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HomeMy WebLinkAboutNC0037508_NPDES Draft Permit_20041221Michael F. Easley, Governor State of North Carolina William G. Ross, Jr., Secretary Department of Environment and Natural Resources Alan W. Klimek, P.E., Director Division of Water Quality December 21, 2004 Mr. James Frye, System Superintendent Moore County Water Pollution Control Plant 1094 Addor Road Aberdeen, North Carolina 28315 DENR-FRO DEC 2 3 2004 DWQ Subject: Transmittal of NPDES Permit DRAFT Permit NC0037508 Moore County Water Pollution Control Plant Moore County Dear Mr. Frye: In response to Moore County's request to renew the NPDES permit for the subject site, the Division of Water Quality (the Division) hereby transmits this permit draft. Please review the attached draft for completeness and accuracy. Concurrent with this notification, the Division is publishing a notice in newspapers having circulation in the general Moore County area, soliciting public comment on this permit draft. Please provide any comments you may have regarding this draft to DENR — DWQ, NPDES Unit no later than 30 days after receiving this draft permit. Following the 30-day public comment period, the Division will review all pertinent comments and take appropriate action prior to issuing a final permit. If you have questions concerning the draft permit, you may e- mail joe.corporon@ncmail.net, or please call me at (919) 733-5083, extension 597. Revising Ammonia (NH3 as N) Limits. Ammonia Limits have been adjusted for toxicity considering IWC of 41%. The previous permit's Monthly Average (Summer) limit has been adjusted to 2.1 mg/L, and a limit of 6.2 mg/L Monthly Average (Winter) has been added to the permit. Per statewide policy, the Division has added ammonia Weekly Average limits to this permit. Because Moore County is a major municipal, Weekly Average limits are calculated as "Monthly Average values times three." This corresponds to a new Weekly Averages of 6.3 mg/L (summer), and 18.6 mg/L (Winter). Although new ammonia limits are notably more stringent, the Division reviewed the permittee's ammonia data and anticipates no future compliance problems with new permit limits. Data for the years 2003 and 2004 indicate average daily ammonia levels regularly reported below detection at 0.5 mg/L with a maximum reported as 0.8 mg/L. Concerning Mercury. As noted in previous letters to you (see correspondence dated August 30, 2002 and August 12, 2003), the Moore County and 155 other facilities in North Carolina are subject to EPA low-level mercury test Method 1631. Please be reminded that you must continue with this, low-level method and required clean sampling techniques. Mercury bioaccumulation in fish tissue from the Lumber River Basin has prompted fish consumption advisories and impaired waterbody designations. Therefore, a Phase II, Total Maximum Daily Load (TMDL) is currently in progress for the Lumber and Waccamaw watersheds. This Phase II program is scheduled for completion by Winter 2006. North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-5083 NCDENR Customer Service 1 800 623-7748 Moore County Moore County Water Pollution Control Plant NPDES Permit NC0037508 Page 2 Renewal Reasonable Potential Analysis. As part of this renewal, the Division conducted Reasonable Potential Analyses (RPA) on contaminants of concern. These include potential toxicants and metals considering Significant Industrial Users (SIUs), previous effluent monitoring, and this facility's Pretreatment Program. This RPA evaluates "reasonable potential" for parameters to exceed North Carolina's instream Water Quality Standards. Having concluded its review, the Division offers the following comments and changes to your previous permit (see table). Table. Permit Renewal -- Changes/Additions: Parameter'' Comments / Renewal Action Ammonia (NH3 as N) ' ... Revised Limits: adjusted Summer Monthly Ave. to 2.1 mg/L; Added Summer Weekly Ave. of 6.2 mg/L; added limits Winter Monthly Ave. 6.3 mg/L and Weekly Ave. 18.6 mg/L. TRC Added Total Residual Chlorine (TRC) Daily Max. limit of 28 µg/L. Copper Yes Action Level Standard, no TOX problem therefore no limits; add monitoring 2/Month Mercury — TMDL for the Lumber River Basin dictates Quarterly monitoring by EPA Method 1631 Silver, Yes Action Level Standard, no TOX problem therefore no limits; continue monitoring 2/Month Zinc . Yes Action Level Standard, no TOX problem therefore no limits; continue monitoring 2/Month *RP = "Reasonable Potential" to exceed instream Water Quality Standard. Finally, in keeping with a newly adopted statewide standard for Total Residual Chlorine (TRC), the Division has added a TRC limit to your permit of 28 µg/L. Res Je R. Corporo DES Unit Enclosure: Draft NPDES Permit NC0037508 cc: ji'ayetteualletRe—gtanal O,ffce; WaterQuali ection [NPDE 't and'FacfSheet]`� NPDES Unit [NPDES Permit and Fact Sheet] Aquatic Toxicology Unit [NPDES Permit and Fact Sheet] EPA Region 4 [NPDES Permit, Fact Sheet, Permit Application, 2°d Species TOX results, PPA 3 events] Permit NC0037508 STATE OF NORTH CAROLINA j DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY TO DISCHARGE WASTEWATER UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION' SYSTEM (NPDES) PERMIT In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North CJina Environmental Management Commission, and the Federal Water Pollution Grontrof Act, as amended, Moore County~1* r' 1 is hereby authorized to discharge wastewatertfrom an outfall locatedat the ‘�f, �> L Moore County Water:FPollutionControl Plant 094.,Addar Road <Moo eCou�nty�,. �s i O f/ L i to receiving waters desi atred:as Aberdeen,C er ekloaate•thin the Lumber River Basin in accordance with eff1 e ilimitati�rxs�, mor ito .rig requirements, and other cokiditions set forth in Parts I, II, III and IV hereof 1 \\ ' \\ This permit shall become efectiye 1 , 2005. This permit and authorization to discharge shall expire at midnight on July 31, 2009. Signed this day , 2005. Alan W. Klimek, PE, Director Division of Water Quality By Authority of the Environmental Management Commission Permit NC0037508 SUPPLEMENT TO PERMIT COVER SHEET All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby revoked, and as of this issuance, any previously issued permit bearing this number is no longer effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the permit conditions, requirements, terms, and provisions described herein. is hereby authorized: Moore County 1. to continue discharging 6.7 MGD of dome c' andundustrial wastewater from the existing wastewater treatment facility consisting/of activated sludge wastewater treatment facilities. The treatment system utlizes: • . . . . . . . . . pre -aeration grit removal primary clarification -----,. first -stage activated sludge intermediate clarification second -stage aeration final eiarification \/' anaerobic sludge digestion sludge\drying beds \ \ 't and post aeration '\ `\ located at the Moore County Water Pollution Control Plant, 1094 Addor Road, Moore County, and % I ' 2 to discharge from said treatment facility through Outfall 001 at a specified location (see attached map) into Aberdeen Creek, a waterbody classified as C waters within the Lumber River Basin. Moore County WWTP Receiving Stream: Aberdeen Creek Drainage Basin: Lumber River Latitude: 35° 04' 04" N Longitude: 78° 28' 07" W Sub -Basin: 03-07-50 Permitted Flow: 6.7 MGD State Grid / USGS Quad: G 2ISW / Pinebluff, N.C. Stream Class: C Moore County WWTP and Discharge Line (Approximate Location) Faci lity Loca Ltion 1. f not tb scale North NPDES Permit NC0037508 Moore County NPDES Permit No. NC0037508 A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge through Outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below: PARAMETERS ` • EFFLUENTLIMITS MONITORING REQUIREMENTS Monthly Average j ;Weekly Average ': Daily 'Maximum:-- Measurement Frequency Sample- TYPe..: *Sample Location- Flow (MGD) 6.7 Continuous Recording I or E BOD, 5 day, 20°C (April 1 — October 31) 2 22.0 mg/L 33.0 mg/L Daily Composite I, E BOD, 5 day, 20°C (Nov. 1 — March 31) 2 30.0 mg/L 45.0 mg/L Daily Composite I, E Total Suspended Solids (TSS) 2 30.0 mg/L 45.0 mg/L Daily Composite. I, E, NH3 as N (April 1 — October 31) 2.1 mg/L 6.3 mg/L ,/ `> - Daily Composite E NH3 as N (Nov. 1 — March 31) 6.2 mg/L 18.6 mg/L /`.. ;% - Daily Composite. E Fecal Coliform (geometric mean) 200 / 100 ml 400 / 10041 \ Daily Grab E Total Residual Chlorine (TRC) 3 ,/\\Z \2$ j g/L Daily Grab E Dissolved Oxygen 4 ,f ,; \ \ Daily Grab E Temperature (°C) S: ,/ \A, Daily Grab E Conductivity \ A \ Daily Grab E pH g 1N... A \ /` : \ Daily Grab E Total Phosphorus \ti \ ' _ \,! Monthly Composite E Total Nitrogen (NO2-N + NO3-N + TKN) `� \ ,`e, \ \ Monthly Composite E - Total Copper !' - �� � `` . e : \ 2/Monthly Composite E Total Zinc r `,, \ \ i % ,\, ` \ 2/Monthly Composite E Total Silver < i' '`, \ ' \-< /„ �\'N \., 2/Monthly Composite E Total Mercury 6 \.A ) ) \ c, N<> Quarterly Composite E Chronic Toxicity 7 :% '->-, \ \ ,/_ i—� \ \ Quarterly Composite E Temperature, °C ,,,' %"� -\. f/ " �'`,``` Variable8 Grab U, D Dissolved Oxygen \ <. ; �> Variable8 Grab U, D + \ See next page for Table Footnotes.\ \ NPDES Permit No. NC0037508 Table Footnotes: 1. Sample Locations: E — Effluent; I — Influent; U — approximately 100 feet Upstream of the outfall; D — Downstream at NCSR 1225. 2. The monthly average effluent BOD5 and Total Suspended Solids concentrations shall not exceed 15 % of the respective influent value (i.e., 85% removal is required). 3. Total Residual Chlorine (TRC) shall be monitored only if chlorine is used to disinfect. 4. Daily average dissolved oxygen effluent concentration shall not fall below 5.0 mg/L. 5. pH shall not fall below 6.0 nor exceed 9.0 standard units. 6. Mercury -- To facilitate the Lumber River's Phase II TMDL process for mercury, the Permittee shall report mercury using sample - collection criteria and test methods established by EPA Test Method 16J'Tlais permit is subject to Special Condition A.(2.). 7. Chronic Toxicity (Ceriodaphnia) at 2.6 %; quarterly during Marchf,Jun'September, December; See Special Condition A. (3.) 8. Variable: instream samples shall be collected upstream and downstrea 3/,week during the summer months of June, July, August, and September; samples shall be collected weekly during the rest 9f$$ie y ar. \ Units: / / \\ mg/L = milligrams per liter Ma-K micrograms per liter;\ Lbs/Day = pounds per day BOD = biochemical oxygen demand ( NH3 as ammom)as nitrogen\ \ ml = milliliter .., .\\�` \ Effluent shall contain no floating-- olids or,foam�vi ihle\'n other than. trace amounts. / NNN, > �\ / — — ,----------- \ \ / \ , \ ✓ \\\ i \ \> f,. NPDES Permit No. NC0037508 SUPPLEMENT TO EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS SPECIAL CONDITIONS A (2). MERCURY REOPENER. The Division may re -open this permit to require mercury load limitations, mercury minimization plans, and/or source water characterization following completion of the Phase IIIVlercury TMDL for the Lumber and Waccamaw River watersheds. Nortl�Carolina Divisiijn'of 'Water Quality �. 1'621�Mai( Service Center Raleigh, North Carolina 27699-1621 Completed Aquatic Toxicity,Test Forms, shall be filed with the Environmental Sciences Branch no later than 30 days after the end of the reporting period for w`hieh,tlie report is made. Test data shall be complete, accurate, include all supporting chemical/physical measurements and a11.coCntration/response data, and be certified by laboratory supervisor and ORC or approved designate signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the form. The report shall be submitted to the,Environmental Sciences Branch at the address cited above. Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be required during the following month. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NPDES Permit No. NC0037508 SUPPLEMENT OT EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS SPECIAL CONDITIONS A. (3.) CHRONIC TOXICITY PERMIT LIMIT (QUARTERLY) The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to Ceriodaphnia dubia at an effluent concentration of 41 %. The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or suequue/ent; versions. The tests will be performed during the months of, March, June, September, and December. Efflu' entsmpling for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes \ If the test procedure, performed as the first test of any s ngl quarter, resultin"a failure or ChV below the permit limit, then multiple -concentration testing shall be performed'at'alnnnimum, in each of fte two following months, as described in "North Carolina Phase II Chronic Whole Efflue tToxicity Tes Procedure's (Revised -February 1998) or subsequent versions. \ i� ..7,-. \\ ' The chronic value for multiple concentration test s w11,be det rrriinedl,using the geometric mea roof the highest concentration having no detectable impairment of reproduction or sure`v2l•arid,the'lowe'st concentration that does have a detectable impairment of reproduction or survival. The definition of "detectable ai3meitt," collection methods; exposure regimes, and further statistical methods are specified in the `N,orth Carolina Phase' I Cf%omo•,Whol Ef \ fluent Toxicity Test Procedure" (Revised - February 1998) or subsequent versions!; 2 \ �, All toxicity testing results reecuir � as part o this � perrru�condi�t'�wiLl be.�tered on the Effluent Discharge Monitoring Form (MR-1) for the months in whicli'test\ere perforitned, using the parametercode TGP3B for the pass/fail results and THP3B for the Chronic Value: Additioally,`DWQ Form AT-3 (original) is to be sent to the following address: Attention: ` { � ` �Envirg mn ent c. iences'B.ranch NOTE: Failure to achieve test conditions as specified in the cited document (such as minimum control organism survival, minimum control organism reproduction, and/or appropriate environmental controls) shall constitute an invalid test and will require immediate follow-up testing, to be completed no later than the last day of the month following the month of initial monitoring. DENR / DWQ / NPDES Unit FACT SHEET FOR NPDES PERMIT, DEVELOPMENT NPDES Permit NC0037508•; INTRODUCTION Moore County Wastewater Treatment Plant (WWTP), herein called Moore County or the permittee, requires a National Pollutant Discharge Elimination System (NPDES) permit to`dispose treated wastewater to the surface waters of the state. The permittee's 5-year NPDES permit expired July 31, . 