NCG190047_2021 DMR_20220225

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG190000
Marinas and Shipbuilding
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDFS Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG190047
Person Collecting Samples: Mike Zawila
Facility Name: Maycraft Fiberglass Products
Laboratory Name: Data Resources
Facility County: Johnston
Laboratory Cert. No.:
Discharge during this period: Yes
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Yes ❑ No
If so, which Tier (I, II, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall001
Outfall002
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
Black Creek
Black Creek
N/A
Date Sample Collected MM/DD/YYYY
10/29/21
10/29/21
46529
24-Hour Rainfall in inches
0.86
0.86
C0530
TSS in mg/L (100 or 50*)
573
4.19
Estimated New Motor/Hydraulic Oil
NCOIL
usage in gal/month
00340
Chemical Oxygen Demand in mg/L (120)
174
58
00400
pH in standard units (6.0 —9.0 FW, 6.8 —
8.75
7.57
8.5 SW)
01105
Aluminum, total recoverable in mg/ L
1.56
0.176
(0.75 FW, 0.24 SW)
01119
Copper, total recoverable in mg/L
0.0248
< 0.005
(0.010 FW, 0.006 SW)
01051
Lead, total recoverable (as Pb) in mg/ L
0.00939
< 0.001
(0.075 FW, 0.22 SW)
01094
Zinc, total recoverable in mg/L (0.126
0.0699
0.01
FW, 0.095 SW)
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average
00552
Non -Polar Oil & Grease in mg/L (15)
N/A
N/A
*Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, includingthe p9ssibility of fines and imprisonmentfor knowing violations."
Signature of Permittee or Delegated Authorized Individual
Jra-� Wals, Com
Email Address
Date
I C/ — gStl_�1.x1>
Phone Number

DATA PAC KAG E
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT :21-MYC-SW-4
CREATED ON : 11/19/2021 ORDER ID: : 2 1 1 1 O3XI O 1
REPORT TO : VALUE ENVIRONMENTAL CUSTOMER ID : VALUE
Paul Zawila JOB ID
5228 Norway Lane EPA REGULATION : CLEAN WATER ACT
Rockhill SC 29732 EPA COMPLIANCE : NPDES
:THANK YOU FOR CHOOSING DATA RESOURCES, INC. AS YOUR SOURCE FOR
QUALITY LABORATORY SERVICES. DATA RESOURCES, INC. STRIVES TO
PROVIDE UNPARALLELLED SERVICE AND SUPPORT REGARDING YOUR SAMPLE
ANALYSIS REQUIREMENTS_ DATA RESOURCES, INC. PROVIDES TECHNICAL
:EXPERTISE, PROJECT MANAGEMENT SKILLS, CUSTOMER SUPPORT, AND
;ACCURATE TEST RESULTS.
.PLEASE TAKE A MOMENT TO REVIEW THE FOLLOWING DATA PACKAGE.
ON THE FOLLOWING PAGES YOU WILL FIND GENERAL REFERENCE INFORMATION
ABOUT THE DATA PRESENTED IN THIS ANALYSIS REPORT. THIS INFORMATION
:AND MORE CAN BE FOUND ON OUR WEBSITE AT HTTP://DATARESOURCESINC.COM
-
C. Greg Mullinax
Project Manager, Data Resources Inc
Bruce E Watt
Laboratory Director, Data Resources Inc - Columbia
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DocID: DMI637349801

PROJECT :21-MYC-SW-4
CREATED ON : 11/19/2021
REPORT TO : VALUE ENVIRONMENTAL
Paul Zawila
5228 Norway Lane
Rockhill SC 29732
DATA RESOURCES INC
DATA PACKAGE
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
ORDER ID:
: 211103X101
CUSTOMER ID
: VALUE
JOB ID
EPA REGULATION : CLEAN WATER ACT
EPA COMPLIANCE : NPDES
FOR ORGANIZATIONAL PURPOSES THE FOLLOWING DATA PACKAGE
IS DIVIDED INTO SECTIONS AS LISTED BELOW:
PAGE SECTION
i COVER PAGE
ii INDEX PAGE (This page)
1 SAMPLE CONTAINER MANIFEST
2 ANALYTICAL DATA -- PERFORMED BY DATA RESOURCES
9 CHAIN -OF -CUSTODY and SAMPLE RECEIPT RECORDS
12 ANALYTICAL DATA -- PERFORMED BY NETWORK PARTNER
N P - AES
SCDHEC: 98016
25 TOTAL PAGES (Not including COVER and INDEX pages)
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DocID: DM1637349801

