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NC0006254_2009 Phase II Environmental Site Assessment Report_20091211
Moore&VanAllen RECEIVED December 11, 2009 Peter J. McGrath Jr. DEC 15 2009 Attorney at Law T 704 331 1081 MRO IHSB 2081 F termcg704 378 ath Petermcgrath@mvalaw.com NC Department of Environment & Natural Reso �.P�ENR a Division of Waste Management Moore & Van Allen PLLC Inactive Hazardous Sites Branch Mooresville Office Suite 4700 100 North Tryon Street 610 East Center Avenue Charlotte, NC 28202-4003 Mooresville, North Carolina 28115 Attention: Bruce Paris Re: Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Dear Mr. Paris: This firm represents Blue Ridge Tissue Corporation (`BRTC"), which, pursuant to an asset purchase agreement, in October 2009 acquired from Omni Supply, Inc. ("Omni"), the real property and improvements located at 1427 Yadkin River Road, Patterson, North Carolina (the "Property"). In connection with the acquisition of the Property, BRTC conducted certain investigations of environmental conditions at the Property. The results of that investigation are contained in the report of Limited Phase II ESA soil sampling and NPS-split sampling prepared by S&ME, dated September 18, 2009 (the "Report"). A copy of the Report is enclosed for your reference. The Report indicates that leakage of oil from two small electrical transformers located inside the boiler house on the Property caused staining soil in a location identified in figure 3A of the Report. In addition, a January 2007 fuel oil spill inside the tissue manufacturing plant caused staining of soil in the vicinity of the tissue manufacturing plant on the Property in the location identified in figure 3C of the Report. Omni Supply excavated the stained soil, conducted post -excavation sampling and filled the excavation with clean fill. A report of that activity is included as well. We request your concurrence that no further action is required with respect to the stained soil resulting from the leakage of oil from the two small electrical transformers or from the January 2007 fuel oil spill. In addition, groundwater sampling undertaken at the time of the investigation revealed the presence of iron in groundwater sampled from MW-1, MW-2, and MW-3 as identified in the Report. We know of no releases of iron that have ever occurred on the Property. We request your concurrence that the iron identified in those samples is naturally occurring and that no further action is necessary with respect to such iron. Research Triangle, NC CHAR2\1215815vl Charleston, SC NC Department of Environment & Natural Resources Division of Waste Management December 11, 2009 Page 2 We appreciate your cooperation in this regard. Please contact me if you have any questions. Very truly yours, Moore &Van All PT T 0 Peter J. McGrath PJM/tsm Enclosure cc: Dave Hallock William Plummer CHAR2\ I215815v 1 Peter McGrath From: Marchik, Diane [DMarchik@gklaw.com] Sent: Wednesday, October 07, 2009 10:01 AM To: Peter McGrath Subject: FW: Soil Remediation at Patterson Importance: High Peter - FYI on progress. Peter - would you be available for a call this morning? I would like to introduce you to Mr. Hallock. Diane Marchik Attorney 780 North Water Street Milwaukee, WI 53202-3590 Phone: 414-273-3500 Direct: 414-287-9220 Fax: 414-273-5198 Email: DMarchik@gklaw.com http://www.gklaw.com **Pursuant to Circular 230 promulgated by the Internal Revenue Service, if this email, or any attachment hereto, contains advice concerning any federal tax issue or submission, please be advised that it was not intended or written to be used, and that it cannot be used, for the purpose of avoiding federal tax penalties unless otherwise expressly indicated. This is a transmission from the law firm of Godfrey & Kahn, S.C. and may contain information which is privileged, confidential, and protected by the attorney -client or attorney work product privileges. If you are not the addressee, note that any disclosure, copying, distribution, or use of the contents of this message is prohibited. If you have received this transmission in error, please destroy it and notify us immediately at our telephone number (414) 273-3500.** -----Original Message ----- From: Dave Hallock [mailto:dhallock@npscorp.com] Sent: Wednesday, October 07, 2009 8:43 AM To: Marchik, Diane Subject: FW: Soil Remediation at Patterson FYI --Original Message ----- From: David.Day@sealedair.com[mailto:David.Day@sealedair.com] Sent: Wednesday, October 07, 2009 8:24 AM To: Ted.Bell@sealedair.com Cc: Keith.Galbraith@sealedair.com; Dave Hallock Subject: Soil Remediation at Patterson Per my discussions with Dane Horna of S&ME the soil remediation at the boiler house and tissue mill was performed Tuesday October 6th. Three post excavation samples were taken at the boiler house. Two were found to be non -detectable for oil and grease and the third was 173 vs. the 250 mg/cu meter required cleanup level. However, an additional bucket of soil was removed as an extra precaution. After the favorable lab results were reported back to the site the excavation was backfilled. 1 • The tissue mill soil excavation was completed with two soil samples taken which are to be analyzed today prior to backfilling. To my knowledge there have been no notifications made to the state regarding this remediation activity. Please contact me if I can be of further assistance. David Day MS, CIH, CSP Manager, EHS Auditing Sealed Air Corporation David.Day@sealedair.com 864.433.2766 Phone 864.630.2839 Cell 864.433.2831 Fax N From: David.Day@sealedair.com[mailto:David.Day@sealedair.com) Sent: Wednesday, October 07, 2009 8:24 AM To: Ted.Bell@sealedair.com Cc: Keith.Galbraith@sealedair.com; Dave Hallock Subject: Soil Remediation at Patterson Per my discussions with Dane Horna of S&ME the soil remediation at the boiler house and tissue mill was performed Tuesday October 6th. Three post excavation samples were taken at the boiler house. Two were found to be non -detectable for oil and grease and the third was 173 vs. the 250 mg/cu meter required cleanup level. However, an additional bucket of soil was removed as an extra precaution. After the favorable lab results were reported back to the site the excavation was backfilled. The tissue mill soil excavation was completed with two soil samples taken which are to be analyzed today prior to backfilling. To my knowledge there have been no notifications made to the state regarding this remediation activity. Please contact me if I can be of further assistance. David Day MS, CIH, CSP Manager, EHS Auditing Sealed Air Corporation David.Day@sealedair.com 864.433.2766 Phone 864.630.2839 Cell 864.433.2831 Fax AECOM Environment RECEIVED AECOM 7041 Old Wake Forest Road, Suite 103, Raleigh, NC 27616-3013 DEC 1 T 919.872.6600 F 919.872.7996 www.aecorn.com 5 2009 NCDENR MRO IHSB October 5, 2009 Mr. Dave Hallock Operations Manager, Tissue & Towel National Packaging Service Corporation 3303 Spirit Way Green Bay, WI 54304 Subject: Phase II Environmental Site Assessment Results Omni Supply, Inc., Facility 1427 Yadkin River Road Patterson, North Carolina Dear Mr. Hallock: AECOM Inc. (AECOM) is submitting this letter report to provide a summary of the Phase 11 Environmental Site Assessment (Phase II ESA) conducted during August 2009 at the property located at 1427 Yadkin River Road in Patterson, North Carolina (Site). The primary objectives of these activities were to evaluate recognized environmental conditions (RECs) in connection with the property, including: • The soil quality in the area where the pipe discharges from inside the pump house directly outside the building; • The soil and groundwater quality in the area of the discharge pipe for the sink located inside the maintenance shop that discharges below ground outside the facility; • The groundwater quality in the area of the earthen wastewater treatment ponds, which have been operated since the 1960s to manage wastewater generated during manufacturing operations; and • The groundwater quality in the area of the concrete wastewater containment area that has been operated since the 1960s to manage wastewater generated during manufacturing operations In summary, one constituent, total iron, was detected in one soil sample above soil screening levels and in all three groundwater wells installed during the Phase II ESA at concentrations exceeding the NC 2L groundwater standard, which is 300 micrograms per liter (ug/L). Groundwater samples detected iron in the three installed wells at concentrations ranging from 18,200 ug/L to 43,400 ug/L. AECOM's Phase I ESA at the site did not show that historic site operations, including a cotton or corn mill, had processes that could be the source of the iron. There has never been a reported release of an iron -containing waste at the site. In addition, the current tissue mill pulp process is not known to use iron substances in the process and is therefore not considered a potential source of the observed iron concentrations. Iron is a naturally -occurring element and its presence is probably due to site geologic conditions. Based on AECOM's experience with groundwater sampling in the subject site area, iron concentrations in groundwater are routinely detected well above the state groundwater standards as a result of background iron concentrations. As such, these results indicate that the iron detected in groundwater wells at the site is due to naturally -occurring geologic conditions. AECOM Environnlen` Mr. Hallock October 5, 2009 Page 2 The sections below provide the background and purpose of the investigation and a discussion of the methods and results. Summary tables, figures, and the laboratory analytical report are provided as attachments. BACKGROUND The Site is located on both sides of Yadkin River Road in Patterson (Caldwell County), North Carolina (Figure 1). The production facility is situated at 1427 Yadkin River Road and an office building and wastewater holding ponds are situated at 2002 Roby Martin Road (Figure 2). The Site is owned by Omni Supply, Inc. The July 2009 AECOM Phase I ESA report identified the following RECs at the property; • Floor drains within the pump house are tied into a plastic pipe that flows outside the building. Therefore, any releases in the building would discharge to the soil outside as no locking valve was observed on the pipe. • The sink located inside the maintenance shop in the facility is piped to discharge directly below ground outside the facility. Therefore, any waste material historically discharged down this sink would impact site soil and potentially groundwater. • The unlined earthen wastewater treatment ponds at the facility have been operated since the 1960s with no documentation of the types of wastes or hazardous materials that may have been discharged to the wastewater treatment system. Because the ponds are unlined, there is potential that leaking wastes stored in the ponds could negatively impact local groundwater quality. • The concrete containment area located below the process area has also been in operation since the 1960s with no documentation that the containment system has been inspected to insure its integrity. Therefore, there is potential that wastewater leaking from the concrete containment area could negatively impact local groundwater quality. The following two additional RECs were identified with respect to the subject site in a previous Phase I ESA report (S&ME, 2008): • Apparent leakage from two transformers located inside the boiler house and migration of the fluid to the exterior of the building, where a site plan indicates a former fuel oil UST was located. (Note: This REC was identified in a prior Phase I ESA conducted by S&ME during November 2008. According to site personnel, soil testing has been performed to verify the adequacy of the cleanup, but this information has not been provided to AECOM.) • The interior fuel oil spill that migrated to the exterior of the east side of the manufacturing facility on January 4, 2007 because sampling was not conducted to confirm that all of the contaminated soil had bee removed. (Note: This REC was identified in a prior Phase I ESA conducted by S&ME during November 2008. According to site personnel, soil testing has been performed to verify the adequacy of the cleanup, but this information has not been provided to AECOM.) AECOM understands that these two additional RECs are being evaluated by the site owner and that soil testing has been performed by others to address these RECs. INVESTIGATIVE ACTIVITIES In August 2009 AECOM personnel performed environmental sampling activities at the above referenced site (Figure 1). The methods of the investigation are described in the following sections. AECOM Env ronmem Mr. Hallock October 5, 2009 Page 3 Surface Soil Sampling Soil samples were collected outside the pump house in the vicinity of the plastic discharge pipe and the maintenance shop sink discharge pipe (Figure 2). Soil borings were advanced to one foot below land surface (ft bls) using a decontaminated stainless -steel hand auger and screened for the presence of volatile organic compounds (VOCs) using a photo -ionization detector (PID). A total of five borings were advanced outside the pump house and two borings were advanced adjacent to the maintenance shop sink discharge pipe. The soil sample exhibiting the highest field screening result from each location was collected and submitted for laboratory analysis of VOCs by USEPA Method 8260B and PAHs by Method 8270C. A composite soil sample was collected from the five borings at the pump house (SB-1) and a composite soil sample from two borings at the maintenance shop sink discharge pipe (SB-2) were submitted for laboratory analysis of priority pollutant metals by Methods 200.7/245.1. Monitoring Well Installation Three Type II (i.e., single casing wells installed in saprolite above bedrock) monitoring wells (MW-2 through MW-4) were installed at the Site in August 2009 (Figure 2). Proposed well MW-1 was not installed because direct push technique (DPT) refusal was encountered at eight feet below land surface (ft bls), likely due to bedrock, and before the water table. Each monitoring well was installed using 4.25" diameter DPT rods and was advanced to refusal using a Geoprobe 8010. Continuous soil samples were collected using 4" diameter Macro -Core TM soil samples. Soils were logged using the Unified Soil Classification System (USCS) by a geologist. During advancement of monitoring well MW-2, a perched water zone was encountered at approximately 20 to 22 ft bls. Soil samples were collected from this zone due to the possibility that the source of the perched water is due to leakage from the unlined treatment ponds, impacting soil in the unsaturated zone above the water table. The soil samples were analyzed for VOCs by EPA Method 8260B, PAHs by Method 8270C, Priority Pollutant Metals by Methods 200.7/245.1, sulfate, iron, and chloride. Monitoring wells were constructed with a two-inch diameter polyvinyl chloride (PVC) casing equipped with 10 feet of 0.010-inch slotted PVC screen. A sand pack was placed around the well screen that extended approximately two feet above the top of the well screen. A bentonite seal was placed approximately two to three feet above the sand pack and hydrated. The remainder of the well annulus was filled with grout to the ground surface. Each well was secured with a locking expansion plug. Monitoring wells MW-2 and MW-3 were completed with a three foot steal "stick-up" casing with a locking cover surrounded by a two -foot by two -foot concrete pad. Monitoring well MW-4 was completed with a flush -mount protective cover surrounded by a two -foot by two -foot concrete pad. A summary of well construction details is provided in Table 1. After installation, monitoring wells MW-2 and MW-3 were developed by pumping until the turbidity decreased. Monitoring well MW-4 was not developed after installation because the well was set in clean medium and coarse sand. No oily sheens, emulsions, or other indicators of free phase product were observed in the water during well development. Groundwater Sampling Groundwater samples were collected from monitoring wells MW-2, MW-3, and MW-4 on August 17, 2009. AECOM personnel measured the static groundwater level in each well prior to sampling using an electronic water level meter. The groundwater levels from the wells are presented on Table 1. AECOM Env rcnn ant AECOM Mr. Hallock October 5, 2009 Page 4 Prior to sampling, water was purged from each well using low -flow techniques and new polyethylene tubing. Monitoring well MW-2 was sampled using a bladder -pump and monitoring wells MW-3 and MW-4 were sampled with