WQ0000485_Monitoring - 03-2022_20220413

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DWR - NonDischarge Monitoring Report Submittal
NORTH CAROLINA
ErtNmnmerticl Quelffly
Monitoring Report Submittal
Permit Number#* WQ0000485
Name of Facility:* Valley Proteins Inc-Rose Hill
Month:* March Year:* 2022
Report Information
Type* Upload Document*
GW-59 scan WQ0000485 GW-59 2.15MB
part 1 2022-03 VPRH.pdf
PDF Only
GW-59 scan WQ0000485 GW-59 1.87MB
part 2 2022-03 VPRH.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2,NDMLR,GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter:* Corey Lanier
Signature:
Date of submittal: 4/13/2022
This will be filled in automatically

Initial Review
........................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Reviewer: Gerald,Wanda
Is the project number correct?* WQ0000485
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Accepted Date: 4/25/2022

VALLEY11 r , , a" , INC.
April 12, 2022
Division of Water Resources
Attn: Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Ground Water Quality Monitoring Report (GWQMR)
Valley Proteins Inc. — Rose Hill
To whom it may concern,
Please find enclosed the Groundwater Quality Monitoring Compliance Report for
Surface Irrigation for the month of March 2022 for our Rose Hill Division.
Should you require any additional information or wish to discuss this matter,
please feel free to contact me at 910.289.2083 x 25119.
Sincerely,
Paul White
District Manager
cc: VP Corporate Office
469',How Cut Road
(Rose&-Iti 11p 1'\ 28458
5M0.877.2:590
81•558.0994
Making 4.:1 t : n .b.I. :i.f:fm- re:>G. ..e IraKrsporIad'uof 866 651 8175
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SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: \�\—N \\
COMPLIANCE REPORT FORMNN- \\_
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from ft)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-1 Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 12.46 ft. Well Diameter: 2 in. pHa5ooHe 6.80 units Temp.Nolo: if °C DRY at
Depth to Water Level 82546: 3.6 Screened Interval: 12.46 ft to 2.46 ft. Spec:Cond. 000sa: µMhos time of
Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checlf--;
Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES ❑ NO here:1 1
LABORATORY INFORMATION
Date sample analyzed 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.96 mg/L Zn-Zinc o1o9z mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 144.00 mg/L Al-Aluminum o1105 mg/L Sodium 7.34 mg/L
pH (Lab)00403 6.80 units Ba-Barium 01007 ug/L
TOC 00680 1 mg/L Ca-Calcium owls mg/L
Chloride 00940 5 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe- Iron 01045 ug!L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 77 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? a Yes(0) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia owls <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method# -..
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 ug/L , method#
___........... .......
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified la retry. I am aware that there are significant penalties for submitting false information incturding the possibility of fincs and imprisonment for kt-rr irigviolations
Paul White-District Manager y---& ZZ
Permittee(or Authorized Agent)Name and Title-Please print or type Signa' e of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: ��
COMPLIANCE REPORT FORM ,,� ����'� ,. ..��..��,-.„ A �%y ----- -..,:- N,„
FACILITY INFORMATION Please Piint Clear(y or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin El Lagoon El Remediation: Infiltration Gallery
X Spray Field El Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No. of wells to be sampled: 11 El Water Source Heat Pump ❑ Other:
(from Pe€mit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-2 Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 6.40 units Temp.00010: 17 8 °C DRY at
Depth to Water Level 82546: 12.8 ft. below measuring point Screened Interval: 30.15 ft. to 20.15ft. Spec. Cond. 00094: µMhos time of
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan check
here:
Samples for metals were collected unfiltered: X YES❑ NO and field acidified: X YES ❑NO i
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0 /100mL Nitrate(NO3)as N ooszo 0.06 mg/L Zn-Zinc o1092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 0.05 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 272.00 mg/L Al-Aluminum o11os mg/L Sodium 10.7 mg/L
pH (Lab)00403 6.40 units Ba-Barium o1007 ug/L
TOC 00680 1.3 mg/L Ca-Calcium oos1s mg/L
Chloride 00940 7 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug1L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5.0 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? IN Yes(0) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NF13as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory, I am aware that there are Snihr nt;penalties for submitting false information including the possibility of fines and imprisonment for ks uing violations
Paul White-District Manager itk,s1 hi y J`2 22_
Permittee(or Authorized Agent)Name and Title-Please print or type Si: re of Permt (or Authorized Agent) (Date)
GW-59 Rev,8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original and '� ~� ,`
GROUNDWATER QUALITY MONITORING: „ _
1 copy to ,Alt„,,--.\\�\\�\\ o \ , \o�\\ti\ \
COMPLIANCE REPORT FORM N
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Note-Discharge UIC
Permit Name(if different): NPDES Other
iFacility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: (910)_660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other
(from Permit)
SAMPLING INFORMATION 'If WELL
WELL ID NUMBER(from Permit): MW-4 Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 28.93 ft. Well Diameter: 2 in. pH45ooHB 5.90 units Temp.00010: 15.7 °C DRY at
Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: 28.93 ft. to 18.93ft. Spec. Cond.00094: µMhos time of
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check
here:si
Samples for metals were collected unfiltered: X YES El NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 010s1 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note: Use MPN reetnoa for niggly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 191.00 mg/L Al-Aluminum o11os mg/L Sodium 9.01 mg/L
pH(Lab)00403 5.90 units Ba-Barium 01007 ug/L
TOC 00680 <0.5 mg/L Ca-Calcium oosis mg/L
Chloride 00940 <5.0 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug!L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5.0 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? M Yes(0) ❑ No(0)
Specific Conductance°Doss µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia°aslo <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 uglL , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my I-nuWledge and belief the information submitted in this report is true.acciiiate>and complete?and that the laoorator,analytical data vvas produced using approved methods of analysis,by a
DWR:;eitified lap-oratory I am aware that there are significant;penalties for submitting Take information inctu"3i toy the pcssibalty'`fines and imprisonment for r no,ving viol-mons,
Paul White-District Mana er
V-1�--"2-'2—
Permittee(or Authorized Agent)Name and Title-Please print or type Sigture of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