.1 . oil.
DATA RESOURCES
OURCES INC
SAMPLE CONTAINER MANIFEST DATARESRD-STE200
1410 ST ANDREWS RD - 57E 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT
:21-MYC-SW-4
CREATED ON
: 2021-11-4
211103X101
ORDER ID; :
REPORT TO
: VALUE ENVIRONMENTAL
CUSTOMER ID : VALUE
Paul Zawila
JOB ID : 1847
Norway Lane
Ro
Rockhill 5C 29732
EPA REGULATION : CLEAN WATER ACT
EPA COMPLIANCE : NPDES
SITE
OUTFALL 001
CONTAINER ID
COLLECTION TIMESTAMP
QTY
MATRIX
C1G
CONTAINER: DESCRIPTION
TYPE SIZE PRESERVATIVE HOLDING
84793
2021-10-2911:19
1
LIQUID
GRAS
TSS—[LOW LEVEL]
Plastic 112 Gal NONE
7 D
9996
2021-10-2911:19
1
LIQUID
GRAB
METALS
Plastic 250 mL 1:1 HNO3
180 D
134046
2021-10-2911:19
1
LfQUiD
GRAB
coo
Plastic 250 mL 1:1 H2SO4
28 D
SITE
OUTFALL 002
CONTAINER
ID
COLLECTION TIMESTAMP
CITY
MATRIX
C1G
CONTAINER: DESCRIPTION
TYPE SIZE PRESERVATIVE
HOLDING
84792
2021-10-2911:26
1
LIQUID
GRAB
TSS--[LOWLEVELI
Plastic 112091 NONE
7 D
9292
2021-10-2911:26
1
LIQUID
GRAB
METALS
Plastic 250 mL 1:1 HNO3
180 D
134047
2021-10-2911:26
1
LIQUID
GRAB
COD
Plastic 250 mL 1:1 Hi
28 D
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PAGE: 1 of 25 DocID: DM1637349801

DATA PACKAGE
PERFORMED AT: DR - COLUMBIA
CERTIFICATION: SCDHEC:40569
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT
:21-MYC-SW-4
CREATED ON
: 11/4/2021
211103X101
ORDER ID: :
REPORTTO
: VALUE ENVIRONMENTAL
CUSTOMER ID : VALUE
Paul Zawila
JOB ID : 1847
5228 Norway Lane
Rockhill SC 29732
EPA REGULATION : CLEAN WATER ACT
EPA COMPLIANCE : NPDES
SITE
CONTAINER.DESCRIPTION
MATRIX GIG COLLECTION TIMESTAMP
CONTAINER ID QTY
TYPE SIZE PRESERVATIVE HOLDING
OUTFALL 001
TSS — [LOW LEVEL]
LIQUID GRAS 2021-10-29 11:19
1 Plastic 1/2 Gal NONE
7 D
TEST
PRIORITY METHOD
TSS
Normal SM 2540 D - 2011
PARAMETER
LIMIT HI PQL DILNTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT QUAL LIMRLO MDL INSTRUMENT
ANALYST
TOTAL SUSPENDED SOLIDS
NA 1 1
mg)L
2021-11-04 09:40 [5.92 days]
573 NA 1
bewatt
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PA GE: 2 of 25 Doc1D: DMI637349801