a peristaltic pump. Water quality measurements of pH, conductivity, temperature, oxidation- reduction potential (ORP), and dissolved oxygen (DO) were collected using a YSI 556 water quality meter with a flow -through cell. Turbidity measurements were collected using a LaMont 2020 Turbidimeter. Once water quality parameters stabilized, groundwater samples were transferred into laboratory prepared sample containers, labeled, and chilled on ice pending shipment via currier to Pace Laboratories in Huntersville, North Carolina. The samples were analyzed for VOCs by EPA Method 8260B, PAHs by Method 8270C, Priority Pollutant Metals by Methods 200.7/245.1, and total dissolved solids (TDS), sulfate, nitrite/nitrate, iron, and chloride. Copies of the groundwater sample collection records are found in Appendix A. INVESTIGATIVE RESULTS The results of the investigative activities are discussed below. Soil boring logs are presented in Appendix A. Electronic copies (on compact disc) of the laboratory reports are provided as Appendix B. Site Hydrology Soil borings were drilled from 0 to 50 feet bls. Based on the soil borings drilled, the site is underlain by partially weathered bedrock. At MW-1, refusal was encountered at 8 feet bls. This refusal depth was assumed to be the bedrock surface. The depth to groundwater ranged from approximately 5 to 40 feet based on water level measurements in the three wells on August 12 and 13, 2009. A groundwater potentiometric map is presented on Figure 3. Based on the available data, groundwater flow direction in the surficial aquifer is towards the east toward the Yadkin River. Soil Analytical Results Detected soil analytical results are summarized on Table 2. The detected soil analytical results were compared to the North Carolina Hazardous Waste Section soil screening levels. The investigation revealed the following; • Ten metals were detected above laboratory reporting limits including, antimony, arsenic, beryllium, chromium, copper, iron, lead, mercury, nickel, and zinc; • Iron, mercury, and zinc were the only metals detected at concentrations above the North Carolina Hazardous Waste Section soil screening levels of 151 mg/kg, 0.015 mg/kg, and 550 mg/kg, respectively. Iron was detected in soil sample MW-2 (20-22') with a concentration of 4,680 mg/kg. Mercury was detected in samples MW-2 (20-22') and SB-1 (0-1') with concentrations of 0.015 mg/Kg and 0.030 mg/kg, respectively. Zinc was detected in soil sample SB-1 (0-1') with a concentration of 806 mg/kg. • Acetone was the only VOC detected in soil above laboratory reporting limits but below the North Carolina Hazardous Waste Section soil screening levels. • No PAHs were detected in soil samples above laboratory reporting limits. • Chloride, nitrogen/nitrate, and sulfate were detected in soil sample MW-2 (20-22') at concentrations of 85.5 micrograms per kilogram (pg/kg), 94.4 pg/kg, and 88.2 pg/kg, respectively. AECCf,.1 Ermmnn en= LCOM Mr. Hallock October 5, 2009 Page 5 Groundwater Analytical Results Detected groundwater analytical results are summarized on Table 3. The investigation revealed the following; • Four metals were detected above laboratory reporting limits including arsenic, iron, lead, and zinc; • Iron was the only metal detected above the North Carolina Groundwater Standard listed in 15A NCAC 2L .0200 (2L Standard) of 300 micrograms per liter (pg/L). Iron was detected in monitoring wells MW-2, MW-3, and MW-4 with concentrations of 43,400 pg/L, 18,200 tag/L, and 33,400 pg/L, respectively; • PAHs were not detected in groundwater samples above laboratory reporting limits; • Chlorobenzene, chloroform, and toluene were the only VOCs detected in groundwater above laboratory reporting limits, but their concentrations were below 2L Standards; • Chloride, sulfate, and total dissolved solids were detected in groundwater at concentrations below their 2L Standards. CONCLUSIONS The results of AECOM's Phase II Environmental Site Assessment at the Omni Supply property in Patterson, North Carolina indicated that the VOCs, PARS, and inorganic parameters tested were not detected at concentrations exceeding applicable standards in soil or groundwater samples. Ten metals were detected in soil samples, but only iron, mercury, and zinc were detected above North Carolina Hazardous Waste Section soil screening levels. Mercury and zinc were not detected in groundwater; therefore, these two metals are not potential contaminants of concern. One constituent, total iron, was detected in one soil sample above soil screening levels and in all three groundwater wells installed during the Phase II ESA at concentrations exceeding the N. C. 2L groundwater standard. AECOM's Phase I ESA at the site did not show that historic site operations, including a cotton or corn mill, had processes that could be the source of the iron. There has never been a reported release of an iron -containing waste at the site. In addition, the current tissue mill pulp process is not known to use iron substances in the process and is therefore not considered a potential source of the observed iron concentrations. Iron is a naturally -occurring element and its presence is probably due to site geologic conditions. Based on AECOM's experience on other projects in the area, iron is routinely detected in groundwater samples well above the state groundwater standards due to background conditions. As such, these results indicate that the iron observed in groundwater wells at the site is due to naturally -occurring geologic conditions. Because iron is a naturally -occurring element and its presence is likely due to geologic conditions at the subject site, it is also possible that the biological breakdown of organic matter in the ponds may create an anaerobic environment that changes the chemistry of the aquifer and allows for iron oxides to be reduced, thereby locally increasing the naturally occurring iron concentration in the aquifer. We believe the elevated iron concentrations in the soil and groundwater at the site are due to background geologic conditions based on the following: • The current tissue mill pulp process is not known to use iron substances in the process; • There has never been a reported release of an iron -containing waste at the site; AECOM Environment AEt.{),M Mr. Hallock October 5, 2009 Page 6 • The concentration of iron detected on site is consistent with DWQ data for other wells in the site area; and • iron is a naturally occurring substance in soil and groundwater. However, because iron was detected in the groundwater wells at concentrations exceeding the groundwater standard, the owner should notify NCDENR to request concurrence that the iron concentrations are naturally occurring and do not require any further actions at the site. If you have any questions concerning this report, or if you would like additional information, please contact Michael Dail or Bill Bremen at (919) 872-6600. Sincerely yours, Mic ael Dail P.G. Staff Geologist Bill Bremen, PE, CPEA Senior Project Managf- Attachments: Tables Figures Appendix A: Groundwater Sample Collection Records Appendix B: Laboratory Analysis Report 9 AECOM Environment I AECOM Tables AECOM r W J m Q F C E O L yy r v N ao N 3 C N N O) p ,� Q Z rM N N O N = > N O y T T (� W L d R p T V T W Z T d J y CD m L L o 0 0 Z T T T co � co°� m � o O o m 0 C N O O N U O Q cri w r� _ O M Z M N N Q. d T T o w a _ m R f1± J Q O L? O CV d a; Co Z o oLo v O .0 CL O m co LO N O H a m m m rn N d o 0 0 0 ++ T T M T M T = o o O o 0 T N M V am C_ N N U � o � 6 04 CU C > f6 3 0 0 c 0 a) c a� 0 'cu z ? E U � H 0 cn 0 4 J f- O o0 m Q Z Z 2 � E 0 C_ #« w 9< h w e w k <<< /%&ƒ S z 2 g 2 z z z CO)/ / ` o v JT \ � CD k � M to o /\ 2\/\ © a z z z @ o � R ❑ � co « k CN N \ n ® \ ® 2 R ® \ / / e f @ i OR / _@ 2$$ Q 2® v 2 04 \ k � S 9 _ dco $ LO / q @ # 0 2 't o m m m % 2\/ S 2 Q% z z z 2 o r w%/ d � z � 2 z k � 2 k E z 2 m � R / k 0 k a £ £ q 2 k g 2 z z / w w a k g\ 1 0® / a o a 0?< = E E$ of Eƒ 0\ o w w LU/®\ m 0 n z w E I 0» w w U z m O n I E g m 1 O=3<< c O O u 5 z n=<=) I o z m / 7 2 o N o \ \ cn �� ) \ E co \n \ƒ m § § 2 6 : ..j \\ §\/ �_ =n- f0 /\ P2\ a \:tcu om > 5> ®/E2 /ƒ§ //ƒ\\ \\\ 2ƒ\k} R�0 // //=Q E22§m (n —J 2a e-mm \fly®m= G\ s c/ o M _ E 2% I< k k E e e m §j/0 m EE/to s 0 (n U) o\\=- z m m & / k cu �a 2 U Q 2 2 w / 0 � ■ I-- a m = a 2 O o g �m Yto CD CD 0 7 CD CD CD m CD\ A G \ Qƒ v Q 2 2 v / § k w n R¥ R / 7 \ § o e a= n y 3 & � n 7 2 � CN % o$ CD (0R R g\ 3 0 \ § # \ \ q Q Q v w \ � � 2 _ 2 0= o G o o R'a « o G 0 S 0 / a 2 2 9 o w v c - a 3 a m LO Cm V) o U') N 7 LU g U m -i 6 S l -ae q d u o o o A CO o (D 00 w Z (1) - n - ® _ z w _ \ � � z / / 0 a c ° O ° 3 0ƒ m u @ w ° % 3 m r« 2 u «± u« E®« E § Lu $ 2 O \ \ \ w \ / u cnOf « m I I o I= n 0 n n =)<* 2 N= Q o e 0 m R / 6 j § \\ C) s= K E2 P =n z E / \/ \ m / CDk \\ \ C)w 7 f\w G ® %�co ®/\ �§ &o6 &£& />G 0--0:E \ e -0 _0 m _ - c - m \ / ] \ / / § C)ca-0 0 m e ] e $ & a) 2 -In z a E 2//0 = k§§8\ m in y = = m })°°Q§a ,±]G� \d\$= k KKK / ~ o e e » - z o o § / Figures AECOM Appendix A Groundwater Sample Collection Records AECOM ENSR I AECOM Well ID: rvq"JZ Low Flow Ground Water Sample Collection Record Client: OMr, 6-pplX Date: %j /D`1 Time: Start am/pm Project No: j 3 66 Finish am/pm Site Location: PAfk-sm, Weather Conds: Govcl y i (fir, w f 4e,.y,? (N 1610is Collector(s): 1. WATER LEVEL DATA: (measured from Top of Casing) - c. Length of Water Column d,61 a b Casing Diameter/Material a. Total Well Length `.�' �,.1{ g ( ) b. Water Table Depth q4, 90 d. Calculated System Volume (see back)>4� qPt 2. WELL PURGE DATA a. Purge Method: all.r b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit - ORP ± 10mV - Sp. Cond. 3% - Drawdown < 0.3' c. Field Testing Equipment used: Make Model Y5 T 556 Serial Number am Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity FlowRateJ Drawdown I Color/Odor (24hr) (Liters) PC) (as/cm) (ma/L) - m-v) (NTU) (ml/min)(Teell 41 211 19 (6 'y-a 3a 50.5 CW� 246 2LO L 6.0 / 4.6� y� z `i6,5 a Sa,0 11 aBb '-5 la-aol 6, ,1 191 13' -36.1 r!•-1`f 156144 S5 10 )�,66 6 0. Ilo '4,65 -3q.4 q'11 ii Some 306 3.7_ a7.'-f8 6.Aa 2w TIT-- - 40.4 6,6'�r n �► 't 375 1 3.qI l2.`12 6.3a 111 1,46 -46.-4 1 q,X5 1310 1 3,6 13.08 6.12 1 3,3� 1tim I -q:f,y 1 5,SL It� t. d. Acceptance criteria pass/tail Yes No N/�9t (continued on back) Has required volume been removed El Has required turbidity been reached ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. I.W 410,w 5,.y 3. SAMPLE COLLECTION: Method: sIX•/ Sam le ID Container Type No. of Containers Preservation Analysis Req. Time /VIW-a.. 10) Comments Signature zi J Date �111164 TNIZ, ' O I Ta,,p f33 '�3G QD aRP —5d.4 �%<b l fl Q, ,ec ", �MiJ50, I315 3,fs� �3,l3 1,53 %-2a w 132e !d �3iF�i 6i2ja AJ1 I,ql -50 r 1) 13a5 ,?, ),3,U4 4,33 1,31 —55,7 I,q'1- u� ii u Well ID: MW Low Flow Ground Water Sample Collection Record Client: 6Mn. 6yru� • Date: 8/ 11bl, Time: Start 1345 am/pm Project No: I3(46-c61-41 Finish am/pm Site Location: Ps*rsan , "L WeatherConds: Collector(s): 1. WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length 13,1W c. Length of Water Column 4.34 (a-b) Casing Diameter/Material �L I PV L b. Water Table Depth 16.i d. Calculated System Volume (see back) v 2. WELL PURGE DATA eo a. Purge Method: � b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit - ORP ± 10mV - Sp. Cond. 3% - Drawdown < 0.3' c. Field Testing Equipment used: Make Model ,56 Serial Number 41ilOM AR 7 g- y'04 Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Rate Drawdown I Color/Odor 194hrl /l itercl N11 !uS/rml Imn/Ll (mV► (NTIJ) (ml/min)(Teel fgdb .0 All 6 aI I 4SI 6.55 - ,u .n 1100 1 g,3► <1-r- No-pi D ;0.52 5.9-11 V-7- d,w� -13.1 6,51 It 1916 it 1 % 5.0 ia.&y 5.H6I 1107 0.41 —15:4 >.35 IT2 II 91� `i=d 6:4-S 6.0 q1I .34 106 150 x5 :5o 111,4-e 16.m4 1 04307 —w.ci 0.43 36 Dp,15 ;a.61� 6.0 4 ^� v,�°�F . I 0-06 o If, I s 1. d. Acceptance criteria pass/fall Yes No N/fj( (continued on back) El El Has required volume been removed Has required turbidity been reached [�/ ❑ ❑ Have parameters stabilized ❑ ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Sample ID Container Type No. of Containers Preservation Analysis Req. Time MW-3 1500 Comments Signature t :) P Date 07/0� ENSR I AECOM . Well ID: /A m4 Low Flow Ground Water Sample Collection Record Client: 06; S'at-V Date: S/ 11164i Time: Start I6U am/pm Project No: I13Ig0-aV!j-,pW1 Finish am/pm Site Location: FA-r5on WL ry1 Weather Conds: Collector(s): I ' �� A 1..WATER LEVEL DATA: (measured from Top of Casing) a. Total Well Length c. Length of Water Column b. Water Table Depth ` ; a1 d. Calculated System Volume (see back; 2. WELL PURGE DATA a. Purge Method: b. Acceptance Criteria defined (see workplan) - Temperature 3% -D.O. 10% - pH + 1.0 unit - ORP ± 10mV - Sp. Cond. 3% - Drawdown < Off c. Field Testing Equipment used: Make Y51 (a-b) Casing Diameter/Material �1i( PVL Model Serial Number 556 r l ;��LIGL i AA Volume Time Removed Temp. pH Spec. Cond. DO ORP Turbidity Flow Ratel Drawdown I Color/Odor /74hrl 11 itarc) (oCl /uS/rml 11; Ll (mV (NTU) (ml/min) ee 3N5 6,66 -46,0 15 q1 Gfe� 44 21,43 C.11 3qy 03 M,4 35.0 £l .5 3 ,1�4 344 .35 -`dlr3 6 T 452 .5 21 5� 6;1� 351 !� 31 -5�2,5 ,yb ►1 11 Iq56 6,5 I 6,13 352 0,9* -g 1,46 ,I ►► d. Acceptance criteria pass/tail Yes No N/ (continued on back) Has required volume been removed ❑ ❑ Has required turbidity been reached [� ❑ ❑ Have parameters stabilized ❑ ' ❑ If no or N/A - Explain below. 3. SAMPLE COLLECTION: Method: Sample ID Container Type No. of Containers Preservation Analysis Req. Time Mti✓ � '� Comments Signature A ' 1 J, Date 7//7/6 Appendix B Laboratory Analysis Report AECOM /!ZAnalytical' evw.pace/abscorn I August 26, 2009 Mr. Bob Wyrick AECOM Environment 7041 Old Wake Forest Road Suite 103 Raleigh, NC 27616 RE: Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Dear Mr. Wyrick: Pace Analytical services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on August 14, 2009. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, 'g.r , era- A.,Y4 � Felicia Grogan felicia.grogan@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac Page 1 of 32 aceAnalytica! MWY/.VaceI8D5.LVR1 i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Charlotte Certification IDS Connecticut Certification #: PH-0104 Florida/NELAP Certification If: E87627 West Virginia Certification #: 357 Virginia Certification #: 00213 Tennessee Certification #: 04010 South Carolina Drinking Water Cod. #: 990060003 South Carolina Certification M 990060001 Asheville Certification IDS Connecticut Certification #: PH-0106 Virginia Certification #: 00072 Tennessee Certification M 2980 South Carolina Certification #: 99030001 South Carolina Bioassay Certification #: 99030002 Pennsylvania Certification #: 68-03578 West Virginia Certification #: 356 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pennsylvania Certification #: 68-00784 North Carolina Wastewater Certification #: 12 North Carolina Field Services Certification M 5342 North Carolina Drinking Water Certification M 37706 New Jersey Certification M NC012 Louisiana/LELAP Certification M 04034 Kentucky UST Certification #: 84 North Carolina Drinking Water Certification #: 37712 North Carolina Bioassay Certification M 9 New Jersey Certification #: NC011 Massachusetts Certification #: M-NCO30 Louisiana/LELAP Certification #: 03095 Florida/NELAP Certification #: E87648 North Carolina Wastewater Certification #: 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. Inc.. 