Mail original i , : e \�\ ® \�`. e` ,-;;W , „
GROUNDWATER QUALITY MONITORING: ,,�°
and 1 copy to \ \\�� \� \\\o\� �\\\�� \\\\O F �e
COMPLIANCE REPORT FORM .,.. ,, -�,��� .a� e
FACILITYINFORIATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑Remediation: Infiltration Gallery
X Spray Field ❑Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit) -_-- ----
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-7A Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Weil Depth: 16 ft. Well Diameter: 2 in. pHa5ooHB 4.70 units Temp.000to: 16.3 °C DRY at
Depth to Water Level 82546: 5.7 ft,below measuring point Screened Interval: 16 ft, to 6 ft. Spec.Cond.00094: µMhos time of
Measuring Point is 2.42 ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checl
Sam ales for metals were collected unfiltered: X YES ii NO and field acidified: X YES 0 NO here:
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N o0615 <0.02 mg/L Pb-Lead 01051 ugiL
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N ooszo 0.05 mg/L Zn-Zinc o1o9z mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note. U e MPN method for Ngnly Lam sa-roes) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Bissolved Solids:Total 70300 279.00 mg/L Al-Aluminum o1105 mg/L Sodium 33.1 mg/L
pH(Lab)00403 4.70 units Ba-Barium 01007 ug/L
TOC 00680 0.6 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 115 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug!L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 25 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? MYes(0) ❑ No(0)
Specific Conductance 00095 uMhos K-Potassium 00937 mg/L VOC 78732: .method# SM 6200C
Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;Nftas N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ------ ug/L ,method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs mg/L VOC Removal
I certify that to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified tilDffT_Rinri I am aware that there are n rttf-t'e n;pmnalties foraubm frarg false`information,including the possibility of fine_and imprrsortr;ent for vr.owrrtg violations /;
Paul White-District Managerilliird I/ —! 2 ZZ.__
Permittee(or Authorized Agent)Name and Title-Please print or type Stgrts `e of Permittee(or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM \ \� \\
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name Field 5-damn ed b farm equi /to re lace No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
__--- _-- (from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): _ MW-8A Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH45ooHa 4.60 units Temp_°onto: 205 oC DRY at
Depth to Water Level 82546: 6.5 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec.Cond.00094: µMhos time of
Measuring Point is 2.5 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sam 0 5.0 gallons Appearance Clear/Tan checl(
Samples for metals were collected unfiltered: X YES LINO and field acidified: X YES ❑ NO there.'
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No, DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N noels <0.02 mg/L Pb-Lead 01051 ug/L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 1.47 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 0.11 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 63.00 mg/L Al-Aluminum cows mg/L Sodium 1.84 mg/L
pH(Lab)00403 4.60 units Ba-Barium 01007 ug/L
TOC oosao 0.50 mg/L Ca-Calcium coals mg/L
Chloride oosao 6 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron o10as ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 23 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? m Yes(0) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;Nil as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 ug/L method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: moil_ Effluent Total VOCs: mg/l- VOC Removal%
t etify that to€is Dust of lily kf0w€ n and iiet the intomrat€on au mrtrsrd in this report-is true gate and mptere, lid€lint the€ctrorato analytical ata a produces usirxp appr rnotretts or arraifima 0p a
O4 rtrfred laboratory,i am rare-Slat there are sipr tiic nt penalties for submitting false irilOrraatton>.ir looting the alb€illy of fines nine.imprisonment for krbalug mdta?:on
Paul White-District Manager s
y/2`-2-2._
Permittee(or Authorized Agent)Name and Title-Please print or type Signattire of Permittee(or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING: Mail original o apy nd \, \ \
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address. 469 Yellow Cut Rd, TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-9 Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 6.60 units Temp.°odic,: 14 °C DRY at
Depth to Water Level 82546: 4.2 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec.Cond.00094: ['Mhos time of
Measuring Point is 3.50 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan chec
Samples for metals were collected unfiltered X YES El NO and field acidified X YES ❑ NO there
LABORATORY INFORMATION
Date sample analyzed. 03/17/2022 03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 0.06 mg/L Pb-Lead 01051 uglL
Coliform: MF Fecal 31616 1 /100mL Nitrate(NO3)as N 00620 0.23 mg/L Zn-Zinc o1o92 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
issolved Solids:Total 70300 213.00 mg/L Al-Aluminum o1105 mg/L Sodium 11.1 mg/L
pH(Lab)00403 6.60 units Ba-Barium 01007 ug/L
TOC 00680 34.9 mg/L Ca-Calcium oasis mg/L
Chloride 00940 8 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug!L Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 25 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? •Yes(0) ❑ No(0)
Specific Conductance°doss µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nrcgen;NO as€,Ammonia Nib-open,Tote) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 1.3 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal
toe that,to the he,,,of my knowledge and belie; tie information submitted in this ert is flue emo te.and camplete.and that the laboratory annlyilme data vtom produr,,o wing agor effioue of andiy5is Ciy a
EriNR-eefilled laboratory tam a-teaP2 that the are signuf ni penaltel2s tor-5rjt auttna taVsz,sntormalrrgt including the osd1ritt}of lines ar 6 imprisonment ment fo)'irnowing sr01s t2e-
Paul White-District Manager lZ —2
Permittee(or Authorized Agent)Name and Title-Please print or type Sign.i"+re o `ermittee(or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING: ry"
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit) --
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-10A Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth 16 ft. Well Diameter: 2 in, pH4500HB 4.60 units Temp.000u 19°4 °C DRY at
Depth to Water Level 82546' 4.2 ft.below measuring point Screened Interval: 16 ft. to 6 ft. Spec.Cond.00094: rtMhos time of
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085' None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear the
Sam les for metals were collected unfiltered: X YES NO and field acidified: X YES NO here:
LABORATORY INFORMATION
Date sample analyzed 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead most ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 <0,02 mg/L Zn-Zinc o1092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P00665 <0.04 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 783.00 mg/L Al-Aluminum o1105 mg/L Sodium 106.0 mg/L
pH(Lab)00403 4.60 units Ba-Barium 01007 ug/L
TOC 00680 3.1 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 294 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 _mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 138 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? igYes(0) ❑ No(0)
Specific Conductance 00095 rtMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia o0s10 0.50 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;Nltas N,Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 0.80 mg/L Ni-Nickel o1067 ug/L , method#
I
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: rrtg/L Effluent Total VOCs: mg/L VOC Removal%
t'reMY'that.to the best of my knowledge end belie`the information sah titted!in this report 15 true accurate,and roMplete and that the laboratory analytical l oat.,was produced using approved nlet1? s.of analysis by a-
DA(Pt-cantired laboratory 1 amaware that thereare aigntcen!pertaltbes for submithno false informat on,including site possdsility art apa and imprisonment for Knowing violations
Paul White-District Manager r� — Y—72 -.2 Z
Permittee(or Authorized Agent)Name and Title-Please print or type Sign re of Pamtttee(or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING: � `
COMPLIANCE REPORT FORM \\ \ .\ \ \-\\
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill.NC 28458 County Duplin ❑ Lagoon III Remediation: Infiltration Gallery
f,
X Spray Field III Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-11A Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pii4500HB 4.40 units Temp.000t( 15 °C DRY at
Depth to Water Level 82546: 5.1 Screened Interval: 16 ft. to 6 ft. Spec.Cond.ono- u.Mhos time of
Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5 0 gallons Appearance Clear chec
Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES ❑ NO here:LA
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N oasis <0.02 mg/L Pb-Lead o10s1 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N oos2o 0.64 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 527.00 mg/L Al-Aluminum o1105 mg/L Sodium 67,1 mg/L
pH(Lab)00403 4.40 units Ba-Barium o1007 ug/L
TOC 00680 2.30 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 133 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 _ug/L Chromium:Total 01034 ug/L
Grease and Oils o0552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 166.0 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? •Yes(0) ❑ No(0)
Specific Conductance 00095 tiMhos K-Potassium 00937 mg/L VOC 78732: . method# SM 6200C
Total Ammonia noslo <0,2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen Mies N Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified Laboratory, I am aware that there are s€gniil nt r for submit-Imo false information,including the possibility n``.nes and imprisonment for knowing violations
Paul White-District Manager 9---/2�2'2_
Permittee(or Authorized Agent)Name and Title-Please print or type Si atura of Permittee(or Authorized Agent) <(Date)

