site:
Is land application ❑ continuous or ❑ intermittent?
d. Does the treatment works discharge or transport treated or untreated wastewater to another
treatment works? ❑ Yes
mgd
® No
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 3 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock INWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works
(e.g., tank truck, pipe).
NIA
If transport is by a party other than the applicant, provide:
Transporter Name
Mailing Address
Contact Person
Title
Telephone Number ( )
For each treatment works that receives this discharge, provide the following:
Name
Mailing Address
Contact Person
Title
Telephone Number ( 1
If known, provide the NPDES permit number of the treatment works that receives this discharge
Provide the average daily flow rate from the treatment works into the receiving facility. mgd
e. Does the treatment works discharge or dispose of its wastewater in a manner not included
in A.B. through A.8.d above (e.g., underground percolation, well injection):
If yes, provide the following for each disposal method:
Description of method (including location and size of site(s) if applicable):
Annual daily volume disposed by this method:
❑ Yes ® No
Is disposal through this method ❑ continuous or ❑ intermittent?
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 4 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
WASTEWATER DISCHARGES:
If you answered "Yes" to question A.8.a, complete questions A.9 throuqh A.12 once for each outfall (including bypass points) through
which effluent Is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question
A.8.a, go to Part B. "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd."
A.9. Description of Duffel!.
a. Outfall number 002
b.
Location City of Havelock 28532
(City or town, if applicable) (Zip Code)
Craven NC
(County) (State)
34°57'11' 76°52'37"
(Latitude) (Longitude)
c. Distance from shore (if applicable) 2.040 ft.
d. Depth below surface (if applicable) 10 ft.
e. Average daily flow rate 1.4 mgd
f. Does this outfall have either an intermittent or a periodic discharge? 0 Yes ® No (go to A.9.g.)
If yes, provide the following information:
Number f times per year discharge occurs:
Average duration of each discharge:
Average flow per discharge: mgd
Months in which discharge occurs:
g. Is outfall equipped with a diffuser? ® Yes ❑ No
A.10. Description of Receiving Waters.
a. Name of receiving water Neuse River
b. Name of watershed (if known) Neuse River
United States Soil Conservation Service 14-digit watershed code (if known):
c. Name of State Management/River Basin (if known): Neuse River
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
d. Critical low flow of receiving stream (if applicable)
acute Unknown
cfs
03020204050020
03020204
chronic Unknown cfs
e. Total hardness of receiving stream at critical low flow (if applicable): Unknown mg/I of CaCO3
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 5 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
A.11. Description of Treatment
a. What level of treatment are provided? Check all that apply.
❑ Primary ® Secondary
El Advanced ® Other. Describe: Denitrification filters
b. Indicate the following removal rates (as applicable):
Design BOD5 removal or Design CBOD5 removal 96
Design SS removal 84
Design P removal 78
Design N removal 91% at current design flow of 2.25 mgd
Other N/A
c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe:
Ultraviolet Disinfection
If disinfection is by chlorination is dechlorination used for this outfall? ❑ Yes ❑ No
Does the treatment plant have post aeration? El Yes 0 No
A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following
parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is
discharged. Do not include information on combined sewer overflows in thls section. All Information reported must be based on data
collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of
40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a
minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart.
Outfall number: 002
PARAMETER
MAXIMUM DAILY VALUE
AVERAGE DAILY VALUE
Value
Units
Value
Units
Number of Samples
pH (Minimum)
6.10
s.u.
XSPOMMeMifii...siiiingimet.401.3.1020.16.1.13001%.,
pH (Maximum)
8.30
s.u.
� _.
w" "
Flow Rate
3.16
mgd
1.46
mgd
1,093
Temperature(Winter)
23.90
°C
17.16
°C
227
Temperature (Summer)
28.60
°C
23.79
°C
446
' For pH please report a minimum and a maximum daily value
POLLUTANT
MAXIMUM DAILY
DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Conc.
Units
Conc.
Units
Number of
Samples
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
BIOCHEMICAL OXYGEN
DEMAND (Report one)
BOD5
63.00
mg/L
2.74
mg/L
728
SM 5210B
ML
CBOD5
NIA
N/A
N/A
N/A
N/A
N/A
N/A
FECAL COLIFORM
1210
No./
100mL
10.088
No./
100mL
718
SM 9222D
ML
TOTAL SUSPENDED SOLIDS (TSS)
22
mg/L
2.64
mg/L
734
SM 2540D
ML
END OF PART A.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 6 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
BASIC APPLICATION INFORMATION
PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR
EQUAL TO 0.1 MGD (100,000 gallons per day).
All applicants with a design flow rate 2 0.1 mgd must answer questions B.1 through 8.6. All others go to Part C (Certification).
B.1. Inflow and Infiltration. Estimate the average number of gallons per day
230,000 gpd
that flow into the treatment works from inflow and/or infiltration.
and rehabilitate sources of I/1 in their collection system.
Briefly explain any steps underway or planned to minimize inflow and infiltration.
The City of Havelock is maintaining ongoing efforts to identify
B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This
map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire
area.)
Please reference Figure 1 for topographic map and Figure 2 for plant site map.
a. The area surrounding the treatment plant, including all unit processes.
b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which
treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable.
c. Each well where wastewater from the treatment plant is injected underground.
d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within 'A mile of the property boundaries of the treatment
works, and 2) listed in public record or otherwise known to the applicant.
e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed.
f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail,
or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed.
B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all
backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g.,
chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow
rates between treatment units. Include a brief narrative description of the diagram.
Please reference Figure 3 through Figure 5 for process flow diagram and the "Additional Information" sheets for process description.
8.4. Operation/Maintenance Performed by Contractor(s).
Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a
contractor? El Yes ❑ No
If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional
pages if necessary).
Name: Svnagro
Mailing Address: 284 Boger Road
Mocksville, NC 27028
Telephone Number. [phone]
Responsibilities of Contractor: Remove and land apply biosolids to permitted sites
B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or
uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the
treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5
for each. (If none, go to question B.6.)
a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule.
N/A
b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies.
❑ Yes ❑ No
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 7 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable).
N/A
as applicable.
as applicable.
since
to 2.8
cycle.
Yes El No
d. Provide dates imposed
For improvements
Indicate dates as
Implementation Stage
- Begin Construction
End Construction
- Begin Discharge
- Attain Operational
e. Have appropriate
Describe briefly:
by any compliance schedule or any actual dates
planned independently of local, State, or Federal
accurately as possible.
Schedule Actual Completion
MM/DD/YYYY MM/DD/YYYY
of completion
agencies, indicate
Plant expansion
the 2014
mgd or 3.5
requirements
for the implementation steps listed below,
planned or actual completion dates,
to 2.25 mgd has been completed
NPDES Permit Renewal. Expansion
mgd are not planned for this permit
been obtained? ❑
N/A N/A
NIA N/A
N/A N/A
Level N/A N/A
permits/clearances concerning other Federal/State
B.6. EFFLUENT TESTING DATA
Applicants that discharge
effluent testing required
on combine sewer overflows
using 40 CFR Part 136
QA/QC requirements for
based on at least three
Outfall Number:
(GREATER THAN 0.1 MGD
to waters of the US must
by the permitting authority
in this section. All information
methods. In addition, this data
standard methods for analytes
pollutant scans and must be
002
ONLY).
provide effluent testing data for the following parameters. Provide
for each outfall through which effluent is discharged. Do not include
the indicated
information
conducted
other appropriate
data must be
reported must be based on data collected through analysis
must comply with QA/QC requirements of 40 CFR Part 136 and
not addressed by 40 CFR Part 136. At a minimum effluent testing
no more than four and on -half years old.
POLLUTANT
MAXIMUM DAILY
DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MLIMDL
Conc.
Units
Conc.
Units
Number of
Samples
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
AMMONIA (as N)
11.40
mg/L
0.118
mg/L .
735
EPA 350.1
ML 0.5/1.0
CHLORINE (TOTAL
RESIDUAL, TRC)
N/A
N/A
N/A
N/A
N/A
N/A
N/A
DISSOLVED OXYGEN
4.80
mg!L
7.58
mg/L
661
SM 4500-H+B
MDL>5.0
TOTAL KJELDAHL
NITROGEN (TKN)
35.00
mg/L
1.287
mg/L
153
EPA 351.2
AL 21,400 Ibs
TN
NITRATE PLUS NITRITE
NITROGEN
y 1
mglL
2.97
mg/L
152
EPA 353.2
AL 21,400 Ibs
TN
OIL and GREASE
N/A
N/A
N/A
NIA
N/A
N/A
N/A
PHOSPHORUS (Total)
2.97
mg!L
0.70
mg/L
151
EPA 365.4
QL 0.7/1.0
TOTAL DISSOLVED SOLIDS
(TDS)
N/A
N/A
N/A
NIA
NIA
NIA
N/A
OTHER
N/A
N/A
N/A
N/A
N/A
N/A
N/A
END OF PART B.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 8 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED: RIVER BASIN:
Renewal Neuse River
BASIC APPLICATION INFORMATION
PART C. CERTIFICATION
All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this
certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which
parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed
Form 2A and have completed all sections that apply to the facility for which this application is submitted.
Indicate which parts of Form 2A you have completed and are submitting:
El Basic Application Information packet Supplemental Application Information packet:
El Part D (Expanded Effluent Testing Data)
® Part E (Toxicity Testing: Biomonitoring Data)
❑ Part F (Industrial User Discharges and RCRA/CERCIA Wastes)
O Part G (Combined Sewer Systems)
ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION.
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment
for knowing violations.
Name and official title Frank Bottorff
Signature f
Telephone number [phone]
Date signed
6e4V
Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment
works or identify appropriate permitting requirements.
SEND COMPLETED FORMS TO:
NCDENR/ DWQ
Attn: NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22.
Page 9 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
SUPPLEMENTAL APPLICATION INFORMATION
PART D. EXPANDED EFFLUENT TESTING DATA
Refer to the directions on the cover page to determine whether this section applies to the treatment works.
Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required
to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following
pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which
effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected
through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and
other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below
any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant
scans and must be no more than four and one-half years old.
See attached analytical results in Tab E
Outfall number: 002 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS.
ANTIMONY
< 3.0
pglL
< 0.056
lb/d
< 3.0
pg/L
< 0.056
lb/d
3
200.8
3
ARSENIC
< 5.0
pg/L
< 0.094
lb/d
< 5.0
pglL
< 0.094
lb/d
3
3113B-04
5
BERYLLIUM
2.0
pg/L
0.0375
lb/d
< 1.33
pglL
< 0.025
lb/d
3
200.7
1
CADMIUM
< 1.0
pg/L
< 0.019
lb/d
< 1.0
pglL
< 0.019
lb/d
3
3113B-04
1
CHROMIUM
< 5.0
pg/L
< 0.094
lb/d
< 5.0
pg/L
< 0.094
lb/d
3
200.7
5
COPPER
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
200.7
10
LEAD
< 5.0
Ng/L
< 0.094
lb/d
< 5.0
pg/L
< 0.094
lb/d
3
3113B-04
5
MERCURY
< 1.0
pglL
< 0.019
lb/d
< 1.0
pg/L
< 0.019
lb/d
7
1631E
1
NICKEL
< 10
pg/L
< 0.188
lb/d
< 10
pglL
< 0.188
lb/d
3
200.7
10
SELENIUM
< 10
pglL
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
3113B-04
10
SILVER
< 5.0
pg/L
< 0.094
lb/d
< 5.0
pglL
< 0.094
lb/d
3
200.7
5
THALLIUM
< 1.0
pg/L
< 0.019
lb/d
< 1.0
pglL
< 0.019
lb/d
3
200.8
1
ZINC
70
pg/L
1.316
lb/d
47.59
pglL
0.894
lb/d
3
3111B-99
10
CYANIDE
< 5
pg/L
< 0.094
lb/d
< 5
NgIL
< 0.094
lb/d
3
4500CNE-99
5
TOTAL PHENOLIC
COMPOUNDS
< 5
pg/L
< 0.094
lb/d
< 5
pglL
< 0.094
lb/d
3
420.1-78
5
HARDNESS (as CaCO3)
119
mglL
2233.0
lb/d
111.3
mg/L
2089.2
lb/d
3
2340C
1
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 10 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MUMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
VOLATILE ORGANIC COMPOUNDS
ACROLEIN
< 100
pg/L
< 1.88
Ib/d
< 100
pg/L
< 1.88
Ib/d
3
EPA 624
100
ACRYLONITRILE
< 50
pg/L
< 0.939
Ib/d
< 50
pg/L
< 0.939
Ib/d
3
EPA 624
50
BENZENE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
BROMOFORM
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
CARBON
TETRACHLORIDE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
CHLOROBENZENE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
CHLORODIBROMO-
METHANE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
CHLOROETHANE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 624
10
2-CHLOROETHYLVINYL
ETHER
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
CHLOROFORM
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
DICHLOROBROMO-
METHANE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
1,1-DICHLOROETHANE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
1,2-DICHLOROETHANE
< 5
pglL
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
TRANS-I,2-DICHLORO-
ETHYLENE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
1 -
ETTHYLENEHYLENE
< 5
pglL
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
1,2-DICHLOROPROPANE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
1,3-DICHLORO-
PROPYLENE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
ETHYLBENZENE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
METHYL BROMIDE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 624
10
METHYL CHLORIDE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 624
10
METHYLENE CHLORIDE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 624
10
TETRA-
C
CHLOLOROETHANE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
ETHYLENELENE YO-
ETH
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
TOLUENE
< 5
pg/L
< 0.094
Ib/d
< 5
pg/L
< 0.094
Ib/d
3
EPA 624
5
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 11 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MLIMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
1,1,1-
TRICHLOROETHANE
< 5
pg/L
<
0.094
Ib/d
< 5
pg/L
<
0.094
Ib/d
3
EPA 624
5
1,1,2-
TRICHLOROETHANE
< 5
pg/L
<
0.094
Ib/d
< 5
pg/L
<
0.094
Ib/d
3
EPA 624
5
TRICHLOROETHYLENE
< 5
pg/L
<
0.094
Ib/d
< 5
pg/L
<
0.094
Ib/d
3
EPA 624
5
VINYL CHLORIDE
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 624
10
Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer
TRICHLOROFLUORO
METHANE
< 5
pg/L
<
0.094
Ib/d
< 4
pg/L
<
0.094
Ib/d
3
EPA 624
5
ACID -EXTRACTABLE COMPOUNDS
P-CHLORO-M-CRESOL
< 20
pg/L
<
0.375
Ib/d
< 20
pg/L
<
0.375
Ib/d
3
EPA 625
20
2-CHLOROPHENOL
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
2,4-DICHLOROPHENOL
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
2,4-DIMETHYLPHENOL
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
4,6-DINITRO-O-CRESOL
< 50
pg/L
<
0.939
Ib/d
< 50
pg/L
<
0.939
Ib/d
3
EPA 625
50
2,4-DINITROPHENOL
< 50
pg/L
<
0.939
Ib/d
< 50
pg/L
<
0.939
Ib/d
3
EPA 625
50
2-NITROPHENOL
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
4-NITROPHENOL
< 50
pg/L
<
0.939
Ib/d
< 50
pg/L
<
0.939
Ib/d
3
EPA 625
50
PENTACHLOROPHENOL
< 50
pg/L
<
0.939
Ib/d
< 50
pg/L
<
0.939
Ib/d
3
EPA 625
50
PHENOL
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
2,4,6-
TRICHLOROPHENOL
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
BASE -NEUTRAL COMPOUNDS
ACENAPHTHENE
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
ACENAPHTHYLENE
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
ANTHRACENE
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
BENZIDINE
< 100
pg/L
<1.88
Ib/d
< 100
pg/L
<
1.88
Ib/d
3
EPA 625
100
BENZO(A)ANTHRACENE
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
BENZO(A)PYRENE
< 10
pg/L
<
0.188
Ib/d
< 10
pg/L
<
0.188
Ib/d
3
EPA 625
10
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 12 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
OutfaII number. 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
3,4 BENZO-
FLUORANTHENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
BENZO(GHI)PERYLENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
BENZO(K)
FLUORANTHENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
BIS (2-CHLOROETHOXY)
METHANE
<10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
BIS (2-CHLOROETHYL)-
ETHER
< 10
pg/L
< 0.188
Ib/d
< 10
pglL
< 0.188
Ib/d
3
EPA 625
10
BIS (2-CHLOROISO-
PROPYL) ETHER
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
BIS (2-ETHYLHEXYL)
PHTHALATE
< 20
pg/L
< 0.375
Ib/d
< 20
pg/L
< 0.375
Ib/d
3
EPA 625
20
4-BROMOPHENYL
ETHER
ETHER
< 10
pg/L
< 0.188
Ib/d
< 10
pglL
< 0.188
Ib/d
3
EPA 625
10
BUTYL BENZYL
PHTHALATE
< 10
pg/L
< 0.188
Ib/d
< 10
pglL
< 0.188
Ib/d
3
EPA 625
10
2-CH
NAPHTHALENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
4-CHLORPHENYL
PHENYL ETHER
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
CHRYSENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
DI-N-BUTYL PHTHALATE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
DI-N-OCTYL PHTHALATE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
DIBENZO(A,H)
ANTHRACENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
1,2-DICHLOROBENZENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
1,3-DICHLOROBENZENE
< 10
pg/L
< 0.188
Ib/d
< 10
pglL
< 0.188
Ib/d
3
EPA 625
10
1,4-DICHLOROBENZENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
3,3-DICHLORO-
BENZIDINE
< 50
pglL
< 0.939
Ib/d
< 50
pg/L
< 0.939
Ib/d
3
EPA 625
50
DIETHYL PHTHALATE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
DIMETHYL PHTHALATE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
2,4-DINITROTOLUENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
2,6-DINITROTOLUENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
1,2-DIPHENYL-
HYDRAZINE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
Ib/d
3
EPA 625
10
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 13 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United Sta es.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MLIMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
FLUORANTHENE
< 10
pg/L
< 0.188
Ib/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
FLUORENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
HEXACHLOROBENZENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
HEXACHLORO-
BUTADIENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
HEXACHLOROCYCLO-
PENTADIENE
< 50
pg/L
< 0.939
lb/d
< 50
pg/L
< 0.939
lb/d
3
EPA 625
50
HEXACHLOROETHANE
< 10
pg/L
< 0.188
lb/d
< 10
NgIL
< 0.188
lb/d
3
EPA 625
10
INDENO(1,2,3-CD)
PYRENE
< 10
pg/L
< 0.188
lb/d
< 10
pg1L
< 0.188
lb/d
3
EPA 625
10
ISOPHORONE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
NAPHTHALENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
NITROBENZENE
< 10
pg/L
< 0.188
lb/d
< 10
pgfL
< 0.188
lb/d
3
EPA 625
10
N-NITROSODI-N-
PROPYLAMINE
< 10
pg/L
<0.188
lb/d
< 10
pg/L
<0.188
lb/d
3
EPA 625
10
N-NITROSODI-
METHYLAMINE
< 10
pg1L
< 0.188
lb/d
< 10
pglL
< 0.188
lb/d
3
EPA 625
10
N-NITROSODI-
PHENYLAMINE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
PHENANTHRENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
PYRENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
1,2,4
TRICHLOROBENZENE
< 10
pg/L
< 0.188
lb/d
< 10
pg/L
< 0.188
lb/d
3
EPA 625
10
END OF PART D.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 14 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock VWUTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
SUPPLEMENTAL APPLICATION INFORMATION
PART E. TOXICITY TESTING DATA
POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the
facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are
required to have one under40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters.
• At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two
species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results
show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include
information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC
requirements for standard methods for analytes not addressed by 40 CFR Part 136.
• In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test
conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a
toxicity reduction evaluation, if one was conducted.
• If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information
requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods.
If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E.
If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to
complete.
E.1. Required Tests. Second species
received. All second
Indicate the number of whole effluent
❑ chronic 0 acute
E.2. Individual Test Data. Complete the
column per test (where each species
toxicity tests pending. Part E will be revised and submitted once second species toxicity results are
species toxicity results will be submitted prior to the expiration of this permit on June 30, 2018.
toxicity tests conducted in the past four and one-half years.
following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one
constitutes a test). Copy this page
Test number:
if
more than three tests are being reported.
Test number:
Test number:
a. Test information.
Test Species & test method number
Age at initiation of test
Outfall number
Dates sample collected
Date test started
Duration
b. Give toxicity test methods followed.
Manual title
Edition number and year of publication
Page number(s)
c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used.
24-Hour composite
Grab
d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each.
Before disinfection
After disinfection
After dechlorination
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 15 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WVI TP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
Test number: Test number: Test number:
e. Describe the point in the treatment process at which the sample was collected.
Sample was collected:
f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both
Chronic toxicity
Acute to)dcity
g. Provide the type of test performed.
Static
Static -renewal
Row -through
h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source.
Laboratory water
Receiving water
1. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used.
Fresh water
Salt water
j. Give the percentage effluent used for all concentrations in the test series.
k. Parameters measured during the test. (State whether parameter meets test method specifications)
pH
Salinity
Temperature
Ammonia
Dissolved oxygen
I. Test Results.
Acute:
Percent survival in 100%
effluent
LC50
95% C.I.
%
%
%
Control percent survival
%
%
%
Other (describe)
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 16 of 17

FACILITY NAME AND PERMIT NUMBER:
City of Havelock WWTP, NC0021253
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Neuse River
Chronic:
NOEC
IC2s
%
%
Control percent survival
%
%
%
Other (describe)
m. Quality Control/Quality Assurance.
Is reference toxicant data available?
Was reference toxicant test within
acceptable bounds?
What date was reference toxicant test
run (MM/DD/YYYY)?
/ /
/ /
/ /
Other (describe)
E.3. Toxicity Reduction Evaluation.
❑ Yes 0 No If yes, describe:
Is the treatment works involved in a
Toxicity Reduction Evaluation?
submitted biomonitoring test information, or information regarding the
the information was submitted to the permitting authority and a summary
Test Information. If you have
and one-half years, provide the dates
/ (MM/DD/YYYY)
E.4. Summary of Submitted Biomonitoring
cause of toxicity, within the past four
of the results.
Date submitted: /
Summary of results: (see instructions)
END OF PART E.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 17 of 17

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
EPA Form 2A Additional Information

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
Additional Information
B.2 Topographic Map
See Figure 1 for topographic map and Figure 2 for plant site map.
B.3.1 Process Flow Description — Permitted Capacity of 2.25 mgd
The Havelock WWTP provides advanced wastewater treatment, including
nitrogen removal, to meet effluent limits for discharge to the Neuse River.
The major processes at the WWTP include screening, grit removal, a single -
stage nitrification activated sludge process, denitrification filters, ultraviolet
disinfection, re -aeration, gravity belt thickening, and stabilized solids storage.
As part of the Phase 1 WWTP expansion, completed in May 2015, an effluent
pump station, an outfall pipeline, a cascade aerator, and a diffuser in the
Neuse River were constructed.
Screening
Influent wastewater is conveyed to the Havelock WWTP by a combination of
gravity interceptors and force mains. The influent flow is combined into a 24-
inch pipeline at the screening facility that passes through a bar screen
designed to remove large solids and debris from the influent wastewater to
prevent clogging and interference with operation of downstream pumps and
other process equipment.
Grit Removal
After passing through the bar screen, the influent wastewater flows to a vortex
(Pista) grit collector through a 24-inch pipe. After the grit is removed, the grit
collector effluent flows to the influent pump stations.
Influent Pump Stations
The Havelock WWTP is equipped with two influent pump stations. Effluent
from the grit removal facility flows through an 18-inch pipe to a tee with a 20-
inch pipe. The 20-inch pipe interconnects two wet wells, which are used in
combination with pumps to convey the influent wastewater to the aeration
basins. Each influent pump station is comprised of a wet well and three
influent pumps. One influent pump station contains three submersible pumps.
The second influent pump station is a dry pit/ wet pit configuration with three
pumps. All pumps are controlled via float switches in the wet well to keep
0:13090810061ENG1Task 040-WWTP NPDES Permit RenewailTab BWorm 2A- Additional Information 2017.doc 1

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
pace with the plant influent flow rate. In addition to raw wastewater, return
activated sludge (RAS) from the secondary treatment stage is returned to the
influent pump station for conveyance to the aeration basin distribution box.
Flow from the influent pump stations are conveyed through 10-inch and 12-
inch pipes to the aeration basin distribution box.
Activated Sludge System
The purpose of the activated sludge system is to achieve the BOD removal,
phosphorus removal, and nitrification necessary to comply with the stringent
effluent requirements in the permit. The activated sludge system includes fine
and coarse bubble aeration basins, intermediate pumping, final clarifier
distribution box, final clarifiers, and RAS and waste activated sludge (WAS)
conveyance.
Fine Bubble Aeration
Wastewater enters the fine bubble aeration basins mixed with RAS through a
distribution box. Two sharp -crested weirs split the flow equally between two
aeration basins. The two circular tanks are equipped with a fine bubble
aeration system with ceramic disc diffusers. The diffusers provide the
dissolved oxygen and mixing necessary for operation of the activated sludge
process.
Coarse Bubble Aeration
The mixed liquor from each of the fine bubble aeration basins flows through
16-inch pipes to the coarse bubble aeration basins for additional BOD
removal and/or nitrification. The three coarse bubble aeration basins are
operated in series in normal operation and are equipped with a coarse bubble
aeration system.
Final Clarifier Pump Station
Effluent from the second -stage aeration basin flows by gravity to the final
clarifier pump station wet well via 16-inch piping. The Final Clarifier Pump
Station lifts the mixed liquor to a high enough elevation that the wastewater
can flow by gravity through the rest of the treatment plant. A 20-inch pipe
conveys the pumped flow from the final clarifier pump station to the final
clarifier distribution box. A polyaluminum chloride (PACI) storage and feed
system is provided to feed PACI to the Final Clarifier Pump Station discharge
to enhance suspended solids removal and provide phosphorus removal in the
final clarifiers via precipitation.
0:13090610061ENGITask 040-WWTP NPDES Permit Renewal\Tab 81Form 2A- Additional Information 2017.doc 2

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
Final Clarifiers
Two 65-foot diameter clarifiers are provided to settle out solids from the mixed
liquor. The final clarifiers provide quiescent flow conditions to allow the mixed
liquor solids to settle to the bottom of the clarifiers. The settled solids are
either returned to the first -stage aeration basins as RAS or wasted to the
Waste Solids Holding Tank as WAS. The clarified effluent flows over the final
clarifier effluent V-notch weirs to the denitrification filters, where the
wastewater undergoes further treatment.
RAS and WAS Conveyance
The RAS and WAS Control Stations control the flow rate of settled activated
sludge from the final clarifiers to the influent pump stations and the Waste
Solids Holding Tank, respectively. WAS flows to the Waste Solids Holding
Tank, and from there is periodically pumped to the gravity belt thickeners for
thickening prior to stabilization and ultimate disposal. The RAS and WAS
flows are measured by four strap -on ultrasonic flow meters, with one RAS flow
meter and one WAS flow meter for each clarifier. RAS and WAS are conveyed
by gravity and manually -operated pinch valves downstream of the flow meters
are used to control the flow rates.
Denitrification Filters
The denitrification filters remove additional suspended solids from the final
clarifier effluent and remove nitrogen through denitrification to comply with the
total nitrogen limit. Final clarifier effluent flows by gravity to three denitrification
filters. An underdrain system collects the filtered wastewater and directs it to a
20-inch pipe that flows by gravity to the disinfection facilities. The Havelock
WWTP uses methanol as its carbon source, and typically adds between 40
and 80 gallons per day to the filters. Backwash water is drained to the Filter
Backwash Waste Detention Basin, and from there is returned to the influent
pump stations.
Ultraviolet Disinfection
Disinfection is accomplished using ultraviolet (UV) disinfection technology.
Filtered wastewater effluent enters the UV disinfection facilities through a 16-
inch and 20-inch parallel pipeline. The old chlorine contact tank was
retrofitted to accommodate the UV modules and now serves as the
disinfection channel.
0:13090610061ENG1Task 040-WWTP NPDES Permit RenewallTab BlForm 2A- Additional Information 2017.doc 3

City of Havelock WWTP
Permit No. NC0021253
Ouffall 002
Re -aeration
The re -aeration facilities are located at the Re -aeration Basin and can be
used to provide additional dissolved oxygen in the UV disinfection effluent.
Two platform -mounted mechanical surface aerators are provided in the Re -
aeration Basin. The backwash supply pumps for the denitriflcation filters are
also located in the Re -aeration Basin.
Effluent Pump Station
The effluent pump station conveys flow through approximately 30,000 linear
feet of 24-inch piping to the Neuse River.
Cascade Aerator
Prior to discharging into the Neuse River, the effluent passes through a
cascade aerator. The cascade aerator is located near the bank of the Neuse
River and increases the effluent's dissolved oxygen levels to meet permit
requirements.
Diffuser in the Neuse River
After passing through the cascade aerator, the effluent discharges into the
Neuse River through a multi port diffuser located approximately 2,040 feet
from the shoreline.
Please reference Figure 3 for the process flow diagram at a permitted
capacity of 2.25 mgd.
B.3.2 Process Flow Description — Future Permitted Flow Capacity of 2.8 mgd
The process flow at a permitted capacity of 2.8 mgd will be the same as at
2.25 mgd, with the exception that the Activated Sludge system will be
upgraded to a 3-Stage BNR basin to meet nutrient limits.
Please reference Figure 4 for the process flow diagram at a permitted
capacity of 2.8 mgd.
0:13090610061ENG1Task 040- 1NTP NPDES Permit Renewal%Tab B1Form 2A-Additional information 2017.doc 4

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
B.3.3 Process Flow Description — Future Permitted Flow Capacity of 3.5 mgd
The process flow at a permitted capacity of 3.5 mgd will be the same as at
2.25 mgd, with the exception that the Activated Sludge system will be
upgraded to a 5-Stage BNR basin to meet nutrient limits.
Please reference Figure 5 for the process flow diagram at a permitted
capacity of 3.5 mgd.
0:13090610061ENGITask 040-WWTP NPDES Permit RenewallTab B1Form 2A-Additional Information 2017.doc

Effluent Discharge Location 002
M h Constructed as Part of Phase 1 of WWTP Expansion
Lat34°57'11"
Long 76° 52' 37"
CII F.HRti'
Influent Force Main
Imo\ F () REST
City of Havelock WWTP Site
Parallel Interceptors
Jiavekx
Cascade Aerator
Gunn P°im
Lending
•
1.
/ '
H
•
Copyright:© 2013 National Geographic Society, i-cubed'
Influent Force Mains
- Gravity Interceptors
- 24-inch Effluent Pipe
USATopa Maps
0 02 04
08
Milos
Hazen.
0:130906\006\ENG1Task 040-WWTP NPDES Permit Renewel1WWTP Location map -Figure 1.mxd
Figure 1
WWTP Location Map
City of Havelock, NC
NC0021253
B.2 of Form 2A
Friday, November 24, 2017

MAINTENANCE
BUILDING
FINAL CLARIFIER
NO2
IC%pl!Il'PJIllpl'lll!',,,i
BLOWER
BUILDING
NO2
CHEMICAL STORAGE
AND FEED FACILITY
DENTTRIFICATION
FILTERS
FINAL CLARIFIER
FLOW DISTRIBUTION
STRUCTURE
FINAL CLARIFIER
NO.1
30906-012 Figure 2.cdr
RAS CONTROL
STATION
TRANSFORMER
0
FINAL CLARIFIER
PUMPING STATION
COARSE BUBBLE
AERATION BASIN
NO. 3
FILTER BACKWASH
WASTE DETENTION BASIN
WASTE SOLIDS HOLDING TANK
WAS CONTROL STATION
ENGINE -
GENERATOR
BUILDING
BAR SCREEN
AND GRIT
REMOVAL
(BYPASS UNIT)
COARSE BUBBLE
AERATION BASINS
NO. 1 S2
0
INFLUENT
PUMPING STATIONS
-� ❑
GRIT REMOVAL "
BAR
SCREEN
STABILIZED SOLIDS
HOLDING BASIN
SOLIDS
HANDLING
BUILDING
SLUDGE
PUMPING
STATION
REAERATION
BASIN
I
EFFLUENT
PUMPING STATION
Figure 2
WWTP Site Map
City of Havelock, NC
NC0021253
B.2 of Form 2A

Plant Influent ♦ / / �
Q=2.25 mgd Bari�Screens
/
�1/1//
Q=2.25 mgd
Cascade
Aerator
Diffuser in
Neuse River
Grit
RemovalNN:7
el
\444
Grit
Q=2.25 mgd
Effluent Pump
Station
Q=2.25 mgd Q=3.55 mgd
/ Influent Pump
Stations
Q=0.15 mgd
Reaeration
Tank
Aeration Basin
I'►ADistribution —►
Box
FBW Waste
Detention Basin
UV Disinfection
FBW Q=0.15 mgd
Q=0.02 mgd Polymer
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump
Solids Holding Thickener
Basin Q=0.01 mgd Q=0.03 rngd
/UMW" - --- Truck Hauling
to Land Application
Legend
FBW = Filter Backwash
FBWR = Filter Backwash Return
RAS = Return Activated Sludge
WAS = Waste Activated Sludge
TWAS = Thickened Waste Activated
Sludge
= Flow Meter
Fine Bubble Coarse Bubble
Aeration Basins Aeration Basins
RAS Q=1.13 mgd
Final
Clarifiers
Denitrification
Filters
—►
Final Clarifier
Pump Station
Polyaluminum
Chloride
Q=3.55 mgd
f Distribution
Box
Q=1.15 mgd
Waste Solids WAS Control RAS Control
Holding Tank Station Station
Q=0.03 mgd Q=1.13 mgd
Figure 3
WWTP Process Flow Diagram:
Permitted Capacity of 2.25 mgd
City of Havelock, NC
NC0021253
B.3 of Fomi 2A
30906-012 Figure 3.cdr

Q=2.8 mgd
Grit
/RemovaPlant Influent //V/
a
Q=2 8 mgd Bar Screens --�
\ v CT CT CZ
/ Influent Pump r
Stations
Q=2.8 mgd
Cascade
Aerator
Diffuser in
Neuse River
Grit
Q=2.8 mgd
Effluent Pump
Station
Q=0.024 mgd
FBWR
Q=4.4 mgd
NRCY
3 Stage BNR Basin
RAS Q=1.4 mgc'
Legend
FBW = Filter Backwash
FBWR = Filter Backwash Return
RAS = Return Activated Sludge
WAS = Waste Activated Sludge
TWAS = Thickened Waste Activated
Sludge
= Flow Meter
Final Clarifier
Pump Station
Q=0.2 mgd
Reaeration
Tank
FBW Waste
Detention Basin
UV Disinfection
FBW Q=0.2 mgd
Q=3.0 mgd
Methanol
Polymer
Denitrification
Filters
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump Waste Solids WAS Control
Solids Holding Thickener Holding Tank Station
Basin Q=0.014 mgd Q=0.038 mgd
Truck Hauling
to Land Application
Q=0.038 mgd
Polyaluminum
Chloride
Final
Clarifiers
Q=4.4 mgd
4-- Distribution 41
Box
Q=1.4 mgd
RAS Control
Station
Q=1.4 mgd
Figure 4
WWTP Process Flow Diagram:
Permitted Capacity of 2.8 mgd
City of Havelock, NC
NC0021253
B.3 of Form 2A
30906-0-..2 figure 3.cdr

-- Q=3.5 mgd
Grit
//// J Removal
Plant Influent ♦ /
Q=3.5 mgd Bar Screens -
Q=3.5 mgd
Grit
Q=3.5 mgd
Cascade Effluent Pump
Aerator Station
ay6.6i4r�+
Diffuser in
Neuse River
30906-012 Figure 3.cdr
Q=5.5 mgd
Influent Pump
Stations
FBWR
10.
NRCY
5 Stage BNR Basin
RAS Q=1.75 mgd
Legend
FBW = Filter Backwash
FBWR = Filter Backwash Return
RAS = Return Activated Sludge
WAS = Waste Activated Sludge
TWAS = Thickened Waste Activated
Sludge
= Flow Meter
Final Clarifier
Pump Station
Q=0.25 mgd
Reaeration
Tank
FBW Waste
Detention Basin
4
UV Disinfection
FBW Q=0.25 mgd
Methanol
Q=3.75 mgd -
•
Q=0.03 mgd Polymer
1
Denitrification
Filters
M
Polyaluminum
Chloride
Q=5.5 mgd
Final f Distribution 41
Clarifiers ce/ Box
- Q=1.8 mgd
Stabilized TWAS Pumps Gravity Be t GBT Feed Pump Waste Solids WAS Control
Solids Holding Thickener Holding Tank Station
Basin Q=0.02 mgd Q=0.05 mgd
visr`ii l;
Truck Hauling
to Land Application
Q=0.05 mgd
M
RAS Control
Station
Q=1.75 mgd
Figure 5
WWTP Process Flow Diagram:
Permitted Capacity of 3.5 mgd
City of Havelock, NC
NC0021253
B.3 of Form 2A

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Sludge Management Plan
(Including Land Application Permit and Agreement with Synargo)

Solids Treatment
Solids in the form of WAS from the Havelock WWTP currently undergo further treatment
for eventual disposal as a land application product. The existing solids processing
facilities include thickening, WAS holding tank, one 1-meter gravity belt thickener (GBT),
polymer feed system, GBT feed pumps, thickened WAS (TWAS) feed pumps, and a
stabilized solids holding basin.
The solids thickening process is designed to reduce the volume of WAS from the activated
sludge process. WAS is removed from the final clarifiers and drained by gravity to the
Waste Solids Holding Tank for short-term storage prior to thickening. Each clarifier has
a separate wasting line and pinch valve in the WAS Control Station for controlling WAS
flow to the Waste Solids Holding Tank. Flow meters in the WAS Control Station indicate
WAS flow rate for each final clarifier. Submersible pumps are provided in the Waste
Solids Holding Tank for pumping WAS to the gravity belt thickeners in the Solids Handling
Building. Chemical conditioning of the solids with polymer is provided to separate the
flocculated solids from the free water. The thickened waste activated sludge (TWAS)
from the GBT is collected in a thickened solids hopper, from which it is pumped to the
Solids Stabilization Tank by two TWAS pumps. Free water is drained back to the Influent
Pump Station.
The stabilized solids holding basin is used to store thickened stabilized solids prior to
liquid land application on permitted privately -owned farmland. Piping is provided for
withdrawal of solids from the holding basin and to Toad the solids into a truck. Decanting
of supernatant to the influent pump stations is also possible using a portable pump.