2004 and they have requested renewal from the Division of Water Quality (the Division). This Fact Sheet summarizes background information and rationale used by the Division'sNPDES Unit to determine permit limits and monitoring conditions. FACILITY. RECORDS REVIEW Facility Description. -The Moore County WWTP (Table 1)_ is a 6.7: MGD publicly owned treatment works (POTW) utilizing a Grade IV activated sludge wastewater treatment facility to treat domestic and industrial wastewater. The Moore County treatment system utilizes.pre-aeration, grit removal, primary clarification, first -stage activated sludge, intermediate clarification, second -stage aeration, final clarification, anaerobic 'sludge digestion,, sludge drying beds, and post -aeration. Table 1. The Moore County WWTP rt F53Facility Information Fr ;u ,.e ,. _,a _y.�( .. o-_. ..�,. „,-.4.-,,,,,,,,,,,,_. �,,...e.�..t 4 'f� 'ti Applicant'/Facility Name. '' The Moore County WWTP {. Applicant Address rrK . 1094 Addor Road � ; ' , Facility Address _ 4 y Aberdeen:, North Carolina 283'15: , , { , . Permitted Fow,(MGD) r `4= r 6.7 , Type i5f,Waste _ ' ?_ ,• ' Industrial and Domestic (4 SIUs) Related Perrot (s) e s ; ' fi • Land -Application WQ0018081 (Anson County) Facility Grade'/ Pe mitt Status is Grade IV, Major / Renewal Drainage Basin `, `; Lumber River Basin . _ -- I County. a .,.. ` w , . .Moore County 1 44 fia iscelaeos1 y z ReceivingFStream-. _ Lumber River Regional Office:; = ' Fayetteville Stream Class carion ,.xk C State Gnd l USGS Topo Quad ' G 21 SW. / Pinebluff, NC 303(d).Liste2M. ,. No •P,eranit Writer„ ;'%z- Joe R. Corporon • ,Subbasin ,.,;:- ,.' 03-07-50 Date x (,• 3Dec04 Drainage Ar'eaf(sq iu) r 36.3 Sunnier 7Q1;0 (cfs) 15.2 Winter 7QI'0c s r. 28.7 30Q2 (cfs), Average Flow (cfs);,, `' 47.2 Lat. 35° 04' 04" Long. 78° 28' 05" TWC (%),' c" 41 % • DRAFT Fact Sheet . . Renewal--.NPDES Peimit NC0037508 Pagel Correspondence Staff Report. Fayetteville Regional Office (FRO) conducted an annual facility inspection and Grady Dobson prepared a Staff Report dated March 22, 2004. The FRO staff found the facility in good condition and in compliance with the permit recommending that the NPDES Unit renew the permit in accordance with the basin plan. Division Records and Permittee's Renewal Application. The current permit expired on July 31, 2004, and the Division received a timely request to renew the permit from the permittee's (Standard Form 2A) on January 20, 2004. COMPLIANCE REVIEW Waste Load Allocation (WLA). The Division prepared the last WLA for the receiving stream in June 1994 and developed effluent limits and monitoring requirements considering an in -stream waste concentration (IWC) of 41 % at 6.7 MGD. The Division views these limits and monitoring requirements appropriate for renewal except as outlined below (see Permitting Approach Summary). Verifying Existing Stream Conditions. This facility discharges to Aberdeen Creek [Stream Index No. 14- 2-11-(6)], a Class C waterbody within the Lumber River Basin. Aberdeen Creek is not listed as "impaired" [not 303(d) listed], However, Aberdeen Creek discharges to Downing Creek, one of 11 waters within the Lumber River Basin with fish advisories for mercury. Concerning Mercury. Beginning in September 2003, the Division required Moore County to monitor Quarterly for mercury using new EPA method 1631. The Division did not impose a permit limit. Conditions have not changed. To date, the Division has received five sample results using Method 1631. Quarterly results, - beginning chronologically from September 2003, indicate mercury levels of 16, 12, 12, 6, and 7 ng/L compared to a potential permit limit of 30 ng/L, based on IWC. Per agreement with EPA, quarterly monitoring will continue without a permit limit until sufficient data have been collected to firmly evaluate reasonable potential. A note will be added to the cover letter stating that the permittee must continue this quarterly monitoring using Method 1631. A "re -opener" clause has been added to the ;permit to emphasize the need to reevaluate should compliance questions arise. DMR Instream and Effluent Data Review. The Division reviewed 44 months of DMRs (January 2001 through October 2004) noting monthly -average flows averaging approximately 5.1 MGD or about 76% of its permitted capacity. DMRs appear regular, thorough, and complete The Division contacted the Permittee to correct the database for mercury and the Permittee complied. Effluent Total Residual Chlorine (TRC). The permittee currently chlorinates and de -chlorinates its effluent un-restricted by a Weekly Average TRC limit. In accordance with statewide. policy requiring TRC limit in all permits, a limit of 28 µg/L will be added to this permit. Whole Effluent Toxicity (WET) Testing. The Division reviewed Moore County quarterly Whole Effluent Toxicity records from January 1997 through September 2004 (32 quarterly tests). The Permittee passed all quarterly toxicity tests during this time period. DRAFT Fact Sheet Renewal -- NPDES NC0037508 Page 2 Notices of Violation (NOVs) and Penalty Assessment. Division records for this facility show no permit limit violations during the time period January 2001 through September 2004. Toxicant Chronic and Acute Impact — Pollutants of Concern (POCs). To establish POCs, the Division reviewed the permit application, discharge monitoring reports (Jan 2001 through Sep 2004), pretreatment data, and the Basin Plan.. The Division then used the standard Reasonable Potential Analysis (RPA) to calculate a maximum predicted concentration for each POC. Each maximum was then compared to the POC's freshwater Chronic Standard (Table 2) and also to its Final Acute Value (%Z FAV) for freshwater (Table 3). If by the above method, a POC showed reasonable potential to exceed its %2 FAV, the Division included a permit limit as a Daily Maximum to protect the receiving stream against acute toxic affects. Similarly, if the maximum exceeded the chronic standard, a Weekly Average limit was added to the permit. Findings and draft permit changes are summarized below (see Renewal Summary, Table 4). Table 2. Moore County WWTP Chronic RPA Findings and Renewal Action Parameter Samples ` (n) Hits ' (n) Maximum Predicted ,...,� Allowable ; Concentration , . ` RP* y/n . .,<, t' Comments / Renewal Action «fir:._ ,. .... .. .... Copper sa, 41 41 493.2 µg/L 17 µg/L Yes Action Level Standard — no toxicity problem, therefore no limit; add monitoring 2/Month Mercury ' 5 5 0.04548 µg/L 12.0 ng/L — Limited database (5 samples by EPA Method 1631). Continue monitoring quarterly. Silver ' 38 10 13.9 µg/L 0.148 µg/L Yes Action Level Standard — no toxicity problem, therefore no limit; add monitoring 2/Month Z inc ' ; 40 40 2,032.5 µg/L 123 µg/L Yes Action Level Standard — no toxicity problem, therefore no limit; add monitoring 2/Month *RP = "Reasonable Potential' to exceed instream Water Quality Standard. Table 3. Moore County WWTP Acute RPA Findings and Renewal Action Parameter 'Samples. (n) Hits (n) Maximum .'Predicted '/2 FAIT) CMC RP* 3 y/n Comments / ' Renewal Action Copper i z 41 41 493.2 µg/L 7.3 µg/L Yes ' Action Level Standard — no toxicity problem, therefore no limit; Add monitoring 2/Month Mercury 5 5 0.04548 µg/L — — No acute limit; Standard based on bio-accumulation (See Table 2). Silver :_ ,:=_ _" =-.' 38 10 13.9 µg/L 1.23 µg/L Yes Action Level Standard — no toxicity problem, therefore no limit; add monitoring 2/Month Z►nc. _ Y_` 40 40 2,032.5 µg/L 67 µg/L Yes Action Level Standard — no toxicity problem, therefore no limit; add monitoring 2/Month *RP = "Reasonable Potential" to exceed mstream Water Quality Standard. DRAFT Fact Sheet Renewal -- NPDES NC0037508 Page 3 Pretreatment Compliance. This NPDES permit requires the Permittee to implement a Long Term Management Plan (LTMP) or pretreatment program, as specified by federal regulations 40 CFR 403 and Title 15A NCAC 2H.0900 of state regulations. The Permittee's LTMP,has been approved by the Division and potential influent parameters were considered during the Reasonable Potential Analysis. Moore County WWTP currently services domestic wastes from several surrounding communities but only 1 Significant Industrial Users (S1U). This SIU provides an average daily discharge of approximately 0.150 MGD or about 2% of Moore County's permitted discharge. Revising Ammonia (NH3 as N) Limits. Ammonia Limits have been adjusted for toxicity considering IWC of 41 %. The previous permit's Monthly Average (Summer) limit has been adjusted to 2.1 mg/L, and a limit of 6.2 mg/L Monthly Average (Winter) has been added to the permit. iPer statewide policy, the Division has added ammonia Weekly Average limits to this permit. Because Moore County is a major municipal, Weekly Average limits are calculated as "Monthly Average values times three." This corresponds to a new Weekly Averages of 6.3 mg/L (summer), and 18.6 mg/L (Winter). Although new ammonia limits are notably more stringent, the Division reviewed the permittee's NH3 data and anticipates no compliance problems with new permit limits. Data for the years 2003 and 2004 indicate average daily ammonia levels consistently reported below detection at 0.5 mg/L with a maximum reported as 0.8 mg/L. RENEWAL SUMMARY Effluent Monitoring Table 4. Permit Renewal -- Recommended Changes/Additions: Parameter. 'RP* -":Comments / Renewal Actiont : A :- Ammonia:; .. (NH3 as 1s1) r .° — Revised Limits: adjusted Summer Monthly Ave. to 2.1 mg/L; Added Summer Weekly Ave. of 6.2 mg/L; added limits Winter Monthly Ave. 6.3 mg/L and Weekly Ave. 18.6 mg/L. TRC, ` - `: ',: Added Total Residual Chlorine (TRC) Daily Max. limit of 28 µg/L. Copper'..; ;':": Yes Action Level Standard, no TOX problem therefore no limits; add monitoring 2/Month ',Mercury::"= — TMDL for the Lumber River Basin dictates Quarterly monitoring by EPA Method 1631 `Silver:-.., ;.":., ;";,, Yes Action Level Standard, no TOX problem therefore no limits; continue monitoring 2/Month Zne:'- -', `t :,' : Yes Action Level Standard, no TOX problem therefore no linuts; continue monitoring 2/Month *RP = "Reasonable Potential" to exceed instream Water Quality Standard. Instream Monitoring Previous Requirements: For Renewal: Conductivity Fecal Coliform Dissolved Oxygen (DO) Temperature Delete fecal coliform and conductivity from instream testing, per Division statewide permitting guidance. No other changes recommended. DRAFT Fact Sheet Renewal -- NPDES NC0037508 Page 4 PROPOSED SCHEDULE OF ISSUANCE Draft Permit to Public Notice: Permit Scheduled to Issue: NPDES UNIT CONTACT December 8, 2004 January ;31, 2005 If you have questie s r gardi .any of the above- information or on the attached permit, please contact Joe Cozdron at 919 733-5083 ext. 597. DATE: R •'G • NAL S FFICE COMMENTS. NAME: . DATE: REGIONAL SUPERVISOR: (,/,,/„) =/Y-a-n-/t_) DATE: NPDES SUPERVISOR: - DATE: DRAFT Fact Sheet Renewal -- NPDES NC0037508 Page 5 MEMORANDUM TO: FROM: THRU: - SUBJECT: DIVISION OF WATER QUALITY March 22, 2004 Dave Goodrich, Supervisor Permitting and Engineering Un Dale Lop Environmental Specialis Paul Ra ter Quality Supervisor Fayettevill egional Office NPDES Staff Report and Recommendations NPDES Permit No. NC0037508 Moore County Water Pollution Control Moore County Please find attached the staff report and recommendations of the Fayetteville Regional Office concerning the renewal of subject NPDES Permit. If you have any questions or require any further information, please advise. DL/bs-m Attachment SOC PRIORITY PROJECT: YES_ NO X If Yes, SOC No. To: Permits and Engineering Unit Water Quality Section Attention: Charles Weaver Date: March 15, 2003 NPDES STAFF REPORT AND RECOMMENDATION COUNTY: Moore Permit No. NC 0037508 PART I - GENERAL INFORMATION 1. Facility and Address: Moore County Water Pollution Control 1094 Addor Road Aberdeen, NC 28315 2. Date of Investigation: December 1, 2003 3. Report Prepared by: Dale Lopez, Environmental Specialist 4. Persons Contacted and Telephone Number: James D. Frye, System Supervisor 910-281-3!146 f 5 Directions to Site: Take SR 1100, south of Addor, for approximately 1 mile. Treatment plant is on right side of road. 6. Discharge Point(s), List for all discharge points: Latitude: 35° 04' 04" Longitude: 78° 28' 07". Attach a U.S.G.S. map extract and indicate treatment facility site and discharge point on map. U.S.G.S. Quad No. G-21-SW U.S.G.S. Quad Name: P nebluff. NC 7. Site size and expansion area consistent with application? Approximately 50 acres X Yes _ No (If No, explain) 8. Topography: (relationship to flood plain included): Flat and terraced; 0-10% slope 9. Location of nearest dwelling: None within 1,000 feet PART I - GENERAL INFORMATION (continued) 10. Receiving stream or affected surface waters: Aberdeen Creek a. Classification: "Class C" b. River Basin and Subbasin No.: Lumber River Basin 03 - 07 - 50 c. Describe receiving stream features and pertinent downstream.uses: Fish and wildlife propagation, secondary recreation, agriculture, and other uses requiring waters of lower quality. PART II - DESCRIPTION OF WASTES AND TREATMENT WORKS 1. a. Volume of wastewater to be permitted: 6.67 MGD (Ultimate Design Capacity) b. What is the current permitted capacity of the Wastewater Treatment facility? 6.6 MGD c. Actual treatment capacity of the current facility (current design capacity). 6.67 MGD d. Date(s) and construction activities allowed by previous Authorizations to Construct issued in the previous two (2) years. N/A e. Please provide a description of existing or substantially constructed wastewater treatment facilities: The existing waste facility consists of the following: 6.67 MGD (design capacity), preaeration and grit removal, primary clarification, first (1st) stage activated sludge, intermediate clarification, second (2nd) stage aeration, final clarification, anaerobic sludge digestion, sludge dryng beds, and post aertion. f. Please provide a description of proposed wastewater treatment facilities: N/A g. Possible toxic impacts to surface waters: N/A h. Pretreatment Program (POTWs only): In development Approved X Should be required Not needed PART II - DESCRIPTION OF WASTES AND TREATMENT WORKS (continued) 2. Residuals handling and utilizing/disposal scheme: The dried sludge is routed to a lined landfill in Anson County. a. If residuals are being land applied, please specify DWQ Permit No. Permit Number WQ0018018, which has never been used. Residual Contractor: N/A Telephone : N/A b. Residuals stabilization: PSRP X PFRP Other c. Landfill: Uwharrie Environmental Landfill, Troy, North Carolina, Montgomery County d. Other disposal/utilization scheme (specify): I 3. Treatment plant classification (attach completed rating sheet): Grade IV (see attached) 4. SIC Code(s): Primary 01 Secondary 55 57 Main Treatment Unit Code: 1 1 0 0 1 PART III - OTHER PERTINENT INFORMATION 1. Is this facility being constructed with Construction Grant Funds or are any public monies involved (municipals only)? N/A 2. Special monitoring or limitations (including toxicity) requests: Please note that the Priority Pollutant Analysis showed greater than detection level amounts for Antimony, Copper, Zinc and Calcium. 