Mail original , . \\\ `
GROUNDWATER QUALITY MONITORING: r f ° ~~ �,
COMPLIANCE REPORT FORM and 1 copy to - d \ = \-� .„ \ -\��\'- \\`
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Faclitty Address: 469 Yellow Cut Rd, TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin El Lagoon ❑ Remediation:Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: f910)660-1173 ❑ Rotary Distributor El Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit) -.
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-12B Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH45ooHe 4.20 units Temp,00010 15 °C DRY at
Depth to Water Level 82546: 6.4 ft.below measuring point Screened Interval: 20 ft_ to 10 ft. Spec.Cond.00094: ttMhos time of
Measuring Point is 3 ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec
Samples for metals were collected unfiltered: X YES ri NO and field acidified: X YES 1=1 NO here:
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N oo6zo 0.1 mg/L Zn-Zinc 01og2 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 460.00 mg/L Al-Aluminum 01105 mg/L Sodium 94.8 mg/L
pH(Lab)00403 4.20 units Ba-Barium o1007 ug/L
TOC 00680 1.90 mg/L Ca-Calcium oos16 mg/L
Chloride 00940 132 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 169 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? in Yes(0) ❑ No(0)
Specific Conductance 00095 ttMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia o0610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen Nljas N Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 0.60 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs: mg/L VOC Removal%
[certify that,to the best of my knowledge and belief the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory I am aware that there are ai niticant alti for tra ltl:rtg false information,including;the p- Ebi)i of fines rid ew nmtre for €ng.violations,
Paul White-District Manager '— /'2- _22._
Permittee(or Authorized Agent)Name and Title-Please print or type Signatu of Permittee(or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING: N ` �� \�'- %
COMPLIANCE REPORT FORM �~ \ \\.
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WO.0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd, TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑ Remediation:Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
- —..._ (from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-13A Date sample collected: 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH4500ND 4.70 units Temp.00010: 15.9 °C DRY at
Depth to Water Level 82546: 6.0 ft.below measuring point Screened Interval: 16 ft. to 6 ft. Spec Cond, 94: pMhos time of
Measuring Point is 3 ft_above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec
Samples for metals were collected unfiltered: X YES❑ NO and field acidified: X YES i [NO here:
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists,Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N oasis 0.06 mg/L Pb-Lead most ug!L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 <0.02 mg/L Zn-Zinc o10s2 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
hum Use 1s1PN m":=ed for highly:uM d samp es) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 25.00 mg/L Al-Aluminum 01105 mg/L Sodium 5.55 m /c L
pH(Lab)00403 4.70 units Ba-Barium 01007 ug/L
TOC 00680 <0.5 mg/L Ca-Calcium oasis mg/L _._
Chloride 0os4o 7 mg/L Cd-Cadmium 01027 ug/L
Arsenic olooz ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper o10a2 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 5.00 mg/L Hg-Mercury 71900 ug!L Lab Report Attached? IM Yes(0) ❑ No(0)
Specific Conductance 00095_ uMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia coslo <0.20 mg/L Mg-Magnesium 00927 mg/L ,method#
. a N ,(38 Nies r, N' g Y'i) Mn-Manganese moss ug/L method#
I _KN as N 00625 <0.50 mgi Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs. mg/L Effluent Total VOCs: rng/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true accurate and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR certified laboratory I am aware that there are significant penalties for submittingfalse information including the possibility of Arcs and intprmgnrnunl.for knuwfn9 violations
Paul White-District Manager ` ----` 2 —.2-1—
Pemiittee(or Authorized Agent)Name and Title-Please print or type Signal re of Permittee(or Authorized Agent) (Date)