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
RALEIGH
LAND APPLICATION OF CLASS B WASTEWATER TREATMENT PLANT RESIDUALS
PERMIT (NON -DEDICATED)
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Havelock
Craven County
FOR THE
continued operation of a residuals management program for the City of Havelock and consisting of the
land application of Class B Wastewater Treatment Plant residuals generated by the approved facilities
listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface
waters, pursuant to the application received January 20, 2015, and in conformity with other supporting
data subsequently filed and approved by the Department of Environment and Natural Resources and
considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of
Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal
regulations.
Tlus permit shall be effective from the date of issuance until March 31, 2017, shall void Permit No.
WQ0000702 issued April 7, 2008, and shall be subject to the following specified conditions and
limitations:
I. SCHEDULES
1. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal
application. [1SA NCAC 02T .0108(b)(2), 02T .105(d), 02T .0109]
2. The Permittee shall be in full compliance with the regional office notification requirements
established in Condition 11I.3. within 90 days of the effective date of this permit. [15A NCAC 02T
.01 08(b)(2)]
3. The Permittce shall submit the Operation and Maintenance (O&M) plan as required in Condition
III.4. to the Division within 90 days of the effective date of this permit. [15A NCAC 02T
.0108(b)(2)]
WQ0000702 Version 3.2 Shell Version 150101 Page 1 of 12

4. The Permittcc shall be in full compliance with the signage requirements established in Condition
ll1.13. within 180 days of the effective date of this permit. [15A NCAC 02T .0108(b)(2)]
ll. PERFORMANCE STANDARDS
1. The subject residuals management program shall be effectively maintained and operated at all times
so there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance
conditions due to improper operation and maintenance, the Permittee shall immediately cease land
applying residuals to the site, contact the Washington regional office supervisor, and take any
immediate corrective actions. [G.S. 143-215.1]
2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02B .0200,
02L .0100]
3. Only residuals generated by the facilities listed in Attachment A are approved for land application in
accordance with this permit. [G.S. 143-215.1]
4. Only the sites listed in Attachment B are approved for residuals land application. [G.S. 143-215.1 ]
5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not
exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant
Loading Rates (CPLRs):
Parameter
Ceiling Concentration
(milligrams per kilogram)
CPLR
(pounds per acre)
Arsenic
75
36
Cadmium
85
34
Copper
4,300
1,338
Lead
840
267
Mercury
57
15
Molybdenum
75
n/a
Nickel
420
374
Selenium
100
89
Zinc
7,500
2,498
The Permittee shall determine compliance with the CPLRs using one of the following methods:
a. By calculating the existing cumulative level of pollutants using actual analytical data from all
historical land application events of residuals, or
b. For land where residuals application have not occurred or for which the required data is
incomplete, by determining background concentrations through representative soil sampling.
[15A NCAC 02T .1105]
6. Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC
02T .1106 (a) and (c). Exceptions to this requirement shall be specified in Attaclunent A. [15A
NCAC 02T .1106]
WQ0000702 Version 3.2
Shell Version 150101 Page 2 of 12

7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing
wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A)
that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T
.1107(a). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107]
8. Setbacks for Class B land application sites shall be as follows:
Setback Description
Setback by application type
(feet)
Vehicular
Surface
Application
Irrigation
Surface
Application
Injection /
Incorporation
Iabitable residence or place of public assembly
under separate ownership or not to be maintained as
part of the project site
400
400
200
Habitable residence or places of public assembly
owned by the Permittee, the owner of the land, or the
lessee/operator of the land to be maintained as pan
of the project site
0
200
0
Property lines
50
150
50
Public right of way
50
50
50
Private or public water supply
100
100
100
Surface waters (streams — intermittent and perennial,
perennial waterbodies, and wetlands)
100
100
50
Surface water diversions (ephemeral streams,
waterways, ditches)
25
100
25
Groundwater lowering ditches (where the bottom of
the ditch intersects the SHWT)
25
100
25
Subsurface groundwater lowering system
0
100
0
Wells with exception to monitoring wells
100
100
100
Bedrock outcrops
25
25
25
Top of slope of embankments or cuts of two feet or
more in vertical height
15
15
15
Building foundations or basements
0
15
0
Water lines
0
10
0
Swimming pools
100
100
100
Nitrification fields
0
20
0
[15A NCAC 02T .1108]
9. Land application areas shall be clearly marked on each site prior to and during any residuals
application event. [15A NCAC 02T .0108(b)(1)]
10. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in
exceedancc of agronomic rates. Appropriate agronomic rates shall be calculated using expected
nitrogen requirements based on the deternuned Realistic Yield Expectations (RYE) using any of the
following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
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b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina
State University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.php).
A copy shall be kept on file and reprinted every five years in accordance with Condition N.S.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee inay use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(littp://www.ncagr.gov/SWC/tech/documents/9th_Guidance_Doc_l 001 09.pd f).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards (ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdfl.
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T .1109(b) (1) (k)]
11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. [15A NCAC 02T
.0108(b)(1)]
12. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer
and iye grass in the winter with both crops to receive residuals), then the second crop can receive an
application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may
be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted
for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [15A
NCAC 02T .0108(b)(1)]
13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee
shall maintain written records of these recommendations and details of their implementation. [15A
NCAC 02T .0108(b)(1)]
14. These residuals land application sites were individually permitted on or after December 30, 1983;
therefore, the compliance boundary is established at either 250 feet from the residual land application
area, or 50 feet within the property boundary, whichever is closest to the residual land application
area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to
remediation action according to 15A NCAC 02L .0106(d) (2) as well as enforcement actions in
accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved
relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. [15A NCAC 02L
.0107(a)]
15. The review boundary shall be established midway between the compliance boundary and the residual
land application area. Any exceedance of groundwater standards at the review boundary shall require
action in accordance with 15A NCAC 02L .0106. [15A NCAC 02L .0108]
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III. OPERATION AND MAINTENANCE REQUIREMENTS
1. The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [15A NCAC 02T .1110]
2. The Washington Regional Office, telephone number [phone], and the appropriate local
government official (i.e., county manager, city manager, or health director) shall be notified at least
48 hours prior to the initial residuals land application to any new land application site. Notification to
the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday,
excluding State Holidays. [15A NCAC 02T .0108(b)(1)]
3. The Washington Regional Office shall be notified via email or telephone, [phone], at least 24
hours prior to conducting any land application activity. Such notification shall indicate, at a
minimum, the anticipated application times, field 1Ds, and location of land application activities. If it
becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be
notified prior to commencing the application to those fields. [15A NCAC 02T .0108(b)(1)]
4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan)
Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan.
The O&M Plan, at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be
taken by the inspector in the event that noncompliance is observed pursuant to the
noncompliance notification requirements under the monitoring and reporting scction of the
permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for
any foreseen fluctuations in residuals quality and indicate the most limiting times for
residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that
land apply multiple times per year but have an annual sampling frequency, may need to
sample during winter months when pathogen reduction is most likely to be negatively
affected by cold temperatures).
[15A NCAC 02T .1100]
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5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in
responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with
15A NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A
NCAC O8G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition
III.4.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information
regarding classification and designation requirements, please contact the Division of Water
Resources' Protection and Enforcement Branch at [phone]. [15A NCAC 02T .0117]
6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall
be maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
7. When the Pennittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [15A NCAC 02T .1110]
8. Residuals shall not be stored at any land application site, unless written approval has been requested
and received from the Division. [G.S. 143-215.1]
9. When the Pennittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
10. When the Pennittee land applies bulk residuals, a suitable vegetative cover shall be maintained on
land application sites onto which residuals are applied, or application shall be in accordance with the
crop management plan outlined by the local Cooperative Extension Office, the Department of
Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist
and as approved by the Division. [15A NCAC 02T .1109(b)(1)]
11. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under
section 4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of
surface water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within
a 24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
If the slope is greater than 10% for surface applied liquid residuals, or if the slope is heater than
18% for injected or incorporated bulk liquid residuals;
h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to
achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the
pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved
variations to the acceptable soil pH (6.0) will be noted in this permit;
g.
i. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in
a USDA no -till program shall be exempted from meeting this vegetative cover requirement;
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j. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
k. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
1. Application exceeds agronomic rates.
[15A NCAC 02T .1109]
12. The following public access restrictions apply to residual land application sites:
a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted
for 365 days after a residuals land application event;
b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land
application event.
[15A NCAC 02T .1109(b) (2)]
13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g.,
1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and
contact information, including the Permittee or applicator's telephone number. Signs shall be posted
in a clearly visible and conspicuous manner at the entrance to each land application site during a land
application event, and for as long as the public access restrictions required under Condition I1I.12.
apply. [15A NCAC 02T .0108(b)(1)]
14. The following harvesting and grazing restrictions apply to residual land application sites after each
land application event:
Harvesting and Grazing Description
Restricted
Duration
Animals shall not be allowed to graze during land application activities and
restricted period. Sites that are to be used for grazing shall have fencing to
prevent access after each land application event.
30 days
Food crops, feed crops and fiber crops shall not be harvested for:
30 days
Turf grown on land where residuals have been applied shall not be harvested for:
12 months
Food crops with harvested parts that touch the residual/soil mixture and are
totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.)
shall not be harvested for:
14 months
When the residuals remain on the land surface for four months or longer prior to
incorporation into the soil, food crop; with harvested parts below the land
surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be
harvested for:
20 months
When the residuals remain on the land surface for less than four months prior to
incorporation Into the soil, food crops with harvested parts below the land
surface shall not be harvested for:
38 months
[I 5A NCAC 02T .1109(b) (3)]
15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that
have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for
those operations where a NMP is required by the US Department of Agriculture — National Resources
Conservation Service (NRCS) or other State Agencies. The Permittee shall calculate allowable
nutrient loading rates based on the provided information and use appropriate reductions.
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For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan
(WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient
Management Plan. [15A NCAC 02T .0108(b) (1), 02T .1104(c) (4)]
16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA)
between the Permittee and landowners or lessees/operators of the land application site is in full force
and effect. These agreements shall be considered expired concurrent with the permit expiration date,
and shall be renewed during the permit renewal process. [15A NCAC 02T .1104(c)(4)]
IV. MONITORING AND REPORTING REQUIREMENTS
1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste
under 40 CFR Part 261 shall not be used or disposed under this perrnit. The analyses
[corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall
be performed at the frequency specified in Attachment A, and the Pennittee shall maintain these
results for a minimum of five years. Any exceptions from the requirements in this condition shall be
specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)Heptachlor
(and its hydroxide)
(0.008)
Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
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3. An analysis shall be conducted on residuals from each source generating facility at the frequency
• specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02'1' .1101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A, and at the time indicated in the sampling
and monitoring sections of the approved O&M plan. The required data shall be specific to the
stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen
reduction requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction
requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this
condition shall be specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)]
5. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attaclunent B on which a residuals land application event will
occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil
Sampling" located in the Sampling Instructions section of the NC Department of Agriculture &
Consumer Services' website (http://www.ncagr.gov/agronomi/pubs.htm). The Permittee shall
maintain these results and a description of the sampling methodologies used to determine soil fertility
for a period of no less than five years, and shall be made available to the Division upon request. At a
minimum, the Standard Soil Fertility Analysis shall include the following parameters:
Acidity
Exchangeable Sodium Percentage
Phosphorus
Potassium
Base Saturation (by calculation)
Magnesium
Calcium
Manganese
Sodium
Cation Exchange Capacity
Percent Humic Matter
Zinc
Copper
pH
[1 SA NCAC 02T .1111(d)]
6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall
be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B
.0505]
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7. The Perinittee shall maintain records tracking all residual land application events. At a minimum,
these records shall include the following:
a. Source of residuals;
b. Date of land application;
c. Location of land application (i.e., site, field, or zone number as listed in Attachment B);
cl. Approximate areas applied to (acres);
e. Method of land application;
f. Weather conditions (e.g., sunny, cloudy, raining, etc.);
g. Predominant Soil Mapping Unit (e.g., CbB2);
h. Soil conditions (e.g., dry, wet, frozen, etc.);
i. Type of crop or crops to be grown on field;
J•
Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State
University Department of Soil Science Website, the printout page shall be kept on file and
reprinted every five years);
k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet
ton per acre;
1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or
wet tons per acre;
m. Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, dry ton per
acre, or wet tons per acre; and
n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other
sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy
metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury,
molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per
acre of phosphorus applied to each field.
[15A NCAC 02T .0109(a)]
8. Three copies of an annual report shall be submitted on or before March 1'. The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting
Forms. Instructions for reporting and annual report forms are available at
httu://portal.ncdenr.org/web/wqlaps/lau/reporting, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .1111(a)]
9. Noncompliance Notification
The Permittce shall report by telephone to the Washington Regional Office, telephone number (252)
946-6481, as soon as possible, but in no case more than 24 hours or on the next working day
following the occurrence or first knowledge of the occurrence of any of the following:
a. Land application of residuals abnormal in quantity or characteristic.
b. Any failure of the land application program resulting in a release of material to surface waters.
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c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
be taken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b) (1)]
V. INSPECTIONS
1. The Permittcc shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T
.0108(b)]
2. Prior to each bulk residuals land application event, the Pennittee or his designee shall inspect the
residuals transport and application facilities to prevent malfunctions, facility deterioration and
operator errors resulting in discharges, which may cause the release of wastes to the environment, a
threat to human health or a public nuisance. The Pennittee shall maintain an inspection log that
includes, at a minimum, the date and time of inspection, observations made, and any maintenance,
repairs, or corrective actions taken. The Pennittee shall maintain this inspection log for a period of
five years from the date of inspection, and this log shall be made available to the Division upon
request. [15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit; may inspect or
copy any records required to be maintained under the terms and conditions of this permit; and may
collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Pennittee to
an enforcement action by the Division in accordance with North Carolina General Statutes 143-
215.6A to 143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals land application events are not carried out in
accordance with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the
permit application and other supporting documentation. [G.S. 143-215.1]
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4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional govenunent agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules
in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 1SA NCAC Chapter 4
and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under
15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of
Chapter 143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
5. In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60 days notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [15A NCAC 02T
.0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program
contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC
02T .0120(b). [15A NCAC 02T .0120]
8. "I'he Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to
pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 24th day of March 2015
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
7-
mmerman, Director
ivisiorfof Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0000702
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}
ATTACHMENT A - Approved Residual Sources
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
Owner
Facility Name
County
Permit
Number
Biological
Residuals
Maximum
Dry Tons
Per Year
Monitoring
Frequency for
Non -hazardous
Characteristics-
Monitoring
b
Frequency for
Metals and
Nutrients 3• s
Monitoring
Frequency for
Pathogen &
Vector Attraction
Reductions'' `
Approved
Mineralization
Rate
[Raw = 0.4:
Aerobic -0.3:
Anaerobic = 0.2:
Compost = 0.11
0.3
City of Havelock
Havelock WWTP
Craven
NC0021253
Yes
415
Annually
Sec Table Below
See Table Below**
Total
415
1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignirability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IV.4.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Generated
(short tons per year)
Monitoring Frequency
(Established in 40 CFR 503 and 15A NCAC 02T .1111)
<319
1/Year
=>319 - <1,650
l/ Quarter (4 times per year)
=>
1,650 - <16,500
1/60 Days (6 times per year)
=>I6.500
1 /month (12 times per year)
If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no
sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual
report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification.
WQ0000702 Version 3.2 Attachment A
Page 1 of 1

ATTACHMENT B - Approved Land Application Sites
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
Field/ Site
Owner
Lessee
County
Latitude
Longitude
Net
Acreage
Dominant Soil Series
Footnotes
NC-CV-I-1 A1
Campbell. Robert G.
McCoy, Charles Myron
Craven
35°12'39"
77'25'06-
8.90
Pa - Pantego fine sandy loam
NC-CV-1-1.B
Campbell. Robert G.
McCoy. Charles Myron
Craven
35°12'38"
77'25'06"
7.00
Pa - Pantego fine sandy loam
NC -CV -I -ICI
Campbell. Robert G.
McCoy. Charles Myron
Craven
35°12'31"
77°25'09-
12.90
Pa - Pantego tine sandy loam
NC-CV-1-1 D
Campbell. Robert G.
McCoy. Charles Myron
Craven
35°12'32-
77°25' I5"
31.20
Pa - Pantego fine sandy loam
NC -CV -I - I E
Campbell, Robert G.
McCoy, Charles Myron
Craven
35° 12'32"
77'25' 18"
16.40
Pa - Pantego fine sandy loam
NC-CV-1-1G
Campbell. Robert G.
McCoy, Charles Myron
Craven
35°12'20-
77°25'02-
9.40
Pa - Pantego fine sandy loam
NC -CV- I -1 H
Campbell. Robert G.
McCoy, Charles Myron
Craven
35° 12' 12"
77°25'0T'
26.00
Pa - Pantego fine sandy loam
NC -CV -I -2A
Campbell. Robert G.
McCoy, Charles Myron
Craven
35°12'20"
77'25'39"
13.50
Pa - Pantego fine sandy loam
NC -CV- I -2A
Campbell. Robert G.
McCoy, Charles Myron
Craven
35° 12' 10"
77°25'23"
5.50
Pa - Pantego tine sandy loam
Total for Comm?
130.8
NC-PA-2-1 A
Spencer Farms. Inc.
Pamlico
35°09'56"
76°49'32-
10.18
Yo - Yongcs loamy fine sand
NC-PA-2-1 B
Spencer Farms, Inc.
Pamlico
35°09'55"
76°49'28"
9.71
Yo - Yongcs loamy fine sand
NC-PA-2-1 C
Spencer Farms. Inc.
Pamlico
35°09'55"
76°49'26"
10.24
Yo - Yonges loamy fine sand
NC-PA-2-1 D
Spencer Fauns, Inc.
Pamlico
35°09'55"
76°49'23"
10.25
Yo - Yonges loamy fine sand
NC-PA-2-I E
Spencer Farms, Inc.
Pamlico
35°09'55"
76°49'20"
10.12
Yo - Yonges loamy fine sand
NC-PA-2-1 F
Spencer Farms, Inc.
Pamlico
35°09'55"
76°49' I T'
10.05
Yo - Yonges loamy fine sand
NC-PA-2-IG
Spencer Farms, Inc.
Pamlico
35°09'55"
76°49' 15"
9.52
Yo - Yonges loamy fine sand
NC-PA-2-2A
Spencer Farms. Inc.
Pamlico
35°09' 1 7"
76°49'20"
2.94
Ar - Argent loam
NC-PA-2-2B
Spencer Farms, Inc.
Pamlico
35°09' 16"
76°49' 15"
6.26
Ar - Argent loam ,
NC-PA-2-2C
Spencer Farms, Inc.
Pamlico
35°09' 16"
76°49' 11"
6.48
Yo - Yongcs loamy fine sand
NC-PA-2-2D
Spencer Farms, Inc.
Pamlico
35°09' l 6"
76°49'07"
7.04
Yo - Yonges loamy fine sand
NC-PA-2-2E
Spencer Farms. Inc.
Pamlico
35°09' 17"
76°49'03-
6.28
Yo - Yonges loamy fine sand
NC-PA-2-3A
Spencer Farms. Inc.
Pamlico
35°09' 19"
76°49'00"
5.42
Yo - Yonges loamy fine sand
WQ0000702 Version 3.2
Attachment B
Page 1 of 3

ATTACHMENT B - Approved Land Application Sites
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
NC-PA-2-3B
Spencer Farms. Inc.
Pamlico
35°09' 19"
76°48'57"
4.04
Yo — Yonges loamy tine sand
NC-PA-2-3C
Spcnccr Farms. Inc.
Pamlico
35°09' 19"
76°48'55"
5.64
Yo — Yonges loamy fine sand
NC-PA-2-3D
Spcnccr Farms. Inc.
Pamlico
35°09' 19"
76°48'51"
8.04
Sk- Stockade loamy tine sand
NC-PA-2-3E
Spencer Farms. Inc.
Pamlico
35°09'20"
76°48'48"
7.42
Sk- Stockade loamy fine sand
NC-PA-2-3F
Spencer Farms. Inc.
Pamlico
35°09'20"
76°48'45"
7.42
Sk- Stockade loamy fine sand
NC-PA-2-3G
Spencer Farms, Inc.
Pamlico
35°09'20"
76°48'42"
6.65
Sk- Stockade loamy fine sand
NC-PA-2-4A
Spencer Farms. Inc.
Pamlico
35°09'27"
76°49'02"
2.43
Yo — Yonges loamy fine sand
NC-PA-2-4B
Spencer Farms. Inc.
Pamlico
35°09'34"
76°48'54"
4.34
Sk- Stockade loamy fine sand
NC-PA-2-4C
Spencer Farms. Inc.
Pamlico
35°09'32"
76°48'54"
4.51
Sk- Stockade loamy fine sand
NC-PA-2-4D
Spcnccr Farms, Inc.
Pamlico
35°09'31"
76°48'53"
3.62
Sk- Stockade loamy fine sand
NC-PA-2-4E
Spencer Farms, Inc.
Pamlico
35°09'29"
76°48'52"
3.55
Sk- Stockadc loamy tine sand
NC-PA-2-4F
Spencer Farms, Inc.
Pamlico
35°09'28"
76°48'52"
3.60
Sk- Stockade loamy fine sand
NC-PA-2-4G
Spencer Farms, Inc.
Pamlico
35°09'26"
76°48'51"
3.55
Sk- Stockade loamy fine sand
NC-PA-2-5A
Spencer Farms. Inc.
Pamlico
35°09'39"
76°49'04"
5.21
Sk- Stockade loamy fine sand
NC-PA-2-5B
Spcncer Farms. Inc.
Pamlico
35°09'40"
76°49'02"
6.48
Sk- Stockade loamy fine sand
NC-PA-2-5C
Spcnccr Farms, Inc.
Pamlico
35°09'40"
76°48'58"
6.16
Sk- Stockade loamy fine sand
NC-PA-2-5D
Spencer Farms, Inc.
Pamlico
35°09'4I"
76°48'55"
6.26
Sk- Stockade loamy tine sand
NC-PA-2-5E
Spencer Farms, Inc.
Pamlico
35°09'41"
76°48'52"
3.90
Sk- Stockade loamy fine sand
NC-PA-2-5F
Spencer Farms. Inc.
Pamlico
35°09'42"
76°48'49"
3.59
Sk- Stockadc loamy fine sand
NC-PA-2-6A
Spencer Farms. Inc.
Pamlico
35°09'51"
76°50'21"
5.21
Sk- Stockade loamy fine sand
NC-PA-2-6B
Spencer Farms, Inc.
Pamlico
35°09'52"
76°50' 17"
6.48
Sk- Stockade loamy fine sand
NC-PA-2-6C
Spencer Farms, Inc.
Pamlico
35°09'53"
76°50' 13"
6.16
Sk- Stockade loamy fine sand
NC-PA-2-6D
Spencer Farms. Inc.
Pamlico
35°09'54"
76°50' 10"
6.26
Yo — Yonges loamy tine sand
NC-PA-2-6E
Spencer Farms. Inc.
Pamlico
35°09'55"
76°50'06"
3.90
Yo — Yonges loamy tine sand
NC-PA-2-6F
Spencer Farms, Inc.
Pamlico
35°09'55"
76°50'04"
3.59
Yu — Yonges loamy fine sand
NC-PA-2-6G
Spencer Farms, Inc.
Pamlico
35°09'56"
76°50'01"
3.84
Ar— Argent loam
WQ0000702 Version 3.2
Attachment B
Page 2 of 3

ATTACHMENT B - Approved Land Application Sites
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
NC-PA-2-7A.
Spcnccr Farms. Inc.
Pamlico
35°09'56"
76°49'59"
2.18
Ar- Argent loam
NC-PA-2-7B
Spencer Farms, Inc.
Pamlico
35°09'57"
76°49'57'
2.57
Ar- Argent loam
NC-PA-2-7C
Spencer Farms. Inc.
Pamlico
35°09'57"
76°49'55"
3.32
Ar - Argent loam
NC-PA-2-7D
Spencer Farms. Inc.
Pamlico
35°09'58"
76°49'53"
3.32
Ar- Argent loam
NC-PA-2-7E
Spencer Farms. Inc.
Pamlico
35°09'59"
76°49'50"
3.26
Ar - Argent loam
NC-PA-2-7F
Spencer Farms, Inc.
Pamlico
35°09'59"
76°49'48"
3.03
Ar- Argent loam
NC-PA-2-7G
Spencer Farms. Inc.
Pamlico
35°I0'00"
76°49'46"
3.53
Ar - Argent loam
NC-PA-2-7H
Spencer Farms, Inc.
Pamlico
35°10'00"
76°49'43"
3.28
Yo - Yonges loamy fine sand
NC-PA-2-71
Spencer Fauns, Inc.
Pamlico
35° 10'01"
76°49'4I"
3.25
Yo - Yongcs loamy fine sand
NC-PA-2-7J
Spencer Farms, Inc.
Pamlico
35°10.0I"
76°49'39"
3.25
Yo - Yonges loamy fine sand
NC-PA-2-7K
Spencer Fauns, Inc.
Pamlico
35° 10'02"
76°49'37"
2.47
1
Yo - Yonges loamy fine sand
Total for County
269.80
Total
400.60
. A re -defined compliance boundary has been approved for this land application site. This re -defined compliance boundary is between fields NC -CV- I - I A and NC -CV- I - I C and shall be
located at 50 feet from the water supply well on Robert G. Campbell's property. Note that the 100-foot setback between wells and the land application area shall still be met.
WQ0000702 Version 3.2
Attachment B Page 3 of 3

SCALE: 1 " = 1 miles
11.0 6-14��
DATE:
PR�OJ ECT NO:
DRAWN BY: MEM
__ 1588 9-059
Fields 7A - , I: l
Al
II ante
Grantsboro
2 F ie7kis 9A - 10;1
„AIM
REFERENCE:
GIS DATA LAYERS WERE OBTAINED FROM ESRI, INC. PLEASE NOTE THIS MAP IS FOR INFORMATIONAL
PURPOSES ONLY. IT IS NOT MEANT FOR DESIGN, LEGAL, OR ANY OTHER USES. THERE ARE NO
GUARANTEES ABOUT ITS ACCURACY, S&ME, INC. ASSUMES NO RESPONSIBILITY FOR ANY DECISION
MADE OR ANYACTIONS TAKEN BY THE USER BASED UPON THIS INFORMATION.
WWW.SMEINC.COIVI
ENGINEERING LICENSE NO: F-0176
SPENCER FAR
SITE NC-P
VICINITY Il
CITY OF HAVELOCK - LAND Al
PAMLICO COUNTY, NO
Bay bon)
rv�
Stonewall
Field Boundary
FIGURE 1
CITY OF HAVELOCK
503 LAND APPLICATION PROGRAM
CRAVEN COUNTY
WQ0000702
SITE LOCATION MAP

}
1
6.111.14119.0
I 11l.U. A( ION
1111111(1D .(( HUN
NEIACltI3
511E/11 11.11
1411ALA('IlLN
11177.11401: UR15
NI:FA('RF:S
SC-PA2-IA
15.08
4.90
10.IA
N(-d'A-2-5A
6.85
2.66
5.21
NC-PA-2-10
13.61
190
9.71
N(--1'A-2.S11
6.51
1.56
6A11 '
NC-PA-2.1C
13.72
3.411
10.24
NC-PA-2.5C
6.53
1.56
6.16
NC-PA-2-II)
13.71
3.16
10.25
NC-PAd-51)
6.52
1.50
6.16
NC:-1'A-2.11.
13.60
3.48
10.12
NC-PA-2-5E.
6.53
IA7
3.90
N(--PA-2-I F
13.5.1
148
10.05
NC-PA-2-5F
5.54
1.85
3.59
N('-V,01-11.
1.1.95
6.43
9.52
REFERENCE:
150AfAlAYrRS WEAL 0IIIN11L01 ROMFSRI.MC rtLANLIRlrr TIIIS NAP IS FOR IIROPUAIIONAL MIRP0.SFS ONLY IT nor NLAIIT FM1 OLLIMI
&FOAL. ON ANY OTNLR LIN.S TIRNL AAR NOOUARNI ILLSNIOVI MS ACCURACY SS'A:.IRC.ASSUI.ILS IIO RFSPONSI0II ITT FOR ANY 1Y019101
LLADP (MAW AC- RNISTAXER RY TNF USLN0ASFR UPON OFF INFORUA1CI4
COMPLIANCE BOUNDARY:
lilt COMPLNI4CC ROUNOAJIYl1RI FACII LIVID APPI ICA110N 311L LS FSTAILISIILDATFITNFR 710f FFT FROM TIIF RF.:HN,ALR UNOArPLICAIIONMrA
00 IOW 1 WITHIN 1111 Pk0PFRIVBININOARYWVI IICIII.YER IS CLUSL51 TOTHE RLLRYINS IAI10APPI IC Ai1ON MA
REVIEW BOUNDARY:
111r. 911All.FrESTARLIS11r0AP0:NI7 L !.:.•II+.`:PAPrI II'A1 ("SS Sl;. S. +, I. LII111. ...++II!..NI, 11.1
; 4IIIM11RO, TIIL NCSRNNL9 LAND APPLICATION API
• iJ1,�?✓fjy� Field 40 fir+ 54
��yr•r.- '�rlit
}�.i�
/ „r F19mbc �y
1.
.%-f��I g ry n.. rr�rYr.. I1ln.bl` .ph,L 4
`tiWIA TJIhe(;ISL/-C• �ff.'r_•r�^fir
• Irrigation Well
• Dwelling
GW Lowenng OJch
1774 Buffer
Field Boundary
Property Boundary
c'513.`;. Af X, (D1111,1PPmu Prl.,.•
0
2
. w
2
0
'II
2
re
a
0
�<
3
za
op
1- <
itya vz
Q < a r
a L a 0
tz a z
W Z
0 W Lt. _ E
�03 Uc3 0
W o0
0- w (3
=i
0
o s
C
u
0
FIGURE 2
CITY OF HAVELOCK
503 LAND APPLICATION PROGRAM
CRAVEN COUNTY
Wg0000702
DETAIL MAP FOR SITES
NC-PA-2-1A THROUGH 1G AND
NC-PA-2-SA THROUGH 5F

0- •
r
tt 9' TS
•
r-
•
_note Ea., nu)ila1G<N. C roEy9, cabal ralU?R1 (,, r, , mmcs CNCSIAJbut ((7. I15UA. (-1303. AC1<, GSlmapp, 10 :rc
s,visslap9. mai u1P 0(3 U6ar COmrPun4Y r• f ,
S IrE, 1111.N
N('-PA-1.2A
NC•PA•2.25
4(.PA44C
PC-PA•2.20
NCPA•2.3E
41C-PA4.3A
NC•PA•2-00
NC-PA-13C
NC-PA-2d0
NC-PA•2-3F:
II5TAI. A('RIS 021•11(F11AC145 NM MIPS
530 256 2.94
1133 517 616
I0.11 3.70 6.41
10.77 1.73 7.04
9.9.3 3.65 611
731 1.16 S.42
6.90 213 417
1.13 2A9 514
1211 434 1.04
9.73 231 7A2
SITE:, 1111D
NC•PA•2-3F
NC.PA•241:
NC•►A-2-4A
N('-PA-1.411
N(:-PA-21C
NC PA-2.1(1
Nf-542.4E
Ne.PA•2-IF
141TAL AC INS 5L}1T31F71 ACRES NM ACRES
9.73 2.11 7.42
9.99 .1.14 4.65
TAR 1AR 3A3
4.42 LOS 434
6.42 1.91 431
3.49 1.17 1.62
3A1 116 335
S.46 116 EEO
3A1 136 333
REFERENCE:
OI.S OATSLAYf RS WERE OStAN. 11 TECH ISM, NC %EASE N0IE Imo MAP 15100 NI 1R1MAI10104. PURPOSE501AY IT 15 NOt MEANT E00 D:SCN.
IEQAI. CH art 01NER USES TIER( Ni£ IIOOINRNOEES ASCOT RS ACCURACY 146E.OIC. ASSUNF.INORESPON*000TY FOR ANY DECISION
NACL UR 'NV ACTIONS TORN Sr Tit USER RASED UPON MS NFOIMATIDI
COMPLIANCE BOUNDARY:
INE CONPE NTCE BOOI[ONtY FOR FACII WD APPI (CATKIN SITE IS ESWAN ISIEO STEITNER 230 FPPT
'RCM HIE RESIOWLS IANO APVLCATION AREA OR SU FEET MITTEN THE PROPERTY 6OIMDARY,
REVIEW BOUNDARY:
11E REVIEW 0010UARY81N.L BE ES TAN ISIED AR0U10 EAt. I LAND AP%ICATDN SIZE MT/WAY
BETWEEN THE OOMPLI NCE BOUNDAJIYNr3 THE PERNIFR CT THE RESIDUALS LAW APPI ICAT100
• Irrigation Wetl
• Dwelling
GW Lowering Ditch
Buffer
Field Boundary
Property Boundary
1,r
•
�
W0 0
V
Z
aW
U
z
(I o-
K a.
LL V rez
WW LL
f-
Z N m
W
1F47., co
1 FIGURE 3
.- �• CITY OF HAVELOCK
[503 LAND APPLICATION PROGRAM
CRAVEN COUNTY
WC100o0702
DETAIL MAP FOR SITES
NC-PA-2-2A THROUGH 2E,
NC-PA-2-3A THROUGH 3G AND
NC-PA-2-4A THROUGH 4G

COMPLIANCE DOUNDMY:
N <F CRIA% WM.COWIWNIY r CACIIIANII MN IS ESINLI511ED ATCITIICR2250fC1 T1N014 INF RF&IAIAI SINW MOM' AI ION MLA
UN SO CL 1011101 TIIE PROPI.NTY SWEAR Y. WIECIILVLII B CI OSEST TO TIE R16111W 1S LOW APPLCAI ION ARCH
REVIEW BOUNDARY:
TNF RENM1 ROsMOAIlt SIMI I RE ESTASI I:IIFOMCU!ID CACI. LAUD APPIICAf101I SIZE MnAVAY w rwr'.: not r..1 :: • 1. 1
PI MINIM Of lit RL SIDUICO IAN) ICAI NHI MrA
Field 6C
.6 RV 1WLD VITAL ACRP1 I1.11.7 2D Ar72IS
NC.PA-2-4A 7.55 231
VC.PA.2.6B 0.31 I56
'(1'A.2.00 7.9/ 1.63
CI I.A.2.6D 5.13 1.57
NI'..4-241: 5.52 112
I
NC.FAQ�T 5.16 137
M'-PA-L6C 5.15 126
'.1 .1'A.2.7A 1.00 052
S('-I'A.2-7B 1.111 1.46
NETALRIS
521
6.43
6.16
626
3.90
339
354
2.15
2.57
Field 61
SITFJ FWD
NI=PA-2-7C
nr•r54.7E
K'-PA.2.7F
M=rA-2-7c
NGrA-2-711
NC-PA-2-71
NC.PA.2-71
NGIIA.2.7K
Field 7
71YPA1. ACRIS 111111 111.l1 111:0
136 1.54
426 1.51
1.50
1.51
5.10
451
4.75
4.75
4AI
1.54
1.51
137
131
131
131
194
332
312
3.26
3A3
333
315
3.25
325
2A7
f% I{�4 1 r} 1
!( �f11 21 �3
/! 1* 6 r
,A `JlE FIoi V, !4 PA•
liil� r t6 qq/1 t i
ia
t1 }/6A( it i+E6 6i11 (T
l f� ii( !E F'cIJ 7K IF
l41 Sw( ill f'I';ficld 7J 'I
j! ( ' F:ieltl 71 11 1
�! I 6I,Fiold.lfi (� ,A l
�Il 1.! lit Ic!d Lc 1/ l TI 6 �j
�$ �Fi01111i, 14 1� l �F}Ii
110111 7 �? t! I r !tj Iri1 I
Field 10}.'� 0 1t5 lA v. O. A
It'..: /q V. ` „.
, j51
r?.f
Field 1A
\
• 1rr4
1.
1�
REFERENCE
NM RATA LAYERS AERE BONNE° FROM ESREIIM.. PIP.ASE NOTE TIM:IIAP I6 FOR INFORMATIONAL PIIRPOLLNONIY. R 10 NOT WPM FOR !WELKIN,
I fGAL, RR ANY GIVER 1/5E5 TIKIIP ARE NO OIMRANI0 E§ ADWf NO ACGIRIACV 6110,MR; ASSOMFSIMRF50ONSIIILRY FRR ANY DCCKNIN
MACE OR ANY ACTORS TAKEN BY THE MR BASED UPON RIM RR ORMAf1ON.
• 1
■ I
FIGURE 4
CITY OF HAVELOCK
503 LAND APPLICATION PROGRAM
CRAVEN COUNTY
w00000702
DETAIL MAP FOR SITES
NC-PA-2-6A THROUGH 6G AND
NC-PA-2-7A THROUGH 71(

BIOSOLIDS MANAGEMENT SERVICE AGREEMENT
This SERVICE AGREEMENT (hereinafter called the AGREEMENT) made and entered into
this 1st day of November 2006 (the EFFECTIVE DATE) by and between City of Havelock, NC
(hereinafter called CUSTOMER), and Synagro Central, LLC, (hereinafter called CONTRACTOR
which term shall include its successors and assigns).
WITNESSETH:
In consideration of the following covenants and AGREEMENTS, the CUSTOMER and the
CONTRACTOR hereby mutually agree as follows:
1. SCOPE
1.1. The CONTRACTOR shall provide biosolids management services that include
removal, transportation, and land application or other beneficial reuse in accordance with the
terms of this AGREEMENT (hereinafter called SERVICES) of the CUSTOMER'S biosolids
which constitute primarily (liquid semi -solids) residue generated during the treatment of
wastewater (hereinafter called BIOSOLIDS) at the city's wastewater treatment plant located
in Havelock, North Carolina (the PLANT).
(011 2. CONTRACTOR OBLIGATIONS
The CONTRACTOR shall:
2.1. Within four (4) weeks after receipt of notice from CUSTOMER, cause the removal,
transportation, and land application of CUSTOMER'S BIOSOLIDS and, in connection
with such activities, maintain AUTHORIZATIONS and landowner AGREEMENTS
required of CONTRACTOR for agricultural land application and/or disturbed land
reclamation in accordance with all applicable LEGAL REQUIREMENTS which are
currently in effect, or which take effect during the term of this AGREEMENT.
2.2. At the written request of CUSTOMER, and as -applicable, provide any
AUTHORIZATIONS which are issued by applicable GOVERNMENTAL
AUTHORITIES for all land approved for BIOSOLIDS land application.
2.3. Notify the CUSTOMER of any notice of violation, action, suit, claim, or legal
proceeding against CONTRACTOR relating to any aspect of the CUSTOMER'S
BIOSOLIDS managed pursuant to this AGREEMENT.
2.4. For BIOSOLIDS which are land applied, employ land application methods approved
or allowed by applicable GOVERNMENTAL AUTHORITIES.
-1-
Havelock Agreement -Final 11 07 06.dac

2.5. Develop and implement monitoring, record keeping, and reporting programs as
required by applicable LEGAL REQUIREMENTS, and as set forth in Section 6 of
this AGREEMENT.
2.6. Provide proof of liability and workers' compensation insurance, as set forth in
Section 4 of this AGREEMENT.
2.7. Indemnify CUSTOMER, and hold harmless CUSTOMER, its subsidiaries, affiliates,
successors and assigns and their respective directors, officers, employees,
shareholders, representatives and agents (hereinafter referred to collectively in this
section as CUSTOMER INDEMNITEES) from and against any and all claims,
liabilities, lawsuits, and causes of action, together with reasonable costs, expenses, and
attorneys' fees associated therewith and all amounts paid in defense or settlement of
the foregoing, which may be imposed upon or incurred by CUSTOMER
INDEMNITEES or asserted against CUSTOMER INDEMNITEES by any other
person or persons (including GOVERNMENTAL AUTHORITIES), to the extent
caused by CONTRACTOR'S breach of its obligations under this AGREEMENT or
violation of applicable LEGAL REQUIREMENTS.
2.8. Comply in all material respects with all LEGAL REQUIREMENTS applicable to
CONTRACTOR'S provision of the SERVICES.
2.9. CONTRACTOR'S obligations to take, receive or beneficially reuse BIOSOLIDS shall
be suspended during a Force Majeure.
3. CUSTOMER
The CUSTOMER shall:
3.1. Provide to CONTRACTOR for off -site beneficial reuse 100% of all liquid
BIOSOLIDS generated at the PLANT.
3.2. Provide CONTRACTOR with reasonable access to the CUSTOMER'S BIOSOLID'S
delivery system, except as reasonably required for safety or emergency considerations,
or planned shutdown of the PLANT. It is agreed that when safety, emergency or
shutdown conditions prevent access, that both parties will attempt to resolve such
conditions as expeditiously as possible.
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Havelock Agreement -Final 11 07 06.dac
Ps")

