NCG030055_2022 DMR_20220407

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Re Tonal Office.
Certificate of Coverage No. NCG030055
Person Collecting Samples: Claude F. Laughter
Facility Name: Meritor Heavy Vehicle Systems LLC
Laboratory Name: Pace analytical Services
Facility County: Henderson
Laboratory Cert. No.: 92594126001, 92594126002
Discharge during this period:
Yes
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? LjYes a No
If so, which Tier (I, II, or III)? n/a
A copy of this DMR has been uploaded electronically via htt s: ea, Aeo.nc.rov/Forms/SW-DMR Yes No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
Outfall1
Outfall2
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
Tr
Tr
N/A
Date Sample Collected MM/DD/YYYY
03/16/2022
03/16/2022
46529
24-Hour Rainfall in inches
.19
.19
C0530
TSS in mg/L (100 or 50*)
9.6
< 2.5
00400
pH in standard units (6.0-9.0 FW,
7.7
7.0
,8-8.5 SW)
01119
Copper, total recoverable in mg/L
'
<
< .005
".010 FW, 0.0058 SW)
.005
01051
Lead, total recoverable in mg/ L
<
< .005
(0.075 FW, 0.22 SW)
.005
Zinc, total recoverable in mg/ L (0.126
01094
FW, 0.095 SW)
.015
.0325
00340
Chemical Oxygen Demand (COD) in
< 25
< 25
mg/L (120)
00552
Non -Polar Oil & Grease in mg/L
< 4.9
1 < 4.9
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of ,ng/L. All other water classifications have a benchmark of — . . .6,
(Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or person who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best o knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false informp* nn inckoft the possibility of fines and imprisonment for knowing violations."
Signa re of Permittee or Delegated Authorized Individual Date
Email Address
Q-10 - i q 7- 27,U 1
Phone Number

Envh»nnutiral
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ S / 0 / 0 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 / 0 / 0 / 5 / 5 /
Facility Name: Meritor Heavy Vehicle Systems LLC
County: Henderson Phone No.: 828 687-2000
Inspector: Claude F. Lau hter
Date of Inspection: 03/16/2022
Time of Inspection:
Total Event Precipitation (inches): 19
Field pH: 7
IAII permits require qualitative monitoring to be performed during a "measurable storm event."
IA "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
( 4ignae4PeittoEq s ee)
1. Outfall Description:
Outfall No. 1 Structure (pipe, ditch, etc.): Fire pond flume
Receiving Stream: Cane Creek
Describe the industrial activities that occur within the outfall drainage area: Heavy manufacturing_,
welding, machining, din assembly
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light,
medium, dark) as descriptors: Blue, light
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and
5 is very cloudy:
1 2O 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
lO 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2O 3 4 5
7. Is there any foam in the stormwater discharge? o Yes No. 0
8. Is there an oil sheen in the stormwater discharge? OYes No. 4P
9. Is there evidence of erosion or deposition at the outfall? O Yes 4PNo.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

EnvO nmentat
QGaftry
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ S / 0 / 0 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 / 0 / 0 / 5 / 5 /
Facility Name: __Mentor Heayy Vehicle Systems LLC
County: Henderson Phone No.: 828 687-2000
Inspector: Claude F. Lau hter
Date of Inspection: 03/16/2022
Time of Inspection: 09:30 a.m.
Total Event Precipitation (inches): .19 Field pH: 7
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office. J
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
1. Outfall Description:
Outfall No. 2 Structure (pipe, ditch, etc.): Ditch, North side
Receiving Stream: Cane Creek
Describe the industrial activities that occur within the outfall drainage area: Heavy manufacturing,
weldipg, machining, ndin assembly.
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light,
medium, dark) as descriptors: Blue, medium
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and
5 is very cloudy:
1 O2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
10 3 4 5
7. Is there any foam in the stormwater discharge? o Yes No. OW
8. Is there an oil sheen in the stormwater discharge? OYes No.0
9. Is there evidence of erosion or deposition at the outfall? o Yes ONo.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