.1 oil
DATA RESOURCES
DATA PAC KAG E
PERFORMED AT: NP - AES
CERTIFICATION: SCDHEC:98016
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT
:21-MYC-SW-4
CREATED ON
: 11/412021
211103X101
ORDER ID:
:
REPORT TO
: VALUE ENVIRONMENTAL
CUSTOMER ID
:VALUE
Paul Zawila
JOB ID
: 1847
5228 Norway Lane
Rockhill SC 29732
EPA REGULATION
: CLEAN WATER ACT
EPA COMPLIANCE : NPDES
SITE
CONTAINER: DESCRIPTION
MATRIX G!G COLLECTION TIMESTAMP
CONTAINER ID
QTY
TYPE
SIZE PRESERVATIVE HOLDING
OUTFALL 001
METALS
LIQUID GRAB 2021-10-29 11:19
1 Plastic
250 mL 1 1 HNO3
180 D
TEST
PRIORITY
METHOD
ALUMINUM [AL]
Normal
EPA 200.7(1994)
PARAMETER
LIMIT HI
PQL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
(DUAL LIMIT LO
MDL INSTRUMENT
ANALYST
ALUMINUM [7429-90-5]
NA
2021-11-4 12:00 [6.00 days]
Performed
NA
#NETWORK
COPPER [CU]
Normal
EPA 200.7 (1994)
PARAMETER
LIMITHI
PQL DILUTON
UNIT
ANALYSISTIMESTAMP [AGED]
RESULT
QUAL LIMITLO
MDL INSTRUMENT
ANALYST
COPPER [7440-50-8]
NA
2021-11-4 12:00 [6.00 days]
Performed
NA
#NETWORK
LEAD [PB]
Normal
EPA 20C.7 (1994)
PARAMETER
LIMITHI
PQL OILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
QUAL LIMITLO
MDL INSTRUMENT
ANALYST
LEAD
NA
2021-11-4 12:00 [6.00 days]
Performed
NA
#NETWORK
ZINC[ZN]
Nomtal
EPA 200.7 (1994)
PARAMETER
LIMIT HI
PQL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
QUAL LIMITLO
MDL INSTRUMENT
ANALYST
ZINC [7440-66-6]
NA
2021-11-412:00 [6.00days]
Performed
NA
#NETWORK
SITE
CONTAINER: DESCRIPTION
MATRIX C!G COLLECTION TIMESTAMP
CONTAINER ID
QTY
TYPE
SIZE PRESERVATIVE
HOLDING
OUTFALL 001
GOD
LIQUID GRAB 2021-10-29 11:19
1 Plastic
250 mL 1:1 H2SO4
28 D
TEST
PRIORITY
METHOD
[410.4] COD
Normal
EPA410.4(1993)
PARAMETER
LIMIT HI
PQL DILLTON
UNIT
ANALYSISTIMESTAMP [AGED]
RESULT
QUAL LIMITLO
MDL INSTRUMENT
ANALYST
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PAGE: 3 of 25 DoclD: DM1637349801

DATA PAC KAG E
PERFORMED AT: NP - AES
CERTIFICATION: SCDHEC:98016
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX:[phone]
SITE CONTAINER' DESCRIPTION
MATRIX C/G COLLECTION TIMESTAMP CONTAINER ID OTY TYPE SIZE PRESERVATIVE HOLDING
OUTFALL 001 COD NA
CONTINUED... 2021-11-412M [6.00days] Performed NA #NETWORK
[_ACCESS THIS INFORMATION ONLINE: Go to http:IiDataResourcesinr-.com and choose the menu option "CUSTOMER LOGIN"
PAGE: 4 of 25 DoclD: DM1637349801

DATA PACKAGE
PERFORMED AT: DR - COLUMBIA
CERTIFICATION: SCDHEC:40569
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT
:21-MYC-SW-4
CREATED ON
: 11/4/2021
211103X101
ORDER ID: :
REPORTTO
: VALUE ENVIRONMENTAL
CUSTOMER ID : VALUE
Paul Zawila
JOB ID : 1847
5228 Norway Lane
Rockhill SC 29732
EPA REGULATION : CLEAN WATER ACT
EPA COMPLIANCE : NPDES
SITE
CONTAINER: DESCRIPTION
MATRIX CIG COLLECTION TIMESTAMP
CONTAINER ID QTY
TYPE SIZE PRESERVATIVE HOLDING
OUTFALL 002
TSS — [LOW LEVEL]
LIQUID GRAB 2021-10-29 11:26
1 Plastic 112 Gal NONE
70
TEST
PRIORITY METHOD
TSS
Normal SM 2540 D-2011
PARAMETER
LIMIT HI PQL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT QUAL LIMI7LO MDL INSTRUMENT
ANALYST
TOTAL SUSPENDED SOLIDS
NA 1 1
mg1L
2021-11-0409:40 [5-92daysl
4.19 NA 1
6ewatt
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PAGE: 5 of 25 _ DoclD: DM1637349801