'nelac; Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 32 aceAnalytical / axw.Pacela6acom i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received 9250959001 SB-1(0-1) Solid 08/12/0909:30 08/14/0913:44 9250959002 SB-1 (0.1) Solid 08/13/0914:00 08/1410913:44 9250959003 MW-2 (20-22) Solid 08/12/09 18:00 08114/0913:44 9250959004 SB-2 (0.1) COMP Solid 08/14/09 10:30 08/14/09 13:44 9250959005 SB-2 (0-1) GRAB Solid 08/14/09 10:30 08/14/09 13:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac` Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 32 aceAnalylical axw.pace/a6soxn i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9260959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 9250959001 SB-1 (0-1) ASTM D2974-87 TNM 1 PASI-C EPA 6010 SHB 12 PASI-A EPA 7471 SAJ 1 PASI-A 9250959002 SB-1 (0-1) ASTM D2974-87 TNM 1 PASI-C EPA 8260 DLK 71 PASI-C EPA 8270 by SIM BET 21 PASI-C 9250959003 MW-2 (20.22) ASTM D2974-87 TNM 1 PASI-C ASTM D516-90 LEP 1 PASI-A EPA 353.2 DMN 3 PASI-A EPA 6010 SHB 13 PASI-A EPA 7471 SAJ 1 PASI-A EPA 8260 ELK 71 PASI-C EPA 8270 by SIM BET 21 PASI-C SM 4500-CI-E LEP i PASI-A 9250959004 SB-2 (0-1) COMP ASTM D2974-87 TNM 1 PASI-C EPA 6010 SHB 12 PASI-A EPA 7471 SAJ 1 PASI-A 9250959005 SB-2 (0-1) GRAB ASTM D2974-87 TNM 1 PASI-C EPA 8260 ELK 71 PASI-C EPA 8270 by SIM BET 21 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac Page 4 of 32 aceAnalytical w»w.pacelabs.com I Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville. NC 28078 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: SB-1 (0-1) Lab ID: 9250959001 Collected: 08/12/09 09:30 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony 3.5 mg/kg 0.69 1 08/18/09 12:45 08/19/09 16:24 7440-36-0 Arsenic 4.5 mg/kg 0.69 1 08/18/09 12:45 08/1910916:24 7440.38-2 Beryllium 0.69 mg/kg 0.14 1 08/1810912:45 0812010918:34 7440-41-7 Cadmium NO mg/kg 0.14 1 08/18/09 12:45 08119/0916:24 7440-43-9 Chromium 17.0 mg/kg 0.69 1 08/18/09 12:45 0811910916*24 7440-47-3 Copper 111 mg/kg 0.69 1 08/18/09 12:45 0811910916:24 7440-50-8 Lead 108 mg/kg 0.69 1 08/1810912:45 08/19/0916:24 7439-92-1 Nickel 29.1 mg/kg 0.69 1 08/18/09 12:45 08/19/09 16:24 7440-02-0 Selenium ND mg/kg 1.4 1 08/18/09 12:45 08119/0916:24 7782-49-2 Silver ND mg/kg 0.69 1 0811810912:45 08119/0916:24 7440-22-4 Thallium ND mg/kg 1.4 1 08/18/09 12:45 08119/0916:24 7440-28-0 Zinc 806 mg/kg 1A 1 0811810912:45 08/19/0916:24 7440-66-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.030 mg/kg 0.0057 1 08/20/09 09:23 08/20/09 13:43 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 29.2 % 0.10 1 08/18/09 08:15 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac`• m Page 5 of 32 ;ace Analytical' tmwpacelabs.corn i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SIB-1 (0-1) Lab ID: 9250959002 Collected: 08/13/09 14:00 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 8270 MSSV PEE PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3545 Acenaphthene NO ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 83-32-9 Acenaphthylene NO uglkg 13.6 1 08118/0914:00 08/24/0916:36 208-96-8 Anthracene NO uglkg 13.6 1 08118/0914:00 08/24/0916:36 120-12-7 Benzo(a)anthracene NO uglkg 13.6 1 08/18/09 14:00 08/2410916:36 56-55-3 Benzo(a)pyrene ND ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 50-32-8 Benzo(b)8uoranthene NO uglkg 13.6 1 08/18/09 14:00 08/24/09 16:36 205-99-2 Benzo(g,h,i)perylene ND ug/kg 13.6 1 0811810914:00 08/2410916:36 191-24-2 Benzo(k)fluoranthene NO uglkg 13.6 1 08118/0914:00 08/24/09 16:36 207-08-9 Chrysene NO ug/kg 13.6 1 0811810914:00 08/2410916:36 218-01-9 Dibenz(a,h)anthracene ND ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 53-70-3 Fluoranthene ND ug/kg 13.6 1 0811810914:00 08/2410916:36 206-44-0 Fluorene ND ug/kg 136 1 0811810914:00 0812410916:36 86-73-7 Indeno(1,2,3-cd)pyrene ND ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 193-39-5 1-Methylnaphthalene ND ug/kg 13.6 1 08/1810914:00 0812410916:36 90-12-0 2-Methylnaphthalene ND ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 91-57-6 Naphthalene ND ug/kg 13.6 1 08118/0914:00 08/24/09 16:36 91-20-3 Phenanthrene ND ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 85-01-8 Pyrene NO ug/kg 13.6 1 08/18/09 14:00 08/24/09 16:36 129-00-0 Nitrobenzene-d5 (S) 44 % 30-120 1 08/18/09 14:00 08/24/09 16:36 4165-60-0 2-Fluorobiphenyl (S) 50 % 30-120 1 08/18/09 14:00 08/24/09 16:36 321-60-8 Terphenyl-dl4 (S) 75 % 30-116 1 08/18/09 14:00 08/24/09 16:36 1718-51-0 826015035A Volatile Organics Analytical Method: EPA 8260 Acetone 390 ug/kg 119 1 08/1810901:34 67-64-1 Benzene ND ug/kg 6.0 1 08/1810901:34 71-43-2 Bromobenzene NO ug/kg 6.0 1 08/18/09 01:34 108-86-1 Bromochloromethane ND uglkg 6.0 1 08/18/09 01:34 74-97-5 Bromodichloromethane NO ug/kg 6.0 1 08/18/09 01:34 75-27-4 Bromoform NO uglkg 6.0 1 08/181090134 75-25-2 Bromomethane ND ug/kg 11.9 1 08/18/0901:34 74-83-9 2-Butanone(MEK) ND ug/kg 119 1 0811810901:34 78-93-3 n-Butylbenzene NO uglkg 6.0 1 08/18/09 01:34 104-51-8 sec-Butylbenzene ND ug/kg 6.0 1 08118/090134 135-98-8 ten-Butylbenzene ND ug/kg 6.0 1 08/18/0901:34 98-06-6 Carbon tetrachloride ND ug/kg 6.0 1 08/1810901*34 56-23-5 Chlorobenzene ND ug/kg 6.0 1 0811810901:34 108-90-7 Chloroethane ND uglkg 11.9 1 08118/090134 75-00-3 Chloroform ND uglkg 6.0 1 08118/0901:34 67-66-3 Chloromethane NO uglkg 11.9 1 08118/0901:34 74-87-3 2-Chlorololuene ND ug/kg 6.0 1 08/18/0901:34 95-49-8 4-Chlorololuene ND ug/kg 6.O 1 08/18/09 01:34 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 6.0 1 08/18/09 01:34 96-12-8 Dibromochloromethane ND ug/kg 6.0 1 0811810901:34 124-48-1 1,2-Dibromoethane(EDB) NO ug/kg 6.O 1 08118/0901:34 106-93-4 Dibromomethane ND ug/kg 6.0 1 0811810901:34 74-95-3 1,2-Dichlorobenzene NO ug/kg 6.0 1 08/18/09 01:34 95-50-1 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. held Page 6 of 32 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. ace Analytical2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wiewpacelabscom Asheville, NC 28804 Huntersville. NC 28078 (828)254-7176 (704)875-9092 i ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: SB-1 (0-1) Lab ID: 9250959002 Collected: 08/13/09 14:00 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 826015035A Volatile Organics Analytical Method: EPA 8260 1,3-Dichlorobenzene ND ug/kg 6.0 1 08/18/09 01:34 541-73-1 1,4-Dichlorobenzene ND ug/kg 6.0 1 08/18/09 01:34 106-46-7 Dichlorodi0uoromethane ND ug/kg 11.9 1 08/18/0901:34 75-71-8 1,1-Dichloroethane ND ug/kg 6.0 1 08/18/09 01:34 75-34-3 1,2-Dichloroethane ND ug/kg 6.0 1 08/18/09 01:34 107-06-2 1,1-Dichloroethene NO ug/kg 6.0 1 08/18/09 01:34 75-35-4 cis-1,2-Dichloroethene NO ug/kg 6.0 1 08/18/09 01:34 156-59-2 trans-1,2-Dichloroethene ND ug/kg 6.0 1 08/1810901:34 156-60-5 1,2-Dichloropropane NO ug/kg 6.0 1 08/18/09 01:34 78-87-5 1,3-Dichloropropane ND ug/kg 6.0 1 08/18/09 01:34 142-28-9 2,2-Dichloropropane ND ug/kg &0 1 08/18/09 01:34 594-20-7 1,1-Dichloropropene NO ug/kg 6.0 1 08/18/09 01:34 563-58-6 cis-1,3-Dichloropropene NO ug/kg 6.0 1 08/18/09 01:34 10061-01-5 trans-1,3-Dichloropropene NO ug/kg 6.0 1 08/18/09 01:34 10061-02-6 Diisopropyl ether NO ug/kg 6.0 1 08/18/09 01:34 108-20-3 Ethylbenzene NO ug/kg 6.0 1 08/18/09 01:34 100-41-4 Hexachloro-1,3-butadiene NO ug/kg 6.0 1 08/18/09 01:34 87-68-3 2-Hexanone NO ug/kg 59.6 1 08/18/09 01:34 591-78-6 Isopropylbenzene (Cumene) NO ug/kg 6.0 1 08/18/09 01:34 98-82-8 p-Isopropyltoluene ND ug/kg &0 1 08/18/09 01:34 99-87-6 Methylene Chloride NO ug/kg 23.8 1 08/18/09 01:34 75-09-2 4-Methyl-2-pentanone (MIBK) NO ug/kg 59.6 1 08/18/09 01:34 108-10-1 Methyl -ten -butyl ether NO ug/k9 6.0 1 08/18/09 01:34 1634-04-4 Naphthalene NO ug/kg 6.0 1 08/18/09 01:34 91-20-3 n-Propylbenzene NO ug/kg 6.0 1 08/18/09 01:34 103-65-1 Styrene ND ug/kg &0 1 08/18/09 01:34 100-42-5 1,1,1,2-Tetrachloroethane NO ug/kg 6.0 1 0811810901:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 6.0 1 08/18/09 01:34 79-34-5 Tetrachloroethene ND ug/kg 6.0 1 08/18/09 01:34 127-18-4 Toluene NO ug/kg 6.0 1 08/18/09 01:34 108-88-3 1,2,3-Trichlorobenzene NO ug/kg 6.0 1 08/18/09 01:34 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 6.0 1 08/18/09 01:34 120-82-1 1, 1, 1-Trichloroethane ND ug/kg 6.0 1 08/18/0901:34 71-55-6 1, 1,2-Trichloroethane ND ug/kg 6.0 1 08/18/09 01:34 79-00-5 Trichloroethene ND ug/kg 6.0 1 08/18/09 01:34 79-01-6 Trichloronuoromethane ND ug/kg 6.0 1 08/18/09 01:34 75-69.4 1,2,3-Trichloropropane ND ug/kg 6.0 1 08/18/09 01:34 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 6.O 1 08/18/09 01:34 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 6.0 1 08/18/09 01:34 108-67-8 Vinyl acetate NO ug/kg 59.6 1 08/18/09 01:34 108-05-4 Vinyl chloride ND ug/kg 11.9 1 08/18/09 01:34 75-01-4 Xylene (Total) ND ug/kg 11.9 1 08/18/09 01:34 1330-20-7 m&p-Xylene NO ug/kg 11.9 1 08/18/09 01:34 1330-20-7 o-Xylene ND ug/kg 6.0 1 08118/09 01:34 95-47-6 Dibromo0uoromethane (S) 102 % 79-116 1 08/18/09 01:34 1868-53-7 Toluene-d8 (S) 97 % 88-110 1 08/18/09 01:34 2037-26-5 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 7 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc �`nelac" ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceftlytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wpaceMOscwn Asheville. NC 28804 Huntersville, NC 28078 ANALYTICAL RESULTS (828)254-7176 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: SB-1 (0-1) Lab ID: 9250959002 Collected: 08/13/0914:00 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 826015035A Volatile Organics Analytical Method: EPA 8260 4-BromoOuorobenzene (S) 97 % 74-115 1 08/18/09 01:34 460-00-4 1,2-Dichloroethane-d4(S) 108 % 69-121 1 08/18/0901:34 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 26.7 % 0.10 1 08/18/09 08:15 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, Inc.. °nelac Page 8 of 32 0 Pace Analytical Services, Inc. Pace Analytical Services, Inc. _49=Analjitical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 ~,psceleba.rorn Asheville. NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 I ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: MW-2 (20-22) Lab ID: 9250959003 Collected: 08/12/0918:00 Received: 08/14/0913:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony NO mg/kg 0.61 1 08/18/09 12:45 08119/0916:29 7440-36-0 Arsenic 2.3 mg/kg 0.61 1 08/18/09 12:45 08/19/09 16:29 7440-38-2 Beryllium 0.27 mg/kg 0.12 1 0811810912:45 0812010918:39 7440-41-7 Cadmium ND mg/kg 0.12 1 08/18/09 12:45 08119/0916:29 7440-43-9 Chromium NO mg/kg 0.61 1 08/18/09 12:45 08/19/09 16:29 7440-47-3 Copper 0.87 mg/kg 0.61 1 08118/0912:45 0811910916:29 7440-50-8 Iron 4680 mg/kg 6.1 1 08118/0912:45 08/19/09 16:29 7439-89-6 Lead 18.7 mg/kg 0.61 1 08118/0912:45 0811910916*29 7439-92-1 Nickel NO mg/kg 0.61 1 08/18/09 12:45 08/19/09 16:29 7440-02-0 Selenium NO mg/kg 1.2 1 08/18/09 12:45 08119/0916:29 7782-49-2 Silver ND mg/kg 0.61 1 08/18/09 12:45 0811910916:29 7440-22-4 Thallium NO mg/kg 1.2 1 08/18/09 12:45 08119/0916:29 7440-28-0 Zinc 21.8 mg/kg 1.2 1 08/18/09 12:45 0811910916:29 7440-66-6 P8 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.015 mg/kg 0.0055 1 08120/0909:23 08/20/0913:45 7439-97-6 8270 MSSV PEE PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3545 Aeenaphthene NO ug/kg 12.4 1 08/1810914:00 08/24/09 17:06 83-32-9 Acenaphlhylene NO ug/kg 12A 1 08/18/09 14:00 08/24/0917:06 208-96-8 Anthracene ND ug/kg 12A 1 08/1810914:00 08/24/0917:06 120-12-7 Benzo(a)anthracene NO ug/kg 12A 1 08/1810914:00 08/24/0917:06 56-55-3 Benzo(a)pyrene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:06 50-32-8 Benzo(b)fluoranthene NO ug/kg 12.4 1 08/1810914:00 08/24/09 17:06 205-99-2 Benzo(g,h,i)perylene NO ug/kg 12.4 1 08/1810914:00 08/24/09 17:06 191-24-2 Benzo(k)Buoranthene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:06 207-08-9 Chrysene ND ug/kg 12.4 1 08/1810914:00 08/24/0917:06 218-01-9 Dibenz(a,h)anthracene ND ug/kg 12.4 1 08118/0914:00 08/24/0917:06 53-70-3 Fluoranthene NO ug/kg 12.4 1 0811810914:00 08/24/0917:06 206-44-0 Fluorene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:06 86-73-7 Indeno(1,2,3-cd)pyrene ND ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:06 193-39-5 1-Methylnaphtha[ene ND ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:06 90-12-0 2-Methylnaphthalene ND ug/kg 12.4 1 08/1810914:00 08/24/0917:06 91-57-6 Naphthalene ND ug/kg 12.4 1 08118/0914:00 08/24/09 17:06 91-20-3 Phenanthrene ND ug/kg 12.4 1 08/18/09 14:00 08/2410917:06 85-01-8 Pyrene ND ug/kg 12.4 1 0811810914:00 08/2410917:06 129-00-0 Nitrobenzene-d5 (S) 37 % 30-120 1 08/18/09 14:00 08/24/09 17:06 4165-60-0 2-Fluorobiphenyl (S) 40 % 30-120 1 08/18/09 14:00 08/24/09 17:06 321-60-8 Terphenyl-d14 (S) 58 % 30-116 1 08/18/09 14:00 08/24/09 17:06 1718-51.0 826015035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 94.1 1 08/18/09 00:58 67-64-1 Benzene ND ug/kg 4.7 1 08/18/09 00:58 71-43-2 Bromobenzene NO ug/kg 4.7 1 08/18/09 00:58 108-86-1 Bromochloromelhane ND ug/kg 4.7 1 08/18/09 00:58 74-97-5 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 9 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. :`nelacI. 2ceAnalytical' e ..Mwb0.s.com i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-2 (20-22) Lab ID: 9250959003 Collected: 08/12/09 18:00 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 8260/5035A Volatile Organics Analytical Method: EPA 8260 Bromodichloromethane ND ug/kg 4.7 1 0811810900:58 75-27-4 Bromolorm NO ug/kg 4.7 1 08/18/09 00:58 75-25-2 Bromomethane NO ug/kg 9.4 1 08/18/09 00:58 74-83-9 2-Butanone (MEK) ND ug/kg 94.1 1 08/18/09 00:58 78-93-3 n-Butylbenzene ND ug/kg 4.7 1 08/18/09 00:58 104-51-8 sec-Butylbenzene NO ug/kg 4.7 1 08/18/09 00:58 135-98-8 tert-Butylbenzene NO ug/kg 4.7 1 08/18/09 00:58 98-06-6 Carbon tetrachloride NO ug/kg 4.7 1 08/18/09 00:58 56-23-5 Chlorobenzene ND ug/kg 4.7 1 08/18/09 00:58 108-90-7 Chloroethane NO ug/kg 9.4 1 08/18/09 00:58 75-00-3 Chloroform ND ug/kg 4.7 1 08/18/09 00:58 67-66-3 Chloromethane ND ug/kg 9.4 1 0811810900:58 74-87-3 2-Chlorotoluene ND ug/kg 4.7 1 08118/0900:58 95-49-8 4-Chlorotoluene ND ug/kg 4.7 1 08/18/09 00:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 4.7 1 08/18/09 00:58 96-12-8 Dibromochloromethane ND ug/kg 4.7 1 08/18/09 00:58 124-48-1 1,2-Dibromoethane(ED8) NO ug/kg 4.7 1 08/18/09 00:58 106-93-4 Dibromomethane NO ug/kg 4.7 1 08/18/09 00:58 74-95-3 1,2-Dichlorobenzene NO uglkg 4.7 1 08/18/09 00:58 95-50-1 1,3-Dichlorobenzene NO uglkg 4.7 1 08/18/09 00:58 541-73-1 1,4-Dichlorobenzene NO ug/kg 4.7 1 08/18/09 00:58 106-46-7 Dichlorodi0uoromethane ND ug/kg 9.4 1 08/18/0900:58 75-71-8 1,1-Dichloroelhane ND ug/kg 4.7 1 08/18/09 00.58 75-34-3 1,2-Dichloroelhane NO ug/kg 4.7 1 08/18/09 00:58 107-06-2 1,1-Dichloroethene NO ug/kg 4.7 1 08/18/09 00.58 75-35-4 cis-1,2-Dichloroethene NO ug/kg 4.7 1 08/18/09 00:58 156-59-2 trans-1,2-Dichloroethene NO ug/kg 4.7 1 08/18/09 00:58 156-60-5 1,2-Dichloropropane NO ug/kg 4.7 1 08/18/09 00:58 78-87-5 1,3-Dichloropropane NO ug/kg 4.7 1 08/18/09 00:58 142-28-9 2,2-Dichloropropane ND ug/kg 4.7 1 08/18/09 00:58 594-20-7 1,1-Dichloropropene ND ug/kg 4.7 1 08/1810900:58 563-58-6 cis-1,3-Dichloropropene ND ug/kg 4.7 1 08/18/09 00:58 10061-01-5 trans-1,3-Dichloropropene ND ug/kg 47 1 08/18/09 00:58 10061-02-6 Diisopropyl ether ND ug/kg 4 7 1 08/18/09 00:58 108-20-3 Ethylbenzene ND ug/kg 4.7 1 08118/0900:58 100-41-4 Hexachloro-1,3-butadiene ND uglkg 4.7 1 08/1810900: 58 87-68-3 2-Hexanone ND ug/kg 47.0 1 0811810900:58 591-78-6 Isopropylbenzene(Cumene) NO ug/kg 4.7 1 0811810900:58 98-82-8 p-Isopropyltoluene NO ug/kg 4.7 1 0811810900:58 99-87-6 Methylene Chloride NO ug/kg 18.8 1 08/18/09 00:58 75-09-2 4-Methyl-2-penlanone (MIBK) NO ug/kg 47.0 1 08/18/0900: 58 108-10-1 Methyl-tert-butyl ether NO ug/kg 4.7 1 08/18/09 00:58 1634-04-4 Naphthalene NO ug/kg 4.7 1 08/18/0900: 58 91-20-3 n-Propylbenzene ND ug/kg 4.7 1 08/18/09 00:58 103-65-1 Styrene ND ug/kg 4.7 1 08/18/09 00.58 100-42-5 1, 1,1,2-Tetrachloroethane NO uglkg 4.7 1 08/18/0900:58 630-20-6 Qua] Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 10 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. "nelacr. 