3.3. Provide CONTRACTOR written notice of the concentration of total nitrogen (as N on
a dry weight basis) in the BIOSOLIDS which CUSTOMER provides, plus all other
information which CONTRACTOR may request to facilitate its compliance with
applicable LEGAL REQUIREMENTS, including without limitation the requirements
of 40 C.F.R. Part 503. Information which CONTRACTOR may obtain shall include,
without limitation, the monthly average concentrations (in milligrams per kilogram) of
arsenic, cadmium, copper, lead, mercury, nickel, selenium, and zinc or other
potentially Hazardous Materials present in the BIOSOLIDS, the level of pathogen
reduction which CUSTOMER has achieved. The methods and procedures by which
CUSTOMER samples and analyzes concentrations of potentially HAZARDOUS
MATERIALS, pathogen reduction, shall comply with methods and procedures
prescribed by applicable LEGAL REQUIREMENTS, including without limitation
40 C.F.R. Part 503. CUSTOMER shall provide CONTRACTOR with a certification
regarding concentrations of HAZARDOUS MATERIALS, pathogen reduction, as
well as certification that all methods and procedures used by customer for the
sampling and analysis of BIOSOLIDS comply with requirements of 40 C.F.R. Part
503, and any other applicable LEGAL REQUIREMENTS. The form of certification,
and the type of information which the CONTRACTOR may request from
CUSTOMER may include the form of certification or the type of information which
CUSTOMER must maintain under 40 C.F.R. § 503.17. CONTRACTOR shall have
the undisputed right to rely upon any information or certification provided by
CUSTOMER, and shall not have any independent duty to investigate or inquire
regarding the subject matter of the CUSTOMER'S certification or of the information
which CUSTOMER provides to CONTRACTOR.
3.4. Not provide to CONTRACTOR any BIOSOLIDS which contain HAZARDOUS
MATERIAL or are hazardous in accordance with 40 C.F.R. Part 261, other federal
law, state law, or which contains a concentration of polychlorinated biphenyls equal to
or greater than 50 milligrams per kilogram of total solids (on a dry weight basis).
3.5. Provide CONTRACTOR with at least [four (4) weeks] advance notice of when
CUSTOMER desires for CONTRACTOR to remove BIOSOLIDS from the PLANT.
3.6. Indemnify, defend, and protect CONTRACTOR from and against all claims, damages,
losses, costs, suits, settlements, causes of action, liabilities, fines, penalties, costs, and
expenses (including but not limited to, investigation and legal expenses, and costs and
expenses associated with Remedial Work) (collectively, CLAIMS) arising out of or in
connection with any acts or omissions of CUSTOMER, or its employees, officers,
directors, representatives, contractors, subcontractors, agents, or affiliates, or any
licensee or invitee of the PLANT (other than CONTRACTOR), or CUSTOMER'S
breach of any of its obligations under this AGREEMENT, or any violation of any
applicable LEGAL REQUIREMENT by CUSTOMER or any of its employees,
officers, directors, representatives, agents, contractors, subcontractors, or affiliates, or
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Havelock Agreement -Final 1 l 07 06.doc

its licensees or invitees (other than CONTRACTOR) or any discrepancy in the
character or composition of the BIOSOLIDS from the PLANT compared to analytical
results, certifications or other information provided by CUSTOMER to
CONTRACTOR.
3.7. From time to time, as requested by CONTRACTOR, review a list of proposed land
application sites at which BIOSOLIDS from the PLANT may be applied, and select
from such sites those sites to which CUSTOMER desires for its BIOSOLIDS to be
applied, and such sites to which it does not desire its BIOSOLIDS to be applied. In
the absence of specific designations by CUSTOMER, CUSTOMER agrees that it shall
have been deemed to select any and/or all of such application as satisfactory locations
for its BIOSOLIDS.
3.8. Notify the CONTRACTOR of operating changes or any other conditions that would
reasonably be expected to affect the BIOSOLIDS handled by CONTRACTOR under
this AGREEMENT.
4. INSURANCE
The CONTRACTOR shall maintain and provide the CUSTOMER evidence of insurance as
follows:
4.1. Worker's Compensation meeting at least the minimum requirements of the laws of the
State of North Carolina, and Employer's Liability with a minimum single limit of
$1,000,000.
4.2. Commercial General Liability and Automobile Liability Insurance to include premises
operations and subcontractors. Completed Operations and Contractual Liability are to
be included under the Commercial General Liability coverage. The insurance policies
will have limits of no less than $1,000,000.00 per occurrence and $ 2,000,000.00
aggregate. CUSTOMER shall be named as an additional insured.
5. PAYMENT
The CONTRACTOR shall provide the CUSTOMER with an accounting of the gallons of
BIOSOLIDS removed from the CUSTOMER'S PLANT, and such other information as shall
be reasonably requested. CONTRACTOR will utilize a measurement method based on the
number of tanker loads of BIOSOLIDS removed from the CUSTOMERS'S PLANT and the
capacity, in gallons, of the tankers. The CUSTOMER will be provided with manifests for all
loads removed by the CONTRACTOR.
5.1. The CONTRACTOR shall submit invoices once each month for SERVICES provided
by CONTRACTOR, using the rates and the amounts agreed in Section 10 of this
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Havelock Agreement -Final 11 07 06.doc

AGREEMENT. The CUSTOMER shall pay all invoices within 30 days after receipt
of the invoice.
5.2. It is agreed that in the event of any dispute concerning invoice amount, CUSTOMER
will pay undisputed invoice amounts within 30 days after receipt of the invoice.
6. RECORD KEEPING
The CONTRACTOR shall maintain records and submit summary reports to the
CUSTOMER after each hauling event (as requested by CUSTOMER) and on an annual,
cumulative basis. Reports shall include information regarding, but not be limited to:
6.1. Number of loads transported and applied with identification of utilization site(s).
6.2. Such other information as will reasonably allow CUSTOMER to fulfill its
recordkeeping, and reporting requirements under applicable LEGAL
REQUIREMENTS and such other information reasonably deemed by the
CUSTOMER as necessary for this AGREEMENT and which is kept by
CONTRACTOR in the normal course of its business.
7. NOTICES
Except as otherwise provided herein, any notice, demand or other contract disputes or shall
be in writing and shall be personally served, sent by commercial courier service or prepaid
registered or certified mail, or sent by telephonic facsimile delivery with confirmation
thereof. Any such notice shall be deemed communicated upon receipt.
7.1. The following address is hereby designated as the legal address of the
CONTRACTOR. Such address may be changed at any time by notice in writing
delivered to CUSTOMER.
Synagro Central, LLC
7014 E. Baltimore Street
Baltimore, MD 21224
[phone]
Fax: [phone]
Attention: [Stephen Toft]
With a copy to:
Alvin L. Thomas 11
General Counsel
Synagro Technologies, Inc.
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Havelock Agreement -Final 11 07 06.do

1800 Bering Drive, Suite 1000
Houston, Texas 77057
[phone]
[phone] (Fax)
7.2. The following address is hereby designated as the legal address of the CUSTOMER.
Such address may be changed at any time by notice in writing delivered to
CONTRACTOR.
Name: City of Havelock
Street Address: PO Drawer 368
Mailing Address: Havelock, NC [28532]
Phone Number: [phone]
Contact Person: Dave Harvell
Fax: [phone]
8. FORCE MAJEURE
Wherever the word "Force Majeure" is used, it should be understood to mean:
8.1. acts of God, landslides, lightning, earthquakes, hurricanes, tornadoes, blizzards and
other adverse and inclement weather, fires, explosions, floods, acts of a public enemy,
wars, blockades, insurrections, riots or civil disturbances;
8.2. labor disputes, strikes, Work slowdowns, or Work stoppages;
8.3. orders or judgements of any Federal, State or local court, administrative agency or
governmental body, if not the result of willful or negligent action of the party relying
thereon;
8.4. power failure and outages affecting the Premises; and
8.5. any other similar cause or event, including a change in law, regulation, ordinance or
permit, provided that the foregoing is beyond the reasonable control of the party
claiming Force Majeure.
If, because of Force Majeure any party's cost is increased by more than 15% or any party
hereto is rendered unable, wholly or in part, to carry out its obligations under this Contract,
then such party shall give to the other party prompt written notice of the Force Majeure with
reasonable full details concerning it; thereupon the obligation of the party giving the notice, so
far as they are affected by the Force Majeure, shall be suspended during, but no longer than,
the continuance of the Force Majeure. The affected party shall use all possible diligence to
remove the Force Majeure as quickly as possible, but his obligation shall not be deemed to
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Havelock Agreement -Final 11 07 06.doc

require the settlement of any strike, lockout, or other labor difficulty contrary to the wishes of
the party involved.
9. TERM
9.1. This AGREEMENT shall be effective from the EFFECTIVE DATE until the 30th day
of September 2011 (the INITIAL TERM). At the end of this term, this
AGREEMENT may be extended on a yearly basis for five (5) additional one year
terms at the option of CUSTOMER and at the mutual agreement in writing of both
parties. The non -defaulting party may terminate this AGREEMENT and shall have no
further obligations to the other party under this AGREEMENT if (i) the other party
fails to observe or perform any material covenant or agreement contained in this
agreement for ten (10) business days after written notice thereof has been given to
such other party by the non -defaulting party or (ii) at any time upon the insolvency of
the other party, or the institution by or against the other party of any proceeding in
bankruptcy or insolvency or for the appointment of a receiver or trustee or for an
assignment for the benefit of creditors.
9.2. CONTRACTOR may terminate this AGREEMENT at any time upon written notice to
CUSTOMER and have no further obligation to CUSTOMER if:
9.2.1. The CONTRACTOR is unable to utilize the BIOSOLIDS due to a change in
any LEGAL REQUIREMENTS that renders the SERVICES illegal, or place
such restrictions or requirements thereon so as to make the provision of the
SERVICES cost prohibitive or to otherwise frustrate the commercial intent of
this AGREEMENT.
9.2.2. The BIOSOLIDS become unsuitable for land application by the
CONTRACTOR by reason of (i) the act or omission of any third party or
CUSTOMER, and through no fault of CONTRACTOR, or (ii) the condition
of the BIOSOLIDS is materially inconsistent with the description and
analysis, certifications or other information the CUSTOMER has provided to
the CONTRACTOR regarding the BIOSOLIDS, or (iii) CUSTOMER
breaches its obligations hereunder regarding the quality of the BIOSOLIDS.
9.3. In the event of any change in federal, state or local law or regulation, or any change in
any one of CONTRACTOR'S permits, which is implemented during the Tenn of this
AGREEMENT and which results in a significant increase or decrease in the cost of
performing the SERVICES, the CUSTOMER and CONTRACTOR agree to attempt
to negotiate a mutually agreeable adjustment to that payment terms specified in this
AGREEMENT. Should agreement not be reached, either party may terminate this
AGREEMENT as specified in Article 9.
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Havelock Agreement -Final 11 07 06.doc

10. PRICE
10.1. Except as otherwise provided in this AGREEMENT, CUSTOMER will pay the
following fixed prices for CONTRACTOR'S SERVICES hereunder for the duration
of the INITIAL TERM of this Agreement
Liquid Land Application = $0.057 per gallon
Mobilization = Included at no charge
503 Compliance Sampling (if needed) = Cost plus 15%
Ag-lime (if needed) = Included at no charge
Land Permitting (min 100 acres) = $25.00 per acre
10.2. Upon increases in CONTRACTOR'S costs due to changes in LEGAL
REQUIREMENTS, CONTRACTOR may no more than once each anniversary year,
request an increase in the fixed prices set forth hereunder. The parties shall in good
faith attempt to negotiate such increase and if successful such shall be effective as of
the beginning of the then most current anniversary of the EFFECTIVE DATE. In
addition, there will be an annual adjustment for price paid for SERVICES provided
by the CONTRACTOR on the anniversary date of the EFFECIVE DATE. The first
adjustment shall be on October 1, 2007, and shall be repeated at the end of each
twelve months thereafter. The adjustment will be the percent increase or decrease in
the Consumer price Index for All Urban Consumers (CPI-U) as published by the U.S.
Department of Labor. The adjustment will be made by multiplying the percent
increase or decrease in the CPI-U over the most recent twelve months reported times
the current unit price and adding or subtracting the adjustment to the price used
during the previous twelve months.
11. MISCELLANEOUS PROVISIONS.
11.1. Assignment. The CUSTOMER and/or CONTRACTOR shall have the right to assign
this AGREEMENT in writing to any successor in interest, subject to the written
approval of the other party, which approval shall not be unreasonably withheld.
11.2. Governing Law. THIS AGREEMENT AND ALL THE RIGHTS AND DUTIES
OF THE PARTIES ARISING FROM OR RELATING IN ANY WAY TO THE
SUBJECT MATTER OF THIS AGREEMENT OR THE TRANSACTIONS
CONTEMPLATED BY IT, SHALL BE GOVERNED BY, CONSTRUED, AND
ENFORCED IN ACCORDANCE WITH THE LAWS OF THE STATE OF
NORTH CAROLINA.
11.3. Costs and Fees. The prevailing party in any legal proceeding brought by or against
the other party to enforce any provision or term of this AGREEMENT shall be entitled
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Havelock Agreement -Final 1 l 07 06.doc

to recover against the non -prevailing party the reasonable attorneys' fees, court costs
and other expenses incurred by the prevailing party.
11.4. Consent to Breach Not Waiver. No term or provision hereof shall be deemed
waived and no breach excused, unless such waiver or consent be in writing and signed
by the party claimed to have waived or consented. No consent by any party to, or
waiver of, a breach by the other party shall constitute a consent to, waiver of, or
excuse of any other different or subsequent breach.
11.5. Severability. If any term or provision of this AGREEMENT should be declared
invalid by a court of competent jurisdiction, (i) the remaining terms and provisions of
this AGREEMENT shall be unimpaired, and (ii) the invalid term or provision shall be
replaced by such valid term or provision as comes closest to the intention underlying
the invalid term or provision.
11.6. ENTIRE AGREEMENT. THIS AGREEMENT INCLUDES AND
INCORPORATES BY REFERENCE AS IF FULLY SET FORTH HEREIN,
ALL OF THE TERMS, CONDITIONS AND OBLIGATIONS CONTAINED IN
THIS AGREEMENT, THE INFORMATION FOR PROPOSERS, SPECIFIC
PROVISIONS, AND DRAFT SERVICE AGREEMENT (AS AMENDED).
THIS AGREEMENT, TAKEN WITH THE INFORMATION FOR
PROPOSERS, SPECIFIC PROVISIONS, AND DRAFT SERVICE
AGREEMENT (AS AMENDED) HERETO CONSTITUTES THE COMPLETE
AND EXCLUSIVE STATEMENT OF THE AGREEMENT BETWEEN THE
PARTIES WITH REGARD TO THE MATTERS SET FORTH HEREIN, AND
ALL OTHER AGREEMENTS, PROPOSALS, AND REPRESENTATIONS,
ORAL OR WRITTEN, EXPRESS OR IMPLIED, WITH REGARD THERETO
ARE SUPERSEDED..
11.7. Amendments. This AGREEMENT may be amended from time to time only by an
instrument in writing signed by the parties to this AGREEMENT.
11.8. Counterparts. This AGREEMENT may be executed in counterparts, which together
shall constitute one and the same contract. The parties may execute more than one
copy of this AGREEMENT, each of which shall constitute an original.
11.9 Preaudit Certification. This instrument has been preaudited in the manner required
by the Local Government Budget and Fiscal Control Act.
Lee . Tillman, Director of Finance
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Havelock Agreement -Final 11 07 06.dcc

12. DEFINITIONS
12.1. "AUTHORIZATIONS" means all authorizations, permits, applications, notices of
intent, registrations, variances, and exemptions, required for the removal,
transportation and land application of BIOSOLIDS in compliance with all applicable
LEGAL REQUIREMENTS.
12.2. `BIOSOLIDS" means sludge meeting Class B pathogen requirements, vector
attraction reduction requirements and pollutant concentrations (as defined by 40 CFR
Part 503 and State of North Carolina requirements for land application). Biosolids
do not include any hazardous materials or substance and must be suitable for land
application under the applicable law.
12.3. "ENVIRONMENTAL LAWS" means any AUTHORIZATION and any applicable
federal, state, or local law, rule, regulation, ordinance, order, decision, principle of
common law, consent decree or order, of any GOVERNMENTAL AUTHORITY,
now or hereafter in effect relating to HAZARDOUS MATERIALS, BIOSOLIDS, or
the protection of the environment, health and safety, or a community's right to know,
including without limitation, the Comprehensive Environmental Response,
Compensation, and Liability Act, the Resource Conservation and Recovery Act, the
Safe Drinking Water Act, the Clean Water Act, the Clean Air Act, the Emergency
Planning and Community Right to Know Act, the Hazardous Materials Transportation
Act, the Occupational Safety and Health Act, and any analogous state or local law.
12.4. "GOVERNMENTAL AUTHORITY" means any foreign governmental authority, the
United States of America, any State of the United States of America, any local
authority, and any political subdivision of any of the foregoing, and any agency,
department, commission, board, bureau, court, tribunal or any other governmental
authority having jurisdiction over this AGREEMENT, BIOSOLIDS, or COMPANY,
HAULER, or any of their respective assets, properties, sites, facilities or operations.
12.5. "HAZARDOUS MATERIALS" means any "petroleum," "oil," "hazardous waste,"
"hazardous substance," "toxic substance," and "extremely hazardous substance" as
such terms are defined, listed, or regulated under ENVIRONMENTAL LAWS, or as
they become defined, listed, or regulated under ENVIRONMENTAL LAWS.
12.6. "LEGAL REQUIREMENT" means any AUTHORIZATION and any applicable
federal, state, or local law, rule, regulation, ordinance, order, decision, principle of
common law, consent decree or order, of any GOVERNMENTAL AUTHORITY,
now or hereafter in effect, including without limitation, ENVIRONMENTAL LAWS.
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Havelock Agreement -Final 11 07 06.dcc

12.7. "REMEDIAL WORK" means investigation, monitoring, clean-up, containment,
removal, storage, remedial or restoration work associated with HAZARDOUS
MATERIALS or BIOSOLIDS.
IN WITNESS WHEREOF, the parties of this AGREEMENT have hereunto set their hands and seals,
dated as o the day and year first herein written.
Have i ck, G . ("CUSTOR")
ATTEST:
ame & Title: QPN2s W • CreQtAa,n Name & Title: ei1 ! ct,N
of\ass,r ` ,e? Cal
c l�ec
Synagro Central, LLC. ("CONTRACTOR")
Name & Title: Alvin L. Thomas, Vice President Name & Title: Dovsha G. Roscoe, Asst. Secretary
-11-
Havelock Agreement -Final 11 07 06.dcc

Amended
Appendix A - Draft Service Agreement
1. General
I. No residuals management operations shall occur on Sundays or legal holidays without
the approval of the Wastewater Treatment Supervisor.
II. All operators shall be well versed with regulations and requirements stipulated in the
EPA 40 C.F.R. Part 503 regulations and the Generator's land application permit
WQ0000702 with the State of North Carolina Department of Environment and Natural
Resources (NCDENR).
III. The total percent solids of the residuals produced by the Generator's facilities shall vary
^ ut s II eet Vector ractio� a uir me ll
from 3% to 6%. 1 e t onTactor mus> tpro rlingii�pi$ t iRion properly in
this range.
IV. The Contractor shall remove all unused materials, tools, equipment and machinery,
waste materials, refuse and other debris from loading area and land application sites.
The Contractor shall see that these sites are at all times left in a neat and orderly
condition.
V. Liquid residuals shall be transported in sealed tank bodies. The capacity of all tankers
and/or any other containers used to calculate the volume of residuals hauled for
payment should be certified by an independent agency capable of performing such
certification. This certification information shall be supplied in writing to the
Wastewater Treatment Supervisor before residuals are hauled for payment.
VL All application and transportation vehicles shall be cleaned no less than once per
month. If residuals are spilled onto vehicles, contractor shall see that the vehicles are
cleaned by the next working day.
VII. The Contractor shall be responsible for repair/replacement of all pavement, driveways,
fences, shrubs, lawns, trees and other public or private property damaged as result of
work performed under agreement with the Generator.
30

VIII. The Contractor shall at all times have a competent project manager or other
representative on the work site who shall have full authority to act for the Contractor
and who shall see that the work under the Contract is executed in accordance with the
agreement documents. All communications with the project manager shall be binding
as if given to the Contractorbut must be confirmed in writing within 24 hours.
2. Permitting
I. The Contractor shall be responsible for the procurement of additional sites suitable for
land application and shall be responsible for obtaining and compiling the information
^ i accordance with f sch dule
necessary for generation of permit applications/renewals. 't a minunum, su cten
acreage must be permitted to annually compensate for the number of acres lost during
the prior year and any increase in biosolids productions. which approval shall not be unreasonably
II. eld A
All sites shall meet the approval of the Generator prior to permitting by the State. The
Generator also reserves the right to prohibit the permitting of any site, but such prohibition is subject to the
reasonableness standard.
III. A copy of the Land Application Permit WQ0000702 and all site maps shall be
maintained on each application vehicle at all times when residuals are being applied.
give Generator reasonable notice
IV. The Contractor shall recciotocimaixigR prior to any correspondence with regulatory
agencies regarding regulatory issues concerning the Generator. All correspondences
shall be copied to the Generator.
V. On a yearly basis, every permitting event, or in the event that development or other
issues require changes in buffers/maps, the Contractor shall be responsible for
providing updated maps for the Land Application Site Books. The project manager
shall evaluate each site during application event for possible adjustments to
buffers/maps.
3. Emergency Response/Spills
I. The Contractor shall submit to the Generator for approval a Spill Control Plan.
II. A copy of the Spill Control Plan shall be maintained in each transport and application
vehicle used by the Contractor.
31

III. Any spills involved with the loading, transportation and/or application of the said
residuals shall be deemed the responsibility of the Contractor and shall be cleaned up
immediately to the sa iasfacig of the Generator, NCDENR, Division of Water Quality
and/or any landowner that may be involved. Any occurrences shall be immediately
reported to the Wastewater Treatment Supervisor.
4. Beneficial Reuse
I. The Contractor shall utilize equipment capable of both surface application and
6ueneur[ra obsarce injection/incorporation end shall provide such capability at the request of the
NifietKittElfat as is required to meet vector attraction reduction requirements.at a negotiated price)
II. No residuals generated by the Generator shall be stored at facilities or land -applied on
land not permitted/approved in the Generator's land application permit for NC DENR.
III. All buffer zones shall be marked MItun prior to land application.
IV. Any interruption (other than inclement weather) of the beneficial reuse activities for any
period of time longer than (2) days shall be reported to the Generator immediately,
when such interruption is determined.
V. The Contractor shall provide adequate supervision of its employees to ensure proper
application techniques are being utilized at all times.
VI. The Contractor shall provide individuals who are capable of and can maintain good
relations with the program participants. Failure to do so shall be grounds for the
immediate suspension of work and the possibility of the revocation of agreement.
VII. The Contractor shall make every effort to provide residuals application to all program
participants.
VIII. The Contractor shall provide the landowner with a copy of the analysis of residuals land
applied to his/her field.(farm report)
DC. Transporters of the Contractor should be aware that they present an image of the
Generator, therefore they should properly and professionally respond to any complaints
by citizens and/or the Generator. This includes but is not limited to obeying all traffic
laws.
32

5. Monitoring/Recordkeeping
I. The Contractor shall be responsible for all monitoring at the land application sites as
required by the Generator's Land Application permit #WQ0000702 and the EPA 40
C.F.R. Part. All residuals sampling shall be the responsibility of the Generator's
WWTP Personnel.
U. All information shall be kept on file with the Contractor and the Generator. The
Generator requires that the Contractor have a database management system for the
storage of data for residuals management activities performed for the Generator. irixx
.
aleftetmerillicgrobatxxxMoceamPolgoaktunntidfigoogoeftoclotammtsgtakxx
III. The Contractor shall keep daily logs indicating tanker loading, transportation, and
application volumes. These logs shall be totaled daily and a copy submitted to the
Generator's Residuals Supervisor no later than 4:00 p.m. on the first working day of the
following week.
IV. A report, after each Iand application event, shall be provided to the Generator indicating
volume of residuals, application rate per acre, land applied, and land application site
information. This information shall include all information as required by the land
application permit and 40 C.F.R. Part 503 regulations. These records shall be
submitted to the Generator by the 15th day of the following month after the application
event
6. Public Education/Acceptance
cooperate with Generator
I. The Contractor shall liedneabertin a Public Education Campaign for the Generator.
U. The Contractor shall assist the Generator with the handling of complaints and/or
questions regarding all residual management activities.
M. The Contractor shall maintain good relations with program participants and shall
provide documented notification of biosolids issues that could impact
program/participants.
IV. The Contractor shall assist the Generator with any other public notification that may be
required by the regulatory agencies.
33

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
First Species Effluent Toxicity Testing Data
2015-2017
1

aceAnalytical
11'41: L I:: i'1'r.s Co,
Pace Analytical Service.
2225 Rivers
tc-.
Mr. Art Hough
City of Havelock
Drawer 368
304 N. Jackson Dr.
Havelock, NC 28532
Project. BIOASSAY 02/18/15
Pace Project No.. 92237G53
Sample: PIPE 001
Parameters Results Units Report Limit Arai red
C dubia Fuil-range Chronic >100
Qualifiers
00
Laboratory Report
Page 1 :Jr 1
Report Date 03105!2015
Date Received 02/18/2315
Lab ID: 92237953001 Collected 32r 7f 15 10 55 Matrix Water
07/18/15 12 40
Reviewed by
Sty Tarle )
stacy.tarlei pacelabs.com
Raleigh Certification IDs
r 6701 Conference Drive. Raleigh NC 27607
North Carolina Wastewater Certification #: 57
Nort' Caroling, 3ioos.sa; Certification # 16
North Carolina Drinking Water Certification # 37731

Effluent Aquatic Toxicity Report Form!Phase II Chronic Ceriodaphnia
Facility Havelock 'Ma NPDES# N� 0021253 NW
Laboratory Performing Test t,'ace Analytical Services in, Kali.rth
Signature of C.R.0 -
Signatu-e of Lab Supervisor
Sample Information
Collection Start Date
Gran
Composite
rDuration:,
Harcness(mg/l
Spec.Conc (pathos/c
Ohionne(mg'l
Sarrple temp at receip
Sample 1
Sample 2
Cortrol
C2/16/15
02/18+1S
l
24
24
48
678
67?
210
<01
•-•0 1
0 5
17 -
Control
Effluent%
Crgei ism#
Z 3 4 5 6 7
Pipe# D01 County Craven
Con1n1e'Its 1,.J#'r,.1-1795_
� f•S'
It-itorr1 7t on'
treatment
pH Initial
pH Final
.tart : tu_
C2/18,a5_
( .I'j rr
02'25'15
12 40 i <.4 1
R.unawt Rr.-.r.... ,.i11 R•r•.•:, i,.• •.•
...
10D
100 100
824
7 86 8 22 7 80
7 70 7 S•2
8 66
t 819
6 :30
24 1
25 1
D.O Initia
D Final
Temp Initial
Temp =tna1
862 : 56 784
8 74 7 69 7 82
796 780
7 83 7 90
8.30 8 44 7 30
25 3 24 4 24 2
811 859
243 246
253
25 3
254 259 241
9 10 1'
# young
21
26
25
28122
24
25
25
20
31
/
-
Adult
(L)ive (D)ead
L
LLL
t
LLLLLL
��
# Young
29
2
23
3
25
4 5 6
25 24 24
7
18
26
9 10
25 25
Chronic Test Results
F,,:tl C-;ntrot Mortal tr
Ccot•..I 3rd br,or
1.•
45
Adult
(Live (D)ead
L
L
L
L
L
L
L
L
L
L
Effluent% # Young
67.5
Adult
(L live ,Dlead
1 2 3 4
36
29
26
L
LL
26
26
6 7 a
23
29
21
9 10
24
25
L
L
L
L
L
L
L
Effluent%
# Young
26
26
31
19
12
24
25
27
21
24
L
-r
90 I
I
IL)tve Adult(D)ead
LLLL
LLLL
L
Effluent% # Young
95
Effluent%
100
Adult
(L)tve tDiead
# Young
Adult
(L pve (D)ead
27
2
23
3
33
L
L
L
4
24
L
5
29
6
31
23
8 9 10
23 27
27
L
L
L
L ;L
L
20
L
2 3 4
23
L
28 27
L
L
5 6 7 8 9 10
32
L
21
L
26
L
26
L
23 23
L
L
4E ticur Mort2114
Cunt'c! Ivy(-,
0,
11jf =�
:;�On:fIcant�'t t r'
Final Mortality Si• ndrean!
or
n
Reproiuctior Ar,u�„
Repro IOEC- N0
E7
Metl•od 11unnrtte
Norma D.sno" Method K:enocorc.
Statts! •.' ,t 13TP !r s Methc1 13
C rr cat 1
Equal Vsanancesaf'Ie 1'
Stt,rshr 4 1F''.` Cnnca 15 OAG?
IJ.-. Ano:ysts ,)' appric.'i:
Effluent ` Rann S.tm Cr trcal Sum
Ovnrall Analysis:
Result = '.r •.• or
Test LOEC= '100 Yn: NOCC= 100
Chronic. Value= • 100 J
MAIL
TO:
AT- Env:ronmertal Sciences Branch
Div cf Water Quality
N DENR
1621 Mail Service Center
Raleigh N C 27699-1621
•:,•1e3;r, use rnghes: test cC..u:entiabun o,
F:•t'1„i.t ,-nn,frntration,vrth r •'i :•`. t1 m{t+1
D'NQ form A- •3 1819' i Rev 1 ' ; 45

Start Date
End Pate.
Samplo Date:
Comments:
2/ 1812015
225/2015
Conc-% 1
Ceriodaphnia Survival and Reproduction Test -Reproduction
Test IDt havelock Sample ;D.
Lab ID. PACE -Pace - Raleigh 7;016 Sample 104.e
Protocol: EPAF 91-EPA i-resh%ater Test SDec.os
CD Ceriodaphnia cfubi
2 3 4 5 6 7 8 9 10
contro: 21.000 26 000 25.000 28.000 22.000 24.00C 25.000 25.000 20.000 31 030
45 29.000 23.000 25.000 25.000 24.000 241.00C 18.000 26.000 25.000 25 000
67.5 36.000 29.000 26.000 26.000 26.000 23 000 29.00C 21.000 24.000 25 000
90 26.000 26.000 31.000 19.000 12.000 24.000 25 oor 21 (100 1.000 24 000
95 27.000 23.000 33.000 24.000 29.000 31.000 23.000 23.000 (.000 27 000
100 20.000 23.000 28 000 27 000 32.000 21.000 2G.000 20.000 23 000 23.0llu
Transform: Untransformed
Conc-% Mean N-Mean Mean
1-Tailed
Min Max CV°o N t-Stat Critical MSD
control 24.700 1.0000 24.700
45 24.400 0.9879 24.400
67.5 26.500 1.0729 26.500
90 23.500 0.9514 23.500
95 26.700 1.0810 26.700
100 24.900 1.0081 24.900
20.000 31.000 13.230 10
18.000 29.000 11.298 10 0 1/5
21.000 36.000 15.635 10 -1.052
12.000 31.000 22.089 10 0.701
23.000 33.000 13.218 10 -1 169
20.000 32.000 14 474 10 -0 1 17
2 2R7
2.287
2.287
.287
2.287
3.912
3.913
3.913
3.913
3.913
Auxiliary Tests
Kolmogorov D Test indicates normal distribution (p > 0.01)
Bartlett's Test indicates equal variances (p = 0.53)
Hypothesis Test (1-tail. 0.05) NOEC LOEC ChV
Dunnett's Test 100 >100
Statistic
0.66608
4.16495
Critical
1.035
15.0863
Skew Kurt
-C.0517 1.15758
TU MSDu MSDp MSB MSE F-Prob df
1 3.91266 0.15841 15.5367 14.6389 0.39198 5, 54
40
Dose -Response Piot
35 -
30
025p
O .
20 -
o -
a a
r , 1 -
-
a
10
r:
0
0
V
4^.
•
1-tail. 0 05 Ie /eI
of significance
Page 1
TOXCalc v5 0.23
Reviewed by:

Pace Analytical
Ceriodaphnia dubia (Ironic Test
Client: Y.:04 t.L)Q. -__ -ifs
( triune 1 ransktr rDate.Tina: .r. -,..-2: l 7-, !•-7-: LS,d-IL-'-i
Age of Organkm: 2-1. LC
Dt:ution 1,\ :tun Bato:r. -4--0-
Star t Date. .:::!-_.iF1L15-___ 'rime:
I' Transfer l)atc::7--- L-0- (C.- Tim:
2!'d Transfer Date._Z 23 \ L.-; Time: i__LL.S7 c."
Ending Date: _2,-2.,6::-_15 rime: ,(1/71-1 _
Concentration Da‘ # 1
Control
46
2
7
Total
NIPDF:S rt- Nit 00e-, I
t-
Organism horn (Datc.ilirne 11-1'1.- -
T uit Fed r Culture 1 _ Organism Source. V.11-14(cti
Terrill Dilation water: _24. 3_ Temp pooled dish. 3
Randonli,cd: Incuhator:
Analyst:
Analyst:
Analyst: I2oviewed by: 4.
2 3
L'=1 o
I 3..
5
7 IL
Total
1 c
7
'total r.
i 2
7
7
1 al . A f_), I _L-1 ! ,.")&.)
'1" ot
' )‘,.-1-4.),-- '
,!
.
2 C !
-ltc
r9
(C) ,..11___i_21 K.:: • 1 Ls 11•-- • 14 r 1 3
Total -_-?--9_ :4,1-2)
- •
•, Luc, - - - ---t--- -
5 i 4 53 i
7
Total .) ,B • -`'S -P---4 , 3;2- : i
; cc Jo
t
t•-j_.,e4 C./
Replicates
5
I‘)
Days 1 Fed By 1 Time
Day 0 — \
Day I
1)ay 2 L
_
8
C., C ._ _:
_/12-
i I
-) :. 3
LC
.--tc...._....i
,DLL) .,-5 at
,
,-,.•_,:. 1.,T
-1 z,----)--
Day 3
Day 4 1-1‘;‘,-.!
1
,•--
DaV
1)av 3'c- -
le
Ds-,''
k__ __ _
C.---Itc__:
j l I C L
1 -- I.2
a 1
9 1t)1
1 4/
I

Pace Analytical
,
liviibiihil ,.
\ Pi )i.s #: CC.''-2) itmidonii/A:: _v_. 1 it I Lite: ---.)6-- tc-;1 'me: q'k
I Mution \Vater lintel.... 402) ( .1.i•tn...' \\.,ccr 1 ,-1 p:
Tcst Omtnism Sourcc.:±-1:410,t1-7-'1'1i Anal \ \I
(_.5 o:..:
Start End SI art End End
't intro(
'Treatment 2
-(=)
fS
1).0, Start End •
Ing/Lt
Control -3.c)c,
"1 icannent J '3(
remperat nrvMarl
Control
Treatment 2
Start
••; I 1.•
•
End Start End
1 \
_
Start End Start End
Par:ureter
.01111.01
('olleet it al Date
4
Same '1 ernp
pi I I ',
--
Chlorine 1 nig/l 1
Conductivity tptS/enit
[
Hardness (ineL)
(1 11' 1.1 !tit
2
u
. (c,
\ ,
• -12_
omok 'Jr • 1,-;

,- • /
-Fiack4A pA Li
f np.-4 14;
•_-_- -
•.•
•••••••••••••• • ••• ••••••••• .• •
Bioassay Chain of Custody Foqn
1 ras`)
Az.ilr,)s::: c----).....-1-- i1/4t., sc.it_f-c)/() Dr. .,--. ,,
____._ ._
11CzqfiCeiVa /?$c3 t.
: 0\61
ic
NH }F-.S
% f.fn J Iut (PA/):. MtL:di 0:h 1(A
p;alt now: %
Sariple Collector: Prirt
Slgnatur-.--)
Sancle riTe:
Composite
...)Eite Started 631s Time. • a- pm
Date Ended .5 Time: i0,55
Samr)14 piH L # Hrs:
Grab
Date.
Clalt101 4.1
AN PM
Method of r'ans;-..ortat:on to the Lab:
Chain ot uustody Release
---' Re h i.-..itti s 1 i
Date
Time
....-1,........-.. • ..,":1=;..2
Ree.i by
.... ",,.7%...,,,, • ....--,•.=,..:17.
'Jaw 1
le „ .-----
IV:, % . •.:^,1
! III)
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/ 2 /5-
j50pal
b6,_J, 0_,,,
I
- .
.
. ..._
_...i,
i
J,
-
Comments
For Pace AtiaTytical, Inc. Use Only
Pace Work Di der Nurter: (11 .57C1`75
,.-.1
RecEiving Temperature: Recei;eBy:
Paco ,\ laly+2a1 Se7v4.1Y.ks, Inc. Address: 0701 C,*oorerence t4 27017 incii-j; (5) '54

L
ttlf, iSa, 1".rt t
l 3c!it td, it i.,.
(_ urt)' :
Fftkl .rl:
Plant Row.
Bioassay Chain of C::usiciciv Form
\IP [Wil--41L91S3()- i 1,
i (! t
$ niple Coliec:tor. Print
Signature;
Sans?le Type:
Composite
Date Started
Date Ended
Grab
ar14.'S •
San pl s r e3 It:
Date:
Sampb Vo:unle:
14.110
Lll
'Method of Transportation to the Lab:.
lime:
Time:
Time:
qclut
11411
Q n is 1;n Lob A
_ 5 AM Dr
/, }r r�n�
tl{. trl
AM or PM
Chilled auri:;g �OiiC'L:?{':(�� r •:•::ter
Chain 4f eustodv k +::ase
Relirlgaishe f `��
Uat '
.tst.
Time
- ^:sr,'ur....-:._..... _r.-_-.--r�.:,
Rect*tiecj By
-
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- _-
Time
T....
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J/�J
_,, ^—.-.x��Zx-.+r':
•
\ I
CrG ,f '
1 '- t , 1
(ra -
1
>� c: t J
,w
Comments:
Pace Wofk Order Number:
Receiving Temperature:
For Pace Analytical, Inc. Use Dilly
R! c 'Ieci
Pare Aralytica' Se vicee, Inc. Address::i;'01 Crtnfert=nt71-- I•lr . R.;:le J: r!1C ::t':

Pace Analytical
Laboratory Report
Mr. Art Hough
City of Havelock
Drawer 368
304 N. Jackson Dr
Havelock. NC 28532
Project Metals 1 /29
Pace Protect No 9223895/
Pace Analytical Serdikr's, Inc
R:', e st'de 1),
Asriev,e NC
525),:�•71
f a q r' 1 O t
Report Date 03!C3/2015
Date Received 02.26/2015
Sample: HAVELOCK BIOASSAY METALS Lab ID: 92238951001 Collected 01;29' 15 08 00 Matrix. WatY.r
Parameters Results Units Report Linn Analyzed Qualifiers
Aluminum ND ugiL 100 93/02/ 15 21 15
Antimony ND Lg'L 5 0 33:02115 21 15
Arsenic ND ug!L 10 0 03102/ 15 21 15
Barium ND ug; L 5 0 03: 02' 15 21 15
Beryllium ND u9;L 1 0 03/02' 15 21 15
Boron 122 ugiL 50 0 03/03/15 15 2C
Cadmium
ND ugiL 1 0 03,0215 21 15
Calc urn 39000 ugiL 100 03/C215 2' 15
Chromium ND ugrl 5 0 03/C215 2' 15
Cobalt
ND ug/L 5 0 03/C2:1 5 2' 15
Copper
NO ug/L 5 C 03/02r 15 21.15
Iron ND ulL3r,
9 50C 0� 0�2 �15: 1 'S
Lead ND 5. C 03'02:15 21 '5
Magnesium 2120 ug/L ,: 1 b
9 100 u3'0� � ., : a t,
Manganese 6.0 ug/L 5 0 03:02:15 21 15
Molybdenum NO ug/L 5 0 03:02;15 21 15
Nickel ND ug/L ,2 , r
Potassium 9 5 G C3•(,2 15 � 1 1,.
6110 ug/L 5300 C3/02/15 21 15
Selenium ND ug/I 10 0 03:02:15 21 15
Silicon 6240 ug/L 100 03:02/ 15 21 15
Silver
ND ugrL 5 0 03'02/15 21 15
Soorurit 80000 ugrL 5000 03/02/15 21 15
Strontium 145 ug/L 5 0 03:02:15 21.15
Thalliam ND ,r /L 1 , 2; 5 5
Tin ND Ja/L 50 03/02/15 21 15
Ti:anrum ND .rg/I 5 0 03r32i 15 21 15
Vanadium ND ug/L 5 0 03/02! 15 21 15
Zinc 37.0 ug/L 13 0 03021' 5 21 15
Reviewed by
Stacy Tart;,•
stacy tarle;c.pacetabs corn
Asheville Certification IDs
2225 Riverside Drive, Asheville. NC 28804
Florida/NEAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #. 37712
North Carolira Wastewater Certification # »0
South Carolina Certriicatior• # 99030001
West Virginia Certification # 356
Virginia/VELAP Certification # 46022?

