NC0006254_Groundwater Monitoring Report July 2020_20200722

PO Box 604 ▪ Fletcher, NC 28732 ▪ PH: 828-667-5001 ▪ Cell: 828-508-4510

July 22, 2020
Mr. Brett Laverty
NCDEQ Division of Water Resources
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

RE: Groundwater Analytical Results – July 2020
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina

Mr. Laverty:

On July 7, 2020, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site located at
1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples from
monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7 and MW-8. The depth to
groundwater in the monitoring wells ranged from 5.28 feet in MW-4 to 49.09 feet in MW-2.
Refer to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well
locations.

All groundwater samples, with the exception of MW-2, were collected using a peristaltic pump
connected to a Horiba U52-2 water quality meter with a flow through cell to collect groundwater
parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP, and turbidity).
Groundwater sample MW-2 was collected using a bailer once three well volumes were removed.
Groundwater from the same bail as the sample was also poured into the flow cell to collect the
approximate parameters. The groundwater samples were submitted on ice to Pace Analytical for
the analysis of barium, iron, manganese, ammonia, TKN, nitrogen, nitrite and nitrate. MW-2 was
also analyzed for total dissolved solids (TDS) using EPA Method SM 2540C. The groundwater
parameters for all samples are outlined in Table 2.

The laboratory analysis of groundwater samples MW-1 detected levels of iron and manganese
above the NCAC 2L groundwater standards. The laboratory analysis of MW-2 detected levels of
arsenic, barium, iron, manganese and ammonia above the NCAC 2L groundwater standards. The
laboratory analysis of groundwater samples MW-3 detected levels of iron, manganese and
ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater
samples MW-4 detected levels of iron and manganese above the NCAC 2L groundwater
standards. Laboratory analysis of groundwater samples MW-6, MW-7 and MW-8 did not detect
any compounds exceeding the NCAC 2L groundwater standards. The analytical results are shown
on attached Table 2 and the attached laboratory data sheets.

During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the
groundwater in monitoring well MW-4. During the July 2020 event a sheen was not observed;
therefore, a volatile organic compound (VOC) analysis was not performed on the sample.
Singleton Environmental, Inc.
Singleton Environmental, Inc.

The compound levels detected in the groundwater analysis for the July 2020 sampling event were
comparable to the March 2020 event. Singleton Environmental, Inc. recommends sampling the
monitoring wells again in October 2020.

If you have any questions you can reach me at [phone].

Sincerely,

Chris Singleton, P.G.
Singleton Environmental, Inc.