DATA PACKAGE
PERFORMED AT: NP - AES
CERTIFICATION: SCDHEC:98016
DATA RESOURCES
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT
:21-MYC-SW4
CREATED ON
: 11/4/2021
211103X101
ORDER ID:
:
REPORTTO
: VALUE ENVIRONMENTAL
CUSTOMER ID
:VALUE
Pau[ Zawila
JOB ID
: 1847
5228 Norway Lane
EPA REGULATION
: CLEAN WATER ACT
Rockhill SC 29732
EPA COMPLIANCE
: NPDES
---[SITE
CONTAINER: DESCRIPTION
MATRIX C1G COLLECTION TIMESTAMP
CONTAINER I❑
OTY
TYPE
SIZE PRESERVATIVE HOLDING
OUTFALL 002
METALS
LIQUID GRAB 2021-10-29 11:26
1 Plastic
250 mL 1:1 HNO3
180 D
TEST
PRIORITY
METHOD
ALUMINUM [AL]
Normal
EPA 200.7(1994)
PARAMETER
LIMITHI
POL DILUTON
UNIT
ANALYSISTIMESTAMP [AGED]
RESULT
QUAL LIMITLO
MDL INSTRUMENT
ANALYST
ALUMINUM [7429-90-5]
NA
2021-114 12:00 (6.00 days]
Performed
NA
#NETWORK
COPPER [CU]
Normal
EPA 200.7 (1994)
PARAMETER
LIMITHI
POL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
QUAL LIMIT LO
MDL INSTRUMENT
ANALYST
COPPER [7440-50-8]
NA
2021-114 12:00 [6.00 days]
Performed
NA
#NETWORK
LEAD [PB]
Normal
EPA 200.7 (1994)
PARAMETER
LIMIT HI
PQL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
QUAL LIMIT LO
MDL INSTRUMENT
ANALYST
LEAD
NA
2021-11412:00 16.00 days]
Performed
NA
#NETWORK
ZINC [ZN]
Normal
EPA 200.7 (1994)
PARAMETER
uMIT HI
PQL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
QUAL LIMIT LO
MDL INSTRUMENT
ANALYST
ZINC [7440-00-0]
NA
2021-114 12:00 [6.00 days]
Performed
NA
#NETWORK
SITE
CONTAINER' DESCRIPTION
MATRIX CIG COLLECTION TIMESTAMP
CONTAINERiD
QTY
TYPE
SIZE PRESERVATIVE HOLDING
OUTFALL 002
COD
LIQUID GRAB 2021-10-29 11:26
1 Plastic
25C mL 1:1 H2SO4
28 D
TEST
PRIORITY
METHOD
[410.41COD
Normal
EPA 410 4 (1993)
PARAMETER
LIMIT Hi
PQL DILUTON
UNIT
ANALYSIS TIMESTAMP [AGED]
RESULT
QUAL LIMIT LO
MDL INSTRUMENT
ANALYST
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PAGE.- 6 of 25 Doc1D: DM1637349801

DATA PACKAGE
PERFORMED AT: NP - AES
CERTIFICATION: SCDHEC:98016
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX: [phone]
SITE CONTAINER: DESCRIPTION
MATRIX CIG COLLECTION TIMESTAMP CONTAINER ID 4TY TYPE SIZE PRESERVATIVE HOLDING
OUTFALL 002 COD NA
CONTINUED... 2021-11-412:00 16.00days] Performed NA #NETWORK
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PAGE 7 of 25 DoclD: DM1637349801

