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HomeMy WebLinkAboutWQ0004972_Monitoring - 03-2022_20220426 n .. ti DWR - NonDischarge Monitoring Report Submittal ' •4 .. NORTH CAROLINA Erwlranmenlcl QHaflly Monitoring Report Submittal .............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................. Permit Number#* WQ0004972 Name of Facility:* Forest Lakes Preserve ELS Month:* March Year:* 2022 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR Forest Lakes_March 2022.pdf 1.98MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2,NDMLR,GW-59). Confirmation Email Address:* Jessica.Mize@pacelabs.com Name of Submitter:* Jessica Mize Signature: jezciu,4 Date of submittal: 4/26/2022 This will be filled in automatically Initial Review ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................. Reviewer: Gerald,Wanda Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Accepted Date: 5/10/2022 Page 1 of 2 NON-DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: WO0004972 MONTH: March YEAR: 2022 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: I_X I Influent: U R Parameter Monitoring Point: Effluent: R Influent: ['Surface Water(SW):I SW Code/Name: n Was There Effluent Flow for this Month Generated At This Facility: Yes: ,J No: [j Operator 50050 00400 50060 00310 00610 00530 31616 00665 00625 00630 00600 00620 ! 70300 00940 D Arrival Catty Rate Fecal A Time Operator ORC (Flow)into Colifonn Total Total 1 2400 Time on on Treatment Residual ROD.5 {Geo-metric Total Rjeldhal Total Nitrate Dissolved L' Clock Sac Site? Sy-stern pH Chlorine 20"C NR-?-N TSS Mon') Phos Nitrogen NO2+NO3. Nitrogen NO?-N Solids Chloride FIRS YIN GPD LNITS mgiL MGd. SIG I. .SFG,L rlUOML MG•L MG-L MG,L MIGiL MGiL \li 1. SIG.L Continuous :i,5leek yilleek Monthly Slnnti, Monthly Moodily Monthly Monthly ,Monthly ,Monthly Monthly 1_...:,, ?year I 0732 0.25 Y 8,000 5.9 -.Wilt _ r 2 1440 0.25 13 8,000 5.9 <0.01 3 1450 0.25 II 8.000 63 <0.01 4 1110 0.25 B 8.000 6.2 <0.01 S 8,000 6 8,000 7 0711 0.50 Y 8,000 6.1 <0.01 8 1055 11.25 IS 8,000 6.3 <0.1)1 9 1450 (1.25 IS 8.000 6.2 <0.111 10 1435 11.25 11 8.000 6.3 <11m l 11 1150 _ 0.25 13 8,000 6.3 <11.01 12 8,000 13 8,000 - 14 0736 0.25 Y 8.000 6.2 <0.111 - Is 0804 0.50 Y 8,000 (i.l <0.E11 re 1425 _ 0.25 B 8,000 (.3 -,0.111 17 11751 0.25 Y 8.000 6,1 :0.01 .. 16 WOO 0.25 13 8.000 5.9 --11.01 19 8,000 =it_ 8,000 I 21 1435 0.25 B 8,000 6,3 <0.01 22 0711 0.50Y 8,000 v 6.1 <0.(11 23 1350 0.25 B 8,000 6.1 <0.01 24 1520 0.25 B 8,000 6.3 <0.1)1 25 1240 0.25 B 8,000 6.2 <0.111 26 8,000 27 8,000 28 0722 0.25 Y 8,000 6.2 <0.01 - 29 0940 0.25 Y 8,000 6.1 <0.0! 2.9 53.3 14.9 24211 8.7 63.5 <11.040 63.5 <0.040 256 42.2 MI 1000 0.25 [3 8.000 6.0 <0.01 - St 0804 0.50 Y 8,000 6.0 <0.01 Aveni5e 8,0011 <0.01 2.9 53.11 14.9 24211 8.7 63.5 <0.04- 63.5 <0.11411 256 422 Daily 3laximum 8,000 6.3 <0.1)1 2.9 53.8 14.9 2420 8.7 63.5 <0.040 63.5 <0.1140 256 42.2 Daily Minimum 8,000 5.9 <0.01 2.9 53.8 14.9 2420 8.7 635 <0.041) 63.5 <0.040 256 42.2 Monthly Limits(s) 2441111 Composite.)I Grab[G) *FLOWS ESTIMATED,FLOW METER INOPERABLE Operator in Responsible Charge(ORC): Glenn Price Grade: Il Phone: 336-996-2841 Check Box if ORC Has Changed: 0 ORC Certification Number: 987931/20771 Certified Laboratories(1):_Pace Analytical Serivices _ (2): , Person(s)Collecting Samples: Glenn Price Mall ORIGINAL and Two COPIES to: ATPN:Non-Discharge Compliance Unit X �~ DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature,I certify that this report is accurate and 1617 Mail Service Center comptete to the best of my knowledge. RALEIGH,NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant N) 1. Does all monitoring data and sampling frequencies meet permit requirements? Y If the facility is non-compliant,please explain in the space below the reason(s)the facility was not in compliance with its permit. Provide in your explanation the date(s)of the non-compliance and describe the corrective action(s)taken. Attach additional sheets if necessary. Flow Estimated.Flow meter inoperable "I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief true,accurate,and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." 