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HomeMy WebLinkAboutWQ0001817_Monitoring - 03-2022_20220420 (2) n .. DWR - NonDischarge Monitoring Report Submittal ti ' •4 ... NORTH CAROLINA Enrlranmenlel QHaflly Monitoring Report Submittal .............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................. Permit Number#* WQ0001817 Name of Facility:* Albemarle Utility Company Month:* March Year:* 2022 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR march MR's 2022.pdf 8.71 MB PDF Only GW-59 March MW's2022.pdf 15.32MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2,NDMLR,GW-59). Confirmation Email Address:* danny.perry@albemarleplantation.com Name of Submitter:* Danny S Perry Signature: c ,y Date of submittal: 4/20/2022 This will be filled in automatically Initial Review .............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................. Reviewer: Gerald,Wanda Is the project number correct?* WQ0001817 Is the monitoring report accepted?* Yes No Regional Office* Washington Accepted Date: 5/9/2022 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTALOF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non-Discharge WQ0001817 UIC _ Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED Hertford N.0 27944 County Pergimans ❑■ Lagoon ❑Remediation: Infiltration Gallery 0 Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#:252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name: North of Holding Lagoon No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-1 Date sample collected: 3/18/2022 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 5.9 units Temp.0o010: 16.1 °C DRY at time of Depth to Water Level 82546: 14.0 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec.Cond.00094: µMhos sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Brown/Tan here: Samples for metals were collected unfiltered: ❑YES It NO and field acidified: ❑YES I.NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N Oos15 0.02 mg/L Pb-Lead o1os1 ug/L Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.03 mg/L Zn-Zinc o1o92 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P oosss mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): pissolved Solids:Total 70300 208 mg/L Al-Aluminum o1105 mg/L pH(Lab)00403 5.9 units Ba-Barium 01007 ug/L TOC 00680 5.7 mg/L Ca-Calcium owls mg/L Chloride o0940 7 mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron oloas ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L , method# (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese o1055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonmer t for knowing iiolations. Shayne Lamb Corporate Secretary. • Fr., 4- 1 2-1' Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(I Authorized Agent) Date) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info!environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12104 Site: MW-1 3/18/2022 9:40 AM Water Jay Baker Test Method Results Date Analyzed Color Color Brown/Tan 03/18/2022 Depth to water, ft. Depth to Water,Ft 14.0 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev 2 0. 1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative Sulfur 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 208 mg/L 03/21/2022 Temperature SM 2550 B-2010 16.1 C 03/18/2022 pH SM 4500 H B-2011 5.9 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 5.7 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 7 mg/L 03/21/2022 Nitrate Nitrogen(Cale) Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0.1993 0.05 mg/L 03/22/2022 Nitrate Nitrogen Subtraction Method 0.03 mg/L 03/30/2022 Report#:: 2022-05052 Pace 1 of 10 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL PROCUALITY-DIV.ESSING UNIT WATER RESOURCES INFORMATION UNIT COMPLIANCE REPORT FORM and 1 copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Pont Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name:East of Baffle Lagoon No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: _ (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-2 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.6 units Temp.00o10: 14.3 °C DRY at time of Depth to Water Level 82546: 2.2 ft.below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.00094: µMhos sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid here:❑ Samples for metals were collected unfiltered: ❑YES It NO and field acidified: ❑YES it NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 <0.03 mg/L Pb-Lead 01os1 ug/L Coliform:MF Fecal 31616 10 colonies /100mL Nitrate(NO3)as N ooszo 0.11 mg/L Zn-Zinc o1o92 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 207 mg/L Al-Aluminum o1105 mg/L pH(Lab)00403 5.6 units Ba-Barium 01007 ug/L TOC 00680 25.6 mg/L Ca-Calcium o0916 mg/L Chloride oosa0 ' 8 mg/L Cd-Cadmium 01027 ug/L Arsenic aloo2 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# Total Ammonia oos10 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that.to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowinr violations. Shayne Lamb Corporate Secretary F .01- VI '- Permittee(or Authorized Agent)Name and Title-Please print or type Signa f Permittee r Authorized Agent) Date) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS infofaenvironmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12105 Site: MW-2 3/18/2022 9:53 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Turbid 03/18/2022 Depth to water, ft. Depth to Water,Ft 2.2 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0, 1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids(TDS) SM 2540 C-2015 207 mg/L 03/21/2022 Temperature SM 2550 B-2010 14.3 C 03/18/2022 pH SM 4500 H B-2011 5.6 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 25.6 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 10 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 8 mg/L 03/21/2022 Nitrate Nitrogen(Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.03 mg/L 03/18/2022 N itrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.14 mg/L 03/22/2022 Nitrate Nitrogen Subtraction Method 0.11 mg/L 03/30/2022 Report#. 2022-05052 Pane 2 of 10 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENNFORMATIONTAL QUALITY-DIV.OF WATER RESOURCES PROCESSING UNIT COMPLIANCE REPORT FORM and 1 copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑Remediation: Infiltration Gallery ❑■ Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South East of Spray field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-3 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.3 units Temp.00010: 13.9 °C DRY at Depth to Water Level 82546: 4.2 -12Mhos time of p ft.below measuring point Screened Interval: 2 ft. to ft. Spec.Cond.00094: µ sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 2 gallons Appearance Brown/Turbid here: Samples for metals were collected unfiltered: ❑YES ii] NO and field acidified: ❑YES •NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 0.04 mg/L Pb-Lead 01051 ug/L Coliform: MF Fecal 31616 5 colonies /100mL Nitrate(NO3)as N 00620 0.20 mg/L Zn-Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 707 mg/L Al-Aluminum o1105 mg/L pH(Lab)00403 5.3 units Ba-Barium 01007 ug/L TOC 00680 17.6 mg/L Ca-Calcium 00916 mg/L Chloride oosao <5 mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 _mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) El No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L — ,method# (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the posrloili'y of fines and imprisonment'nr I,nowi ig violations. Shayne Byrum- Corporate Secretary Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) 0 ate) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS infotaenvironmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12106 Site: MW-3 3/18/2022 10:06 AM Water Jay Baker Test Method Results Date Analyzed Color Color Brown/Turbid 03/18/2022 Depth to water, ft. Depth to Water,Ft. 4.2 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0, 1993 <200lJg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 2 (dry)gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 707 mg/L 03/21/2022 Temperature SM 2550 B-2010 13.9 C 03/18/2022 pH SM 4500 H B-2011 5.3 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 8-2014 17.6 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 5 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 < 5 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.04 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0, 1993 0.24 mg/L 03/22/2022 Nitrate Nitrogen Subtraction Method 0.20 mg/L 03/30/2022 Report#:: 2022.05052 Pano 1 of to SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV. GROUNDWATER QUALITY MONITORING: INFORMATIONOF WATER RESOURCES PROCESSING UNIT COMPLIANCE REPORT FORM and Copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans 0 Lagoon ❑Remediation: Infiltration Gallery 0 Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name: South West of Spray field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-4 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400:5.8 units Temp.00010: 15 2 °C DRY at Depth to Water Level 8254s: 4.5 ft.below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.00094: µMhos time of sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here:❑ Samples for metals were collected unfiltered: ❑YES 0 NO and field acidified: ❑YES It NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 0.02 mg/L Pb-Lead 01051 ug/L Coliform: MF Fecal 31616 37 colonies /100mL Nitrate(NO3)as N o0620 0.14 mg/L