weather.gov
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Temperature (OF)
Pressure
Precipitation
(in.)
a
Time
Wind
Vis.
Weather
Sky
Relative
Wind
Chill
Heat
Index
t
(edt)
(mph)
(mi.)
Cond.
6 hour
Humidity
(F)
(F)
altimeter
sea
3
e
Air
Dwpt
(in)
level
1 hr 6 hr
hr
Max. Min.
(mb)
16
07:54
Calm
5.00
Light
BKN065
48
47 48 45
96%
NA
NA
30.13
1019.5
0.09 0.19
Rain
OVC080
Fog/Mist
16
06:54
Calm
4.00
Rain
BKN020
46
45
96%
NA
NA
30.14
1019.9
0.09
Fog/Mist
BKN025
OVC044
16
05:54
SE 3
10.00
Light
OVC018
45
43
93%
NA
NA
30.14
1019.9
0.01
Rain
16
04:54
Calm
10.00
Light
FEW032
46
42
86%
NA
NA
30.14
1019.6
Rain
BKN075
OVC095
16
03:54
S 3
10.00
Overcast
BKN055
46
42
86%
NA
NA
30.15
1020.1
OVC090
16
02:54
Calm
10.00
Overcast
OVC046
46
42
86%
NA
NA
30.17
1020.6
16
01:54
Calm
10.00
Overcast
BKN044
46
42 56 45
86%
NA
NA
30.19
1021.3
OVC060
16
00:54
Calm
10.00
A Few
FEW055
47
42
83%
NA
NA
30.20
1021.9
Clouds
15
23:54
Calm
10.00
Fair
CLR
48
42
80%
NA
NA
30.22
1022.4
15
22:54
Calm
10.00
Fair
CLR
50
43
77%
NA
NA
30.23
1022.9
15
21:54
S 3
10.00
Fair
CLR
53
43
69%
NA
NA
30.22
1023.0
15
20:54
SE 5
10.00
Fair
CLR
55
43
64%
NA
NA
30.21
1022.7
15
19:54
S 3
10.00
Fair
CLR
56
42 61 56
60%
NA
NA
30.22
1023.0
15
18:54
S 6
10.00
Fair
CLR
57
43
60%
NA
NA
30.21
1022.7
15
17:54
S 6
10.00
Fair
CLR
58
42
56%
NA
NA
30.22
1023.1
15
16:54
S 9
10.00
Fair
CLR
59
43
56%
NA
NA
30.24
1023.8
15
15:54
S 10
10.00
A Few
FEW110
60
40
48%
NA
NA
30.24
1023.6
Clouds
15
14:54
SW 8
10.00
Overcast
OVC110
61
40
46%
NA
NA
30.26
1024.2
15
13:54
Calm
10.00
A Few
FEW050
60
39 60 35
46%
NA
NA
30.28
1024.8
Clouds
15
12:54
S 10
10.00
Mostly
BKN120
58
42
56%
NA
NA
30.32
1026.1
Cloudy
15
11:54
S 7
10.00
Partly
SCT120
55
41
59%
NA
NA
30.32
1026.4
Cloudy
15
10:54
S 7
10.00
A Few
FEW110
51
32
48%
NA
NA
30.34
1027.2
Clouds
15
09:54
Calm
10.00
A Few
FEW110
45
31
58%
NA
NA
30.34
1027.2
Clouds
15
08:54
Calm
10.00
Partly
SCT110
39
29
67%
NA
NA
30.34
1027.3
Cloudy
15
07:54
Calm
10.00
Mostly
BKN110
35
30 37 33
82%
NA
NA
30.34
1027.3
Cloudy