174 24- Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official-Please print or type) Baron Neal McDuffie(Authorized Agent) Field Services Director(Pace Analytical Services) (Permittee-Please print or type) (Position or Title) 2N Riverside Plaza .Suite 800 3/31/21 Chicago.II 60606 (Permit Exp.Date) (Permittee Address) 01002 Arsenic 31504 Coliform,Total 00600 Nitrogen,Total 00929 Sodium 01022 Boron 00094 Conductivity 00630 NO2&NO3 00931 SAR 00310 BOD5 01042 Copper 00620 NO3 00745 Sulfide 01027 Cadmium 00300 Dissolved Oxygen 00556 Oil&Grease 00515 TDS 00916 Calcium 31616 Fecal Coliform WQ09 PAN(Plant Available) 00010 Temperature 00940 Chloride 01051 Lead 00400 pH 00625 TKN 50060 Chlorine,Total 00927 Magnesium 32730 Phenols 00680 TOC Residual 71900 Mercury 00665 Phosphorus,Total 00530 TSS/TSR 01034 Chromium 00610 NH3 as N 00937 Potassium 00076 Turbidity 00340 COD 01067 Nickel 00545 Settleable Matter 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at(919)733-5083,extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. •If signed by other than the Permittee,delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)(2)(D). Page 2 of 2 NON-DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE.USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: O004972 MONTH: March YEAR: 2022 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Loading(inches) =[Volume Applied(gallons)x 0.1336(cubic feet/gallon)x 12(inches/foot)]/[Area Sprayed(acres)x 43,560(square feetiacre)or =[Volume Applied(gallons)I[Area Sprayed(acres)x 27,152(gallonslacre-iinch). Maximum Hourly Loading(inches) =Daily Loading(inches)/[Time irrigated(minutes)/60(minutes/hour)] Monthly Loading(inches) =Sum of Daily Loading(inches) 12 Month Floating Total(inches) =Sum of this month's Monthly Loading(inches)and previous 11 month's Monthly Loadings(inches) Average Weakly Loading(inches) =[Monthly Loading(inches/month)/Number of days in the month(days/month)]x 7(days/week) Did irrigation Occur At This Facility: Did Irrigation Occur On This Field: Did Irrigation Occur On Thls Field: Yesn No YeR No: 0 yen No:❑ Field Number: Field Number: Area Sprayed(acres): 3-4 Area Sprayed(acres): Cover Crop: Cover Crop: Permitted Hourly ate Inches: 4.1 Permitted Hourly ate(inches): WEATHER CONDITIONS Permitted Yearly Rate(inches): 46.6 Permitted Yearly Rats(inches): D A weather Temperature storage \I.1zm..1: kl.,imum T Code- at Preeq,xe- Lagoon Voilaue Tube Da,:. H'.rly Volonw Time bat, Ready F. .lnrhwu,ii bey Fro:-h,o,l .Appliat Imgatal L.i.hne tr,,,,I Impial L,ainn Loulinv FF1 inches lift r.11hxls milulo, In'ha nmu[.. Ic.h.. inch. I CI 46 0 2.6 Cl 67 I) 2.5 a PC 62 0 2.4 4 C 69 - 0 2.2 42.48(1 3011 0.46 0.09 • S 6 T 7 Cl 48 n 2.6 s CI 63 II 2.4 9 PC 60 Il 2.2 1e PC 57 Il 2.2 42.480 inn 0.46 ((.I>r) 11 C 66 I) 3.3 12 13 14 R 42 11.6 2.8 - is CI 68 0 2.8 16 Cl 62 0 2.7 17 R 44 0.75 2.6 IC R 74 0.21 2.6 10 20 21 R 59 1.114 2.2 22 CI 49 0 2.1 23 Cl 68 0 2.0 42.480 :un 11.411 0.09 24 PC 72 0 3.1 25 PC 70 0 3.0 2e 27 28 CI „ 0 2.7 2'1 PC 51 0 2.6 31i , C 56 0 2.4 42.480 3111 11.4/, 0.09 31 C 52 0 3.2 Taal CalloomAleerhly Lmaina iled.,.l 1.84 12 Stanch F[naliox Total IIlioh rl 2(1.37 .. Avrrane Weekly Lomlloa llochr.l 0.3! • ...E •Weather Cedes:C-clear,PC-partly cloudy,CI-cloudy,R-rain.:mu-,nun.Si-sleet Spray Irrigation Operator in Responsible Charge(ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: II Mail ORIGINAL and Two COPIES to: ATTN:Non-Discharge Compliance Unit X r ... �[, A -_ �t DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature,1 certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH,NC 27699-1617 DENR Form NDAR-1 (5/2003) NON-DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate(by inserting Y(es)or N(o)in the appropriate box)whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put(NA)in the compliant box.) Compliant(Y,N) I. The application rate(s)did not exceed the limit(s)specified in the permit. II 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s)in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. II S. The freeboard in the treatment and/or storage lagoon(s)was not less than the II limit(s)specified in the permit. If the facility is non-compllant,please explain in the space below the reason(s)the facility was not in compliance with its permit. Provide in your explanation the date(s)of the non-compliance and describe the corrective action(s)taken. Attach additional