I oil
DATA RESOURCES
DATA PACKAGE
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBiA SC 29210
BUS: 803-561-0331
FAX: [phone]
PROJECT :21-MYC-SW-4
CREATED ON : 11/4/2021
211103X101
ORDER ID: :
REPORTTO : VALUE ENVIRONMENTAL
CUSTOMER la : VALUE
Paul Zawila
JOB ID : 1847
5228 Norway Lane
Rockhill SC 29732
EPA REGULATION : CLEAN WATER ACT
EPA COMPLIANCE : NPDES
REPORT FIELDS DEFINED:
ANALYSIS or SERVICE PERFORMED = The Requested analysis or service performed.
RESULT = The value or answer acquired from requested analysis or service performed.
BDL (Below Detection Limit) indicates result is below listed RDL.
ND (Not Detected) indicates result is below listed MDL.
< (Less than symbol) indicates that result is lower than value reported
> (Greater than symbol) indicates that result is higher than value reported
UNIT = Unit of measure.
dwb = Indentifes result value as Dry Weight Basis.
QUAL = Additional qualification on result [See DATA QUALIFIERS DEFINED section].
RDL = (Reportable Detection Limit) The lowest calibrated result achievable by stated analytical method.
MDL = (Method Detection Limit) The lowest result achievable by stated analytical method.
METHOD = The stated methodology employed for the analysis or service performed.
ANALYSIS DR = The date and time when analysis or service was performed.
ANALYST LOCATOR= The analyst and location that performed the analysis or service. All work is performed by
a division of Data Resources Inc. unless alternate certification number is provided in this field.
PRIORITY = The requested turn -around priority.
DATA QUALIFIERS DEFINED.
C = Analytical result has been confirmed with multiple analyses.
I = Estimated result, result is < RDL but > MDL.
JC = See Job Comments.
J 1 = In replicate analyses surrogate recoveries (2 or more for acid fraction, 2 or more for base/neutral fraction,
1 or more for volatile fraction) were out of range but > 10%. The result is an estimated value.
J2 = In replicate analyses surrogate recoveries (2 or more for acid fraction, 2 or more for base/neutral fraction,
1 or more for volatile fraction) were out of range and < 10%. The result is an estimated value.
J3 = In replicate analyses internal standard area counts were out of range. The result is an estimated value.
OH = Holding Time expired prior to analysis
OH2 = Holding Time expired prior to re -analysis. Initial analysis was performed in holding but with estimated results.
M1 = The MS %R is outside acceptable control limits. However, MSIMSD RPD is in acceptable control limits.
2:1 = The BOD reported result failed to meet the Two One Rule.
SC = See Sample Comments.
2-CHLOROETHYLVINYLETHER -vs- **2-CHLOROETHYLVINYLETHER NOTED ON ANALYSIS REPORT:
Past studies show that 2-Chloroethylvinylether undergoes hydrolysis when collected in preserved (HCI to pH<2)
VOC vials. SCDHEC requires a sampling protocol to involve NON -preserved VOC vials when this parameter is needed.
To provide the best quality data for this parameter, DR will perform a separate analysis at an additional cost.
Should you request this parameter and only provide preserved VOC vials, the analysis of this parameter will be
performed and the parameter identity prefixed with ** to identify this potential issue occuring.
AROCHLOR RESULTS:
Any positive Arochlor result would require analysis for total PCB as decachlorobiphenyl by method 508A (MCL = 0.5 ug/L).
LABORATORY pH, CHLORINE, and TEMPERATURE RESULTS:
If analysis occurs in the lab in excess of 15 minutes of collection, then the result MAY NOT be used for compliance.
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PAGE. 8 of 25 DocID: DM1637349801