15
06:54
Calm
10.00
Mostly
BKN110
35
30
82%
NA
NA
30.33
1026.9
Cloudy
15
05:54
Calm
10.00
Mostly
BKN100
34
29
82%
NA
NA
30.33
1026.8
Cloudy
15
04:54
Calm
10.00
Fair
CLR
33
29
85%
NA
NA
30.34
1027.0
15
03:54
Calm
10.00
Fair
CLR
34
29
82%
NA
NA
30.35
1027.6
15
02:54
Calm
10.00
A Few
FEW110
36
29
76%
NA
NA
30.37
1028.1
Clouds
15
01:54
Calm
10.00
A Few
FEW120
37
30
54 37
76%
NA
NA
30.37
1028.1
Clouds
15
00:54
Calm
10.00
Fair
CLR
39
28
65%
NA
NA
30.38
1028.3
14
23:54
S 5
10.00
Fair
CLR
40
29
65%
36
NA
30.39
1028.9
14
22:54
Calm
10.00
Fair
CLR
43
28
56%
NA
NA
30.39
1029.2
14
21:54
Calm
10.00
Fair
CLR
48
26
42%
NA
NA
30.38
1029.1
14
20:54
SE 5
10.00
Fair
CLR
51
25
36%
NA
NA
30.36
1028.6
14
19:54
S 7
10.00
Fair
CLR
54
24
61 54
31 %
NA
NA
30.35
1028.0
14
18:54
S 9
10.00
Fair
CLR
57
24
28%
NA
NA
30.34
1027.4
14
17:54
S 15
10.00
Fair
CLR
59
24
26%
NA
NA
30.33
1027.1
G 20
14
16:54
S 10
10.00
Fair
CLR
60
24
25%
NA
NA
30.33
1027.1
G17
14
15:54
Vrbl7
10.00
Fair
CLR
60
24
25%
NA
NA
30.34
1027.5
G 20
14
14:54
SE
10.00
Fair
CLR
59
21
23%
NA
NA
30.37
1028.2
12G
21
14
13:54
S 12
10.00
Fair
CLR
60
23
60 28
24%
NA
NA
30.39
1029.0
G16
14
12:54
S 8
10.00
Fair
CLR
56
25
30%
NA
NA
30.43
1030.4
14
11:54
S 3
10.00
Fair
CLR
51
26
38%
NA
NA
30.44
1031.0
14
10:54
Calm
10.00
Fair
CLR
44
27
51 %
NA
NA
30.45
1031.5
14
09:54
Vrbl3
10.00
Fair
CLR
37
26
65%
NA
NA
30.44
1031.5
14
08:54
Calm
10.00
Fair
CLR
31
25
79%
NA
NA
30.43
1031.1
14
07:54
NW 3
10.00
Fair
CLR
29
24
31 28
82%
NA
NA
30.42
1030.7
14
06:54
NW 6
10.00
Fair
CLR
30
24
79%
24
NA
30.40
1029.8
14
05:54
NW 7
10.00
Fair
CLR
31
24
76%
24
NA
30.38
1029.1
14
04:54
NW 8
10.00
Fair
CLR
30
23
75%
22
NA
30.37
1028.7
14
03:54
NW 3
10.00
Fair
CLR
29
23
78%
NA
NA
30.36
1028.7
14
02:54
Calm
10.00
Fair
CLR
30
22
72%
NA
NA
30.36
1028.8
14
01:54
Calm
10.00
Fair
CLR
31
23
45 30
72%
NA
NA
30.36
1029.1
14
00:54
Calm
10.00
Fair
CLR
32
23
69%
NA
NA
30.36
1029.0
13
23:54
Calm
10.00
Fair
CLR
37
18
46%
NA
NA
30.35
1028.7
13
22:54
Calm
10.00
Fair
CLR
38
19
46%
NA
NA
30.34
1028.8
13
21:54
S 3
10.00
Fair
CLR
40
18
41 %
NA
NA
30.34
1028.6
13
20:54
SW 7
10.00
Fair
CLR
43
17
35%
39
NA
30.31
1027.7
13
19:54
S 6
10.00
Fair
CLR
45
17
50 41
33%
42
NA
30.29
1027.0
13
18:54
S 7
10.00
Fair
CLR
48
17
29%
45
NA
30.27
1026.2
13
17:54
S 10
10.00
Fair
CLR
49
19
31 %
45
NA
30.25
1025.5
13
16:54
E 7
10.00
Fair
CLR
50
15
25%
47
NA
30.25
1025.3
13
15:54
SE 8
10.00
Fair
CLR
49
15
26%
46
NA
30.25
1025.2