sheets if necessary. "I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief true,accurate,and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." . �(/� 7" a C ' 1- Baron Neal McDuffie (Signature of Penmitee)* Date (Name of Signing Official-Please print or type) Baron Neal McDuffie (Authorized Agent) Field Services Director(Pace Analytical Services) (Permittee-Please print or type) (Position or Title) 2N.Riverside Plaza,Suite 800 3/31/2021 Chicago.II 60606 (Permit Exp.Date) (Permittee Address) *If signed by other than the Permittee,delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)(2)(D). Pace Analytical Services,LLC aceAnalytieal 1377 South Park Drive Kemersville,NC 27284 www.pacelabe.cors (704)977-0981 April 11, 2022 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lakes Pace Project No.: 9259584/ Dear Tracy Overdurf: Enclosed are the analytical results for sample(s)received by the laboratory on March 29,2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures =��QQ pCCRF0'fo REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, ( i without the wntten consent of Pace Analytical Services,LLC. Page 1 of 24 9ga A/p- Pace Analytical Services,LLC aceAnalytical 1377 South Park Drive Kemersville,NC 272847284 ww.pac.laba.com (704)977-0981 1 CERTIFICATIONS Project: Forest Lakes Pace Project No.: 92595841 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222 North Carolina Wastewater Certification#:40 Pace Analytical Services Eden 205 East Meadow Road Suite A,Eden,NC 27288 North Carolina Wastewater Certification#:633 North Carolina Drinking Water Certification#:37738 VirginiaNELAP Certification#:460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 24 Pace Analytical Services,LLC aceAnalytical® 1377 South Park Drive Kemersville,NC 27284 vrww puelabs com (704)977-0981 SAMPLE ANALYTE COUNT Project: Forest Lakes Pace Project No.: 92595841 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92595841001 MW-1 EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 9222D-2015 LRB 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 5310B-2014 MJP 1 PASI-A 92595841002 MW-2 EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 9222D-2015 LRB 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 5310B-2014 MJP 1 PASI-A 92595841003 MW-3 EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 9222D-2015 LRB 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 5310B-2014 MJP 1 PASI-A 92595841004 MW-4 EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 9222D-2015 LRB 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 5310B-2014 MJP 1 PASI-A 92595841005 Effluent SM 2540C-2015 AED 1 PASI-E SM 2540D-2015 SRS 1 PASI-E EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 5210B-2016 MWF 1 PASI-E Calilert-18 LRB 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.01993 NDS 1 PASI-A EPA 351.2 Rev 2.01993 MFO 1 PASI-A EPA 353.2 Rev 2.01993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 SMT 1 PASI-A PASI-A=Pace Analytical Services-Asheville PASI-E=Pace Analytical Services-Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 24 Pace Analytical Services,LLC 1377 South Parkrive7.. ceAna/yticaI5 Kemersville,NC 27284 www.pacoiabs.com (704)977-0981 1 ANALYTICAL RESULTS Project Forest Lakes Pace Project No.: 92595841 Sample: MW-1 Lab ID: 92595841001 Collected: 03/29/22 09:46 Received: 03/29/22 12:15 Matrix:Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 353.2 NO2/NO3 unpres EDN Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate 0.045 mg/L 0.040 1 03/29/22 16:54 14797-55-8 MBIO 9222D Fecal Collform EDN Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms ND CFU/100 mL 1.0 1 03/29/22 14:36 03/30/22 14:15 300.0 IC Anions 28 Days Analytical Method:EPA 300.0 Rev 2.1 1993 Pace Analytical Services-Asheville Chloride 1.3 mg/L 1.0 1 03/31/22 20:16 16887-00-6 5310B TOC Analytical Method:SM 5310B-2014 Pace Analytical Services-Asheville Total Organic Carbon 3.3 mg/L 1.0 1 03/31/22 17:47 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 24 Pace Analytical Services,LLC aceAnalytical® 1377 South Park Drive Kemersville,NC 27284 www.pacnlaba.caa (704)977-0981 1 ANALYTICAL RESULTS Project: Forest Lakes Pace Project No.: 92595841 Sample: MW-2 Lab ID: 92595841002 Collected: 03/29/22 10:00 Received: 03/29/22 