Cleaning lab war or WET testing
Steps
Clean pickle jar with 1/10 oz liquinox and tap water
Rinse with cold tap water twice.
Mix up 10% nirtic acid solution in fume hood wear appropriate PPE.
Rinse pickle jar with 10% nitric acid solution with lid on jar.
Rinse jar with deionized water twice.
Rinse jar with pesticide grade acetone. Use fume hood and wear PPE as required.
Rinse jar with deionized water three times.
Take jar to sampling point effluent sampler.
Replace sampler tubing with new food grade silicone tubing
Rinse tubing and jar 3 time with sample water. Ensure jar is filled with sample water.
Empty jar and put in sampler and begin sampling.
Repeat steps every sampling event.
Initials/ date

Effluent Toxicity Report Form - Chronic Pass/Fail and. Acute LCS) Date:: 04/21/15
Facility: CITY OF HAVELOCK WWTP NPDES#:
Laboratory Performing Test: PACE ANALYTICAL
X
5igna u�= • Operator in Responsi
igna ur La •or.; tory
Work Order: 92244399
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
1 2 3 4 5 6
NC0021253 Pipe#: 001 County: CRAVEN
Comments:
* PAJEED: 8.27t Reduction *
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
7 8 9 10 11 12
# Young Produced
35
33
36
28
32
34
26
33
27
29
33
29
Adult (L) ive (D) ead LLLLLLLLLLLL
Effluent %: 90%
TREATMENT 2 ORGANISMS 1 2
3 4 5 6 7 8 9 10 11 12
# Young Produced
33
33
25
30
24
31
29
28
27
29
27
28
Adult (L) ive (D) ead
Chronic Test Results
calculated t = 2.063
Tabular. t = 2.508
% Reduction = 8.27
% Mortality
Avg.Reprod.
0.00
Control
31.25
Control
0.00
Treatment 2
28.67
Treatment 2
Control CV
10.580*
% control orgs
producing 3rd
brood
100*
PASS FAIL
X
Check One
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
7.71
7.20
8.30
7.95
s
t e
a n
✓ d
t
1st sample
7.13
8.10
8.07
7.85
1st sample 2nd sample
7.38
7.69
8.26
8.59
s
t
a
r
t
1st
7.58
7.68
8.40
8.45
s
e t e
n a n
d r d
t
sample 2nd sample
6.39
4.85
7.73
6.05
7.78
6.99
6.25
5.98
LC50/Acute Toxicity Test
(Mortality expressed as %,
Complete This For Either Test
Test Start Date: 04/08/15
Collection (Start) Date
Sample 1: 04/06/15 Sample 2: 04/08/15
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
1 S S
Sample 1 X 24 hrs L A A
U M M
X 24 hrs T P P
Sample 2
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
50
241
779
762
<0.1
<0.1
0.9
0.5
combining replicates)
%
%
%
%
%
%
t*
Is
o
LC50 =
95% Confidence Limits
Concentration
Mortality
start/end
Method of Determination
Moving Average - Probit
Spearman Karber Other
Note: Please
Complete This
Section Also
Control
start/end
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
High
Conc.
D.O.

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 04/21/15
Facility: CITY OF HAVELOCK WWTP NPDES#: NC0021253 Pipe#: 001 County:CRAVEN (4111
Laboratory Performing Test: PACE ANALYTICAL
Reduction: 8.27t
CONTROL 90% Effluent
# Replicates 12 12
Female Live 12 12
Adult Male 0 0
Adult Dead 0 0
Adult Mortality 0.00W 0.00t
# Neonates 375 344
Mean # Neonates 31.250 28.667
Standard Deviation 3.306 2.807
Coefficient of Variation 10.580*
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 C 26-5.2500 13 E 29 0.3333
2 E 24-4.6667 14 C 32 0.7500
3 C 27-4.2500 15 E 30 1.3333
4 E 25-3.6667 16 C 33 1.7500
5 C 28-3.2500 17 C 33 1.7500
6 C 29-2.2500 18 C 33 1.7500
7 C 29-2.2500 19 E 31 2.3333
8 E 27-1.6667 20 C 34 2.7500
9 E 27-1.6667 21 C 35 3.7500
10 E 28-0.6667 22 E 33 4.3333
11 E 28-0.6667 23 E 33 4.3333
12 E 29 0.3333 24 C 36 4.7500

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
i x(n-i-1)
COEFFICIENTS AND DIFFERENCES
x(i) a(i) x(n-i-1) - x(i)
1 4.7500 -5.2500
2 4.3333 -4.6667
3 4.3333 -4.2500
4 3.7500 -3.6667
5 2.7500 -3.2500
6 2.3333 -2.2500
7 1.7500 -2.2500
8 1.7500 -1.6667
9 1.7500 -1.6667
10 1.3333 -0.6667
11 0.7500 -0.6667
12 0.3333 0.3333
1
w _
206.9167
0.4493
0.3098
0.2554
0.2145
0.1807
0.1512
0.1245
0.0997
0.0764
0.0539
0.0321
0.0107
X 198.6524
Calculated W = 0.960 Critical W = 0.884
0.960 z 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
F =
Test Passes!
F test for Homogeneity of Variance
Control variance
10.9318
Effluent variance 7.8788
1.39
10.0000
9.0000
8.5833
7.4167
6.0000
4.5833
4.0000
3.4167
3.4167
2.0000
1.4167
0.0000
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
1.39 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
31.3 - 28.7
t = = 2.063
1.252
Degrees of freedom = 22
Critical. t = 2.508
2.063 < 2.508
Test passed. There is not a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test PASSES

Ceriodaphnia dubia Chronic Pass/Fail T. xicity Test
Client: a_VEA1
Q.
Culture T ransfer (Date/Ti.. _ -�1- IDES #: o 3 im
Age of Or �( 1 � Organism Boni n
Organism: ( at / �—r— (batealme)•
Dilution Water Batch:Time Fed (Culture):
Start Date: -- ' - Temp Dilution Water:
1n Traasfex Date: Time • Analyst: Sr . Rando
Time: 2" Analyst ^-Zy^
d T3ransfer Date: 1 Timc: 3j
Ending Date: - Analyst •til—
" Time: Analyst
Control ---------------------------------------------------------------------------R ewed by: 5�
Day 2 1
# Young Produced
Adult: Live, Dead
Day 5
# Young Produced
Adult: Live, Dead
Da 7
# Young Produced
Adult: Live, Dead
# Total Produced
# Young Produced
Adult: Live, Dead
L
1
3 4 5 6
2 3
31,t4
2
4
ag
5
0
6
'6/7 619
5 6 7
ir--
7
5
7
8 9 10T 11 12
/9 5 7 @efstom.
I1-. e.-- 1--
8 9 101 '11 12
8 9 10 11 12
l 2 3 4 5 6 7 8
Da 5 1 2
# Young Produced
Adult: Live, Dead
Organism source: i
Temp Mock solutio
zed: t/ Incubator:
Collection (Start) Date
1' Sample: 4-4-li:"-A 5
Sample Type/Daration
Sample
2Sample
Hardness
•(mom)
Conductivity
(EhS/cm)
• Chlorine
()
Sample Temp
pH 100%
Days
Day 0
Day 1
. Day2
Day 3
Day 4 .
Day 5
Fed By
SI
Da 6
y iDT
Time
133o
I12
2'd Sample: 4-815
Control
2i
1st Sample 2nd Sample
,I .
PH
Start i End
Start End
Start
End
;Control
'r"71
7zD
7. 6.1. (04
1;5
e Ie
7. (QfS
Treatment
�
�, 30
1
D.O.
Start
Start j Endi`
Start
End
l
G, 1 5
Y.
0. 1 O
6 31
14, C5
1, 7 s
Co.
TreatmentContro
�,L�
. $�
1.73 i
10,y5
C
1�.Qd<.na
,gin:
' Temp.
Start
grad
gt�1Pm,i
6'd..,.a :
:

1,.7a. cal
{ a 1
.+�vurllcr IL rvtllllC.
B;oassay Chain of Custody
Document Number'
r-RAL-CS-007-i ev.01
ua:e Revised: June 22, 2012
Page 1 of 1 —
Issuing Authority:
Pace Carolinas Quality Office
Facility Name:
Address:
Bioassay Chain of Custody Form
30.5-0)
I , �• P.O. Box:
Phone #t
Contact r- ---634.01 h
County :
Effluent Dilution 1WC : t
� ��� 1 (� Test Method: CPo1(&¢prmi
Plant Flow: ��
Sample Collector: Print
Signature
Sample iypg_
Composite
Date Started
Date Ended
Samples per Hr:
Grab
NPDES permit #: bi Cip—_463_, pipo: 00
Time:
Time:
# Hrs:
s
C;C� .dr PM
LI ' Jor PM
Date: Time: AM or PM
Sample Volume: : . ` )1 Chilled during Collection?
Method of Transportation to the Lab:
Comments:
For Pac pa&ygicail, Inc, Use only --
Pace Work Order Number: t/L `It-131f 1
Receiving Temperature: p . Y 0 Received By:
Pace Analytical Services, Inc. Address: 6701 Conference Dr., Raleigh, NC 27607 Phone: [phone]

/c*W
Facility Name:
Address: . 3
County.:
idu ut,,erit name: riots' June 22, 201z
Bioassay Chain of.Custody
Document Number. Page 1 of
issuing Authortfy:
F RAL-CS-007 rev.01 ► Pace Carolinas Qualify Office
Bioassay Chain of Custody Form
6 1:- go, JwrJck r `fie Ali-
P r P.O. Box:
• Phone #: • -5a S� (D31`)oI
Effluent Dilution (1WC):41
Plant Flow. C r -1 ih (r
Sample Collector:
&ample TYpe•
Composite
• Date Started •
Date Ended -
. Samples per Hr:
Grab
Contact
PDES permit #:I S 0 Q‘ i ?5 3 pipe: 0 p
Test Method: e, l PO, fe, E'l,)► & Du4�P/r
6.7 1Time:
S Time:
# Hrs..
r PM Y1l a1,0 "Ms c f\--1" io/JO\
rP M
Date: Time: Ali! or PM
Sample Volume:
Chilled during Collection? Yes or No
Method of Transportation to the Lab:
• Chain of Gustody e ease
Date Time
5330
Date
y-1d -r 5-
/ 761)
o846
j
N
Comments:
Pace Work Order Number
Receiving Temperature:
For Pace Analytical, Inc. Use Only
• ,C4't- Received By.: G
Pace Analytical Services, Inc. Address: 6701 Conference Dr., Raleigh, NC 27607 Phone: [phone]

Eenvironmenta , Inc. [phone] . FAX [phone] ''"
P O. Box 16414, Greenville, SC 29606
Craftsman Court. Greer, SC 29650
TOXICITY IDENTIFICATION EVALUATION
USING EDTA CHELATION
TO INVESTIGATE THE POTENTIAL ROLE
OF COPPER AND ZINC IN EFFLUENT TOXICITY
Facility: City of Havelock, NC
Sample ID: WWTP Effluent
April 2015
Page 1 of 22

1.0 INTRODUCTION
In March 2015 a chronic pass/fail toxicity test of effluent from the City of Havelock wastewater
treatment plant (WWTP) indicated a failure. Under the Division of Water Resources ATB Action Level
Document for Copper and Zinc (10/25/2000), a toxicity test failure must be followed either by
acceptance of copper and zinc limits or by testing options to confirm that these metals were not the cause
of toxicity. In response to the March 2015 toxicity failure, the City of Havelock has opted to use Option
3, which involves the EDTA treatment under a Toxicity Identification Evaluation to investigate the role
of copper and zinc. Specifically, a sample of effluent was tested for chronic toxicity with and without
addition of the metal chelator EDTA. EDTA is effective for removal of toxicity caused by cationic
metals such as copper and zinc. This report presents the results of the investigation.
Page 2 of 22
Havelock : TIE/EDTA Investigation
ETT; April 2015

2.0 SAMPLE COLLECTION
A sample of effluent was collected on March 20, 2015. It was assigned ETT ID#44986.
3.0 TREATMENT METHODOLOGY
A stock solution of 500 mg/L of disodium EDTA was prepared by adding 0.5 g of solid to 1000
mL of deionized water.
10 mL of the 500 mg/L stock solution were added to 1000 mL of Havelock effluent. This
provided an aliquot of effluent with 5 mg/L of EDTA.
The 5.0 mg/L EDTA spiked effluent was diluted with surface water to prepare test concentrations
of 45, 60, 75, 90 and 100%. These samples were used to initiate the test and to renew the test
solutions on Day 2 and Day 5 of the test, as per NCDENR protocols.
An aliquot of surface water also was spiked with 5.0 mg/L of EDTA to function as an EDTA
control.
Page 3 of 22
Havelock : TIE/EDTA Investigation ETT; April 2015

4.0 TOXICITY TESTING METHODS
Toxicity testing was conducted using the Shoat -term Methods for Measuring the Chronic Toxicity of
Effluents and Receiving Waters to Freshwater Organisms Method 2002 EPA-821-R-02-013 and modified
per NCDENR protocols. The test organism was Ceriodaphnia dubia and the dilution water was Hardness
Adjusted (45-50 mg/L) Surface Water. Test organisms were fed 2-5 hours prior to test initiation with
Pseudokirchneriella subcapitata and YAT. Each test dilution was comprised of ten replicates of 1 test
organism.
Ceriodaphnia dubia
1.Temperature: 25°C ± 1
2.Light: 100 ft-cd; 16 hr It/8 hr dk
3.Test Chamber Size: 30 mL plastic cup
4.Test Solution Volume: 15 mL
5.Renewal: Day 2 and day 5
6.Age of Test Organisms: <24 hours
7.No. of Neonates / Test Chamber 1
8.No. Replicates / Dilution 10
9.Feeding: Daily
10.Cleaning of Test Chambers: None
11.Aeration: None
12.Dilution Water Hardness adjusted (45-50 mg/L) surface water
13.Effluent Concentrations: 0, 45, 60, 75, 90, 100%
14.Dilution Factor: NA
15.Test Duration: 7 days
Havelock : TIE/EDTA Investigation
Page 4 of 22
ETT; April 2015

5.0 RESULTS AND DISCUSSION
5.1 Review of Results
Measured Copper in untreated effluent: <5.0 ug/L
Measured Zinc in untreated effluent: 51.0 ug/L
Toxicity test results for treated samples are summarized by treatment, as follows;
Untreated Effluent
(Baseline Test)
5 mg/L EDTA
Spiked Effluent
5.2 Baseline Test
Mean Reproduction By Test Concentration
0% 45% 60% 75% 90% 100% IC25 Results
21.8 16.9 19.1 19.4 21.8 22.6 >100% Sample not toxic
21.8 20.3 19.8 22.1 20.9 18.7 > 100% Sample not toxic
There was no chronic toxicity found in the untreated effluent. In as much as the sample was identified as
being chronically toxic in the March 2015 pass/fail chronic test, it seems likely that whatever toxicity
may have been present had degraded or volatilized. Toxicity due to cationic metals, such as copper and
zinc, is persistent and would be expected to continue to be present in the sample after the holding period.
Thus, this is evidence that toxicity in the original test was not a result of elevated aqueous copper or zinc.
5.3 Spiked 5 mg/L EDTA Test
No toxicity was present in the untreated sample, therefore the effect of EDTA could not be determined.
5.4 Measured Metal Concentrations
Measured concentrations of copper and zinc were too low to be a potential cause of toxicity. It would be
expected that copper concentrations would need to exceed 30 ug/L and zinc concentrations exceed 200
ug/L to result in chronic toxicity.
Page 5 of 22
Havelock : TIE/EDTA Investigation ETT; April 2015

F1'h 6.0 SUMMARY
• No toxicity was present in the untreated sample.
• Test results indicate that toxicity did not result from copper and zinc. There are two lines of
evidence for this conclusion;
1). Toxicity was not persistent. Toxicity due to copper and/or zinc would be expected to be
persistent in as much as these metals do not degrade or volatilize.
2). Measured concentrations of copper and zinc were too low to result in chronic toxicity to the
test organism Ceriodaphnia dubia.
• The effectiveness of EDTA treatment for chelation of copper and zinc could not be determined
due to the absence of toxicity in the untreated sample.
Havelock : TIE/EDTA Investigation
Page 6 of 22
ETT; April 2015

APPENDIX A
Untreated Effluent
AT-3 form and Bench Sheet
Page 7 of 22
Havelock : TIE/EDTA Investigation ETT; April 2015

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility:
Laboratory
Signature o
Sampl
Collec
Comp
Hard
Spec. C
Chl
Sample t
Control
Effluent %
45.0%
Effluent %
60.0%
Effluent %
75.0%
Effluent
90.0%
Effluent %
100.0%
MAIL
TO:
ve r I VI- rimvt LL) 4\ NPDES # NC 0021253 PipeA 001 County: Craven
osite
orine
Performing Test: ETT Environmental, Inc.
ad
Comments:
Baseline for EDTA
f O.R.C. Signature of Lab Supervisor
Treatment
Test
Start Date
Time
Info
04/15/15
1150
End Date
04/22/15
Time
12:50
9Information
Sample
Sample Control
(Start
1Renewal1
Renewal2
1Stan
( I Renewal1
'Renewal
I
:ion Start Date
.3/20/15
Treatment
100%
100%
100%
/
2
Grab
pH Init.
8.1
8.3
8.2
Control
Control
Control
(Duration)
X
pH Final
86
8.5
8.6
6.1
8.2
8.1
8.1
8.0
8.0
ness (mg/L)
50.0
D.O.Init
9.8
9.3
8.5
8.2
8.0
8.1
Ind. (umhos.cm)
712
215
D.O. Final
7.6
7.9
7.6
8.0
7 8
(mglL)
<0.05
Temp Init
24.3
24.7
24.5
24.3
7.4
emp. at Receipt
0.6
Temp Fula!
25.3
25.5
252
25.3
24.7
25.5
24.7
Chronic
Test Results
25.2
Final Cont Mon. %
0%
Organism #
% Cont 3rd Brood
80%
1 2 3 4 5 6 7 8 9 10 11 12
Mean
Control Repro CV
26%
# Young
31
27
13
25
26
14
18
22
21
21
none
none
21.8
48 Hour Mortality
(L)ive
(D)ead
LLLLLLLLLL
none
,none
-
Control IWC
oof10
0of10
1
2
3
4
5
6
7
8
9
10
11 12 Mew
Significant?
No
# Young
27
22
0
22
0
24
25
14
20
15
none
none
16.9
Final Mortality Sign. @
Adult
(L)ive
(D)ead
L
L
L
L
L
L
L
L
L
L
none
% R
none
22.5%
%
or
no conc
1
2
3
4
5
6
7
8
9
10
Mean
Reproduction Analyses
Repro LOEC= >100.00% NOEC= 100.0%
Method: Steel's Test
Normal Dist? no Method Kolmogorov
Statistic 1.141 Critical 1.035
Equal Var? yes Method samerrs
Statistic 14.06 Critical 15.10
Non -Parametric Analysis (if applicable):
# Young
29
18
18
20
16
19
23
20
21
7
19.1
Adult
(L)ive
(D)ead
LLLLLLLLLL
r Red
12.4%
1
2
3
4
5
6
7
8
9
10
Mean
# Young
25
20
0
22
16
22
25
24
22
18
19.4
Adult
(L)ive
(D)ead
LLLLLLLLLL
-'
11.o%
Method: Steel's Test
Effuent % Rank Sum Critical
1
2
3
4
5
6
7
8
9
10
Mean
45.0% 93.50 75.00
60.0% 90.00 75.00
# Young
24
21
19
23
28
22
26
17
21
17
21.8
75.0% 98.00 75.00
Adult
(L)ive
(D)ead
L
L
L
L
L
L
L
L
L
L
., Red
0.0%
90.0% 104.00 75.00
100.0% 108.50 75.00
1 2 3
4 5 6 7 8
9 10
Mean
Overall Analysis IC25= >100%
Result = PASS/FAIL or
Test LOEC: >100.00% NOEC= 100.0%
Chronic Value= >100%
# Young
25
21
24
23
25
21
27
21
24
15
22.6
Adult
(L)ive
(D)ead
L
L
L
L
L
L
L
L
L
L
o Red
-3.7%
Environmental Sciences Branch
Division of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
t% Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95
Page 8 of 22

ource Prep 1 1 2
fed
lime led & renew
New temp. "C
Old temp. "C
D=Deed N/A -Lost or not used
Test Day
3 4 5
6 7 8
'1/4110 4-1
M3 4-9
M64-9
D84-3
F6 4.3
A94.3
44950 E
44950 F
449501
44950J
A
b
+11J+15
31
control
8
+4+9
14
27
C
3
10
13
D
+4+8
13
25
E
+4+8
14
26
F
4
10
14
G
3
+7+8
18
H
+4+7
11
22
I
+4+7
10
21
J
+3+8
10
21
+
60
75
+ 4+6
+3+7
D
+5+5
0
+4.10
•4+8
4
+3*5
+3+3
*5+6
12
12
0
10
13
10
12
9
18
17
22
0
22
0
24
25
14
20
15
19
+4+4
10
18
+3+10
5
18
+3+7
10
20
+3+5
8
16
+5+7
7
19
. 5+7
11
23
•3+5
12
20
16.9
*3+7
11
21
3
4
7
19.1
l5
z5
•4+7
9
20
D
0
+ 5+6
11
22
+3+5
8
16
+3+7
12
22
+4+8
13
25
+3+7
14
24
+5+8
9
22
AM
AM
C, +7 PM
AM
02 10 Phl
14.7
15.3
AM
05`.9Ahi
JC
0925 AL1
+4*6
+ 4*/
+3+7
+3+8
+5+6
+5+7
*3*8
+6+9
+2+7
+4+5
+3+6
A.i5+/
+5+7
.5+9
+4+6
+5+7
+4+7
+5+8
+3+7
*4+9
+3*3
AM
AM
01 2" PM
14.5
25.5
JG
01 05 PM
8
1,3
11
8
12
16
11
11
8
12
8
14
9
10
13
13
10
14
11
11
9
18
14
21
19
23
2t-
22
26
17
21
17
15
21
24
23
25
21
27
21
24
15
End Date
22-Apr-15
12 so PI)' FJ
25.21
19.4
21.8
LabA
44..1e6
Client
CITY OF HAVELOCK
Sample ID
EFFLUENT
NPDES#
NC
County
0
Month
4
Start & fed Date
15-Apr-15
Start & fed Time
1150
Started & fed By
Test Organism
Noo. born date
AM
Ceriodaphnla dubia
14-Apr-15
Neo. born time
1700.2150
Test Type
NCCD
Dilution Water
NC H2O4-8.15
Units for Conc.
%3rd BROOD
Test vessels
30 mi
Test volume
15 mi
Incubator 9
1
Light
161U8dk
Initial Temp "C
Selenastrum
/25
0.05 mi
VAT
0.05 ml
Test method
CPA
Comments
• 44950 CON E.F,I,J
CON TEMP
INITIAL- 24.3
DAY 2- 24.7
DAY 5- 24.7
DAY 2. NCH2O4-15.15
Page 9 of 22

APPENDIX B
EDTA Treated Effluent
AT-3 form and Bench Sheet
Havelock : TIE/EDTA Investigation
Page 10 of 22
ETT; April 2015

Effluent Aquatic Toxicity Report Form/Phase II Chronic CeriodaDhnia
Facility: CITY OF HAVELOCK: EDTA TREATED NPDES # NC 0021253 Pipet 001 County: Craven
Laboratory Performing Test: ETT Environmental, Inc.
X✓'
Comments:
Treated w/ 5 mg/L EDTA
Signature of O.R.C. Signature of Lab Superviso
of
Test
Start Date
Time
End Date
Time
Info
04/15/15
1150
04/22/15
12:13
Sample Information
Sample 1
Sample 2 Control
(Start
'Renewal 1'Renewal 2
Start
(Renewal 1
(Renewal
I
Collection Start Date
03non5
Treatment
100%
100%
100%
/ Control
2
Grab
pH Init.
6 1
8.3
8.2
7.9
Contra
Control
Composite (Duration)
X
7.9
7.8
pH Final
8.6
8.5
8.6
8.1
8.0
8.1
Hardness (mg/L)
50.0
D.O. bit
8.6
8.1
8.1
8.5
8.3
Spec. Cond. (umhos.cm)
712
215
D.O. Final
7.8
8.0
7.3
80
8.1
Chlorine (mg/L)
<0.05
Temp Inn
0.0
24.7
24.6
0.0
77
73
Sample temp. at Receipt
0.6
Temp Final
25.3
25.5
252
25.3
0.0
0.0
Chronic
25 5
Test Results
25.2
Final Cont Mort. '
0%
Organism #
1 2
% Cont 3rd Brood
80%
3 4 5 6 7 8 9 10 11 12
Mean
Control Repro CV
26%
Control
# Young
31
27
13
25
26
14
18
22
21
21
none
none
21.8
48 Hour Mortality
(L)ive
(D)ead
LLLLLLLLLL
none
none
Control
IWC
Oof10l 0of10
1
2
3
4
5
6
7
8
9
10
11 12 Men
Significant? No
Effluent %
# Young
23
20
17
23
24
21
28
25
13
9
Adult
(L)ive
none
none
20.3
o Red
Final Mortality Sign. @
45.0%
(D)ead
L
L
L
L
L
L
L
L
L
L
I
none
none
6.9%
%
or
no Conc
--
Reproduction Analyses
1
2
3
4
5
6
7
8
9
10
Mean
Repro LOEC= >100.00%
Effluent %
# Young
24
19
22
27
5
23
25
20
15
18
NOEC= 100.0%
60.0%
Adult
(L)ive
(D)ead
L
L
L
L
L
L
LLL
L
19.8
v Red
Method: Dunnetts t Test
Normal Dist? es
Y Method xamayorov
1
2
3
4
5
6
7
8
9
10
9.2%
Mean
Statistic 0.939 Critical 1.035
Equal Var? yes Method Bartlenns
Statistic 0.80 Critical
Effluent %
# Young
28
14
16
25
24
28
29
26
16
15
15.10
Adult%
22.1
Red �Method:
Non -Parametric Analysis (if applicable):
Dunnetts t Test
75.0%
(L)ive
(D)ead
L
L
L
L
L
L
L
L
L
L-1.4%
Effuent % Calc. t Critical
45.0% 0.57 2.28
1
1
2
3
4
5
6
7
8
9
10
Mean
60.0% 0.76
2.28
Effluent %
# Young
24
22
14
22
11
25
26
24
21
20
Adult
20.9
75.0% -0.11 2.28
(L)ive
;:, Red
90.0% 0.34 2 28
90.0%
(D)ead
L
L
L
L
L
L
L
L
L
L
4.1%
100.0% 1.18 2.28
Overall Analysis IC25= >100%
1 2 3 4 5 6 7 8 9 10 Moan
Result = PASS/FAIL or
Effluent %
# Young
27
17
5
13
25
17
23
19
20
21
18.7
100.0%
Adult
(L)ive
(D)ead
L
L
L
L
L
L
L
L
L
L
%o Red
Test LOEC: >100.00% NOEC= 100.0%
14.2%
Chronic Value= >100%
MAIL
TO:
Environmental Sciences Branch
Division of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
*Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
1-% Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95
Page 11 of 22

ource Ire
Test Day
1
1
[(14-Z
34.9
4-9
4-3
4.3
4-3
44950 E
4950 F
49501
4950J
- - u 0 ( 8
Total
A
6
+1U+114
31
control
B
+4+9
27
C
3
10
13
D
+4+8
13
25
E
+4+8
14
26
F
4
10
14
G
3
+7+8
18
H
+4+7
110
22
1
+4+7
10
21
J
IA
1
+3+8
10
217"
45
60
75
renew
9
17
23
C
D
E
F
3
5
+7+5
17
12
11
20
17
23
G
H
8
C
D
E
F
5
+4+5
+10+9
12
24
21
+5+8
+3+8
+5+,-
5
3
6
15
14
8
6
•2
13
28
25
13
9
24
19
+3+7
+5+8
12
14
22
27
0
5
5
G
H
+4+7
12
23
+4+7
+4+8
14
8
25
20
20.3
J
6
9
15
A
B
C
0
E
F
G
H
+3+5
+3+y
3
10
lb
11
18
2t1
14
5
11
16
+4+8
+5+7
+6+8
+4+7
5
+8+16
13
12
14
15
25
24
28
29
26
19.8
5
11
16
A
A
AM
llme led & renew 91 +S PM
New temp. °C
Old temp. °C
D=Dead N/A -Lost a not used
AM
r411148..
AM
02 16 PM
24./
LS..i
AM
05 ]0 81.1
JC
8 24 AM
4
+3+b
+4+7
4
,4+8
3
+5+8
-6+5
-2+7
+3+6
+3+3
+J+IU
+3+8
5
+3+6
+6+5
+3+5
.4+7
+3+8
+2+8
+3+5
AM
AM
tiPN
24.b
25.5
D
JG
1, 05 PM
11
13
11
10
10
8
12
15
15
12
14
14
6
4
14
9
12
8
10
13
15
14
22
14
22
11
25
26
24
21
20
ll
17
5
13
25
17
23
19
20
21
End Date
21-Apr-lb
FJ
25.1
22.1
20.9
18.7
TSbl-
44 8 EDTA
Client
\CITY OF HAVELOCK
Sample ID
EFFLUENT
NPDES#
NC
County
0
Month
4
Start & fed Date
15-Apr-15
Start & fed Time
1150
Started 8 fed By
AM
Test Organism
Ceriodaphnla dubia
Neo. bom date
14-Apr-15
Neo. born time
1700-2150
Test Type
f4CCD
Dilution Water
fI�JC H204-8-15
Units for Conc. i'1
%3rd BROOD
Test vessels
30 mi
Test volume
15 ml
Incubator #
1
Light
16168dk
Initial Temp °C
25
Selenastrum
3.05 m1
YAT
105 ml
Test method
.PA w2,.A o>O, 1 Ion:
Lon, meals
+44950 CON E,F,I,J
SAMPLE TREATED WITH EDTA
SEE SPEC PROJ BOOK
FOR DETAILS
DAY 2. NCH20 4-15-15
Page 12 of 22

APPENDIX C
Chain of Custody
Page 13 of 22
Havelock : TIE/EDTA Investigation ETT; April 2015

; � 1 �• ET°
•f
PO Box -.6414, Greenville, SC 29606-74t4
[phone]. [phone] Far [phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
WWW.ETTre4VIRON. NTAL.CCM
CHAIN OF CUSTODY RECORD
Page 1 of 1
Client: J%l / 0 , l r 71 L.&% 6//
Program
Containers
Preservative
Parameters
Facility:
a„ l/ C. AS(7) (4 (&) 7 P
I Clean Water Act
Stornxvatcr
—
✓:
rs
-
-0
Z
it of Containers
t ,
;�
o
_
g.
>
I-I1.1S6+
2-HCL
a= oti
6. pd,s
Whole Effluent Tosierh
N
N
i
Macioiuvcilcbrntc II:)
Chernizel Analysis & Other
11 <II FIV'1 (Sll\!!)ISM/ .I.1
State: 1 , NPDES #: AI C1 z d 1 c.53
Acutc
Chronic
Test Organisms
SAMPLE ID
U
=
6
(Composite only)
CompositcStnrt Date
Tlme
;Grab or Composite)
Sample Catlealan Date` Time
Sign, and Print below
the dotted line
Collectchl by
�i r
P.
=
¢
Acute Multi -Cone.
—
-
—
C.)
ci
c
:J
—
c
v
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2
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ID. ambigua
c
—
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a
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a
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=
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✓/A (7'' ``'rt
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'fiffg&
316
il
to
m
r
P'-r, r5 %rrAA rat
N
rV
:7CA P ii P
Special Instructions:
Sample Custody Transfer Record
Date Time Relinquished By / Organization, Received By / Organization
Secure
Area
R°ccipt
Temp aC
Sample
Preserved?
/11.31i S133 0
O. -Ati r i fsl,/ii L 6,, 1 0fi lIFID! 1‘ GL;
P 5
aa�,
/P/N
��5 =
it,- . , Gam—
e. a,
ir
COMPOSITE &4MPL!NG PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEAIPERATURE MONITORING PROCEDURES
Sample temperature during collection and tansport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bas.
HOLD TIME PROCEDURES
For toxicity resting the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used afer 72 hott-s from sample collection.

APPENDIX D
Copper and Zinc Analyses
Page 15 of 22
Havelock : TIE/EDTA Investigation ETT; April 2015

Client
Dear Client:
Rogers &Callcott
ENVIRONMENTAL
ETT Environmental
Bob Kelley
PO Box 16414
Greenville. SC 29606-7414
Laboratory Report
Project: Wastewater
Work Order: 5040627
Received: 04/15/2015 10:00
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on April 15.2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted. all analyses
performed under NELAP ecrtifieation have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval
for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee. or the
person responsible for delivering to the person addressed. you may not copy or deliver this message to anyone else. If you receive this message by
mistake. please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager. at kara.hrkachrrogersandcallcott.com or
(864)-335-4956 if you have any questions about this report.
Report Approved By:
Kam Hrkach
Project Manager
-L. P.•,� S6 1, i Lc
Adlift
rogersandcallcott•corn
This report may not be reprothiced except infra without written permission from Rogers & Callcott. Inc.
Page 16 of 22
Page 1 of 7

Rogers & Callcott
ENVIRONMENTAL
Certificate of Analysis
Client
ETT Environmental
Bob Kelley
PO Box 16414
Greenville, SC 29606-7414
South Carolina Greenville Laboratory Identification 23105
South Carolina Cohaubia Laboratory Identification 40572
North Carolina Laboratory Certification Number 27
North Carolina Drinking Water Lab Number 45710
NEL4P Utah Certificate Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Wastewater
Work Order: 5040627
Received: 04/15/2015 10:00
Sample Number Sample Description Matrix
Sampled Type
5040627-01 44986 Wastewater 0320115 10:30
PO Bo. 5655 f;n.rnnke
•
rogersandcallcott.com
0423/2015 13:36 This report may not be reproduced except inPdgeltlqt41:Pgen permission from Rogers & Calicoll. Inc.
Page 2 of 7 I

Rogers & Callcott
ENVIRONMENTAL
ETT Environmental
PO Box 16414
Greenville. SC 29606-7414
Project: Wastewater
Work Order: 5040627
Reported: 04/23/15 13:36
Sample Number
Sample Description
Parameter
Total Metals
Copper
Zinc
Sample Data
5040627-01
44986 collected on 03/20/15 10:30
Reporting
Result Limit Units DF Analyzed Method
ND 0.005 mg/L 1.00 04/21 15 14:32 EPA 200.7
0.051 0.010 mg/L 1.00 04;21 15 14:32 EPA'_( 7
Flag Analyst Batch
MLR B5D0574
MLR B5D0574
PC) Bov 5655 Creem�dle, SC 296C6 426 I a•rf„r;at t_,r cc villa. >i= 29607
rogersandcallcott.com
04/23.201S 13:36 This report may not he repiv 1uced except inF geuh1rmttp2,n pemnsstoon from Rogers & ('uncoil, Inc.
Page 3 of 7

a Rogers & Callcott
F �YIRONMLwrAl
ETT Environmental Project: Wastewater
PO Box 16414 Work Order: 5040627
Greenville, SC 29606-7414 Reported: 04,23 15 13:36
Parameter
EPA 200.7 Metal Digestion
EPA 200.7
Sample Preparation Data
Batch Sample ID
Prepared
Analyst
B5D0574 5040627-01 04/16/2015 08:08 MLR
rogersandcailcott.com
04/23,2015 13:36 This report may not be reproduced ercep: inPiiiyeitfigIofiggen permission from Rogers & Collcoii, Inc.
I Page4of7 I

Rogers &Callcott
ENVIRONMEN IAL
ETT Environmental
PO Box 16414
Greenville, SC 29606-7414
Project: Wastewater
Work Order: 5040627
Reported: 04/23/15 13:36
Data Qualifiers and Definitions
ND Analyte NOT DETEL 1 l:,D at or above the reporting limit
NR Not reported
PO B,,. 5655 Green :1i, ! !_ 1`'0 .12a r.t ,•.I L'..,;,
rogersandcallcott.com
04/23/2015 13:36 This report may not be reproduced except in pdgeiftutftlitgen percussion from Rogers & Collcoll, Inc.
Page 5 of 7

ETT
environmental
PO Box .6414, ;xeenv1le, SC 29806-741e
[phone]. [phone] Fax .[phone]
Shipping Address: 4 Craflumen Ct. Geer SC 2985E
W W W.rTTCr, WWI 0NV 0.0.111..0 OM
Client:
CHAIN OF CUSTODY RECORD
«Oktoz/1
IPage __L_ of __L_ I
Facility:
State: \'PULS
SAMPLE ID
0
Special instructions'
Program
Containers
Campos:te onh
Conpnl:r Senn ❑nc
Time
(Crab n.t' c;«et
Simple Calleenw our
Time
Sign, and Print below
he Coned line
Collected b�
0
C
i • U
P resenva t ivc
Parame ers
'-IR504
2• NCI.
;.1n.03
.1 Sa0H
5.7Mc
5. Odw
Acute
Wkole Entail To•IcIty
Otranto
Test Orga alum
G
c
0-
.0
U
t1
0
tr
L
Chomica: Analysis & Cthe•
C fz,i
�UL
Sample ('ustody Transfer Record
Date
Time Relinquished By : ttganization
4��s�1s i CC
n
0
eu
a1POSJTE SAMPLING PROCEDURES
nposnc samples must be collected over a 24 hour period.
e Proportional: 1 sample each hour for e4 hours. Equal volut
I minimum 1 sample even• 4 hours over 2J hours.
t• Proportional As per instructions in NPDES permit.
Recc'vcd By - Orstanlz3t:m
TEa1PERATG•'RL' .4JUAY'1'ORJNG PROCEDURES
Sample temperature during collection and transpor must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ize in sealed bags.
.HOLD TL(EPROCF,D!:RES
Sett Ire
Area
Receip: Sample
Temp °C Preserved''
For tnvicir testing the sample must first be used t.i:hin 36 hours
of sample collection (complcenn nfenniposi.e sample).
Sample may net be used after 72 Ilona ±Tom sample collection.
1

Rogers &Caltcott
pr
ENVIRONMENTAL
Client:
Carrier Name:
Sample Receipt Verification
Date Work 0(il
U
Order:
Received: 1(1
FedEx UPS US Mail Courier Field Services Other:
Tracking Number:
Receipt Criteria
Y
e
s,
o
A
Comments
I
Shippingcontainer / cooler intact?
Damaged Leaking
Other:
Custody seals intact?
COC included with samples?4
COC signed when relinquished and received?4
Sample bottles intact?
Damaged Leaking
Other:
Sample ID on COC agree with label on bottle(s)?
Date / time on COC agree with label on bottle(s)?
Number of bottles on COG agrees with number of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
Temp at recetpt recorded on COC
Samples cooled? Temp measured ► ith IR thermometer - SN 97050067
Ice Cold Packs
Dry Ice
None
Samples requiring pH preservation at proper pH?
Note Samples for metals analysis may be preserved upon receipt in the lub
Samples dechlorinated for parameters requiring chlorine removal at
the time of sam . le collection?
If in-house preservation used — record Lot #
HCL
H3PO4
H2SO4
HNO3
NaOH
Other
Comments:
Were non-conformance issues noted at sample receipt? Yes or
Non -Conformance issue other than noted above:
Revised July 2014
Completed by:_____
Page 22 of 22
Page 7 of 7

P.0, Box 1E414, Greenv Ile. 5C 29606
(£64) B77-6942 . FAX (B64) 877.6938
4 Craftsman Ccur,, Greer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Plant
NPDES #: NC0021253
Test Date: 13-Oct-15
Laboratory ID#: T45892
Test Reviewed and Approved By:
4/
1211T
Ai -
Robert W. Kelley, Ph.D. Farbad Rostampour
QA/QC Officer Laboratory Director
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
SCDHEC Certification #23104
NCDENR Certification # 022
Pace I of 6