Zn-Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus:Total as P o0665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): dissolved Solids:Total 70300 191 mg/L Al-Aluminum o1105 mg/L pH(Lab)00403 5.8 units Ba-Barium 01007 ug/L TOC 00680 24.2 mg/L Ca-Calcium 00916 mg/L Chloride oog4o <5 mg/L Cd-Cadmium 01027 ug/L Arsenic o1002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper o1042 mg/L ORGANICS: (by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# _ Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method# _ (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was?roduced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility)f fines and imprisonment fci-kr nv'inc violations. Shayne Lamb-Corporate Secretary it Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee or Authorized Agent) t'Date) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info*environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12107 Site: MW-4 3/18/2022 10:18 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/18/2022 Depth to water, ft. Depth to Water,Ft 4.5 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev 2 0,1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids(TDS) SM 2540 C-2015 191 mg/L 03/21/2022 Temperature SM 2550 B-2010 15.2 C 03/18/2022 pH SM 4500 H B-2011 5.8 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 24.2 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 37 Colonies/100mL 03/18/2022 Chloride SM4500 Cl E-2011 < 5 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.16 mg/L 03/22/2022 Nitrate Nitrogen Subtraction Method 0.14 mg/L 03/30/2022 Report# 2022-05052 Patio a nt in SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL PRTY-DIV.OCESSING G UNIT WATER RESOURCES INFORMATION PR CE COMPLIANCE REPORT FORM and Copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑Remediation: Infiltration Gallery ❑■ Spray Field El Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name: South West of Sprayfield No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-5 Date sample collected: 3/18/2022 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.2 units Temp.00010: 14.3 °C DRY at Depth to Water Level 8254s: 4.9 ft.below measuring point Screened Interval: 12 ft. to 2 ft. Spec.Cond.00094: µMhos time of sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here:❑ Samples for metals were collected unfiltered: ❑YES it NO and field acidified: ❑YES in NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 0.06 mg/L Pb-Lead 01051 ug/L Coliform:MF Fecal 31616 2 colonies /100mL Nitrate(NO3)as N oos2o 0.09 mg/L Zn-Zinc 01092 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): )issolved Solids:Total 70300 142 mg/L Al-Aluminum o1105 mg/L pH(Lab)00403 6.2 units Ba-Barium o1007 ug/L TOC 00680 17.5 mg/L Ca-Calcium mists mg/L Chloride oosao <5 mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils o0552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron m1045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# Total Ammonia ow() <0.2 mg/L Mg-Magnesium 00927 mg/L , method# (Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese o1055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. jj Shayne Lamb - Corporate Secretary 1 1 2_2. Permittee(or Authorized Agent)Name and Title-Please print or type erm (or Authorized Agent) (Date) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax snn 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS infotaenvironmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12108 Site: MW-5 3/18/2022 10:30 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/18/2022 Depth to water, ft. Depth to water,Ft. 4.9 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 142 mg/L 03/21/2022 Temperature SM 2550 B-2010 14.3 C 03/18/2022 pH SM 4500 H B-2011 6.2 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 17.5 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 2 Colonies/100mL 03/18/2022 Chloride SM4500 CIE-2011 < 5 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.06 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0, 1993 0.15 mg/L 03/23/2022 Nitrate Nitrogen Subtraction Method 0.09 mg/L 03/30/2022 Report#.' 