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 NO21NO3 unpres EDN Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate 2.5 mg/L 0.040 1 03/29/22 16:55 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms ND CFU/100 mL 1.0 1 03/29/22 14:36 03/30/22 14:15 300.0 IC Anions 28 Days Analytical Method:EPA 300.0 Rev 2.1 1993 Pace Analytical Services-Asheville Chloride 6.3 mg/L 1.0 1 03/31/22 20:31 16887-00-6 5310B TOC Analytical Method:SM 5310B-2014 Pace Analytical Services-Asheville Total Organic Carbon ND mglL 1.0 1 03/31/22 18:08 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 24 Pace Analytical Services,LLC aceAnalytical® 1377 South Park Drive Kemersvllle,NC 27284 www.pacelabt.eora (704)977-0981 ANALYTICAL RESULTS Project Forest Lakes Pace Project No.: 92595841 Sample: MW-3 Lab ID: 92595841003 Collected: 03/29/22 10:24 Received: 03/29/22 12:15 Matrix: Water Parameters Results Units Report Llmit DF Prepared Analyzed CAS No. Qual 353.2 NO21NO3 unpres EDN Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate 11.5 mg/L 0.20 5 03/29/22 17:19 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms ND CFU/100 mL 1.0 1 03/29/22 14:36 03/30/22 14:15 300.0 IC Anions 28 Days Analytical Method:EPA 300.0 Rev 2.1 1993 Pace Analytical Services-Asheville Chloride 25.1 mg/L 1.0 1 03/31/22 20:45 16887-00-6 5310B TOC Analytical Method:SM 531013-2014 Pace Analytical Services-Asheville Total Organic Carbon ND mg/L 1.0 1 03/31/22 18:26 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 24 Pace Analytical Services,LLC aceAnalytical m 1377 South Park Drive Kemersville.NC 27284 www.psc.labs.cam (704)977-0981 1 ANALYTICAL RESULTS Project Forest Lakes Pace Project No.: 92595841 Sample: MW-4 Lab ID: 92595841004 Collected: 03/29/22 10:12 Received: 03/29/22 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 NO2/NO3 unpres EDN Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate ND mg/L 0.040 1 03/29/22 17:02 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015 Pace Analytical Services-Eden Fecal Coliforms ND CFU/100 mL 1.0 1 03/29/22 14:36 03/30/22 14:15 300.0 IC Anions 28 Days Analytical Method:EPA 300.0 Rev 2.1 1993 Pace Analytical Services-Asheville Chloride 3.8 mg/L 1.0 1 03/31/22 20:59 16887-00-6 5310B TOC Analytical Method:SM 53108-2014 Pace Analytical Services-Asheville Total Organic Carbon ND mg/L 1.0 1 03/31/22 19:20 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 24 Pace Analytical ServIces,LLC aceAnalytical® 1377 South Park Drive Kemersville,NC 27284 www.pacelaba.can (704)977-0981 I ANALYTICAL RESULTS Project Forest Lakes Pace Project No.: 92595841 Sample: Effluent Lab ID: 92595841005 Collected: 03/29/22 09:31 Received: 03/29/22 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! 2540C Total Dissolved Solids Analytical Method:SM 2540C-2015 Pace Analytical Services-Eden Total Dissolved Solids 256 mglL 25.0 1 03/30/22 11:32 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Eden Total Suspended Solids 14.9 mg/L 6.4 1 03/30/22 16:45 353.2 NO2/NO3 unpres EDN Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Eden Nitrogen,Nitrate ND mg/L 0.040 1 03/29/22 16:51 14797-55-8 5210B BOD,5 day EDN Analytical Method:SM 5210B-2016 Preparation Method:SM 5210B-2016 Pace Analytical Services-Eden BOD,5 day 2.9 mg/L 2.0 1 03/30/22 10:11 04/04/22 10:53 R6 Colilert-18 Fecal Coliform EDN Analytical Method:Colilert-18 Preparation Method:Colilert-18 Pace Analytical Services-Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 03/29/22 15:51 03/30/22 10:11 El Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation Pace Analytical Services-Asheville Total Nitrogen 63.5 mg/L 0.040 1 04/11/22 16:40 300.0 IC Anions 28 Days Analytical Method:EPA 300.0 Rev 2.1 1993 Pace Analytical Services-Asheville Chloride 42.2 mg/L 1.0 1 03/31/22 21:14 16887-00-6 350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia 53.8 mg/L 1.0 10 04/07/22 16:03 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2.0 1993 Preparation Method:EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeldahl,Total 63.5 mg/L 2.5 5 04/08/22 02:34 04/09/22 08:49 7727-37-9 353.2 Nitrogen,N021NO3 pres. Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 ND mg/L 0.040 1 04/07/22 12:08 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 8.7 mg/L 0.15 3 04/04/22 17:36 04/05/22 17:04 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 24 Pace Analytical Services,LLC aceAnalytical m 1377 South Park Drive Kemersville,NC 27284 www.pacalabs.com (704)977-0981 QUALITY CONTROL DATA Project Forest Lakes Pace Project No.: 92595841 QC Batch: 688247 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92595841005 METHOD BLANK: 3596830 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 03/30/22 11:31 LABORATORY CONTROL SAMPLE: 3596831 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Dissolved Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 3596832 92595882001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 423 423 0 Results presented on this page are in the units Indicated by the'Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 24 Pace Analytical Services,LLC aceAnalytical a 1377 Soule Park Drive Kemersville,NC 272847284 www.pacelabs.ccrn (704)977-0981 QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 688186 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92595841005 METHOD BLANK 3596600 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 03/30/22 16:43 LABORATORY CONTROL SAMPLE: 3596601 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE: 3596602 92595898001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 2180 1770 21 SAMPLE DUPLICATE: 3596603 92595972001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 27.6 27.7 0 Results presented on this page are In the units indicated by the"Unita"column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services.LLC. Page 10 of 24 Pace Analytical Services,LLC aceAnalytical` 1377 South Park Drive Kemersville,NC 27284 www.paeelabs.eom (704)977-0981 QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 688021 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite,Unpres.EDN Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004,92595841005 METHOD BLANK: 3596099 Matrix: Water Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004,92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,Nitrate mg/L ND 0.040 03/29/22 16:59 LABORATORY CONTROL SAMPLE: 3596100 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,Nitrate mg/L 1.5 1.6 105 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3596101 3596102 MS MSD 92595877004 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc, Conc. Result Result %Rec °Ao Rec Limits RPD Qual Nitrogen,Nitrate mg/L 26,4 1.5 1.5 28.0 28.1 106 112 90-110 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3596103 3596104 MS MSD 92595841005 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Nitrate mg/L ND 1.5 1.5 1.5 1.5 97 97 90-110 0 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full. Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 24 Pace Analytical Services,LLC m aceAnalytical 1377 South Park Drive Kemersville,NC 27284 ' www.panlabs.cam (704)977-0981 i QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 688163 Analysis Method: SM 5210B-2016 QC Batch Method: SM 5210B-2016 Analysis Description: 5210E BOD,5 day Final EDN Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92595841005 METHOD BLANK: 3596543 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD,5 day mg/L ND 2.0 04/04/22 10:11 LABORATORY CONTROL SAMPLE: 3596544 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers BOD,5 day mg/L 198 201 102 84.6-115 SAMPLE DUPLICATE: 3596546 92595887002 Dup Parameter Units Result Result RPD Qualifiers BOO,5 day mg/L 140 138 1 R6 Results presented on this page are In the units Indicated by the"Units'column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 24 Pace Analytical Services,LLC aceAnalytical a 1377 South Park Drive Kemersvi[le,NC 27284 www.pacelabs.com (704)977-0981 QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 688014 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF)-EDN Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004 METHOD BLANK: 3596049 Matrix: Water Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 03/30/22 14:15 METHOD BLANK: 3596051 Matrix: Water Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 03/30/22 14:15 SAMPLE DUPLICATE: 3596050 92595890003 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 255 255 0 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 24 Pace Analytical Services,LLC aceAnalytical 1377 Soule Park 284 Kemersvflle,NC 