13
14:54 Vrbl6
10.00
Partly
SCT080
46
14
27%
43
NA
30.27
1026.3
Cloudy
13
13:54
S 6
10.00
Fair
CLR
41
14 41 16
33%
37
NA
30.31
1027.9
13
12:54
Vrb15
10.00
Fair
CLR
36
12
37%
32
NA
30.34
1029.1
13
11:54
NW 3
10.00
Fair
CLR
32
10
40%
NA
NA
30.35
1029.6
13
10:54
NW 7
10.00
Fair
CLR
26
9
48%
18
NA
30.35
1030.0
13
09:54
NA
10.00
Fair
CLR
23
8
53%
NA
NA
30.34
1029.7
13
08:54
NA
10.00
Fair
CLR
20
8
60%
NA
NA
30.33
1029.3
D
Max. Min.
altimeter
sea
3
a
Time
Wind
Vis.
Sky
Air
D:v t
p 6 hour
Relative
Wind
Heat
(in.)
,evel
(mb)
1 hr 6 hr
hr
t
(edt)
(mph)
(mi.)
Weather
Cord.
Humidity
hill
Chill
Index
e
Temperature (,F)
(F)
(F)
Pressure
Precipitation
(in.)
National Weather Service Back to previous page
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Disclaimer
Last Modified: Febuary, 7 2012
Privacy Policy

ceAnalytical
wrrw.pacdabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Stormwater-3/16
92594126
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92594126001
Outfall #1 Fire Pond Flume
EPA 1664B
HND
1
PASI-C
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
KH
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 2540D-2015
ZMC
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2016
MMB
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92594126002
Outfall #2 North Ditch
EPA 1664B
HND
1
PASI-C
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
KH
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 2540D-2015
ZMC
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2016
MMB
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 34

f 'IaceAnal lcal
www.paeelabs.om
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #1 Fire Pond Flume Lab ID: 92594126001 Collected: 03/16/22 09:15 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND
mg/L
4.9
1
03/22/22 21:32
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services - Charlotte
Aldrin
ND
ug/L
0.050
1
03121/2216:16
03/2212216:16
309-00-2
alpha-BHC
ND
ug/L
0.050
1
03/21/22 16:16
03/2212216:16
319-84-6
beta-BHC
ND
ug/L
0.050
1
03121/2216:16
03/22/22 16:16
319-85-7
delta-BHC
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
57-74-9
alpha -Chlordane
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
5103-71-9
gamma -Chlordane
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
5103-74-2
4,4'-DDD
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
72-54-8
4,4'-DDE
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
72-55-9
4,4'-DDT
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
50-29-3
Dieldrin
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
60-57-1
Endosulfan I
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
959-98-8
Endosulfan 11
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
1031-07-8
Endrin
ND
ug/L
0.050
1
03/2112216:16
03/22/22 16:16
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
7421-93-4
Heptachlor
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:16
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
11104-28-2
PCB-1232 (Aroolor 1232)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
11096-82-5
PCB, Total
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:16
1336-36-3
Toxaphene
ND
ug/L
0.50
1
03/21/22 16:16
03122/2216:16
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
111
%
10-154
1
03/21/22 16:16
03/22/22 16:16
877-09-8
Decachlorobiphenyl (S)
99
%
10-184
1
03/21/22 16:16
03/22/22 16:16
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND
ug/L
5.0
1
03/21/22 12:20
03/22/22 07:36
7440-50-8
Lead
ND
ug/L
5.0
1
03/21/22 12:20
03/22/22 07:36
7439-92-1
Zinc
15.0
ug/L
10.0
1
03/21/22 12:20
03/22/22 07:36
7440-66-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA
625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
83-32-9
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in
full,
Date: 03/30/2022 11:20 AM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 34