11�aceAnaljltical w»w.pace/alns.com i Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntenwille, NC 28078 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: MW-2 (20-22) Lab ID: 9250959003 Collected: 08/12/09 18:00 Received: 08/14/0913:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,1,2,2-Tetrachloroelhane ND ug/kg Tetrachloroethene NO ug/kg Toluene ND ug/kg 1,2,3-Trichlorobenzene NO ug/kg 1,2,4-Trichlorobenzene NO ug/kg 1,1,1-Trichloroelhane NO ug/kg 1,1,2-Trichloroethane NO ug/kg Trichloroethene NO ug/kg Trichloro0uoromethane NO ug/kg 1,2,3-Tfichloropropane NO ug/kg 1,2,4-Tfimethylbenzene NO ug/kg 1,3,5-Trimethylbenzene NO ug/kg Vinyl acetate ND ug/kg Vinyl chloride ND ug/kg Xylene (Total) ND ug/kg m&p-Xylene NO ug/kg o-Xylene ND ug/kg Dibromolluoromethane (S) 104 Toluene-d8(S) 97 4-8romo8uorobenzene (S) 96 1,2-Dichloroethane-d4 (S) 113 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 19.1 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg Nitrogen, Nitrite 94.4 mg/kg Nitrogen, NO2 plus NO3 ND mg/kg 4500 Chloride in Soil Analytical Method: SM 4500-CI-E Chloride 85.5 mg/kg ASTM D516-90 Sulfate Soil Analytical Method: ASTM D516-90 Sulfate 88.2 mg/kg Date: 08/26/2009 09:36 AM 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 4.7 1 47.0 1 9.4 1 9.4 1 9A 1 4.7 1 79-116 1 88-110 1 74-115 1 69-121 1 0.10 1 10 1 10 1 10 1 61.8 1 61.8 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac` 08/18/09 00:58 79-34-5 08/18/09 00:58 127-18-4 08/18/09 00:58 108-88-3 08/18/09 00:58 87-61-6 08/18/09 00:58 120-82-1 08/1810900:58 71-55-6 08/18/09 00:58 79-00-5 08/18/09 00:58 79-01-6 08/18/09 00:58 75-69-4 08/18/09 00:58 96-18-4 08/18/09 00:58 95-63-6 08/18/09 00:58 108-67-8 08/18/09 00:58 108-05-4 08/18/09 00:58 75-01-4 08/18/09 00:58 1330-20-7 08/18/09 00:58 1330-20-7 08/18/09 00:58 95-47-6 08/18/09 00:58 1868-53-7 08/18/09 00:58 2037-26-5 08/18/09 00:58 460-00-4 08/18/09 00:58 17060-07-0 08/18/09 08:15 08/18/09 18:00 08/18/09 18:00 08/18/09 18:00 08/21/09 09:03 16887-00-6 08/21/09 11:32 14808-79-8 Page 11 of 32 aceAnalytical j x»w.pecelab5.can i Project: OMNI SUPPLY 13140-007-000l Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside D, Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: S13-2 (0-1) COMP Lab ID: 9250959004 Collected: 08/14/09 10:30 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony ND mg/kg 2A 5 08118/0912:45 08/20/09 17:10 7440-36-0 Arsenic ND mg/kg 2.4 5 08/1810912:45 08/2010917:10 7440-38-2 Beryllium 2.1 mg/kg 0.49 5 08/18/09 12:45 08/20/0917:10 7440-41-7 Cadmium ND mg/kg 0.49 5 08/18/09 12:45 08/20/09 17:10 7440-43-9 Chromium 18.7 mg/kg 2.4 5 08/1810912:45 08/2010917:10 7440-47-3 Copper 16.2 mg/kg 2.4 5 08/18/09 12:45 08/20/09 17:10 7440-50-8 Lead 13.7 mg/kg 2.4 5 08/18/09 12:45 0812010917:10 7439-92-1 Nickel 13.3 mg/kg 2.4 5 08/18/09 12:45 08/20/09 17:10 7440-02-0 Selenium ND mg/kg 4.9 5 08/18/09 12:45 08120/0917:10 7782-49-2 Silver ND mg/kg 2A 5 08/18/09 12:45 08/20/09 17:10 7440-22-4 Thallium ND mg/kg 4.9 5 08118/0912:45 08/20/09 17:10 7440-28-0 Zinc 197 mg/kg 4.9 5 08118/0912:45 08/20/09 17:10 7440-66-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.0082 mg/kg 0.0048 1 08/20/09 09:23 08/20/09 13:48 7439-97-6 Percent Moisture Analytical Method. ASTM D2974-87 Percent Moisture 16.0 % 0A0 1 08/1910914:12 Date: 08/26/200909:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Without the written consent of Pace Analytical Services, Inc.. 11nelac` P8 Page 12 of 32 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 117p~.pacelebs cum Asheville, NC 28804 Huntersvilie, NC 28078 (828)254-7176 (704)875-9092 i ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: SB-2 (0-1) GRAB Lab ID: 9250959005 Collected: 08/14/09 10:30 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 8270 MSSV PFE PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3545 Acenaphthene NO ug/kg 12A 1 08/18/09 14:00 08/2410917:36 83-32-9 Acenaphthylene NO ug/kg 12.4 1 08/18/09 14:00 08/2410917:36 208-96-8 Anthracene NO ug/kg 12.4 1 08/18/09 14:00 08/24/0917:36 120-12-7 Benzo(a)anthracene NO ug/kg 12.4 1 08/1810914:00 08/24/0917:36 56-55-3 Benzo(a)pyrene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:36 50-32-8 Benzo(b)0uoranthene NO ug/kg 12.4 1 08/1810914:00 08/24/0917:36 205-99-2 Benzo(g,h,i)perylene NO ug/kg 12.4 1 08/1810914:00 08/24/0917:36 191-24-2 Benzo(k)0uoranthene ND ug/kg 12.4 1 08/18/09 14:00 08/24/0917:36 207-08-9 Chrysene NO ug/kg 12.4 1 0811810914:00 08124/0917:36 218-01-9 Dibenz(a,h)anthracene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:36 53-70-3 Fluoranthene NO ug/kg 12.4 1 08118/0914:00 08/24/0917:36 206-44-0 Fluorene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:36 86-73-7 Indeno(1,2,3-cd)pyrene NO ug/kg 12.4 1 08/18/09 14:00 08/24/09 17:36 193-39-5 1-Methylnaphthalene NO ug/kg 12.4 1 08/1810914:00 08/24/0917:36 90-12-0 2-Methylnaphthalene NO ug/kg 12.4 1 0811810914:00 08/24/0917:36 91-57-6 Naphthalene NO ug/kg 12.4 1 0811810914:00 08124/0917:36 91-20-3 Phenanthrene NO ug/kg 12.4 1 0811810914:00 08/24/0917*36 85-01-8 Pyrene NO ug/kg 12.4 1 0811810914:00 08/24/0917:36 129-00-0 Nitrobenzene-d5 (S) 43 % 30-120 1 08/18/09 14:00 08/24/09 17:36 4165-60-0 2-Fluorobiphenyl (S) 45 % 30-120 1 08/18/09 14:00 08/24/09 17:36 321-60-8 Terphenyl-d14(S) 76% 30-116 1 0811810914:00 08124/0917:36 1718-51-0 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone NO ug/kq 96.6 1 08/18/09 01:16 67-64-1 Benzene NO uq/kq 4.8 1 08/18/09 01:16 71-43-2 Bromobenzene NO uglkg 4.8 1 08/18/09 01:16 108-86-1 Bromochloromethane NO ug/kg 4.8 1 08/18/09 01:16 74-97-5 Bromodichloromethane NO ug/kg 4.8 1 08/18/09 01:16 75-27-4 Bromoform NO ug/kg 4.8 1 08/18/09 01:16 75-25-2 Bromomethane NO ug/kg 9.7 1 08/18/09 01:16 74-83-9 2-Butanone (MEK) NO ug/kq 96.6 1 08/18/09 01:16 78-93-3 n-Butylbenzene ND ug/kg 4.8 1 08/18/09 01:16 104-51-8 sec-Butylbenzene NO ug/kg 4.8 1 08/18/09 01:16 135-98-8 lert-Butylbenzene NO ug/kg 4.8 1 08/18/09 01:16 98-06-6 Carbon tetrachloride ND ug/kg 4.8 1 08/18/09 01:16 56-23-5 Chlorobenzene NO ug/kg 4.8 1 08/18/09 01:16 108-90-7 Chloroethane NO ug/kg 9.7 1 08/18/09 01:16 75-00-3 Chloroform NO ug/kq 4.8 1 08/18/09 01:16 67-66-3 Chloromethane NO ug/kg 9.7 1 08/18/09 01:16 74-87-3 2-Chlorololuene NO ug/kg 4.8 1 08/18/09 01:16 95-49-8 4-Chlorotoluene NO ug/kg 4.8 1 08/18/09 01:16 106-43-4 1,2-Dibromo-3-chloropropane NO ug/kg 4.8 1 08/18/09 01:16 96-12-8 Dibromochloromethane NO ug/kg 4.8 1 08/18/09 01:16 124-48-1 1,2-Dibromoethane(EDB) NO ug/kg 4.8 1 08118/0901: 16 106-93-4 Dibromomethane NO ug/kg 4.8 1 08/18/09 01:16 74-95-3 1,2-Dichlorobenzene NO ug/kg 4.8 1 08/18/09 01:16 95-50-1 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 13 of 32 This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, Inc fnelac ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aeeAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 / - wwnaac"Ioom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 i ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: SB-2 (0.1) GRAB Lab ID: 9250959005 Collected: 08/14/09 10:30 Received 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 826015035A Volatile Organics Analytical Method: EPA 8260 1,3-Dichlorobenzene ND ug/kg 4.8 1 08/18/09 01:16 541-73-1 1,4-Dichlorobenzene ND ug/kg 4.8 1 08/18/09 01:16 106-46-7 Dichlorodi8uoromethane ND ug/kg 9.7 1 0811810901:16 75-71-8 1,1-Dichloroethane ND ug/kg 4.8 1 0811810901:16 75-34-3 1,2-Dichloroethane ND ug/kg 4.8 1 08/18/09 01:16 107-06-2 1,1-Dichloroethene ND ug/kg 4.8 1 08/1810901:16 75-35-4 cis-1,2-Dichloroethene ND ug/kg 4.8 1 08/18/0901: 16 156-59-2 trans-1,2-Dichloroethene ND ug/kg 4.8 1 08/18/09 01:16 156-60-5 1,2-Dichloropropane ND ug/kg 4.8 1 08/18/09 01:16 78-87-5 1,3-Dichloropropane ND ug/kg 4.8 1 08/18/0901:16 142-28-9 2,2-Dichloropropane ND ug/kg 4.8 1 08/18/09 01:16 594-20-7 1,1-Dichloropropene ND ug/kg 4.8 1 08/18/09 01:16 563-58-6 cis-1,3-Dichloropropene ND ug/kg 4.8 1 08/18/09 01:16 10061-01-5 trans-1,3-Dichloropropene ND ug/kg 4.8 1 08/18/09 01:16 10061-02-6 Diisopropyl ether ND ug/kg 4.8 1 08/18/09 01:16 108-20-3 Ethylbenzene ND ug/kg 4.8 1 08/1810901*16 100-41-4 Hexachloro-1,3-butadiene NO ug/kg 4.8 1 08/1810901:16 87-68-3 2-Hexanone NO ug/kg 48.3 1 08/18/0901: 16 591-78-6 Isopropylbenzene(Cumene) ND ug/kg 4.8 1 08/1810901:16 98-82-8 p-Isopropyltoluene NO ug/kg 4.8 1 08/18/09 01:16 99-87-6 Methylene Chloride ND ug/kg 19.3 1 08/18/09 01:16 75-09-2 4-Methyl-2-pentanone(MIBK) ND ug/kg 48.3 1 08/18/0901:16 108-10-1 Methyl -ten -butyl ether ND ug/kg 4.8 1 08/18/09 01:16 1634-04-4 Naphthalene ND ug/kg 4.8 1 08/18/09 01:16 91-20-3 n-Propylbenzene ND ug/kg 4.8 1 0811810901:16 103-65-1 Styrene ND ug/kg 4.8 1 08/18/09 01:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 4.8 1 08/1810901:16 630-20-6 1,1,2,2-Tetrachloroethane NO ug/kg 4.8 1 08/1810901:16 79-34-5 Tetrachloroethene ND ug/kg 4.8 1 08/18/09 01:16 127-18-4 Toluene ND ug/kg 4.8 1 08/18/09 01:16 108-88-3 1,2,3-Trichlorobenzene NO ug/kg 4.8 1 08/18/0901:16 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 4.8 1 08/18/09 01:16 120-82-1 1, 1, 1-Trichloroethane ND ug/kg 4.8 1 0811810901: 16 71-55-6 1,1,2-Trichloroethane ND ug/kg 4.8 1 08/18/09 01:16 79-00-5 Trichloroethene ND ug/kg 4.8 1 08118/0901:16 79-01-6 Trichlorofluoromethane ND ug/kg 4.8 1 08/18/0901:16 75-69-4 1,2,3-Trichloropropane ND ug/kg 4.8 1 08/18/09 01:16 96-18-4 1,2,4-Trimethylbenzene ND ugikg 4.8 1 08/18/09 01:16 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 4.8 1 08/18/09 01:16 108-67-8 Vinyl acetate ND ug/kg 48.3 1 08/18/09 01:16 108-05-4 Vinyl chloride NO ug/kg 9.7 1 08/18/09 01.16 75-01-4 Xylene (Total) NO ug/kg 9.7 1 08/18/09 01:16 1330-20-7 m&p-Xylene NO ug/kg 9.7 1 08/18/09 01.16 1330-20-7 o-Xylene ND ug/kg 4.8 1 08/18/09 01:16 95-47-6 Dibromolluoromethane (S) 103 % 79-116 1 08/18/09 01:16 1868-53-7 Toluene-d8 (S) 97 % 88-110 1 08/18/09 01:16 2037-26-5 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 14 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nela& ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. _ aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 j wvw.perolabscom Asheville, NC 28804 Runtersville, NC 28078 (828)254-7176 (704)875-9092 i ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Sample: SB-2 (0-1) GRAB Lab ID: 9250959005 Collected: 08/14/09 10:30 Received: 08/14/09 13:44 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 826015035A Volatile Organics Analytical Method: EPA 8260 4-Bromo0uorobenzene (S) 95 % 74-115 1 08/18/09 01:16 460-00-4 1,2-Dichloroethane-d4 (S) 109 % 69-121 1 08/18/09 01:16 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 19.1 % 0A0 1 08/18/09 08:15 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac`r; Page 15 of 32 ZXAnalyfical' / e»w.pacelaes.com i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA OC Batch: OEXT/7733 Analysis Method: EPA8270 by SIM QC Batch Method: EPA 3545 Analysis Description: 8270 MSSV PAH by SIM Associated Lab Samples: 9250959002, 9250959003, 9250959005 METHOD BLANK: 323485 Associated Lab Samples: Parameter Matrix: 9250959002, 9250959003, 9250959005 Blank Units Result Solid Reporting Limit Analyzed 1-Methylnaphthalene ug/kg NO 10.0 08/24/09 13:11 2-Methylnaphthalene ug/kg ND 10.0 08/24/09 13:11 Acenaphthene ug/kg ND 10.0 0812410913:11 Acenaphthylene ug/kg ND 10.0 08124/0913:11 Anthracene ug/kg NO 10.0 08/24/09 13:11 Benzo(a)anthracene ug/kg NO 10.0 08124/0913:11 Benzo(a)pyrene ug/kg NO 10.0 08/24/09 13: 11 Benzo(b)fluoranthene ug/kg NO 10.0 08/24/0913: 11 Benzo(g,h,i)perylene ug/kg NO 10.0 08/24/09 13:11 Benzo(k)Fluoranthene ug/kg ND 10.0 08/2410913: 11 Chrysene ug/kg NO 10.0 0812410913: 11 Dibenz(a,h)anthracene ug/kg ND 10.0 08/24/0913: 11 Fluoranthene ug/kg ND 10.0 08/24/09 13:11 Fluorene ug/kg ND 10.0 08/2410913:11 Indeno(1,2,3-cd)pyrene ug/kg NO 10.0 08/24/09 13:11 Naphthalene ug/kg NO 10.0 08/24/0913: 11 Phenanthrene ug/kg NO 10.0 08/24/0913: 11 Pyrene ug/kg NO 10.0 08/24/0913: 11 2-Fluorobiphenyl (S) % 39 30-120 08/24/09 13:11 Nitrobenzene-d5 (S) % 30 30-120 08/24/09 13:11 Terphenyl-d14(S) % 104 30-116 08/24/09 13:11 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 323486 Units Spike Cone. LCS Result LCS % Rec % Rec Limits 1-Methylnaphthalene ug/kg 33.3 25.5 77 29-108 2-Methylnaphthalene ug/kg 33.3 26.0 78 30-104 Acenaphthene ug/kg 33.3 20.3 61 38-109 Acenaphthylene ug/kg 33.3 23.1 69 41-109 Anthracene ug/kg 33.3 22.1 66 45-114 Benzo(a)anthracene ug/kg 33.3 22.3 67 45-109 Benzo(a)pyrene ug/kg 33.3 21.3 64 47-117 Benzo(b)Buoranlhene ug/kg 33.3 21.1 63 32-113 Benzo(g,h,i)perylene ug/kg 33.3 19.1 57 10-149 Benzo(k)fluoranthene ug/kg 33.3 20.7 62 41-104 Chrysene ug/kg 33.3 20A 60 35-116 Dibenz(a,h)anthracene ug/kg 33.3 18.6 56 13-139 Fluoranthene u9/kg 33.3 22.0 fib 43-110 Fluorene ug/kg 33.3 22.2 67 45-111 Indeno(1,2,3-cd)pyrene ug/kg 33.3 19.9 60 17-135 Naphthalene ug/kg 33.3 24A 72 26-120 Date :08126/200909:36AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 16 of 32 _® Pace Analytical Services, Inc. aceAnalytical 2225 Riverside Dr. J wmv�w�Oscxn Asheville, NC 28804 (828)254-7176 i QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 LABORATORY CONTROL SAMPLE: 323486 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Phenanthrene ug/kg 33.3 22.3 67 45-110 Pyrene ug/kg 33.3 22.0 66 38-114 2-Fluorobiphenyl(S) % 87 30-120 Nitrobenzene-d5 (S) % 65 30-120 Terphenyl-d14 (S) % 85 30-116 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac" Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 17 of 32 2ceAnalXical wmvpacelab& w i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MSV/7989 Analysis Method: EPA8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics Associated Lab Samples: 9250959002, 9250959003, 9250959005 METHOD BLANK: 323248 Matrix: Solid Associated Lab Samples: 9250959002, 9250959003. 9250959005 Blank Reporting Parameter Units Result Limit Analyzed 1, 1, 1,2-Tetrachloroelhane ug/kg NO 5.0 0811710923:45 1, 1, 1-Trichloroethane ug/kg ND 5.0 0811710923:45 1, 1,2,2-Tetrachloroethane ug/kg ND 5.0 0811710923:45 1, 1,2-Trichloroethane ug/kg NO 5.0 08117/0923:45 1,1-Dichloroethane ug/kg NO 5.0 08/1710923:45 1,1-Dichloroethene ug/kg NO 5.0 08/17/09 23:45 1,1-Dichloropropene ug/kg ND 5.0 08/17/09 23:45 1,2,3-Trichlorobenzene ug/kg NO 5.0 08/17/09 23:45 1,2,3-Trichloropropane ug/kg NO 5.0 08/17/0923:45 1,2,4-Trichlorobenzene ug/kg ND 5.0 08/17/09 23:45 1,2,4-Trimethylbenzene ug/kg ND 5.0 0811710923:45 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/1710923:45 1,2-Dibromoethane(EDB) ug/kg NO 5.0 0811710923:45 1,2-Dichlorobenzene ug/kg NO 5.0 08117/0923:45 1,2-Dichloroethane ug/kg NO 5.0 08/1710923:45 1,2-Dichloropropane ug/kg ND 5.0 08/17/09 23:45 1,3,5-Trimethylbenzene ug/kg ND 5.O O8/17/09 23:45 1,3-Dichlorobenzene ug/kg ND 5.0 08/1710923:45 1,3-Dichloropropane ug/kg NO 5.0 08/17/09 23:45 1,4-Dichlorobenzene ug/kg ND 5.0 08/17/0923:45 2,2-Dichloropropane ug/kg ND 5.0 0811710923,45 2-Butanone(MEK) ug/kg ND 100 0811710923:45 2-Chlorotoluene ug/kg NO 5.0 08/17/09 23:45 2-Hexanone ug/kg NO 50.0 08/17/09 23:45 4-Chlorotoluene ug/kg ND 5.0 08/17/09 23:45 4-Methyl-2-pentanone(MIBK) ug/kg ND 50.0 08/1710923:45 Acetone ug/kg ND 100 0811710923,45 Benzene ug/kg NO 5.0 08/17/09 23:45 Bromobenzene ug/kg NO 5.0 08/17/09 23:45 Bromochloromethane ug/kg ND 5.0 08/17/09 23:45 Bromodichloromethane ug/kg ND 5.0 08/1710923:45 Bromoform ug/kg ND 5.O 08/17/09 23:45 Bromomethane ug/kg NO 10.0 08/17/09 23:45 Carbon tetrachloride ug/kg NO 5.0 08/17/09 23:45 Chlorobenzene ug/kg NO 5.0 08/17/09 23:45 Chloroethane ug/kg ND 10.0 08/17/0923:45 Chloroform ug/kg ND 5.0 08/17/0923,45 Chloromelhane ug/kg NO 10.0 08/17/09 23:45 cis-1,2-Dichloroethene ug/kg NO 5.0 08/17/09 23:45 cis-1,3-Dichloropropene ug/kg NO 5.0 08/17/09 23:45 Dibromochloromethane ug/kg ND 5.0 08/17/09 23:45 Dibromomelhane ug/kg ND 5.0 08/17/09 23:45 Dichlorodinuoromethane ug/kg ND 10.0 08/17/09 23:45 Dale: 08/26/20090936 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac" Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 32 2ceAnalXlllcal' wxwpsce/abscan i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside D, Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA METHOD BLANK: 323248 Associated Lab Samples: Parameter Matrix: 9250959002, 9250959003, 9250959005 Blank Units Result Solid Reporting Limit Analyzed Diisopropyl ether ug/kg NO 5.0 08/17/09 23:45 Ethylbenzene ug/kg NO 5.0 08/17/0923:45 Hexachloro-1,3-buladiene ug/kg NO 5.0 08/17/09 23:45 Isopropylbenzene (Cumene) ug/kg NO 5.0 08/17/09 23:45 m&p-Xylene ug/kg ND 10.0 08/17/09 23:45 Methyl-terl-butyl ether ug/kg NO 5.0 08/17/09 23:45 Methylene Chloride ug/kg NO 20.0 08/17/09 23:45 n-Butylbenzene ug/kg NO 5.0 08/17/09 23:45 n-Propylbenzene ug/kg NO 5.0 08/17/09 23:45 Naphthalene ug/kg NO 5.0 08117/0923:45 o-Xylene ug/kg NO 5.0 08/17/09 23:45 p-Isopropylloluene ug/kg NO 5.0 08/17/09 23:45 sec-Butylbenzene ug/kg NO 5.0 08/17/09 23:45 Styrene ug/kg NO 5.0 08/17/09 23:45 ten-Butylbenzene ug/kg ND 5.0 08/17/09 23:45 Tetrachloroethene ug/kg ND 5.0 08/17/09 23:45 Toluene ug/kg ND 5.0 08/17/09 23:45 trans-1,2-Dichloroelhene ug/kg ND 5.0 08117/0923:45 trans-1,3-Dichloropropene ug/kg ND 5.0 08/17/09 23:45 Trichloroethene ug/kg ND 5.0 08117/0923:45 Tdchlomfluoromethane ug/kg ND 5.0 08117/0923:45 Vinyl acetate ug/kg ND 50.0 08/17/09 23:45 Vinyl chloride ug/kg ND 10.0 08/17/09 23:45 Xylene (Total) ug/kg ND 10.0 08/17/09 23:45 1,2-Dichloroelhane-d4(S) % 112 69-121 08117/0923:45 4-Bromoduorobenzene (S) % 96 74-115 08/17/09 23:45 Dibromofluoromethane(S) % 103 79-116 08117/0923:45 Toluene-d8(S) % 99 88-110 08/17/09 23:45 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 323249 Units Spike Conc. LCS Result -CS % Rec %Rec Limits 1,1,1,2-Tetrachloroelhane ug/kg 50 55.7 111 75-137 1, 1. 