DATA RESOURCES
DATA PACKAGE
SAMPLE RECEIPT RECORDS:
- CHAIN OF CUSTODY
- SAMPLE RECEIPT REVIEW
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBIA SC 29210
BUS: 803-561-0331
FAX:[phone]
ACCESS THIS INFORMATION ONLINE: Go to http://DataResourceslnc.com and choose the menu option "CUSTOMER LOGIN"
PAGE: 9 of 25 DocID: DM1637349801

i
loll
OATA RESOURCES
211103X101 i 2.1-MYC-Sti'V-4
CREAiEG t3N : 2 21-11-3
REPORT To : VALUE ; ENVIRONMENTAL
Paul Zawila
5228 Norway Lane
Rockhill SC 29732
SAMPLE RECEIPT
REVIEW PAGE
DATA RE'S0URCES INC
1410 ST ANDRIEWS RD - STE 200
COLUMBIA SC 29210
BUS: 303.561-033 5
FAX: [phone]
dORDE DRL7EFt:211103X 01
CUSTC)MzR if) ; VALUE
JOB ID 1847
EPA REGULATION : CLEAN WATER ACT
EPA COMPLIANCE : NPIES
Delivered via: OR FIELD TECH CLIENT "'M COMMERCIAL COURIER (Specify)
YES NO
Are custody sells used?
is/Are sanople(s) received at temperature of =< EC?
IF NO: Sample Temp at Collection C Ripon Receipt C Time span hourW
Are shippigg containers 1 coolers received in good condition?
Are the Chiain of Custody documents included?
Are the Chain r �i Custody documents complete?
Are sample cotftainers intact and seated?
Were Data, Resources provided containers used?
Is sample Volume received adequate for requested tests?
Are ail sam: pie ntainers accounted for accoeding to the Chain of Custody?
Are all samples' received within holding times?
Are VOC vials free of head space (<6mm bubble)? (check NA it no vials received)
r
0
f Discrepancies Noted, Corrective actions taken for nonconforming samples, or Additional Cpmalents;
NIA
1-1
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PAGE; 10 of 25 DocID: DMI637349801

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DATA RESOURCES
DATA PACKAGE
NETWORK PARTNER SECTION:
NP - AES
DATA RESOURCES INC
1410 ST ANDREWS RD - STE 200
COLUMBlA SC 29210
BUS: 803-561-0331
FAX: [phone]
ACCESS _THIS INFORMATION ONLINE: Go to hUp//DataResourceslnc.com and choose the menu option "CUSTOMER LOGIN"
PAGE., 12 of 25 DocID: DM1637349801

ATA
1tESOURGES INC
ANALYTICAL REPORT
CLIENT
Value Environmental
5228 Norway bane
Rockhill SC 29732
ATTENTION
Paul Zawila
PROJECT ID
211103X 101 /21-MYC-S W-4
LABORATORY REPORT NUMBER
2111678
DATE
November 16, 2021
Data Review By
MG�o`Ic�
Masoudi
ct Manager, AES
NOTE:
ss otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
Presidential Drive, Atlanta, GA 30340.
is SCDHEC certified laboratory # 98016, NCDENR certified tab # 562, GA certified lab # FI—E87582,
AP certified laboratory # E87582
I support services for this project are provided by Data Resources, Inc. All questions regarding this report
Id be directed to your Data Resources, Inc. Columbia Project Manager at 803.561.0331 or Data Resources, Inc.
nville Project Manager at 864.232.8761.
PAGE: 13 of 25 19g6LQ.1Dy%37349801

1111
DATA RESOURCES
SAMPLE CONTAINER MANIFEST
:> CUSTODY and ANALYSES
GOING TO: NP - AES
,;?; III(,�, -�°6
DATA RESOURCES l C
1410 ST t1IVDRZ= WS RD - STE 200
COLt MBIA SC 25210
BUS: 803-561-0331
FAX. [phone]
PROJCCT
: 21 103X101 121-11 YC-SW-4
CREATED ON
: 2D 1-1 -3
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PAGE. 14 of25 PS6�q.2D(yjt37349&01

SAMPLE CONTAINER MANIFEST
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PAGE. 15 of 25 Pg§tD.�D11 §37349801

PROJECT
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PR GE: 16 of 25 j9y fi p4l# 137349801