Mail original „, „ c,,,, ' ,*\ , . ����'L���\\\ ,� \\-1 AZ ,
GROUNDWATER QUALITY MONITORING:
and 1 copy to O\ \ \\" \"\\\ \ O\ \\\
COMPLIANCE REPORT FORM \ \ 1 \� . .
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date_ 3/31/20125
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
'Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill.NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-14A Date sample collected- 3/17/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.20 units Temp.000lc 16.8 °C DRY at
Depth to Water Level 82546: 3.9 ft. below measuring point Screened Interval: 10 ft, to 2.5 ft_ Spec.Cond.00094: µMhos time of
Measuring Point is 3 ft_above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan chec
Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES ri NO here:1- -[
LABORATORY INFORMATION
Date sample analyzed: 03/17/2022-03/24/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N o0615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0 /100mL Nitrate(NO3)as N 60620 0.46 mg/L Zn-Zinc o1092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):.
Dissolved Solids:Total 70300 1100.00 mg/L Al-Aluminum 01105 mg/L Sodium 113 mg/L
pH(Lab)00403 5.20 units Ba-Barium 01007 uglL
TOC 00680 3.60 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 325 mg/L Cd-Cadmium 01027 ug/L _
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oosas 277 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? is Yes(0) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732 ,method# SM 6200C
Total Ammonia o0610 <0.20 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;NF(as N;Ammonia Nitrogen,Total) --- Mn-Manganese 61055 ug/L , method#
TKN as N 00625 <0.50 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg1L VOC Removal%
I certify that to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR cedified'tabrr iriy,;I am aware that there are wtgnifi rO penalties for sueti€thng false,information,including the possibility of fines and rerpfit.onment for kn+ in violations
1/`lz--1 2—
Paul White-District Manager
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)

