WQ0023181_Monitoring - 03-2021_20210415

INTERNATIONAL© PAPER
Global Sourcing — Fiber Supply
PO Box 710
865 John L Riegel Road
Riegelwood NC 28456
910 362 3329(Office)
910 342-2869(Fax)
April 6, 2021
NC Department of Environmental and Natural Resources
Division of Water Quality—Information Processing Unit
1617 Mail Service Center
Raleigh,NC 27699-1677
Dear Sir/Madam,
Enclosed are the completed original and one copy of report#GW59, GW59A, and the lab
report used to complete GW59.
Regards,
Lez
Ben Burger LL
Fiber Specialist a Q g

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DIV.OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT
and 1 copy to:
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Pont Clearly or Type m ,.7�
_ } Q /�i / PERMIT Number(jUL� �3f`� Expiration Date: _� g
Facility Name: l trre_r /Gilt,' Ape] - irC,(�cje't,1c;/ 67,D/f'// Non-Discharge UIC
Permit Name(if different): NPDES NG6 9.10000 Other
Facility Address: 2J4 l CO I I,Y'I 5 ice c) TYPE OF PERMITTED OPERATION BEING MONITORED
N r l I ►1A /1/6 ?756 3 County /AAA f re'1 ❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
Contact Person: &ip) g7fJef Telephone#:ICU"602/-O//O ❑ Rotary Distributor ❑ Land Application ofjS ludge .
Well Location/Site Name: iV f¢ No. of wells to be sampled: A/ 4- El/ Water Source Heat Pump ,� Other.P,1/C �c'c/ 4- Vt lei
(from Permit) fJLie,lj-jt5- Li'i'4°J ,sj�S ft'/".
SAMPLING INFORMATION /1 If WELL
WELL ID NUMBER(from Permit): NI~4 Date sample collected: _3/k./ U 3- I FIELD ANALYSES: WAS
Well Depth: 1 ft. Well Diameter: in. pH 00400: units Temp.00010: °C DRY at
Mhos time of
Depth to Water Level 82546: Air,1i- ft.below measuring point Screened Interval: ft. to ft. Spec.Cond. 00094: µ sampling,
Measuring Point is it/I,/} ft. above land surface Relative M.P. Elevation: Ai/A- ft. Odor 00085: check
Volume of water pumped/bailed before sampling: �i4 gallons / Appearance /J/� here:
Samples for metals were collected unfiltered: LI YES ❑ NO and field acidified: ❑YES ❑ NO
LABORATORY INFORMATION _ A/ �^`� , / �—o� /
Date sample analyzed: 'I'�-2 c-C) 3I Laboratory Name: 5 ✓ v Certification No../'1�7 i/�'Nt 9;9.y
PARAMETERS NOTE:Values shouId1reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N o0613 mg/L Pb-Lead olosi ug/L
Coliform: MF Fecal 31616 /100mL Nitrate(NO3)as N 00620 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 mg/L
(Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 76 mg/L Al-Aluminum o1105 mg/L
pH(Lab)00403 7, ti units Ba-Barium o1007 ug/L
TOC 00680 mg/L Ca-Calcium oosss mg/L
Chloride 00940 is I mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils ooss2 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS,HPLC)
Phenol 32730 C) i C`a Y-1 ug/L Fe-Iron o10a5 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance 000ss AMhos K-Potassium 00937 mg/L VOC 7873 , method#
Total Ammonia 00610 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N oo6zs mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DVVR-certified laboratory. I am aware thatha there are significant penalties for submitting false information,including the possibility g
of fines and imprisonment for knowing violations.
.1.. ...'1.‘, ll`C ;►l IA/ 61-l I �yt,f- - CI' hi Vec I' , /I's 1 e4,)- ' A1/�/ / 0i/9-/
Permitte�-(or Authorized Agent)Name and Title/Please print or type Signature of Permit or Authorized Agent) �t�)
GW-59 Rev.3-1-2016

GW-59A COMPLIANCE REPORT FORM Permit# LI Q c)o3/ /
(Submit one each monitoring period with GfV-59forum)
Enter date monitoring results were due.( ) Will this monitoring report(GW-59 and GW-59A) YES NO
be submitted after the established due date?
2 Was any required information missing on the GW-59 report forms? YES NO
IF the answer to question 1 or 2 is"YES", list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?If the answer is "Yes",contact the Regional Office for guidance.
4 Are any monitored constituents equal to or above the established standards? YES NO
If the answer to question 4 is "NO", skip to section 8.
if the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below:
5 For the constituents identified in question 4 above,have standards been exceeded previously for the YES NO
same constituent(s)in the same well(s)in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES';list in the space provided below, each well with constituent(s)exceeding
standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years).
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO
if the answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE.If the answer is "NO", monitoring wells maybe improperly
located;contact the Regional Office.
7 Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem?
if the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines,and/or penalties.
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report(Compliance Report GW-59A)Is true and complete to the best of my knowledge.
/37&,13
//1//5
natur Permittee(or Aut red Agent)
Date
G\\-59.k 12/8/2003