2022-05052 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OFT ENVIRONMENTAL OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and Copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑Remediation: Infiltration Gallery 0 Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name: West Of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW - 6 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp.00o10: 14.9 °C DRY at time of Depth to Water Level 82546: 7.8 ft.below measuring point Screened Interval: -2 ft. to -12 ft. Spec.Cond.00094: µMhos sampling, Measuring Point is 3 ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Brown here: Samples for metals were collected unfiltered: ❑YES 0 NO and field acidified: ❑YES ®NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 0.02 mg/L Pb-Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.04 mg/L Zn-Zinc 01092 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 889 mg/L Al-Aluminum 01105 mg/L pH(Lab)00403 5.8 units Ba-Barium 01007 ug/L TOC 00680 7.4 mg/L Ca-Calcium 00916 mg/L Chloride 00940 ' 338 mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that.to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. Shayne Lamb - Corporate Secretary )0111 - 1 Z.2j Permittee(or Authorized Agent)Name and Title-Please print or type Sig• .. • ,_ ori) (Date) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax "' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info'a environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12109 Site: MW-6 3/18/2022 10:41 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Brown 03/18/2022 Depth to water, ft. Depth to Water,Ft. 7.8 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids(TDS) SM 2540 C-2015 889 mg/L 03/21/2022 Temperature SM 2550 B-2010 14.9 C 03/18/2022 pH SM 4500 H B-2011 5.8 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 7.4 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 338 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0, 1993 0.06 mg/L 03/23/2022 Nitrate Nitrogen Subtraction Method 0.04 mg/L 03/30/2022 Report#:: 2022-05052 Paaa R nt 1 n SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and Copy to: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name: West of Baffle lagoon No.of wells to be sampled: 10 ❑ Water Source Heat Pump 0 Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW -7 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 16.9 ft. Well Diameter: 2 in. pH 00400: 5.9 units Temp.mow: 14.2 °C DRY at Depth to Water Level 82546: 3.4 ft.below measuringft. to 16.9Mhos time of p point Screened Interval: 11.9 ft. Spec.Cond.00094: µ sampling, Measuring Point is 2.5 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Red/Tan here:n Samples for metals were collected unfiltered: ❑YES • NO and field acidified: ❑YES iiNO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No.94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N oos15 0.02 mg/L Pb-Lead o1051 ug/L Coliform:MF Fecal 31616 <1 colonies /100mL Nitrate(NO3)as N 00620 0.08 mg/L Zn-Zinc 01092 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 280 mg/L Al-Aluminum 01105 mg/L pH(Lab)00403 5.9 units Ba-Barium 01007 ug/L TOC 00680 12.9 mg/L Ca-Calcium 00916 mg/L Chloride oosao 33 mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 FtMhos K-Potassium 00937 mg/L VOC 7873 ,method# Total Ammonia oo610 0.392 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NHras N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that.to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of tines and imprisonment for know,-ig violations. Shayne Lamb - Corporate Secretary Fri 4 'Vt 1.2 Permittee(or Authorized Agent)Name and Title-Please print or type Si, of Permitt (or Authorized Agent) (gate) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12110 Site: MW-7 3/18/2022 9:30 AM Water Jay Baker Test Method Results Date Analyzed Color Color Red/Tan 03/18/2022 Depth to water, ft. Depth to Water,Ft. 3.4 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 392 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative Sulfur 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 280 mg/L 03/21/2022 Temperature SM 2550 B-2010 14.2 C 03/18/2022 pH SM 4500 H B-2011 5.9 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 12.9 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 33 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.10 mg/L 03/23/2022 Nitrate Nitrogen Subtraction Method 0.08 mg/L 03/30/2022 ±tpo'.# 2022-05052 Pane 7 of 10 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENINFORMATIONAL QUALITY-DIV.PROCESSING OF WATER RESOURCES PR CESSI G UNIT COMPLIANCE REPORT FORM and 1 copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑Remediation: Infiltration Gallery ❑� Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑Land Application of Sludge Well Location/Site Name: East of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW - 8 Date sample collected:3/30/2022 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.1 units Temp.o0010: 14.7 °C DRY at Depth to Water Level 82546: 3.1 ft.below measuringMhos time of point Screened Interval: 5 ft. to 15 ft. Spec.Cond.00094: µ sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here:n Samples for metals were collected unfiltered: ❑YES • NO and field acidified: ❑YES IN NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N oos15 <0.02 mg/L Pb-Lead o1051 ug/L Coliform: MF Fecal 31616 1200 colonies /100mL Nitrate(NO3)as N 00620 0.15 mg/L Zn-Zinc wow mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P doss5 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 362 mg/L Al-Aluminum 01105 mg/L pH(Lab)00403 6.1 units Ba-Barium o1007 ug/L TOC 00680 12.2 mg/L Ca-Calcium 00916 mg/L Chloride oosao 108 mg/L Cd-Cadmium 01027 ug/L Arsenic o1002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# Total Ammonia 00610 0.332 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility or tines and imprisonment for knowir g violations. Shayne Lamb - Corporate Secetary MA' 4 Zl. tr Permittee(or Authorized Agent)Name and Title-Please print or type Sig f Permitte or Authorized Agent) (date) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12111 Site: MW-8 3/18/2022 11:23 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/18/2022 Depth to water, ft. Depth to Water,Ft 3.1 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev,2 0,1993 332 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 362 mg/L 03/21/2022 Temperature SM 2550 B-2010 14.7 C 03/18/2022 pH SM 4500 H B-2011 6.1 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 12.2 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 1200 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 108 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.15 mg/L 03/23/2022 Nitrate Nitrogen Subtraction Method 0.15 mg/L 03/30/2022 �',f # 2322-05052 � SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENINFORMATIONAL QUALITY-DIV.PROCESSING OF WATER RESOURCES ROCESSI G UNIT COMPLIANCE REPORT FORM and 1 copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ0001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑Remediation: Infiltration Gallery ❑■ Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor LI Land Application of Sludge Well Location/Site Name: West of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW - 9 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.6 units Temp.00010: 15.3 °C DRY at time of Depth to Water Level 82546: 4.0 ft.below measuring point Screened Interval: 4 ft. to 14 ft. Spec.Cond.00094: µMhos sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: ❑YES I■I NO and field acidified: ❑YES It NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists, Inc Certification No.94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L Coliform:MF Fecal 31616 64 colonies /100mL Nitrate(NO3)as N 00620 0.18 mg/L Zn-Zinc 01092 mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): )issolved Solids:Total 70300 121 mg/L Al-Aluminum 01105 mg/L pH(Lab)00403 6.6 units Ba-Barium 01007 ug/L TOC 00680 17.4 mg/L Ca-Calcium 00916 mg/L Chloride 00940 6 mg/L Cd-Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 _ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# _ Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method# (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L ,method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief.the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DW R-certified laboratory. I am aware that there are significant penalties for,submitting false information,including the possibility of fines and imp•risonment for known ig violations. Shayne Lamb - Corporate Secretary 4,, , t �m/ \� It Permittee(or Authorized Agent)Name and Title-Please print or type Sign. . -of Permitte j(or Authorized Agent) Date GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12112 Site: MW-9 3/18/2022 10:55 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/18/2022 Depth to water, ft. Depth to Water,Ft 4.0 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev 2 0, 1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids(TDS) SM 2540 C-2015 121 mg/L 03/21/2022 Temperature SM 2550 B-2010 15.3 C 03/18/2022 pH SM 4500 H B-2011 6.6 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 17.4 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 64 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 6 mg/L 03/21/2022 Nitrate Nitrogen(Cale) Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 < 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.18 mg/L 03/23/2022 Nitrate Nitrogen Subtraction Method 0.18 mg/L 03/30/2022 Report# 2022-05052 Paae 9 of 10 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM and copy t0: 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non-Discharge WQ001817 UIC Permit Name(if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford N.C. 27944 County Perquimans ❑■ Lagoon ❑Remediation: Infiltration Gallery ❑■ Spray Field ❑Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South of Spray Field No.of wells to be sampled: 10 ❑ Water Source Heat Pump ❑Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER(from