aceAnalytical
www.pacelabs cm
i(
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: Outfall #1 Fire Pond Flume Lab ID: 92594126001 Collected: 03/16/22 09:15 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Acenaphthylene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
208-96-8
Anthracene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
120-12-7
Benzo(a)anthracene
ND
ug/L
6.0
1
03/23/22 04:30
03/23/22 21:03
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
7005-72-3
Chrysene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
03/23/22 04:30
03/23/22 21:03
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
606-20-2
Di-n-octylphthalate
ND
uglL
5.0
1
03/23/22 04:30
03/23/22 21:03
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
117-81-7
Fluoranthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
206-44-0
Fluorene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
193-39-5
Isophorone
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
78-59-1
Naphthalene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
87-86-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2022 11:20 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 34

aceAnalytical
www.pacelabsXW
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #1 Fire Pond Flume Lab ID: 92594126001 Collected: 03/16/22 09:15 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Phenanthrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
85-01-8
Phenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
108-95-2
Pyrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
129-00-0
1,2,4-Tdchlorobenzene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:03
120-82-1
2,4,6-Tdchlorophenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
87
%
10-120
1
03/23/22 04:30
03/23/22 21:03
4165-60-0
2-Fluorobiphenyl (S)
89
%
15-120
1
03/23/22 04:30
03/23/22 21:03
321-60-8
Terphenyl-dl4 (S)
107
%
11-131
1
03/23/22 04:30
03/23/22 21:03
1718-51-0
Phenol-d6 (S)
35
%
10-120
1
03/23/22 04:30
03/23/22 21:03
13127-88-3
2-Fluorophenol (S)
13
%
10-120
1
03/23/22 04:30
03/23/22 21:03
367-12-4
2,4,6-Tribromophenol (S)
26
%
10-137
1
03/23/22 04:30
03/23/22 21:03
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
Benzene
ND
ug/L
1.0
1
03/18/22 18:34
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
03/18/22 18:34
75-27-4
Bromoform
ND
ug/L
2.0
1
03/18/22 18:34
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/18/22 18:34
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
03/18/22 18:34
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
03/18/22 18:34
108-90-7
Chloroethane
ND
ug/L
2.0
1
03/18/22 18:34
75-00-3
Chloroform
ND
ug/L
2.0
1
03/18/22 18:34
67-66-3
Chloromethane
ND
ug/L
2.0
1
03/18/22 18:34
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
03/18/22 18:34
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
03/18/22 18:34
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
03/1812218:34
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
03/1812218:34
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
03/18/22 18:34
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
03/18/22 18:34
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
03/18/22 18:34
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
2.0
1
03/18/22 18:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
03/1812218:34
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
03/18/22 18:34
78-87-5
cis- 1,�-Dichloropropene
ND
ug/L
2.0
1
03/18/22 18:34
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
03/18/22 18:34
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/18/22 18:34
100-41-4
Methylene Chloride
ND
ug/L
2.0
1
03/18/22 18:34
75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
03/18/22 18:34
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
03/18/22 18:34
127-18-4
Toluene
ND
ug/L
1.0
1
03/18/22 18:34
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1
03/18/22 18:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
03/18/22 18:34
79-00-5
Trichloroethene
ND
ug/L
2.0
1
03/18/22 18:34
79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
1
03/18/22 18:34
75-69-4
Vinyl chloride
ND
ug/L
2.0
1
03/18/22 18:34
75-01-4
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 03/30/2022 11:20 AM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 34