3. Important SOC, JOC, or Compliance Schedule Dates (please attach): N/A Date Submission of Plans and Specifications N/A Begin Construction N/A Complete Construction N/A PART III - OTHER PERTINENT INFORMATION (continued) 4. Alternative Analysis Evaluation: Has the facility evaluated all of the nondischarge options available? Please provide regional perspective for each option evaluated. Spray Irrigation: N/A Connection to Regional Sewer System:. N/A Subsurface: N/A Other disposal options: N/A 5. Other Special Items: PART IV - EVALUATION AND RECOMMENDATIONS It is recommendation of this office that the permit application be processed and the appropriate permit issued. Water Quality Regional Supervisor Date IPE4deV4'LS61(3) we±iAda3 I WATER POLLUTION CONTROL SYSTEM OPERATORS CERTIFICATION COM:MISSION CLASSIFICATION. • i RATING SHEET. FOR WATER POLLUTION CONTROL SYSTEMS FACILITY INFORMATION: NAME OF FACILITY: /de/e&- UNT G /ii /®i/ 7'F4 G6/) DA147-iPat )2/9,-/7- ..tom- 4 MAILING ADDRESS: 1 D l AD b vie /Q®f4„ D 6 E- Ai /'e l COUNTY:Ri04R L' CONTACT PERSON:JAM5.S Aiye. TELEPHONE: % (9/ 0) 8 —Jam/ .PERMTT NO: G' C D go? Check One: NC j WQ. HEALTH OP TELEPHONE: i(9/O) g / - 3 / $16 ORC: %%AmF5 1::/91E RATING INFORMATION: (Before completing this section, please refer to pages 2-4) PERMITTED FLOW: , 6 7 MGD BNR? ' YES CHECK CLASSIFICATION: WAS 1'EWA 1'bR: 1 COLLEC:1ION: SPRAY IRRIGATION SUBSURFACE PHYSICAL/CHEMICAL GRADE I NO 4 LAND APPLICATION GRADE II RATED BY: �� REGION: f'f 0 DATE: 1 /5 -A REGIONAL OFFICE TELEPHONE NUMBER: (9/D) `74 6'6 15 /EXT: 7/ L Classification of Biological'Water Pollution Control Treatment Systems: Grade I Biological WPCS = Septic tank/sand filter systems - Biological lagoon systems Constructed wetlands and associated appurtenances Grade II Biological WPCS Systems that utilize an activated sludge or fixed growth process with a permitted flow less than or equal to 0.5 million gallons per day (mgd) Grade III Biological WPCS - Systems that.utili7e an activated sludge or fixed growth process with a permitted flow of greater than 0.5 through 2.5 million gallons per day (mgd) - Grade II systems that are required to achieve biological nutrient reduction * 1/ Grade IV Biological WPCS - Systems that utilizing an activated sludge or fixed growth process with a permitted flow of greater than 2.5 million gallons per day (mgd) = Grade III systems that are required to achieve biological nutrient reduction * * Biological Nutrient Reduction - The reduction of total nitrogen or total phosphorous by an activated sludge or fixed growth process as required by the facilities permit. Classification of Collection Water Pollution Control Systems: (whichever provides lowest grade) Same grade as biological water pollution control system. Grade of system: Based on population served: 1,500. or Less = Grade I 1,501 to 15,000 = Grade II 15,001 to 50,000 =. Grade III 50,001 or more = Grade IV Classification of Spray Irrigation Water Pollution Control Systems: Systems which utilize spray irrigation for the reuse or disposal of wasterwater. These systems include: septic tanks, sand filter, oil/water separators, lagoons, storage basins, screening, sedimentation. Systems other than those listed above shall be subject to additional classification. Classification of Land Application of Residuals Systems: Systems permitted and dedicated for land application of residuals that are produced by a water pollution control system or contaminated soils. Classification of Physical/Chemical Water Pollution Control Treatment Systems: Grade I Physical/Chemical: Any water pollution control system that utilizes a primarily physical process to treat wastewater. This classification includes groundwater remediation systems. ** Grade II Physical/Chemical: Any water pollution control system that utilizes a primarily chemical process to treat wastewater. This classification includes reverse osmosis, electrodialysis, and ultrafiltration systems. ** ** Any water pollution -,control system that utilizes a phyical/chemical process to enhance an activated sludge or fixed growth process, shall not be -subject to additional classification. Classification of Subsurface Water Pollution Control Systems: Systems which utilize the soil for subsurface treatment and disposal of wastewater and/or are required to have a certified operator under 15A NCAC 18A.1961. ***j *** Any subsurface system that has as part of its treatment process a water pollution control ' systems that may be classified under Rules .0302 through .0307 of this section shall be. subject to midional classification. Definitions Activated Sludge - shall mean a biological wastewater treatment process in which predominantly biodegradable polluntants in wastewater are absorbed, or adsorbed by living aerobic organisms and bacteria: Chemical Process - shall mean a wastewater pollution control system process consisting exclusively of the addition of chemicals to treat wastewater. Collection System - shall mean a continuous connections of pipelines, conduits, .pumping stations, and other related constructions used to conduct wastewater to the water pollution control system. Electrodialysis System - 'shall mean a system utlizing a selective separation of dissolved solids process that is based on electrical charge and diffusion through a semipermeable membrane. Physical Process shall mean any water pollution control system process consisting of electrodialysis, adsorption, absorption, air stripping, gravimetric sedimentation, floation, and filtration as a means of treatment. Reverse Osmosis System - shall mean a system which utilizes solutions and semipermable membranes to separate and .treat wastewater. Ultrafiltration System - shall mean a system which utilizes a membrane filter to remove pollutants from wastewater. Water Pollution Control System - shall mean any system for the collection, treatment, or disposal of wastewater and is classified under the provision of G.S. 90A-37. Note: Please refer to G.S. 90A-37 for additional information and definitions. ENVIRONMENTAL SCIENCE CORP . ' REPORT OF ANALYSIS • Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 Date Received January 21, 2004 Description 13718 - Moore County WWTP Sample ID EFFLUENT 0119122 Collected By Collection Date : 01/19/04 09:05 Parameter 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 29, 2004 SC Sample # L141764-01 Site ID . Project # : TBL-13718 ( Result Det. Limit ! Units Method Date Dil. Cyanide Hardness, calcium Total Phenol by 4AAP Thallium Mercury Antimony Arsenic Beryllium Cadmium Calcium Chromium Copper Lead Nickel Selenium Silver Zinc Gbt, R�= PP Volatile Organics Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride y Chlorobenzene Chlorodibromomethane Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane BDL BDL BDL BDL 0m0.095 - BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0050 mg/1 1 335.3 mg/1 Calc. 0.040 mg/1 420.2 0.0010 - mg/1 200.8 0.00020 mg/1 245.1 0.0050 mg/1 200.7 0.010 mg/1 200.7 0.0020 mg/1 200.7 0.0050 mg/1 20'0.7 0.50 mg/1 200.7 0.010 ..mg/1 200.7 0.010 mg/1 200.7 0.0050 mg/1 200.7 0.010 mg/1 200.7 0.010 mg/1 200.7 0.0050 mg/1 200.7 0.030 mg/1 200.7 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0:0010 mg/1 0.050 mg/1 0.0050 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 0.0010 mg/1 01/23/04 1 01/23/04 1 01/28/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04- 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1. 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/04 1 624 01/22/0.4 1 624 01/22/04 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) . Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, 'CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004„ TN - 2006," VA - 00109, WV - 233 Page 1 of 6 11 1 MONITORING REPORT(MR) VIOLATIONS for: PERMIT: NCO037508 FACILITY: Moore County Public Utilities - Moore County WPCF C6UNTY: Moore REGION: Fayetteville _ Monitoring Violation MONITORING oorpxu` nEpnnT /pp| LooxTow pxnAwsTsn 10'200 .001 Effluent Copper, Total (as Cu) 10 ' 2oo1 001 Effluent Phosphorus, Total (asp) Reporting Violation vmumnw UNIT OF oALcuuATso DATE FREQUENCY MEASURE LIMIT VALUE 1031K1 2:month ug8 103101 Monthly mg0 1031/01 Monthly mO8 ^10m1m1 uxmonth uo/I VIOLATION TYPE Frequency Violation Frequency Violation Frequency Violation Frequency Violation Frequency Violation VIOLATION ACTION a|ma Pre -Production Violation a|ms pne'pmuucUon mu|aoun 8|MS pm-=muu000n Violation B|mS Pre -Production Violation e|mo ' Pre -Production Violation MONITORING nUTFAu VIOLATION UNIT OF cALouuATso LOCATION PARAMETER DATE FREQUENCY MEASURE LIMIT VALUE --11--'2001--001- - -Emu*m'-oyan0&�Tvf;a_|<a��_cn7------l113om1 zxndmffi -ug71r VIOLATION TYPE Parameter Missing VIOLATION ACTION --a|MS — Pre -Production Violation MONITORING REPORT(MR) VIOLATIONS for: 003750. Report Date: 02/12/04 Page: 1 of 1 PERMIT: NC0037508 FACILITY: Moore County Public Utilities - Moore County WPCF COUNTY: Moore REGION: Fayetteville Monitoring Violation MONITORING -OUTFALL VIOLATION UNIT OF CALCULATED REPORT / PPI LOCATION PARAMETER • DATE FREQUENCY MEASURE LIMIT • VALUE VIOLATION TYPE' VIOLATION ACTION 01 --2003 001 Effluent Chlorine, Total Residual 01/04/03 5 X week ug/I Frequency Violation None 01 - 2003 001 Effluent Coliform, Fecal MF, M-FC 01/04/03 , 5 X week #/100n11 Frequency Violation None Broth,44.5C 01 - 2003 001 Effluent Nitrogen, Ammonia Total (as N) 01/04/03 5 X week mg/I Frequency Violation None 11 - 2003 001 Effluent. Nitrogen, Ammonia Total (as N) 11/29/03 5 X week mg/I Frequency Violation None 12 - 2002 001 Effluent Silver, Total (as Ag) 12/31/02 2 X month ug/I Frequency Violation None 01 - 2003 001 Effluent pH 01/04/03 5 X week su Frequency Violation None Whole Effluent Toxicity Testing Self -Monitoring Summary FACILITY REQUIREMENT February 16, 2004 YEAR JAN FEB MAIL AI'R MAY JIJN JUL AIJU STEP OCT NOV DEC Moore:Cobnty WWTP '. •• chr bin: 41 a% Y 2000 - - Pass - - • Pass - - Pass - Pass NC0037508/001 Bcgin:6/I/2000 Frcqucncy.Q Mar Jun Sep Dec + NonComp Single 2001 - - Pas's - Pass -- - Pass - Pass County: Monte Region: 1q(O Subbasin: LUM511 2002 - - Pass - - Pass - - Pass - - Pass PF: 6.7 - •Special 2003 - - Pass - - Pass - - Pass - - Pass 7Q10: 15.2 • IWC(%; 40.54 2004 Mt. Gilead WWTP chr lim: 3.2% • 2000 - - Pass - - NR Pass - H Pass - Pass NC0021105/001 Begin:3/I/2000 Frequency Q Mal Jun Scp Dec + NonComp Single 2001 - - NR NR Pass Pass - - Pass - - Pass County:Montgomery ' Region: FRO Subbasin: YADIO - 2002 - - Pass - - Pass - - Late Pass - Pass PF:.0.85• Special 2003 - - Pass - - Pass - - Pass - - Pass 7Q10: 40,. ' IWC(%;3.2 - 2004 North Barnett Regional WWTI' 24 hr.Fthd p/f ac him: 90% NC0021636/001 Begin:10/1/2001 Frequency Q. + Jan Apr Jul Oc1 County: Remelt , Region: FRO Subbasin: CPFO7 PF: 0.6 Special' '7Q10: 550.0 IWC(%;0,17 +' NonComp Single 2000 Pass - - Pass - - Pass - - Pass - - 2001 Pass - - Pass - - Pass - - Pass - - 2002 Pass - - Pass - - Pass - - Pass - - 2003 Fail.Pass - - Pass - - Pass - - Pass . 2004 P9rklon WWTP chr lim: 90% NC0026921/001 Begin: I/1/2000 Frequency Q , Jan Apr Jul Oct County:Robeson : Region:IRO Subbasin:.LIJM53 PF: 0.2 . Special 7Q10: 0.0 IWC(%: 1110 + NonComp Single 2000 Fail Pass >100 Pass - - Fail 94.84 NR . 82.13 35.30 35.30 2001 82.16 82.16 35.4 94.9 - - Pass - - Fail >100 35.4 2002 >100 .- 7 Pass - - Pass - - Fail . 94.9. <25 2003 25 >100 33.5 Pass - - Fail ' 94.9 >100 Pass - - • 2004 Pembroke WWII' chr lira: 1.7% 2000 Late Pass - Pass - - Pass - - Pass NC0027103/001 Begin:6/1/2000 Frequency Q Jan Apr Jul Oct 4 NonComp Single 2001 Pass - - Pass - - Pass - - Pass County:Robeson Region: FRO Subbasin: LUM51 2002 Pass - - Pass - - Pass - - Pass PF: 1.33 ' . . Special 2003 Pass - - Pass - - Pass - - Pass 7Q10: 114 IWC(%: 1.8 2004 Pass Raeford WWTP . chr lim: 9% 2000 - Pass - - Pass - - Invalid - Pass Pass NC0026514/001 Begin:7/I/1996 Frequency 0 P/F + Feb May Aug Nov . NonComp Single • 2001 - Pass - - Pass - - Pass - - Pass County:_Hoke . Region: FRO Subbasin: CPFIS 2002 - Pass - - Pass - - Fail >18 >18 Pass PF: 3.0 Special 2003 - Pass - - Fail 5.20 >18,Pass Pass - - Pass 7Q10: 49.0... f1VC1%;5.67 2004 Red Springs WWTP chr lim: 90% NC0025577/001 Begin:5/1/2000 Frequency Q . •Jan Apr Jul Oct + NonComp Single • County:Robeson • Region: FRO Subbasin: LUM52 PF: 2.5 . Special Effective 12/1/02, signed 12/27/02, expires 12/1/04 7Q10: 0.07 IWC(%;98 2000 Late >90 - 17.7 <12.5 35.4 . 17.7 17.7 35.4 >90 17.7 35.4 2001 <12.5 61.2 82.2' >90 35.4 35.4 >90 82.2 <12.5 <12.5 61.2 Invalid 2002 Late Late >90 >90 • 82.2 35.4 >60 - >90 58.1 58.1 33.5 2003 <12:5 >90 33.5 >90 17.7 58.1 58.1 >90 >90 <12.5 17.7 33.5 2004 Robbins WV/TT' chr lim: 10% 2000 Pass - - Pass - - Pass - - • Pass - NC0062855/001 Bcgin:7/I/2002 Frequency Q ' Jan Apr Jul Oct , + NonComp Single 2001 Pass - - Pass - - Pass - - NR Pass County:Moore Region: FRO Subbasin: CPFIO 2002 Pass - - Pass - - Pass - - Pass - PF: .1.3 Special - 2003 pass - - • Pass - - Pass - - Pass 7QI0: 15.9 IWC.(% 10 2004 Rockingham WWTP . chr lim: 8% 2000 - Pass - . - Pass - - Pass - - • Pass . - NC0020427/001 Bcgin:WI/1999 Frequency Q P/F + Feb May Aug Nov + NonComp Single 2001 - Pass - - .Pass - - Pass - - Pass - County:Richmond Region: FRO Subbasin: YAD16 2002 - Pass • - - Pass - - Pass - - Pass - PF: 9.0 Special - 2003 - Pass - - P. ss - _ _ _-___P_ass.>32 - - Pass>32 -- 7Q10: 153 IWC(%:8.0 - --- - 2004 - - - Roseboro WWTP • - chr lim: 52% NC0026816/001 Begin:12/1/2003 Frequency Q P/F + Feb May Aug Nov County:Sampson Region: FRO ',Subbasin: CPF19 PF: 0.49 .Special 7Q10: 1.0 IWC(%:52 • NonComp Single 2000 - Pass - _ _ - - _Pass - - Pass - - Pass 2001 - Pass - - Pass - ,•, - Pass - - Pass 2002 - Pass - - Pass - - Pass - - Pass 2003 - - Pass - - Pass . - - Pass - - Pass 2004 • Smithfield Packing Cn, Tarheel Div. chr lim: 0.58% • 2000 Pass - - Pass - - Pass - - Pass - -NC0078344/001 Begin:12/1/2002 Frequency Q Jan Apt Jul Oct 4 NonComp Single 2001 Pass - - Pass - - ' Pass - - Pass,Pass - Connty:Bladen- Region: FRO Subbasin; CPFI6 2002 Pass - Pass - - Pass -. - Pass - PF: 3.0 Special . ' 2003 pass - - Pass - - Pass - - Pass - ' 7Q10: 795 IWC(7: IJ.58 2004 . 4 Pre 2000 Data Available, LEGEND: PERM = Permit Items irement LET = Administrative Letter- Target Frequency = Monitoring frequency: Q- Quarterly: h4- Monthly; BM- Bimonthly; SA- Semiannually: A- Annually; OWD- Only when discharging; D. Nisconunued monitoring requirement Begin .first month required 7Q IU= Receiving stream low flow criterion refs • = gtinrterly monitoring increases to monthly upon hrilure or N Months that testing must occur - es. Jan, Apr, Jul, Oct - NonComp = Current Compliance Requirement PF = Permitted flow (MOD) IWC'%= lnstream waste coocencrati Pih.