1 -Trichloroethane ug/kg 50 56.9 114 70-140 1, 1,2,2-Tetrachloroelhane ug/kg 50 55.4 111 74-133 1, 1,2-Trichloroethane ug/kg 50 54.9 110 79-129 1,1-Dichloroethane ug/kg 50 57A 115 72-139 1,1-Dichloroethene ug/kg 50 59.3 119 69-154 1,1-Dichloropropene ug/kg 50 56.3 113 74-138 1,2,3-Trichlorobenzene ug/kg 50 52.8 106 71-150 1,2,3-Trichloropropane ug/kg 50 55.0 110 74-135 1,2,4-Trichlorobenzene ug/kg 50 46.0 92 68-150 1,2,4-Trimethylbenzene ug/kg 50 54A 108 70-130 1,2-Dibromo-3-chloropropane ug/kg 50 58.1 116 65-146 1,2-Dibromoelhane(EDB) ug/kg 50 56.6 113 77-136 Date: 08/26/200909:36AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac" Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 19 o132 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 .Paoe1a6srorn Asheville, NC 28804 Huntersville, NC 28078 QUALITY CONTROL DATA (828)254-7176 (704)075-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 LABORATORY CONTROL SAMPLE: 323249 Spike LIDS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2-Dichlorobenzene ug/kg 50 51.6 103 75-141 1,2-Dichloroethane ug/kg 50 59.9 120 74-134 1,2-Dichloropropane ug/kg 50 56.3 113 77-138 1,3,5-Trimethylbenzene ug/kg 50 53.0 106 65-128 1,3-Dichlorobenzene ug/kg 50 49.8 100 76-133 1,3-Dichloropropane ug/kg 50 56.1 112 79-132 1,4-Dichlorobenzene ug/kg 50 48.2 96 75-137 2,2-Dichloropropane ug/kg 50 51.6 103 73-137 2-Butanone(MEK) ug/kg 100 113 113 61-138 2-Chlorotoluene ug/kg 50 51.8 104 73-138 2-Hexanone ug/kg 100 116 116 58-159 4-Chlorotoluene ug/kg 50 52.2 104 75-136 4-Me(hyl-2-pentanone (MIBK) ug/kg 100 115 115 74-139 Acetone ug/kg 100 127 127 58-150 Benzene ug/kg 50 52.5 105 71-140 Bromobenzene ug/kg 50 55.6 111 72-144 Bromochloromethane ug/kg 50 55.3 111 78-133 Bromodichloromethane ug/kg 50 54.9 110 78-133 Bromoform ug/kg 50 55.2 110 74-132 Bromomethane ug/kg 50 36.4 73 63-184 Carbon tetrachloride ug/kg 50 57.7 115 73-143 Chlorobenzene ug/kg 50 50.5 101 77-137 Chloroethane ug/kg 50 577 115 68-146 Chloroform ug/kg 50 57.2 114 75-137 Chloromethane ug/kg 50 56A 112 54-143 cis-1,2-Dichloroethene ug/kg 50 58.8 118 71-143 cis-1,3-Dichloropropene ug/kg 50 55.4 111 76-133 Dibromochloromethane ug/kg 50 54.2 108 77-131 Dibromomelhane ug/kg 50 55.8 112 63-184 Dichlorodifluoromethane ug/kg 50 53.2 106 36-173 Diisopropyl ether ug/kg 50 %6 113 68-144 Ethylbenzene ug/kg 50 51.8 104 69-141 Hexachloro-1,3-buladiene ug/kg 50 51.2 102 70-152 Isopropylbenzene (Cumene) ug/kg 50 53.0 106 77-143 m&p-Xylene ug/kg 100 104 104 72-138 Methyl-tert-butyl ether ug/kg 50 58.3 117 2-138 Methylene Chloride ug/kg 50 61.8 124 69-136 n-Bulylbenzene ug/kg 50 48.9 98 65-128 n-Propylbenzene ug/kg 50 53.7 107 72-139 Naphthalene ug/kg 50 59.5 119 61-138 o-Xylene ug/kg 50 53.3 107 74-137 p-Isopropyltoluene ug/kg 50 51.2 102 66-128 sec-Butylbenzene ug/kg 50 54.1 108 72-140 Styrene ug/kg 50 52.0 104 76-137 tert-Bulylbenzene ug/kg 50 55.8 112 68-141 Tetrachloroethene ug/kg 50 49.5 99 72-136 Toluene ug/kg 50 49.9 100 69-139 trans-1,2-Dichloroethene ug/kg 50 54.6 109 72-144 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 20 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac IceAnalytical' w»w.pacelabscom I Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter 323249 Units Spike Cone. LCS LCS Result % Rec trans-1,3-Dichloropropene ug/kg 50 55.7 Trichloroethene ug/kg 50 53.4 Trichloro9uoromethane ug/k9 50 55.3 Vinyl acetate ug/kg 100 38.8J Vinyl chloride ug/kg 50 59.0 Xylene (Total) ug/kg 150 157 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromelhane (S) % Toluene-d8(S) % Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 111 73-135 107 75-136 111 69-144 39 50-150 LO 118 61-145 105 73-138 111 69-121 98 74-115 106 79-116 96 88-110 MATRIX SPIKE SAMPLE: Parameter 323471 Units 9251021003 Result Spike Cone. MS Result MS % Rec % Rec Limits Qualifiers 1,1-Dichloroethene ug/kg NO 67A 86.0 127 33-158 Benzene ug/kg ND 67.9 72.1 106 46-143 Chlorobenzene ug/kg NO 67.9 71.3 105 29-159 Toluene ug/kg ND 67.9 70.2 103 38-145 Trichloroethene ug/kg ND 67.9 75.3 111 70-130 1,2-Dichloroethane-d4 (S) % 112 69-121 4-Bromofluorobenzene (S) % 90 74-115 Dibromofiuoromethane (S) % 100 79-116 Toluene-d8(S) % 98 88-110 SAMPLE DUPLICATE: 323470 Parameter Units 9250959005 Result Dup Result RPD Max RPD 1,1,1,2-Tetrachloroethane ug/kg ND ND 30 1, 1, 1-Trichloroethane ug/kg ND ND 30 1, 1,2,2-Tetrachloroethane ug/kg ND ND 30 1,1,2-Trichloroethane ug/kg ND NO 30 1,1-Dichloroethane ug/kg ND ND 30 1,1-Dichloroethene ug/kg ND ND 30 1,1-Dichloropropene ug/kg ND ND 30 1,2,3-Trichlorobenzene ug/kg ND ND 30 1,2,3-Trichloropropane ug/kg ND ND 30 1,2,4-Trichlorobenzene ug/kg ND ND 30 1,2,4-Trimethylbenzene ug/kg ND ND 30 1,2-Dibromo-3-chloropropathe ug/kg ND ND 30 1,2-Dibromoethane (EDB) ug/kg NO ND 30 1,2-Dichlorobenzene ug/kg NO ND 30 1,2-Dichloroethane ug/kg NO ND 30 1,2-Dichloropropane ug/kg NO NO 30 1,3,5-Trimethylbenzene ug/kg NO ND 30 1,3-Dichlorobenzene ug/kg NO NO 30 Dale: 08/261200909:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac r; Qualifiers Page 21 of 32 aceAnalytical / v.»w.parzkbs.carn i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA SAMPLE DUPLICATE: 323470 Parameter 9250959005 Units Result Dup Result RPD Max RPD 1,3-Dichloropropane ug/kg NO NO 30 1,4-Dichlorobenzene ug/kg NO NO 30 2,2-Dichloropropane ug/kg ND NO 30 2-Butanone (MEK) ug/kg ND NO 30 2-Chlorotoluene ug/kg NO NO 30 2-Hexanone ug/kg NO NO 30 4-Chlorotoluene uglkg NO NO 30 4-Methyl-2-pentanone (MIBK) uglkg NO NO 30 Acetone ug/kg NO 42.2J 30 Benzene uglkg NO NO 30 Bromobenzene ug/kg NO NO 30 Bromochloromethane ug/kg ND NO 30 Bromodichloromethane uglkg NO ND 30 Bromoform ug/kg NO NO 30 Bromomethane ug/kg NO ND 30 Carbon tetrachloride ug/kg NO ND 30 Chlorobenzene ug/kg NO ND 30 Chlomethane ug/kg NO NO 30 Chloroform ug/kg NO NO 30 Chloromethane ug/kg NO NO 30 cis-1,2-Dichloroethene ug/kg NO ND 30 cis-1,3-Dichloropropene ug/kg ND NO 30 Dibromochloromelhane ug/kg ND NO 30 Dibromomethane ug/kg NO NO 30 Dichlorodifluoromethane ug/kg NO NO 30 Diisopropyl ether ug/kg ND NO 30 Ethylbenzene ug/kg NO NO 30 Hexachloro-1,3-butadiene uglkg NO NO 30 Isopropylbenzene (Cumene) ug/kg NO NO 30 m&p-Xylene ug/kg NO NO 30 Methyl-tert-butyl ether uglkg NO NO 30 Methylene Chloride ug/kg NO ND 30 n-Butylbenzene ug/kg NO ND 30 n-Propylbenzene ug/kg NO NO 30 Naphthalene ug/kg NO NO 30 o-Xylene ug/kg NO ND 30 p-Isopropylloluene ug/kg NO ND 30 sec-Butylbenzene ug/kg NO NO 30 Styrene ug/kg NO NO 30 ten-Butylbenzene ug/kg NO NO 30 Tetrachloroelhene uglkg NO NO 30 Toluene ug/kg NO NO 30 trans-1,2-Dichloroethene ug/kg NO NO 30 trans-1,3-Dichloropropene u9/kg NO NO 30 Trichloroethene ug/kg NO NO 30 Trichlorofluoromethane uglkg NO NO 30 Vinyl acetate ug/kg NO NO 30 Vinyl chloride uglkg NO NO 30 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 22 of 32 °nelac aceAnalytical w»w.pecelebs.com i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, INC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE DUPLICATE: 323470 9250959005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Xylene (Total) ug/kg ND ND 30 1,2-Dichloroethane-d4 (S) % 109 113 0 4-Bromofluorobenzene (S) % 95 92 6 Dibromofluoromethane (S) % 103 100 6 Toluene-d8 (S) % 97 98 3 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. elac-: Page 23 of 32 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 .Pace/abs.� Asheville, NC 28804 Huntersville, NC 28078 i (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 QC Batch: WETA/5692 Analysis Method: EPA 353.2 QC Batch Method EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite Associated Lab Samples: 9250959003 METHOD BLANK: 323775 Matrix: Solid Associated Lab Samples: 9250959003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/kg ND 1.0 08/18/09 1747 Nitrogen, Nitrite ni ND 1.0 08/18/09 17:47 Nitrogen, NO2 plus NO3 mg/kg NO 1.0 08/18/09 17:47 LABORATORY CONTROL SAMPLE: 323776 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/kg 50 52.7 105 90-110 Nitrogen, Nitrite mg/kg 10 10.6 106 90-110 Nitrogen, NO2 plus NO3 mg/kg 50 52.7 105 90-110 MATRIX SPIKE SAMPLE: 323777 9250463001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/kg NO 474 509 107 90-110 Nitrogen, Nitrite mg/kg NO 94.8 120 124 90-110 MO Nitrogen, NO2 plus NO3 mg/kg ND 474 509 107 90-110 SAMPLE DUPLICATE: 323778 9250486001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Nitrogen, Nitrate mg/kg ND ND 20 Nitrogen, Nitrite mg/kg 18.4 25.4 8 20 Nitrogen, NO2 plus NO3 mg/kg ND ND 20 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac" Page 24 of 32 �ce ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 %ow.pacebbs.coar Asheville, NC 28804 Hunlersville, NC 28078 (828)254-7176 i (704)875-9092 QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 QC Balch: WETAIS713 Analysis Method: ASTM D516-90 OC Balch Method: ASTM D516-90 Analysis Description: ASTM D516-90 Sulfate Soil Associated Lab Samples: 9250959003 METHOD BLANK: 325408 Matrix: Solid Associated Lab Samples: 9250959003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/kg NO 50.0 08/21/0911:30 LABORATORY CONTROL SAMPLE: 325409 Spike LCS 1-CS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Sulfate mg/kg 200 202 101 90-110 MATRIX SPIKE SAMPLE: 325410 9250959003 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Sulfate mg/kg 88.2 247 313 91 75-125 SAMPLE DUPLICATE: 325412 9251068002 Dup Max Parameter Units Result Result RED RPD Qualifiers Sulfate mg/kg 412 389 6 20 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 25 of 32 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 w 'Pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 QC Balch: MERP/2326 Analysis Method: EPA 7471 QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury Associated Lab Samples: 9250959001. 9250959003, 9250959004 METHOD BLANK: 323535 Matrix: Solid Associated Lab Samples: 9250959001, 9250959003, 9250959004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury mg/kg NO 0.0050 08/20/0913:09 LABORATORY CONTROL SAMPLE: 323536 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/kg .067 0.065 98 80-120 MATRIX SPIKE SAMPLE: 323537 9250504001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury mg/kg 0.38 .076 0.38 5 75-125 MO SAMPLE DUPLICATE: 323538 9250504002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Mercury mg/kg 0.0058 0.0060 4 20 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, Inc.. nelac,, Page 26 of 32 m aceAnalytical vvnvpacelabs.mm i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA OC Batch: MPRP/4925 Analysis Method: EPA 6010 QC Batch Method: EPA 3050 Analysis Description: 6010 MET Associated Lab Samples: 9250959001, 9250959003, 9250959004 METHOD BLANK: 323540 Matrix: Solid Associated Lab Samples: 9250959001, 9250959003, 9250959004 Blank Reporting Parameter Units Result Limit Antimony mg/kg ND Arsenic mg/kg ND Beryllium mg/kg ND Cadmium mg/kg ND Chromium mg/kg ND Copper mg/kg ND Iron mg/kg ND Lead mg/kg ND Nickel mg/kg ND Selenium mg/kg ND Silver mg/kg ND Thallium mg/kg ND Zinc mg/kg 1.5 Analyzed 0.50 08/19/0914:54 0.50 08/19/0914:54 0.10 08/19/0914:54 0.10 08/19/0914:54 0.50 08/19/0914:54 0.50 08/19/0914:54 5.0 08/19/0914:54 0.50 08/19/0914:54 0.50 08/19/0914:54 1.0 08/19/0914:54 0.50 08/19/0914:54 1.0 08/19/0914:54 1.0 08/19/0914:54 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 323541 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony mg/kg 50 50.3 101 80-120 Arsenic mg/kg 50 49.7 99 80-120 Beryllium mg/kg 50 58.0 116 80-120 Cadmium mg/kg 50 50.2 100 80-120 Chromium mg/kg 50 50.7 101 80-120 Copper ni 50 49.2 98 80-120 Iron mg/kg 500 532 106 80-120 Lead mg/kg 50 49.9 100 80-120 Nickel mg/kg 50 51.0 102 80-120 Selenium mg/kg 50 49.8 100 80-120 Silver mg/kg 25 25.5 102 80-120 Thallium mg/kg 50 48.1 96 80-120 Zinc mg/kg 50 49.8 100 80-120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers MATRIX SPIKE SAMPLE: Parameter 323542 Units 9250804001 Result Spike Cone. MS Result MS % Rec % Rec Limits Qualifiers Antimony mg/kg 4.0 52.3 52.6 93 75-125 Arsenic mg/kg 20.9 52.3 70.0 94 75-125 Beryllium mg/kg 0.64 52.3 54.8 104 75-125 Cadmium mg/kg 1A 52.3 45.9 85 75-125 Chromium mg/kg 32.5 52.3 73.6 79 75-125 Copper mg/kg 112 52.3 142 56 75-125 MO Date: O8126/2009 09.36 AM REPORT OF LABORATORY ANALYSIS Page 27 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc :'nelac ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. _ aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 emvpsceebs.c Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 i QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 MATRIX SPIKE SAMPLE: 323542 9250804001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Iron mg/kg 9210 523 8640 -109 75-125 MO Lead mg/kg 45.6 52.3 72.8 52 75-125 MO Nickel mg/kg 15.4 52.3 56.8 79 75-125 Selenium mg/kg 2.6 52.3 53.6 98 75-125 Silver mg/kg 0.69 26A 25.8 96 75-125 Thallium mg/kg ND 52.3 37.1 71 75-125 MO Zinc mg/kg 199 52.3 230 59 75-125 MO SAMPLE DUPLICATE: 323543 Parameter Units 9250921009 Result Dup Result RPD Max RPD Qualifiers Antimony mg/kg 8A 16.0 66 20 R1 Arsenic mg/kg 0.83 1.3 41 20 R1 Beryllium mg/kg 1.1 1.0 7 20 Cadmium mg/kg 3.1 2.3 30 20 R1 Chromium mg/kg 182 379 70 20 Rl Copper mg/kg 101 99.7 1 20 Iron mg/kg 21900 21800 1 20 Lead mg/kg 715 1770 85 20 Nickel mg/kg 27.9 23.9 16 20 Selenium mg/kg 2.5 1.7 38 20 RI Silver mg/kg 0.15J AW 20 Thallium mg/kg NO NO 20 Zinc mg/kg 106 99.4 6 20 Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS This report shall Trot be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac, Page 28 of 32 11�aceAnalytical® wxw.pacelaescarn i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA OC Balch: PMST/2650 Analysis Method: ASTM D2974-87 OC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 9250959001, 9250959002, 9250959003, 9250959005 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE DUPLICATE: 323321 9250921011 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 12.6 12.7 1 25 SAMPLE DUPLICATE: 323322 9251006001 Cup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 14.8 14.8 0 25 Date: 081261200909:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. n -,elac ,. Page 29 of 32 aceAnalytical / e»wpacebbs.carn I Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 QC Batch: WETA/5712 Analysis Method: Sell 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 9250959003 METHOD BLANK: 325404 Associated Lab Samples: 9250959003 Parameter Units mg/kg Chloride LABORATORY CONTROL SAMPLE: 325405 Parameter Units Chloride mg/kg MATRIX SPIKE SAMPLE: 325407 Parameter Units Chloride mg/kg SAMPLE DUPLICATE: 325406 Parameter Chloride Date: 08/26/2009 09:36 AM Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 50.0 0812110909:03 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 200 211 105 90-1'10 9250959003 Spike MS MS % Rec Result Cone. Result % Rec Limits Qualifiers 85.5 247 336 101 75-125 9250959003 Dup Max Units Result Result RPD RPD Qualifiers mg/kg 85.5 84.4 1 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. °nelac Page 30 of 32 aceAnalytical e»w.pacelabs.com I Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: PMST12654 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 9250959004 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE DUPLICATE: 323966 9250713009 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 4.1 3.9 3 25 SAMPLE DUPLICATE: 323967 9251062002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 7.9 9.7 20 25 Date: 08126/200909:36 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac` Page 31 of 32 aceAnalytical www.pece/a63.cam i QUALIFIERS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9250959 '.�19ii[�7:E9 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 Q04)875-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES PAST -A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyle recovery in the laboratory control sample (LCS) was outside QC limits. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten limes greater than the blank or were below the reporting limit. R1 RPD value was outside control limits. Date: 08/26/2009 09:36 AM REPORT OF LABORATORY ANALYSIS Page 32 of 32 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Melac` N N O >al PalaaS N o o y a tPawn� L L 0 K o o uo � tl m 3 o a w (N/A) ouuol40 lanPlsea �. aI away r o z Jm _ a I m ❑ m } L L _Oi K N O y A 1 m z D L. L �. mo .attlJ+r z a � m 09L8 1NIA tIsay slsNsuyt rm loueylayp c w S a, V a FOiSzaN HOaN IOH a OONH P2NBSBla11(1 , aQ $ SL3NIVINOO JOp I,� � d d zed NOLL03llO�ltl dW3L 31d WVS pp �$S 4 n i S m � o a o E _ R chi w O1 o n 3 di V.)< $ 8" � a d € € C0 o o y _ (MOOrd 9V =O) 3dA 318Wtl V �L V a 7 W N rL E p aaooxlaitlw m O._ r y� b Z K 0 6✓�i036ro arc rc PP PLP yyWW�� � U � E ; .aZ-QIII Q NN ZF �1¢n8> J Fi33d�o3 ati6 � Q _ w I,L CN pp 0 /J 1 1 2 O $ 3 f( w g J$ < S .J ^ y r �I o E u Y'/ CD c to s V) V, s.. uYrc cS d � rc pW311 a n m w a ace Analytical' / Sample Condition Upon Receipt Client Name: lq c5ed p" Project # 90?5029 0 Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑- Client [I Commercial l�PacerOtOther r Custody Seal on Cooler/Box Present: L� yes ElIGi no Seals intact: yes ❑ no Packing Material: []Bubble Wrap ❑Bubble Bags ,_,/None rrx, r+--�r��*�r:`<rax L'J ❑Other �, Thermometer Used. -Gu f12 / 72490786 Type of fee: YV)Jt Blue None LI/ Samples on ice, cooling process has begun Temp Correction Factor: Add / bt ac • � C Corrected Cooler Temp.: C Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No Comments: Date and Initials of per son 9 nVI contents: d'a /Y a) Chain of Custody Present: ?Ves ONO OWA 1. Chain of Custody Filled Out: faces ONO OWA 2. Chain of Custody Relinquished: L41es ONO ElN/A 3. Sampler Name & Signature on COC: tags ONO OWA 4. Samples Arrived within Hold Time: XTves ONO OWA 5. Short Hold Time Analysis (<72hr): Oves We I]WA 6. Rush Turn Around Time Requested: (]Yes 21F. ON/A 7, Sufficient Volume: lelles ONO OWA 8. Correct Containers Used: -Pace Containers Used: Gw.s ON. ayes ONO OWA OWA 9. Cont fners Intact: tKs ONO OWA 10. - Filtered volume received for Dissolved tests OYes ONO /A it - Sample Labels match CDC: -Includes dale/time/ID/Analysis Matrix: 121VOs ONO :5 Z' OWA 12. All containers needing preservation have been checked- All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliform, TOC, OaG, WI-DRO imter) .)rK5 ONO [k�es ONO �s ON. OWA OWA 13. ..