r'I(t/ COM 11l1'11A IN 4 t,RW{:Nil'0m W' re a uiiuir11 d1^r'h'l„4Utl:U4 O,1185
i Vda,:buusV war veark anon dorrag porr l.�iV+r
Enter date monitoring results were due.(03131/2022)Will this monitoring report(GW-59 and GW-59A)
be submitted after the established due date? No
2 Was any required information missing on the GW-59 report forms? No
IF the answer to question 1 or 2 is`YES"list in the space provided below the well identification number(s)and explain the
problems encountered in obtaining the required information.
MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co,INC;moving the
replacement well 10'due North per DEQ direction.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missingidenfiliication
plate,area overgrown,etc.)?If the answer is"Yes",contact the Regional Office for guidance No
4 Are any monitored constituents equal to or above the established standards? YES
If the answer to question 4 is"NO",skip to section 8
If the answer to question 4 Is"YES"list the affected wells individually with constituent(s)and concentration(s)exceeding
standards in the space provided below:
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
5 For the constituents identified in question 4 above,have standards been exceeded previously for the same
constituent(s)In the same well(s)In the last two years?
i If the answer to question 5 is"NO",skip to section 8.
If the answer to question 5 is"YES",list in the space provided below,each well with consfituent(s)exceeding standards,
Iconcentration(s)reported,and sample collection date for each occurrence(for the last two years).
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
6
Are the monitoring wells listed in Section 5 located at or beyond the review boundary? YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE.If the answer is "NO",monitoring wells may be Improperly located;contact the
Regional Office.
7 is the permlttee implementing previously approved actions required by the Division Involving this groundwater quality
',.problem? YES
Ilf the answer to question 7 is'YES"describe those actions in the space provided below
If the answer to question 7 is"NO",contact the Regional Office within 90 days;en evaluation may be
;_required to determine the impact the waste disposal system is having at the review and compliance
'...boundaries surrounding this facility.Failure to do so may subject thepermittee fo a Notice of Violation,
tines andforponalttes.
Additional monitoring was performed to identify constituents of TOC in MW No.9.The facility has been
communicating with Mr,Geoff Kegley in the Wilmington Regional Office.
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with
GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above Information was evaluated and the Information submitted in this report
(Compliance Report GW-59A)is true and complete to the best of my knowledge.
Signature of Permit a for Authorized Agent) Dace

