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Home My WebLink AboutNCG500244_Semi-Annual Sampling Results_20220429#=CL# April 29, 2022 LIMS USE: FR - RUSSELL SUTTON LIMS OBJECT ID: 92600621 92600621 Project: Pace Project No.: RE: Mr. Russell Sutton Premier Magnesia 102 Commerce STreet Waynesville, NC 28786 Outfall 4/21 Dear Mr. Sutton: Enclosed are the analytical results for sample(s) received by the laboratory on April 21, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com Project Manager 1(828)254-7176 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 14 #=CP# CERTIFICATIONS Pace Project No.: Project: 92600621 Outfall 4/21 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 1 Lab ID:92600621001 Collected:04/21/22 10:20 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:121 Date(s)4/21/22 04/29/22 09:121 Time(s)10:20 04/29/22 09:121 Flow 480 GPM 04/29/22 09:121 Analytical Method: Pace Analytical Services - Charlotte Field Data Performed by Pace 04/29/22 09:111 Collected By M.Swann 04/29/22 09:111 Collected Date 4/21/22 04/29/22 09:111 Collected Time 10:20 04/29/22 09:111 pH 8.0 Std. Units 04/29/22 09:111 Temperature 17.8 deg C 04/29/22 09:111 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 2 Lab ID:92600621002 Collected:04/21/22 10:21 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:161 Date(s)4/21/22 04/29/22 09:161 Time(s)10:21 04/29/22 09:161 Flow Dry- Now Flow 04/29/22 09:161 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 3 Lab ID:92600621003 Collected:04/21/22 10:22 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:171 Date(s)4/21/22 04/29/22 09:171 Time(s)10:22 04/29/22 09:171 Flow Dry- No Flow 04/29/22 09:171 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 4 Lab ID:92600621004 Collected:04/21/22 10:27 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:181 Date(s)4/21/22 04/29/22 09:181 Time(s)10:27 04/29/22 09:181 Flow 300 GPM 04/29/22 09:181 Analytical Method: Pace Analytical Services - Charlotte Field Data Performed by Pace 04/29/22 09:181 Collected By M.Swann 04/29/22 09:181 Collected Date 4/21/22 04/29/22 09:181 Collected Time 10:27 04/29/22 09:181 pH 7.7 Std. Units 04/29/22 09:181 Temperature 12.9 deg C 04/29/22 09:181 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 5 Lab ID:92600621005 Collected:04/21/22 10:25 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:191 Date(s)4/21/22 04/29/22 09:191 Time(s)10:25 04/29/22 09:191 Flow 480 GPM 04/29/22 09:191 Analytical Method: Pace Analytical Services - Charlotte Field Data Performed by Pace 04/29/22 09:201 Collected By M.Swann 04/29/22 09:201 Collected Date 4/21/22 04/29/22 09:201 Collected Time 10:25 04/29/22 09:201 pH 7.8 Std. Units 04/29/22 09:201 Temperature 19.8 deg C 04/29/22 09:201 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 6 Lab ID:92600621006 Collected:04/21/22 10:30 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:201 Date(s)4/21/22 04/29/22 09:201 Time(s)10:30 04/29/22 09:201 Flow 250 GPM 04/29/22 09:201 Analytical Method: Pace Analytical Services - Charlotte Field Data Performed by Pace 04/29/22 09:211 Collected By M.Swann 04/29/22 09:211 Collected Date 4/21/22 04/29/22 09:211 Collected Time 10:32 04/29/22 09:211 pH 7.7 Std. Units 04/29/22 09:211 Temperature 11.6 deg C 04/29/22 09:211 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 7 Lab ID:92600621007 Collected:04/21/22 10:32 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:221 Date(s)4/21/22 04/29/22 09:221 Time(s)10:32 04/29/22 09:221 Flow 150 GPM 04/29/22 09:221 Analytical Method: Pace Analytical Services - Charlotte Field Data Performed by Pace 04/29/22 09:221 Collected By M.Swann 04/29/22 09:221 Collected Date 4/21/22 04/29/22 09:221 Collected Time 10:32 04/29/22 09:221 pH 7.8 Std. Units 04/29/22 09:221 Temperature 11.6 deg C 04/29/22 09:221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 14 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92600621 Outfall 4/21 Sample:# 8 Lab ID:92600621008 Collected:04/21/22 10:35 Received:04/21/22 14:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: Pace Analytical Services - Charlotte Flow Monitoring Data Performed by Pace 04/29/22 09:221 Date(s)4/21/22 04/29/22 09:221 Time(s)10:35 04/29/22 09:221 Flow 10 GPM 04/29/22 09:221 Analytical Method: Pace Analytical Services - Charlotte Field Data Performed by Pace 04/29/22 09:231 Collected By M.Swann 04/29/22 09:231 Collected Date 4/21/22 04/29/22 09:231 Collected Time 10:35 04/29/22 09:231 pH 7.8 Std. Units 04/29/22 09:231 Temperature 19.1 deg C 04/29/22 09:231 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 14 #=QL# QUALIFIERS Pace Project No.: Project: 92600621 Outfall 4/21 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 14 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92600621 Outfall 4/21 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92600621001 # 1 92600621002 # 2 92600621003 # 3 92600621004 # 4 92600621005 # 5 92600621006 # 6 92600621007 # 7 92600621008 # 8 92600621001 # 1 92600621004 # 4 92600621005 # 5 92600621006 # 6 92600621007 # 7 92600621008 # 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 04/29/2022 09:25 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 14 Page 13 of 14 Page 14 of 14