Permit): MW-10 Date sample collected:3/18/2022 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.5 units Temp.00o10: 14.7 °C DRY at Depth to Water Level 82546: 4.8 ft.below measuring point Screened Interval: 5 ft. to 14 ft. Spec.Cond.00094: µMhos time of sampling, Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None _ check Volume of water pumped/bailed before sampling: 5.0 _gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: ❑YES It NO and field acidified: ❑YES IIIIIII NO LABORATORY INFORMATION Date sample analyzed:3/18/2022 Laboratory Name: Environmental Chemists„ Inc Certification No. 94 PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite(NO2)as N 00615 0.02 mg/L Pb-Lead 01051 ug/L Coliform:MF Fecal 31616 4 colonies /100mL Nitrate(NO3)as N 00620 0.03 mg/L Zn-Zinc olosz mg/L Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units): )issolved Solids:Total 70300 104 mg/L Al-Aluminum 01105 mg/L pH(Lab)00403 6.5 units Ba-Barium 01007 ug/L TOC 00680 6.9 mg/L Ca-Calcium oos16 mg/L _ Chloride oo940 ' <5 mg/L Cd-Cadmium 01027 ug/L Arsenic o1002 ug/L Chromium:Total 01034 ug/L Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC) Phenol 32730 ug/L Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0) Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 ,method# Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L , method# _ (Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L , method# TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method# For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowinc violations. i W .W, 22/ Shayne Lamb Corporate SecretaryI Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee 7.r Authorized Agent) t ( ate) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Mar 30, 2022 862 Holiday Island Road Customer PO#: Hertford NC 27944 Customer ID: 09110024 Attention: Report#: 2022-05052 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-12113 Site: MW-10 3/18/2022 11:10 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/18/2022 Depth to water, ft. Depth to Water,Ft. 4.8 feet 03/18/2022 Ammonia Nitrogen EPA 350.1,Rev.2.0, 1993 <200 pg/L 03/23/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/18/2022 Odor Qualitative None 03/18/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 104 mg/L 03/21/2022 Temperature SM 2550 B-2010 14.7 C 03/18/2022 pH SM 4500 H B-2011 6.5 units 03/18/2022 Total Organic Carbon (TOC) SM 5310 B-2014 6.9 mg/L 03/21/2022 Fecal Coliform SM 9222 D-2015 MF 4 Colonies/100mL 03/18/2022 Chloride SM4500 CI E-2011 < 5 mg/L 03/21/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2,Rev 2.0, 1993 0.02 mg/L 03/18/2022 Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 03/23/2022 Nitrate Nitrogen Subtraction Method 0.03 mg/L 03/30/2022 Comment: wutail1/4.6\ ryit Reviewed by: ill ,31.AQ.\-0---/ Report#.: 2022-05052 Paap 1n,,r 1n GW-59A COMPLIANCE REPORT FORM Permit# (A)a (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due.( 30+Will this monitoring report(GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES _ NO ! IF the answer to question 1 or 2 is"YES",list in the space provided below the well identification number(s)and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO identification plate,area overgrown,etc.)?If the answer is "Yes",contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s) exceeding st d rds in the space provided below: > s cam -- *(c -,33 5 For the constituents identified in question 4 above,have standards been exceeded previously for the YES NO same constituent(s)in the same well(s) in the last two years? If the answer to question 5 is"NO", skip to section 8. If the answer to question 5 is "YES",list in the space provided below, each well with constituent(s)exceeding standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO 0' If the answer is "YES",a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is "NO",monitoring wells maybe improperly located;contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO P groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO",contact the Regional Office within 90 days;an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines,and/or penalties. 8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report(Compliance Report GW-59A)is true and complete to the best of my knowledge. Signature of Permittee(or Authorized Agent) Date GW-59A 12/8/2003 AAntic, h a ,), D),,2,, L_e' pH ( h h ci,lvr;ePe 5 ^ r� p 332 7yc\ 52- 4,, 1 1%- i t r j/VI . -'--": 44 - ' .. , • 1-) •itl • 41...j ' ,-.''• ; ; . $ i •e•:,:. '''* v--- .", 14 r::„.,41 i, ., ,-....„ .k.e% ..i.. j. ' 1 :),43 C, ,...,,, . •-:, ,..,1 ..pik ... c.,, • i f•if1/41), i,:,.. 'Ill•I'' ta:..... . 4,:e t-i i— ""i . 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