= Pass/Fail lest AC Anne GI4R=Chronic Data Notation,'" - Fathead Minnow; • - Ceriodophnia sp.; my - Mysid ',twisty; (`IiV - Chronic value; P - Mortality of staled percentage at highest concentration; at - Performed bar D WQ Aquatic To,. Unit; bl - Dad test Reporting Notation: --- ,. Oat nor required; NR, Not repose . Facility AO why Stains: 1-inactive, N -Newly Issued(To construct). If -.Active but not discharging; 'I -More data ilvadable Iim month in question; • • = ORC signature. needed 4 MONITORING REPORT(MR) VIOLATIONS for: �FacllltyName Report Date: 02/12/04 Page: 1 of 1 PERMIT: NC0037508 FACILITY: Moore County Public Utilities - Moore County WPCF COUNTY: Moore REGION:. Fayetteville Monitoring Violation MONITORING OUTFALL REPORT / PPI LOCATION PARAMETER 10 - 2001 001 Effluent Copper, Total (as Cu) 10 - 2001 001 Effluent Nitrogen, Total (as N) 10 - 2001 001 Effluent Phosphorus, Total (as P) 10 - 2001 001 Effluent Silver, Total (as Ag) 10 - 2001 001 Effluent Zinc, Total (as Zn) Reporting Violation VIOLATION UNIT OF CALCULATED DATE FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION 10/31/01 2 X morith - ug/I 10/31/01 Monthly mg/I 10/31/01 Monthly mg/I 10/31/01 2 X month ug/I 10/31/01 2 X month ug/I Frequency Violation Frequency Violation Frequency Violation Frequency Violation Frequency Violation 'BIMS Pre -Production Violation BIMS Pre -Production Violation. BIMS Pre -Production Violation BIMS Pre -Production Violation BIMS Pre -Production Violation MONITORING OUTFALL »REPORT / PPI LOCATION PARAMETER 11 - 2001 001 Effluent Cyanide, Total (as Cn) VIOLATION UNIT OF CALCULATED DATE FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION 11/30/01 2 X month ug/I Parameter Missing BIMS Pre -Production Violation Report Date: 02/12/04 Page: 1 of iP14tIoi-cCatebory; '" • ::',F,:ttodi;60-1-C•atdd - • ,„ • . PERMIT: NC0037508 FACILITY: Moore County Public Utilities - Moore County WPCF COUNTY: Moore REGION: Fayetteville Monitoring Violation MONITORING OUTFALL •REPORT / PPI VIOLATION UNIT OF CALCULATED LOCATION PARAMETER DATE FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION 01 - 2003 001 Effluent Chlorine, Total Residual- 01/04/03 5 X week ug/I Frequency Violation None 01-- 2003- - -001— --Effluent Coliform, Fecal MF, M-FC 01/04/03 5 X weik Broth,44.5C 01 - 2003 001 Effluent Nitrogen, Ammonia Total (as N) 11 - 2003 001. Effluent Nitrogen, Ammonia Total (as N) 12 - 2002 001 Effluent Silver, Total (as Ag) 01 - 2003 001 Effluent pH 01/04/03 5 X week 11/29/03 5 X week 12/31/02 2 X month 01/04/03 5 X week #/100m1 mg/I mg/I ug/I su Frequency Violation None Frequency Violation 'None Frequency Violation None Frequency Violation None Frequency Violation None :Whole Effluent Toxicity Testing Self -Monitoring Summary 'FACILITY - - .. REQUIREMENT February 16, 2004 YEAR SAN FEB MAR APR MAY J11N JUL, AUG SEP OCT NOV DEC 'Moore County-WWTP. chr lim: 41 % 9 2000 - - Pass - - Pass - - Pass NC0037508/001 Begin:6/12000 Frequency Q, Mar Jun Sep Dec + NonComp-Single' 2001 - - Pass - - Pass - - Pass County: Moore Region: FRO . Subbasin: LUM50 2002 - - Pass - - Pass - - Pass PF: 6.7 • Special 2003 - - Pass - - Pass - - Pass '7Q10: 15.2 IWC(%; 40.54 .2004 Pass Pass Pass Pass MI. Gilead WWTP chr lim: 3.2% -NC0021105/001 Begin:3/I/2000 Frequency Q Mar Jun Sep Dec ,Counly:Montgomery ' Region: FRO . Subbasin: YADIO .... PF: 0.85 • Special 7Q10: 40 IWC(%; 3.2 + NonComp Single 2000 - - Pass - - NR Pass - H Pass - Pass 2001 - - NR NR Pass Pass - - Pass - - Pass 2002 - - Pass - - Pass - - Late Pass ' - Pass 2003 - - Pass - - Pass - - Pass - - Pass 2004 Norlh,Harnett Reglonal WWTP 24 hr Fihd p/f ac lim: 90% NC0021636/001 Begin:10/1/2001 Frequency Q + Jan Apr Jul Oct County: Harnett Region: FRO Subbasin: CPF07 PF: 0.6 Special 7Q10: 550.0 IWC(% 0,17 'Parkton:WWTP " chr lim: 90% _'NC0026921/001 Begin:1/1/2000Frequency Q -- Jan -Apr Jul Oct County: Robeson Region: FRO Subbasin: LUM53 PF: 0.2 -- 7Q10: 0.0 IWC(%; 100 + NonComp Single 2000 Pass ' - - Pass - - Pass - - Pass 2001 Pass - - Pass - - Pass - - Pass 2002 Pass - - Pass - - Pass - - Pass 2003 Fail,Pass - - Pass - - Pass - - Pass 2004 + NonComp Single 2000 Fail Pass >100 Pass _ - - Fail 94.84 _ NR_ 82.13. 35.36 35.36 2001 82.16 82.16 35.4 94.9 - - Pass - - Fail >100 35.4 2002 >100 - Pass - - Pass - Fail 94.9 <25 --2003-<25 -- -- - >10- 0- - 33:5 -Pass--- - - --- - - Fail 94,9 >100 Pass - - ' 2004 Pembroke WWTl' - . chr lim: 1.7% NC0027103/001 Begin:6/l/2000 Frequency Q Jan Apr,lul Oct + NonComp Single County:Robeson Region: FRO Subbasin: LUMSI PF: 1.33 • Special 7Q10: 114- I\VC(%: 1.8 2000 Late' Pass - Pass - - Pass - - Pass 2001. Pass • - - Pass - . - Pass - Pass 2002 Pass - - Pass - - Pass - - Pass 2003 Pass - Pass - - Pass - - Pass 2004 Pass Raeford WWTP' • . . - chr lim: 9% 2000 - Pass - - Pass - - Invalid - Pass Pass NC0026514/001 Begin:7/I/1996 Frequency Q P/F + Feb May Aug Nov . NonComp Single 2001 - Pass - - - Pass - - Pass - - Pass County:Hoke Region: FRO Subbasin: CPF15 ' 2002 - Pass - - Pass - - Fail >18 >18 Pass PF: 3.0 Special 2003 - Pass - - Fail 5.20 >18,Pass Pass - - Pass . 7Q I0: 49.0 _ • . IWC(%; 8.67 • 2004 • •Red SpringsWWTP •' chrlim: 90% 2000 Late >90 - 17.7 <12.5 35.4 17.7 17.7 35.4 >90 17.7 35.4 NC0025577/tJ01 Begin:5/1/2000 . Frequency Q Jan Apr Jul Oct + NonComp ▪ Single 2001 <12.5 61.2 82.2 >90 35.4 35.4 >90 82.2 <12.5 <12.5 61.2 Invalid County: Robeson - Region: FRO Subbasin: LUM52 2002 Late Late >90 >90 82.2 35.4 >00 - >90 58.1 58.1 33.5 PF: 2.5 Spccia1 ElTective 12/1/02, signed 12/27/02, expires 12/1/04 2003 <12.5 >90 33.5 >90 17.7 58.1 58.1 >90 >90 <12.5 17,7 33.5 7QI0:-0.07 IWC(%'98 2004 Robbins WWFP • chrlim: 10% NC0062855/001 begin:7/1/20112 Frequency 0 ' Jan Apr Jul Oct + NonComp Single County:Moore " 'Region: FRO Subbasin: CPFI0 Special .7Q10: 15.9 • IWC(%; 10 2000 Pass 2001 Pass 2002 Pass 2003 pass 2004 Pass - - Pass Pass - - Pass Pass - - Pass Pass - - Pass - - • Pass - - NR - - Pass - - Pass Pa- ss Rockingham WWfr' - , chrlim:8% '.NC0020427/00I - Begin:6/1/1999 Frequency Q P/F + Feb May Aug Nov + NonComp Single County:Richmond Region: FRO Subbasin: YAD16 PF: 9.0 Special 7Q10: 153 IWC(%; 8.0 2000 - Pass 2001 - Pass 2002 - Pass . 2003 - Pass 2004 - . - Pass - - Pass - - - Pass - - Pass - - - Pass - - Pass - - Pass - - Pass >32 - Pass Pass Pass Pass,>32 Rosoboro WWTP • chr lim: 52% 2000 - Pass - - Pass - - - Pass - - Pass NC0026816/001 Begin:12/1/2003 Frequency Q P/F + Feb May Aug Nov NonComp Single 2001 - Pass - - Pass - - Pass - - Pass County:Sampson Region: FRO Subbasin: CPF19 2002 - Pass - - Pass - - Pass - - Pass PF: 0.49 ,Special • 2003 - Pass - - Pass - - Pass, - - pass 7QI0: 1.0 IWC(14i;52. 2004 Smithfield Packing Cu, Tanceel Div. ebr lim: 0.58% NC0078344/001 Begin:12/12002 Frequency Q Jan Apr Jul Oct 'County:Bladen • . Region: FRO Subbasin: CPF16 PFi 3.0 Special 7Q10: 795 I W C('0,• 0,58 • NonComp Single 2000 Pass - - Pass , 2001 Pass - - Pass 2002 Pass - - Pass 2003 pass - - Pass 2004 - - Pass - - Pass - - - ' Pass - - . Pass,Pass - - - Pass - - Pass - Pass - - Pass - 4' -Pre 2000 Data Available LEGEND: PERM = Permit Requirement LET = Administrative Letter : Target . Ft equency = Monitoring frequency; Q- Quarterly: M- Monthly; BM- Bimonthly; SA- Semiannually; A. Annually; OWD- Only when discharging; D- Discontinued monitoring requirement Begin First.month required 7Q10 = Receiving stream low, ❑ow criterion (cl's , + = quarterly monitoring increases to monthly upon failure or N Months that testing most occur - ex. Jan, Apr, Jul, Oct • NonComp = Current Compliance Requirement PF = Permitted Hove (MUD) IWC% =lnstream waste concentrati P/F = Pass/Fnil test AC = Acute CHR = Chronic Data Notation: f - Fathead Minnow; • - Ceriodaphnia sp.; my - Mysid shrimp: (-ti V - Chronic value; P - Mortality am:lied percentage at highest concentration; at - Performed b) MVO Aquatic Tox Unit: bt - Bad test Reporting Notation: --- - Data not required; NR: Not reporte Faci lit Activity Slaw::: I - Inactive, N -Newly lssued(To construct); II - Active but not discharging; t-More data available 1'nr month in question; • = ORC sign:nm,• needed 4 WATER. POLLUTION CONTROL .SYSTEM OPERATORS CERTIFICATION COMMISSION CLASSIFICATION RATING SHEET FOR WATER POLLUTION CONTROL SYSTEMS FACILITY INFORMATION: NAME OF FACILITY: MAILING ADDRESS: COUNTY: - CONTACT PERSON: J,9Mi.S A;f7 E TELEPHONE pLL1J y/��/ QJPD� /2i9.11:7" R r: it)e 6R E3l g ORC: j,4mFS /`-iF'j/t TELEPHONE: (0:/' ).- $% - RATING INFORMATION: (Before completing this section, please refer to pages 2-4) , PERMITTED FLOW: , 4 7 MGD BNR? CHECK CLASSIFICATION: WASTEWATER: COLLECTION: 2 YES SPRAY IRRIGATION SUBSURFACE LAND APPLICATION PHYSICALJCHEMICAL GRADE I GRADE II RATED BY: REGION: D NO 4 DATE: � 4 REGIONAL OFFICE TELEPHONE NUMBER: (. 9/D '74 S 6 -) K /EXT: 7/ Classification of Biological Water Pollution Control- Treatment Systems: - Grade I Biological WPCS - Septic tank/sand filter systems Biological lagoon systems - Constructed wetlands and associated appurtenances Grade II Biological WPCS - Systems that utilize an activated sludge or fixed growth process with a permitted flow less than or equal to 0.5 million gallons per day (mgd) Grade III Biological WPCS - Systems that.utili7e an activated sludge or fixed growth process with a permitted flow of greater than 0.5 through 2.5 million gallons per day (mgd) - Grade II systems that are required to achieve biological nutrient reduction * Grade IV Biological WPCS - Systems that utilizing an activated sludge or fixed growth process with a.permitted flow of greater than 2.5 million gallons per day (mgd) = Grade III systems that are required to achieve biologicaljnutrient reduction * * Biological Nutrient Reduction - The reduction of total nitrogen or total phosphorous by an activated sludge or fixed growth • process as required by the facilities permit. Classification of Collection Water Pollution Control Systems: (whichever provides lowest grade) Same grade as biological water pollution control system. Grade of system: Based on population served: 1,500. or Less = Grade I 1,501 to 15,000 = Grade II 15,001 to 50,000 = Grade III 50,001 or more = Grade IV Classification of Spray Irrigation Water Pollution Control Systems: Systems which utilizespray irrigation for the reuse or disposal of wasterwater. These systems include: septic tanks, sand filter, oil/water separators, lagoons, storage basins, screening, sedimentation. Systems other than those listed above shall be subject to additional classification. Classification of Land Application of Residuals Systems: Systems permitted and dedicated for land application of residuals that are produced by a water pollution control system or contaminated soils. • Classification of Physical/Chemical Water Pollution Control Treatment Systems: Grade I Physical/Chemical: Any water pollution control system that utilizes a primarily physical process to treat wastewater. This classification includes groundwater remediation systems. ** Grade II Physical/Chemical: Any water pollution control system that utilizes a primarily chemical process to treat wastewater:. This classification includes reverseosmosis, electrodialysis, and ultrafiltration systems. ** ** Any water pollutioricontrol system that utilizes a phyicallchemical process to enhance an activated sludge or fixed growth process, shall not be -subject to additional classification. Classification of Subsurface Water Pollution Control Systems: Systems which utilize the soil for subsurface treatment and disposal of wastewater and/or are required to have a certified operator under 15A NCAC 18A.1961. *** • *** Any subsurface system that has as part of its treatment process a water pollution control systems that may be classified under Rules .0302 through .0307 of this section shall be subject to addional classification. ' MONITORING REPORT(MR) VIOLATIONS for: Permit,`NC0037508 Facility Name.: % aram_Name ,° egion "-,' ounty Violation. Category: Subbasm: %. - Report Date: -02/12/04 Page: 1 of 1 rogram Categor, Violatioh.Action: PERMIT: NC0037508 FACILITY: Moore County Public Utilities- Moore County WPCF COUNTY: Moore REGION: Fayetteville Monitoring Violation MONITORING OUTFALL REPORT / PPI LOCATION PARAMETER 10 - 2001 ° 001 Effluent Copper, Total (as Cu) • VIOLATION DATE 10/31/01 FREQUENCY 2 X month UNIT OF CALCULATED MEASURE LIMIT VALUE VIOLATION TYPE ug/I Frequency. Violation 10 - 2001 001 Effluent Nitrogen, Total (as N) 10 - 2001 001 Effluent Phosphorus, Total (as P) 10 - 2001 001 Effluent Silver, Total (as Ag) 10 -.2001 001 Effluent Zinc, Total (asZn) Reporting Violation 10/31/01 Monthly 10/31/01 Monthly 10/31/01 2 X month 10/31/01 2 X month mg/I mg/I ug/I ug/I Frequency Violation Frequency Violation Frequency Violation Frequency Violation VIOLATION ACTION BIMS - - Pre -Production Violation BIMS Pre -Production Violation BIMS Pre -Production Violation BIMS Pre -Production Violation BIMS Pre -Production Violation MONITORING .OUTFALL REPORT / PPI LOCATION PARAMETER 11 - 2001 001 Effluent Cyanide, Total (as Cn) VIOLATION UNIT OF CALCULATED DATE FREQUENCY MEASURE LIMIT VALUE 11/30/01 2 X month ug/I VIOLATION TYPE 'Parameter Missing VIOLATION ACTION BIMS Pre -Production Violation -MONITORING REPORT(MR) VIOLATIONS for: Report Date: 02/12/04 Page: 1 of 1 Permit: NC0037508',1" 'rags Between 11 2002 {anted 1g 2fl03 ` Region % Violation.Category: % Program Category: % ;Facility Name: % ; ' : Param Name: % .County: % Subbasin: % Violation Action: % PERMIT: NC0037508 FACILITY: Moore County Public Utilities - Moore County WPCF COUNTY: Moore REGION: Fayetteville Monitoring Violation MONITORING OUTFALL VIOLATION UNIT OF CALCULATED REPORT / PPI LOCATION PARAMETER DATE - FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION - - 01 = 2003 001 -Effluent Chlorine, Total Residual 01/04/03 5 X-week - ug/I Frequency Violation None 01 - 2003 001 Effluent Coliform, Fecal MF, M-FC 01/04/03 5 X week #/100m1 Frequency Violation None Broth,44.5C 01 - 2003 001 Effluent Nitrogen, Ammonia Total (as N) 01/04/03 5 X week mg/I Frequency Violation None 11 - 2003 001 Effluent Nitrogen, Ammonia Total (as N) 11/29/03 5 X week mg/1 Frequency Violation None 12 - 2002 001 Effluent Silver, Total (as Ag) 12/31/02 2 X month ug/I Frequency Violation None 01 - 2003 001 Effluent pH 01/04/03 5 X week su Frequency Violation None Whole .Effluent Toxicity Testing Self -Monitoring Summary i..r_eb uary 16-2004; FACILITY _-_- REQUIREMENT YEAR JAN FEB MAR APR MAY JUN JUL AUG SEP OCT V'G'''-` DEC 3 `MooCefCobrity_W}VTp,,,.. chr lim: 41 % Y 2000 - Pass - - Pass - - Pass - - Pass NC0037508/001 Begin:6/I/2000 Frequency Q Mar Jun Sep Dec + NonComp Single 2001 - - Pass - - Pass - - Pass - - Pass County: Moore Region: FRO Subbasin: LUM50 2002 - - Pass - - Pass - - Pass - - Pass PF: 6.7 - Special 2003 - Pass - - Pass - _ - Pass - - Pass 7Q10: 15.2 1WC(% 40.54 1�20i Mt. Gilead WWTP chr lim: 3.2% 2000 - - Pass - - NR Pass - H Pass - Pass NC002I 105/001 Begin:3/I/2000 Frequency Q Mar Jun Sep Dec + NonComp Single 2007 - - NR NR Pass Pass - - Pass - - Pass ,County: Montgomery Region: FRO Subbasin: YAD10 2002 - - Pass - - Pass - - Lale Pass - Pass PF: 0.85 • Special 2003 - - Pass - - Pass, - - Pass - - Pass 7Q10: 40. IWC(%;3.2 2004 North Harnett Regional WWTP 24 hr Fthd p/fac lim: 90% NC0021636/001 Begin:10/1/2001 Frequency Q + Jan Apr Jul Oct County: Harnett Region: FRO Subbasin: CPF07 PF: 0.6 Special 7Q 10: 550.0 IWC(%; 0.17 + NonComp Single 2000 Pass - - - Pass - - Pass - - Pass 2001 Pass - - Pass - - Pass - - Pass 2002 Pass - - Pass - - Pass - - Pass 2003 Fail,Pass - - Pass - - Pass - - Pass 2004 Parkton WWTP - chr lim: 90% 2000 Fail Pass >100 Pass - - Fail 94.84 NR 82.13 35.36 35.36 NC0026921/00I Begin: I/12000 Frequency Q - Jan Apr Jul Oct +- NonComp Single 2001 82.16 - 82.16 - 35.4 94.9 - - - Pass - _ - Fail >100 35.4 County:Robeson Region: FRO Subbasin: LUM53 2002 >100 - - Pass - - Pass - - Fail . 