cc: Dave Hallock, Blue Ridge Tissue Corporation

Attachments
@A
@A @A
@A
@A
@A
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MW-2
MW-3
MW-4
MW-1
@A
MW-5
MW-7
MW-6
MW-8
1
2
8
0
12601
3
2
0
1340
1360
1380
124014201240
1420
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community
Figure
60540673
1
May 2017
§
0 200 400Feet
1 inch = 200 feet
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R
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R
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Whisnant RdYad
k
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R
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Yadkin
R
iver
Roby Martin Rd#0
Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina
Legend
Property Boundary
Yadkin River Flow Direction
#Land Surface Elevation Contour (ft above mean sea level)
Monitoring Well Location
Abandoned Water Well#0@A
Well ID Date Installed Total Depth (feet
bls)
Screened Interval
(feet bls)
Top of Casing
Elevation (feet msl)
Date Water Level
Measured
Depth to Water (feet
BTOC)
Groundwater Elevation
(feet msl)
MW-1 02/08/11 11 6-11 1253.71 07/14/20 11.82 1,241.89
MW-2 08/12/09 50 40-50 1323.03 07/14/20 49.09 1,273.94
MW-3 08/13/09 20 10-20 1299.02 07/14/20 16.18 1,282.84
MW-4 08/13/09 15 5-15 1247.23 07/14/20 5.28 1,241.95
MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A
MW-6 08/06/14 29 19-29 1341.55 07/14/20 26.67 1,314.88
MW-7 08/06/14 24 14-24 1274.41 07/14/20 17.98 1,256.43
MW-8 08/06/14 20 10-20 1253.14 07/14/20 14.05 1,239.09
Notes:
bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged
AECOM
Table 1
Monitoring Well Construction and Groundwater Elevations
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina
Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8
Sample Date 07/14/20 07/14/20 07/14/20 07/14/20 07/14/20 07/14/20 07/14/20
Temperature (°C)NS 18.79 N/A 20.18 19.30 20.99 16.77 17.95
pH (standard units)NS 5.82 N/A 6.37 6.40 5.76 6.28 6.05
Specific Conductivity (mS/cm)NS 0.42 N/A 0.52 0.262 0.027 0.105 0.131
Dissolved Oxygen (mg/L)NS 0.88 N/A 1.04 3.34 7.06 5.70 9.12
ORP (mV)NS 22.0 N/A 5.0 6.0 64.0 66.0 60.0
Turbidity (NTU)NS 5.9 N/A 10.1 2.8 1.8 7.6 4.2
Total Barium (ug/L)700 203 1,530 211 90 91.6 53 15.9
Total Iron (ug/L)300 28,100 68,900 26,200 14,800 61.9 ND ND
Total Manganese (ug/L)50 4,500 1,090 2,660 1,000 23.8 ND ND
Aresenic (ug/L)10 ND 12.8 ND ND ND ND ND
Chromium (ug/L)10 ND 6.1 ND ND ND ND ND
Lead (ug/L)15 ND ND ND ND ND ND ND
Amonia (mg/L)1.5 0.59 15.5 15.1 1 ND ND ND
TKN (mg/L)N/A 0.8 14.2 12.2 ND ND ND ND
Nitrogen NO2 plus NO3 (mg/L)N/A ND ND 0.18 ND ND 1.1 4.2
Nitrate (mg/L)10.0 ND ND 0.13 ND ND 1.1 4.2
Nitrite (mg/L)1.0 ND 0.05 0.044 ND ND ND ND
Total Disolved Solids (mg/L)N/A N/A 344 N/A N/A N/A N/A N/A
Notes:
Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7
2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20
°C - degrees Celsius
µS/cm - microsiemens per centimeter
EPA - United States Environmental Protection Agency mg/L - milligrams per liter
mV - millivolt
NA - Not analyzed NS - No standard
NTU - Nephelometric Turbidity Unit
RCRA - Resource Conservation Recovery Act
Bold samples indicate concentrations above the 2L Standard
*MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample.
2L
Standard
Field Parameters
Analytical Parameters
Table 2
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina
#=CL#
August 10, 2020
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92485972
92485972
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
P.O. Box 2012
Enka, NC 28728
BLUE RIDGE TISSUE 7-14-2020
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on July 14, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
Revised Report: Report revised to add additional elements - As,Cr, Pb
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen for
[e-mail]
Project Manager
Lorri Patton
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92485972001 MW-1 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
92485972002 MW-2 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 2540C-2011 1 PASI-AJNS
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
92485972003 MW-3 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
92485972004 MW-4 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
92485972005 MW-6 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
92485972006 MW-7 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
92485972007 MW-8 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ADMN
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-1 Lab ID:92485972001 Collected:07/14/20 10:00 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 07/17/20 00:06 7440-38-2 BC07/16/20 10:1910.0 1
Barium 203 ug/L 07/17/20 00:06 7440-39-307/16/20 10:195.0 1
Chromium ND ug/L 07/17/20 00:06 7440-47-307/16/20 10:195.0 1
Iron 28100 ug/L 07/17/20 00:06 7439-89-607/16/20 10:1950.0 1
Lead ND ug/L 07/17/20 00:06 7439-92-107/16/20 10:195.0 1
Manganese 4500 ug/L 07/17/20 00:06 7439-96-507/16/20 10:195.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.59 mg/L 07/17/20 10:13 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 0.80 mg/L 07/21/20 06:21 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 07/15/20 11:02 M10.040 1
Nitrogen, Nitrate ND mg/L 07/15/20 11:02 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 07/15/20 11:02 14797-65-0 M10.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2020 09:20 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-2 Lab ID:92485972002 Collected:07/14/20 10:30 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic 12.8 ug/L 07/17/20 00:09 7440-38-2 BC07/16/20 10:1910.0 1