� Initials en completed Samples checked for dechlorination: Elves ONO PtVA 14. Headspace fn VOA Vials (>6mm): OYes ONO 17WA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot If if purchased): OYes ONO Elves ONO eNIA WWA 16. Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time, Field Data Required? Y / N Project Manager Review: 0'4 1fi(9:� Date: 811( 16 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wil be sent to the North Carolina Certification (mice r i e nut of hnkl inreirrnrt nracarvativn nut of tmmin inrnrrart rnntainn.c\ 2ceAnaljdical' vnnvpacetabs.00m i August 26, 2009 Mr. Bob Wyrick AECOM Environment 7041 Old Wake Forest Road Suite 103 Raleigh, NC 27616 RE: Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Dear Mr. Wyrick: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on August 18, 2009. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, '9A.oqa�' Felicia Grogan felicia.grogan@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. °nelac` Page 1 of 27 aceftlytical wmxpacela6s.com I Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Anatytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Charlotte Certification IDs Connecticut Certification #: PH-0104 Pennsylvania Certification M 68-00784 Florida/NELAP Certification If: E87627 North Carolina Wastewater Certification #: 12 West Virginia Certification M 357 North Carolina Field Services Certification M 5342 Virginia Certification #: 00213 North Carolina Drinking Water Certification M 37706 Tennessee Certification #: 04010 New Jersey Certification M NCO12 South Carolina Drinking Water Cent. #: 990060003 Louisiana/LELAP Certification If 04034 South Carolina Certification M 990060001 Kentucky UST Certification #: 84 Asheville Certification IDs Connecticut Certification #: PH-0106 North Carolina Drinking Water Certification #: 37712 Virginia Certification #: 00072 North Carolina Bioassay Certification #: 9 Tennessee Certification #: 2980 New Jersey Certification M NC011 South Carolina Certification #: 99030001 Massachusetts Certification M M-NC030 South Carolina Bioassay Certification M 99030002 Louisiana/LELAP Certification #: 03095 Pennsylvania Certification #: 68-03578 Florida/NELAP Certification #: E87648 West Virginia Certification M 356 North Carolina Wastewater Certification M 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac Page 2 of 27 ace Analytical' www.pacela0.s.com i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received 9251168001 MW-2 Water 0811710914:00 08118/0916:35 9251168002 MW-3 Water 08117/0915:00 08/18/0916:35 9251168003 MW-4 Water 08/17/0917:00 08/18/0916:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac` Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 27 0Analytical .pscelabs.can i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 9251168001 MW-2 ASTM D516-90 LEP 1 PASI-A EPA 353.2 SAJ 3 PASI-A EPA 6010 SHB 13 PASI-A EPA 7470 SAJ 1 PASI-A EPA8260 MCK 63 PASI-C EPA8270 BET 21 PASI-C SM 2540C TEE 1 PASI-A SM 4500-CI-E LEP 1 PASI-A 9251168002 MW-3 ASTM D516-90 LEP 1 PASI-A EPA 353.2 SAJ 3 PASI-A EPA 6010 SHB 13 PASI-A EPA 7470 SAJ 1 PASI-A EPA 8260 MCK 63 PASI-C EPA 8270 BET 21 PASI-C SM 2540C TEE 1 PASI-A SM 4500-CI-E LEP 1 PASI-A 9251168003 MW-4 ASTM D516-90 LEP 1 PASI-A EPA 353.2 SAJ 3 PASI-A EPA 6010 SHB 13 PASI-A EPA 7470 SAJ 1 PASI-A EPA 8260 MCK 63 PASI-C EPA 8270 BET 21 PASI-C SM 2540C TEE 1 PASI-A SM 4500-CI-E LEP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac Page 4 of 27 11�;aceAnalyfical' wvw.pace/abscarn I Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Sample: MW-2 Lab ID: 9251168001 Collected: 08/17/0914:00 Received: 08/18/0916:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony NO ug/L 5.0 1 08/21/09 11:10 08/24/09 17:44 7440-36-0 Arsenic ND ug/L 5.0 1 08/21/09 11:10 08/24/09 17:44 7440-38-2 Beryllium NO ug/L 1.0 1 08121/0911:10 0812410917:44 7440-41-7 Cadmium NO ug/L 1.0 1 0812110911:10 0812410917,44 7440-43-9 Chromium NO ug/L 5.0 1 08/21/09 11:10 08124/0917,44 7440-47-3 Copper NO ug/L 5.0 1 08121/0911:10 08124/0917:44 7440-50-8 Iron 43400 ug/L 50.0 1 08/21/09 11:10 08/24/0917:44 7439-89-6 Lead NO ug/L 5.0 1 08/21/09 11:10 08/24/0917:44 7439-92-1 Nickel 22.0 ug/L 5.0 1 08/21/09 11:10 08/24/09 17:44 7440-02-0 Selenium ND ug/L 10.0 1 08/21/09 11:10 08/24/0917:44 7782-49-2 Silver NO ug/L 5.0 1 08/2110911:10 08/24/0917:44 7440-22-4 Thallium ND ug/L 10.0 1 08/21/09 11:10 08/24/09 17:44 7440-28-0 Zinc 106 ug/L 10.0 1 08/2110911:10 0812410917:44 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury NO ug/L 0.20 1 08/24/09 09:43 08/24/09 12:22 7439-97-6 8270 MSSV PAH SPE Analytical Method: EPA 8270 Preparation Method: EPA 3535 Acenaphthene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 83-32-9 Acenaphthylene NO ug/L 11.1 1 0811910914:00 08/2110917*15 208-96-8 Anthracene NO ug/L 11.1 1 08119/0914:00 0812110917:15 120-12-7 Benzo(a)anthracene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 56-55-3 Benzo(a)pyrene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 50-32-8 Benzo(b)nuoranthene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 205-99-2 Benzo(g,h,i)perylene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 191-24-2 Benzo(k)Ouoranthene NO ug/L 11.1 1 08/19/09 14:00 08/211091715 207-08-9 Chrysene ND ug/L 11A 1 08/19/09 14:00 08/21/0917*15 218-01-9 Dibenz(a,h)anthracene ND ug/L 11A 1 08/19/09 14:00 08/21/09 17:15 53-70-3 Fluoranthene NO ug/L 11A 1 08/19/09 14:00 08/21/09 WAS 206-44-0 Fluorene NO u9/L 11A 1 08/19/09 14:00 08/21/09 17:15 86-73-7 Indeno(1,2,3-cd)pyrene NO ug/L 11A 1 08/19/09 14:00 08/21/09 17:15 193-39-5 1-Methylnaphthalene ND ug/L 11A 1 08/19/09 1400 08/21/09 17:15 90-12-0 2-Methylnaphthalene ND ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 91-57-6 Naphthalene ND ug/L 11A 1 08/19/09 14:00 08/21/09 17:15 91-20-3 Phenanthrene NO ug/L 11.1 1 08/19/09 14:00 08/21/0917:15 85-01-8 Pyrene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:15 129-00-0 Nitrobenzene-d5 (S) 27 % 10-120 1 08/19/09 14:00 08/21/0917:15 4165-60-0 2-Fluorobiphenyl (S) 45 % 10-120 1 08/19/09 14:00 08/21/09 17:15 321-60-8 Terphenyl-dl4 (S) 59 % 10-116 1 08/19/09 14:00 08/21/0917:15 1718-51-0 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO ug/L 25-0 1 08/20/09 06:17 67-64-1 Benzene NO ug/L 1.0 1 08/20/09 06:17 71-43-2 Bromobenzene NO ug/L 1.0 1 08/20/09 06:17 108-86-1 Bromochloromethane NO ug/L 1.0 1 08/20/09 06:17 74-97-5 Bromodichloromethane NO ug/L 1.0 1 08/20/09 06:17 75-27-4 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS Page 5 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac aceAnalytical ewwpecelabs.rom I Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-2 Lab ID: 9251168001 Collected: 0811710914:00 Received: 0811810916:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Bromoform ND ug/L 1.0 1 08/20/09 06:17 75-25-2 Bromomethane ND ug/L 5.0 1 08/20/09 06:17 74-83-9 2-Bulanone(MEK) ND ug/L 5.0 1 08120/0906:17 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 08/2010906:17 56-23-5 Chlorobenzene ND ug/L 1.0 1 08/2010906:17 108-90-7 Chloroethane ND ug/L 1.0 1 08/2010906: 17 75-00-3 Chloroform ND ug/L 1.0 1 08/2010906: 17 67-66-3 Chloromethane ND ug/L 1.0 1 08/2010906:17 74-87-3 2-Chlorololuene ND ug/L 1.0 1 08/20/0906: 17 95-49-8 4-Chlorololuene ND ug/L 1.0 1 08/20/0906:17 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/20/09 06:17 96-12-8 Dibromochloromelhane ND ug/L 1.0 1 08/20/09 06:17 124-48-1 1,2-Dibromoethane(EDB) NO ug/L 1.0 1 08/20/0906.17 106-93-4 Dibromomethane NO ug/L 1.0 1 08/20/09 06:17 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 08/20/09 06:17 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 08/20/09 06:17 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 08/20/09 06:17 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 08120/0906:17 75-71-8 1,1-Dichloroelhane NO ug/L 1.0 ..1 - 08/20/0906:17 75-34-3 1,2-Dichloroelhane NO ug/L 1.0 1 08120/0906:17 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 08/20/09 06:17 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 08/20/09 06:17 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 08/20/09 06:17 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 08120/0906:17 78-87-5 1,3-Dichloropropane NO ug/L 1.0 1 08120/0906:17 142-28-9 2,2-Dichloropropane NO ug/L 1.0 1 08/20/09 06:17 594-20-7 1,1-Dichloropropene NO ug/L 1.0 1 08/20/0906:17 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 0812010906:17 10061-01-5 trans-1,3-Dichloropropene NO ug/L 1.0 1 08/20/09 06:17 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 08/20/09 06:17 108-20-3 Ethylbenzene ND ug/L 1.0 1 08120/0906:17 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/20/0906:17 87-68-3 2-Hexanone NO ug/L 5.0 1 08/20/09 06:17 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 08/20/09 06:17 99-87-6 Methylene Chloride ND ug/L 2.0 1 08/20/09 06:17 75-09-2 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 1 08/20/0906:17 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 08/20/09 06:17 1634-04-4 Naphthalene ND ug/L 1.0 1 08/20/09 06:17 91-20-3 Styrene ND ug/L 1.0 1 08/20/09 06:17 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/20/09 06:17 630-20-6 1,1 2,2-Tetrachloroethane ND ug/L 1.0 1 08/20/0906:17 79-34-5 Tetrachloroethene ND ug/L 1.0 1 08/20/09 06:17 127-18-4 Toluene 1.0 ug/L 1.0 1 08/20/09 06:17 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/20/09 06:17 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/20/09 06:17 120-82-1 1,1, 1-Trichloroethane ND ug/L 1.0 1 08/20/0906: 17 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 08120/0906:17 79-00-5 Date: 08126/200909:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac': Page 6 of 27 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalj&al 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 w Patxli Asheville, NC 28804 Huntersville, NC 28078 ANALYTICAL RESULTS (828)254-7176 (704)075-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Sample: MW-2 Lab ID: 9251168001 Collected: 08/17/09 14:00 Received: 08/18/09 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 8260 MSV Low Level Trichloroethene Trichloro0uoromethane 1,2, 3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromo8uoromethane (S) 1,2-Dichloroelhane-d4 (S) Toluene-d8 (S) 2540C Total Dissolved Solids Total Dissolved Solids 353.2 Nitrogen, N021NO3 unpres Nitrogen, Nitrate Nitrogen, Nitrite Nitrogen, NO2 plus NO3 4500 Chloride Chloride ASTM D516-90 Sulfate Water Sulfate Date: 08/26/2009 09:35 AM Analytical Method: EPA 8260 ND ug/L NO ug/L ND ug/L ND ug/L ND ug/L NO ug/L NO ug/L 99 % 102 % 108 % 101 % Analytical Method: SM 2540C 222 mg/L Analytical Method: EPA 353.2 ND mg/L ND mg/L NO mg/L Analytical Method: SM 4500-CI-E 10.5 mg/L Analytical Method: ASTM D516-90 NO mg/L 1.0 1.0 1.0 2.0 1.0 2.0 1.0 87-109 85-115 79-120 70-120 20.0 1 0.10 1 0.10 1 0.10 1 5.0 1 5.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. := nelac` 08/20/09 06:17 79-01-6 08/20/09 06:17 75-69-4 08/20/09 06:17 96-18-4 08/20/09 06:17 108-05-4 08/20/09 06:17 75-01-4 08/20/09 06:17 1330-20-7 08/20/09 06:17 95-47-6 08/20/09 06:17 460-00-4 08/20/09 06:17 1868-53-7 08/20/09 06:17 17060-07-0 08/20/09 06:17 2037-26-5 08/21/09 20:59 08/19/09 10:08 08/19/09 10:08 08/19/09 10:08 08/24/09 15:44 16887-00-6 08121 /09 14:06 14808-79-8 Page 7 of 27 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 v .pecelabs corn Asheville, NC 28804 Hunterwille, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Sample: MW-3 Lab ID: 9251168002 Collected: 08117/0915:00 Received: 08/18/09 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony NO ug/L 5.0 1 0812110911:10 08/24/09 18:03 7440-36-0 Arsenic 5.1 ug/L 5.0 1 08/21/09 11:10 08/24/09 18:03 7440-38-2 Beryllium ND ug/L 1.0 1 08/21/09 11:10 08/24/09 18:03 7440-41-7 Cadmium NO ug/L 1.0 1 08121/0911:10 08/24/0918:03 7440-43-9 Chromium NO ug/L 5.0 1 08121/0911:10 0812410918:03 7440-47-3 Copper NO ug/L 5.0 1 08121/0911:10 08/2410918:03 7440-50-8 Iron 18200 ug/L 50.0 1 08/21/0911:10 0812410918,03 7439-89-6 Lead NO ug/L 5.0 1 08/21/09 11:10 08/2410918:03 7439-92-1 Nickel 8.7 ug/L 5.0 1 08/21/09 11:10 08/24/09 18:03 7440-02-0 Selenium NO ug/L 10.0 1 08/21/09 11:10 08/24/09 18:03 7782-49-2 Silver NO ug/L 5.0 1 08/21/09 11:10 08/24/09 18:03 7440-22-4 Thallium NO ug/L 10.0 1 08/21/09 11:10 08/24/09 18:03 7440-28-0 Zinc 52.8 ug/L 10.0 1 08/21/09 11:10 08/24/09 18:03 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury NO ug/L 0.20 1 08/24/0909:43 08/24/0912:27 7439-97-6 8270 MSSV PAH SIDE Analytical Method: EPA 8270 Preparation Method: EPA 3535 Acenaphthene ND ug/L 11.1 1 08/19/09 14:00 08/2110917:41 83-32-9 Acenaphthylene ND ug/L 11.1 1 08/19/09 14:00 08/2110917:41 208-96-8 Anthracene ND ug/L 11.1 1 08119/0914:00 08/21/09 17:41 120-12-7 Benzo(a)anthracene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 56-55-3 Benzo(a)pyrene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 50-32-8 Benzo(b)Ouoranthene NO ug/L 11.1 1 08/19/0914:00 08/21/09 17*41 205-99-2 Benzo(9,h,i)perylene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 191-24-2 Benzo(k)Ouoranthene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 207-08-9 Chrysene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 218-01-9 Dibenz(a,h)anthracene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 53-70-3 Fluoranthene NO uglL 11.1 1 08/19/09 14:00 08/21/09 17,41 206-44-0 Fluorene NO uglL 11.1 1 08/19/09 14:00 08/21/09 17:41 86-73-7 Indeno(1,2,3-cd)pyrene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 193-39-5 1-Methylnaphthalene ND ug/L 11.1 1 08/1910914:00 08/21/0917:41 90-12-0 2-Methylnaphthalene ND ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 91-57-6 Naphthalene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 91-20-3 Phenanthrene NO ug/L 11.1 1 08/1910914:00 0812110917:41 85-01-8 Pyrene ND ug/L 11.1 1 08/19/09 14:00 08/21/09 17:41 129-00-0 Nitrobenzene-d5 (S) 24 % 10-120 1 08/19/09 14:00 08/21/09 17:41 4165-60-0 2-Fluorobiphenyl (S) 36 % 10-120 1 08/1910914:00 08/21/09 17:41 321-60-8 Terphenyl-d14(S) 57 % 10-116 1 08/19/09 14:00 08/21/0917:41 1718-51-0 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 08/20/09 06:36 67-64-1 Benzene NO ug/L 1.0 1 08/20/09 06:36 71-43-2 Bromobenzene NO ug/L 1.0 1 08/20/09 06:36 108-86-1 Bromochloromethane NO ug/L 1.0 1 08/20/09 06:36 74-97-5 Bromodichloromethane NO ug/L 1.0 1 08/20/09 06:36 75-27-4 Date: 08/26/2009 09:35AM REPORT OF LABORATORY ANALYSIS Page 8 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc_ ;° nelac` ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wnw.pecelabscors Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 I (704)875-9092 ace ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Sample: MW-3 Lab ID: 9251168002 Collected: 08/17/0915:00 Received: 08118/0916:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Bromoform NO ug/L 1.0 1 08/20/09 06,36 75-25-2 Bromomethane NO ug/L 5.0 1 0812010906:36 74-83-9 2-Butanone(MEK) NO ug/L 5.0 1 08/20/09 06:36 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 08/20/09 06:36 56-23-5 Chlorobenzene 1.0 ug/L 1.0 1 08/20/09 06:36 108-90-7 Chloroethane NO ug/L 1.0 1 08/20/09 06:36 75-00-3 Chloroform 3.4 ug/L 1.0 1 08/20/09 06:36 67-66-3 Chloromethane NO ug/L 1.0 1 08/20/09 06,36 74-87-3 2-Chlorotoluene NO ug/L 1.0 1 08/20/09 06:36 95-49-8 4-Chlorotoluene NO ug/L 1.0 1 08/20/09 06,36 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 3.0 1 08/20/09 06:36 96-12-8 Dibromochloromethane NO ug/L 1.0 1 08/20/09 06:36 124-48-1 1,2-Dibromoelhane(EDB) NO ug/L 1.0 1 08/20/09 06:36 106-93-4 Dibromomethane NO ug/L 1.0 1 08120/0906:36 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 08/20/09 06:36 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 08/20/09 06:36 541-73-1 1,4-Dichlorobenzene NO uglL 1.0 1 08/20/09 06:36 106-46-7 Dichlorodi0uoromethane NO ug/L 1.0 1 0812010906:36 75-71-8 1,1-Dichloroethane NO ug/L 1.0 1 0812010906:36 75-34-3. 