Analytical Envi4enmental
Services, Inc
Date:
16-Nov-21
Client:
Value Environmental
Client Sample ID:
9996
Project Name:
21.1103X101/21-MYC-SW-4
Collection Date:
10/29/2021 11:19:00 AM
Lab ID:
21311678-001
Matrix:
Aqueous
Analyses
Result
Reporting
Qua] Units BatchID
Dilution
Date Analyzed Analyst
Limit
Factor
Trace Elements
by ICPIMS E200.8
(E200.2)
Aluminum
1560
50.0
ug/L 325442
1
11110/202118707
EA
Copper
24.8
5.00
ug/L 325442
1
11/10/202118:07
EA
Lead
9.39
1.00
ug/L 325442
1
11/101202118:07
EA
Zinc
69.9
10.0
ug/L 325442
1
111101202118:07
EA
Qualifiers: . Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analytc not NFLAC certihcd
B j Analyte detected in the associated method blank
I
Greatce than Result value
PAGE: 17 of 25
E Estimated (value above quantitation range)
S Spike Recovery outside limose due to matrix
Nan See ease narrative
Y Attalyzcd in the Fab which is a deviation Imn the nlztlwd
< Less than Result value
I Estimated value detected below Reporting Limit
19g§�P�PYJ�37349801

Analytical Env! onmental Services, Inc Date: 16-Nov-21
Client: Value Environmental Client Sample ID: 134046
Project Name: 214103XI01121-MYC-SW-4 Collection Date: 10/29/2021 11:19:00 AM
Lab ID: 211111678-002 Matrix: Aqueous
Reporting Dilution
Analyses Result Qual Units l3atchID Date Analyzed Analyst
Limit Factor
Chemical Oxygen Demand (COD) E410.4
Chemical OxI ygen Demand 174
Qualifiers: ' Ualue, ceeds maximum contaminant level
i
BR111 Below reporting limit
11 Holding times for preparation or analysis exceeded
N Analyte not NELAC testified
B Aualylc detected in the associated method blank
n Greater than Result value
MCI mglL R469739 1 11/09/202116:45 SK
E Estimated (value above quardution range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
PAGE: 18 of 25 19SBCDMI§37349801

Analytical Envh
onmental Services, Inc
Date:
€6-Nov-21
Client: V
lue Environmental
Client Sample ID:
9292
Project Name: 21'1103X101/21-MYC-SW4
Collection Date:
10/29/2021 11:26:00 AM
Lab ID: 2111678-003
Matrix:
Aqueous
Analyses
Result
Reporting
Qual Units 13atchID
Dilution
Date Analyzed Analyst
Limit
Factor
Trace Elements by ICPIMS E200.8
(E200.2)
Aluminum
176
50.0
ug/L 325442
1
11/10/202118:10 EA
Copper
BRL
5.00
ug/L 325442
1
11/101202118:10 EA
Lead
BRL
1.00
ug/L 325442
1
11/101202118:10 EA
Zinc
44.1
10.0
ug/L 325442
l
11/10/2021 €8:10 EA
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N . Analyle not NELAC certified
B ! Analyte detcetcd in the associated method blank
> I Greater than Result value
E Estimated (value above quantization range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Attalyzed in the lab which is a deviation from the 9nethad
< Less than Result value
I Estimated value detected below Reporting Limit
PAGE: 19 of 25 19$6CD7DCW JV7349801

Analytical Envi'onmental
Services, Inc
Date: 16-Nov-21
Client. V
lue Environmental
Client Sample ID:
134047
Project Name: 211103X101/21-MYC-SW-4
Collection Date:
10/29/2021 11:26:00 AM
Lab ID: 21.11678-004
Matrix:
Aqueous
Analyses
y
Result
Reporting
Qua, Units BatchlD
Dilution
Date Analyzed Analyst
Limit
Factor
Chemical Oxygen
Demand (COD) E410.4
Chemical Oxygenl
Demand 58.0
10.0 mf)L R469739
1 11/09/202116:45 SK
Qualifiers: * Value exceeds ataximum contaminant level E Estimated (value above quanlitation range)
RRL Maw reporting limit S Spike Recovery outside limits due to matrix
H Holding tines for prcparatiun or analysis oxccoded Narr See case narrative
I I
N Avtalytg not NELAC certified F Analyzed in the lab which is a deviation from the method
H Analyte detected in the associated method blank < Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
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