Effluent Toxicity Report Form - Chronic Mysidopsis Pass/Fail
Facility: City of Havelock NPDES # NC0021253 Pipe#: 01
Laborat terming est. T nvironmental Inc, County: Craven
� Comments:
X
Signature of Operator in
X
Signature of Laboratory Supervisor
Data: 23-Oct-15
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving 0
Original 0
Weight (per Original)
Fecundity (gravid/total females
Treatment 2 Replicates
Survtving 0
Original 0
Weight (per Original)
Fecundity (gravid/total females
Water Quality Data
Control
pH Initial
pH Final
DO Initial
DO Final
Tamp Initial
Tamp Final
S&truty Initial
Treatment
pH Initial
pH Final
DO initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
CoUection Start Date
Grab
Composite (Duration)
Conductivity ({tmhoslcm)
Chlorine (mg/L)
Sample Temp. at Receipt
2
2
5 5
4
-
3
V
4
o
4
r
4
a
4
5 5
4
3
4
5
.4
4
0.00097 0.00115
1 0/1 1n
0.00075
.-.
0.00057
0.00104
0.00077
0.00121
0.00115
010
2
1/1
0/2
1/1
0/1
5
3
5
5
'
5
5
a
2
r
4
8
g
4
5
5
5
5
3
4
5
0.00079
1 1/2
0.00110
1Ct
0.00114
nn
0.00110
0.00104
_�
0.00074
___
0.00094
0.00113
112
Day
- a 0 7
8.5
8.3
8.1
82
8.2
8.3
8.3
8.0
7.8
7.9
7.7
7.8
7.9
8.0
6.5
7.0
6.4
6.6
5.7
7.1
6.8
5.8
4.1
4.7
4.3
4.7
5.0
5.3
25.4
25.3
25.5
25.6
25.4
25.5
25.3
25.8
25.9
26.0
26.0
25.8
25.7
25.9
24.9
25.1
25.3
25.2
25.5
25.9
25.8
0
_ - . 0 7
8.7
8.3
8.3
8.3
82
8.3
8.3
8.1
7.0
7.9
7.8
7.9
8.0
8.1
6.5
6.9
6.1
6.4
6.9
7.1
8.9
5.1
4.9
3.8
4.8
4.6
5.1
5.5
25.0
25.5
25.4
25.6
25.5
25.4
25.4
25.8
25.9
26.0
28.0
25.a
25.7
25.9
24.9
24.8
28.5
28.5
25.1
25.1
25.1
2
10111/15
10/13/15
10/15/15
24 hours
24 hours
24 hours
689
694
722
<0.05
0.06
40.05
0.0
0.0
2.8
not frozen not frozen
Test Data: 10/13/15
Effluent Teat Concentration: 15%
5 replicates wore set for each control teal replicate; where <5 aro shown the organisms wore lost during ronewel.
5 replicates wore set for each troatmont tort ropllcato; whore <5 are shown the organisms were lost during renewal.
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
I97.1% I
1 0226(
I94.4% I
[ 0.2221
Avg Fecundity. 35.7%
Avg Fecundity: 44.3%
Test Results
Significant Mortality?
Yes No
I I X I
Chock Ono
Cato. t
Tabular t
Fecundity
Growth
0.159
1.94
Cale. t
Tabular t
NA•
1.77
contrd fecundity leas than 50%
PASS FAIL
I X 1
Chad( Ono
DWQ Form AT4(6/99)
Page 2 of 6
Page 2 of 6

l
rep
Day 1
bead Lost
Day 2
Dead Lost
Day 3
Dead Lost
Day 4
bead Lost
Day 5
Deed Lost
Day 6
Dead Lost
Day 7
Dead Lost
eight
mg
Fecundity
I N-Grav Gravid
(source
Su Mini
control
k'illb
A
0
0
0
0
0
00
0
0
0
0
0
0
0
0.97
1
0
5
B
0
0
0
0
0
0
0,
0
0
0
0
0
0
0
1.15
1
1
5
C
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0.75
2
0
4
D
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0.57
0
0
3
E
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1.04
0
1
4
F
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0.77
2
0
4
G
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1.21
0
1
4
H
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1.15
1
0
4
15
A
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0.79
1
1
3
B
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.1
2
1
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.14
2
0
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.1
2
1
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.04
0
0
5
F
0
0
0
0
0
0
1
1
0
1
0
0
0
0
0.74
0
1
2
G
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0.94
1
1
4
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.13
0
0
5
0
A
_
0
B
0
C
0
D
0
E
0
F
0
G
0
H
...
0
0
A
_
0
B
0
c
0
D
0
E
0
F
0
G
0
H
0
0
%
A
0
B
0
c
0
D
0
E
0
F
0
G
0
H
-
0
A
r
0
B
0
C
0
0
0
E
0
F
0
G
0
H
0
J
0
renew
JC
I JC
JC
1 AM
I JC
AM
End Date
fed
JC
JC
JC
AM
JC
AN
I 20-Oct-15
Mee tsd $ anew
04:40 PM
02:00 PM
03:00 PM
10:32 AM
10:25 AM
C5:57 AM
25.91
02:10 PM
I I PH
New lamp. C
25.5
25.4
25.6
25.5
25.4
25.4
Old Weep . •c
25.8
25.9
26
26
25.8
25.7
flaiN
Lob,
T45892
Client
HAVELOCK
Ssmp1.10
WWTP
NPDESI
0
County
0
Month
10
start a td Dot.
13-Oct-15
Start & tad Tim.
1428
Started a t.d By
JC
Tut Orpsntsm
Amerlcamysis bahia
N.o. bom ditto
7 DAYS
N.o. bom tim.
ABS HATCH 6-OCT-
Tsst Type
NCCPF
Motion Water
CRYSTAL SEA
Cutts for Conc.
%
%3rd BROOD
Test vessels
400 ml
Test volume
150 ml
Incubators
1
Light
161U8dk
tnttlsl Temp •C
25
Artemis
750
Tut method
EPA 021.R-02-013.1007
Comments
AU reps have 10
organisms unless noted otherwise.
.CON TEMP:
INITAL -
DAY 1-
DAY 2 -
DAY 3 -
DAY 4-
DAY 5-
DAY 6-
25.4
25.3
25.5
25.6
25.4
25.5
25.3
Pate 3 of 6

� `
lb
�`•
Sample Custody Transfer Record
Date Time Relinquished By / Organization Received By / Organization
cn
0
f
7
�,
"*Y
rri
IState:41 . NPDES m: /PC 00aAa33 --
w
a
w
0
(G) Grab (C) Composite
;
-((DAA
vl
„k
I
�
(0ON
11
N
O
v'1
(Composite only)
Composite Stan Date' Time
n
R
tg
co
1
O
p'
V
w
(Grab or Composite)
Sample Collection Dotei Time
II1
2
3�
Sign, and Print below
the dotted line
Collected by
•`
Cicnn Water Act
Storni watcr
'V
o
Sediment
as
v
Non-Regulutaty
a
11 of Containers
•
Plastic
o
1ir,
'P
_
1
�{y
,, I
+t`
Gloss
li
44.
Volume
a
\
lee
s ,, g '
&
ri
Acute Pass/Pail
r
Acute Mldti-Cone.
S
rChronic Pass/Fail
`?
Chronic IYllllli-Cone.
a
7
o
n
C. (labia.
N
D. nmbigua
H
Fathead Minnow
.
a
Mysicl Shrimp
-O
Nn.
Silverside
1 lyallcla
3•
no
Chirununms
m
'1'1 L!I'lil
e
WI.;R
3
MncroitiVG'Iebrate ID
i V RI
(1
��
Chemical Analysis & Other
c
C.)A
n
C
(7 �.
b
I w
42
CA
CIO
Ell' ASSI(iNIsD L,AI3 ID 11

CHAIN u CUSTODY RECORD
PO Box 16414, Greenville, SC 29806-7414
[phone], [phone] Fax[phone]
Shipping Address: 4 Craflsman Ct, Greer, SC 29650
WWW.ETrIENVIRONMWTAL.COM
fPa=e of—
Client: (1��•
I OCk
Program
Containers
Preservative
Parameters
Facility: 4
21O,ril-
LCIcan Water Act
Stormwater
I Non -Regulatory _
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volur
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 *C. Samples must not be frozen. Use water ice in sealed bass.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ETT
PO Box 16414. Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
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W N W.ETTCNVI RCNMCNTAL.COM
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Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal voluleveryor at minimum 1 sample eve4 hours over 24 hours.
Flow Proportional -der instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used ithin 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

EIT. (E84) 877.6942 . FAX [phone]
PO. Bax 1 E414, Greene Ile. SC 29605 4 Craftsman Court. Greer. SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Plant
NPDES #: NC0021253
Test Date: 12-Jan-16
Laboratory ID#: T46334
Test Reviewed and Approved By:
Robert W. Kelley, Ph.D.
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. included results pertain only to provided samples.
•
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022
Page 1 of 6

Effluent Toxicity Report Form - Chronic Mysidopsis Pass/Fail Date: 21-Jan-16
Facility: City of Havelock NPDES # NC0021253 Pipe#:
Laborato P-.. •••'• • - ■ n u -nt
Comments:
County: Craven
Signature of Operator i pontsib rge
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving 0
Original sly
Weight (per Original)
1
2
3
4
5
6
7
4
4
5
5
5
5
4
4
5
4
5
5
5
5
5
4
0.00097
0.00115
0.00075
0.00057
0.00104
0.00077
0.00121
0.00115
Fecundity (gravid/total females;
Treatment 2 Replicates
Surviving aY
Original 0
Weight (per Original)
1/2
1
010
2
1/3
3
0/1
4
1/3
0/1
0/0
0/1
4
4
4
4
4
5
5
3
5
5
5
5
4
5
5
5
0.00111
0.00089
0.00083
0.00075
0.00090
0.00093
0.00128
0.00073
Fecundity (gravid/total females;
Water Quality Data
Control
pH Initial
pH Final
00 Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Start Date
Grab
Composite (Duration)
Conductivity (Nrnhos/crn)
Chlorine (mg/L)
Sample Temp. at Receipt
0/1
1/1
0/0
1/3
Day
0/2
0/4
0/2
0/1
0
1
2
7
8.4
8.3
8.3
8.2
8.3
8.3
8.2
7.9
8.0
7.8
7.9
8.0
8.0
8.3
7.0
6.1
7.1
6.2
6.6
6.5
6.4
5.2
6.1
5.0
5.0
5.0
5.4
5.7
25.4
25.6
25.2
25.3
25.0
25.4
25.6
25.7
26.1
25.8
25.7
25.8
28.1
25.9
25.3
25.7
25.5
24.9
25.0
24.8
25.3
0
1
- - v r
8.4
8.3
8.3
8.2
8.3
8.3
8.2
8.0
8.1
7.8
8.0
8.2
8.0
8.3
7.2
6.7
7.1
6.2
6.6
6.3
6.5
5.1
5.4
4.7
4.4
5.0
4.7
5.4
25.0
25.3
25.6
25.3
25.0
25.2
25.6
25.7
28.1
25.8
25.7
25.8
26.1
25.9
25.2
24.8
24.6
25.2
26.7
26.3
25.7
1
2
1-10-16
1-12-16
1-14-16
24 hours
24 hours
24 hours
781
766
795
<0.05
<0.05
<0.05
1.2
0.0
2.4
partially
frozen
Test Date: 01/12/16
Effluent Test Concentration: 15%
5 replicates were set for each control test replicate; where <5 are shown the organisms were lost during renewal.
5 replicates were set for each treatment test replicate; where <5 are shown the organisms were lost during renewal.
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
94.7%
0.205
84.6%
0.191
Avg. Fecundity: 27.3%
Avg. Fecundity: 14.3%
Test Results
Significant Mortality?
Yes No
t 1
x
Check One
Growth
Calc. t
Tabular 1
Fecundity
Rank Sum
Crit. Value
0.51
1.94
•
•
PASS FAIL
1 x I
Check One
'Control fecundity <50%; not used as endpoint
DWQ Form AT-4 (6/99)
Page 2 of 6

lb Day
1
Lost
Day 2
L oed Losteed
Day 3 IDay 4
iLost ead Lost
Day 5 L Day6r Day 7
pond Lost oad Lost boad Lost
/Weight Fecundity
mg J N-Grav Gravd
SOurce
rep
and
Survival
control
f\
A
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0.6
1
1
4
B
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0.91
0
0
4
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.2
2
1
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.04
1
0
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.18
2
1
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.02
1
0
5
G
0
0
0
0
1
0-
0
0
0
0
0
0
0
0
0.86
0
0
4
H
0
0
0
0
0
0
0
0
0
0
000
0
11
1.02
1
0
4
15
A
0
0
1
00
0
0
0
0
0
0
0
0
0
1.11
1
0
4
B
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0.89
0
1
4
C
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0.83
0
0
4
D
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0.75
2
1
4
E
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0.9
2
0
4
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0.93
4
0
5
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.28
2
0
5
H
_ 0
0
0
0_
1
0
0
0
0
0
1
0
0
0
0.73
1
0
3,
O
A
-
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
O
A
-
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
O
A
-
-
-
0
B
0
c
0
0
0
E
0
F
0
G
0
•��
H
0
A
0
-
B
0
C
0
0
0
0
E
0
F
0
G
0
H
0
J
MD.. I
4
AN
Jq
N
AN
FJ 1
End Date
ad
4
AN
df
N
AN
FJ
I
19-Jan-16
Cum led a more
02.55 PM
02.11 PM
02.43 PM
03.20 PM
12.22 PM
03.34 PM
04.12 PY 1 ) AN
N.. tenn. •c
25.3
25.6
25.3
25.0
25.2
25.6
Old temp •c
25.7
26.1
25.8
25.7
25.8
26.1
25.9 I
Labs
T46334
Client
HAVELOCK
Sample ID
EFFLUENT
NPOES/
NC
County
0
Month
1
Start & red Date
12-Jan-16
Start & red Ttms
1600
Started & tad By
RH
Test organism
Americamysis bahia
Neo. bom date
7 DAY
Neo. born time
ABS HATCH 1-5-16
Test Type
NCCPF
Dilution water
INSTANT OCEAN
Untie tor Conc.
%
%3rd BROOD
Test vessels
400 mi
Test volume
150 mi
Incubator 0
1
Light
161U8dk
Initial Temp •C
25
Artemis
750
Test method
EPA 521.0.02413 1007
Comments
All reps have 5
organisms unless noted otherwise.
CON TEMP:
INITIAL- 25.4
DAY 1 - 25.6
DAY 2- 25.2
DAY 3 - 25.3
DAY 4 25
DAY 5- 25.4
DAY 6 25.6
Page 3 of 6

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WW W-CTT[NVIAONMCNTAL.COM
CHAIN k,I, CUSTODY RECORD
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Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ET,'
PO Box 16414, Greenville, SC 29808-7414
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
WW W.CTTENVIRONHCNTALCOM
CHAIN ut+i CUSTODY RECORD
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between
Time Proportional: 1 sample each hour for 24 hours. Equal volut 0.0 and 6.0 *C. Samples must not be frozen. Use water ice in sealed bags.
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional- Der instructions in NPDES permit.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

i► trn , Ine.
(E84) B77.8 i42 . FAX [phone]E
P O. Box 1 E414. Greenv Ile. SC 29606
4 Craftsman Court. Greer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES #: NC0021253
Test Date:
Laboratory 1D#: T46884
Test Reviewed and Approved By;
Robert W. Kelley, Ph.D.
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Numbcr E87819
Honda Dept. of Health. Included results pertain only to provided samples
19-Apr-16
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022
Page 1 of 6

Effluent Toxicity Report Form - Chronic Mysidopsis Pass/Fail Date: 29-Apr-16
Facility: City of Havelock WWTP NPDES #Mc QDa 1.15&Pipe#: 004, County: Craven
Labor ertormingjTe(EYI Environmental Inc. Comments:
x yy�j
Signature of Opera
X
Signature of Laboratory Supervisor
Res
large
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving 8
Original 8
Weight (per Original)
1
2
3
4
5
6
7
8
5
5
4
4
5
4
4
5
5
5
4
5
5
4
5
5
0 00156
0.00179
0.00135
0.00149
0 00202
0 00151
0.00172
0.00183
Fecundity (gravid/total females, 1/1
Treatment 2 Replicates
Surviving tt
Original if
Weight (per Original)
Fecundity (gravid/total females:
Water Quality Data
Control
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlonne (mg/L)
Sample Temp. at Receipt
1
0/2
2
0/1
3
2/2
4
1/2
5
1/3
6
0/0
7
2/2
6
5
5
4
5
5
5
5
5
5
5
5
5
5
5
5
5
0.00219
0.00215
0.00181
0.00225
0.00228
0.00182
0.00162
0.00205
3/3
1/2
1/1
1/1
Day
1/1
0/0
1/3
2/2
0
1
2
3
4
5
6
8.1
8.0
8.3
8.0
8.1
8 0
8.3
7.8
7.7
7.6
7.6
7.7
7.8
7.7
7.5
6.7
6.4
6.6
7.4
73
67
5.7
4.5
5.3
5.0
5.2
5.0
5.4
25.2
25 3
25.4
25.1
25.3
25.3
25.3
25 8
26 0
25.7
25.8
26.0
26.0
26.0
24.5
24 7
24.9
24.9
25.1
25.0
24.6
0
1
2
3
4
5
6
7
82
80
B3
8.0
8.1
8.2
83
7.9
7.9
7.9
7.9
7.6
7.9
7.9
7.4
6 6
6.4
6.7
7.5
7.1
6.5
54
41
5.5
4.9
53
4.0
4.7
25.0
25 3
25.5
25.2
25.3
25 4
25.6
25.8
26.0
25.7
25.8
26.0
26.0
26.0
24 4
24.5
25.0
25.0
24.6
24.8
24.7
1
2
3
17-Apr-16
19-Apr-16
21-Apr-16
x
x
x
738
758
777
0.06
<0.05
<0.05
0.1
0.2
0.9
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
94 7%
1.66
97.5%
2.02
Avg Fecundity 53.8%
Avg. Fecundity. 76.9%
Test Results
Signficant Mortality?
Yes No
X
Check One
Growth
Calc t
Tabular 1
Fecundity
Rank Sum
Crit Value
-2.60
1.94
PASS
FAIL
X
Check One
Test Date. 02/09/16
Effluent Test Concentration. 3%
5 replicates were set for each control test replicate; where <5 are shown the organisms were lost dunng renewal.
5 replicates were set for each treatment test replicate, wfiere <5 are shown Me organisms were lost dunng renewal.
DWO Form AT-4 (6/99)
Page 2 of 6

Day 1
Dead Lost
Day 2
Dead Lost
Day 3
Dead Lost
Day 4
Dead Lost
Day 5
Dead Lost
Day 8
Dead Lost
Day 7
Dead Lost
Weight
mg
Fecundity
N-Grav Gravld
'source
rep
Survival
c \I
f�
A
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.56
0
1
5
B
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.79
2
0
5
C
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1.35
1
0
4
D
0
0
1
0
0
0
0
0
0
0,
0
0
0
0
1.49
0
2
4
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.02
1
1
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1.51
2
1
4
G
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1.72
0
0
4
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.83
0
2
5
15
A
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.19
0
3
B
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.15,
1
1
5
C
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1.81
0
1
4
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.25
0
1
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.28
0
1
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.82
0
0
5
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.82
2
1
5
H
0
0
0
0
0
0
0
0
0
0
0
0_
0
0
2.05
0
2
5
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
_
_
0
r-�
0
0
A
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
c
0
D
0
E
0
F
0
G
0
H
0
O
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
J
0
W..FI
JG
AN
AN
AN
,14
End Date
a.
N
4
AN
AN
AN
dG
I 26-Apr-16
toss.&,....
11:47AM
02,27PM
11,03AM
11'.20AM
1147AM
01 22 PM
0247PM I 1 AN
N.. limp •c
25.3
25.5
25.2
25.3
25.4
25.6
om 1.a,p •c
25.8
26
25.7
25.8
26
26
261
Lab•
T46884
Client
HAVELOCK
ssmpte CD
EFFLUENT
NPDEss
NC
County
0
Month
4
start a ted Date
19-Apr-16
Start & tad Time
1500
Started & fed By
AM
Test Organism
Amertcamysts bahia
Nee. bom date
7 DAY
Nee. bom time
ARO HATCH 4-12-1;
Test Type
NCCPF
Dilution water
INSTANT OCEAN
Units for Conc.
%
%3rd BROOD
Test vessels
400 ml
Test volume
150 ml
incubators
1
Light
16IU8dk
intttsITemp 'C
25
Artemis
750
Test method
EPA 0214R4024314 1007
Comments
All reps have 5
organisms unless noted otherwise.
CON TEMP:
INITIAL- 25.2
DAY 1- 25.3
DAY 2 - 25.4
DAY 3- 25.1
DAY 4- 25.3
DAY 5- 25.3
DAY 6 - 25.3
Page 3 of 6

CHAIN uF CUSTODY RECORD
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
W WW.ETT ENV!R OHM ENT AL.COM
Page of
Client:
r7 </e= �c.+ �/
`�?
Program
Containers
Preservative
Parameters
Facility:,t l J , ,� L y
(mot-)6,56 ) �ef 7—r 7mP/I/" 7747
C1cnn Wnlcr AO
Slornlwatcr
Scdimcnl
Non -Regulatory -
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State: y( NPDES #: tie09, Jr q
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Chronic
Test organisms
SAMPLE ID
(C) Crab (C) Composite
(Composite only)
Composite Stan Date
Time
(Grab or Composite)
Semple Collection Dote
Time
Sion, and Print below
the dotted line
Collected by
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Special Instructions:
Sample Custody Transfer Record
Date Time Relinquished By / Organization Received By / Organization
Secure
Area
Receipt
Temp °C
Sample
Preserved?
11911(D
Ogg
«.ps
i, �Tr
O. t
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: I sample each hour for 24 hours. Equal volui
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional \per instructions in NPDES permit
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
1
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.
1

ETJ'
PO Box 16414. Greenvale, SC 29808-7414
[phone], [phone] Fax[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
WWW.ETTCNVIRONM ENTALCOM
CHAIN or, CUSTODY RECORD
'Page
of
Client: //
/4• VCC,/Cr K
Program
Containers
Preservative
Parameters
Facility: )CS�F(A Joffe. ,/,� fe,"/ li
_�/n7 ���
'Clain Water Act 1
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6-Odter
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Macroinverlebrn(c ID ---
Chemical Analysis & Other
li I"I' ASSIGNED1.Al3 ID II
State: t� NPDES #: �i� �d/ 3
Acu Le
Chronic
Tat Organisms
SAMPLE ID
(G) Grub (C) Composite l
(Composite only)
Composite Sum Date
TimeSempk
(Grab or Composite)
Collection Dote
Time
Sign, and Print below
the dotted line
by
Acute Pass/Foil
Acute Multi-Conc.
Chronic Pass/Fail
xi
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Special Instructions: , —� ' Am.—,_ < e
Sample Custody Transfer Record
Date Time Relinquished By / Organization Received B1' / Organization
Secure
Area
Receipt
Temp `C
Sample
Preserved?
«0 C
Ipys
�— 7``= ,ie/r/'
(If R) 1(0
(230
UPS
4 ,,,,- ;. 'p, vo ETr
1 0.
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volur
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit_
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ET''
PO Box 18414, Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
www.CTrCNVt RONM tftAL.COM
Client:
CHAIN Vr, CUSTODY RECORD
Page t/ of�_
Pro ram 1 Containers IPrccen•ari •
Facility: Lt%l/Pc- Are77--,e4X T7/,1A
Clean Water Act
IStormwatcr
E
cC7i�
Non -Regulatory _ I
1fl of Containers
o
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Whole Effluent Toxicity
^
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State: /YC
I(G) Cott] (C) CongmxIlc
NPDES #: /V 'c7 �/, ,53
Acute
Chronic
Test Organisms
SAMPLE ID
(Composite only)
Composite Start Date
Time
(Grab or Composite)
Sample Collection Date
Time
Sign, and Print below
the dotted line
Collected by
Acute Pass/Fail
Acute Multi-Conc. I
_
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=
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L.
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✓
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✓
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G. C
8g�c
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Special Instructions:
-
Sample Custody Transfer Record
Date Time Reli d B / Ora. ization Received By / Organization
Secure
Area
Receipt
Temp =C
Sample
Preserved?
ta. .t
/ j , ^,' I e , f q- (-'
Fb!C WW 1 P
L
t 2
o
PS
-
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: I sample each hour for 24 hours. Equal volur
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As r instructions in NPDES pemtiL
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bass.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

env ninmenta , Inc.
(E64) 877.6942 . FAk [phone]
P O. Box 1 E414 Greenv Ile. SC 29606
4 Craftsman Court. Greer. SC 29650
Americamvsis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES #: NC002 1253
Test Date:
Laboratory ID#: T47373
'Lest Reviewed and Approved By:
Aitd 4/
19Jul-16
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC Officer Laboratory Director
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples
SCDHEC Certification #23104
NCDENR certification # 022
Page 1 of 6

Effluent Toxicity Report Form - Chronic Mvsidopsis Pass/Fail
Date:
Facility: City of Havelock WWTP NPDES # Pipe#: County: Craven l
Laborato :� T Environmental Inc.
X .,4�-
Comments:
Signature of Operator in R sponsible Charge ,
x , /, - i,
Signature of Laboratory Supervisor -
AIL UKIU VAL CU: t:nvlronmental Sciences Branc
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving a
Original a
Weight (per Original)
Fecundity (gravid/total females
Treatment 2 Replicates
Surviving a
Original 8
Weight (per Original)
Fecundity (grevidfotal females
Water Quality Data
Control
pH Initial
pH Final
D0 initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Start Dale
Grab
Composite (Duration)
Conductivity (pmhos/om)
Chlorine (mg/L)
Sample Temp at Receipt
2
3
4
5
6
7
8
5
4
3
5
5
3
5
3
5
4
3
5
5
3
5
4
0.342
0.473
0.393
0.442
0.398
0.373
0.222
0.148
112
2/2
2
1/1
3
2)2
4
1/2
5
111
6
112
7
1/2
8
4
4
3
4
4
5
3
1
4
5
4
5
5
5
4
2
0.255
0.272
0.238
0.370
0.334
0.448
0.318
0.230
1/1
111
2f3
1/1
Day
2/3
2/2
Oro
1/1
0
2
3
4
5
8.0
8 1
8.2
8.2
8.2
8.3
8.3
7.9
8.3
7.8
8.1
79
79
82
7.4
68
6.6
65
6.6
7.3
77
5 3
5.4
4.7
5.2
5.1
5.7
5.5
25.4
25.6
25.3
25 7
25.4
25.5
25.7
26.1
25.9
25.9
26.0
26.1
25.9
25.9
25.5
25.7
26.0
26.5
26 4
26 6
27.0
0
2
3
4
5
6
7
8.0
8.2
8.2
8.2
8.2
8.2
8.3
8.0
7.9
7.9
8.0
8 1
8.1
8.2
7.5
6.7
6.7
6.7
6.6
7.3
7.7
56
44
47
5.2
5.2
5.7
6.2
25 0
25.7
25.3
25.7
25.4
25.5
25.5
26.1
25.9
25.9
26.0
26.1
25.9
25.9
25.7
25.6
26.3
26.3
24.6
25.5
25.1
1
2
3
17-Jul-16
19-Jul•16
21-Jul-16
x
x
x
723
733
660
<0.05
<0 05
<0 05
0.2
0.2
0.3
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
97.1%
0.349
82 4%
0.308
Avg Fecundity. 75. 0%
Avg. Fecundity. 90.6%
Test Results
Significant Mortality?
Yes No
X
Check One
Growth
Calc t
Tabular I
Fecundity
Rank Sum
Cnt. Value
0.86
1 94
PASS
66
51
FAI L
X
Cheek One
Test Dale: 07/19/113
Effluent Test Concentration. 15%
5 replicates were set for each control test replicate: where <5 are shown the organisms were lost dunng renewal
5 replicates were set for each treatment test replicate: where <5 are shown the organisers were lost dunng renewal.
DWQ Forrn AT-4 (6/99)
Page 2 of 6

Day 1
(Joao Lost
Day 2
Deed Losl
Day 3
Dena Lost
Day 4
deed Lost
Day 5
❑earl Lost
Day 6
Deem Lost
Day 7
Deea Lost
Weight
mg
Fecundtty
N-Grer Grey a
source
rep
Survival
1
ntrol
A
0
0
C
0
0
0
0
0
0
0
0
0
0
0
1.71
1
1
5
B
0
0
C
0
0
0
0
0
0
0
0
0
0
1
1.89
0
2
4
C
0
0
0
1
0
0
0
0
0
1
0
0
0
0
1 18
0
1
3
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.21
0
2
5
E
0
0
C
0
0
0
0
0
0
0
0
0
0
0
199
1
1
5
F
0
0
0
1
0
0
0
0
0
0
0
0
0
1
1 12
0
1
3
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1 11
1
1
5
H
0
0
1
0
0
0
0
0
0
0
0
0
0
0.59
_ 1
1
3
15
A
0
0
0
0
0
0
0
0
0
0
0
0
0
1 02
0
4
B
CCU
0
0
0
1
0
0
C
0
0
0
0
1.36
0
4
C
0
0
1
1
0
0
0
0
0
0
0
0
0
0
095
1
2
3
D
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1.85
0
4
E
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1.67
1
2
4
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.24
0
2
5
G
0
0
1
1
0
0
0
0
0
0
0
0
0
0
127
0
0
3
H
0
0
0
2
0
0
0
0
1
0
0
0
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0
1
1
0
A
0
8
0
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0
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I 26-Jul-16
ur.l..ar.r..
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0,3 Au
C353 PH
25.91
0333PH AM
R.. Irmo •C
25.7
25.3
25.7
25.4
25.5
25.5
Cc 'Imp •c
26. 1
25.9
25.9
26
26. 1
25.9
Lab/
747373
Client
HAVELOCK WWTP
Semple 10
EFFLUENT
NPOES/
0
County
0
Monlh
7
Start a fed Date
19-Jul-16
SIGH 8 fed Time
1515
Started d fed By
JG
Tot Organtem
Amencays;s bania
Neo. born Data
7 DAYS
Neo. born ❑mo
ARO HATCH 12-JUL
Test Type
SCCPF
Dilution Water
INSTANT OCEAN
Una.lor Conc.
%
103ro BROOD
Teat v.aa0l.
400 mi
te.t volume
150 ml
Incubator /
1
Llghl
16198DIc
Initial Temp •C
25
Alum 1.
750
7..1 molhod
EPA e31 R 02.01a 1007
Comments
All reps hevc 5
organisms unless note0 Otherwise
CON TEMP
INITIAL 25 4
DAY 1- 25.6
DAY 2- 25 3
DAY3- 257
DAY 4 25.4
DAY 5- 25.5
DAY 6 - 25.7
Page 3 of 6

Erg
PO Box 18414, Grammies, SC 29806.7414
[phone] [phone] Fa c(884) 677 8938
Shipping Address: 4 Craftsman Ct. Greer, SC 29650
W W W.[TTCNVI gONM[NTAL.0 CM
CIIAIN OF CUSTODY RECORD
Pasc f ofJ
Client: /
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Program
Containers
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Time
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Sample Calkstte. Date
Time
Sign, and Print below
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Sample Custody Transfer Record
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7/4
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volur
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit
TEA PER4TURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 'C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIAIE PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

)
ET
1
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Falc(864) 877 8938
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
www.ETTENVI no NM ENTAI.CON
CHAIN uF CUSTODY RECORD
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SAMPLE ID
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 (lour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volue
or at minimum 1 sample every 4 hours over 24 hours.
now Proportional: As oer instructions in NPDES permit.
TEA{PERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

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PO Box 16414, Greenvile. SC 29606-7414
[phone], [phone] Fax[phone]
Shipping Address: 4 Craftsman CL Greer. SC 29650
WW W.CTTCN VI RONN tlT4L.COM
CHAIN OF CUSTODY RECORD
Page / of_/_
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Facility �� /jam /� '� 1 -/r y� { t
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Cumposhesun Date
Time
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Time
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volui
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use eater ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

EIT.
P.O. BOX 1E414, GreenvIle, SC 29606
(E64) 877-6942 . FAN [phone]
4 Craftsman Court, Greer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES #: NC0021253
Test Date: 11-Oct-16
Laboratory 1D#: T47853
Test Reviewed and Approved By:
Robert W. Kelley, Ph.D
QA/QC Officer
Certification #E87819
Test results presented in this rcpon conform to all requirements of
NELAC. conducted under NELAC Certification Number E87819
Honda Dept of Health. Included results pertain only to provided samples
Farhad Rostampour
Laboratory Director
SCDH EC Certification #23104
NCDENR Certification # 022
Page 1 of 6

Effluent Toxicity Report Form -
bait. 11-Vt:t-JO
Facili : CITY OF HAVELOCK NPDES # NC0021253 Pi•e#: 001 Count : Craven
Laboratory Pe • • ,. fo SETT `r.•,Ironmental Inc.
Comments:
Signature of Operator in Responsible Charge .
X --/ / l'
Signature of Laboratory Supervisor
me A iv llnr/rnwi ♦ r m
r nvlronmentat sciences tiranc
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Sur ving #
Original #
Weight (per Original)
Fecundity (gravid/total females)
Treatment 2 Replicates
Surviving #
Original #
Weight (per Onginal)
Fecundity (gravid/total females)
Water Quality Data
Control
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Stan Date
Grab
Conposile (Duration)
Conductivity (prmoshxn)
Chlonne (mg/L)
Sample Temp at Receipt
2
3
4
4
5
5
5
5
4
5
4
4
5
5
5
5
4
5
0.5200
0.4775
0.3880
0.4940
0.3980
0.3820
0.5550
0.4420
1/2
2/2
2
3
212
4
3/4
2/3
2/2
313
4
5
5
5
3
5
4
4
4
5
5
5
4
5
5
4
0.4325
0.3740
0.3500
0.3580
0.5350
0.5520
0.3320
0.4725
2/2
112
Day
2/2
2/2
0/1
1/2
0
2
8.3
8.0
8.2
8.2
8.2
8 1
8.3
7.7
7.9
7.9
7.8
7 7
7.8
8 2
7 4
6.6
6 7
6.3
6.5
7.0
6.7
5.4
6.1
50
5.3
69
4.5
6.0
25.2
25 3
25.6
25.4
' 25.2
25.1
24.9
26.3
26.0
26.1
25.9
26 3
26.0
26.3
25.1
25.6
24.7
24.9
25.0
24.7
24.8
0
2
8.3
8 1
8.2
8.3
8.2
8 3
8.3
7.8
7.9
7.9
8.0
8.2
8.0
82
75
7.5
62
61
6.2
65
6.2
5.5
5.0
4.6
5.1
6.7
49
61
25.0
25.4
25.6
25.7
25.6
25.3
25.7
26.3
26.0
26 1
25.9
26 3
26.0
26 3
24.8
26.3
25.5
25.7
24.8
24.9
25.0
09-Oct-16
11.Oct-16
13-Oct• 16
24hr
24 fir
24 fir
405
445
445
<0.05
c0.05
<0.05
0.2
0.2
2.2
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
100.0%
0.457
94.6%
0.426
Avg. Fecundity. 86.5%
Avg Fecundity. 75.0%
Test Results
Significant Mortality?
Yes
No
X
Calc I
Tabular I
Calc t
Tabular t
PASS
Check One
G myth
0.82
1.76
Fecundity
0.36
1.76
FAIL
X
Check One
Test Dale.
Effiuent Test Concentration:
5 replicates were set for each control lest replicate, where <5 are shown the organisms were lost dunng renewE
5 replicates were sal for each treatment lest replicate, where <5 are shown the organisms were lost dunng rene
DWO Form AT-4 (6/99)
Page 2 of 6

Day
1
Lost
Day 2
Dead Lost
Day 3
Deno Loal
Day 4
Daac Lost
Day 5
Dead toot
Day 6
Dead Lost
Day 7
peed Lost
Weight
mg
Fecundity
tv.Grav Grev,c
Source
rep
Deed
Survival
1ntrol
A
0
0
0
0
0
0
0
0
0
1
0
0
0
0
2.08
1
1
4
8
0
0
0
0
0
0
0
C
0
0
0
1
0
0
1.91
0
2
4
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.94
0
1
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.47
0
2
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.99
1
3
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.91
2
5
G
0
C
0
0
0
0
0
0
0
0
0
0
0
222
0
2
4
H
0
0
L
C
0
0
0
0
0
0
0
0
0
0
221
0
3
5
O
A
0
a
0
C
0
D
0
E
0
F
0
G
0
H
0
O
A
0
E
0
C
0
D
0
E
0
F
0
G
0
H
0
O
A
0
8
0
c
0
D
0
E
0
F
0
G
0
H
0
A
8
0
C
0
D
0
E
0
F
0
G
0
H
0
A
0
0
0
0
0
C
0
0
C
0
0
0
0
1 73
C
4
8
0
C
0
0
0
0
0
0
0
0
0
0
0
0
1 87
0
2
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1 75
1
1
5
D
0
C
0
0
0
0
0
0
0
0
0
0
0
0
1 79
0
1
5
1 5
E
1
0
0
0
0
0
0
0
0
1
0
0
0
0
2.14
0
2
3
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.76
0
2
5
G
1
0
0
0
0
0
0
0
0
0
0
0
0
0
' 66
1
0
4
H
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1 89
1
1
4
lie...
FJ
JG
JG
JG
AM
JG
End Date
fec
FJ
JG
JG
..iG
AM
JG
Tr.t.c a fere.
044/P1e
..14.PN
0] ]t PM
1L.Y AN
01 e]PM
o.Oa PM
l
18-Oct-16
AM
Einerir... 1e,r0 ..
25.4
25.6
25.7
25 6
25.3
25.7
•. -. Pod
Cc IV., -C
26.3
26
26.1
25.9
26.3
26
26.31
co,,,,,,......,,,, -c
25.3
25.6
25.4
25.2
25. 1
24.9
Lab,
T47853
Client
CITY OF HAVELOCK
Semple 10
EFFLUENT
NPDESS
NC
County
0
Month
10
Start 8 fed D.te
11-Oct-16
St.rt & tod Time
12.00 PM
Started & fed By
AM
Te.t Organism
AmerIcantysls bailie
Neo born date
7
Nao born time
ARO HATCH 10-4-16
Teat Type
NCCPF
Dilution Water
CRYSTAL SEA
Units for Conc.
%
%Ste BROOD
Teal 1a
400 ml
Taal volume
150 ml
incubators
1
Light
1611/8dk
!nibs! lamp •c
25
Artemis
750
Teal method
EPA e21•R-01-014 I00/
Comments
All rcps bout 5
organisms unless noted Otherwise
Control mI temp
D=DeaC N/A -Lost or not used
Page 3 of 6