CO Laboratories
•
Accurate. Timely. .Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC,27511
Phone: [phone] FAX: [phone]
Friday, March 26, 2021
International Paper, Inc. (IN019)
Attn: Ben Burger
SR 1102, 247 CR Collins Road
Norlina, NC 27563
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: NPDES
ENCO Workorder(s): CE04119
Dear Ben Burger,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, March 17, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 1 c=

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SAMPLE SUMMARY/LABORATORY CHRONICLE
-Client ID: Wet Yard Pond Lab ID: CE04119-01 Sampled: 03/16/21 11:32 Received: 03/17/21 10:30
Parameter $gam Hold Date/Time(s1 Prep Date/Time(s1 Analysis Date/Time(s)
EPA 420.1 NO PREP 04/13/21 03/24/21 10:42 03/26/21 10:18
Field ***DEFAULT PREP 03/16/21 11:46 03/16/21 11:32 03/16/21 11:32
***
SM 2540C-2011 NO PREP 03/23/21 03/19/21 13:15 03/19/21 13:15
SM 45001 E-2011 NO PREP 04/13/21 03/17/21 12:59 03/17/21 14:46
SM 4500H+6-2011 NO PREP 03/16/21 11:46 03/24/21 12:14 03/24/21 12:14
SM 5220D-2011 Same 04/13/21 03/22/21 09:16 03/22/21 12:12
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 2 of 9
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SAMPLE DETECTION SUMMARY
L..
Client ID: Wet Yard Pond Lab ID: CE04119-01
Nubia Rnatha Dee MI. 2QL Units MONA t stal
Chemical Oxygen Demand 35 10 10 mg/L SM 5220D-2011
pH 7.4 1.0 1.0 pH SM 4500H+B-2011 Q-01
Temperature 11.3 0 0 °C Field
Temperature for pH(deg.C) 22 pH SM 4500H+B-2011 Q-01
Total Dissolved Solids 76 50 50 mg/L SM 2540C-2011
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 3 of 9