27284 wtwl.pacelabi.com (704)977-0981 QUALITY CONTROL DATA • Project Forest Lakes Pace Project No.: 92595841 QC Batch: 688024 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal ColifomJ EDN Laboratory: Pace Analytical Services-Eden Associated Lab Samples: 92595841005 SAMPLE DUPLICATE: 3596113 92595945001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN/100mL 4.1 2.0 69 D6 SAMPLE DUPLICATE: 3596114 92595830002 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN/100mL ND ND Results presented on this page are In the units Indicated by the'Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in fug, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 24 Pace Analytical Services,LLC ® 1377 South Park Drive aceAnalytical Kemersville.NC 27284 r www.pacalabs.com (704)977-0981 I QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 688491 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004,92595841005 METHOD BLANK: 3598062 Matrix: Water Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004,92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 03/31/22 13:33 LABORATORY CONTROL SAMPLE: 3598063 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chloride mg/L 50 51.1 102 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3598064 3598065 MS MSD 92596226016 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chloride mg/L 8360 50 50 7560 8460 -1610 204 90-110 11 M1,R1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3598066 3598067 MS MSD 92596226026 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chloride mg/L 7910 50 50 6840 6570 -2150 -2700 90-110 4 M1 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 24 Pace Analytical Services,LLC aceAnalytical® 1377 South Park 284 Kemersville,NC 27284 % www.pae.Iabuma (704)977-0981 I QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 689852 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92595841005 METHOD BLANK: 3604848 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,Ammonia mg/L ND 0.10 04/07/22 15:23 LABORATORY CONTROL SAMPLE: 3604849 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,Ammonia mg/L 5 4.8 96 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3604850 3604851 MS MSD 92595814001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Ammonia mg/L 0.20 5 5 5.0 5.0 97 97 90-110 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3604852 3604853 MS MSD 92595830001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Ammonia mg/L 1.2 5 5 6.2 6.2 99 99 90-110 0 Results presented on this page are In the units Indicated by the"Units'column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 24 Pace Analytical Services,LLC aceAnalytical of 1377 South Park Drive Kemersville,NC 27284 f www.pacalabs.com (704)977-0981 i QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 689954 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92595841005 METHOD BLANK: 3605309 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,Kjeldahl,Total mg/L ND 0.50 04/09/22 07:20 LABORATORY CONTROL SAMPLE: 3605310 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,Kjeldahl,Total mg/L 10 10.1 101 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3605313 3605314 MS MSD 92596508009 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Kjeldahl,Total mg/L ND 10 10 9.3 9.9 92 99 90-110 7 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3607182 3607183 MS MSD 92595866001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Kjeldahl,Total mg/L 7.3 10 10 16.7 16.2 94 90 90-110 3 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 24 aceAna Pace Analytical Services,LLC lytical m 1377 South Park Drive Kemersville,NC 27284 trtvw.petalabLccm (704)977-0981 i QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 689980 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite,preserved Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92595841005 METHOD BLANK: 3605376 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,NO2 plus NO3 mg/L ND 0.040 04/07/22 11:39 LABORATORY CONTROL SAMPLE: 3605377 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,NO2 plus NO3 mg/L 2.5 2.6 102 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3605378 3605379 MS MSD 92596527024 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,NO2 plus NO3 mg/L 0.42 2.5 2.5 2.7 2.7 91 92 