aceAnalytical
rww.�acelabs.caa
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #1 Fire Pond Flume Lab ID: 92594126001 Collected: 03/16/22 09:15 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH at 25 Degrees C
420.4 Phenolics, Total
Phenolics, Total Recoverable
450OCNE Cyanide, Total
Cyanide
5220D COD
Chemical Oxygen Demand
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
102 %
70-130 1
03/18/2218:34 460-00-4
103 %
70-130 1
03/18/2218:34 2037-26-5
104 %
70-130 1
03/18/2218:34 17060-07-0
Analytical Method: SM 254OD-2015
Pace Analytical Services - Asheville
9.6 mg/L
2.5 1
03/18/2216:31
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
7.7 Std. Units
0.10 1
03/18/22 13:22
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
ND mg/L
0.020 1
03/29/22 09:13 03/29/22 12:27 64743-03-9
Analytical Method: SM 4500-CN-E-2016 Preparation
Method: SM 4500-CN-E-2016
Pace Analytical Services -Asheville
ND mg/L
0.0080 1
03/22/22 18:44 03/23/22 03:01 57-12-5
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
ND mg/L
25.0 1
03/30/22 02:32 03/30/22 05:56
H3
Sample: Outfall #2 North Ditch Lab ID: 92594126002 Collected: 03/16/22 09:30 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
4.9
1
03/22/22 21:32
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA
608.3
Pace Analytical Services - Charlotte
Aldrin
ND ug/L
0.050
1
03121/2216:16
03/22/22 16:28
309-00-2
alpha-BHC
ND ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
319-84-6
beta-BHC
ND ug/L
0.050
1
03/21/22 16:16
03122/2216:28
319-85-7
delta-BHC
ND ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
319-86-8
gamma-BHC (Lindane)
ND ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
58-89-9
Chlordane (Technical)
ND ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
57-74-9
alpha -Chlordane
ND ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
5103-71-9
gamma -Chlordane
ND ug/L
0.050
1
03121/2216:16
03/22/22 16:28
5103-74-2
4,4'-DDD
ND ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
72-54-8
Date: 03/30/2022 11:20 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 34

/�qalceAnalyfical"
f rrrrw.pacNabs.cae
f
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #2 North Ditch
Parameters
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92594126002 Collected: 03/16/22 09:30 Received: 03/17/22 14:30 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical
Services - Charlotte
4,4'-DDE
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
72-55-9
4,4'-DDT
ND
ug/L
0.050
1
03/2112216:16
03/22/22 16:28
50-29-3
Dieldrin
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
60-57-1
Endosulfan I
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
959-98-8
Endosulfan 11
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
1031-07-8
Endrin
ND
ug/L
0.050
1
03/2112216:16
03/22/22 16:28
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
7421-93-4
Heptachlor
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
1
03/21/22 16:16
03/22/22 16:28
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
11141-16-5
PCB-1242 (Aroolor 1242)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
53469-21-9
PC13-1248 (Aroclor 1248)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
11096-82-5
PCB, Total
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
1336-36-3
Toxaphene
ND
ug/L
0.50
1
03/21/22 16:16
03/22/22 16:28
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
80
%
10-154
1
03/21/22 16:16
03/22/22 16:28
877-09-8
Decachlorobiphenyl (S)
78
%
10-184
1
03/21/22 16:16
03/22/22 16:28
2051-24-3
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical
Services - Asheville
Copper
ND
ug/L
5.0
1
03/21/22 12:20
03/22/22 07:58
7440-50-8
Lead
ND
ug/L
5.0
1
03/21/22 12:20
03/22/22 07:58
7439-92-1
Zinc
32.5
ug/L
10.0
1
03/21/22 12:20
03/22/22 07:58
7440-66-6
625 RVE
Analytical Method:
EPA 625.1 Preparation Method: EPA
625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
208-96-8
Anthracene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
207-08-9
4-13romophenylphenyl ether
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
101-55-3
Butylbenzylphtha late
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
95-57-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2022 11:20 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 34