ET'i
PO Box 18414. Greenville, SC 296067414
[phone], [phone] Fa c(884) 877 6938
Shipping Address: 4 Craftsman Ct, Greer. SC 29650
www.crrtw+n wa wr+w-raL.con
CHAIN OF CUSTODY RECORD
Paae o`'
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Program
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Macnrinver(ebrnle ID
State:'jC NPDES #: {'.j" CO a / 3
acute
Chronic
Test Organisms
-
SAMPLE ID
I(C) Crnb (C) Cnmpnsite
(Composite only)
Composite Sian Date
Tima
(Grab or Composite)
Sample Collodion Date
Time
Sign, and Print below
the dotted line
Collected by_
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Date Time Relinquished By / Organization Received By / Organization
Secure
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Temp aC
Sample
Preserved?
10-id•ib
irk
o.1 bares rr-ty of oelocrA U )TP
)0114
9I5
-e-er- up
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES pemlit.
TEAFERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ET,'
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax[phone]
Slipping Address: 4 Craftsman Ct, Greer, SC 29650
W W W.<TT'MvlfON.sprrA4COM
CHAIN uF CUSTODY RECORD
fPase I of t
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�j
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Chronic
Tot Organisms
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a-
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Camp:mite Start Dote
Time
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S.mpkCotteni°n Moe
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Sample Custody Transfer Record
Date Time Relinquis ed By / Organization Received By / Organization
Secure
Area
Receipt
Temp 'C
Sample
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0-ce5/0-1A1 &Wale tat-N 03 U3-n°
1oi13)(Io
OP6
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be benveen
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ETr'
1
tn)r ae ap '
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax[phone]
Shipping Address: 4 Craftsman Ct. Greer. SC 29650
W WW.tcrrCMV Iwo Nr+cNTAL.con
CHAIN u.el CUSTODY RECORD
Page L of�
1..1Ienr: C , ,,,�
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Facility: AS fe Cd
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ASSI(iNI I) LA8 11)11
State- NC, NPDES #: ,/dy��,fer
O / ' 5 3
Acute Chronic
T
Test Organisms
SAMPLE ID
I(C) Crnb (C) Composlla
(Composite only)
c.v.:45tanDaa
Time
(Grab or Composite)
SompkCollection Date
The
Sign, and Print below
the dotted line
Collected by
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Date
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Time Relinquished By / Or ization Received By / Organization
Secure
Area
Receipt
Temp `C
Sample
Preserved?
WilllCo
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volur
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must firs be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ET.Inc.
P.O. Box 1 E414, Greenv Ile. SC 29605
(664) 877-8 2 . FA)( [phone]
4 Craftsman Court, Greer. SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES #; NC0021253
Test Date: 10-Jan-17
Laboratory ID #: T48371
Test Reviewed and Approved By:
4/
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC Officer Laboratory Director
Certification #E87819
Test results presented m this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
SCDHEC Certification#23104
NCDENR Certification # 022
Page 1 of 6

Date:
10-Jan-17
- Chronic Mysidopsis Pass/Fail
Facili : Havelock NPDES # NC0021253 Piee#: 001 Coun : Craven
Laboratory Performing Test: ETT Environmental Inc.
x �� f,i I��
Comments.
Signature of Operator in Re�paisible Charge
X /C�'� .' `I • /
Signature of Laboratory Supervisor•
TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving 8
Onginal 8
Weight (per Original)
Feamdlty (gravldltotal females)
Treatment 2 Replicates
Surviving 8
Onglnal N
Weight (per Original)
Fecundity (gravid/total females)
Water Quality Data
Control
pH Initial
pH Final
DO Initial
D0 Final
Temp Inroal
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/L)
Sample Tenp. at Receipt
2
3
4
5
6
7
5
5
4
5
5
5
5
5
5
5
4
5
5
5
5
5
0.246
0.214
0.225
0 274
0.360
0 298
0.276
0.350
2(3
t/3
2
0/0 2/2
3
4
2/2
5
2/3
6
7
3/4
8
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
0.398
0.280
0.248
0.362
0.240
0.338
0.330
0.330
1/1
2/4
2/2
1/2
Day
112
1/3
010
0
2
3
4
5
6
7
8.3
8.1
82
8.2
81
82
8.2
7.9
8 1
7.8
7.7
7.8
7.9
7.9
7.5
6.3
6.9
6.8
6.7
6.8
7 5
5.9
5.8
5.1
4.3
5.3
5.9
5.6
25.2
25.4
25.5
25.3
25.3
25.2
25.1
26.2
26 1
26.1
26 1
26.1
26.3
28.0
25.6
25.5
25 8
26.3
26.3
24 8
25.6
0
2
3
4
5
6
7
8.3
8.1
8.2
8.2
8.1
8.2
8.2
79
8.2
7.8
78
80
7.9
77
7.6
7.6
6.6
6.5
6.6
6.7
6.7
59
60
4.8
45
5.3
5.3
55
25.0
25.6
25.8
25.6
25.7
25.4
25.6
26.2
26.1
26.1
26 1
26.1
26.3
26 0
25 7
25.4
25.6
25.7
24.3
24.1
24.8
09-Jan-17
11-Jan-17
13-Jan-17
24 fir
24 fir
24 fir
825
644
664
<0.05
<0.05
012
0.0
0.6
0 9
not frozen
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
100.0%
0.280
100.0%
0.316
Avg. Fecundity: 70.3%
Avg. Fecundity. 69.0%
Test Results
Significant Mortality7
Yes No
Calc t
Tabular t
Check One
G owth
-1.29
1.76
Fecundity
Rank Sum
Cnt Value
PASS
51
39
FAIL
Check One
Test Date
Effluent Test Concentration
5 replicates were set for each control test replicate; where <5 are shown the organisms were lost during renewa
5 replicates were set for each treatrnent test replicate: where u5 ere shown the organisms were lost during rene
DWQ Form AT-4 (8/99)
Page 2 of 6

Day 1
Deac Lost
Day 2
Deac Loe1
Day 3
Dead Lost
Day 4
Dead Lost
Day 5
Deed Lost
Day 6
Dead Lost
Day 7
[]eau Lost
Weight
mg
Fecundity
I. Gray Graric
source
rep
Survival
ontrol
A
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.23
1
2
5
B
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.07
2
1
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0.9
0
0
4
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.37
0
2
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
18
0
2
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
149
2
5
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.36
0
1
5
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.75
3
5
15
A
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.99
G
1
5
B
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.4
2
2
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.24
C
2
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.81
1
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.2
1
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.69
2
1
5
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.65
0
1
5
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.65
0
0
5
0
A
0
8
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
O
A
0
B
0
C
0
0
0
E
0
F
0
0
IH
0
dare.
FJ
JC
JG
JC
AM
AM
End Dale
Fe:
FJ
JC
JG
JC
AM
AM
Ter lee. rere.
02.20 PM
01,41,0
I, Oe AM
12 sr PM
121, PM
0)0]PM
I 17-Jan-17 AM
Em,.r, he. teat -c
25.6
25.8
25.6
25.7
25.4
25.6
t2 n PM
CK lee. •c
26.2
26.1
26.1
26.1
26.1
26.3
261
dorlreiNew film . •d
25.4
25.5
25.3
25.3
25.2
25.1
Labe
T48371
Client
Havelock
Sample ID
WWTP
NPDES■
NC0021253
County
Craver
Month
1
Stan 8 tad Dale
10-Jan-17
Start & tad Time
02:30 PM
Started & red By
AM
Test 0rganIsm
Amencamysis bahla
Reoborn date
ARO HATCH 1.3-17
Rao born time
7
lest 1 ypa
SCCD
Dilution Water
INSTANT OCEAN
Units for Cone
%
%era BROOD
Taal I.
400 nil
Teat volume
150nil
Incubators
1
Light
16i08dk
'now lamp •c
25
Arteml.
750
T e.! method
EPA 821. e.02-01e 1ott
Comments
All reps have 5
organisms unless noted otherwise
Control .ni lernp
D=Deac N/A -Lust or rot uses
Page 3 of 6

Erg
PO Box 16414, OREENVILLE. 8O 29606-7414
(9641 677-6942, (6001 891-3325 F4x:(8641 $77 6938
BMIPPIN8 ACCRETE: 4 CRAFTSMAN CT, OREER, 80 29650
WW W.ETTEN,NRONM ENTAL.CCM
CHAIN (_,r, CUSTODY RECORD
Pagc j_ of --�—
client:
! / ' oTr
trIG/
Program
Containers
Preservative
Parameters
Facility: ct /% yJSf� � / / �j%17%P%%� / //f f
Llean Water Act
it
0
to
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2
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`Li
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14 of Containers 1
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a
a
0
g
--
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I41.7504
2- HCL
)-HNO3
4-NaOH
6ZuAe
Other
whole Effluent Toxicity
Macroinvcriebralc ID 1
F.TI ASSIGNED LAI3 ID I/
State: 4/ NPDES #: 44 0002/22S3
Acute
Chronic
Test Organisms
SAMPLE ID
4 (G) Grab (C) Composite
(Composite only)
CamomsiteStart Due
Time
(Grab or Composite)
suapkCeeeeiie°Dale
Time
Collected by
Acute Pass/Fail
Acute Multi-Conc.
Chronic Pass/Fail
Chronic Multi-Conc.
t
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d
D. ambigua
Fathead Minnow
Mysid Shrimp
e.
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us
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Chironomus
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3
Chemical Analysis & Other
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�F 37Il4
Special Instructions:
Sample Custody Transfer Record
Dale Time Relinquished By / Organization Received By / Organization
Secure
Area
Receipt
Temp °C
sample
Preserved?
/7q/7
�-�
.- / /Cr'I/ of 9yehr,- Oct.)> >J
11►011-7
OV
UPS
Crr
a.v T
---
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours, Equal volut
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

21
Ln
0
ET 1
PO BOx 16414, OattNV,LLI. BC 29606.7414
10641 877-6942, 18001 891.2325 FAx:[phone]E
BMIVPIND ADDRESS: 4 CRAFT/MAN CT, DREIR, 6C 29050
W W W.tTT(TI VIMOMM[MTAL.GOM
CHAIN ...F CUSTODY RECORD
'Page 1_ ofL
Client:
(/ Or d%, -
Program
Containers
Preservative
Parameters
Facility: /gyp y�
/le � • Lrr(1,-,e • An /
Clean Water Act
IStormwater
c
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to
INon -Regulatory
# of Containers
a
a
0
v
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>
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=
1-H2SO4
2- HCL
3-HNO3
a-NaOH
e Oibcr
Whole Effluent Toxicity
TIE/TRE
WER
Macroinvertebrate ID
Chemical Analysis & Other
0
5
:II
Z
0
;n
i
is
State: G NPDES #•,i Q . . 5 3
Acute
Chronic ic
Tat Organisms
SAMPLE ID
1(G) Grab (C) Com poall!
(Composite only)
Composite sun oar
Coot
Time
(Grub or Composite)
Sample Collection oar
Time
Collected by
Acute Pass/Fail
Acute Multi-Conc.
Chronic Pass/Fai)
Chronic Multi-Conc.
Li
9
an
8
O
[Fathead Minnow
Mysid Shrimp
:0
`
>
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0
u
G
2
Chirononws
-/ S-
I-/a-/7
ll j
l-1i-/7
lib
{�
✓
..5
(�
✓
_
/c.Colec ,
Special Instructions:
Sample Custody Transfer Record
Date Time Relinquished By / Organization Received By / Organization
Secure
Area
Receipt
Temp °C
Sample
Preserved?
//`/%
Ix
/) % '��-3- /CI / ar /ode 4
UPS
—11-17
O 5t11
UPS
XL.I.
0.6
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

CHAIN ,i CUSTODY RECORD
PO pox 16414, OwCCNVIuc, BC 29605-7414
18641 877.6942, (8001 891.2325 F4x:[phone]
SHIPPING AGGRESS: 4 CRAiTSMAN CT. 13Raaq. 8C 29650
W WW.CTT[N V laaNM 6NTAL.COM
Client: J 1 \4
Facility: LW
(Page of
# c�Ja-.rick-t- P
State: (" NPDES #: NL Oq ,?1 75.3
SAMPLE ID
NTt�.1 `L
(G) Grab (C) Compoeie
(Composite only)
Composite Start Due Time
ilcr l��'
(Grab or Composite)
Sum Collection Dale Time
Program
Containers
Preservative
Parameters
Collected by
3
U
0C
cn
0
0
rn
0
60
z
9
0
U
9
0
0
N
o
I.H2504
2• HCL
3•HNO3
4-NaOH
8 S•We
6.O
Y Other
Whole Effluent Toxicit
Acute Chronic
es
0
0
Q
0
0
a
u
U
Test Orpantsms
3
el
O
Chemical Analysis & Other
EAT ASSIGNED LAB ID N
`137j0
1
Special Instructions:
Sample Custody Transfer Record
Date Time
/fN
°qv
Re1ingtied By / Organization
Received By / Organization
Ira0S( 0_4\4-1-6-‘6611._ LOLLTP
Secure
Area
Receipt
Temp °C
Sample
Preserved?
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal vulur
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.
J

ETI.
[phone] . FA [phone]
P 0. Box 16+414 Greenv Ile. SC 29606
4 Craftsman Coun, Graff. SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES #: NC0021253
Test Date: I8-Apr-17
Laboratory ID #: T49110
Test Reviewed and Approved By:
...4.r fit;... j.
Robert W Kelley, Ph.D. Forbad Rostampour
QA/QC Officer Laboratory Director
Certification 0E87819
Test results presented in tics repon conform to all requirements of
NELAC. conducted under NELAC Certification Number E87819
Flonda Dept. of Health. Included results penain only to provided samples
SCDHEC Certification 423104
NCDENR Certification 4 022
Page 1 of 6

Effluent Toxicity Report Form - Chronic Mvsidopsis Pass/Fail
Date:
18-Apr-17
Facili : Havelock
NPDES # NC0021253 Pi.e#: 001 Coun : Craven
Laborato P in�Te .
ETT Environmental Inc.
Comments:
Signature of Operator in Responsi
rg /�]
Signature of Laboratory Supervisor
: >':nvironmental Sciences Branc
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving #
Original #
Weight (per Onginalj
Fecundity (grawd/total females)
Treatment 2 Replicates
Surviving #
Onginal #
Weight (per Onginap
Fecundity tgravid/lotal females)
Water Quality Data
Control
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Ternp Final
Salinity Initial
Sample
Collection Stan Date
Grab
Composite (Duration)
Conductivity Ipmhos/cm1
Chlonne (mg4.)
Sample Temp. at Receipt
2
3
4
5
6
7
8
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
0 350
0.366
0.364
0.372
0.316
0.344
0.326
0.386
2/3
3/5
2
0/4
3
2/4
4
3/4
5
2/5
6
4/5
7
1/4
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
0.380
0.388
0.416
0.344
0.516
0.334
0.342
0.400
2/2
1/2
2/4
0/2
Day
4/4
1/3
2/2
2/3
0
2
3
4
5
8.4
8.2
8.2
80
80
79
7.9
80
7.7
7.4
75
77
6.9
7.7
7.3
7.2
7.2
6 1
6.5
6.2
7.8
5.6
5.0
4 3
5.8
5.4
3.6
5.1
25.3
25.5
25.5
25.7
25.3
25.2
25.1
26.2
26.2
26.2
25.8
25.9
25.0
25.8
24.3
23.8
24.0
24.7
24.9
25.1
25.2
0
2
3
4
5
82
8.2
8.2
8.2
8.1
8.0
7.8
8.0
7.9
7.5
7.6
7.7
7.4
7 7
7.0
7.0
6.9
5.9
6.1
6.4
7.5
5.2
5.9
3.9
4.5
4.9
4.8
5.0
25.0
25 6
25 7
25.4
25.7
25.4
24.5
26 2
26.2
26.2
25.8
25 9
25.0
25.8
24.1
24.2
24.5
27.1
24.2
24.5
24.6
16-Apr-17
18-Apr-17
20-Apr-17
24 hr
24 hr
24 hr
737
728
808
0.07
<0.05
0.21
0.0
1 0
3.0
partially frozen
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
100.0%
0.353
100.0%
0.389
Avg. Fecundity 49.6%
Avg Fecundity 62.5%
Test Results
Significant Mortality%
Yes No
Calc I
Tabular t
Check One
Growth
-1.52
1.76
Fecundity
Rank Sum
Cnt Value
PASS
75.5
39
FAIL
X
Check One
Test Date
Effluent Test Concentration
5 replicates were set for each control test replicate where <5 are shown the organisms were lost during renewa
5 replicates were set for each treatment test replicate. where <5 are shown the organisms were lost during rene
DWO Form AT-4 (6/99)
Page 2 of 6

Day 1
Dead Lost
Day 2
Dead Lost
Day 3
Dead Lost
Day 4
Dead Lost
Day 5
Dead Lost
Day 6
Dead Lost
Day 7
Dead Lost
Weight
mg
Fecundity
N.Grav Gravid
50urCe
rep
Survival
)ntrol
0
0
0
0
0
D
0
0
0
0
0
0
0
0
1.75
1
2
5
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.83
2
3
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.82
4
0
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.86
2
2
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
158
3
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.72
_•
2
5
G
0
0
0
0
C
0
0
0
0
0
0
0
0
0
1.63
1
4
5
h
_
0
0
0
0
0
0
0
_
0
0
0
0
0
1.93
3
1
5
0
o
B
0
C
3
D
0
E
F
0
G
0
H
0
0
0
A.
E
0
C
0
D
0
E
0
F
0
G
0
H
o
0
A
0
6
-
C
0
D
0
E
0
F
0
G
0
r
0
0
A
0
6
.,
C
0
D
0
E
0
F
0
G
0
0
15
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1 2
0
5
6
0
0
3
G
0
0
0
0
0
0
0
0
0
184
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.08
2
2
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1 72
2
0
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.58
0
4
5
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.67
2
1
5
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
17'
0
2
5
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
2
5
a.,...
JG
JG
FJ
FJ
AM
JG
End Date
eta
JG
JG
FJ
FJ
AM
JG
Ten. r.e a ren.•
a]]erw
C2/I PL.
a: 21 Pr.
,:1]eu
12 SZ
-. . e•
25.81
I 25-Apr-17 rJ
em.em ne. tera =
25.6
25.7
25.4
25.7
25.4
24.5
a::.: is
OW i.rno •C
26.2
26.2
26.2
25.8
25.9
25
ee-oei Me. to-r :
25.5
25.5
25.7
25.3
25.2
25.1
Labe
T49110
Client
Havelock
Semple to
VVWTP
NPDESe
NC0021253
County
Craven
Month
4
Stan & fad Date
18-Apr.17
Start & fed Time
01 30 PM
Stalled S fed By
AM
Toot organism
Amencamysis Bahia
Neo. bom date
11-Apr-17
Neo. bom time
0
Test Type
NCCPF
(Mutton water
INSTANT OCEAN
Units for Conc.
r
%3rd BROOD
Test vessels
400 MI
Test volume
150 ml
Incubator
1
Light
,,61t78ok
Initial Temp •C
25
Anemia
750
Test method
CPA 121.0.02.ate leo;
Comments
411 reps have 5
horganisms unless noted otherwise
ontrol ini temp
IDrganisms rec'd from Aquatic Indicators
7 days old on amval
D=read N!A-Lost or not used
Page 3 of 6

ET,'
PO BOX 16414, ORKeNv,LLC. 90 29606.7414
(0641 577-6942, 1800)891-2325 Fax:18641 B77 6938
SMIPPINfl AooR[aa: 4 CRAIT.MAN CT. ORC[R, 90 29680
W W W.CTT[N VIRONM(NT4L-COM
CHAIN OF CUSTODY RECORD
Page _� of
Client: I e , O / �
�t /-6VP (j6x
Program
Containers
Preservative
Parameters
Facility: mST le u/G 7tPc...-p
4����" T[ p4n
Q
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Stormwater
c
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Non -Regulatory 1
I#of Containers
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1-H2s04
2-HCL
3-HNO3
4:NaOH
i- �`
6-ah�
Whole Effluent Toxicity
y
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WER
Macroinvertcbratc Ill
Chemical Analysis & Other
GI-P ASSIGNED LAB ID it
'//�
State: NC NPDES #: K. ( /a.3
Acute
Chronic
Test Organisms
SAMPLE ID
I (G) Grnb (C) Coin posits
(Composite only)
Composite Start 0•Ic
Time
r
(Grab oComposite)
Samp a Collection Dam
Time
Collected by
Acute Pass/Fail
Acute Multi-Conc.
Chronic Pass/Fail
Chronic Multi-Conc.
'a`
'O
v
D. ambigua
Fathead Minnow
Mysid Shrimp
y
>
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Chirononms
f
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' /47/7
&O,
7Zv,'
V
2V
..I
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Jf,
9 eo Cam%/c�
Lf9noA
I
I
Special Instructions:
Sample Custody Transfer Record
Date Time Relinquished By / Organization Received By / Organization
Secure
Area
Receipt
Temp 'C
Sample
Preserved?
/7 /7
aW
7 =� G',Xs oF
y/1817
080
Fed Ex
► -
o. a
'
,,
_
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volui
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0'C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ETTi
PO Box 16414, elecCNVILLt, BC 29606.7414
[phone], [phone] •4x:[phone]
SNIPPING AOOnt99: 4 CRAFTSMAN CT, Oaten, 9C 29650
W W W.CTTEN V ISONMENTAL,CGM
CHAIN OF CUSTODY RECORD
'Page _fofl_ I
Client: ,
C2 rif O F kP/O�ir
Program
Containers
Preservative
Parameters
Facility: - die W /er 7rp9i e4>< P I / �7 /y1
Clean Water Act
'Clean
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Non-Regulatory
IN of Containers
u
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s-c
Whole Effluent Toxicity
C:]
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L2�j
Mncroinvertebmlc ID 1
Chemical
ETT ASSIGNED LA© ID N
State: /VG NPDES #: A{/( 000?/ A5.2
Acute (Chronic
Test Organisms
SAMPLE ID
(G) Grab (C) Compoaltc
(Composite only)
Composite Start Date
Thee
(Grab or Composite)
sm Coan t nn Date
Time
Collected b
Acute Pass/Fail
Acute Multi -Cone.
Chronic Pass/Fail
V_
O
U
_-
2
o
y
cs
.p
u
c
co
s
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Fathead Minnow
a
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¢
a
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Chironomus
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✓
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%yG �AC�//�lfv�i
1/91f pPj•
Special Instructions: to n a,,rrtvck2, 0,2„.1,00
-ke, 1I d Ut is flat'
e. I A5 -Po . nd -b e i + wife -I-ke I-ol 0#. `fh.P-- of -e brit c. was 62/3 -Pule o
ses+1erl fi \,v5D i- cpPew red -b Kav- I ei kgd i 46.. coo( , . — 6-D
-.
Sample Custody Transfer Record
DDate/ By/Organiizza't'ion Received
Secure
Area
Receipt
Temp °C
Sample
Preserved?
7,Tiimmee
if /
6 0
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/� /
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Utr ✓
uid
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IJRLvIk rm.( T7rrN JIJPs o � 1 In
c/�� .51:).„..Tha,
5p-r b--3 - 1 Cdf+v r)_ 4rznop.4)- h c.
-
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volul
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection

ETI'
PC Box 16414, GAs[NVILLt. 8C 29606-7414
18841 877-8942. 181301 891-2325 F4x:18641 877 6938
31-1:95m5 AooRtSti- 4 CAArrAMAN CT, 0AtaA. BC 29660
W W W.tTTGN V IRONM[NTAL.COM
CHAIN OF CUSTODY RECORD
'Page A__ of
L1tent:/yI�
��t,_,�,
_r V`.tx:_ (1JWl
(j�'
Program
Containers
Preservative
Parameters
-yam
Facility: ky_ks Acv IT.La \ _T _ _,,, L
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(Sediment
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Y
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1.H2SOJ
3�HN0Jso
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Whole Mum Toxicity
WER 1
Macroinvenebratc ID
ETI' ASSIGNED LAI3 ID 8
�Y
State: j NPDES #: NC �0 21 a,
Acute
Chronic
Tat Organisms
SAMPLE ID
I(G) Grnb (C) Campaelle
(Composite only)
Composite Start Date
Time
(Crab or Composite)
Sample Collection Date
Time
Collected by
.µ6..
Ili
v
¢
Acute Multi-Conc.
Chronic Pass/Fail
Chronic Multi-Conc.
C. dubia
m11
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i
Fathead Minnow
Mysid Shrimp
73
R
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es
rJ
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x
C
-
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Chemical Analysis & Other
K
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V
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fat
V
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]
✓
'` ,gee_ Co11zckian
4f9rloc
1
Special Instructions.
Sample Custody Transfer Record
Date Time Relm uished By / Organization Received By / Organization
Secure
Arca
Receipt
Temp 'C
Sample
Preserved?
Lilt Ci'
1oS
)"'L v? 0 41-6,vebclh t ouj
P
t 17
1(U
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volui
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

Eam ,Inc.
PO t3vx 1(r31a 1:3feenvl1E SC 29606
(E64) 8774942 . FO [phone]
4 Craftsman Coun, Greer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES #: NC0021253
Test Date: I8-,1u1-17
Laboratory ID #: T49644
Test Reviewed and Approved By:
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC Officer Laboratory Director
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
SCDHEC Certification #23104
NCDENR Certification # 022
Page 1 of 6

•
Effluent Toxicity Report Form - Chronic Mysidoosis Pa
V .....
V
Facili : Havelock NPDES # NC0021253 Pi•e#: 001 Count : Craven
Lab ,yrsy ITT Environmental Inc.
Comments:
Signature of Opera' On Responsible C arge
x �� `i---- /7
i 7'
Signature of Laboratory Supervisor
Environmental Sciences Branc
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving #
Original #
Weight (per Original)
Fecundity (gravid/total females)
Treatment 2 Replicates
Surviving #
Onginal #
Weight (per original)
Fecundity (gravid/total females)
Water quality Data
Control
pH Initial
pH Final
D0 Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Stan Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/t.)
Sample Temp. at Receipt
2
3
4
5
6
4
3
4
5
4
5
5
5
4
4
5
5
4
5
5
5
0 390
0.213
0.262
0.360
0.440
0.362
0.324
0.354
1/2
1/1
2
2/3
3
1/2
4
1/1
5
3/3
3/5
2/2
3
3
5
4
4
4
5
5
5
5
5
4
4
4
5
5
0 212
0.188
0.322
0 368
0 283
0 338
0 336
0 308
2/2
2/2
0/0
2/2
Day
2/2
2/2
2/2
3/3
0
2
3
4
8.0
8.0
6.2
8.0
8.2
8.2
8.3
7.8
78
73
77
77
7.9
8.0
7.0
66
64
6.3
6.8
72
62
5.1
5.3
5.0
4.9
4.9
3.8
5.2
25.4
25.5
25.4
25.5
25.4
25 2
25 2
26 7
26.7
26 9
26 5
26.7
26.7
26.5
24 7
25 5
26.0
26.0
26.2
26.2
27.1
0
2
3
4
81
8.0
83
7.9
82
8.1
8.3
79
80
76
79
7.6
8.0
8.0
6.8
6.8
6.7
6.2
6.8
6.7
6.4
5.2
5.0
44
47
48
4.5
59
25 0
25.7
25 6
25.9
25.2
25 4
25.5
26.7
26 7
26.9
26 5
26 7
26 7
26.5
24 3
24.3
25.6
25.6
23.8
24.0
25.5
16-Jul-'7
18-Jul-17
20-Jul-17
24 hr
24 hr
24hr
730
698
646
<0.05
0 07
<0.05
0.7
0 8
2.2
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
94.6%
0.338
89.2%
0.294
Avg. Fecundity: 78.3%
Avg Fecundity: 100.0%
Test Results
Significant Mortality?
Yes
No
x
Cale. t
Tabular t
Check one
Growth
1.30
1.76
Fecundity
Rank Sum
Cnt Value
PASS
70
49
FAIL
Check One
Test Date:
Effluent Test Concentration
5 replicates were set for each control test replicate, where <5 are shown the organisms were lost during renewa
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during rene
DWO Form AT-4 (6199)
Page 2 of 6

Day 1
Dead Lost
Day 2
Deed Lost
Day 3
Dead Lost
Day 4
Dead Lost
Day 5
Dead Lost
Day 6
Dead Lost
Day 7
Dead Lost
Weight
mg
Fecundity
N-Grav Gravid
source
rep
Survival
'OntrOl
A
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1.56
1
1
4
B
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0.85
0
1
3
C
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1.31
1
2
4
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.8
1
1
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
1
176
0
1
4
F
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.81
0
3
5
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.62
2
3
5
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
177
0
2
5
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
--
0
O
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
~^
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
15
A
0
0
0
0
1
0
0
0
1
0
0
0
0
0
1.06
0
2
3
B
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0.94
0
2
3
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.61
0
0
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1.47
0
2
4
E
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1.13
0
2
4
F
0
0
0
0
0
0
0
0
0
0
0
0
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1
1.35
0
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G
0
0
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0
0
0
0
0
0
0
0
0
0
0
168
0
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H
0
0
0
0
0
0
0
0
0
0
0
0
0
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1.54
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Renew
FJ
JG
FJ
AM
AM
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End Date
eel
FJ
JG
FJ
AM
AM
JG
I .i s, -f',,
Time red a renew
Oh3.1 PC
03.32 PM
C3.06, PC
10.34 AM
11.36 AM
0322 PM
_u}c
I 25-Jul-17 AM
Eln.rom Mew l.m;. -c
25.7
25.6
25.9
25.2
25.4
25.5
04 13 PM
Old tame •e
26.7
26.7
26.9
26.5
26.7
26.7
26.51
Control New temp. -c
25.5
25.4
25.5
25.4
25.2
25.2
Lebd
T49644
Client
Havelock
Sample ID
WWTP
NPOES#
NC0021253
County
Craven
Month
7
Start d fed Date
18-Jul-17
Start & fed Tim.
03:30 PM
Started & fed By
AM
Test organism
Americamysis bahia
Noe. born dote
11-Jul-17
Nee. born time
0
Test Type
NCCPF
Dilution Water
INSTANT OCEAN
Units for Cont.
%
:Ord BROOD
Test vessels
400 MI
Test volume
150 ml
Incubators
1
Light
161U8dk
Initial Temp 'C
25
Anemia
750
Test method
EPA 621-e-02.034 1007
Comments
All reps have 5
organisms unless noted otherwise.
Control .ni temp
Organisms rec'd from
Aquatic Indicators
D=Dead NIA -Lost or not used
Page 3 of 6

CHAIN trr, CUSTODY RECORD
PO Sax 16414. GREENVILLE. 5C 29606-7414
t9641 877-6942, t8001 891-2325 FAx:t8641 877 6936
SHIPPING AGGRESS: 4 CRAFTSMAN CT. GREER. 5C 29650
W W W.ETTEN V IRONM ENTA4GOM
Page of
Client: t `
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Program
Containers
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Facility:
1 Akkler 1(ect} - o1\
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Whole Effluent Tonicity
P
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Mncroinvertebrate ID 1
Chemical Analysis & Other
ETT ASSIGNED LAB ID !!
State: NPDES it:
Acute
Chronic
Test Organisms
SAMPLE ID
1(G) Crab (C) Composite 1
(Composite only)
Composite Stan Date
Time
(Gab or Composite)
sir.* conmitia° Date
Time
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Acute Pnss/Fail
Acute Multi -Cone.
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Sample Custody Transfer Record
Date Time Relinquished By / Organization Received By / Organization
Secure
Area
Receipt
Temp °C
Sample
Preserved?
-4.il11�i05Ci
V-,g0a
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7f 1
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: I sample each hour for 24 hours. Equal volur
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.
7

CO
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PO BOX 16414, GREENVILLC, SC 2915136.7414
(8641 877-6942, I8001 891-2325 FAx:[phone]
SHIPPING ADDRESS: 4 CRAFTSMAN CT, GREER. 9C 29680
W W W.ETTEN V IRONMENFAL.COM
CHAIN VF CUSTODY RECORD
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Sample Custody Transfer Record
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Area
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Sample
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11-�-
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7[91,10
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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
FIOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

2)
to
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PO fax 1 6414. GRCENVILLE. SC 29606-7414
1864) 877-6942. I800) 891-2325 F4x:1564) 677 693E
SHIPPING ADDRESS: 4 CRArr5uAN Cr, GREER. SC 29650
W W W.CTTCNV IRO NMCMTAL.COM
Client: Chi `_ , _ (_domel
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(G) Grab (C) Corn polio
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Composite Stan Date Time
(Grab or Composite)
Sample Collection Date Time
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CHAIN of CUSTODY RECORD
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A.MGI.IcA 1b
Secure
Area
Receipt
Temp °C
2,Z
Sample
Preserved?
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

ra% env lronmental.Inc.
P.0, BOX 16414, Greenv Ile. SC 29606
[phone] . FAX [phone]
4 Craftsman Court. Grier, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES #: NC0021253
Test Date: 10-Oct-17
Laboratory Sample ID #: T50175
Test Reviewed and Approved By:
47
nelac.1
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC Officer Laboratory Director
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E878I9
Florida Dept. of Health. Included results pertain only to provided samples.
SCDHEC Certification #23104
NCDENR Certification # 022
Page 1 of 6

Date:
10-Oct-17
-Chronic Mysidopsis Pass Fail
Facili : Havelock NPDES # NC0021253 Pi.e#: 001 Coun :
Craven
Laboratory Performing Test: ETT Environmental Inc.
Comments:
x
Signature of Operator in Responsible Charge
X
Signature of Laboratory Supervisor
I
MAIL ORIGINAL TO: Environmental Sciences Branc
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
Surviving #
Original #
Weight (per Original)
Fecundity (gravid/total females)
Treatment 2 Replicates
Surviving #
Original #
Weight (per Original)
Fecundity (gravid/total females)
Water Quality Data
Control
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/L)
Sample Temp. at Receipt
1
2
3
4
5
6
7
8
5
4
5
3
4
4
5
5
5
4
5
3
4
4
5
5
0.346
0.350
0.404
0.517
0.355
0.465
0.436
0.342
3/4
1
3/3
2
2/3
3
2/2
4
2/3
5
2/3
6
2/3
7
1/2
8
4
5
5
5
5
4
4
4
4
5
5
5
5
5
4
5
0.395
0.362
0.380
0.402
0.404
0.218
0.288
0.300
2/3
1/2
2/2
Day
1/2
0/0
3/3
0
1
2
3
4
5
6
7
7.9
8.0
8.0
7.9
8.0
8.0
8.1
7.8
7.5
7.5
7.5
7.7
7.6
8.1
7.4
7.4
7.3
6.6
6.8
6.9
7.4
5.0
3.7
4.7
3.5
3.9
4.6
5.9
25.8
25.4
24.5
25.2
25.1
25.0
25.1
26.8
26.4
26.8
26.7
26.5
26.6
26.7
25.0
26.4
26.6
26.8
24.7
24.8
24.8
0
1
2
3
4
5
6
7
8.0
8.0
8.0
7.9
8.0
8.0
8.1
7.9
7.9
7.5
7.6
7.7
7.7
8.1
7.7
7.7
7.9
6.6
6.8
6.9
7.6
6.2
4.9
3.9
4.1
4.0
4.1
6.2
25.8
25.2
25.6
25.5
25.7
25.6
25.4
26.8
26.4
26.8
26.7
26.5
26.6
26.7
25.8
26.0
24.0
23.0
23.5
23.6
23.7
08-0 ct-17
10-Oct-17
12-Oct-17
24 hr
24hr
24 hr
790
784
780
<0.05
<0.05
<0.05
0.7
1.0
1.7
%Survival
Avg Weight (mg)
%Survival
Avg Weight (mg)
100.0%
0.412
94.7%
0.344
Avg. Fecundity: 74.0%
Avg. Fecundity: 81.0%
Test Results
Significant Mortality?
Yes
No
X
Calc. t
Tabular t
Check One
Growth
1.75
1.76
Fecundity
Rank Sum
Crit. Value
PASS
61
51
FAIL
Check One
Test Date:
Effluent Test Concentration:
5 replicates were set for each control test replicate; where <5 are shown the organisms were lost during renews
5 replicates were set for each treatment test replicate; where <5 are shown the organisms were lost during rene
DWQ Form AT-4 (6/99)
Page 2 of 6

Day 1
Dead Lost
Day 2
Dead Lost
Day 3
Dead Lost
Day 4
Dead Lost
Day 5
Dead Lost
Day 6
Doad Lost
Day 7
Dead Lost
Weight
mg
Fecundity
N-Grav Gravid
source
rep
Survival
control
'+'
A
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.73
1
3
5
B
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1.4
0
3
4
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.02
1
2
5
D
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1.55
0
2
3
E
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1.42
1
2
4
F
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1.86
1
2
4
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.18
1
2
5
H
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.71
1
1
5
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
0
A
0
B
0
C
0
D
0
E
0
F
0
G
0
H
0
15%
A
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1.58
1
2
4
B
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.81
1
1
5
C
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1.9
0
2
5
D
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.01
0
1
5
E
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.02
1
1
5
F
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1.09
0
0
4
G
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1.15
0
1
4
H
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1.5
0
3
4
Renew
AM
JG
FJ
FJ
JG
AM
End Date
Fed
AM
JG
FJ
FJ
JG
AM
Time 1eC a renew
06:0$ PM
04-.34 PM
03'23 PM
0316 PM
11.11 AM
04.04 PM
26.71
I 1 7-Oct-1 7 AM
E1.4ent New lamp. •c
25.2
25.6
25.5
25.7
25.6
25.4
03.43 PM
OM temp. •c
26.8
26.4
26.8
26.7
26.5
26.6
Control New temp •C
25.4
24.5
25.2
25.1
25.0
25.1
Lab#
T50175
Client
Havelock
Sample ID
WWTP
NPDES#
NC0021253
County
Craven
Month
10
Start & fed Date
10-Oct-17
Start & fed Time
03:00 PM
Started & fed By
JC
Test Organism
AMERICAMYSIS BA
Neo. born date
03.Oc1-17
Neo. bom time
0
Test Type
NCCPF
Dilution Water
INSTANT OCEAN
Untie for Cone.
%
Ye3rd BROOD
Test vessels
400 ml
Test volume
250 ml
incubator
1
Light
1611./8dk
Initial Temp eC
25.8
Artemis
750
Test method
EPA 021-R•02.014:1007
Comments
All reps have 5
organisms unless noted otherwise.
Control ini teraMIMMII
EACH REP HAS 5 ORGANISMS.
ORGANISMS SOURCE= ARO 10/10/17
7 DAYS OLD
D=Dead N/A -Lost or not used
Page 3 of 6

ET'
PO BoX 16414, GREENVILLE. SC 29606-7414
I8641 877-6942, I800) 891-2325 FAX:[phone]
SNIPPING ADDRESS: 4 CRAFTSMAN CT. GRECR. SC 29650
W W W. CTTEN V I RONM CNTAL.COM
CHAIN uF CUSTODY RECORD
Page f of
Client:
C, / (O' / 6i/e4e/.-
Program
Containers
Preservative
-
Parameters
Facility:11 ,,( �' .,[. J J
vl+ )7 4,4 �E' /^ " : i"c / l it i t P/ l? T
Clean Water Act
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t1-I' ASSIGNED LAI3 ID !!
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Chronic
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SAMPLE ID
(G) Grab (C) Composite
n
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Time
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qy IYiI I�1 FYI
Sample Custody Transfer
Date, Time
Record
- lin uished By / Organization
Received By / Organization
Secure
Area
Receipt
Temp °C
Sample
Preserved?
744
,- �/
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tojoiN
laao
UPS
Err
.41/tt..)0,31),a0
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum I sample every 4 hours over 24 hours.
Flow Proportional. ' er instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

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Composite Start Date
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Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volur
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

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Time Proportional: 1 sample each hour for 24 hours. Equal volut
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional:r instructions in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Annual Priority Pollutant Analysis Data
2014-2017