94.9 <25 PF: 0.2 Special - 2003 <25 _ ___ _>100_-_33.5_ -Pass__ - _ - -Fail- -94.9- _- _>_100. Pass - _ ------- 7Q10: 0.0 IWC(%; 100 2004 Pembroke WWTP chr lim: 1.7% 2000 Late Pass - Pass - - Pass - - Pass NC0027103/001 Begin:6/I/2000 Frequency Q Jan Apr Jul Oct + NonComp Single 2001 Pass - - Pass - - Pass - - Pass County: Robeson Region: FRO Subbasin: LUM51 2002 Pass - - Pass - - Pass - - Pass PF: 1.33 . Special 2003 Pass - - Pass - - Pass - - Pass 7Q10: 114 IWC(%; 1.8 2004 Pass Raeford WWTP chr lim: 9% 2000 - Pass - - Pass - - Invalid - Pass Pass NC0026514/001 Begin:7/I/I996 Frequency Q P/1' + Feb May Aug Nov • NonComp Single • 2001 - Pass - - Pass - ' - Pass - - Pass County:Hoke - , Region: FRO Subbasin: CPFIS 2002 - Pass - - Pass - - Fail >18 >18 Pass PF: 3.0 Special 2003 - Pass - Fail 5.20 >18,Pass Pass - - Pass 7Q10: 49.0 ,. 11VC(%;8.67 2004 • Red Springs WWTP chr rim: 90% NC0025577/001 Begin:5/I/2000 Frequency Q Jan Apr Jul Oct - + NonComp Single County: Robeson Region: Rio Subbasin: LUM52 PF: 2.5 Special Effective 12/1/02, signed 12/27/02, expires 12/1/04 7Q10: 0.07 IWC(%; 98 2000 Late >90 - 17.7 <12.5 35.4 17.7 17.7 35.4 >90 17.7 35.4 2001 <72.5 61.2 82.2 >90 35.4 35.4 >90 82.2 <12.5 <12.5 61.2 Invalid 2002 Lale Lale >90 >90 82.2 35.4 >90 - >90 58.1 58.1 33.5 2003 <125 >90 33.5 >90 17.7 58.1 58.1 >90 >90 <12.5 17.7 33.5 2004 Robbins WWTP chr lim: 10% NC0062855/001 Begin:7/1/2002 Frequency Q Jan Apr Jul Oct + NonComp Single County:Moore Region: FRO Subbasin: CPFIO PF: 1.3 Special 7Q10: 15.9 . IWC(%; 10 2000 Pass 2001 Pass. 2002 Pass 2003 pass 2004 Pass - - Pass - - • Pass Pass - - Pass - - NR Pass - - Pass - - Pass Pass - - Pass - - Pass Pa- ss ,Rockingham WWTP . chr lim: 8% NC0020427/001 Begin:6/I/1999 Frequency Q P/F + Feb May Aug Nov + NonComp Single County: Richmond Region: FRO Subbasin: YAD16 PF: 9.0 Special 7Q10: 153 IWC(%; 8.0 2000 - Pass 2001 - Pass 2002 - Pass • 2003 - Pass 2004 - - Pass - - Pass - - Pass - - Pass - - Pass - - Pass - Pass - - Pass,>32 Pass Pass Pass Pass>32 Roseboro WWTP chr lim: 52% NC0026816/001 Begin:12/1/2003 Frequency Q P/F + Feb May Aug Nov County:Sampson Region: FRO Subbasin: CPF19 PF:0.49 . ,Special 7Q10: 1.0 I\VC(%; 52 NonComp Single 2000 - Pass - - Pass - - Pass - - Pass 2001 - Pass - - Pass - - Pass - - Pass 2002 - Pass - - Pass - - Pass - - Pass 2003 - Pass - - Pass - - Pass - - Pass 2004 Smithfield Packing Co, Tarheel Div. chr lim: 0.58% NC0078344/001 . Begin:12/12002 Frequency Q Jan Apr Jul Oct County:Bladen Region: FRO Subbasin: CPFI6 PF: 3.0 Special 7Q10: 795 IWC(1.,;0.58 + NonComp Single 2000 Pass - - Pass 2001 Pass - - Pass 2002 Pass - Pass 2003 Pass - - Pass 2004 - - Pass - - Pass - - Pass - - Pass,Pass - - - Pass - - Pass - - - Pass - - Pass - Y Pre 2000 Data Available LEGEND: PERM = Permit Requirement LET = Administrative Letter - Target Frequency = Monitoring frequency: Q- Quarterly; M- Monthly; BM- Bimonthly; SA- Semiannually; A- Annually; OWD- Only when discharging; D- Discontinued monitoring requirement Begin -= First month required 7Q10 = Receiving stream low flow criterion (cis += quarterly monitoring increases to monthly upon failure or N Months that testing must occur - ex.lan, Apr, Jul, Oct NonComp = Current Compliance Requirement PF = Permitted Bow (1%.113D) IWC%= Instream waste concentrate I'/F = Pass/Fail test AC = Acute CIiR = Chronic . Data Notation: f - Fathead Minnow; • - Ceriodaphniasp.; my-.Mysid shrimp; C'hV - Chronic value; P - Mortality or stated peteentage at highest concentration; at - Performed by DWQ Aquatic Tox Unit; bt - Bad test Reporting Notation: --- , Data not required; NR - Not reporte Facility Activity Status: I - Inactive, N -Newly Issued(T: construct): li - Active but not discharging; t-More data available for month in question; • = ORC signatmc needed 4 Whole Effluent Toxicity Testing Self Monitoring Summary FACILITY REQUIREMENT .P6b- arv:1 6-2000: YEAR JAN FEB MAR APR MAY JUN JUL AUG SEP OCT NOV DEC Lumberton WWTP PERM CHR LIM: 11%; UPON EXP CHR LIM 21% Y 1996 •-- Pass Pass Pass Fail NC0024571/001 Begin9/1/1994 Frcqucncy:QP/F + Feb May Aug Nov NonComp:SINGLE 1997 --- Pass Pass Pass Pass County: Robeson Region: FRO Subbasin: LUM51 1998 --- Pass --- Pass .-- --- Pass --- --- Pass PF: 10.0 • Spacal 1999 .-. .Pass Pass Pass Pass 7Q10: 120 - 1WC(%)11 Order: 2000 Pass(s) Monsanto/001,002 Perm 24hr p/f ac lim: 90% fthd (combined outfall) Y 1996 --- Pass --• Pass NC0003719/002 Bcgin 1/1/1996 Frcqucncy:Q P/F + Feb May Aug Nov NonComp:Singlc 1997 --- Pass --- Pass County: Cumberland Region: FRO Subbasin: CPF15 1998 --- Pass •-- Pass PF: 1.3 Special 1999 --- Pass --- Late -7QI0:791.0 IWC(%)0.25 Order:• 2000 Pass Pass --- - Pass • Pass --- Pass Pass --- Pass Fail Pass, ass --- Pass [Moore County WWTP-1 PERM CHRLIM: 41% Y i..1996,,--, C Pass Pass --- Pass 1NC0037508/001-.Beg n-11I/1995 Frequency:Q P/F + Mar Jun Sep Dec NonComp:SINGLE 1997 --- Pass --- Pass --- Pass County: Moore Region: FRO Subbasin: LUM50 ' 1998 Pass --- Pass Pass -•- Pass PF: 6.7 Special 1999 --- Pass --• Pass Late 7Q10: 15.2 IWC(%)40.54 Order: 2000 Pass Pass Late Pass Pass Mt. Gilead WWTP Perm chr lim: 3.2% (New perm 3/1/2000) 1996 --- Pass NC0021105/001 Begin I I/1/1994 Frequency:Q P/F -+ Mar Jun Sep Dec NonComp:SINGLE 1997 --- Pass County: Montgomery Region: FRO Subbasin: YADIO 1998 --- - Fail - PF: 0.85 - Spacial_ - - _ __ _ 1999 --- . _Pass 7Q10: 40 IWC(%)3.2 Order: 2000 Late --- Fail Fait --- -Fail - Pass- Fail Late Pass Late Pass Pass' Pass,Pass _-- Late Pass Pass - Pass Pass Pass National Mechanical Carbon Corp. Pcrm chr lim: 90% (Grab) 1996. Pass Pass --- Pass NC0060747/001 Begin 9/1/1996 Frcquency:QP/F ' + Jan Apr Jul Oct NonComp:Single 1997 Pass Pass --- --- Pass County:Harnett Region: FRO Subbasin:CPF18 1998 Pass Pass --- --- Pass PF: 0.026 Special 1999 Pass Pass --- --- Fail 7Q10: 0.0 IWC(%) 100 Order: 2000 Pass Pass Pass Pass Fail Pass Parkton WWTP PERM CHR LIM: 90% (New perm 1/1/2000) 1996 Pass --- Pass NC0026921/001 Begin I/1/1995 Frequcncy:Q P/F + Jan Apr Jul Oct NonComp:SINGLE 1997 Pass --- Pass County: Robeson Region: FRO Subbasin: LUM53 1998 Late Pass Late PF: 0.2 Special 1999 Fail Pass Pass 7Q10: 0.0 IWC(%) 100 Order- 2000 Pass NR/Pass Pass Pass Fail Pass Late Pass --- N R Fail,Fail Late Pass --- --- Pass Pembroke WWTP PERM CHR LIM: 1.7% 1996 Pass NC0027103/001 Begin 12/1/1994 Frequcncy:Q P/F + Jan Apr Jul Oct NonComp:SINGLE 1997 Fail County:Robcson Region: FRO Subbasin:LUMSI 1998 Pass PF: 1.33 Special _ 1999 pass 7Q10:'114 IWC(%)1.8 Order: 2000 Pass Pass Pass Pass Pass Pass Late Pass -•- Pass Pass --- Pass Pass Pass Pass Raeford WWTP ' Pcrm chr lim: 9% 1996 --- NR/Pass Pass 'NC0026514/001 Begin7/I/1996 Frequcncy:Q.P/F + Feb May Aug Nov NonComp:Singlc. 1997 --- Pass --- --- Pass County:Hoke Region:FRO Subbasin:CPFI5- - 1998 --- Late Pass --- Pass PF:. 3.0 Special 1999 --_ Late Pass --- Late _7Q10:49.0 IWC(%)8.67 Order. 2000 Pass Pass NR/Pass Pass --• .-- Pass Pass --- Pass Pass Pass Red Springs WWTP Pcrm chr lim: 90% 1996 82 35 <12.5 >90 >90 >90 >90 Late >90 --- >90 NC0025577/001 Begin 8/1/1995 Frequcncy:Q P/F + Jan Apr Jul Oct NonComp:Singlc 1997 82 N R 61 >90 - >90 --- 35.35 N R >90 County: Robeson Region: FRO Subbasin: LUM52 1998 Late Late Late ->12.5 >90 Late 35 61 >90 --- --- PF: 2.5 special 1999 35 >90 --- >90 --- --- 35 >90 --- >90 --- •7Q10: 0.07 IWC(%)98 Order: 2000 Robbins WWTP Pcrm chr lim: 9%; upon cxp 1.3MGD chr lim 10% 1996 Passl,Pess --- --• Pass,Passt Pass --- --- Pass NC0062855/001 Begin5/1/I997 Frcqucncy:QP/F + Jan Apr Jul Oct + NonComp:Singlc 1997 Pass --- Pass .-- Pass Pass County:Moore Region: FRO Subbasin:CPFIO 1998 Pass Pass Pass --- Pass PF: 1.0 Sisiel 1999 Pass Pass Pass Pass 7Q10: 15.9 IWC(%)8.9 Order. 2000 Rockingham WWTP Perm chr lim: 28%;upon rcloc Pee Dec R. chr lim 8% 1996 --- Pass NC0020427/001 Begin6/1/1999 Frcqucncy:QP/F + Feb May Aug Nov + NonComp:Single 1997 --- Pass County:Richmond Region: FRO Subbasin:YAD16 1998 --- Fail PF: 6.0 special 1999 -.. Pass 7Q10: 23.4 IWC(%)28.4 Order: 2000 Pass Pass --- Pass --- Pass Pass --- Pass Pass Pass - --- Pass - Pass Pass Pass Pass Y Pre 1996 Data Available LEGEND: PERM =-Permit Requircmcn LET = Administrative Letter - Tar Frequency = Monitoring frequency: Q- Quarterly; M- Monthly; BM Bimonthly; SA- Semiannually; A- Annually; OWD- Only when discharging; D- Discontinued monitoring m Begin =.First month required 7Q10 = Receiving stream low flow criterion (c + = quarterly monitoring increases to monthly upon failure or Months that testing must occur - ex. Jan, Apr, Jul, 0 NonComp = Current Compliance Requireme `PF = Perrnittcd-flow (MGD) IWC% = Instrcam waste concentrati P/F = Pass/Fail test AC = Acute CHR = Chronic . Data Notation: f - Fathead Minnow; • - Ccriodaphnia sp.; my - Mysid shrimp; ChV - Chronic value; P - Mortality of stated percentage at highest concentration; at - Performed by DWQ Aquatic Tox Unit; b Reporting Notation: --- = Data not required; NR - Not repor Facility Activity Status: I - Inactive, N - Newly Issued(To construct); H - Active but not discharging; f-More data available for month in question; = ORC signat 4 AT& NCDENR North Carolina Department of Environment and Natural Resources Michael F. Easley, Governor December 10, 2003 Dennis Brobst Moore County Public Works Director P. O. Box 1927 Carthage, NC 28327 Subject: COMPLIANCE BIOMONITORING INSPECTION Moore County Water Pollution Control Plant • NPDES. Permit No. NC0037508 Moore County Dear Mr. Brobst: William G. Ross Jr., Secretary Alan W. Klimek, P.E., Director Coleen H. Sullins, Deputy. Director Division of Water Quality Enclosed you will find a copy of the Compliance Biomonitoring Inspection report for the inspection conducted the week of December 1, 2003. The inspection included the same objectives as that of a routine Compliance Evaluation. Inspection (conducted on December 1 & 2) plus an Aquatic Toxicity (AT) test tio evaluate the biological effect of the facility's discharge on test organisms. As part of the inspection a tour of the Wastewater Treatment Plant was conducted. All observations and a .recommendation are in Part D. Summary of Findings/Comments of this inspection report. The results of the (AT) will be forwarded to you when the,Division of Water Quality (AT) Laboratory completes them. Additionally, plant effluent samples were taken at the WWTP outfall for the following parameters which are. currently in your. NPDES Permit: total phosphorus, ammonia as . nitrogen, nitrate as N, nitrite I as' N, TKN as N, zinc, copper, silver, total suspended solids, and five-day biochemical. oxygen demand. The results of' .these parameters will be forwarded to you when the Division of Water Quality Chemistry Laboratory completes the analyses. You and your staff are commended for your. continued efforts to comply with the NPDES permit. If you have any questions or comments concerning this report or require clarification on part(s) of this report, please feel free to contact me at 910/486-1541. Sincerely, Dale Lopez Environmental Specialist /dl Enclosures cc: James Delmo Frye, ORC Kevin Bowden, DWQ, ESB, ATU One NorthCarolina 225 Green Street — Suite 714, Fayetteville; North Carolina 28301-5043 1' ; , attire, Phone: 910-486-1541 1 FAX: 910-486-07071 Internet: www.enr.state.nc.us/ENR!!' An Equal Opportunity / Affirmative Action Employer - 50 % Recycled 110 % Post Consumer Paper United States Environmental Protection Agency Washington, D.C. 20460 EPA Water Compliance Inspection' Report Form Approved. OMB No. 2040-0057 Approval expires 8-31-98 Section A: 'National Data System Coding (i.e., PCS) Transaction Code NPDES yr/mo/day • Inspection 1 N 2 i s I 3 1 N00037s08 1 11 121 ' 03/12/ 01 1 17 181J If Type Inspector Fac Type 19I s 1 , 20 L-I 1 •1 11 I I I 1 I I I I 1 166 Remarks 211 I I I I I I I I I I I I l. 1 I I I 1 I I I I I I I I "I I I I "I Inspection Work Days . Facility Self -Monitoring Evaluation Rating B1 QA ----- 67 L 5.0 169 701 1 • • 71 Lai 72 U.. -------- ----------Reserved---- 731 I 174 751 1 I I -1 1 1 .1 80 Section B: Facility Data - Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include POTW name and NPDES permit Number) . Moore County WPCF 1060 Addor Road Aberdeen NC 28315 Entry Time/Date . 1 11I:00 N4 03/12/01 Permit Effective Date 00/06/01 Exit 03:'00 Time/Date ,PM 03/12/01 4 . Permit Expiration Date 04/07/31 Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s) James D Frye/ORC/910-281-3146/ James Frye//910-281-3146; dames Frye1/910-28-1-3146/ Other Facility Data . Name, Address of Responsible Official/Title/Phone and Fax Number Contacted Gary Frick, PO Box 813 Pine Bluff NC 283731/910-281-3146/. No Section C: Areas Evaluated During Inspection (Check only those areas evaluated) Permit Flow Measurement Operations &Ma;ntenance Records/Reports Self -Monitoring Program Facility Site Review . Effluent,/Receiving War_ers Section D: Summary of Finding/Comments (Attach:additional sheets of narrative land checklists as necessary) Recommendation: In order to reduce the algae buildup at the weirs o* the f nal1 replace the brushes of the Ford Hall brush assentbl.ias. The.following list t:F From la;e constitute an average of 0.2 to 0.3 MGD of flow that were subtracted `' reporting onto the DMRs: a) decant from the digesters, b) drainage from the dirying clarifiers, d) all waste activated sludge of MLSS from both the First Stage and rlr,r:ifiers, _lease repair or ..n•r.::lant wastewaters .,.ea. o-. main mete.