90-110 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3605380 3605381 MS MSD 92596527025 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,NO2 plus NO3 mg/L 0.40 2.5 2.5 2.7 2.7 90 90 90-110 0 Results presented on this page are In the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 24 Pace Analytical Services,LLC aceAnalytical0 1377 South Park Drive Kemersville,NC 27284 ! www.paalabe.com (704)977-0981 I QUALITY CONTROL DATA Project Forest Lakes Pace Project No.: 92595841 QC Batch: 689236 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus,Total Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92595841005 METHOD BLANK: 3601737 Matrix: Water Associated Lab Samples: 92595841005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 04/05/22 16:58 LABORATORY CONTROL SAMPLE: 3601738 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3601739 3601740 MS MSD 92595814001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phosphorus mg/L 0.12 2.5 2.5 2.7 2.7 102 105 90-110 2 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3601741 3601742 MS MSD 92595830001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phosphorus mg/L 1.9 2.5 2.5 4.5 4.4 103 99 90-110 2 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 24 Pace Analytical Services,LLC aceAnalytical 1377 South Park Drive Kemersville,NC 27284 wwwpaealaDs.tom (704)977-0981 QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92595841 QC Batch: 688549 Analysis Method: SM 5310B-2014 QC Batch Method: SM 5310B-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004 METHOD BLANK: 3598254 Matrix: Water Associated Lab Samples: 92595841001,92595841002,92595841003,92595841004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 03/31/22 15:28 LABORATORY CONTROL SAMPLE: 3598255 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.3 97 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3598256 3598257 MS MSD 92595832001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Total Organic Carbon mg/L 1,7 25 25 26.1 26.2 98 98 90-110 0 Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 20 of 24 Pace Analytical Services,LLC aceAnalytical m 1 South Park 84 Kemersvllle,NC 27284 www.pacelabs.cots (704)977-0981 QUALIFIERS Project: Forest Lakes Pace Project No.: 92595841 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used.The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. R1 RPD value was outside control limits. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 24 Pace Analytical Services,LLC aceAnalytical® 1377 South Park Drive Kemersville,NC 27284 www.pacalabs.ccm (704)977-0981 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lakes Pace Project No.: 92595841 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92595841005 Effluent SM 2540C-2015 688247 92595841005 Effluent SM 25400-2015 688186 92595841001 MW-1 EPA 353.2 Rev 2.0 1993 688021 92595841002 MW-2 EPA 353.2 Rev 2.0 1993 688021 92595841003 MW-3 EPA 353.2 Rev 2.0 1993 688021 92595841004 MW-4 EPA 353.2 Rev 2.0 1993 688021 92595841005 Effluent EPA 353.2 Rev 2.0 1993 688021 92595841005 Effluent SM 52108-2016 688163 SM 5210B-2016 688246 92595841001 MW-1 SM 9222D-2015 688014 SM 92220-2015 688015 92595841002 MW-2 SM 9222D-2015 688014 SM 92220-2015 688015 92595841003 MW-3 SM 92220-2015 688014 SM 92220-2015 688015 92595841004 MW-4 SM 92220-2015 688014 SM 92220-2015 688015 92595841005 Effluent Colilert-18 688024 Colilert-18 688025 92595841005 Effluent TKN+NO3+NO2 690813 Calculation 92595841001 MW-1 EPA 300.0 Rev 2.1 1993 688491 92595841002 MW-2 EPA 300.0 Rev 2.1 1993 688491 92595841003 MW-3 EPA 300.0 Rev 2.1 1993 688491 92595841004 MW-4 EPA 300.0 Rev 2.1 1993 688491 92595841005 Effluent EPA 300.0 Rev 2.1 1993 688491 92595841005 Effluent EPA 350.1 Rev 2.0 1993 689852 92595841005 Effluent EPA 351.2 Rev 2.0 1993 689954 EPA 351.2 Rev 2.01993 690534 92595841005 Effluent EPA 353.2 Rev 2.0 1993 689980 92595841005 Effluent EPA 365.1 Rev 2.0 1993 689236 EPA 365.1 Rev 2.0 1993 689325 92595841001 MW-1 SM 5310B-2014 688549 92595841002 MW-2 SM 5310B-2014 688549 92595841003 MW-3 SM 5310B-2014 688549 92595841004 MW-4 SM 5310B-2014 688549 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/11/2022 04:42 PM without the written consent of Pace Analytical Services,LLC. 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