Barium 1530 ug/L 07/17/20 00:09 7440-39-307/16/20 10:195.0 1
Chromium 6.1 ug/L 07/17/20 00:09 7440-47-307/16/20 10:195.0 1
Iron 68900 ug/L 07/17/20 00:09 7439-89-607/16/20 10:1950.0 1
Lead ND ug/L 07/17/20 00:09 7439-92-107/16/20 10:195.0 1
Manganese 1090 ug/L 07/17/20 00:09 7439-96-507/16/20 10:195.0 1
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 344 mg/L 07/18/20 17:1325.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 15.5 mg/L 07/17/20 10:15 7664-41-70.30 3
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 14.2 mg/L 07/21/20 06:22 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 07/15/20 11:130.040 1
Nitrogen, Nitrate ND mg/L 07/15/20 11:13 14797-55-80.040 1
Nitrogen, Nitrite 0.050 mg/L 07/15/20 11:13 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2020 09:20 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-3 Lab ID:92485972003 Collected:07/14/20 10:45 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 07/17/20 20:59 7440-38-207/17/20 01:4710.0 1
Barium 211 ug/L 07/17/20 20:59 7440-39-307/17/20 01:475.0 1
Chromium ND ug/L 07/17/20 20:59 7440-47-307/17/20 01:475.0 1
Iron 26200 ug/L 07/17/20 20:59 7439-89-607/17/20 01:4750.0 1
Lead ND ug/L 07/17/20 20:59 7439-92-107/17/20 01:475.0 1
Manganese 2660 ug/L 07/17/20 20:59 7439-96-507/17/20 01:475.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 15.1 mg/L 07/17/20 10:16 7664-41-70.30 3
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 12.2 mg/L 07/21/20 06:23 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.18 mg/L 07/15/20 11:140.040 1
Nitrogen, Nitrate 0.13 mg/L 07/15/20 11:14 14797-55-80.040 1
Nitrogen, Nitrite 0.044 mg/L 07/15/20 11:14 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2020 09:20 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-4 Lab ID:92485972004 Collected:07/14/20 13:00 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 07/17/20 21:09 7440-38-207/17/20 01:4710.0 1
Barium 90.1 ug/L 07/17/20 21:09 7440-39-307/17/20 01:475.0 1
Chromium ND ug/L 07/17/20 21:09 7440-47-307/17/20 01:475.0 1
Iron 14800 ug/L 07/17/20 21:09 7439-89-607/17/20 01:4750.0 1
Lead ND ug/L 07/17/20 21:09 7439-92-107/17/20 01:475.0 1
Manganese 1000 ug/L 07/17/20 21:09 7439-96-507/17/20 01:475.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 1.0 mg/L 07/17/20 10:17 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 1.1 mg/L 07/21/20 06:25 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.046 mg/L 07/15/20 11:190.040 1
Nitrogen, Nitrate 0.046 mg/L 07/15/20 11:19 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 07/15/20 11:19 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2020 09:20 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-6 Lab ID:92485972005 Collected:07/14/20 11:45 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 07/17/20 21:12 7440-38-207/17/20 01:4710.0 1
Barium 91.6 ug/L 07/17/20 21:12 7440-39-307/17/20 01:475.0 1
Chromium ND ug/L 07/17/20 21:12 7440-47-307/17/20 01:475.0 1
Iron 61.9 ug/L 07/17/20 21:12 7439-89-607/17/20 01:4750.0 1
Lead ND ug/L 07/17/20 21:12 7439-92-107/17/20 01:475.0 1
Manganese 23.8 ug/L 07/17/20 21:12 7439-96-507/17/20 01:475.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 07/17/20 10:19 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 07/21/20 06:28 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 07/15/20 11:160.040 1
Nitrogen, Nitrate ND mg/L 07/15/20 11:16 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 07/15/20 11:16 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2020 09:20 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-7 Lab ID:92485972006 Collected:07/14/20 12:30 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 07/17/20 21:15 7440-38-207/17/20 01:4710.0 1
Barium 53.0 ug/L 07/17/20 21:15 7440-39-307/17/20 01:475.0 1
Chromium ND ug/L 07/17/20 21:15 7440-47-307/17/20 01:475.0 1
Iron ND ug/L 07/17/20 21:15 7439-89-607/17/20 01:4750.0 1
Lead ND ug/L 07/17/20 21:15 7439-92-107/17/20 01:475.0 1
Manganese ND ug/L 07/17/20 21:15 7439-96-507/17/20 01:475.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 07/17/20 10:20 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 07/21/20 06:29 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 1.1 mg/L 07/15/20 11:170.040 1
Nitrogen, Nitrate 1.1 mg/L 07/15/20 11:17 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 07/15/20 11:17 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2020 09:20 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Sample:MW-8 Lab ID:92485972007 Collected:07/14/20 11:15 Received:07/14/20 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 07/17/20 21:19 7440-38-207/17/20 01:4710.0 1
Barium 15.9 ug/L 07/17/20 21:19 7440-39-307/17/20 01:475.0 1
Chromium ND ug/L 07/17/20 21:19 7440-47-307/17/20 01:475.0 1
Iron ND ug/L 07/17/20 21:19 7439-89-607/17/20 01:4750.0 1
Lead ND ug/L 07/17/20 21:19 7439-92-107/17/20 01:475.0 1
Manganese ND ug/L 07/17/20 21:19 7439-96-507/17/20 01:475.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 07/17/20 10:26 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 07/21/20 06:30 7727-37-907/21/20 00:290.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 4.2 mg/L 07/15/20 11:150.040 1
Nitrogen, Nitrate 4.2 mg/L 07/15/20 11:15 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 07/15/20 11:15 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