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ANALYTICAL RESULTSIl
Description: Wet Yard Pond Lab Sample ID:CE04119-01 Received: 03/17/21 10:30
Matrix: Surface Water Sampled:03/16/21 11:32 Work Order:CE04119
Project: NPDES Sampled By:Client
Classical Chemistry ParametersIl
^-ENCO Cary certified anayte[NC 5911
Analvte WAS Number) Bsslalts Hu Unita DE Mlz4 EQL Datd1 Mffitlad Mahood fly h1atcs
Chemical Oxygen Demand^ 35 mg/L 1 10 10 1C22012 SM 5220D-2011 03/22/21 12:12 JOC
Chloride[16887-00-6y 1.9 U mg/L 1 1.9 5.0 1C17029 SM 4500CI E-2011 03/17/21 14:46 JAH
pHA 7.4 pH 1 1.0 1.0 1C24016 SM 4500H+B-2011 03/24/21 12:14 ZGW Q-01
Temperature for pH(deg.C) 22 pH 1 1C24016 3M 4500H+B-2011 03/24/21 12:14 ZGW Q-01
Total Dissolved Solids^ 76 mg/L 1 50 50 1C19010 SM 2540C-2011 03/19/21 13:15 LII
Field Parameters
Analvte fCAS Numberl Results Has !milt RE MQL PQL Balms Method Analliad lix 1191ca
Temperature 11.3 °C 1 0 0 1C18005 Field 03/16/21 11:32 CLI
Classical Chemistry Parameters
^-ENCO Orlando certified analyte[NC 4291
Analvte (CAS Number) BEMs flu ltpila RE sfL PQL hatch &Mod &Woad fix Batas
Phenolics^ 0.034 U mg/L 1 0.034 0.050 1C24013 EPA 420.1 03/26/21 10:18 KG
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 4 of 9
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QUALITY CONTROL DATAIl
Classical Chemistry Parameters-Quality Control
Batch 1C17029-NO PREP LLL
Blank(1C17029-BLK1) Prepared:03/17/2021 12:59 Analyzed:03/17/2021 14:37II
Spike Source %REC RPD
Anahste Result Elan POL Units Level Result %REC Limes RPD limit Notes
Chloride 1.9 U 5.0 mg/L L
LCS(1C17029-BS1) Prepared:03/17/2021 12:59 Analyzed:03/17/2021 14:38
Spike Source %REC RPD
-And Result Elan P01. Units Level Rua/ %REC Lea RPD Limit Notes
Chloride 100 5.0 mg/L 100 101 80-120
Duplicate(1C17029-DUP1) Prepared:03/17/2021 12:59 Analyzed:03/17/2021 14:42
Source:CE02243-01
Spike Source %REC RPD
Anahrte Result flan Mk !inits Level Result %REC Limits RPD Limit Notes
Chloride 57 5.0 mg/L 57 0.3 10
Matrix Spike(1C17029-MS1) Prepared:03/17/2021 12:59 Analyzed:03/17/2021 14:39
Source:CE02242-02
Spike Source %REC RPD
Analvte Result Elan P0L Units Level Result %REC Limits RPD Limit Notes
Chloride 40 5.0 mg/L 37.5 1.9 U 107 80-120
Matrix Spike Dup(1C17029-MSD1) Prepared:03/17/2021 12:59 Analyzed:03/17/2021 14:40
Source:CE02242-02 1
Spike Source
Limit M�
%REC RPD
- aisie Result Elan SQL Una Rei�ltt units%REC RPD_Maisie1
Chloride 38 5.0 mg/L 37.5 1.9 U 102 80-120 5 25
Batch 1C19010-NO PREP
Blank(1C19010-BLKI) Prepared&Analyzed:03/19/2021 13:15
Spike Source %REC RPD 1
AneMa Result Elan M. Units Level Root %REC Limits RPD Limit M it4.
Total Dissolved Solids 50 U 50 mg/L
LCS(1C19010-BS1) Prepared&Analyzed:03/19/2021 13:15
Spike Source %REC RPD
Analvte Result Elan P01 Units Level Rehm %REC limits RPD Limit Notes
Total Dissolved Solids 990 50 mg/L 1000 99 80-120
Duplicate(1C19010-DUP1) Prepared&Analyzed:03/19/2021 13:15II
Source:CE02069-02
Spike Source %REC RPD
Analvte Result Elan P01. Units Level golds %REC Limits RPD Limit Mel_
Total Dissolved Solids 620 50 mg/L 660 6 20
Duplicate(1C19010-DUP2) Prepared&Analyzed:03/19/2021 13:15
Source:CE02069-01
Spike Source %REC RPD
Amble Remit flag l'QL Units Level Result %REC Limits RPD Limit Notes
Total Dissolved Solids 50 U 50 mg/L 50 U 20
Batch 1C22012-Same
FINAL This report relates only to the sample as receNed by the laboratory,and may only be reproduced in full. Page 5 of 9 1

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QUALITY CONTROL DATA
1
Classical Chemistry Parameters-Quality ControlII
Batch 1C22012-Same-Continued L
Blank(1C22012-BLK1) Prepared:03/22/2021 09:16 Analyzed:03/22/2021 12:12
Spike Source %REC RPD
Anahtte Result Elite KR Units Level goads %REC Limits RPD LiMlit Notes
Chemical Oxygen Demand 10 U 10 mg/L L
LCS(1C22012-BS1) Prepared:03/22/2021 09:16 Analyzed:03/22/2021 12:12 ■
Spike Source %REC RPD
Ananda Re&u(t Ban PQL Units Level Roidt %REC Limits RPD Limit Notes
Chemical Oxygen Demand 520 10 mg/L 500 103 90-110
Matrix Spike(1C22012-MS1) Prepared:03/22/2021 09:16 Analyzed:03/22/2021 12:12II
Source:CE03245-02
Spike Source %REC RPD
Analvte Result Flan PQL Units Level R %REC Limits RPD Limit Notes
Chemical Oxygen Demand 590 10 mg/L 526 52 102 90-110
Matrix Spike Dup(1C22012-MSD1) Prepared:03/22/2021 09:16 Analyzed:03/22/2021 12:12II
Source:CE03245-02
Spike Source %REC RPD
Anahtte Result Elan POI Units Level Result %REC Limits RPD l jib Notes
Chemical Oxygen Demand 580 10 mg/L 526 52 100 90-110 1 5
Batch 1C24016-NO PREP
LCS(1C24016-BS1) Prepared&Analyzed:03/24/2021 12:14
Spike Source %REC RPD
AnaMe Result Dan P0. Units Level g %REC limits RPD Limit Notes
pH 6.9 1.0 pH 7.00 99 99-101
Duplicate(1C24016-DUP1) Prepared&Analyzed:03/24/2021 12:14II
Source:CE03232-01
Spike Source %REC RPD
Ananda Result Rae PM Units Level gsyit %REC limit RPD Limit Notes
PH 6.5 1.0 pH 6.5 0 25 L
Classical Chemistry Parameters-Quality Control
Batch 1C24013-NO PREP
Blank(1C24013-BLK1) Prepared:03/24/2021 10:42 Analyzed:03/26/2021 10:18111
'
Spike Source %REC RPD
Analvte Result Rae Q41 Units Level )Iseult %REC Limitg RPD UMR l
Phenolics 0.034 U 0.050 mg/L
LCS(1C24013-BS1) Prepared:03/24/2021 10:42 Analyzed:03/26/2021 10:18
Spike Source %REC RPD
finable Result Elan P01. Units Level ges& %REC Limits RPD Limit Notes
Phenolics 0.47 0.050 mg/L 0.500 95 90-110
Matrix Spike(1C24013-MS1) Prepared:03/24/2021 10:42 Analyzed:03/26/2021 10:18
Source:AE01991-01
Spike Source %REC RPD
Amble Result flan P01. Units Level g %REC Limy RPD Limit Notes
Phenolics 0.45 0.050 mg/L 0.500 0.034 U 89 90-110 QM-07,
QM-12
FINAL This report relates only in the sample as received by the laboratory,and may only be reproduced in full. Page 6 of 9