- reading _ beds, c) scum from the (cont.) Name(s) and Signatures) of Inspector(s) Agericy/Office/Phone and Fax '—le Lopes FRO TQ/,•'J10 468-1'_41197.0-z86-070' / Numbers Date /0 A___ Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers ' Date �q . /2,h1`03 64„:44.60.p41.141 EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete. DESCRIPTION OF MOORE COUNTY WATER POLLUTION CONTROL PLANT: Moore County Water Pollution Control Plant is a Grade 1V Biological WPCS. The following is a brief facility description: raw sewage comes from twelve monitoring/metering stations (the furthest is Carthage), a Plant Influent sewage flowed through the mechanical center flow bar screen to the Grit Chamber (with aeration from blower), to two Primary Clarifiers (75 ft diameter by 10 ft deep), to the First Stage Aeration Basin (70 ft by 30 ft by 15 ft deep, four chambers with air diffusers, with approximately three hours of retention time), the chemical unit/building houses the blowers that supply the diffuser air to both the Primary and Secondary Aeration Basins, to the two Intermediate Clarifiers (90 ft diameter by 12 ft deep), the overflow from the Intermediate Clarifiers goes to the Second Stage Aeration Basins (90 ft by 30 ft by 15 ft deep, four chambers with air diffusers, with approximately four hours of retention time), the flow travels to two Final Clarifiers (105 ft diameter by 12 ft deep), the overflow from the Final Clarifiers goes to the Chlorine Contact Basin (30 minutes of detention time), the effluent is then dechlorinated with sulfur dioxide, and the dechlorinated Plant Effluent 001 (with an average of 200 micrograms per liter of chlorine) travels through a 36 inch diameter ductile iron pipe to the receiving stream, Aberdeen Creek. The waste activated sludge flows to two Anaerobic Digesters. The digested sludge is then pumped to 36 drying beds (each 100- ft by 44 ft). The dried sludge is hauled to a lined landfill in Anson County. SECTION D: SUMMARY OF FINDINGS/COMMENTS: PLANT TOUR-- 1. The following list of in-plant'wastewaters constitute an average of 0.2 to 0.3 MGD of flow that were subtracted from the main flow meter reading for reporting onto the DMRs: a) decant from the digesters (continuous flow), b) drainage from the drying beds (continuous flow), c) scum from the clarifiers (continuous flow), d) all Waste Activated Sludge (WAS) of MLSS from both the First Stage and the Second Stage Aeration Basins, e) any drainage from a tank or a unit when being cleaned. 2. Process control for the wastewater treatment plant was based on the following analyses: MLSS, turbidity, BOD, ammonia, alkalinity, pH, 30 to 60 minute settleometer, Sludge Age, F/M ratio, and the clarifier sludge blanket. The Primary Clarifier's sludge blanket is maintained at 2 ft or less, the Intermediate Clarifier's sludge blanket is maintained at 1 to 1'/2 feet of sludge blanket, and the Final Clarifier's sludge blanket is maintained between Y2 to 1- foot depth. The target for the lst and 2d stages was 1,800 mg/L to_2,000 mg/L. 3. The Plant Influent Fisher Porter Ultrasonic Flowmeter, located at the Parshall Flume, was calibrated on October 10, 2003 by ISI (within 2% error). It was noted that there was less than 2% error when the before and after calibration were compared. 4. The refrigerator at the Plant Influent was 3 degrees Centigrade, and the refrigerator at the Plant Effluent was 0 degrees Centigrade. 5. A Royce Model 711 Suspended Solids/Interface Meter analyzed the Mixed Liquor Suspended Solids (MLSS). 6. Each troughof the two final clarifiers was continuously brushed with a brush assembly (Ford Hall) that was attached to the scum arm. NPDES yrlmolday 3 I _1C0037508 111 121 03 / 12 /01 • Inspection Type 18LI (cont.) 1 Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) the Second Stage Aeration Basins, e) any drainage from a tank or a unit when being cleaned. The effluent DtiR for August 2003 was crosschecked.with the laboratory bench sheets and with the commercial laboratory report sheers. There were no discrepancies observed. The inspection of the areas rioted did. not- reveal any defec ences. - . LABORATORY INSPECTION: 1. Expiration dates of the pH buffers: pH 4 = January 4, 2005 pH 7 = September 2004 pH 10 = May 2005 2. The BOD incubator thermometer indicated 19.5 degrees Centigrade. 3. The operator measured Temperature and Dissolved Oxygen with a YSI meter. 4. TSS drying oven was 103 degrees Centigrade. 5. The pH meter was sloped daily with a three-point calibration technique using the 4, 7, and 10 pH buffers (the NPDES permit limit range is 6 to 9 pH). .• 6. The following were the NPDES parameters that were analyzed at the facility: Conductivity, Dissolved Oxygen, Temperature, Total Suspended Solids (TSS), Ammonia as Nitrogen, Fecal Coliforms, Chlorine residual, and pH. 7. The Plant Effluent 001 DMR for August 2003 was crosschecked with the laboratory bench sheets and with the commercial laboratory report sheets. There Were no discrepancies observed. RECOMMENDATION--- 1. In order to reduce the algae buildup at the weirs of the final clarifiers, please repair or replace the brushes of the Ford Hall brush assemblies. Name an\d Signature of Inspecto Agency/Office/Telephone Date Dale Lopez j�� .✓n ,, NCDENR/ Fayetteville/ (910) 486-1541 12/10/03 lataA A Section D: Summary of Findings/Comments Brief Facility Description: FACILITY SITE REVIEW No N/A 1. Treatment units properly operated and, maintained. No N/A 2. Standby power or other equivalent provision provided. Yes o N/A 3. Adequate alarm system for power or equipment failure available. 4. Sludge disposal procedures appropriate: No N/A a. Disposal of sludge according to regulations No N/A .b. State approval for sludge disposal received. Y21 No N/A 5. Sufficient sludge disposed of to maintain treatment process equilibrium. Y s No N/A 6. The ORC and Backup Operator are officially designated with NCDENR/DWQTraining and Certification Unit. No N/A 7. Adequate spare parts and supplies inventory maintained. No N/A 8. Plant has general -safety' structures such as rails around or covers over tanks, pits, or wells. No N/A 9. Plant is generally clean, free from open trash areas. No N/A N/A N/A No N/A No 10. Screening: , r a. Manual (M tlyi dCQ vi.,&- L) b. Mechanical (ec,'TtE FLOW 8.4,E ,Se iPc 4 c. Buildup of debris d. Screenings properly disposed of.. (S F ) 11'. Grit Removal: N/A a. Excessive organic content in the grit chamber N/A b. Excessive odors (4Ao N/A c. Grit poperly disposedof. ,0 G bA) 7y L4NP fit- Page 2 Yes Yes Yes Ye Yes e Yes Yes 12. N/A N/A N/A N/A N/A N/A N/A o N/A N/A N/A Yes No Yes No Yes No Yes No Yes No Yes No Yes No Yes No Yes Yes Yes Yes Yes Yes Yes Yes No Yes No Yes No Yes No N/A� N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Primary clarifier: a. Excessive gas bubbles b. Blackand odorous wastewater c. Poor suspended solids removed d. Excessive buildup of solids in center well of circular clarifier e. Weirs level f. Weir blockage g. Evidence of short circuiting h. Lack of adequatescum removal i. Excessive floating sludge j. Broken sludge scraper: 13. Trickling Filter: a. Trickling filter ponding(indicating clogged media) b. Leak at center column of trickling filter's distribution arms c. Uneven distribution of flow on trickling filter surface d.. Uneven or discolored growth e. Excessive sloughing of growth f. Odor g. Clogging of trickling filter's distribution arm orifices h. Filter flies, worms, or snails. 14. Activated Sludge Basins/Oxidation Ditches: a. Dead spots b. Failure of surface ,aerators c. Air rising in clumps d. Dark foam or bad color e. Thick billows of white, sudsy foam f. Air rising unevenly g. Excessive air leaks in compressed air piping. 15. Stabilization Ponds/Lagoons: a. Excessive weeds including duckweed in stabilization ponds b. Dead fish or aquatic organisms c. Buildup of solids around influent pipe d. Excessive scum on surface. • Yes No Page 3 'es Yes Yes Yes Yes Yes Yes --HE4(c i'iF/��.5 H/`iO A 6-noLG 16. Secondary Clarifier: %�o r �) A rev Jt/ i c f9G6'9E $ r)/t. D i)P r Yile aleos. N/A a. Excessive gas bub les on sur ace N/A b. Level overflow weirs N/A c. Weir blockage N/A d. Evidence of short circuiting N/A e: Excessive buildup of solids in center well of circular clarifier N/A f. Pin floc in overflow 041 1444 ,14; tzi' tta,t 1-;La.) N/A g. Effective scum rake • NIA h. Floating sludge on surface N/A i.. Excessive high sludge blanket N/A j. Clogged sludge withdrawal ports on secondary clarifier. 17. Filtration: Yes No N/Ai a. Filter surface clogging Yes No N/A b. Short filter run Yes No N/A c. Gravel displacement of filter media Yes No N/A d. Loss of filter media during backwashing Yes No N/A e. Recycled filter backwash water in excess of 5 percent Yes No N/A f. Formation of mudballs in filter media, 18. Chlorination Unit: Yes N/A a. Sludge buildup in contact chamber Yes T N/A b. Gas bubbles Yes T N/A c... Floating scum and/or solids o N/A d. Adequate ventilation of chlorine feeding room and storage area No N/A e. NIOSH-approved 30 minute air pack No N/A f. All standing chlorine cylinders chained iri place No N/A g. All personnel trained in the use of chlorine es No N/A h. Proper chlorine feed; storage, and reserve supply. 19. Ultraviolet radiation disinfection present and in use: I 20. Dechlorination: pNo N/A a.. Proper storage of sulfur dioxide cylinders e No N/A b. Adequate ventilation of sulfur dioxide feeding room es _ To N/A c. Automati su fur dioxide feed or-eedback control operating proper13 //4& .G6-2 Yes No N/A/A Yes No N/A Yes No N/A Yes No N ,/Ay 21. Aerobic Digester: a. Excessive foaming in tank b. Noxious odor c. Mechanical aeration failure d. Clogging of diffusers. No N/A No N/A Yes o N/A Yes N/A Yes Yes No NoN/A Page 4 22. Anaerobic Digester: Yes N/A a. Floating cover tilting No N/A b. Gas burner operative Yes Yes Yes 23. Sludge Drying and/or disposal: N/A a. Poor sludge distribution on drying beds N/A b. Vegetation in drying beds N/A ,c. Dry sludge remaining in drying beds No N/A d. Dry sludge stored on site No N/A e. Filtrate from sludge drying beds returned to front of plant N/A f. Sludge disposal through county landfill. N/A g. Sludge land applied. 24. Filter Press: 4 Yes No N A/A/ a. High level of solids in filtrate fromfilter presses or vacuum filters Yes No N/A b. Thin filter cake caused by poor dewatering . Yes No N/A c. Sludge buildup on belts and/or rollers of filter press Yes No /A d. Excessive moisture in belt filter press sludge cake. 25. Polishing Ponds or Tanks: Yes No /N a. Objectionable odor, excessive foam, floating solids, or oil sheens on water surface Yes No N/A b. Solids or scum accumulations in tank or at side of pond Yes No N/A, c. Evidence of bypassed polishing ponds or tanks because of low _.,/ capacity. -26. Plant Effluent: Yes N/A a. Excessive suspended solids, turbidity, foam, grease, scum, color, and other macroscopic particulate matter present Yes (j N/A b. Potential toxicity (dead fish, dead plant at discharge) No N/A c. Outfall discharge lineeasily accessible. 27 4 Flow Measurement: a. Proper placement of flow measurement device b. Flow meter calibrated 0'/3 o% 3 sby1 S'1)c edia4Atefil c. Buildup of solids in flume or weir d. Broken or cracked flume or weir e. Clogged or broken stilling wells f. Weir plate edge corroded or damaged g. Flow measurement error less than 10%. Page 5 No N/A No N/A No N/A No N/A 28. Sampling: a. Sampling and analysis completed on parameters specifiedby pemit b. Composite sample temperatures maintained at 4 degrees Celsius or less (but abovefreezing) during sampling c. Contract laboratory used for sample analysis d. Effluent composite samples obtained are flow proportional. RECORDKEEPING AND REPORTING es No . N/A 1. Records and reports maintained as required by permit. No N/A 2. All required information available, complete, and current. es No N/A 3. Records maintained for 3 years arid all sludge records maintained for.5 years. 0esNo N/A 4. Analytical results consistent with data reported on DMRs. 5. Sampling and analyses data adequate and include: , Aes No N/A a.. Dates, times, and location of sampling No. N/A . b: Name of individualperformingsampling e No N/A c. Results of analyses and calibration No N/A d. Dates of analyses No N/A e. Name of person performing analyses. 6 Monitoring records adequate and include: No N/A a. Monitoring charts kept for. 3. years No N/A b. Flowmeter calibration records kept for 3 years. GgeckCD 44)01)5T ao03� Ye,) No N/A 7. The pH meter is calibrated daily with two buffers and checked with a third buffer and properly documented. No N/A 8. Expiration dates of pH buffers adequate. No N/A 9. All thermometers used in NPDES.permit reporting is calibrated annually with an NIST certified thermometer or 'a traceable, thermometer annually and documented. No N/A 10. The following NPDES permit required parameters are analyzed on site: pH, Temperature, Dissolved Oxygen and Chlorine Residual. Yes No Page 6 es No N/A 11. The NPDES permit required parameter Total Chlorine Residual is analyzed by approved method. es No N/A 12. BOD incubator temperature maintained at 20 +/- 1 Degrees Celsius and the temperature maintained in a log for every day of operation. es No N/A 13. Fecal coliform incubator maintained at 44.5 +/- 0.2 Degree Celsius and the temperature maintained in a log for every day of operation. 14. Plant records adequate and include: No N/A a. 0 & M Manual No N/A b. "As -built" engineering drawings No N/A c. Schedules and dates of equipment maintenance repairs(A1/ R , ) Yes No. /A d. Equipment data cards. 15. Pennittee.is meeting compliance schedule: es No . N/A 16. DMRs complete and include all NPDES permit required parameters. es No N/A 17. The facility has a permitted flow greater than 5 MGD and is required to operate seven days per week 24 hours a day. No N/A 18. ORC visitation logs available and current. es No N/A 19. ORC certified at a level equal to or greater than the classification of the wastewater facility: es No N/A 20. Backup Operator certified at one level less than the classification of the wastewater facility or greater. es No N/A 21. Current copy of the complete NPDES permit on site. es No N/A 22. Facility description verified as contained in NPDES permit. es No N/A 23. Facility analyzes process control parameters for example: MLSS, MCRT, Settleable Solids and others that are applicable. No N/A , 24. Industrial Waste Surveys (IWS) sent to all possible Significant Industrial•Users (SIUs) within the last five years (especially new industries). Revised 7/16/01 by Belinda Henson AV;41i7rA NCDENR North Carolina Department of Environment and Natural Resources Michael F. Easley, Governor February 11, 2004 Phillip Boles Moore County Public Works Director 703 Pinehurst Avenue P.O. Box 756 Carthage, NC 28327 William G. Ross Jr., Secretary Alan W: Klimek, .P.E.,Director ColeenH. Sullins, Deputy Director Division of Water Quality Subject:. COMPLIANCE BIOMONITORING INSPECTION LABORATORY RESULTS Moore County Water Pollution Control Plant NPDES Permit No. NC0037508 Moore County Dear Mr. Boles: This - letter concerns the laboratory results of samples that were collected during the Compliance Biomonitoring Inspection that was conducted during the week of December 1, 2003. 