1,2-Dichloroethane NO ug/L 1.0 1 08/20/09 06:36 107-06-2 1,1-Dichloroelhene NO uglL 1.0 1 08/20/09 06:36 75-35-4 cis-1,2-Dichloroelhene NO ug/L 1.0 1 08120/0906:36 156-59-2 trans-1,2-Dichloroelhene NO ug/L 1.0 1 08/20/09 06:36 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 0812010906:36 78-87-5 1,3-Dichloropropane NO ug/L 1.0 1 08/20/09 06:36 142-28-9 2,2-Dichloropropane NO ug/L 1.0 1 08/20/09 06:36 594-20-7 1,1-Dichloropropene NO ug/L 1.0 1 08/20/09 06:36 563-58-6 cis-1,3-Dichloropropene NO ug/L 1.0 1 08/20/09 06:36 10061-01-5 trans-1,3-Dichloropropene NO ug/L 1.0 1 08/20/09 06:36 10061-02-6 Diisopropyl ether NO ug/L 1.0 1 08/20/09 06:36 108-20-3 Ethylbenzene NO ug/L 1.0 1 08/20/0906:36 100-41-4 Hexachloro-1,3-butadiene NO ug/L 1.0 1 08/20/0906:36 87-68-3 2-Hexanone NO ug/L 5.0 1 08/20/09 06:36 591-78-6 p-Isopropyltoluene NO ug/L 1.0 1 08/20/09 06:36 99-87-6 Methylene Chloride NO ug/L 2.0 1 08/20/09 06:36 75-09-2 4-Methyl-2-pentanone(MIBK) NO ug/L 5.0 1 0812010906:36 108-10-1 Methyl-tert-butyl ether NO ug/L 1.0 1 08/20/09 06:36 1634-04-4 Naphthalene NO ug/L 1.0 1 0812010906:36 91-20-3 Styrene NO ug/L 1.0 1 08/20/09 06:36 100-42-5 1,1,1,2-Tetrachloroethane NO ug/L 1.0 1 08/20/09 06:36 630-20-6 1,1,2,2-Tetrachloroethane NO ug/L 1.0 1 08/20/0906:36 79-34-5 Tetrachloroethene NO uglL 1.0 1 08/20/09 06:36 127-18-4 Toluene NO ug/L 1.0 1 08/20/09 06:36 108-88-3 1,2,3-Trichlorobenzene NO ug/L 1.0 1 08/2010906:36 87-61-6 1,2,4-Trichlorobenzene NO ug/L 1.0 1 08/20/09 06:36 120-82-1 1,1,1-Trichloroethane NO ug/L 1.0 1 08/2010906:36 71-55-6 1,1 2-Trichloroethane ND ug/L 1.0 1 0812010906:36 79-00-5 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS Page 9 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. "nelac aceAnaljdkal - mrw.pacNa6scan i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-3 Lab ID: 9251168002 Collected: 08/17/09 15:00 Received: 08/18/09 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 8260 MSV Low Level Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Toluene-d8(S) 2540C Total Dissolved Solids Total Dissolved Solids 353.2 Nitrogen, N021NO3 unpres Nitrogen, Nitrate Nitrogen, Nitrite Nitrogen, NO2 plus NO3 4500 Chloride Chloride ASTM D516-90 Sulfate Water Sulfate Date: 08/26/2009 09:35 AM Analytical Method: EPA 8260 ND ug/L ND ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L 99 103 110 101 Analytical Method: SM 2540C 344 mg/L Analytical Method: EPA 353.2 ND mg/L ND mg/L ND mg/L Analytical Method: SM 4500-CI-E 19.1 mg/L Analytical Method: ASTM D516-90 21.9 mg/L 1.0 1 08/20/09 06:36 79-01-6 1.0 1 08/20/09 06:36 75-69-4 1.0 1 08/20/09 06:36 96-18-4 2.0 1 08/20/09 06:36 108-05-4 1.0 1 08/20/09 06:36 75-01-4 2.0 1 08/20/09 06:36 1330-20-7 1.0 1 08/20/09 06:36 95-47-6 87-109 1 08/20/09 06:36 460-00-4 85-115 1 08/20/09 06:36 1868-53-7 79-120 1 08/20/09 06:36 17060-07-0 70-120 1 08/20/09 06:36 2037-26-5 20.0 1 0.10 1 0.10 1 0.10 1 5.0 1 5.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac`,; 08/21/09 20:59 08119/09 10:08 08/19/09 10:08 08119/09 10:08 08/24/09 15:44 16887-00-6 08/21/09 14:09 14808-79-8 Page 10 of 27 aceAnalytical wxw.paoelabs.rom I Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-4 Lab ID: 9251168003 Collected: 0811710917:00 Received: 08118/0916:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3010 Antimony NO ug/L 5.0 1 08/21/09 11:10 08/24/09 18:08 7440-36-0 Arsenic NO ug/L 5.0 1 08/21/09 11:10 08/24/09 18:08 7440-38-2 Beryllium NO ug/L 1.0 1 08/2110911:10 08124/0918:08 7440-41-7 Cadmium NO ug/L 1.0 1 08121/0911:10 0812410918:08 7440-43-9 Chromium ND ug/L 5.0 1 08/21/09 11:10 08/24/09 18:08 7440-47-3 Copper NO ug/L 5.0 1 08/21/09 11:10 08/24/0918:08 7440-50-8 Iron 33400 ug/L 50.0 1 0812110911:10 08/24/09 18:08 7439-89-6 Lead NO ug/L 5.0 1 08/21/09 11:10 08/24/09 18:08 7439-92-1 Nickel NO ug/L 5.0 1 08/21/09 11:10 08/24/09 18:08 7440-02-0 Selenium NO ug/L 10.0 1 08/21/09 11:10 08/24/09 18:08 7782-49-2 Silver NO ug/1- 5.0 1 08/21/09 11:10 08/24/09 18:08 7440-22-4 Thallium NO ug/L 10.0 1 08/2110911:10 08/24/0918:08 7440-28-0 Zinc NO ug/L 10.0 1 08/21/09 11:10 08/24/09 18:08 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury NO ug/L 0.20 1 08/24/09 09:43 08/24/09 12:30 7439-97-6 8270 MSSV PAH SPE Analytical Method: EPA 8270 Preparation Method: EPA 3535 Acenaphthene NO ug/L 11.1 1-' :::08/19109 14:00 08/21/09 18:07 83-32-9 Acenaphthylene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 208-96-8 Anthracene NO ug/L 11.1 1 0811910914:00 08/21/0918:07 120-12-7 Benzo(a)anthracene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 56-55-3 Benzo(a)pyrene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 1807 50-32-8 Benzo(b)nuoranthene ND ug/L 11A 1 08/19/09 14:00 08121/0918:07 205-99-2 Benzo(g,h,i)perylene ND ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 191-24-2 Benzo(k)nuoranthene ND ug/L 11.1 1 08/19/0914:00 08/21/09 18:07 207-08-9 Chrysene ND ug/L 11A 1 08/19/09 14:00 08/21/0918:07 218-01-9 Dibenz(a,h)anthracene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 53-70-3 Fluoranlhene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 206-44-0 Fluorene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 86-73-7 Indeno(1,2,3-cd)pyrene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 193-39-5 1-Methylnaphthalene NO ug/L 11.1 1 08/19/09 14:00 08/21/09 18:07 90-12-0 2-Methylnaphthalene NO ug/L 11.1 1 08/19/09 14:00 0812110918:07 91-57-6 Naphthalene NO ug/L 11.1 1 0811910914:00 08/2110918:07 91-20-3 Phenanthrene NO ug/L 11.1 1 0811910914:00 08/21/09 18:07 85-01-8 Pyrene ND ug/L 11A 1 08/1910914:00 0812110918:07 129-00-0 Nitrobenzene-d5 (S) 30 % 10-120 1 08119/0914:00 08/21/09 18:07 4165-60-0 2-Fluorobiphenyl (S) 52 % 10-120 1 08/19/09 14:00 08/21/09 18.07 321-60-8 Terphenyl-di4(S) 63% 10-116 1 08/19/09 14:00 08/21/0918:07 1718-51-0 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO ug/L 25.0 1 08/20/09 06:56 67-64-1 Benzene NO ug/L 1.0 1 08/20/09 06:56 71-43-2 Bromobenzene NO ug/L 1.0 1 08/20/09 06:56 108-86-1 Bromochloromethane NO ug/L 1.0 1 08/20/09 06:56 74-97-5 Bromodichloromethane NO ug/L 1.0 1 08/20/09 06:56 75-27-4 Dale: 08126/200909:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac`' Page 11 of 27 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnaiytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 %wxpacxlabsc Asheville, NC 28804 Huntersville, NC 28078 i (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Sample: MW-4 Lab ID: 9251168003 Collected: 08/17/0917:00 Received: 08118/0916:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 8260 MSV Low Level Analytical Method: EPA 8260 Bromoform ND ug/L 1D 1 08/2010906:56 75-25-2 Bromomethane ND ug/L 5.0 1 08/20/09 06:56 74-83-9 2-Butanone(MEK) ND ug/L 5.0 1 08/20/09 06:56 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 08/20/09 06:56 56-23.5 Chlorobenzene ND ug/L 1.0 1 08/20/0906:56 108-90-7 Chlomethane ND ug/L 1.0 1 08/2010906:56 75-00-3 Chloroform NO ug/L 1.0 1 08/20/09 06:56 67-66-3 Chloromethane NO ug/L 1.0 1 08/20/09 06:56 74-87-3 2-Chlorotoluene NO ug/L 1.0 1 08/20/09 06:56 95-49-8 4-Chlorotoluene NO ug/L 1.0 1 08120/0906:56 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 3.0 1 08/2010906:56 96-12-8 Dibromochloromelhane NO ug/L 1.0 1 08/20/09 06:56 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1D 1 08/2010906:56 106-93-4 Dibromomethane ND ug/L 1.0 1 08/20/09 06:56 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 08/20/09 06:56 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 08/20/09 06:56 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 08120/0906:56 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 0812010906:56 75-71-8 1,1-Dichloroethane ND ug/1- 1.0 1 08/20/09 06:56 75-34-3 1,2-Dichloroethane NO ug/L 1.0 1 08/20/09 06:56 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 08/20/09 06:56 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 08/20/09 06:56 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 08/20/0906:56 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 08/20/09 06:56 78-87-5 1,3-Dichloropropane NO ug/L 1.0 1 08/20/09 06:56 142-28-9 2,2-Dichloropropane NO ug/L 1.0 1 08/20/09 06:56 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 08/20/09 06:56 563-58-6 cis-1,3-Dichloropropene NO ug/L 1.0 1 08/20/09 06:56 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 08/20/09 06:56 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 08/20/09 06:56 108-20-3 Ethylbenzene NO ug/L 1.0 1 08/20/09 06:56 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 0812010906,56 87-68-3 2-Hexanone ND ug/L 5.0 1 08/2010906:56 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 08/20/09 06:56 99-87-6 Methylene Chloride ND ug/L 2.0 1 08/20/09 06:56 75-09-2 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 1 08/20/09 06:56 108-10-1 Methyl-terl-bulyl ether NO ug/L 1.0 1 08/20/09 06:56 1634-04-4 Naphthalene NO ug/L 1.0 1 0812010906:56 91-20-3 Styrene NO ug/L 1.0 1 08/20/09 06:56 100-42-5 1,1,1,2-Tetrachloroelhane NO ug/L 1.0 1 0812010906:56 630-20-6 1, 1,2,2-Tetrachloroelhane ND ug/L 1.0 1 08120/0906:56 79-34-5 Tetrachloroethene ND ug/L 1.0 1 08/20/09 06:56 127-18-4 Toluene ND ug/L 1.0 1 08/20/09 06:56 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/20/09 06:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/20/09 06:56 120-82-1 1, 1, 1-Trichloroethane ND ug/L 1.0 1 08120/0906:56 71-55-6 1. 1, 2-Trichloroethane ND ug/L 1.0 1 08/20/09 06:56 79-00-5 Date: 08/261200909:35 AM REPORT OF LABORATORY ANALYSIS Page 12 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac 2ceAnajfXical wwwpacelabs.cwn i Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Sample: MW-4 Lab ID: 9251168003 Collected: 08/17/09 17:00 Received: 08/1810916:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Trichlomethene Trichloro0uoromethane 1,2, 3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromo0uoromelhane (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2540C Total Dissolved Solids Total Dissolved Solids 353.2 Nitrogen, N021NO3 unpres Nitrogen, Nitrate Nitrogen, Nitrite Nitrogen, NO2 plus NO3 4500 Chloride Chloride ASTM D516-90 Sulfate Water Sulfate Date: 08/26/2009 09:35 AM Analytical Method: EPA 8260 NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L 98 % 104 % 108 % 101 % Analytical Method: SM 2540C 276 mg/L Analytical Method: EPA 353.2 ND mg/L NO mg/L NO mg/L Analytical Method: SM 4500-CI-E 13.9 mg/L Analytical Method: ASTM D516-90 NO mg/L 1.0 1 08/20/09 06:56 79-01-6 1.0 1 08/20/09 06:56 75-69-4 1.0 1 08/20/09 06:56 96-18-4 2.0 1 08/20/09 06:56 108-05-4 1.0 1 08/20/09 06:56 75-01-4 2.0 1 08/20/09 06:56 1330-20-7 1.0 1 08/20/09 06:56 95-47-6 87-109 1 08/20/09 06:56 460-00-4 85-115 1 08/20/09 06:56 1868-53-7 79-120 1 08/20/09 06:56 17060-07-0 70-120 1 08/20/09 06:56 2037-26-5 20.0 1 0.10 1 0.10 1 0.10 1 5.0 1 5.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac`r. 08/21/09 21:00 08/19/09 10:08 08/19/09 10:08 08/19/09 10:08 08/24/09 15:44 16887-00-6 08/21/09 14:09 14808-79-8 Page 13 of 27 0 2ceAnalytical wnwpscebbs.a%n i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MSV/8010 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 324276 Matrix: Associated Lab Samples: 9251168001, 9251168002, 9251168003 Blank Parameter Units Result Water Reporting Limit Analyzed 1,1,1,2-Telrachloroelhane ug/L NO 1.0 08/20/0900:30 1,1,1-Trichloroethane ug/L ND 1.0 08/2010900:30 1,1,2,2-Telrachloroelhane ug/L NO 1.0 08/2010900:30 1,1,2-Trichloroethane ug/L NO 1.0 0812010900:30 1,1-Dichloroethane ug/L ND 1.0 08/20/09 00:30 1,1-Dichloroethene ug/L NO 1.0 08/2010900:30 1,1-Dichloropropene ug/L NO 1.0 08/2010900:30 1,2,3-Trichlorobenzene ug/L ND 1.0 08/20/09 00:30 1,2,3-Trichloropropane ug/L ND 1.0 0812010900:30 1,2,4-Trichlorobenzene ug/L ND 1.0 08/20/09 00:30 1,2-Dibromo-3-chloropropane ug/L ND 3.0 08/20/09 00:30 1,2-Dibromoethane (EDB) ug/L NO 1.0 08/20/09 00:30 1,2-Dichlorobenzene ug/L NO 1.0 08/20/09 00:30 1,2-Dichloroethane ug/L NO 1.0 08120/0900:30 1,2-Dichloropropane -. ug/L NO 1.0 08/20/09 00:30 1,3-Dichlorobenzene ug/L NO 1.0 08/20/09 00:30 1,3-Dichloropropane ug/L ND 1.0 08/20/09 00:30 1,4-Dichlorobenzene ug/L NO 1.0 08/20/09 00:30 2,2-Dichloropropane ug/L NO 1.0 08/20/09 00:30 2-Butanone(MEK) ug/L NO 5.0 08/2010900:30 2-Chlorotoluene ug/L NO 1.0 08/20/09 00:30 2-Hexanone ug/L NO 5.0 08/20/09 00:30 4-Chlorotoluene ug/L NO 1.0 08/20/09 00:30 4-Methyl-2-penlanone(MIBK) ug/L NO 5.0 08/20/09 00:30 Acetone ug/L NO 25.0 08/20/09 00:30 Benzene ug/L NO 1.0 08/20/09 00:30 Bromobenzene ug/L NO 1.0 08/20/09 00:30 Bromochloromethane ug/L NO 1.0 08/20/09 00:30 Bromodichloromelhane ug/L NO 1.0 08/20/09 00:30 Bromoform ug/L ND 1.0 08/20/09 00:30 Bromomethane ug/L NO 5.0 08/2010900:30 Carbon tetrachloride ug/L ND 1.0 08/20/09 00:30 Chlorobenzene ug/L NO 1.0 08/20/09 00:30 Chlomethane ug/L NO 1.0 0812010900:30 Chloroform ug/L NO 1.0 08/20/09 00:30 Chloromethane ug/L NO 1.0 08/20/09 00:30 cis-1,2-Dichloroethene ug/L NO 1.0 08/20/0900:30 cis-1,3-Dichloropropene ug/L ND 1.0 0812010900:30 Dibromochloromethane ug/L ND 1.0 08/2010900:30 Dibromomelhane ug/L NO 1.0 08120/0900:30 Dichlorodifluoromethane ug/L NO 1.0 08/2010900:30 Diisopropyl ether ug/L NO 1.0 08/20/09 00:30 Ethylbenzene ug/L NO 1.0 08/20/09 00:30 Date: 08/26/2009 09:35AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, wilhoul the written consent of Pace Analytical Services, Inc.. Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 27 °nelac 11�;aceAnalytical' w»w.peceWbs.rom I Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA METHOD BLANK: 324276 Associated Lab Samples: Parameter Matrix: 9251168001, 9251168002, 9251168003 Blank Units Result Water Reporting Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 08120/0900:30 m8p-Xylene ug/L ND 2.0 08/20/09 00:30 Methyl -tent -butyl ether ug/L ND 1.0 08/20/09 00:30 Methylene Chloride ug/L ND 2.0 08/20/09 00:30 Naphthalene ug/L NO 1.0 08/20/09 00:30 o-Xylene ug/L NO 1.0 08/20/09 00:30 p-Isopropyltoluene ug/L NO 1.0 08/20/09 00:30 Styrene ug/L NO 1.0 08/20/09 00:30 Tetrachloroethene ug/L NO 1.0 08/20/09 00:30 Toluene ug/L NO 1.0 08/20/09 00:30 trans-1,2-Dichloroethene ug/L - NO 1.0 08/2010900:30 trans-1,3-Dichloropropene ug/L ND 1.0 0812010900:30 Trichlorcethene ug/L NO 1.0 08/20/09 00:30 Trichlorofluoromethane ug/L ND 1.0 08/2010900:30 Vinyl acetate ug/L NO 2.0 08/2010900:30 Vinyl chloride ug/L ND 1.0 08/20/09 00:30 1,2-Dichloroethane-d4 (S) % 108 79-120 08/20/09 00:30 4-Bromofluorobenzene (S) % 98 87-109 08/20/09 00:30 Dibromolluoromelhane (S) % 98 85-115 08/20/09 00:30 Toluene-d8 (S) % 100 70-120 08/20/09 00:30 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 324277 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.9 110 83-125 1, 1, 1-Trichloroethane ug/L 50 53.6 107 80-129 1,1,2,2-Tetrachloroethane ug/L 50 50.3 101 73-127 1, 1, 2-Trichloroetha ne ug/L 50 53.1 106 77-123 1,1-Dichloroethane ug/L 50 52.9 106 76-129 1,1-Dichloroethene ug/L 50 54.7 109 78-146 1,1-Dichloropropene u9/L 50 55.5 111 79-134 1,2,3-Trichlorobenzene ug/L 50 53.5 107 70-150 1,2,3-Trichloropropane ug/L 50 52.4 105 72-125 1,2,4-Trichlorobenzene ug/L 50 54.1 108 68-127 1,2-Dibromo-3-chloropropane ug/L 50 56.0 112 65-128 1,2-Dibromoethane (EDB) ug/L 50 53.5 107 81-125 1,2-Dichlorobenzene ug/L 50 50.4 101 82-126 1,2-Dichloroethane ug/L 50 54.8 110 72-126 1,2-Dichloropropane ug/L 50 54.4 109 80-127 1,3-Dichlorobenzene ug/L 50 50.8 102 82-124 1,3-Dichloropropane ug/L 50 52.3 105 79-124 1,4-Dichlorobenzene ug/L 50 50.6 101 79-125 2,2-Dichloropropane ug/L 50 41.4 83 58-140 2-Bulanone(MEK) ug/L 100 112 112 50-134 2-Chlorololuene ug/L 50 51A 103 81-126 Dale: 08126/200909:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `neh Page 15 of 27 m Pace Analytical Services, Inc. Analytical 2225 Riverside Dr. x nvpacekbscan Asheville, NC 28804 I (828)254-7176 QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 LABORATORY CONTROL SAMPLE: 324277 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits 2-Hexanone ug/L 100 107 107 58-138 4-Chlorotoluene ug/L 50 53.7 107 82-126 4-Methyl-2-penlanone (MIBK) ug/L 100 109 109 70-131 Acetone ug/L 100 128 128 50-146 Benzene ug/L 50 51.1 102 78-128 Bromobenzene ug/L 50 53.3 107 81-127 Bromochloromethane ug/L 50 51.2 102 73-124 Bromodichloromethane ug/L 50 52.4 105 81-125 Bromoform ug/L 50 45.9 92 71-125 Bromomethane ug/L 50 61A 122 50-150 Carbon tetrachloride ug/L 50 57.4 115 81-137 Chlorobenzene ug/L 50 50.2 100 82-126 Chloroethane ug/L 50 44.0 88 69-140 Chloroform ug/L 50 51.2 102 77-129 Chloromethane ug/L 50 42.6 85 54-139 cis-1,2-Dichloroelhene ug/L 50 53.8 108 76-133 cis-1,3-Dichloropropene ug/L 50 55.9 112 76-127 Dibromochloromethane ug/L 50 51.0 102 77-125 Dibromomethane ug/L 50 52.6 105 77-125 Dichlorodifiuoromethane ug/L 50 41.9 84 50-150 Dusopropyl ether ug/L 50 50.7 101 74-131 Ethylbenzene ug/L 50 52.0 104 80-127 Hexachloro-1,3-butadiene ug/L 50 51.9 104 78-145 m&p-Xylene ug/L 100 108 108 82-127 Methyl-tert-butyl ether ug/L 50 52.9 106 71-130 Methylene Chloride ug/L 50 49.2 98 67-133 Naphthalene ug/L 50 51.6 103 52-136 o-Xylene ug/L 50 55.7 111 83-124 p-Isopropyltoluene ug/L 50 56.4 113 73-122 Styrene ug/L 50 48.1 96 80-130 Tetrachlomethene ug/L 50 48.3 97 78-128 Toluene ug/L 50 51.4 103 76-126 trans-1,2-Dichloroelhene ug/L 50 50.9 102 78-134 trans-1,3-Dichloropropene ug/L 50 50.0 100 75-125 Trichloroethene ug/L 50 54.9 110 79-127 Trichlorofluoromethane ug/L 50 50A 101 76-148 Vinyl acetate ug/L 100 65.2 65 50-150 Vinyl chloride ug/L 50 52.7 105 67-143 1,2-Dichloroethane-d4 (S) % 101 79-120 4-BromoBuorobenzene(S) % 99 87-109 Dibromo0uoromethane (S) % 101 85-115 Toluene-d8(S) % 99 70-120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS Page 16 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac`' ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. 