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #2 North Ditch Lab ID: 92594126002 Collected: 03/16/22 09:30 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
7005-72-3
Chrysene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
03/23/22 04:30
03/23/22 21:32
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
117-81-7
Fluoranthene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
206-44-0
Fluorene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
193-39-5
Isophorone
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
78-59-1
Naphthalene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
87-86-5
Phenanthrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
85-01-8
Phenol
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
108-95-2
Pyrene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
03/23/22 04:30
03/23/22 21:32
120-82-1
2,4,6-Tdchlorophenol
ND
ug/L
10.0
1
03/23/22 04:30
03/23/22 21:32
88-06-2
Surrogates
Nitrobenzene-d5 (S)
82
%
10-120
1
03/23/22 04:30
03/23/22 21:32
4165-60-0
2-Fluorobiphenyl (S)
78
%
15-120
1
03/23/22 04:30
03/23/22 21:32
321-60-8
Terphenyl-d14 (S)
101
%
11-131
1
03/23/22 04:30
03/23/22 21:32
1718-51-0
Phenol-d6 (S)
46
%
10-120
1
03/23/22 04:30
03/23/22 21:32
13127-88-3
2-Fluorophenol (S)
58
%
10-120
1
03/23/22 04:30
03/23/22 21:32
367-12-4
2,4,6-Tdbromophenol (S)
97
%
10-137
1
03/23/22 04:30
03/23/22 21:32
118-79-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2022 11:20 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 34

aceAnalytical
www.pecolabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #2 North Ditch Lab ID: 92594126002 Collected: 03/16/22 09:30 Received: 03/17/22 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropen e
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH at 25 Degrees C
Date: 03/30/2022 11:20 AM
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
104 %
102 %
102 %
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
ND mg/L
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
7.0 Std. Units
1.0
1
03/18/22 18:51
71-43-2
2.0
1
03/18/22 18:51
75-27-4
2.0
1
03/18/22 18:51
75-25-2
2.0
1
03/18/22 18:51
74-83-9
2.0
1
03/18/22 18:51
56-23-5
2.0
1
03/18/22 18:51
108-90-7
2.0
1
03/18/22 18:51
75-00-3
2.0
1
03/18/22 18:51
67-66-3
2.0
1
03/18/22 18:51
74-87-3
2.0
1
03/18/22 18:51
124-48-1
2.0
1
03/18/22 18:51
95-50-1
2.0
1
03/18/22 18:51
541-73-1
2.0
1
03/18/22 18:51
106-46-7
2.0
1
03/18/22 18:51
75-34-3
2.0
1
03/18/22 18:51
107-06-2
2.0
1
03/18/22 18:51
75-35-4
2.0
1
03/18/22 18:51
156-59-2
2.0
1
03/18/22 18:51
156-60-5
2.0
1
03/18/22 18:51
78-87-5
2.0
1
03/18/22 18:51
10061-01-5
2.0
1
03/18/22 18:51
10061-02-6
1.0
1
03/18/22 18:51
100-41-4
2.0
1
03/18/22 18:51
75-09-2
2.0
1
03/18/22 18:51
79-34-5
2.0
1
03/18/22 18:51
127-184
1.0
1
03/18/22 18:51
108-88-3
2.0
1
03/18/22 18:51
71-55-6
2.0
1
03/18/22 18:51
79-00-5
2.0
1
03/18/22 18:51
79-01-6
2.0
1
03/18/22 18:51
75-69-4
2.0
1
03/18/22 18:51
75-01-4
70-130 1
70-130 1
70-130 1
2.5 1
0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/18/22 18:51 460-00-4
03/18/22 18:51 2037-26-5
03/18/22 18:51 17060-07-0
03/18/22 16:32
03/18/2213:26 H3
Page 10 of 34

! aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwater-3/16
Pace Project No.: 92594126
Sample: Outfall #2 North Ditch
Parameters
Lab ID: 92594126002 Collected: 03/16/22 09:30 Received: 03/17/22 14:30 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
420.4 Phenolics, Total
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
Phenolics, Total Recoverable
ND mg/L 0.020 1 03/29/22 09:13 03/29/22 12:27 64743-03-9
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016
Pace Analytical Services -Asheville
Cyanide
ND mg/L 0.0080 1 03/22/22 18:44 03/23/22 03:05 57-12-5
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg/L 25.0 1 03/30/22 02:32 03/30/22 05:56
Date: 03/30/2022 11:20 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 34