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Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
553603
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972001, 92485972002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2941561
Associated Lab Samples:92485972001, 92485972002
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 BC07/16/20 22:06
Barium ug/L ND 5.0 07/16/20 22:06
Chromium ug/L ND 5.0 07/16/20 22:06
Iron ug/L ND 50.0 07/16/20 22:06
Lead ug/L ND 5.0 07/16/20 22:06
Manganese ug/L ND 5.0 07/16/20 22:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2941562LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 510500 102 85-115
Barium ug/L 500500 100 85-115
Chromium ug/L 517500 103 85-115
Iron ug/L 51805000 104 85-115
Lead ug/L 514500 103 85-115
Manganese ug/L 516500 103 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2941563MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485579001
2941564
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 286 107 70-130101 5286ND306290
Barium ug/L 286 102 70-13096 528618.1 309 292
Chromium ug/L 286 105 70-13099 6286ND300283
Iron ug/L 2860 108 70-130102 52860ND31002940
Lead ug/L 286 102 70-13096 6286ND291274
Manganese ug/L 286 103 70-13097 628613.9 308 291
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2941565MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485855001
2941566
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 286 105 70-130104 0286ND303302
Barium ug/L 286 101 70-130101 028617.9 308 306
Chromium ug/L 286 106 70-130104 1286ND302298
Iron ug/L 2860 109 70-130109 02860160047304710
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2941565MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485855001
2941566
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 286 94 70-13093 1286ND269266
Manganese ug/L 286 101 70-130100 128622.4 312 309
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
553926
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972003, 92485972004, 92485972005, 92485972006, 92485972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2943151
Associated Lab Samples:92485972003, 92485972004, 92485972005, 92485972006, 92485972007
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 07/17/20 20:40
Barium ug/L ND 5.0 07/19/20 11:56
Chromium ug/L ND 5.0 07/17/20 20:40
Iron ug/L ND 50.0 07/17/20 20:40
Lead ug/L ND 5.0 07/17/20 20:40
Manganese ug/L ND 5.0 07/17/20 20:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2943152LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 454500 91 85-115
Barium ug/L 476500 95 85-115
Chromium ug/L 491500 98 85-115
Iron ug/L 46905000 94 85-115
Lead ug/L 472500 94 85-115
Manganese ug/L 483500 97 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943153MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485972003
2943154
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 100 70-13098 2500ND506495
Barium ug/L 500 103 70-130103 0500211724724
Chromium ug/L 500 104 70-130103 1500ND519516
Iron ug/L 5000 104 70-130117 25000262003140032100
Lead ug/L 500 99 70-13099 1500ND497493
Manganese ug/L 500 104 70-130116 2500266031803240
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943155MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92486036001
2943156
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 102 70-130104 2500ND512522
Barium ug/L 500 102 70-130104 1500140649658
Chromium ug/L 500 102 70-130104 25000.018
mg/L
526 538
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943155MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92486036001
2943156
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Iron ug/L 5000 96 70-130100 35000280076107810
Lead ug/L 500 96 70-13098 25000.016
mg/L
494 506
Manganese ug/L 500 98 70-13099 250068.2 556 565
REPORT OF LABORATORY ANALYSIS
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Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
554228
SM 2540C-2011
SM 2540C-2011
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2944655
Associated Lab Samples:92485972002
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 07/18/20 17:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2944656LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 240250 96 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92485851015
2944657SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 3040 23090
Parameter Units
Dup
Result QualifiersRPDResult
92486358002
2944658SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 193 3187
REPORT OF LABORATORY ANALYSIS
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Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
553968
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972001, 92485972002, 92485972003, 92485972004, 92485972005, 92485972006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2943254
Associated Lab Samples:92485972001, 92485972002, 92485972003, 92485972004, 92485972005, 92485972006
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 07/17/20 09:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2943255LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.05 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485467001
2943257
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 105 90-110105 05ND5.3 5.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943258MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485467003