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QUALITY CONTROL DATA
Classical Chemistry Parameters-Quality Control
Batch 1C24O13-NO PREP-Continued
Matrix Spike Dup(1C24013-MSD1) Prepared:03/24/2021 10:42 Analyzed:03/26/2021 10:18
Source:AE01991-01
Spike Source %REC RPD
hnalvte Result Ban PQL Units Level Nowt %REC Limit:`: RPD Limit Notm
Phenolics 0.58 0.050 mg/L 0.500 0.034 U 117 90-110 27 10 QM-07,
QM-12
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 7 of 9

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit(MDL)and the laboratory method
reporting limit(MRL),adjusted for actual sample preparation data and moisture content,where applicable.
U The analyte was analyzed for but not detected to the level shown,adjusted for actual sample preparation
data and moisture content,where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument.This value is considered an estimate.
MRL Method Reporting Limit.The MRL is roughly equivalent to the practical quantitation limit(PQL)and is
based on the low point of the calibration curve,when applicable,sample preparation factor,dilution
factor,and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence(85%or greater
confidence)to make a"tentative identification".
P Greater than 25%concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte-MDL/MRL reported to the highest reporting limit of the component analyses.
Q-01 Analysis performed outside of method-specified holding time.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 8 of 9

L4 .1 .Ic
_o9 10775 Central Port Dr. 4810 Executive Park Court.Suite 111 102-A Woodwinds Industrial Ct.
1Orlando.FL 32824 Jacksonville,FL 32216.6469 Cary.NC 27511
[phone] [phone] Fax[phone] [phone] Fax[phone] Page of
Client Name Project Number Requested Analyses Requested Turnaround
International Paper, Inc.(IN019) [none]
Times
Address Project Name/Desc
SR 1102,247 CR Collins Road NPDES 3 1W Note:e requests seyt to
acceptance by the facility
co
City/ST2ip PO k/Billing Info Um
• CO
Norlina, NC 27563 P Ci E Standard
1Tel Fax Reporting Contact W m
o
[phone] Ben Burger C4� Expedited
Sampler(s)Name.Affiliation(Print) Billing Contact 2 to
Ben Burger to in cCaa Due / /__
Sampler(s)Signature Site Location;Time Zone O Lab Workorder
U a C.Ef)4119
Preservation(See Codes)(Combine as necessary)
Collection Matrix Total r7 of
Item Pt Sample ID(Field Identification) Collection Date Time Comp/Grab (see codes) Containers Sample Comments
Wet Yard Pond 111.4i44 )t stt, U SW 4 X X X X____+ 1 J‘.'.%
U
<--Total#of Containers
Sample Kit Prepared By Dat;Time Ref; uished By Dat rme Received B Date/Time
3 1 \- ..3-I--)2( la30
Co ntsiSpecial Reporting Requirements Relinquis y - Dat line slued Data?line
Relinquished By Date.?me Received y Date?me
$i'yi
r Ws&Tamps on Receipt Condition Upo Receipt
-'c 7 1 Acceptable Unacceptable
Matrix:GW-Groundwater SO-Soil OW-Drinking Water SE-Sediment SW-Surface Water WW-Wastewater A-Air O.Other(detail in comments) Preservation:I-Ice H-HCI N-HNO3 S-H2SO4 NO-NaOH 0-Other(detail in comments)
Note:All samples submitted to ENCO Labs are In accordance with the terms and conditions listed on the reverse of this form,unless prior written agreements exist