24-hour Outfall 001 effluent composite samples were collected on December 2 and December 5 by Dale Lopez (DWQ-FRO) for use in a chronic Ceriodaphnia dubia pass/fail toxicity test. The Division of Water Quality Aquatic Toxicology Laboratory, located on Reedy Creek Road in Raleigh, completed the aquatic toxicity analysis. The test using these samples resulted in a pass, but these results should not be used for compliance monitoring purposes. The test was deemed invalid due to organism feeding criteria. Additionally, the Division of Water Quality Chemistry Laboratory (located on Reedy Creek Road in Raleigh) completed the testing of samples from the December 2nd 24-hour composite sample: Analyses Parameters Outfall 001 Total Suspended Solids (TSS) 12 mg/L NH3 as N • 0.02 mg/L TKN as N 1.4 mg/L NO2 plus NO3 as N 22 mg/L Total Phosphorus as P 2.6 mg/L BOD 0 12 mg/L 225 Green Street — Suite 714, Fayetteville, North Carolina 28301-5043 Phone: 910-486-15411 FAX: 910-486-07071 Internet: www.enr.state.nc.us/ENR/ An Equal Opportunity.! Affirmative Action Employer - 50 % Recycled t 10 % Post Consumer Paper NorthCarolina naturally Mr. Boles Page 2 February 11;2004 If you have any questions or comments concerning this report or require clarification on part(s) of this report, please feel free to contact me at 910/486-1541. Environmental Specialist /d1 cc: Kevin Bowden, DWQ, ESB, ATU James Delmo Frye, ORC, Moore County Water Pollution Control Plant Department of Public Utilities Wastewater Treatment Plant 1094 Addor Road Aberdeen, NC 28315 aanty February 10, 2004 P/gaaace Re: Results for EPA Expanded Requirements for Permit Renewal NPDES Permit No. NC0037508 Mrs. Valery Stephens NCDENR/D WQ/NPDES 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Mrs. Stephens: • Telephone: (910) 281-3146 Facsimile: (910) 281-2047 DENR-FRO Q� FEB 13 2004 I sent a letter with our plant permit renewal that we would run the Priority Pollutant Analysis and a Fat Head Minnow Toxicity in January.' We would then begin to piggy back tilte. remaining test with our regular quarterly testing starting in March: Please find enclosed'a copy of the results from January 2004. I will send you results for the remaining test as we receive them. If additional information is needed, please do not hesitate to call me at 910-281-3146. Sincerely James D. Frye, System Superintendent JDF/sab cc: Mr. Paul Rawls, Fayetteville Regional Office, DEM Mr. Charles Weaver, NPDES Unit Mr. Kevin Bowden, Aquatic Toxicology Unit Mr. Steve Wyatt, County Manager Mr. Phillip Boles, Director of Public Utilities at ENVIRONMENTAL SCIENCE CORP . Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 Ole REPORT OF ANALYSIS Date Received January 21, 2004 Description 13718 - Moore County WWTP 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 29, 2004 ESC Sample # : L141764-01 Site ID Sample ID EFFLUENT 0119122 Collected By Project # : TBL-13718 Collection Date : 01/19/04.09:05 Parameter Result Det. Limit Units (Method Date Dil. Cyanide BDL 0.0050 mg/1 3351.3 01/23/04 1 Hardness calcium — mg/1 Calc. 01/23/04 1 Total Phenol by 4AAP BDL 0.040 mg/1 1420.2 01/28/04 1 Thallium 0.0010 mg/1 200.8 01/22/04 1 Mercury BDL 0.,00020 mg/1 245:1 01/22/04 1 v BDL Antimony e,.o0811 0.0050 mg/1 200.7 01/22/04 1 Arsenic BDL 0.010 mg/1 200.7 01/22/04 1 Beryllium BDL 0.0020 mg/1 200.7 01/22/04 1 Cadmium BDL 0.0050 mg/1 200.7 01/22/04 1 Calcium 0.50 mg/1 200.7 01/22/04 1 Chromium /�` t BDL 0.010. mg/1 200.7 01/22/04 1 Copper 7 g�( Ooon � 0.010 mg/1 2007.;01/22/04 1 Lead fq / BDL 0.0050 mg/1 200.7 01/22/04 1 Nickel BDL 0.010 mg/1 200.7 '01/22/04 1 Selenium BDL 0.010 mg/1 200.7 01/22/04 1 Silver BDL 0.0050 mg/1 200.5 01/22/04 1 Zinc Iliaallil 0.030 mg/1 200.'7 01/22/04 1 PP Volatile Organics Benzene BDL 0.0010 mg/1 624 01/22/04 1 Bromodichloromethane - BDL 0.0010 mg/1 624 01/22/04 1 Bromoform BDL 0.0010. mg/1 624 ' 01/22/04 1 Bromomethane BDL 0.0010 mg/1 624 01/22/04 1 Carbon tetrachloride BDL 0.0010 mg/1 624 '01/22/04 1 Chlorobenzene BDL 0.0010 mg/1 624 01/22/04 1 Chlorodibromomethane BDL 0-.0010 mg/1 624 , 01/22/04 1 Chloroethane BDL 0.0010 mg/1 624 01/22/04 1 2-Chloroethyl vinyl ether BDL 0.050 mg/1 624 01/22/04 1 Chloroform BDL 0.0050 mg/1 624 01/22/04 1 Chloromethane - BDL 0.0010 mg/1 624 61/22/04 1 1,2-Dichlorobenzene BDL 0.0010 mg/1 624 01/22/04 1 1,3-Dichlorobenzene BDL 0.0010 mg/1 624 01/22/04 1 1,4-Dichlorobenzene BDL 0.0010 mg/1 624 01/22/04 1 1,1-Dichloroethane BDL 0.0010 mg/1 624 01/22/04 1 BDL - Below Detection Limit ' Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL-1E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 1 of 6 ENVIRONMENTAL SCIENCE CORP . Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 Date Received Description Sample ID ' Collected By, . Collection Date : Parameter REPORT OF ANALYSIS January 21, 2004 13718 - Moore County WWTP EFFLUENT 0119122 01/19/04 09:05 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 29, 2004 ESC Sample # : L141764-01 Site ID . Project # : TBL-13718 Result Det. Limit Units Method Date Dil. 1,2-Dichloroethane BDL 0.0010 mg/1 624 01/22/04 1 - 1,1-Dichloroethene • BDL 0.0010 mg/1 624 01/22/04 1 trans-1,2-Diehloroethene BDL 0.0010 mg/1 624 01/22/04 1 1,2-Dichloropropane BDL 0.0010 mg/1 624 01/22/04 1 cis-1,3-Dichloropropene BDL 0.0010 mg/1 624 01/22/04 1 trans-1,3-Dichlbropropene BDL 0.0010 mg/1 624 01/22/04 1 Ethylbenzene BDL 0.0010 mg/1 624' 01/22/04 1 Methylene Chloride BDL 0.0050 mg/1 624 01/22/04 1 1,1,2,2-Tetrachloroethane BDL 0.0010 mg/1 624 01/22/04 1 Tetrachloroethene BDL 0.0010 mg/1 624 01/22/04 1 Toluene BDL 0.0050 mg/1 624 01/22/04 1 1,1,1-Trichloroethane BDL 0.0010 mg/1 624 01/22/04 1 1,1,2-Trichloroethane BDL 0.0010 mg/1 624 01/22/04 1 Trichloroethene BDL 0.0010 mg/1 624 , 01/22/04 1 Vinyl chloride BDL 0.0010 Sur-r` Vinyl , mg/1 624 01/22/04 1 Toluene-d8 i:.:.(r!t J+ L CO Rec. 624 01/22/04 1 Dibromofluoromethane °-Ig0 % Rec. 624 01/22/04 1 4-Bromofluorobenzene % Rec. 624 01/22/04 1 Pesticide/PCBs 1 Aldrin BDL 0.00050 mg/1 608 01/24/04 1 Alpha BHC BDL 0.00050 mg/1 608 01/24/04 1 Beta BHC BDL 0.00050 mg/1 608 01/24/04 1 Delta BHC BDL 0.00050 mg/1 608 01/24/04 1 Gamma BHC BDL 0.00050 mg/1 608 01/24/04 1 Chlordane BDL 0.0050 mg/1 608 01/24/04 1 4,4-DDD BDL 0.00050 mg/1 608 01/24/04 1 4,4-DDE BDL 0.00050 mg/1 608 01/24/04 1 4,4-DDT BDL 0.00050 mg/1 608 01/24/04 1 Dieldrin BDL 0.00050 mg/1 608 01/24/04 1 -Endosulfan I BDL 0.00050 mg/1 608 01/24/04 1 Endosulfan II BDL 0.00050 mg/1 608 01/24/04 1 Endosulfan sulfate BDL 0.00050 mg/1 608 01/24/04 1 Endrin BDL 0.00050 mg/1 608 01/24/04 1 Endrin aldehyde BDL 0.00050 mg/1 608 01/24/04 1 Heptachlor BDL 0.00050 mg/1 608 01/24/04 1 Heptachlor epoxide BDL 0.00050 mg/1 608 01/24/04 1 Hexachlorobenzene BDL 0.00050 mg/1 6:08 01/24/04 1 BDL - Below Detection. Limit. i Det. Limit - Estimated Quantitation Limit(EQL) I Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FLi EB7487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN -12006, VA - 00109, WV - 233 Page 2 of 6 'ENVIRONMENTAL S C I ENCE CORP . Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 PP Base/Neutral Extractables 1 Acenaphthene BDL 0.010 mg/1 625 01/23/04 1 Acenaphthylene BDL 0.010 mg/1 625 01/23/04 1 Anthracene BDL 0.010 mg/1 625 01/23/04 1 Benzidine BDL 0.050 mg/1 625 01/23/04 1 Benzo(a)anthracene BDL 0.010 mg/1 625 01/23/04 1 Benzo(b)fluoranthene BDL 0.010 mg/1 625, 01/23/04 1 Benzo(k)fluoranthene BDL 0.010 mg/1 625 01/23/04 1 Benzo(g,h,i)perylene BDL 0.010 mg/1 625 01/23/04 1 Benzo(a)pyrene BDL 0.010 mg/1 625 01/23/04 1 Bis(2-chlorethoxy)methane BDL 0.010 mg/1 625 01/23/04 1 Bis(2-chloroethyl)ether BDL 0.010 mg/1 625 01/23/04 1 Bis(2-chloroisopropyl)ether BDL 0.010 mg/1 625. 01/23/04 1 4-Bromophenyl-phenylether BDL 0.010 mg/1 625' 01/23/04 1 2-Chloronaphthalene BDL 0.010 mg/1 625' 01/23/04 1 4-Chlorophenyl-phenylether- BDL 0.010 mg/1 625 01/23/04 1 Chrysene BDL 0.010 mg/1 625 01/23/04 1 Dibenz(a,h)anthracene BDL 0.010 mg/1 625 01/23/04 1 3,3-Dichlorobenzidine BDL 0.010 mg/1 625 01/23/04 1 2,4-Dinitrotoluene BDL 0.010 mg/1 625 01/23/04 1 2,6-Dinitrotoluene BDL 0.010 mg/1 625 01/23/04 1 Fluoranthene BDL 0.010 mg/1 625 01/23/04 1 Fluorene BDL 0.010 mg/1 625 , 01/23/04 1 Hexachlorobenzene BDL 0.010 mg/1 625 01/23/04 1 Hexachloro-1,3-butadiene BDL 0.010 mg/1 625 01/23/04 1 Hexachlorocyclopentadiene BDL 0.010 mg/1 625 01/23/04 1 BDL - Below Detection Limit I Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 1-2327, CT- PH-0197, FL -; E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN-'2006, VA - 00109, WV - 233 Page 3 of 6 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 29, 2004 Date Received January 21, 2004 ESC Sample # L141764-01 Description 13718 - Moore County WWTP 1. Sample ID EFFLUENT 0119122 Site ID Collected By Project # : TBL-13718 Collection Date : 01/19/04 09:05 Parameter Result Det. Limit Units ;Method Date Dil. Methoxychlor BDL 0.00050 mg/1 608 01/24/04 1 ToxaphenePCB 1016 BDL 0.010 mg/1 608 01/24/04 1 PCB 1221 BDL 0.00050 mg/1 1608 01/24/04' 1 BDL 0.00050 mg/1 :608 01/24/04 1 PCB 1242 PCB 1232 BDL 0.00050 mg/1 1608 01/24/04 1 PCB 1248 BDL 0.00050 mg/1 ,608 01/24/04 1 BDL 0.00050 mg/1 !608 01/24/04 1 PCB 1254 BDL 0.00050 mg/1 608, 01/24/04 1 PCB 1260 BDL 0.00050 mg/1 1608 01/24/04 1 Pest/PCBs er at Decachlo'r`oben `1 p y MINt 0.00050 % Rec. 1608 01/24/04 1 Tetrachloro-m-xylene q2M10 0.00050 % Rec. 1 608 01/24/04 1 ENVIRONMENTAL SCIENCE CORP . Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 Date Received Description Sample ID REPORT OF ANALYSIS January 21, 2004 13718 - Moore County WWTP EFFLUENT 0119122 Collected By Collection Date : 01/19/04 09:05 Parameter Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine Phenanthrene Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene PP Acid Extractables 4-Chloro-3-methylphenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol �rrdga eta et Recovery Nitrobenzene-d5 2-Fluorobiphenyl p-Terphenyl-d14 Phenol-d5 2-Fluorophenol 2,4,6-Tribromophenol 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 , 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 29, 2004 ESC Sample # : L141764-01 Site 'ID . I ' Project # : TBL-13718 1 , Result Det. Limit Units [Method BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL 0.010 mg/1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - KY - 90010, KYUST - 0016, NC - ENV375,DW21704, Note: The reported analytical results relate only to This report shall not be reproduced, except in Reported: 01/29/04 09:13 Printed: 01/29/04 09:13 % Rec. % Rec. % Rec. % Rec. % Rec. % Rec. 1625 I625 ,625 1625 I,625'„ 1625 1625 625 625 625 625 6251 625, 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 1 625'1 625 I Cheli Boucher, Date Dil. 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04 01/23/04, 01/23/04 01/23/04 JL� ' ". 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 ESC Representative Certification Numbers: j 1-2327, CT- PH-0197,'FL-,E87487, GA - 923, IN - C-TN-el ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 the sample submitted. full, without the written approval from ESC. Page 4 of 6 Attachment A List of Analytes with QC Qualifiers Sample # L141764-01 Analyte , Qualifier Chloromethane J4 Vinyl chloride J4 Benzidine J3 Isophorone J4 Benzylbutyl phthalate J4 4,6-Dinitro-2-methylphenol J4 Cyanide W 4,4-DDE J4 Tetrachloro-m-xylene J2 Page 5 of 6 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning J2 J3 Surrogate recovery limits have been exceeded; values are outside lower control limits The associated batch'QC was outside the established; quality control range for precision. J4 The associated batch QC was outside the established for accuracy. W (ESC)-The laboratory analysis was from a sample container Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detaildd,ihformation concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unless qualified as 'R' (Rejected). quality control range collected in an improper Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. Control Limits 2-Fluorophenol 31-119 Nitrobenzene-d5 43-118 Dibromfluoromethane 79-126 83-119 Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 81-114 82-116 2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 65-129 72-126 TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 6 of 6 TBL Laboratory 2401 West 5th Street Lumberton,NC 28359 Report. Phone(9 1 0) 738-6 190 (910) 671-8837 -- Collected by: (print): Collected by (signature): Sample ID 'Matrix: SS - Soil/Solid GW marks: elinquished by. (Signature) elip by: (Sign Prrrjec tame: 0e3r2_ CJiI Project.H. TTTBL :1:37 IDH: !Rush?' ( Lab MUST Be Notified ) Same Day 200% Next Day. 100% Two Day.. 50% Comp/Grab Matrix' 1_,OLAD Depth Alternate billing information: -ESC Key: P.0.11: '73 D Results Neerfrrl: FAX? No_Y•r; I Dale iltatH Analy sis/Container/Preserva(ive cr vf a; • kr) 3 I _v71 z ( wi I .31 7,1 • • -- I ()( 05 / )(1 )1: )4!. )( roundwa ter WW - VVasteWa ter DW - Drinking Water 01.- Dale: °AMA Dale: L-42/11 Dale: -.2O-8/ • )C Time: Recee by: (Signalu Time: Received for 613-by (Si3”,70 it, lu. FedEx 1Cou ier I emp: Dale: Bottles Received: ( 1 ime: Chain of Custody Page of Prepared by: 4/11. ENVIIZONI1TENTAI, SCIENCE CORI'. I 2065 Lebanon Road NIL Juliet. TN 371)2 Phone (615) 758-5858 _Phone (800) 767-5859 FAX (615)78-5856 CoCode: TIILLAB Ternplate/Prelogin Cooler #: Shipped Via: Remarks/Conlarninant (lab use only) Sarnple fl (lab only) LILL t-764e4 N 0C .) r I? I: f,171?-1.. , 2_ sY Ey. A L. N T l'emp Other Condition: pH Checked: 1 NCF: 9 TBL Laboratory 2401 West 5th Street Lumberton,NC 28359 Alternate billing information: Report. 