P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
PARAMETERS Date Analyst Code
Ammonia Nitrogen as N, mg/1
Total Kjeldahl Nitrogen as N,mg/1
Nitrate -Nitrite as N, mg/1
Total Phosphorus as P, mg/I
Oil & Grease (HEM), mg/1
Phenol, ug/1
/'6' Total Cyanide, mg/1
Total Hardness, mg/1
Total Dissolved Residue, mg/1
Antimony, ug/I
Arsenic, ug/1
Beryllium, ug/1
Cadmium, ug/1
Copper, ug/I
Total Chromium, ug/1
Lead, ug/1
Nickel, ug/1
Selenium, ug/1
Silver, ug/I
Thallium, ug/1
Zinc, ug/1
Effluent Analysis Method
0.06 06/03/14 ALB 350.1 R2-93
1.54 06/02/14 ANO 351.2 R2-93
3.66 05/30/14 ANO 353.2 R2-93
0.93 06/02/14 ALB 365.4-74
<5.0 05/30/14 SEJ 1664B
<5 06/06/14 SEJ 420.1-78
<0.005 06/05/14 SEJ 4500CNE-99
119 06/04/14 TRB 2340C-97
461 06/02/14 LW 2540C-97
<3.0 06/20/14 LFJ EPA200.8
<5.0 06/04/14 MEL 31138-04
<1.0 06/03/14 LFJ EPA200.7
<1.0 06/06/14 MEL 3113B-04
<10 06/03/14 LFJ EPA200.7
<5.0 06/03/14 LFJ EPA200.7
<5.0 06/09/14 MEL 31138-04
<10 06/03/14 LFJ EPA200.7
<10 06/04/14 MEL 31138-04
<5.0 06/03/14 LFJ EPA200.7
<1.0 06/20/14 LFJ EPA200.8
48 06/05/14 MTM 31118-99
Drinking Water ID. 37715
wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 204 H
DATE COLLECTED: 05/29/14
DATE REPORTED : 06/25/14
REVIEWED BY:

litIlinnOn [lacmcgaqk
111Minimmaiwwwwwwww.
P.O. BOX 7085. 114 OAKMONT DRIVE
GREENVILLE. N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
VOLATILE ORGANICS
EPA METF?OD 624
CLIENT ID:
ANALYST:
DATE COLLECTED:
DATE ANALYZED:
DATE REPORTED:
PARAMETERS, ug/I
k 1. • Chloromethane
2.. Vinyl Chloride
3. • Bromomethane
4.. Chloroethane
.5. Trichlorofluoromethane
1,1-Dichloroethane
f7. .Methylene Chloride
8. trans-1,2-Dichloroethene
9. 1,1-Dichloroethene
"..c1.0. Chloroform
-11. 1,1,1-Trichloroethane
-12. Carbon Tetrachloride
-13. Benzene
14. 1,2-Dichloroethane
--15. Trichloroethene
•.-16. 1,2-Dichloropropane
Bromodichloromethane
s18. 2-Chloroethylvinyl Ether
19. cis-1,3-Dichloropropene
r20. Toluene
-.21. • trans-1,3-Dichloropropene
22. 1,1,2-Trichloroethane
•.23. Tetrachloroethene
--24. Dibromochloromethane
-25. Chlorobenzene
26. Ethylbenzene
- 27. Bromoform
r 28. • 1,1.2,2-Tetracldoroethane
1,3-Dichlorobenzene
"•30. 1,4-Dichlorobenzene
Ns 31. 1,2-Dichlorobenzene
- 32. Acrolein
- 33. Acrylonitrlle
Effluent
<10.00
<10.00
<10.00
<10.00
<5.00
<5.00
<10.00
<5.00
<5.00
<5.00
< 5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
< 5.00
< 5.00
<5.00
<5.00
<5.00
< 5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
< 100.00
<50.00
Drinking water ID: 37715
Wastewater ID: 10`
PHONE [phone]
FAX [phone]
204 H
MAO
06/20/14
06/27/14
07/07/14

ININEaml
O. BOX 7085, 114 OAKMONT DRIVE
1REENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
CLIENT ID:
ANALYST:
DATE
DATE
DATE
DATE
COLLECTED:
EXTRACTED:
ANALYZED:
REPORTED:
PARAMETERS, ug/1
Effluent
▪ .1. N-Nitrosodimethylamine
---2. Phenol
f 3. Bis(2-Chloroethyl) Ether
+. 4. 2-Chlorophenol
srr 5. 1,3-Dichlorobenzene
6. 1,4-Dichlorobenzene
1,2-Dichlorobenzene
u- 8. Bis(2-Chloroisopropyl) Ether
' 9. Hexachloroethane
w 10. N-Nitrosodi-N-Propylamine
--11. Nitrobenzene
�.12. Isophorone
-13. 2-Nitrophenol
.r 14. • 2,4-Dimethylphenol
15. Bis(2-Chloroethoxy) Methane
-•16. 2,4-Dichlorophenol
17. 1,2,4-Trichlorobenzene
Naphthalene
.s 19. Hexachlorobutadiene
4-Chloro-3-Methylphenol
21. Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
- 23. 2-Chloronaphthalene
Acenaphthylene
....25. Dimethylphthalate
-26. • 2,6-Dinitrotoulene
27. Acenaphthene
- 28. 2,4-Dinitrophenol
sa 29. r:4-Nitrophenol
2,4-Dinitrotoluene
.+31. Fluorene
32. - Diethylphthalate
>133. 4-Chlorophenyl Phenyl Ether
34. 4,6-Dinitro-2-Methylphenol
35. N-Nitrosodiphenylamine
36. 4-Bromophenyl Phenyl Ether
---37. Hexachlorobenzene
_ 38. Pentachlorophenol
39. Phenanthrene
--40. Anthracene
41. Di-N-Butylphthalate
= 42. Fluoranthene
43. Benzidine
44. Pyrene
Butylbenzylphthlate
Benzo[a]anthracene
47. 3,3-Dichlorobenzadine
48. Chrysene
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<20.00
< 10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<50.00
<50.00
�-< 10.00
<10.00
<10.00
<10.00
< 50.00
<10.00
<10.00
<10.00
<50.00
< 10.00
<10.00
<10.00
<10.00
<100.00
< 10.00
< 10.00
< 10.00
<10.00
< 10.00
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
204 H
CHS
06/20/14
06/26/14
07/01/14
07/07/14
Page: 1

BroeHroullia [I]cur pcga tA
11111111111.11111111111
ass..
P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC ,28532
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
CLIENT ID:
ANALYST:
DATE COLLECTED:
DATE EXTRACTED:
DATE ANALYZED:
DATE REPORTED:
PARAMETERS, ugll
Effluent
49.
-- 50.
-� 51.
52.
.53.
54.
55.
-r 56.
57.
Bis(2-Ethylhexyl)phthalate
Di-N-Octylphthalate
Benzo[b]fluoranthene
Benzo[k]fluoranthene
Benzo[a]pyrene
Indeno(1,2,3-C,d)pyrene
Dibenzo[a,h]anthracene
Benzo[g,h,ijperylene
1,2-Diphenylhydrazine
<20.00
<10.00
<10.00
<10.00
< 10.00
<10.00
< 10.00
< 10.00
<10.00
Drinking Water ID: 37715
Wastewater ID: 1A��
PHONE [phone]
FAX [phone]
204 H
CHS
06/20/14 Page: 2
06/26/14
07/01/14
07/07/14

Envi rota Nrineot:.-Ikc.,
P.O. Box. '7Ot5. 114 Oakmont Dr.
Grcenvil 1 �• 1►C' 27t;58
environ rim t nll inC.Com
Plume (2 — 2I756-6208 • Fax [phone]
Cl,IEN -11': 204 H
Week: 23
CITY C/FHAVELOCK
MR. A.RTHOUGH
WASTEWATER TREATMENT PLANT
304 N- JACKSON DRIVE
HAVE LOCK NC 28532
(252) 4-44-6421
COLLECTION
SAMPLE LC7CATON
Effluent
DATE
5.*1t
TIME
Ic3o
DISINFECTION
• C'IILORINI
�Y LIV
• NONE
CHAIN OF CUSTODY RECORD
Page L (t _ 1
CHLORINE NEUTRALIZED AT COLLECTION
<2
L?.
Luz
LZ
Gv
tgP-
pH CHECK (LAB)
G
G G
G G G G
CONTAINER TYPE. PG
c
C A A
A A
A
CHEMICAL PRESERVATION
o
E,_
W W
Z
c
OJ U
0
J
00
OPT
x OF CONTAINERS
I 1 15
C9
Q
Nitrate -Nitrite
T. Phosphorus
0
0
U
tn
ev
W
625 Duplicate 1
625 Duplicate 2
EPA 624 (APA)
624 Duplicate 1
624 Duplicate 2
PARAMETERS/TESTS
A -NONE D-NAOH
B -HNO., E•HCL
C - H. SO F - ZINC ACETATE/NAG
G - NATH!OSULFATE
CLASSIFICATION:
LiWASTEWATER (NPDES)
DRINKING WATER
DWGGW
SOLID WASTE SECTION
QUI HED BY I
RELINQUISH D
RELINQUISHED 8Y (SIG.)
AM L R) J1PATETIME RE
DATETIME
DATEEITIME
BY (SIG.)
RECEIVED BY (SIG
RECEIVED BY (SIG.)
CHAIN OF CUSTODY MAINTAINED
DURING SUJPMENT/DELIVERY
N
SAMPLES COt I FCTED BY:
(Please Print)
A/
SAMPLES RECEIVED IN LAB AT Of L,°C
DATETIME
3L3
DATETIME
DATETIME
COMMENTS:
4r-L _P rase Crfi (ei colc/ resh,j�
(02 c" / e, L,f` awl/
ORM Ir5
Lt' — 4SE READ Instructions for completing this form on the reverse side.
l
Sampler must place a "C" for composite sample or a "G" for
Grah samnlp in tha hlnrkc hma fnr nark wromntn..nn...,..1
N( 2'77S41

E� nVinm Inc:.
P C.). i' . 114 Oakmont Dr.
r-eenville. NC 2785;
c>t -2 NImnmcnt 1 ilie .c•r.om
p If -7 cme f 2521 756-621)8 • Fax [phone] ; 3
C L[ENT: 204 H Week: 23
CITE OF HAVELOCK
MF� - Aar HOUGH
WAS STEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HA_ %/'ELOCK NC 28532
(25Z) '114.6421
SAMPLE LOCATION
Effluent
COLLECTION
DATE
TIME
10.m
I�ISINFIC1ION
15
CHAIN OF( -.STODY RECORD
CHLORINE NEUTRALIZED AT COLLECTIOI
LA -
pH CHECK (LAB)
1
G
G
G
CONTAINER TYPE, PiG
(
•
•
A
A A
624 Duplicate 1
PARAMETERS,TESTS
CH
EMICAL PRESERVATION
A - NONE D•NAOH
B -HNO E -HCL
C-KSO, F - ZINC ACETATE Nk
G - NA TH!OSULF,ATE
RHINO HED
RELINQUISH
Y (SIG.)
RELINQUISHED BY (SIG.)
R)
DATETIME
' /6,'3�
DATETIME
DATETIME
REC _I BY (SIG.)
RECE D BY (SIr "I
RECEIVED EY (SIG.)
DATETIME
lG/htA 3Z7
DATETIME
1
DATETIME
COMMENTS:
I,•.1
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
DWQGW
❑ SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING+I}2p1ENT/DELIVERY
N
SAMPLES COLLECTED BY:
(Pease Print)
SAMPLES RECEIVED IN LAB
Ccshp.
=ORM /t5
fPLEASE READ Instructions for completing this form on the reverse side.
Sampler must place a'C" for composite sample or a "G` for N ° 277435
Grab sarrinle. in tI1P. IllnrkC a..n1ra fnr aarh noromofnr . ...

IWnaDMEgn
Ecurp[rtlge,
Drinking Water ID: 37715
Wastewater ID: 10
.0. BOX 7085. 114 OAKMONT DRIVE PHONE [phone]
GREENVILLE. N.C. 27835-7085 FAX [phone]
CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK. NC 2853E_
PARAMETERS
Ammonia Nitrogen as N, mg/I
Total Kjeldahl Nitrogen as N,mg/1
Nitrate -Nitrite as N, mg/I
Total Phosphorus as P, mg/I
Oil & Grease (HEM), mg/I
Phenol, ug/1
Total Cyanide, mg/l
Total Hardness, mg/I
Total Dissolved Residue, mg/1
Antimony, ug/I
Arsenic, ug/I
Beryllium, ug/I
Cadmium, ug/I
Total Chromium, ug/I
Copper, ug/I
Lead, ug/1
Nickel, ug/1
Selenium. ug/1
Silver, ug/I
Thallium, ug/1
Zinc, ug/I
Effluent Analysis Method
Date Analyst Code
<0.04 05/21/15 RND 350.1 R2-93
1.57 05/27/15 RND 351.2 R2-93
5.66 05/22/15 KDB 353.2 R2-93
2.11 05/28/15 AKS 365.4-74
<5.0 05/21/15 SEJ 1664B
<5 06/06/15 SEJ 420.1-78
<0.005 05/29/15 SEJ 4500CNE-99
110 05/26/15 TRB 2340C-97
465 05/26/15 KKF 2540C-97
<3.0 05/26/15 LFJ EPA200.8
<5.0 06/02/15 MTM 311313-04
<1.0 05/29/15 LFJ EPA200.7
<1.0 06/01/15 MTM 3113B-04
<5.0 05/29/15 LFJ EPA200.7
<10 05/29/15 LFJ EPA200.7
<5.0 05/29/15 MTM 3113B-04
< 10 05/29/15 LFJ EPA200.7
< 10 06/08/15 MTM 311311-04
<5.0 05/29/15 LFJ EPA200.7
< 1.0 05/26/15 LFJ EPA200.8
55 06/01/15 JMN 311111-99
ID#: 204 H
DATE COLLECTED: 05/20/15
DATE REPORTED : 07/14/15
REVIEWED BY:

BIAVENglin 1lo [lECErylrgaS
P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
si\A
VOLATILE ORGANICS
EPA METHOD 624
CLIENT ID:
PHONE [phone]
FAX [phone]
204 H
ANALYST: MAO
DATE COLLECTED: 05/20/15
DATE ANALYZED: 05/23/15
DATE REPORTED: 07/14/15
Effluent
PARAMETERS, ug/l
1. Chloromethane
2. Vinyl Chloride
3. Bromomethane
4. Chloroethanc
5. Trichlorofluoromethane
6. 1,1-Dichloroethane
7. Methylene Chloride
8. trans-1,2-Dichloroethene
9. 1,1-Dichloroethene
10. Chloroform
11. 1, I ,1-Trichloroethane
12. Carbon Tetrachloride
13. Benzene
14. 1,2-Dichloroethane
15. Trichloroethene
16. 1,2-Dichloropropane
17. Bromodichloromethane
18. 2-Chloroethylvinyl Ether
19. cis-1,3-Dichloropropene
20. Toluene
21. trans-1 i-Dichloropropene
22. 1,1,2-Trichloroethane
23. Tetrachloroethene
24. Dihromochloromethane
25. Chlorohenzene
26. Ethvlbenzene
27. Bromoform
28. 1,1,2,2= retrachloroethane
29. 1,3-Dichlorobenzene
30. 1,4-Dick lorobenzene
31. 1,2-Dichlorobenzene
32. Acrolein
33. Acrvlonitrile
<10.00
<10.00
<10.00
<10.00
<5.00
<5.00
<10.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
< 5.00
<5.00
<5.00
<5.00
<5.00
< 5.00
<5.00
< 5.00
< 100.00
<50.00

INuQMEO ONC@IT
parmiR@
-.0. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT:
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 873 t
REVIEWED BY:
froabk
r,
SEMIVOLATILE ORGANICS
EPA METHOD 625
CLIENT ID:
204 H
ANALYST: CHS
DATE COLLECTED: 05/20/15
DATE EXTRACTED: 05/22/15
DATE ANALYZED: 06/18/15
DATE REPORTED: 07/14/15
PARAMETERS, ug/I
Effluent
1.
N-Nitrosodimethylamine
< 10.00
2.
Phenol
< 10.00
3.
Bis(2-Chloroethvl) Ether
< 10.00
4.
2-Chlorophenol
< 10.00
5.
1,3-Dichlorobenzene
< 10.00
6.
1,4-Dichlorobenzene
< 10.00
7.
1,2-Dichlorobenzene
< 10.00
8.
Bis(2-Chloroisopropyl) Ether
< 10.00
9.
Hexachloroethane
< 10.00
10.
N-Nitrosodi-N-Propylamine
< 10.00
11.
Nitrobenzene
< 10.00
12.
Isophorone
< 10.00
13.
2-Nitrophenol
< 10.00
14.
2,4-Dbnethylphenol
< 10.00
15.
Bis(2-Chloroethoxy) Methane
< 10.00
16.
2,4-Dichlorophenol
< 10.00
17.
1,2,4-Trichlorobenzene
< 10.00
18.
Naphthalene
< 10.00
19.
Hexachlorobutadiene
< 10.00
20.
4-Chloro-3-Methy!phenol
< 20.00
21.
Hexachlorocvclopentadiene
< 10.00
22.
2.4,6-Trichlorophenol
< 10.00
23.
2-Chloronaphthalene
< 10.00
24.
Acenaphthvlene
< 10.00
25.
Dimethylphthalate
< 10.00
26.
2,6-Dinitrotoulene
< 10.00
27.
Acenaphthene
< 10.00
28.
2,4-Dinitrophenol
< 50.00
29.
4-Nitrophenol
< 50.00
30.
2,4-Dinitrotoluene
< 10.00
31.
Fluorene
< 10.00
32.
Diethylphthalate
< 10.00
33.
4-Chlorophenyl Phenyl Ether
< 10.00
34.
4,6-Dinitro-2-Methylphenol
< 50.00
35.
N-Nitrosodiphenylamine
< 10.00
36.
4-Bromophenyl Phenyl Ether
< 10.00
37.
Hexachlorobenzene
< 10.00
38.
Pentachlorophenol
< 50.00
39.
Phenanthrene
< 10.00
40.
Anthracene
< 10.00
41.
Di-N-Butylphthalate
< 10.00
42.
Fluoranthene
<10.00
43.
Benzidine
< 100.00
44.
Pvrene
< 10.00
45.
Bntylbenz} Iphthlate
< 10.00
46.
Benzola]anthracene
< 10.00
47.
3,3-Dichlorobenzadine
< 10.00
48.
Chrysene
< 10.00
Page: 1

tHdI[FMR@H liampaTak
P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
11,
Drinking water ID: 37715
CLIENT ID:
wastewater ID: 10
PHONE [phone]
FAX [phone]
204 H
ANALYST: CHS
DATE COLLECTED: 05/20/15
DATE EXTRACTED: 05/22/15
DATE ANALYZED: 06/18/15
DATE REPORTED: 07/14/15
Effluent
PARAMETERS, ug/1
49. Bis(2-Ethylhexyl)phthalate
50. Di-N-Octylphthalate
51. Benzo[b]fluoranthene
52. Benzo[lc]fluoranthene
53. Benzo[alpyrene
54. I ndeno(1,2,3-C,d)py rene
55. Dihenzo[a,h]anthracene
56. Benzo[g,h,i]pervlene
57. 1,2-Diphenv lhydrazine
<20.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
Page: 2

Environment 1, Inc.
P.O. Box 7085, 114 Oakmont Dr.
Greenville. NC 27858
CHAIN OF CUSTODY RECORD
Page 1 of
cm -uumenu nu;.CoM
Phone (253 ) 7 56-6205 •Fay
CLIENT: 204 H
CITY OF HAVELOCK
MR. ART HOUGH
(252)7S6-+)G_�
Week: 23
PLANT[21
DISLNTEC.'
[j
I'EON
CE11.OR NL-
uv
NONT
.-
CHLORINE NEUTRALIZED AT COLLECTION
%)4
n
�2�'
`
�
,i</Z
4
,q..
pH CHECK (LAB)
f
PP
PP
GGPP
PP
GGGGGG
CONTAINER TYPE. P/G
WASTEWATER TREATMENT
304 N. JACKSON DRIVE
HAVELOCK NC 28532
[phone]
CCCCCCDC
A
A
A
A
AEEE
CHEMICAL
PRESERVATION
A - NONE D- NAOH
B • HNO, E • HCL
C- H,S0{ F- ZINC ACETATE!NAOH
G - NATHIOSULFATE
TOTAL CHLORINE, nigil
OR will AT COLLECTION
TEMPERATURE. (C
AT COLLECTION
OF CONTAINERS
[irnrnoniaT4tro.
i•
2o
L
E
,
o
I.
c,
E;
g
O
o
�,
4
0
�s
C
Hardness
..41717
H
_T
'
EPA 625
625 Duplicate 1
625 Duplicate 2
EPA 624 (APA)
624 Duplicate 1
624 Duplicate 2
PARAMETE RS/TESTS
COLLECTION
SAMPLE LOCATION
DATE
TIME
Effluent
(IJ/(cS
br 7-►f+Y
•3
.
:,'i
'it,.
ya
,;
.
a
r
#
. ,t
T.:CLASSIFICATION.
Li WASTEWATER(NPOES)
[ji DRINKING WATER
LI DWO'GW
ij SOLID WASTE SECTION
�
—
-,
CHAIN OF CUSTODY
DURING
(SEAL) MAINTAINED
SHIPMENT/DELIVERY
Y N
SAMPLES CO
(Please ring
TE►4BY,
is
•
_
SAMPLES RE EIV i W
LAB AT' 9 'C
REUNQUISHED BY ( tG ( PLER)
ONETIME
H'f-SSMOS
RECE)V D Y (SIG.)
ATE/IME
/oitMr
1
DATEME
I
COMMENTS:SA�
RE UISH G.)
ETME
I
RECEIVED BY I I
RELINOUISHED BY (SIG.)
DATE/PME
1
RECEIVED BY (SIG.)
DATEI1ME
FOAM n5
PLEASE READ Instructions for completing this form on the reverse side.
Sampler must place a "C" for composite sample or a "G" for
Grab sample in the blocks above for each parameter requested. N 2 ( 2 8 4 5

IngoQonno{in �o �
COT (pCIIMIRg
'.0. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
Drinkina Water In. 1171s
Wastewater ID: 10
PHONE (252) 75C -
FAX [phone]t.
CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
PARAMETERS
Ammonia Nitrogen as N, mg/I
Total Kjeldahl Nitrogen as N,mg/I
Nitrate -Nitrite as N, nig/I
Total Phosphorus as P, mg/l
Oil & Grease (HENI), mg/I
Amkk Phenol, ug/I
Total Cyanide, mg/I
Total Hardness, mg/I
Total Dissolved Residue, mg/1
Antimony, ug/I
Arsenic. ug/I
Beryllium, ug/I
Cadmium. ug/I
Total Chromium, ug/I
Copper, ug/I
Lead, ug/I
Nickel, ug/I
Selenium, ug/I
Silver. ug/I
Thallium, ug/I
Zinc, ug/1
Effluent Analysis Method
Date Analyst Code
0.06 02/24/17 AKS 350.1 R2-93
0.91 02/27/17 AKS 351.2 R2-93
1.74 02/24/17 MF 353.2 R2-93
1.26 02/27/17 RAJ 365.4-74
<5 02/24/17 SEJ 1664B
<5 03/01/17 SEJ 420.1-78
<0.005 03/02/17 SEJ 4500CNE-99
105 02/27/17 KKM 2340C-97
444 02/28/17 SDB 2540C-97
<3.0 03/24/17 JMN EPA200.8
<5.0 03/07/17 MTM 3113B-04
2 03/06/17 LFJ EPA200.7
< 1.0 03/08/17 MTM 3113B-04
<5.0 03/06/17 LFJ EPA200.7
< 10 03/06/17 LFJ EPA200.7
<5.0 03/09/17 MTM 3113B-04
< 10 03/06/17 LFJ EPA200.7
< 10 03/15/17 MTM 3113B-04
<5.0 03/06/17 LFJ EPA200.7
< 1.0 03/24/17 JMN EPA200.8
70 03/06/17 LFJ EPA200.7
ID#: 204 H
DATE COLLECTED: 02/23/17
DATE REPORTED : 04/03/17

lawilmangER
-o
[1:1TememW
P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
VOLATILE ORGANICS
EPA METHOD 624
CLIENT ID:
PHONE [phone]L
FAX [phone]
204 H
ANALYST: MAO
DATE COLLECTED: 02/23/17
DATE ANALYZED: 03/08/17
DATE REPORTED: 04/03/17
Effluent
PARAMETERS, ug/l
1. Chloromethane
2. Vinyl Chloride
3. Bromomethane
4. Chloroethane
5. Trichlorofluoromethane
6. 1,1-Dichloroethane
7. Methylene Chloride
8. trans-1,2-Dichloroethene
9. 1,1-Dichloroethene
10. Chloroform
11. 1,1,1-Trichloroethane
12. Carbon Tetrachloride
13. Benzene
14. 1,2-Dichloroethane
15. Trichloroethene
16. 1,2-Dichloropropane
17. Bromodichloromethane
18. 2-Chloroethybrinyl Ether
19. cis-I,3-Dichloropropene
20. Toluene
21. trans-1,3-Dichloropropene
22. 1,1,2-7'richloroethane
23. Tetrachloroethene
24. Dibromochloromethane
25. Chlorobenzene
26. Ethylbenzene
27. Bromoform
28. 1,1,2,2-Tetrachloroethane
29. 1,3-Dichlorobenzene
30. 1,4-Dichlorobenzene
31. 1,2-Dichlorobenzene
32. Acrolein
33. Acrylonitrile
< 10.00
< 10.00
< 10.00
< 10.00
<5.00
< 5.00
< 10.00
<5.00
< 5.00
< 5.00
<5.00
< 5.00
<5.00
<5.00
<5.00
<5.00
<5.00
<5.00
< 5.00
<5.00
< 5.00
< 5.00
<5.00
<5.00
<5.00
< 5.00
< 5.00
<5.00
< 5.00
<5.00
< 5.00
< 100.00
<50.00

11ll Flo Ilacupurak
'.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
PHONE [phone]
FAX [phone]
CLIENT ID: 204 H
ANALYST: JAP
DATE COLLECTED: 02/23/17
DATE EXTRACTED: 02/27/17
DATE ANALYZED: 03/02/17
DATE REPORTED: 04/03/17
PARAMETERS, ug/1
Effluent
1. N-Nitrosodimethylamine
<10.00
2. Phenol
<10.00
3. Bis(2-Chloroethyl) Ether
<10.00
4. 2-Chlorophenol
<10.00
5. 1,3-Dichlorobenzene
<10.00
6. 1.4-Dichlorobenzene
<10.00
7. 1,2-Dichlorobenzene
<10.00
8. Bis(2-Chloro-l-methylethvl) Ether
<10.00
9. Hexachloroethane
<10.00
0. N-Nitrosodi-N-Propylamine
<10.00
1. Nitrobenzene
<10.00
2. Isophorone
<10.00
3. 2-Nitrophenol
<10.00
4. 2,4-Dimethvlphenol
<10.00
5. Bis(2-Chloroethoxy) Methane
<10.00
6. 2,4-Dichlorophenol
<10.00
7. 1,2,4-Trichlorobenzene
<10.00
8. Naphthalene
<10.00
9. Hexachlorobutadiene
<10.00
20. 4-Chloro-3-Methylphenol
<20.00
21. Hexachlorocyclopentadiene
<10.00
22. 2,4,6-Trichlorophenol
<10.00
23. 2-Chloronaphthalene
<10.00
24. Acenaphthylene
<10.00
25. Dimethylphthalate
<10.00
26. 2.6-Dinitrotoulene
<10.00
27. Acenaphthene
<10.00
28. 2,4-Dinitrophenol
<50.00
29. 4-Nitrophenol
<50.00
30. 2,4-Dinitrotoluene
<10.00
31. Fluorene
<10.00
32. Diethylphthalate
<10.00
33. 4-Chloropheny 1 Phenyl Ether
<10.00
34. 4,6-Dinitro-2-Methylphenol
<50.00
35. N-Nitrosodiphenylamine
<10.00
36. 4-Bromophenyl Phenyl Ether
<10.00
37. Hexachlorobenzene
<10.00
38. Pentachlorophenol
<50.00
39. Phenanthrene
<10.00
40. Anthracene
<10.00
41. Di-N-Butylphthalate
<10.00
42. Fluoranthene
<10.00
43. Benzidine
<100.00
44. Py rene
<10.00
45. Butylbenzylphthlate
<10.00
46. Benzo[alanthracene
<10.00
47. 3,3-Dichlorohenzadine
<10.00
48. Chrysene
<10.00
Page: 1

BARI-EMIR Flo [Inc©Tpumb,d
.nki nn wah.r i
P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N.C. 27835-7085
CLIENT: CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, N28532
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
wastewater ID:
PHONE [phone],
FAX [phone]
CLIENT ID: 204 H
ANALYST: JAP
DATE COLLECTED: 02/23/17
DATE EXTRACTED: 02/27/17
DATE ANALYZED: 03/02/17
DATE REPORTED: 04/03/17
Effluent
PARAN1ETERS, ug/I
49. Bis(2-Ethylhexyl)phthalate
50. Di-N-Octylphthalate
51. Benzolb]fluoranthene
52. Benzo[k]tluoranthene
53. Benzo[a]pvrene
54. lndeno(1,2,3-C,d)pyrene
55. Dibenzo[a,h]anthracene
56. Benzo[g,h,i]perylene
57. 1,2-Diphenvlhydrazine
<20.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
<10.00
Page: 2

Environment I.
P.O. L'ox 7085. 114 Oakmont Dr.
Greenville. NC 27858
CHAIN OF CU! ))DY RECORD
Page I of
environment I Inc .com
Phone (_25 21 756-6208 • Fax [phone]
CLIENT: 204 H Week: 12
CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK NC 28532
[phone]
I)Iti1NI
1 CTION
CHLORINF
LC) �
,
CHLORINE NEUTRALIZED AT COLLECTION
IA
U V
'-�_
/
, ,�r
,�
�2�{
,�
�;
2
1!_
-2
pH CHECK (LAB)
P
P
I'
(.
I;
(;
(.
G
G
CONTAINER TYPE. PiG
❑
NONE
I>
I'
P
P
(;
G
I,
CCCCCCDC
A
A
A
\
A
E
E
i.
CHEMICAL PRESERVATION
TOTAL CHLORINE. mgil
OR ug/l AT COLLECTION
TEMPERATURE. 'C
AT COLLECTION
# OF CONTAINERS
r
z
5
°
.Zs
4
—
r
=_
^
c
_
W
p
-
_
_
J
=
C.;'
r
c
-
;f
7
EPA 625
—
=
N
'�
=
=
N
EPA 624 (APA)
624 Duplicate 1
624 Duplicate 2 1
PARAMETERS/TESTS
A - NONE D -NAOH
B - HNO3 E - HCL
C- H.SO, F- ZINC ACETATE/NAOH
G - NA THIOSULFATE
COLLECTION
SAMPLE LOCATION
DATE
TIME
Emuenl
12y 0
IDS
-3
14
C
r
C
'-
~
-
C'
C
C
.
CI
C
CLASSIFICATION:
WASTEWATER(NPDESI
DRINKING WATER
DWQ:'GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
CD N
SAMPLES COLLECTED BY
Pnnt)
(Please
yq�7 7�f S
SAMPLES RECEIVED IN LAB AT Z• fs- °C
COMMENTS.
RELINQUISHED BY (SIG.) (SAMPLER)
�QUISHED
/� DATETIME
j1. 3 r
l 1!
RECEIV )SIG.)
Z ATE'TIME
/23/01
DATETIME
Z�
BY (SIG.)
uH��ME
RECEIVED BY SIG.
RELINQUISHED BY (SIG.)
DATETIME
1
RECEIVED BY (SIG )
DATE/TIME
1
FORM 05
PLEASE READ Instructions for completing this form on the reverse side.
Sampler must place a C" for composite sample or a "G•• for
Grab sample in the blocks above for each parameter requested.
N° 328183

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Second Species Toxicity Testing Results 2017-2018
(Results will be submitted prior to the expiration of the existing NPDES Permit on 6/30/2018)

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Exceptionally Performing Facilities, Reduction of Monitoring Frequency Analysis
t

Attachment A
Calculations for the City of Havelock WWTP Effluent Data for Monitoring Frequency Reduction Analysis
NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
Date
BODS (Summer) BODS (Winter)
TSS
Units
mg/L
mR/L
mI.
ma/L
me/L
#/100 mL
3-year average
2.58
3.41
2.60
0.12
0.08
1.92
No. data points
446.00
289.00
734.00
446.00
289.00
717.00
Monthly
Average Permit
5
10
30
0.5
1
35
Limit
Avg % of Permit
Limit
52%
34%
9%
24%
8%
5%
Sampling Results
11
9
0
4
0
2
> 200% of PL
Weekly Average
Permit Limit
7.5
15
45
1.5
3
276
Weekly Average
0
3
0
0
0
0
Violations in Past
Year

Attachment B
City of Havelock WWTP NPDES Permit Renewal Discharge Monitoring Report Data
10/1/2014 to 9/30/2017
Date BOD5 (Summer) BOD5 (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
Units mg/L mg/L . mg/L mg/L mg/L #/100 mL
10/1/2014
<2.0
<2.5
0.08
2
10/2/2014
<2.0
<2.5
0.11
<1
10/3/2014
<2.0
<2.5
<0.04
<1
10/4/2014
10/5/2014
10/6/2014
<2.0
<2.5
<0.04
<1
10/7/2014
<2.0
<2.5
<0.04
1
10/8/2014
<2.0
2.7
0.06
<1
10/9/2014
<2.0
<2.5
0.07
1
10/10/2014
2.9
<2.5
<0.04
1
10/11/2014
10/12/2014
10/13/2014
<2.0
3.8
<0.04
<1
10/14/2014
<2.0
<2.5
<0.04
<1
10/15/2014
<2.0
<2.5
0.08
<1
10/16/2014
<2.0
<2.5
<0.04
<1
10/17/2014
<2.0
<2.5
<0.04
1
10/18/2014
10/19/2014
10/20/2014
<2.0
<2.5
0.27
<1
10/21/2014
<2.0
<2.5
<0.04
3
10/22/2014
<2.0
<2.5
0.27
1
10/23/2014
<2.0
<2.5
0.07
1
10/24/2014
<2.0
<2.5
0.07
2
10/25/2014
10/26/2014
10/27/2014
<2.0
<2.5
0.05
<1
10/28/2014
<2.0
<2.5
0.05
3
10/29/2014
<2.0
<2.5
0.06
2
10/30/2014
<2.0
<2.5
0.07
3
10/31/2014
<2.0
<2.5
0.04
5
11/1/2014
11/2/2014
11/3/2014
3.2
<2.5
<0.04
1
11/4/2014
2.8
<2.5
0.06
5
11/5/2014
<2.0
<2.5
0.05
5
11/6/2014
<2.0
<2.5
0.07
1
11/7/2014
<2.0
<2.5
0.12
1
11/8/2014
11/9/2014
11/10/2014
2.5
<2.5
0.06
1
11/11/2014
11/12/2014
<2.0
<2.5
0.04
<1
11/13/2014
<2.0
<2.5
0.04
1
11/14/2014
3.6
<2.5
0.06
35
11/15/2014
11/16/2014
11/17/2014
11/18/2014
11/19/2014

NH3-N
Date BODS (Summer) BODS (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
11/20/2014
11/21/2014
11/22/2014
11/23/2014
11/24/2014
11/25/2014
11/26/2014
11/27/2014
11/28/2014
11/29/2014
11/30/2014
12/1/2014
2.9
6.0
0.06
<1
12/2/2014
<2.0
<2.5
0.07
<1
12/3/2014
<2.0
<2.5
0.04
2
12/4/2014
6.3
<2.5
<0.04
520
12/5/2014
<2.0
<2.5
0.06
11
12/6/2014
12/7/2014
12/8/2014
<2.0
<2.5
1.76
1
12/9/2014
<2.0
<2.5
0.33
<1
12/10/2014
3.0
<2.5
0.05
<1
12/11/2014
<2.0
<2.5
0.13
2
12/12/2014
<2.0
<2.5
0.11
14
12/13/2014
12/14/2014
12/15/2014
<2.0
<2.5
0.13
2
12/16/2014
<2.0
<2.5
0.14
<1
12/17/2014
<2.0
<2.5
0.11
<1
12/18/2014
<2.0
<2.5
<0.04
1
12/19/2014
<2.0
<2.5
<0.04
<1
12/20/2014
12/21/2014
12/22/2014
<2.0
<2.5
<0.04
<1
12/23/2014
2.5
<2.5
<0.04
7
12/24/2014
<2.0
<2.5
0.08
1
12/25/2014
12/26/2014
12/27/2014
12/28/2014
12/29/2014
<2.0
<2.5
0.07
1
12/30/2014
<2.0
<2.5
<0.04
2
12/31/2014
1/1/2015
1/2/2015
<2.0
<2.5
<0.04
<1
1/3/2015
1/4/2015
1/5/2015
<2.0
<2.5
0.04
1
1/6/2015
<2.0
<2.5
<0.04
3
1/7/2015
<2.0
<2.5
<0.04
3
1/8/2015
2.6
<2.5
<0.04
1
1/9/2015
<2.0
<2.5
0.04
1
1/10/2015
1/11/2015
1/12/2015
<2.0
<2.5
0.07
<1

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
1/13/2015
<2.0
<2.5
0.06
<1
1/14/2015
<2.0
<2.5
0.09
2
1/15/2015
<2.0
<2.5
<0.04
1
1/16/2015
<2.0
<2.5
<0.04
<1
1/17/2015
1/18/2015
1/19/2015
1/20/2015
<2.0
<2.5
0.11
<1
1/21/2015
<2.0
<2.5
0.23
<1
1/22/2015
<2.0
<2.5
<0.04
<1
1/23/2015
<2.0
<2.5
<0.04
<1
1/24/2015
1/25/2015
_ 1/26/2015
<2.0
<2.5
<0.04
1
1/27/2015
<2.0
<2.5
_
0.07
<1
1/28/2015
3.2
<2.5
0.10
8
_
1/29/2015
<2.0
<2.5
_
0.27
1
1/30/2015
<2.0
<2.5
<0.04
<1
1/31/2015
2/1/2015
2/2/2015
2/3/2015
<2.0
<2.5
<0.04
<1
2/4/2015
<2.0
<2.5
0.30
<1
2/5/2015
<2.0
11.0
0.11
1
2/6/2015
<2.0
<2.5
0.09
<1
2/7/2015
2/8/2015
2/9/2015
<2.0
<2.5
0.07
<1
2/10/2015
<2.0
<2.5
0.09
<1
2/11/2015
<2.0
<2.5
<0.04
<1
2/12/2015
<2.0
<2.5
0.09
1
2/13/2015
<2.0
<2.5
<0.04
5
2/14/2015
2/15/2015
2/16/2015
<2.0
<2.5
0.07
<1
2/17/2015
2.9
3.4
<0.04
5
2/18/2015
<2.0
<2.5
<0.04
<1
2/19/2015
<2.0
<2.5
<0.04
<1
2/20/2015
2/21/2015
2/22/2015
2/23/2015
2/24/2015
2/25/2015
2/26/2015
<2.0
<2.5
<0.04
1
2/27/2015
<2.0
<2.5
0.10
<1
2/28/2015
3/1/2015
3/2/2015
<2.0
<2.5
<0.04
<1
3/3/2015
<2.0
<2.5
0.05
<1
3/4/2015
<2.0
<2.5
0.05
<1
3/5/2015
<2.0
<2.5
0.08
1
3/6/2015
<2.0
<2.5
0.19
1
3/7/2015

NH3-N
Date BOD5 (Summer) BOD5 (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
3/8/2015
3/9/2015
<2.0
<2.5
0.20
<1
3/10/2015
<2.0
<2.5
<0.04
<1
3/11/2015
2.9
<2.5
0.10
<1
3/12/2015
<2.0
<2.5
<0.04
1
3/13/2015
<2.0
<2.5
0.06
<1
3/14/2015
3/15/2015
3/16/2015
<2.0
<2.5
0.13
<1
3/17/2015
<2.0
<2.5
0.11
<1
3/18/2015
<2.0
<2.5
0.63
<1
3/19/2015
<2.0
<2.5
0.63
<1
3/20/2015
<2.0
<2.5
0.20
2
3/21/2015
3/22/2015
3/23/2015
<2.0
<2.5
0.10
<1
3/24/2015
7.2
<2.5
0.11
<1
3/25/2015
<2.0
<2.5
0.13
<1
3/26/2015
<2.0
<2.5
0.07
<1
3/27/2015
<2.0
<2.5
0.07
<1
3/28/2015
3/29/2015
3/30/2015
<2.0
<2.5
<0.04
<1
3/31/2015
<2.0
<2.5
<0.04
<1
4/1/2015
<2.0
<2.5
0.07
<1
4/2/2015
<2.0
<2.5
0.10
4
4/3/2015
4/4/2015
4/5/2015
4/6/2015
<2.0
<2.5
0.37
<1
4/7/2015
<2.0
<2.5
0.11
<1
4/8/2015
<2.0
<2.5
0.07
<1
4/9/2015
<2.0
<2.5
0.11
3
4/10/2015
<2.0
<2.5
0.08
3
4/11/2015
4/12/2015
4/13/2015
<2.0
<2.5
0.14
0
4/14/2015
<2.0
<2.5
0.20
3
4/15/2015
2.2
<2.5
0.13
<1
4/16/2015
<2.0
<2.5
0.06
<1
4/17/2015
<2.0
<2.5
0.06
<1
4/18/2015
4/19/2015
4/20/2015
11.0
<2.5
0.08
1
4/21/2015
12.0
<2.5
<0.04
<1
4/22/2015
>15*
<2.5
<0.04
3
4/23/2015
>11*
<2.5
0.10
6
4/24/2015
4/25/2015
4/26/2015
4/27/2015
<2.0
<2.5
0.12
<1
4/28/2015
5.5
<2.5
0.14
<1
4/29/2015
<2.0
<2.5
0.09
<1
4/30/2015
<2.0
<2.5
0.08
12