Valley Proteins,Inc-Rose Hill(WQ0000485)Groundwater Monitoring Well 2 Year Exceedance History Report
TDS 500 10A 11A 14A
March-22 783 527 1100
November-21 801 722 1230
July-21 706 522 1010_
March-21 684 866
November-20 642 844
July-20 592 908
March-20 659 1180
pH 6.5-8.5 2 4 7A 8A 10A j 11A 12B �13A 14A
March-22 _ 6.40 5.9 4.7 1 4.6 4.6 4.4 4.2 4.7 5.2
_ __ _
November-21 5.50 4.30 4.50 4.00 4.30 4.20 4.20 5.00
July-21 6.10 5.60 4.90 4.60 5.90 4.70 4.60 5.40 5.00
March-21 6.40 5.70 4.90 4.70 5.30 5.00 5.10 5.90 5.40
November-20 6.40 4.50 5.00 4.60 5.00 4.80 5.30 5.70
July-20 6.20 5.10 5.60 5.60 4.30 4.20 5.00 5.80
March-20 4.00 5.40 4.90 5.10 5.00 4.90 5.20
TOC 10 9
March-22 34.9
November-21 26.4
July-21 25.9
March-21 32.9
November-20 43.2
July-20 37.7
March-20
Chloride 250 10A 14A
March-22 294 325 I
November-21 353 .
July-21 425 275
March-21
November-20 295 285
July-20 299
March-20 339
Sulfate 250 14A
March-22 277
November-21 322
July-21
March-21
November-20
July-20
March-20 342

1 viral 111 1i 1 ei it . hl le,,1, ists, 'Inc.
enviroc ' 1 1 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Mar 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-11984 Site: MW-1 3/17/2022 12:30 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 03/17/2022
Depth to water,ft. Depth to Water,Ft. 3.6 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1994 7.34 mg/L 03/23/2022
Sulfate EPA 300.0,Rev.2.1,1993 77 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 144 mg/L 03/18/2022
Temperature SM 2550 B-2010 17.0 C 03/17/2022
pH SM 4500 H B-2011 6.8 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 03/23/2022
Total Organic Carbon(TOC) SM 5310 B-2014 1.0 mg/L 03/21/2022
Fecal Coliform SM 9222 0-2015 MF <1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 5 mg/L 03/21/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.96 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method 0.96 mg/L 03/24/2022
Total Nitrogen(Caic)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 03/23/2022
Total Nitrogen Total Nitrogen 1.0 mg/L 03/24/2022
Report#:: 2022-04985 Page 1 of 11

1 . �1 e 1' I r l'
ion e t , � , sts ; � c
11
® 11 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
. III11 ���� 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoCiPenvironmentalchemists.com
Valley Proteins-Rose Hill Date of Report: Mar 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-11985 Site: MW-2 3/17/2022 12:10 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Tan 03/17/2022
Depth to water, ft. Depth to Water,Ft. 12.8 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1994 10.7 mg/L 03/23/2022
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 272 mg/L 03/18/2022
Temperature SM 2550 B-2010 17.8 C 03/17/2022
pH SM 4500 H B-2011 6.4 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.05 mg/L 03/23/2022
Total Organic Carbon(TOC) SM 5310 B-2014 1.3 mg/L 03/21/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 7 mg/L 03/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.06 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method 0.06 mg/L 03/24/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 03/23/2022
Total Nitrogen Total Nitrogen <0.5 mg/L 03/24/2022
Report#:: 2022-04985 Page 2 of 11

h 4 viro 1,el ta e i ists, ce
��� 'v,, / ; , ;, 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
� �� M 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Mar 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-11986 Site: MW-4 3/17/2022 11:35 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 03/17/2022
Depth to water, ft. Depth to Water,Ft. 5.8 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1994 9.01 mg/L 03/23/2022
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 191 mg/L 03/18/2022
Temperature SM 2550 B-2010 15.7 C 03/17/2022
pH SM 4500 H B-2011 5.9 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 03/23/2022
Total Organic Carbon(TOC) SM 5310 B-2014 <0.5 mg/L 03/21/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 <5 mg/L 03/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mglL 03/24/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 03/23/2022
Total Nitrogen Total Nitrogen <0.5 mg/L 03/24/2022
Report#:: 2022-04985 Page 3 of 11