2943259
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 105 90-110105 05ND5.2 5.3
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
553969
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2943260
Associated Lab Samples:92485972007
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 07/17/20 10:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2943261LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.25 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943262MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485972007
2943263
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 104 90-110104 05ND5.2 5.2
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2943264MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92486036001
2943265
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 109 90-110110 058.3 13.8 13.8
REPORT OF LABORATORY ANALYSIS
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Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
554559
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972001, 92485972002, 92485972003, 92485972004, 92485972005, 92485972006, 92485972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2946047
Associated Lab Samples:92485972001, 92485972002, 92485972003, 92485972004, 92485972005, 92485972006, 92485972007
Matrix:Water
Analyzed
Nitrogen, Kjeldahl, Total mg/L ND 0.50 07/21/20 06:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2946048LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 9.910 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2946049MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485494001
2946050
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 97 90-11094 2100.91 10.6 10.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2946051MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485972004
2946052
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 96 90-11094 2101.1 10.7 10.5
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
553327
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92485972001, 92485972002, 92485972003, 92485972004, 92485972005, 92485972006, 92485972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2940072
Associated Lab Samples:92485972001, 92485972002, 92485972003, 92485972004, 92485972005, 92485972006, 92485972007
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.040 07/15/20 11:09
Nitrogen, Nitrite mg/L ND 0.040 07/15/20 11:09
Nitrogen, NO2 plus NO3 mg/L ND 0.040 07/15/20 11:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2940073LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.61.5 104 90-110
Nitrogen, Nitrite mg/L 1.01 100 90-110
Nitrogen, NO2 plus NO3 mg/L 2.62.5 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2940074MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92485972001
2940075
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 63 90-11063 01.5ND 0.94 0.94
Nitrogen, Nitrite mg/L M117390-11074 11ND0.76 0.77
Nitrogen, NO2 plus NO3 mg/L M12.5 67 90-11068 02.5ND 1.7 1.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2940076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92486098002
2940077
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 84 90-11086 21.5ND 1.3 1.3
Nitrogen, Nitrite mg/L 1 103 90-110104 210.066 1.1 1.1
Nitrogen, NO2 plus NO3 mg/L 2.5 93 90-11095 22.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.BC
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92485972
BLUE RIDGE TISSUE 7-14-2020
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92485972001 553603 553760MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972002 553603 553760MW-2 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972003 553926 553955MW-3 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972004 553926 553955MW-4 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972005 553926 553955MW-6 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972006 553926 553955MW-7 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972007 553926 553955MW-8 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92485972002 554228MW-2 SM 2540C-2011
92485972001 553968MW-1 EPA 350.1 Rev 2.0 1993
92485972002 553968MW-2 EPA 350.1 Rev 2.0 1993
92485972003 553968MW-3 EPA 350.1 Rev 2.0 1993
92485972004 553968MW-4 EPA 350.1 Rev 2.0 1993
92485972005 553968MW-6 EPA 350.1 Rev 2.0 1993
92485972006 553968MW-7 EPA 350.1 Rev 2.0 1993
92485972007 553969MW-8 EPA 350.1 Rev 2.0 1993
92485972001 554559 554589MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972002 554559 554589MW-2 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972003 554559 554589MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972004 554559 554589MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972005 554559 554589MW-6 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972006 554559 554589MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972007 554559 554589MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92485972001 553327MW-1 EPA 353.2 Rev 2.0 1993
92485972002 553327MW-2 EPA 353.2 Rev 2.0 1993
92485972003 553327MW-3 EPA 353.2 Rev 2.0 1993
92485972004 553327MW-4 EPA 353.2 Rev 2.0 1993
92485972005 553327MW-6 EPA 353.2 Rev 2.0 1993
92485972006 553327MW-7 EPA 353.2 Rev 2.0 1993
92485972007 553327MW-8 EPA 353.2 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
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Page 21 of 24
Page 22 of 24
Page 23 of 24
Page 24 of 24