'aceft lI / ical 2225 Riverside Dc 9800 Kincey Ave. Suite 100 e pacelabs.mn Asheville, NC 28804 Huntersville, NC 28078 QUALITY CONTROL DATA (828)254-7176 (704)875-9092 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 324749 324750 MS MSD 9251168001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L NO 50 50 65.8 67.7 132 135 60-150 3 30 Benzene ug/L NO 50 50 57.5 59.2 115 118 74-136 3 30 Chlorobenzene ug/L ND 50 50 56.6 58.8 113 118 79-135 4 30 Toluene ug/L 1.0 50 50 59.5 61.7 117 121 73-131 4 30 Trichloroethene ug/L NO 50 50 60.3 61.2 121 122 73-131 1 30 1,2-Dichloroethane-d4 (S) % 106 107 79-120 4-BromoBuorobenzene (S) % 95 97 87-109 Dibromofluoromethane (S) % 97 97 85-115 Toluene-d8(S) % 100 100 70-120 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. vela& Page 17 of 27 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wuwpacebbscom Asheville, NC 28804 Huntersville, NC 28078 j (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 QC Batch: MERP/2330 Analysis Method: EPA 7470 OC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 9251168001, 9251168002. 9251168003 METHOD BLANK: 325438 Matrix: Water Associated Lab Samples: 9251168001, 9251168002, 9251168003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 0812410912:10 LABORATORY CONTROL SAMPLE: 325439 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.8 112 80-120 MATRIX SPIKE SAMPLE: 325440 9251013001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury ug/L NO 2.5 2.4 95 75-125 SAMPLE DUPLICATE: 325441 9251168001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Mercury ug/L ND ND 25 Dale: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the mllen consent of Pace Analytical Services, Inc.. nelac"r. Page 18 of 27 ZaceAnalytical ivimpacebbs." i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Balch: MPRP14941 Analysis Method: EPA 6010 QC Balch Method: EPA3010 Analysis Description: 6010 MET Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 325426 Associated Lab Samples: Parameter Matrix: 9251168001, 9251168002, 9251168003 Blank Units Result Water Reporting Limit Analyzed Antimony ug/L ND 5.0 08/2410917:21 Arsenic ug/L NO 5.0 08/2410917:21 Beryllium ug/L NO 1.0 08/2410917:21 Cadmium ug/L NO 1.0 08/24/0917:21 Chromium ug/L NO 5.0 08/2410917:21 Copper ug/L NO 5.0 08/24/0917:21 Iron uglL NO 50.0 08/2410917:21 Lead ug/L NO 5.0 08/24/0917:21 Nickel ug/L ND 5.0 08124/0917:21 Selenium ug/L ND 10.0 08124/0917:21 Silver ug/L ND 5.0 08124/0917:21 Thallium ug/L ND 10.0 08/24/0917:21 Zinc ug/L ND 10.0 0812410917:21 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 325427 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 499 100 80-120 Arsenic ug/L 500 487 97 80-120 Beryllium ug/L 500 507 101 80-120 Cadmium ug/L 500 481 96 80-120 Chromium ug/L 500 499 100 80-120 Copper ug/L 500 515 103 80-120 Iron ug/L 5000 5030 101 80-120 Lead ug/L 500 493 99 80-120 Nickel ug/L 500 495 99 80-120 Selenium ug/L 500 489 98 80-120 Silver uglL 250 253 101 80-120 Thallium ug/L 500 473 95 80-120 Zinc ug/L 500 487 97 80-120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers MATRIX SPIKE SAMPLE: 325428 9251051001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Antimony ug/L ND 500 541 108 75-125 Arsenic ug/L ND 500 567 112 75-125 Beryllium ug/L ND 500 502 100 75-125 Cadmium ug/L ND 500 482 96 75-125 Chromium ug/L 7.5 500 506 100 75-125 Copper ug/L ND 500 525 105 75-125 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS Page 19 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc nelac ace Analytical® al' bs.ccn 1 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr.. ;;',. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE SAMPLE: 325428 9251051001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Iron ug/L 276 5000 5090 96 75-125 Lead ug/L NO 500 457 91 75-125 Nickel ug/L 29.3 500 502 95 75-125 Selenium uglL ND 500 553 110 75-125 Silver ug/L ND 250 277 111 75-125 Thallium ug/L ND 500 409 82 75-125 Zinc ug/L 176 500 719 109 75-125 SAMPLE DUPLICATE: 325429 Parameter Units 9251168001 Result Dup Result Antimony ug/L ND NO Arsenic ug/L ND ND Beryllium ug/L ND NO Cadmium ug/L ND ND Chromium ug/L NO 1 7J Copper ug/L NO .77J Iron ug/L 43400 45300 Lead _ ug/L NO ND Nickel ug/L 22.0 23.0 Selenium uglL NO ND Silver ug/L NO .42J Thallium ug/L NO NO Zinc ug/L 106 110 Dale: 08/26/2009 09:35 AM RPD REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full, without the written consent of Pace Analytical Services, Inc.. nelac` Max RPD 20 20 20 20 20 20 4 20 _ 20 4 20 20 20 20 4 20 Qualifiers Page 20 of 27 / ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 vmwpacelaes.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 I QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 QC Batch: WETA/5727 Analysis Method: SM 4500-CI-E QC Balch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 326598 Matrix: Water Associated Lab Samples: 9251168001, 9251168002, 9251168003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 5.0 0812410915:44 LABORATORY CONTROL SAMPLE: 326599 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 21.1 105 90-110 MATRIX SPIKE SAMPLE: 326600 9250855001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloride mg/L 33.3 20 52.1 94 75-125 MATRIX SPIKE SAMPLE: 326603 9250753007 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloride mg/L 8.2 20 28.2 100 75-125 SAMPLE DUPLICATE: 326602 9251168001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chloride mg/L 10.5 10.5 0 20 SAMPLE DUPLICATE: 326604 9250753008 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chloride mg/L ND NO 20 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 'vela&. Page 21 of 27 ZeAnalyfkal' wawpecelabs.carn 1 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 QC Batch: WET/9480 Analysis Method: SM 2540C QC Batch Method: SM 2540C Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 326010 Matrix: Water Associated Lab Samples: 9251168001, 9251168002, 9251168003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L NO 20.0 08/21/09 20:55 LABORATORY CONTROL SAMPLE: 326011 Parameter Units Total Dissolved Solids mg/L Spike LCS LCS % Rec Cone. Result % Rec Limits 250 246 98 80-120 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers SAMPLE DUPLICATE: 326012 9251085006 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids mg/1- 2970 2980 0 20 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. , nelac Page 22 of 27 2ceAnalytical' wew.pscelses.com i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: OEXT/7743 Analysis Method: EPA 8270 QC Batch Method: EPA 3535 Analysis Description: 8270 Water PAH MSSV Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 324014 Associated Lab Samples: Parameter Matrix: 9251168001, 9251168002, 9251168003 Blank Units Result Water Reporting Limit Analyzed 1-Methylnaphthalene ug/L NO 10.0 08/2110913:24 2-Methylnaphthalene ug/L ND 10.0 08/21/09 13:24 Acenaphthene ug/L ND 10.0 08121/0913:24 Acenaphthylene ug/L ND 10.0 0812110913:24 Anthracene ug/L ND 10.0 08/2110913:24 Benzo(a)anthracene ug1L ND 10.0 08/21/09 13:24 Benzo(a)pyrene ug/L ND 10.0 08/21/09 13:24 Benzo(b)Suoranthene ug/L ND 10.0 0812110913:24 Benzo(g,h,i)perylene ug/L NO 10.0 08/2110913:24 Benzo(k)fiuoranthene ug/L NO 10.0 08121/0913:24 Chrysene ug/L NO 10.0 08121/0913:24 Dibenz(a,h)anthracene ug/L NO 10.0 08/21/09 13:24 Fluoranthene ug/L NO 10.0 08/2110913:24 Fluorene ug/L NO 10.0 08/2110913:24 Indeno(1,2,3-ed)pyrene ug/L ND 10.0 08/21/09 13:24 Naphthalene ug/L ND 10.0 08/2110913:24 Phenanthrene ug/L NO 10.0 08/2110913:24 Pyrene ug/L ND 10.0 08/2110913:24 2-Fluorobiphenyl (S) % 40 10-120 08/21/09 13:24 Nitrobenzene-d5 (S) % 31 10-120 08/21/09 13:24 Terphenyl-dl4(S) % 46 10-116 08121/0913:24 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 324015 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1-Methylnaphthalene ug/L 50 21.6 43 29-108 2-Methylnaphthalene ug/L 50 19.0 38 30-104 Acenaphthene ug/L 50 23.8 48 39-109 Acenaphthylene ug/L 50 23.9 48 41-109 Anthracene ug/L 50 25.6 51 45-114 Benzo(a)anthracene ug/L 50 23.6 47 45-109 Benzo(a)pyrene ug/L 50 23.9 48 47-117 Benzo(b)nuoranthene ug/L 50 22.7 45 32-113 Benzo(g,h,i)perylene ug/L 50 34.9 70 10-149 Benzo(k)fluoranlhene ug/L 50 20.4 41 41-104 Chrysene ug/L 50 25.2 50 35-116 Dibenz(a,h)anthracene ug/L 50 30.3 61 13-139 Fluoranthene ug/L 50 22.8 46 43-110 Fluorene ug/L 50 23.1 46 40-111 Indeno(1,2,3-cd)pyrene ug/L 50 31.3 63 17-135 Naphthalene ug/L 50 19.4 39 26-120 Date: 08/261200909:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, withoul the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 23 of 27 nelac 0 2ceAnajfj6cal wmxpac0abscan Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntenwille, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 324015 Spike LCS LCS %Rec Parameter Units Cone. Result %Rec Limits Qualifiers Phenanthrene ug/L 50 27.3 55 45-110 Pyrene ug/L 50 26.2 52 38-114 2-Fluorobiphenyl (S) % 45 10-120 Nitrobenzene-d5 (S) % 34 10-120 Terphenyl-d14(S) % 50 10-116 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 324016 9250891011 Parameter Units Result MS Spike Conc. MSD Spike Cone. 324017 MS Result MSD Result MS % Rec MSD % Rec %Rec Limits Max RPD RPD Qual 1-Methylnaphthalene ug/L ND 125 125 49.5 52.6 40 42 29-108 6 30 2-Methylnaphthalene ug/L ND 125 125 44.2 46.3 35 37 30-104 5 30 Acenaphthene ug/L ND 125 125 54.5 74.1 44 59 17-104 31 30 R1 Acenaphthylene ug/L NO 125 125 55.6 61.9 44 50 10-200 11 30 Anthracene ug/L NO 125 125 59.6 75.1 48 60 10-150 23 30 Benzo(a)anthracene ug/L NO 125 125 59.9 75.2 48 60 10-172 23 30 Benzo(a)pyrene ug/L NO 125 125 67.7 84.3 54 67 10-173 22 30 Benzo(b)Fluoranthene ug/L ND 125 125 79.0 95.7 63 77 10-200 19 30 Benzo(g,h,i)perylene ug/L ND 125 125 60.4 72.0 48 58 10-120 17 30- Benzo(k)fluoranthene ug/L NO 125 125 80.7 97.7 65 78 10-145 19 30 Chrysene ug/L ND 125 125 62.6 79.6 50 64 10-146 24 30 Dibenz(a,h)anthracene ug/L NO 125 125 57.6 75.0 46 60 10-120 26 30 Fluoranthene ug/L ND 125 125 58.4 74.6 47 60 20-120 24 30 Fluorene ug/L NO 125 125 60.3 74.6 48 60 10-109 21 30 Indeno(1,2,3-cd)pyrene ug/L ND 125 125 55.2 64.9 44 52 11-120 16 30 Naphthalene ug/L ND 125 125 46.5 45.5 37 36 10-120 2 30 Phenanthrene ug/L ND 125 125 63.3 80.5 51 64 10-145 24 30 Pyrene ug/L NO 125 125 68.8 89.8 55 72 13-114 26 30 2-Fluorobiphenyl (S) % 43 54 10-120 Nitrobenzene-d5 (S) % 37 46 10-120 Terphenyl-d14(S) % 50 61 10-116 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac'~. Page 24 of 27 �Jceftlyfical' w»wPecelaAs.rom i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. - 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA QC Balch: WETA/5714 Analysis Method: ASTM D516-90 OC Balch Method: ASTM D516-90 Analysis Description: ASTM D516-90 Sulfate Water Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 325724 Matrix: Water Associated Lab Samples: 9251168001, 9251168002, 9251168003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L NO 5.0 08/21/0913:58 LABORATORY CONTROL SAMPLE: 325725 Spike LCS LCS % Rec Parameter Units Conc. Result %Rec Limits Qualifiers Sulfate mg/L 20 19.1 95 90-110 MATRIX SPIKE SAMPLE: 325726 9250925001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg/L 9.9 20 25.0 76 75-125 MATRIX SPIKE SAMPLE: 325732 9251168001 Spike MS MS %Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg/L ND 20 23.1 97 75-125 SAMPLE DUPLICATE: 325731 9250925002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Sulfate mg/L ND ND 20 SAMPLE DUPLICATE: 325733 9251168002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Sulfate mg/L 21.9 22.6 3 20 �FICa[Q38ifl3tZtFDIr%4bY:lu.' REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `nelac" Page 25 of 27 IceAnalytical' wswPWebb&com i Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETA/5694 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 9251168001, 9251168002, 9251168003 METHOD BLANK: 324045 Matrix: Water Associated Lab Samples: 9251168001, 9251168002, 9251168003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L NO 0.10 08/19/09 10:08 Nitrogen, Nitrite mg/L NO 0A0 08/19/09 10:08 Nitrogen, NO2 plus NO3 mg/L NO 0.10 08/19/09 10:08 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntenwille, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 324046 Spike LCS LCS %Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.2 105 90-110 Nitrogen, Nitrite mg/L 1 1.0 105 90-110 Nitrogen, NO2 plus NO3 mg/L 5 5.2 105 90-110 MATRIX SPIKE SAMPLE: 324047 9251168001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Nitrogen, Nitrate mg/L NO 5 4.3 86 90-110 Nitrogen, Nitrite mg/L NO 1 0.93 93 90-110 Nitrogen, NO2 plus NO3 mg/L NO 5 4.3 86 90-110 SAMPLE DUPLICATE: 324048 9251168002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Nitrogen, Nitrate mg/L NO NO 20 Nitrogen, Nitrite mg/L NO NO 20 Nitrogen, NO2 plus NO3 mg/L NO NO 20 Date: 08/26/2009 09:35 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac~ Page 26 of 27 aceAnalytical' wmvpacela6s.cwn 1 Project: OMNI SUPPLY 13140-007-0001 Pace Project No.: 9251168 DEFINITIONS Pace Analytical Services, Inc. _. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyle) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES PAST -A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS R1 RPD value was outside control limits. Dale: 08/26/2009 09:35AM REPORT OF LABORATORY ANALYSIS Page 27 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nelac G a J le peNl saldweg Lr) 3 _ z :.O Z_ O Z O F Y^ ! Y W t T m O �--� a ~O �/�) U Z ialoop paleag Rpolsn0 (NIA) --I 1 uo p ,w.a w (N/A) auuoly0 lenpisaa O 3 0 Z 7 0. ui dwal i Z K qn J\ o= Q O F V F m < O O Jp a'•'//• V• J D LL g Z O N a T�bJ m w 2 otxn 9 f F IN/A tisal SIS6leuvt 'm 0 L E loueylayl m %VeN i) ll3 < 2 HORN y IOH E a a %NH Ol "OS-H � (� paNaSaJdUn " - m E b " S — �Y S83NItl1N00 d0 # W N0110311001V dW313ldWVS w O a a /u0� O m \e N N s s 0 _h o Q E W a w a N-- t .1 t2 O w w F U ¢? z m z u < J O LYZ CJ > 1 u~ > _ 3 (� s i V � (dW00=9 9tltl0=0) 3dA13ldWtlS i g GT7 W aal o� saeo" peep aesl 3000 xlaltlW m a E E m " -- o33amo3 ago aa° a ci a' a c m-uo,�° 4 o33a9i 03 a F0 r z y ` §( ' w � O w F U ? LU $C a E JmN 1 1 O L E IL i p E O _a �o o� CO d G c o E o 'a #W311 a u A ¢ u S' g�>-.^-S3eif.! `r I.I.i. . I r . i•'1' I •11 - e3- . S= a ',.rdceClient Name: 4 _um Project# Ccu-er: L' Fed E< D UPS [ USFS ❑ C:ert [ Cnr .e;-; Fz;:= 02+_.- Custody Seal on Cooler!2ex Pres-rt. ❑yes r I nv Seals I:, _-!: [ y=s rc Pr I ❑ Bu.,ol2 I �,. [ubhL Packing(Material: `-' Y;,ap gags ❑ None I_IOther t Th erm omeier Used T'50 - Type of Ice: Blue Mona JQ-Samc:es on is-, ro3ng p:_cess has begun Cooler Tamcerature - _I r L Slcioei_al Tissue is Frozen: Yes NO NIA Dac=_ and inir, o{pe ��eamining ^ Uc • ccntam•-:_ OJ Ter_ shoulc to atove freezing to 5'C Comments: Chain Or Custody Present: Fd�es ONO 0N/A Chain of Custody Filled Out Ehes ❑Noy ❑N/A 2 Chain of Custody Relinquished. - LWeS ONO ❑N/A 3. Sampler Name & Signature on COC: (H'es ON62 -ON/A 4_ Samples Arrived within Hold Time. ifYes ONO. ON/A 5. - Short Hold Time Analysis (<72hr): pans ONO '' ON/A 6, Rush Turn Around Time Requested: Oyes ago ❑N/A 7, �. Sufficient Volume: ,9Yes ONO ON/A g_ Correct Containers Used: - (,yes ONO ON/A g. -Pace Containers Used: ,fC7Yes ONO ❑N/A - �ontamers Intact es (-)No- - ❑N/A 10.. -dlered volume received for Dissolved tests OYes ON. `-[�K/A 11. >ample Labels match COC: V'Yes ONO ❑NIA 12, -Includes dale/lime/ID/Analysis Matrix `-'T _ di -container, needing preservation have been checked. C;i'As ONO, ON/A 13. ,II conlamers needing preservation are found to be m p'(es O ONO [)N/A omphance with EPA recommendation. xcepliom: VOA. colilorm, TOC. O&G. Wh DRO (water) Oyes ONO Initial when completed iampies checked for dechlormation. -B4es ONO ❑N/A 14. ieadspace in VOA Vials (>6mm): OYes PRo ON/A 15. 'rip Blank Present: ❑Yes ONO 'Brv/A 16. Yip Blank Custody Seals Present Ores ONO 4RNIA 'ace Trio Blank Lot M (it purchased): N/A :lient Notification/ Resolution: Person Contacted. Comments/ Resolution: Date(Time: Field Data Required? Y / N / NIA Project Manager Review: L_9�w Date: RIWO9