J'" 1 itof � e
�� �� � � � ��; , e fists, � roc.
p, �% / , �� 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Mar 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-11987 Site:MW-7A 3/17/2022 1:00 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 03/17/2022
Depth to water,ft. Depth to Water,Ft 5.7 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1994 33.1 mg/L 03/23/2022
Sulfate EPA 300.0,Rev.2.1,1993 25 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev,2.0,1993 <0.2 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 279 mg/L 03/18/2022
Temperature SM 2550 B-2010 16.3 C 03/17/2022
pH SM 4500 H B-2011 4.7 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 03/23/2022
Total Organic Carbon(TOC) SM 5310 B-2014 0.6 mg/L 03/21/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 115 mg/L 03/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method 0.05 mg/L 03/24/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 03/23/2022
Total Nitrogen Total Nitrogen <0.5 mg/L 03/24/2022
Report#:: 2022-04985 Page 4 of 11

� viro� , , ;e� .�. � i� I� a: .,ists, �� 111;C.
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U
�� 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
� � ��� � sM 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
/� , r�„ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Mar 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-11988 Site:MW-8A 3/17/2022 1:15 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Tan 03/17/2022
Depth to water,ft. Depth to Water,Ft. 6.5 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1994 1.84 mg/L 03/23/2022
Sulfate EPA 300.0,Rev.2.1,1993 23 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 63 mg/L 03/18/2022
Temperature SM 2550 B-2010 15.7 C 03/17/2022
pH SM 4500 H B-2011 4.6 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.11 mg/L 03/23/2022
Total Organic Carbon (TOC) SM 5310 B-2014 0.5 mg/L 03/21/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 6 mg/L 03/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 1.47 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method 1.47 mg/L 03/24/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 03/23/2022
Total Nitrogen Total Nitrogen 1.5 mg/L 03/24/2022
Report#:: 2022-04985 Page 5 of 11

viro� t le i 111 e g ists,
c
6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,N.0 27954 252.473.5702 Lab/Fax
���� Co) 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Mar 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Daterme Matrix Sampled by
22-11989 Site: MW-9 3/17/2022 11:50 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Tan 03/17/2022
Depth to water, ft. Depth to Water,Ft. 4.2 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1994 11.1 mg/L 03/28/2022
Sulfate EPA 300.0,Rev.2.1,1993 25 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 213 mg/L 03/18/2022
Temperature SM 2550 B-2010 14.0 C 03/17/2022
pH SM 4500 H B-2011 6.6 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 03/23/2022
Total Organic Carbon(TOC) SM 5310 B-2014 34.9 mg/L 03/21/2022
Fecal Coliform SM 9222 D-2015 MF 1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 8 mg/L 03/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 363.2,Rev.2.0,1993 0.06 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.28 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method 0.23 mg/L 03/24/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1093 1.3 mg/L 03/23/2022
Total Nitrogen Total Nitrogen 1.6 mg/L 03/24/2022
Report#:: 2022-04985 Page 6 of 11

l%vr 1 ,;e e, , rists, lyc
d 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
, 1C�rn 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
7t 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Mar 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-04985
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-11990 Site:MW-10A 3/17/2022 10:30 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 03/17/2022
Depth to water,ft Depth to Water,Ft. 4.2 feet 03/17/2022
Sodium EPA 200.7,Rev 4.4,1894 106 mg/L 03/23/2022
Sulfate EPA 300.0,Rev.2.1,1993 138 mg/L 03/21/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.5 mg/L 03/23/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/17/2022
Odor Qualitative None 03/17/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 783 mg/L 03/18/2022
Temperature SM 2550 B-2010 14.2 C 03/17/2022
pH SM 4500 H B-2011 4.6 units 03/17/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 03/23/2022
Total Organic Carbon (TOC) SM 5310 B-2014 3.1 mg/L 03/21/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/17/2022
Chloride SM4500 CI E-2011 294 mg/L 03/21/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.20,1993 <0.02 mg/L 03/17/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 03/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/24/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 0.8 mg/L 03/23/2022
Total Nitrogen Total Nitrogen 0.8 mg/L 03/24/2022
Report#:: 2022-04985 Page 7 of 11