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
5/1/2015
<2
<2.5
0.06
2
5/2/2015
5/3/2015
5/4/2015
< 2
< 2.5
0.06
<1
5/5/2015
< 2
< 2.5
0.09
<1
5/6/2015
< 2
< 2.5
0.08
8
5/7/2015
2.5
< 2.5
0.11
1
5/8/2015
< 2
< 2.5
0.2
4
5/9/2015
5/10/2015
5/11/2015
< 2
< 2.5
0.11
17
5/12/2015
< 2
< 2.5
0.18
5/13/2015
< 2
< 2.5
0.17
1
5/14/2015
< 2
< 2.5
< 0.04
< 1
5/15/2015
2.7
< 2.5
0.18
< 1
5/16/2015
5/17/2015
5/18/2015
2.1
< 2.5
0.05
<1
5/19/2015
< 2
< 2.5
< 0.04
< 1
5/20/2015
3.5
8.3
< 0.07
2
5/21/2015
< 2
< 2.5
< 0.04
3
5/22/2015
< 2
< 2.5
0.06
< 1
5/23/2015
5/24/2015
5/25/2015
5/26/2015
3.4
< 2.5
< 0.04
5
5/27/2015
< 2
< 2.5
0.91
4
5/28/2015
< 2
< 2.5
0.07
2
5/29/2015
<2
<2.5
0.08
< 1
5/30/2015
5/31/2015
6/1/2015
> 26
3.5
0.08
1
6/2/2015
> 13
< 2.5
0.07
1
6/3/2015
> 13
< 2.5
0.1
2
6/4/2015
> 13
< 2.5
0.09
3
6/5/2015
> 13
<2.5
0.07
6/6/2015
6/7/2015
6/8/2015
2.5
<2.5
0.11
3
6/9/2015
<2
<2.5
0.05
< 1
6/10/2015
< 2
< 2.5
0.05
3
6/11/2015
< 2
< 2.5
< 0.04
6
6/12/2015
<2
<2.5
0.1
1
6/13/2015
6/14/2015
6/15/2015
< 2
< 2.5
0.09
5
6/16/2015
<2
<2.5
0.13
3
6/17/2015
<2
<2.5
0.12
23
6/18/2015
<2
<2.5
0.07
5
6/19/2015
<2
<2.5
0.06
< 1
6/20/2015
6/21/2015
6/22/2015
< 2
< 2.5
< 0.04
9
6/23/2015
<2
<2.5
0.19
6

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
6/24/2015
< 2
< 2.5
0.15
6
6/25/2015
<2
<2.5
0.05
3
6/26/2015
<2
<2.5
0.06
6
6/27/2015
6/28/2015
6/29/2015
<2
<2.5
< 0.04
8
6/30/2015
<2
<2.5
0.05
6
7/1/2015
<2
<2.5
0.06
10
7/2/2015
<2
< 2.5
0.07
4
7/3/2015
7/4/2015
7/5/2015
7/6/2015
<2
<2.5
<0.04
17
7/7/2015
<2
<2.5
<0.04
36
7/8/2015
<2
<2.5
0.07
7
7/9/2015
<2
<2.5
0.06
5
7/10/2015
<2
<2.5
0.08
7
7/11/2015
7/12/2015
7/13/2015
<2
<2.5
<0.04
48
7/14/2015
2.3
<2.5
< 0.04
11
7/15/2015
<2
<2.5
<0.04
5
7/16/2015
<2
<2.5
0.19
207
7/17/2015
<2
<2.5
0.07
1
7/18/2015
7/19/2015
7/20/2015
<2
<2.5
0.06
<1
7/21/2015
<2
<2.5
0.12
2
7/22/2015
<2
<2.5
0.1
30
7/23/2015
<2
<2.5
0.12
19
7/24/2015
5.9
5.3
0.36
7
7/25/2015
7/26/2015
7/27/2015
< 2
<2.5
0.12
3
7/28/2015
< 2
<2.5
11
2
7/29/2015
<2
<2.5
0.13
12
7/30/2015
<2
<2.5
0.11
121
7/31/2015
<2
<2.5
0.09
35
8/1/2015
8/2/2015
8/3/2015
<2
<2.5
0.05
8/4/2015
<2
<2.5
0.06
6
8/5/2015
<2
<2.5
<0.04
1
8/6/2015
< 2
<2.5
0.11
1
8/7/2015
<2
<2.5
1.77
8/8/2015
8/9/2015
8/10/2015
<2
<2.5
0.07
17
8/11/2015
<2
<2.5
0.07
12
8/12/2015
<2
<2.5
< 0.04
9
8/13/2015
<2
<2.5
0.05
3
8/14/2015
< 2
<2.5
0.04
8/15/2015
8/16/2015

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
8/17/2015
<2
<2.5
0.09
8/18/2015
<2
<2.5
0.08
2
8/19/2015
< 2
< 2.5
0.08
8/20/2015
<2
<2.5
<0.04
5
8/21/2015
<2
<2.5
0.08
< 1
8/22/2015
8/23/2015
8/24/2015
<2
<2.5
0.07
3
8/25/2015
< 2
< 2.5 .
0.07
3
8/26/2015
<2
<2.5
0.07
1
8/27/2015
<2
<2.5
0.08
2
8/28/2015
<2
<2.5
0.07
1
8/29/2015
8/30/2015
8/31/2015
<2
<2.5
0.08
21
9/1/2015
<2
<2.5
0.09
12
9/2/2015
<2
<2.5
0.11
9/3/2015
< 2
< 2.5
0.08
1
9/4/2015
<2
<2.5
0.08
9/5/2015
9/6/2015
9/7/2015
9/8/2015
<2
<2.5
0.12
1
9/9/2015
< 2
< 2.5
3.31
2
9/10/2015
<2
<2.5
0.1
1
9/11/2015
<2
<2.5
0.08
2
9/12/2015
9/13/2015
9/14/2015
2
< 2.5
< 0.04
3
9/15/2015
< 2
< 2.5
0.04
10
9/16/2015
< 2
< 2.5
0.04
4
9/17/2015
<2
<2.5
<0.04
6
9/18/2015
<2
<2.5
<0.04
2
9/19/2015
9/20/2015
9/21/2015
< 2
< 2.5
< 0.09
9/22/2015
< 2
< 2.5
1.7
2
9/23/2015
2.1
<2.5
0.26
1
9/24/2015
<2
<2.5
<0.04
9/25/2015
<2
<2.5
<0.04
9/26/2015
9/27/2015
9/28/2015
<2
<2.5
<0.04
9/29/2015
2.2
3
0.04
< 1
9/30/2015
< 2
< 2.5
< 0.04
3
10/1/2015
< 2
< 2.5
< 0.04
5
10/2/2015
< 2
< 2.5
< 0.04
3
10/3/2015
10/4/2015
10/5/2015
< 2
< 2.5
< 0.04
6
10/6/2015
< 2
< 2.5
< 0.04
4
10/7/2015
< 2
< 2.5
0.34
1
10/8/2015
< 2
< 2.5
< 0.04
< 1
10/9/2015
< 2
< 2.5
< 0.04
<1

NH3-N
Date BODS (Summer) BODS (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
10/10/2015
10/11/2015
10/12/2015
<2
<2.5
<0.04
<1
10/13/2015
< 2
< 2.5
0.17
< 1
10/14/2015
< 2
< 2.5
0.04
<1
10/15/2015
< 2
< 2.5
0.06
2
10/16/2015
< 2
< 2.5
0.06
< 1
10/17/2015
10/18/2015
.
10/19/2015
< 2
< 2.5
0.07
8
10/20/2015
< 2
< 2.5
0.07
4
10/21/2015
< 2
<2.5
0.10
<1
10/22/2015
< 2
< 2.5
< 0.04
< 1
10/23/2015
< 2
< 2.5
0.05
2
10/24/2015
10/25/2015
10/26/2015
< 2
< 2.5
0.05
< 1
10/27/2015
< 2
< 2.5
0.06
1
10/28/2015
< 2
< 2.5
0.05
1
10/29/2015
< 2
< 2.5
0.05
<1
10/30/2015
< 2
< 2.5
0.09
< 1
10/31/2015
11/1/2015
11/2/2015
< 2
< 2.5
0.04
4
11/3/2015
<2
<2.5
0.14
3
11/4/2015
< 2
< 2.5
0.05
2
11/5/2015
< 2
< 2.5
< 0.04
1
11/6/2015
< 2
< 2.5
0.04
< 1
11/7/2015
11/8/2015
11/9/2015
<2
<2.5
<0.04
11/10/2015
< 2
< 2.5
< 0.04
2
11/11/2015
11/12/2015
< 2
< 2.5
< 0.04
11/13/2015
< 2
< 2.5
< 0.04
< 1
11/14/2015
11/15/2015
11/16/2015
< 2
< 2.5
< 0.04
<1
11/17/2015
<2
<2.5
<0.04
<1
11/18/2015
2.4
< 2.5
0.4
<1
11/19/2015
< 2
< 2.5
0.05
0
11/20/2015
<2
< 2.5
0.04
2
11/21/2015
11/22/2015
11/23/2015
< 2
< 2.5
0.07
< 1
11/24/2015
< 2
< 2.5
< 0.04
11/25/2015
< 2
< 2.5
< 0.04
1
11/26/2015
14
11/27/2015
11/28/2015
11/29/2015
11/30/2015
<2
<2.5
0.07
<1
12/1/2015
< 2
<2.5
< 0.04
<1
12/2/2015
<2
<2.5
0.04
4

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
12/3/2015
<2
<2.5
<0.04
2
12/4/2015
<2
< 2.5
<0.04
3
12/5/2015
12/6/2015
12/7/2015
3.2
<2.5
0.04
2
12/8/2015
< 2
< 2.5
0.05
< 1
12/9/2015
<2
<2.5
<0.04
<1
_
12/10/2015
<2
<2.5
<0.04
<1
12/11/2015
< 2
< 2.5
< 0.04
< 1
12/12/2015
12/13/2015
12/14/2015
<2
<2.5
<0.04
1
12/15/2015
< 2
< 2.5
< 0.04
1
12/16/2015
<2
<2.5
<0.04
< 1
12/17/2015
< 2
< 2.5
< 0.04
1
12/18/2015
< 2
< 2.5
< 0.04
< 1
12/19/2015
12/20/2015
12/21/2015
< 2
< 2.5
<0.04
< 1
12/22/2015
< 2
< 2.5
< 0.04
< 1
12/23/2015
< 2
< 2.5
< 0.04
< 1
12/24/2015
12/25/2015
12/26/2015
12/27/2015
12/28/2015
2.5
< 2.5
< 0.04
1
12/29/2015
< 2
< 2.5
< 0.04
<1
12/30/2015
< 2
< 2.5
< 0.04
1
12/31/2015
< 2
< 2.5
< 0.04
< 1
1/1/2016
1/2/2016
1/3/2016
1/4/2016
< 2
< 2.5
< 0.04
< 1
1/5/2016
4
< 2.5
< 0.04
1
1/6/2016
< 2
< 2.5
< 0.04
< 1
1/7/2016
<2
< 2.5
< 0.04
1
1/8/2016
<2
< 2.5
< 0.04
1
1/9/2016
1/10/2016
1/11/2016
< 2
< 2.5
< 0.04
<1
1/12/2016
< 2
< 2.5
0.05
<1
1/13/2016
< 2
< 2.5
0.07
< 1
1/14/2016
<2
<2.5
<0.04
1
1/15/2016
<2
< 2.5
< 0.04
< 1
1/16/2016
1/17/2016
1/18/2016
1/19/2016
<2
< 2.5
< 0.04
< 1
1/20/2016
< 2
< 2.5
< 0.04
2
1/21/2016
< 2
< 2.5
< 0.04
< 1
1/22/2016
<2
< 2.5
<0.04
< 1
1/23/2016
1/24/2016
1/25/2016
<2
< 2.5
<0.04
11

NH3-N
Date BODS (Summer) BODS (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
1/26/2016
<2
<2.5
<0.04
2
1/27/2016
< 2
< 2.5
< 0.64
4
1/28/2016
8.3
0.0811
5
1/29/2016
2.6
< 2.5
0.06
20
1/30/2016
1/31/2016
2/1/2016
< 2
< 2.5
0.09
649
2/2/2016
6.7
10
0.18
6
2/3/2016
< 2
< 2.5
0.06
1
2/4/2016
4
6.5
0.18
10
2/5/2016
<2
2.7
0.12
9
2/6/2016
2/7/2016
2/8/2016
< 2
< 2.5
< 0.04
1
2/9/2016
< 2
10
0.04
< 1
2/10/2016
< 2
< 2.5
< 0.04
1
2/11/2016
< 2
< 2.5
< 0.04
1
2/12/2016
< 2
< 2.5
< 0.04
1
2/13/2016
2/14/2016
2/15/2016
<2
< 2.5
0.11
< 1
2/16/2016
< 2
< 2.5
0.05
2
2/17/2016
<2
< 2.5
<0.04
< 1
2/18/2016 •
< 2
< 2.5
0.07
1
2/19/2016
< 2
< 2.5
0.05
1
2/20/2016
2/21/2016
2/22/2016
<2
< 2.5
0.05
< 1
2/23/2016
<2
< 2.5
0.05
< 1
2/24/2016
< 2
< 2.5
0.07
2
2/25/2016
< 2
< 2.5
0.06
1
2/26/2016
< 2
< 2.5
0.09
1
2/27/2016
2/28/2016
2/29/2016
4
< 2.5
0.05
1
3/1/2016
< 2
< 2.5
0.07
1
3/2/2016
3.5
< 2.5
0.06
1
3/3/2016
< 2
< 2.5
0.06
< 1
3/4/2016
< 2
< 2.5
0.04
< 1
3/5/2016
3/6/2016
3/7/2016
< 2
< 2.5
< 0.04
1
3/8/2016
< 2
< 2.5
0.05
< 1
3/9/2016
< 2
< 2.5
0.07
24
3/10/2016
< 2
< 2.5
0.05
< 1
3/11/2016
< 2
3.7
0.06
< 1
3/12/2016
3/13/2016
3/14/2016
< 2
< 2.5
0.05
< 1
3/15/2016
< 2
< 2.5
0.08
1
3/16/2016
3.7
< 2.5
0.09
1
3/17/2016
< 2
< 2.5
0.04
< I.
3/18/2016
< 2
< 2.5
0.07
2
3/19/2016

Date BODS (Summer) BOD5 (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
3/20/2016
3/21/2016
< 2
< 2.5
0.14
< 1
3/22/2016
< 2
< 2.5
0.08
< 1
3/23/2016
< 2
< 2.5
0.05
1
3/24/2016
< 2
< 2.5
0.05
< 1
3/25/2016
3/26/2016
3/27/2016
3/28/2016
< 2
< 3.1
0.09
4
3/29/2016
2.6
< 2.5
0.1
< 1
3/30/2016
< 2
< 2.5
0.1
1
3/31/2016
< 2
< 2.5
0.07
<1
4/1/2016
<2
< 2.5
0.08
1210
4/2/2016
4/3/2016
4/4/2016
<2
< 2.5
0.06
<1
4/5/2016
<2
< 2.5
0.09
<1
4/6/2016
<2
< 2.5
0.05
<1
4/7/2016
<2
< 2.5
0.05
1
4/8/2016
2.30
< 2.5
< 0.04
1
4/9/2016
4/10/2016
4/11/2016
<2
< 2.5
0.06
<1
4/12/2016
<2
< 2.5
0.06
2
4/13/2016
<2
< 2.5
0.07
<1
4/14/2016
<2
< 2.5
0.04
<1
4/15/2016
<2
< 2.5
0.07
<1
4/16/2016
4/17/2016
4/18/2016
2.40
< 2.5
0.05
2
4/19/2016
<2
< 2.5
0.06
<1
4/20/2016
<2
< 2.5
0.09
<1
4/21/2016
<2
< 2.5
0.07
<1
4/22/2016
<2
< 2.5
0.12
<1
4/23/2016
4/24/2016
4/25/2016
2.70
< 2.5
0.080
<1
4/26/2016
<2
< 2.5
0.08
<1
4/27/2016
<2
< 2.5
0.08
<1
4/28/2016
<2
< 2.5
0.19
1
4/29/2016
<2
< 2.5
0.06
1
4/30/2016
5/1/2016
5/2/2016
<2
<2.5
0.07
<1
5/3/2016
<2
< 2.5
0.07
1
5/4/2016
<2
<2.5
0.04
1
5/5/2016
< 2
< 2.5
0.04
<1
5/6/2016
<2
<2.5
<0.04
2
5/7/2016
5/8/2016
5/9/2016
3.7
< 2.5
< 0.04
<1
5/10/2016
< 2
< 2.5
0.05
<1
5/11/2016
<2
< 2.5
0.05
2
5/12/2016
< 2
< 2.5
< 0.04
<1

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
5/13/2016
<2
<2.5
0.05
4
5/14/2016
5/15/2016
5/16/2016
2.5
4
0.09
2
5/17/2016
< 2
< 2.5
0.04
3
5/18/2016
< 2
< 2.5
<0.04
<1
5/19/2016
< 2
< 2.5
<0.04
3
5/20/2016
2.2
< 2.5
0.07
1 •
5/21/2016
5/22/2016
5/23/2016
< 2
< 2.5
0.06
<1
5/24/2016
< 2
< 2.5
0.07
1
5/25/2016
<2
<2.5
0.05
<1
5/26/2016
2.6
< 2.5
0.06
2
5/27/2016
<2
< 2.5
0.07
2
5/28/2016
5/29/2016
5/30/2016
5/31/2016
2.8
<2.5
0.08
10
6/1/2016
2.2
<2.5
0.05
<1
6/2/2016
3.4
<2.5
0.05
<1
6/3/2016
3.9
<2.5
< 0.04
<1
6/4/2016
6/5/2016
6/6/2016
4
<2.5
0.08
9
6/7/2016
3.3
<2.5
0.11
3
6/8/2016
3
<2.5
0.04
4
6/9/2016
<2
<2.5
< 0.04
1
6/10/2016
2.2
<2.5
< 0.04
1
6/11/2016
6/12/2016
6/13/2016
3
<2.5
< 0.04
2
6/14/2016
<2
<2.5
< 0.04
7
6/15/2016
<2
<2.5
0
<1
6/16/2016
2.5
<2.5
0.06
326
6/17/2016
<2
<2.5
< 0.04
1
6/18/2016
6/19/2016
6/20/2016
11
<2.5
0.06
1
6/21/2016
< 2
<2.5
0.07
3
6/22/2016
< 2
<2.5
0.08
5
6/23/2016
< 2
<2.5
0.12
2
6/24/2016
< 2
<2.5
0.16
2
6/25/2016
6/26/2016
6/27/2016
2.6
<2.5
0.08
2
6/28/2016
< 2
<2.5
0.07
1
6/29/2016
<2
<2.5
0.06
<1
6/30/2016
3.5
<2.5
0.05
1
7/1/2016
<2
<2.5
0.05
3
7/2/2016
7/3/2016
7/4/2016
7/5/2016
7.4
< 2.5
0.16
7

NH3-N
Date BODS (Summer) BOD5 (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
7/6/2016
< 2
< 2.5
0.11
8
7/7/2016
2.2
< 2.5
< 0.04
4
7/8/2016
< 2
< 2.5
0.09
3
7/9/2016
7/10/2016
7/11/2016
< 2
< 2.5
0.26
4
7/12/2016
< 2
< 2.5
0.07
3
7/13/2016
< 2
< 2.5
0.08
2
7/14/2016
< 2
< 2.5
0.08
3
7/15/2016
< 2
< 2.5
0.11
4
7/16/2016
7/17/2016
7/18/2016
<2
<2.5
0.06
63
7/19/2016
<2
<2.5
0.08
231
7/20/2016
<2
<2.5
< 0.04
6
7/21/2016
<2
<2.5
0.05
9
7/22/2016
2.4
< 2.5
< 0.04
3
7/23/2016
7/24/2016
7/25/2016
2.4
< 2.5
0.04
42
7/26/2016
< 2
< 2.5
< 0.04
35
7/27/2016
<2
< 2.5
< 0.04
<1
7/28/2016
2.3
< 2.5
0.04
1
7/29/2016
2.8
<2.5
0.05
4
7/30/2016
7/31/2016
8/1/2016
2.7
<2.5
0.07
2
8/2/2016
2.8
< 2.5
0.08
1
8/3/2016
3.7
< 2.5
0.11
1
8/4/2016
3
< 2.5
0.12
1
8/5/2016
4.6
< 2.5
0.09
1
8/6/2016
8/7/2016
8/8/2016
3.9
<2.5
0.12
<1
8/9/2016
3.2
<2.5
0.08
2
8/10/2016
2.8
< 2.5
0.08
3
8/11/2016
<2
< 2.5
0
2
8/12/2016
<2
< 2.5
0.12
<1
8/13/2016
8/14/2016
8/15/2016
2.7
<2.5
0.05
1
8/16/2016
<2
<2.5
0.05
1
8/17/2016
< 2
< 2.5
< 0.04
4
8/18/2016
<2
< 2.5
< 0.04
7
8/19/2016
2.5
< 2.5
0.07
8/20/2016
8/21/2016
8/22/2016
9.6
3.6
0.07
58
8/23/2016
4.4
2.9
0.12
4
8/24/2016
2.7
5.8
0.17
18
8/25/2016
4.2
< 2.5
0.13
4
8/26/2016
2.8
< 2.5
0.1
2
8/27/2016
8/28/2016

NH3-N
Date BODS (Summer) BODS (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
8/29/2016
3.7
<2.5
0.06
6
8/30/2016
2.5
< 2.5
< 0.04
2
8/31/2016
2.8
<2.5
<0.04
7
9/1/2016
2.6
< 2.5
0.06
6
9/2/2016
2.6
< 2.5
0.04
11
9/3/2016
9/4/2016
9/5/2016
9/6/2016
2.3
< 2.5
0.07
154
9/7/2016
< 2
< 2.5
0.06
9
9/8/2016
< 2
< 2.5
< 0.04
7
9/9/2016
< 2
<2.5
0.05
2
9/10/2016
9/11/2016
9/12/2016
< 2
2.8
0.06
25
9/13/2016
< 2
< 2.5
0.06
16
9/14/2016
<2
<2.5
0.07
13
9/15/2016
< 2
< 2.5
0.08
6
9/16/2016
< 2
< 2.5
0.09
5
9/17/2016
9/18/2016
9/19/2016
5.3
< 2.5
0.12
1
9/20/2016
<2
<2.5
0.06
14
9/21/2016
3.2
< 2.5
0.08
2
9/22/2016
<2
< 2.5
0.11
1
9/23/2016
<2
< 2.5
0.04
<1
9/24/2016
_
9/25/2016
9/26/2016
< 2
< 2.5
< 0.04
1
9/27/2016
3.8
<2.5
0.04
<1
9/28/2016
< 2
< 2.5
< 0.04
< 1
9/29/2016
< 2
< 2.5
< 0.04
1
9/30/2016
<2
<2.5
<0.04
1
10/1/2016
10/2/2016
10/3/2016
2.5
2.8
< 0.04
<1
10/4/2016
<2
<2.5
0.060
1
10/5/2016
< 2
< 2.5
< 0.04
< 1
10/6/2016
3.2
<2,5
<0.04
< 1
10/7/2016
4.3
<2.5
<0.04
< 1
10/8/2016
10/9/2016
10/10/2016
<2
<2.5
<0.04
1
10/11/2016
< 2
< 2.5
< 0.04
< 1
10/12/2016
<2
< 2.5
< 0.04
3
10/13/2016
<2
< 2.5
< 0.04
< 1
10/14/2016
<2
<2,5
< 0.04
< 1
10/15/2016
10/16/2016
10/17/2016
<2
<2.5
0.04
1
10/18/2016
<2
< 2.5
0.04
1
10/19/2016
< 2
< 2.5
0.06
< 1
10/20/2016
< 2
< 2.5
0.05
< 1
10/21/2016
2.4
< 2.5
0.07
1

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
10/22/2016
10/23/2016
10/24/2016
2.1
< 2.5
0.07
<1
10/25/2016
2.2
< 2.5
0.05
4
10/26/2016
<2
<2.5
0
<1
10/27/2016
< 2
< 2.5
< 0.04
<1
10/28/2016
<2
<2.5
0.06
1
10/29/2016
10/30/2016
10/31/2016
< 2
2.7
0.05
<1
11/1/2016
<2
< 2.5
< 0.04
1
11/2/2016
9
< 2.5
0.06
<1
11/3/2016
.
8.7
< 2.5
0.05
24
11/4/2016
9.6
< 2.5
0.14
1
11/5/2016
11/6/2016
11/7/2016
< 2
< 2.5
0
5
11/8/2016
8.1
< 2.5
0.07
<1
11/9/2016
4.6
<2.5
0.05
1
11/10/2016
6.5
<2.5
0
< 1
11/11/2016
11/12/2016
11/13/2016
11/14/2016
<2
<2.5
<0.04
<1
11/15/2016
12
<2.5
<0.04
<1
11/16/2016
12
< 2.5
0.05
<1
11/17/2016
6.8
< 2.5
0.06
<1
11/18/2016
26
< 2.5
<0.04
<1
11/19/2016
11/20/2016
_
11/21/2016
<2
<2.5
0.09
<1
11/22/2016
< 2
<2.5
0.09
< 1
11/23/2016
25
< 2.5
0.05
< 1
11/24/2016
11/25/2016
11/26/2016
11/27/2016
11/28/2016
24
< 2.5
<0.04
<1
11/29/2016
26
<2.5
<0.04
<1
11/30/2016
13
< 2.5
<0.04
<1
12/1/2016
24
<2.5
0.05
<1
12/2/2016
24
9.9
0.04
1
12/3/2016
12/4/2016
12/5/2016
12
2.6
0.04
<1
12/6/2016
63
<2.5
< 0.04
<1
12/7/2016
13
<2.5
0.060
< 1
12/8/2016
2.3
<2.5
0.08
<1
12/9/2016
<2
<2.5
0.14
<1
12/10/2016
12/11/2016
12/12/2016
2
<2.5
0.12
1
12/13/2016
<2
<2.5
0
< 1
12/14/2016
2
<2.5
< 0.04
< 1

NH3-N
Date BODS (Summer) BODS (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
12/15/2016
5.5
<2.5
< 0.04
2
12/16/2016
3.6
<2.5
< 0.04
< 1
12/17/2016
12/18/2016
12/19/2016
< 2
<2.5
0.04
< 1
12/20/2016
2.6
<2.5
< 0.04
< 1
12/21/2016
< 2
<2.5
0.07
1
12/22/2016
< 2
3
0.09
< 1
12/23/2016
12/24/2016
12/25/2016
12/26/2016
12/27/2016
<2
<2.5
0.06
<1
12/28/2016
<2
<2.5
0.06
< 1
12/29/2016
< 2
<2.5
0.08
<1
12/30/2016
4.2
<2.5
0.05
1
12/31/2016
1/1/2017
1/2/2017
1/3/2017
< 2
< 2.5
0.05
< 1
1/4/2017
<2
<2.5
<0.04
<1
1/5/2017
< 2
< 2.5
0.07
< 1
1/6/2017
3.1
< 2.5
0,08
< 1
1/7/2017
1/8/2017
1/9/2017
< 2
< 2.5
0.06
< 1
1/10/2017
< 2
< 2.5
0.04
1
1/11/2017
< 2
< 2.5
0.04
< 1
1/12/2017
< 2
< 2.5
.< 0.04
< 1
1/13/2017
6.3
< 2.5
0.06
1/14/2017
1/15/2017
1/16/2017
1/17/2017
< 2
< 2.5
0.050
< 1
1/18/2017
3.1
< 2.5
0.15
<1
1/19/2017
10
< 2.5
0.09
<1
1/20/2017
< 2
< 2.5
0.080
<1
1/21/2017
1/22/2017
1/23/2017
< 2
< 2.5
<0.04
< 1
1/24/2017
< 2
< 2.5
0.05
< 1
1/25/2017
< 2
< 2.5
<0.04
< 1
1/26/2017
21
< 2.5
0.07
< 1
1/27/2017
21
< 2.5
0.06
< 1
1/28/2017
1/29/2017
1/30/2017
< 2
<2.5
0.04
< 1
1/31/2017
< 2
< 2.5
0.04
< 1
2/1/2017
7.8
< 2.5
0.04
< 1
2/2/2017
<2
<2.5
<0.04
< 1
2/3/2017
< 2
< 2.5
0.06
< 1
2/4/2017
2/5/2017
2/6/2017
< 2
<. 2.5
0.07
<1

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) . Fecal Coliform
(Summer)
2/7/2017
<2
<2.5
0.06
1
2/8/2017
< 2
9.8
0.08
< 1
2/9/2017
< 2
< 2.5
0.05
1
2/10/2017
< 2
< 2.5
0.12
1
2/11/2017
2/12/2017
2/13/2017
2.1
< 2.5
0.08
1
2/14/2017
< 2
< 2.5
0.13
< 1
2/15/2017
< 2
< 2.5
0.08
< 1
2/16/2017
<2
<2.5
0.83
2
2/17/2017
<2
<2.5
0.06
8
2/18/2017
2/19/2017
2/20/2017
< 2
< 2.5
0.06
1
2/21/2017
<2
<2.5
0.08
2
2/22/2017
<2
<2.5
0.07
< 1
2/23/2017
<2
<2.5
0.07
< 1
2/24/2017
<2
3.1
0.1
1
2/25/2017
2/26/2017
2/27/2017
< 2
< 2.5
0.06
1
2/28/2017
< 2
< 2.5
0.09
< 1
3/1/2017
2.4
< 2.5
0.08
2
3/2/2017
3.5
< 2.5
0.11
< 1
3/3/2017
< 2
< 2.5
0.11
< 1
3/4/2017
3/5/2017
3/6/2017
< 2
< 2.5
0.15
1
3/7/2017
< 2
< 2.5
0.07
< 1
3/8/2017
< 2
< 2.5
0.08
0
3/9/2017
< 2
< 2.5
0.06
1
3/10/2017
3
< 2.5
0.07
< 1
3/11/2017
3/12/2017
3/13/2017
2.1
< 2.5
0.08
< 1
3/14/2017
<2
< 2.5
< 0.04
< 1
3/15/2017
<2
< 2.5
0.06
< 1
3/16/2017
< 2
< 2.5
0.06
1
3/17/2017
< 2
< 2.5
<0.04
1
3/18/2017
3/19/2017
3/20/2017
< 2
< 2.5
0.05
<1
3/21/2017
2.4
< 2.5
0.06
< 1
3/22/2017
2.3
< 2.5
0.08
<1
3/23/2017
2.9
< 2.5
< 0.04
1
3/24/2017
< 2
2.6
0.07
< 1
3/25/2017
3/26/2017
3/27/2017
3.4
< 2.5
0.09
< 1
3/28/2017
3.8
< 2.5
0.1
1
3/29/2017
3
< 2.5
0.09
1
3/30/2017
2.6
< 2.5
0.07
1
3/31/2017
2.4
< 2.5
0.09
< 1
4/1/2017

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
4/2/2017
4/3/2017
3
< 2.5
0.08
< 1
4/4/2017
4.8
<2.5
0.08
4
4/5/2017
4.2
< 2.5
0.08
6
4/6/2017
2.6
< 2.5
< 0.04
24
4/7/2017
2.5
< 2.5
0.07
3
4/8/2017
4/9/2017
4/10/2017
< 2
< 2.5
0.06
< 1
4/11/2017
2.3
< 2.5
0.08
< 1
4/12/2017
2.4
<2.5
0.06
5
4/13/2017
2.1
<2.5
0.09
< 1
4/14/2017
4/15/2017
4/16/2017
4/17/2017
3.1
< 2.5
0.13
< 1
4/18/2017
3
< 2.5
0.17
1
4/19/2017
2.5
< 2.5
0.16
1
4/20/2017
3
<2.5
0.09
< 1
4/21/2017
2.7
< 2.5
0.12
< 1
4/22/2017
4/23/2017
4/24/2017
2.4
2.9
0.12
7
4.9
•4/25/2017 2.7
0.1
1
4/26/2017
< 2
2.6
0.11
< 1
4/27/2017
2
<2.5
0.09
53
4/28/2017
< 2
< 2.5
0.09
2
4/29/2017
4/30/2017
5/1/2017
3.9
< 2.5
0.13
1
5/2/2017
2.7
<2.5
0.16
< 1
5/3/2017
2.5
<2.5
0.17
< 1
5/4/2017
2.5
<2.5
0.16
1
5/5/2017
4.1
< 2.5
0.12
1
5/6/2017
5/7/2017
5/8/2017
3.5
<2.5
0.05
2
5/9/2017
4.2
<2.5
0.1
< 1
5/10/2017
3.2
< 2.5
< 0.04
< 1
5/11/2017
3.5
< 2.5
0.13
435
5/12/2017
3.9
< 2.5
0.06
1
5/13/2017
5/14/2017
5/15/2017
2.8
<2.5
0.28
<1
5/16/2017
4.9
<2.5
0.14
101
5/17/2017
2.1
<2.5
0.05
43
5/18/2017
2.9
< 2.5
< 0.04
9
5/19/2017
3.2
<2.5
0.12
1
5/20/2017
5/21/2017
5/22/2017
2.1
< 2.5
0.15
23
5/23/2017
2.4
<2.5
0.14
31
5/24/2017
<2
2.5
0.08
< 1
5/25/2017
2.7
3.2
0.15
< 1

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
5/26/2017
2.9
<2.5
0.11
< 1
5/27/2017
5/28/2017
5/29/2017
5/30/2017
2.5
<2.5
0.12
< 1
5/31/2017
3.3
<2.5
0.09
< 1
6/1/2017
2.9
< 2.5
0.1
2
6/2/2017
2.1
< 2.5
0.08
1
6/3/2017
6/4/2017
6/5/2017
2.8
< 2.5
0.16
4
6/6/2017
2.1
< 2.5
0.34
< 1
6/7/2017
<2
<2.5
<0.04
1
6/8/2017
< 2
< 2.5
0.11
2
6/9/2017
< 2
< 2.5
0.06
< 1
6/10/2017
6/11/2017
6/12/2017
2.4
< 2.5
0.09
1
6/13/2017
< 2
< 2.5
_
0.1
< 1
6/14/2017
< 2
< 2.5
0.18
< 1
6/15/2017
< 2
< 2.5
0.21
< 1
6/16/2017
< 2
< 2.5
0.14
< 1
6/17/2017
6/18/2017
6/19/2017
< 2
< 2.5
0.09
4
6/20/2017
< 2
< 2.5
0.04
2
6/21/2017
< 2
< 2.5
0.08
2
6/22/2017
< 2
2.7
0.13
1
6/23/2017
3.5
< 2.5
0.17
< 1
6/24/2017
6/25/2017
6/26/2017
< 2
< 2.5
0.11
< 1
6/27/2017
< 2
< 2.5
0.06
< 1
6/28/2017
< 2
< 2.5
0.06
4
6/29/2017
< 2
< 2.5
0.07
< 1
6/30/2017
< 2
< 2.5
0.07
< 1
7/1/2017
7/2/2017
7/3/2017
< 2
< 2.5
0.09
1
7/4/2017
7/5/2017
< 2
< 2.5
0.07
3
7/6/2017
< 2
< 2.5
0.06
1
7/7/2017
< 2
< 2.5
0.1
< 1
7/8/2017
7/9/2017
7/10/2017
< 2
< 2.5
0.1
1
7/11/2017
< 2
< 2.5
0.06
< 1
7/12/2017
< 2
< 2.5
0.08
< 1
7/13/2017
< 2
< 2.5
0.07
1
7/14/2017
< 2
< 2.5
0.2
< 1
7/15/2017
7/16/2017
7/17/2017
< 2
< 2.5
0.13
< 1
7/18/2017
< 2
< 2.5
0.09
1

Date BODS (Summer) BODS (Winter) TSS NH3-N NH3-N (Winter) Fecal Coliform
(Summer)
7/19/2017
< 2
< 2.5
0.16
< 1
7/20/2017
< 2
< 2.5
0.07
< 1
7/21/2017
< 2
< 2.5
0.1
< 1
7/22/2017
7/23/2017
7/24/2017
< 2
< 2.5
0.1
6
7/25/2017
< 2
< 2.5
0.1
< 1
7/26/2017
<2
< 2.5
0.09
< 1
7/27/2017
<2
< 2.5
0.07
1
7/28/2017
< 2
< 2.5
0.07
< 1
7/29/2017
7/30/2017
7/31/2017
< 2
< 2.5
0.07
< 1
8/1/2017
< 2
< 2.5
0.07
< 1
8/2/2017
< 2
< 2.5
0.1
2
8/3/2017
< 2
< 2.5
0.08
1
8/4/2017
< 2
< 2.5
0.08
< 1
8/5/2017
8/6/2017
8/7/2017
3.7
< 2.5
0.14
2
8/8/2017
< 2
< 2.5
0.11
3
8/9/2017
< 2
< 2.5
0.07
1
8/10/2017
< 2
< 2.5
0.06
< 1
8/11/2017
< 2
< 2.5
<0.04
1
8/12/2017
8/13/2017
8/14/2017
<2
< 2.5
0.16
< 1
8/15/2017
<2
2.8
0.06
< 1
8/16/2017
< 2
< 2.5
0.06
1
8/17/2017
< 2
< 2.5
0.08
1
8/18/2017
2.2
< 2.5
0.11
5
8/19/2017
8/20/2017

NH3-N
Date BODS (Summer) BODS (Winter) TSS NH3-N (Winter) Fecal Coliform
(Summer)
8/21/2017
< 2
< 2.5
0.08
8
8/22/2017
< 2
< 2.5
0.1
4
8/23/2017
< 2
< 2.5
0.08
34
8/24/2017
< 2
< 2.5
0.05
12
8/25/2017
< 2
< 2.5
0.05
6
8/26/2017
8/27/2017
8/28/2017
< 2
< 2.5
0.06
10
8/29/2017
< 2
< 2.5
< 0.04
15
8/30/2017
< 2
< 2.5
0.05
11
8/31/2017
< 2
< 2.5
0.05
4
9/1/2017
<2
<2.5
0.05
< 1
9/2/2017
9/3/2017
9/4/2017
9/5/2017
< 2
< 2.5
< 0.04
98
9/6/2017
< 2
< 2.5
< 0.04
40
9/7/2017
< 2
< 2.5
< 0.04
147
9/8/2017
<2
<2.5
0.05
80
9/9/2017
9/10/2017
9/11/2017
<2
<2.5
0.06
14
9/12/2017
< 2
< 2.5
0.08
12
9/13/2017
< 2
< 2.5
0.08
2
9/14/2017
<2
<2.5
0.09
2
9/15/2017
< 2
< 2.5
0.04
10
9/16/2017
9/17/2017
9/18/2017
<2
<2.5
0.05
9
9/19/2017
13
< 2.5
0.06
35
9/20/2017
4.9
<2.5
<0.04
20
9/21/2017
<2
<2.5
<0.04
6
9/22/2017
< 2
< 2.5
0.27
10
9/23/2017
9/24/2017
9/25/2017
<2
<2.5
0.14
3
9/26/2017
2.5
<2.5
0.09
9/27/2017
< 2
< 2.5
0.18
< 1
9/28/2017
<2
<2.5
0.06
< 1
9/29/2017
<2
<2.5
0.05
1
9/30/2017
_