4'ef Phone(910) 738-6190 FAX: (910) 671-8837 ' Collected by: (print): Proirme: (Dor4a, CD(...7)1 Client Project #: ESC Key: -T8L- 13-7 18 Site/Facility ID#: Collected by (signature): 'Rush?' (.Lab MUST Be Notified) Same Day 200% Next Day. 100% Two Day. 50% Sample ID Comp/Grab Matrix' Wk.,0 Depth ci—c-5' 3 Date Results Neefiffl: FAX? _.No_Y:?, -I CO'S Anay sis/Container/Preservative -40 . Ct • 2e1,; `XI w • A-! r6 ! v); E : co • Ai ! Date _ M 0165 i X )1 'Matrix: SS - Soil/Solid GW, elinquished by. (Signature alinq by: (Sign re) d b0Signature) th roundwa ter Date: AVA Date: Date: WW - WasteVVa ter DW - Drinking Water 07' . Time: 1 Receilec by: (Signatu e:. Tinie: /1 Time: 1 ed Received for lab by: (Signature) L L Chain of Custody Page of Prepared by: 4/11' ENVIRONMENTAL SCIENCE CORP. 12065 Lebanon Road Mt Juliet, TN 37122 Phone (615) 758-5858 Phone (800) 767-5859 FAX (615) 758-5859 CoCode: TIILLAB (lab use only) Template/Prelogin Cooler #: Shipped Via: Remarks/Contaminant 0 I U Sample # (lab only) 1 r,3 r • z l!71 7.147TY.ii pl I Flow ()tiler S5iiifilsTeliirriTd via: LI UPS FedEx Courier Li -_______._•_____ Temp Ternp: Bottles Received: 9 Condition: (lab use only) ' . Date: Time: pH Checked: 1NCF: "y Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:1/30/2004 x Facility: Moore County WWTP Laboratory: Meritech, Inc. IPDES # NC0037508 Pi Signature of Operator in Responsible Charge Signature of Laboratory Supervisor pe #: County: Moore Comments [ P MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 1/20/2004 / 11:45 AM % Eff. Control Repl. Surviving # Original # Wt/original (mg) 10.25 Surviving # Original # Wt/original (mg) 20.5 Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 411 61.5 Surviving # Original # Wt/original (mg) 82 Surviving # Original # Wt/original (mg) Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration pH (SU) Init/Fin DO (mg/L) !nit/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (°C) 'est Organisms 1 2 3 Avg Wt/Surv. Control 10 10 10 10 10 101 10 10 0.327 0.340 0.248 0.288 10 10 10 10 10 10 10 10 0.297 0.311 0.340 0.289 8 10 8 10 10 10 10 10 0.207 0.287 0.270 0.302 10 8 8 9 10 10 10 10 0.278 0.252 0.251 0.273 9 8 9 8 10 10 10 10 0.271 0.273 0.276 0.276 6 6 5 5 10 10 10 10 0.255 0.215 0.197 0.208 0 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) (0.3011 1100.0 [0.301 100.0 0.3091 1 90.01 0.267 87.5 0.264 185.01 0.274 55.0 0.2191 1 2 3 8.08 / 8.06 8.08 / 8.06 8.09 / 8.08 8.09 / 8.08 8.07 / 8.05 7.98 / 8.00 7.81 / 7.87 / 7.78 / 7.08 7.80 / 7.11 7:61 / 7.06 7.65 / 7.07 7.81 /7.127.87/7.117.72,/7.13 / 25.0 / 24.8 25.0 / 24.8 25.0 / 24.7 25.0 / 24.7 25.0 / 24.8 25.0 / 24.8 25.0, . / 24.8 / 0 1 2 3 7.63 / 7.86 7.61 / 7.83 7.65 / 7.90 7.63 / 7.88 7.21 / 7.83 7.90 / 7.80 ,7.76 : / 7.78 / 7.91 / 7.15 7.94 / 7.16 8.01 / 6.98 8.04 / 7.00 7.92 / 7.08 7.88 / 7.00 17.73 ' / 6.98 / 25.0 / 24.9 25.0 / 24.8 25.0 / 24.8 25.0 / 24.7 25.0 / 24.8 25.0 / 24.8 125.0 / 24.7 / 1 2 3 1/18/2004 1/19/2004 1/22/2004 24.00 24.00 .24.00. 466 . 450 446 <0.1 <0.1 <0.1 0.2 0.2 0.2 Cultured In -House r Outside Supplier F Hatch Date/Time 1/19/2004 / 2:30 PM Normal Hom. Var. NOEC LOEC ChV Method Crit t/rsum Conc. 10.25% 20.50% 41.00% 61.50% 82.00% Survival Growth IrI ICI 41.00% 62% 62% 82% 50% 71% Steel's Dunnett 10 2.41 Calc t/rsum 18• -0.4244 ' 14 1.7101 12 1.8599 10 1.3356 10 4.0943 Result Pass Fail ChV 50% DWQ Form AT-5 (8/03) MERITECH Chronic Fathead Minnow Benchsheet Transfer and Feeding Dates and Times Test Initiation Data: Start Date: 1- Start Time: Initials/Signature: s•Li Date/Time Fed Date/Time Born ;j. ,• .1.2 • a Transfer Date Time Initials Day 1 Day 2 1••,)..),.0%.4.. Day 3 1•4?-;.-.•,, Day 4 Day 5 -t • - Test Termination Data: Initials/Signature: 723- End Date: 1. :0 -01„... • End Time: octS• # of Organisms per Chamber: i Q.) . Test Vessel Size: c1-"....9 Test Solution Volume: . Temp. of Stock: # of Reps: LI Date Time 1 Day 0 i •;•10- ip14 Day 1 I -a., 1-•;,1-• Day 2 I tly,•1 Day 3 1-T“,, Facility ()I'D° rci_ NPDES Dilution Water:SA-;1$11. Randomization: NO Incubator #: Feeding Initials • Time 2 Day 4 l.1%4 - Day 5 • -;.•••••i, Day 6 4'7,3 Initials Time 3 Initials MERITECH, INC. ;Ur FISH LARVAL SURVIVAL/pROWTH DATA SHEET CHRONIC FATHEAD MINNOW FACILITY: Ork.r,rc NPDES #: cc)c) DATE OF TEST: -o-o- 11-,474 DATE WEIGHED: i -;•;`.3-- C4 ORGANISM: Pt‘A,kreci'ht;.:)l,k CONC r • ) • REP. A B D A B D A B D !•• PAGE OF OUTFALL: • INITIALS: FOIL WT. (nig) FOIL WT. + ORG. (mg) \ D. f."-; o WT. OF ORG. (mg) # ORG. I 0 MEAN WT/ ORG. (mg) 0 c.T3s(0 (6 , 7 rg c6 D\LjOJ < 0 • - • • r. 0 Z,Sk,9 u-1 7-P, 86). t) S. On, •?- \.4.0 Y.)). • 10 10 10 ,f) SURV % 100 Cio 0.L.)40 0- • - 6. oo s MERITECH, INC. FISH LARVAL SURVIVAL/GROWTH DATA SHEET CHRONIC FATHEAD MINNOW I' FACILITY: .1 NPD.ES #: l`.ir.E-)' DATE OF TEST: DATE WEIGHED: 1.a-t• ORGANISM: P!,�.:�,i CONC REP. A B C D A B C D A B C D PAGE i`j= OF a. OUTFALL: INITIALS: FOIL WT. FOIL WT. + WT. OF # ORG. MEAN WT/ (mg) ORG. (mg) ORG. (mg) ORG. (mg) )04cs )I l 11- (. S-r) v i , . c_\ • Yc3 • S-4. 9D- • Jr/ • i :' • • ii • ii irT,C.„) tl t Conc. I r.�t3:-• f. I I 1 2 i 1 T l o l° I C I 1 ,Renarks ramp. initial la 1.=1I.riC--- I._.,:-r. I I-,, (..) 174 .`c ti. 1 1 + I Final. IU ,. I:.t,to:�. I.-.,..1: 1::.,;.s., 1:,!-4.�s 1��: r )��i:`� u . 0. In i ti a 1 11-1. Fk-24.. I-?gi b..1),,;CI. ti. - 7. , i n a I .;-.\ i% t: -[ l (Ti: 1- 1'i::-�... 177.1E 2 1" f. t I :�-10 I 17':.; , 1=,,�:, i ::. I cil:--i_:_ I �=��= I i. ci =I 7. ,-;1.)1 �ina.I 1 cc. I=T=ci 1,�P:,. IE3c )- I �.�?91'7, ,=(t;� ^t l 14, s3 I 1 Atir. a i i n i iy 1• 1 1 1 1 1 1 1 f 1 Hardness I • I I .I r.Dn.dut t Tn.; eia 1 I'=:7 () Ia,', 7 I;Ai n 1 3,? I -.e!Sc, D Ic.•:.> `a 1 _:al ITS 1.-. 13767 I`C,_: -11.•m r 13_s« .I TV) I-'" Res. .. Chlorine or, ne Ir t 11 t l 4.o: t I.• n. 1 14,0.1 I tr.: 4i I Lc 1. I ' Conc. .ierp �;. 11 1 2 1 3 1 6 1 I I . ,. i.:'� '�` I I _ I / I P. mil l r k S Initial1,1• I e :7 fr I..�.'•>..a I_°,-•C> • I).a- & I -6 . J I Fill?-1 I o .i 1 iC' 3-.- . L_''Dtk ,. 1^Z� 1 i,). J. ��-: I �.�, �� I � i � (�._. �' (.:L.E �(-: i• n art:~, ! n i i a 1 1"4r. ,. I .T5?-a- I' 1'--i�.,y I .t"c- I.'r?; 1 7, S�I 1`• i';1 i-i n a ► 1 , ;;+. 1.)-‘2-, I --1—,7 - . I -<<.' I ; 1. 1 '7-1 0 I - . I 1` I >%c , 1 •'. --1 :: 1 r•';'. I>,-4 i I'V t.(;.— I 7.7 71 ,` fi n a l 1-.- c='.. i-7)= �r I '+`-�.ci I i. I t • L_ I F� . �=''' C, 'i a!i,n1:y 1 I :� I • D 1 I rlard ness I I 1 I I I I Cond,, t, . ;En ti a l l L 0 I "i 't' i A}: ,. I hF '-f 1 .:- 1- > 0 1. 1 "7 I Chi i ne Ie:_,z: I I:'.; 1 .;•;-, I'_ I ,^t. i <-..:.y i 1> > 1 pH initial MERITEC Chenical DB r i n3 tons Facilityn`,cc;:-a ;r< NPDES fi,� y��Sc :Test Datesl: ; Start r JC:r,.iEnd L Test Organism: it. Analyst Test Time: E _ Start ;;u�;�-E rd <:;•�;>i-_ Conc. Temp. 1 Day I I .3 I ,,, ,,, t (' i 1? Y I f o( 7 i Remarks 4 � Initial I, .i'� .. .o I I. Z ' 1 C '-^i`{;S L�4�. �': I;.`r'..t.. � 1�=r ',: 1.�ti.. .tip I ?..-. l' -1 • I ..),,: C? I J.U. ins Lial 1 T->r 1`RF.) 1 Il` k- I= ' 1 tl7 17.7..RI I »; 1 -\ t IH "y+,, I 'c I'!.!� 11, I i 1 I- 1 pH Initial I:- ; 1`; `=: I` :i. •IGC Ico l 7 'cri" -7S l 1 Alkalinity Final ( =. i ) I Pa192 IF. P c-1 <ri 1`.'{-'{� 1 I` 1 1 1 1 1 • I 1 11ardness . I La_ I ) t4,4._ I . I L i I I I Conduc:.lnitialI.^:LID' la ..3I:Z:rO 1�i'i:k 13.11:t I l>-3.1 ,".) ) _ ~final 1 _� 1 _ C.-it)! 3tJ�I:ri7 2- D `I `` 1 • Res. Chlorine f : I --, t I r 1 ',o. 0110,E I I'-..i_ s � tom: �t 1 4.:'. i �; 7 � - •! I ! .�� . 1 II , ai./^i. Final tina► Day aH Initial Day ChetiCa1 _ fa. Physical cal Dei.a_m inn .ions Facility ^::..._.� i 1 r~- NPDES fis`Jrsr eYr,:Test Dates Test Sta-rt�"�rs:� End,•,1�, ;�-- Organism: ,�; �: analyst Test Time: Start)1kice,:- 1 Day Conic . i 4 L. !: I, I 1 2 1 3 1 4 1 Temp. Ini tttlal I 1 '?4';7 1 1 $.� Final I ` -f.{--6 1 is-;r. 1 •1,;< 1 }rtich I).O. n�l.,.1aI s-se; 1•41.2?s rival H !n1 7-1aI I'T== I f :.. -, 1:41, 1 I 1 1 I I Final Alkal1n77:y Hardness I- -5:; 17, (Y Conduct. Initial! 1 " ; i ,9,b 1 .1"2,:.),:1, I Final 1.5�ii 1 • '7't}13 Ieti13u I,L`C. Res. Chlorine 1:.-J. kJ:), I •c;t r. 1 ::. k 0 1 / • ,D I . 1. 1;c:c 1 7.7S1 7:cf el I 1 I I(-17..)1 Remarks I Day. 1 Conc. i-,i r.:T.'.t. I I I 2 I 3 1 4 1 5 1 5 I/ 1 Te_mp. Initial 14:••, I z_•,:`> I_a.�,. IDS. I i'<l 1.-'.-0 I. .OI Final: I i-' , I :3.r-1 I ):. - 1-_I.,.,.. 1 4 1=�&2$ ;1 . Y 1 -f " D..0. In.1tjal 1", ): t l4--4.- Il .1,.. I,<<-'1 1 r,C.?79?.7I 1 FinaI I:i-Zp/:h ., PH Initial 1- - 1:I: �4 1::1•J,.-I -1 r� 1',3. I`I. )--I .-7S 1 r i na.l 1• '. 1'V='I c:� I =';c;°Z 1::ci). 1-7 .. 7- I r . .c"17)-, - Afkaiinity 1' 1 1.1 1 1 1 1 Hardness ! 1 ! .1 1 1 1 Conduct Initial =, ':? I a ,t'7 I ( 3l :3 1:�1r,i; 1..-`;^isi 4 I m��S' 1 _final I:�`i 7; 1'39i'0 l ice; 1.t- i3 , I IIF='" I Rag. Chiorine 1�_�:_€, I C.3>>1 i'.-Ci./i. I'LK.).1 I! J,1 1L:.t Remarks 1 1 .) r Day , 2' n'='MD. . ini t_c1!_.,Cj : 1 3• ..11 4! 5 1 0 1/ 1 Remarks Final I r;,: , 1�...4.( i.1 . O. i n i l a) L..r i S, 1• ;a'I i �-i final 11)'t I.1- i i„ DH Initial Final II,`�h:?. ��t-i �� ..�'!•:� 1a `:1 1)-9 "L3 1 1 lSt-Ai I`;:°ca li,1, 'z;I7.7' I ( iri 1"):vc) 1 'i 1.-<4I i�L11 : `fir' I I'__� I' 17• :(pi "x1 14' 1 'ikai,nity 15;; I I I'` 1 1 1 Hardness Imo?„ i Si.;- I I I 1 1 Conduct . 7n 4 t := 42.0 I1?'h7i` I 4001ur_:z 1;(--7 4 1 Li. 1 Fin a1 1ti J 1 lc 1 I.I. I j r i h I1 h -I I _l+•�F I U`71._i I14.;I`-' 1 :?es. C^l or Tie. 1 // rf I L t;',. ILL--,, I/.J),. If;,.`{ I, =..? I / . 11 MERITECH Mortality Data: Chronic Fathead Test Start Date/Time I + s. ;, . End Date/Time Concentration Co.-, Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 Rep #2 Rep #3 Rep #4 Concentration i( --,I5 • ., Day 0 Rep #1 t2 Day 1 L) 0 a e_ Cs) 0 0 2 0 Day 2 Day 3 Day 4 Day 5 Rep #2 4,�� �"� 6.) ( (1) t Rep #3 CJ ( .i C) 0 o (__1 Rep #4 i �) CD Concentrationi;•c J, Day6 Day7 f ) Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 \.J C1 () ( ( ) Rep #2 Rep #3 if.---) j Rep #4 (1 0 J C) cT ; �. 0 MERITECH Mortality Data: Chronic Fathead Test Start Date/Time End Date/Time Concentration L1•. Day 0 Day 1 Day 2 Day 3 Day 4 Day5 Day 6 Day 7 Rep #1 0C) • Rep #2 0 f--- C) Rep #3 0 (7) (') Rep #4 0 (1) 0 ) I Concentration (,-)1.5 '(_ Rep #1 Rep #2 0 Rep #3 Rep #4 Concentration Day 0 Day 1 Day 2 - Day 3 Day 4 Day Day 6 Day 7 II -1) CI) 0C) C.) 0 o 0.0 Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Rep #1 0 Day 6. Day 7 Rep #2 C) 0 ,_/ 7.-.-..-\ . I . , Rep #3 0 0 k. . t '''N 1 . Rep #4 CT. ) C) ,.:\ i---- N.......) ... 1 (-.-72j Collector's Signature: Client Information 1 CIient: t\ F'Ci (, ` i 4 TBL PO Box 589 Lumberton, NC 28359 910-738-6190 Merited, Inc. r ,; - Bioassay Sample Chain of Custody 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 M Q., Type of Faculty uenerming .L.,..,J1. • Sample information _ Sampling Site: C 1 ► lw_Q_Cl Sample Type: Grab Sampling Time: START Date: t END Date: t Sample Chilled (Covered witl.ce): Yes Collector's Name (Print): f ' �e-� -C Zip: Pol# r3.3 NPDES #: = )e i`t 3 `? 5D Phon: eQ 1- i re Pipe Number: • Composite # of Containers Q I 'i ' 1O'-i Time: 9 , 15 C1VI PM i 19 I n,- Time: ;-1: l ; �M IPM ✓ No e'oxke:ty Test Information Test Required: Chronic: Test Organism: Ceriodaphnia; Dubia: Acute: Pimephales promelas: Mysidopsis bahia: �' IWC: Toxicity Test Concentration(s): List Any Special Requirements: Shipping information Relinquished By: Received By: Relinquished By: Received By: Sample Temperature (C°): Date: Time:....,' :`� CPM Date: /- /7 -oc( Time:47 .S AM PM Date: /-1 ? •dfG Time: . AM PM Date: Time: AM PM Method of Shipment: WTC(p/i) UPS Fed -Ex Circle One Other: Sample Receiving (Laboratory Use Only) Received From: Received By: 'D , Sample Temperature (C°): Date: ; ii: )cc/ Time: Sample Condition: .1: Client Information Client: ''\ Contact: Add City Cou: Type. Meritech, Inc. Bioassay Sample Chain of Custody 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 t c, •'7 C r TBL PO Box 589 Lumberton, NC 28359 910-738-6190 Sample Information Sampling Site: Sample Type: Grab Sampling Time: START END Sample Chilled (Covered with Ice): Yes Collector's Name (Print : + p : l° E.)/Collector's Signature: �.;.., .,,,, � _ . `-� Zip: 0/2 :)/7 -r& 3 I PO 675. NPDES #: uc-33'-1t2 (4. Pipe Number: c;InfIS Composite # of Contai Date: i. `?�( Time: I - .� Date: Li Time: -1� (� fin - PM '� � No -r • Toxicity Test Information ‘-\Q Test Required: Chronic: Test Organism: Ceriodaphniai Dubia: Acute: PimephaIes pi•omelas: Mysidopsis bahia: IWIu: Toxicity Test Concentration(s): List Any Special Requirements: Shipping Information Relinquished By: `'' y';fu •, - r " r { Received" B ry . Date: j �, �� Time: =;a ''/may NOM RelinquishedY , �� Date: i 1 ��- Time: c> 1 c: i�JskPM Date: Time: il`o ° A►� PM Received By: Date: /- - p Time: %/Da AM ' M Sample Ten erature C ( ): Method of Shipment: WTC(p/u) UPS Fed -Ex /' B ' t.a O _o " / Circle One Other: Sample Receiving (Laboratory Use Only) Received From: -repEx Received By: �� �-UJ r' �P 1 , / Date: /- l - 64 Time: ' `f S AV PM Sample Temperature (C°): a;;") L/ ' ti Sample Condition Bioassay Sample Chain of Custody 642 Tamco Rd Reidsville, NC 27320 .(336) 342-4748 Client Information Client: i Contact: r, w,ec TBL PO Box 589 Lumberton, NC 28359 910-738-6190 LTC) 1vC _ Zip: Meritech, Inc t r 1 i t'l LL.( L- ( -21Z PO # `j NPDES. #: Phone: -3f01 Pipe Number: Sample Information Sampling Site: r7) jus \t Sample Type: Grab Composite Sampling Time: START Date: , &DD: 61 Time: END Date: 9 as ! oq Sample Chilled (Covered with ice): Yes - .Collector's Name (Print): i s-rpA lM�r�u 'Collector's Signature: e fi # of!Containers 3 • Ltd' M PM Time: 9 :I 6.Mk PM No Toxicity Test information Test Required: Chronic:c„.6.1 fAb Test Organism: Acute: IWC: Toxicity Test Concentration(s): List Any Special Requirements: Ceriodaphni i Dubia: Pimephales promelas:x. Mysidopsis bahia: Shipping Information Relinquished By: �� y,�t „4l•.: Received B. Relinquished By: Received By: Sample Temperature (C'): Time: ,-- .� )PM Time: ��'l ( PM cs Time:: A M Time: AM PM Method of Shipment: WTC(p%u) !UPS Fed -Ex Circle One Other: Date: - Date: Date: Date: Sample Receiving (Laboratory Use Only) Received From: ram( . Ex,/; Received By: /i r"t1 L Date: t z1-l. t( Sample Temperature (C°): c' - L / 0/3 - Sample Condition Time:! ; / L 7) ( AM PM • Title: Moore County File: moore Transform: NO TRANSFORMATION Kolmogorov Test for Normality D= D* = 0.1388 0.7025 (p-value > 0H_00) Critical D* = 1.035 (alpha = 0.01', N = 24) = 0.895 (alpha = 0.05 , N = 24) Data PASS normality test (alpha = 0.01). Continue analysis. Title: Moore County File: moore Transform: NO TRANSFORMATION Bartlett's Test for Homogeneity of Variance Calculated B1 statistic = 14.4886 (p-value = 0.0128) Data PASS B1 homogeneity test at 0.01 level. Continue analysis. Critical B = 15.0863 (alpha = 0.01, df = 5) = 11.0705 (alpha = 0.05, df = 5) • Title: Moore County File: moore Transform: NO TRANSFORMATION Summary Statistics on Data 'TABLE 1 of 2 GRP IDENTIFICATION N MIN MAX MEAN 1 control 4 0.2480 0.3400 2 •10.25% 4 0.28900.30 08 3 0.3400� 0.3093 20.5% 4 0.2070 0.3020 0.2665 4 41% 4 0.2510 0.2780 0.2635 5 61.5% 4 0.2710 0.2760 0.2740 6 82% 4 0.1970 0.2550 0.2188 Title: Moore County File:, moore Transform: Summary Statistics on Data NO TRANSFORMATION TABLE 2 of 2' GRP IDENTIFICATION VARIANCE SD SEM C.V. % 1 control 0.0017 0.0415 ,0.0208 13.8095 2 10.25% 0.0005 0.0224 ;0.0112 3 20.5% 7.2517 0.0017 0.0418 :0.0209 15.6718 4 41% 0.0002 0.0140 �0.0070 5 61.5% 5.3176 0.0000 0.0024 0.0012 0.8940 6 82% 0.0006 0.0253 ,0.0126 11.5551 • Title: Moore County File: moore Transform: ANOVA Table • NO TRANSFORMATION SOURCE DF SS MS F Between 5 0.0206 0.0041 Within (Error) 18 0.0144 ,0.0008 5.1417 Total 23 0.0351 (p-value = 0.0042) Critical F = 4.2479 (alpha = 0.01, df = 5,18) = 2.7729 '(alpha = 0.05, df = 5,18) Since F > Critical F REJECT Ho: All equal (alpha = 0.05) Title: Moore County File: moore Transform: Dunnett's Test - TABLE 1 OF 2 NO TRANSFORMATION Ho:Cont'rol<Treatment TRANSFORMED MEAN CALCULATED IN SIG GROUP IDENTIFICATION MEAN ORIGINAL UNITS T STAT 0.05 1 control 0.3008 2 0.3008 10.25% 0.3093 0,.3093 30.2665 -0.4244 4 20.5% 0.2665 41% 0.2635 1.7101 5 61.5% 0.2740 Oi.2635 1.8599 6 82 % 0.2188 0�• 2740 1.3356 01.2188 4.0943 * Dunnett critical value = 2.4100 (1 Tailed, alpha=:0.05, df = 5,18) Title: Moore County File: moore Dunnett's Test Transform: TABLE 2 OF 2 NO TRANSFORMATION Ho:Control<Treatment GROUP NIDENTIFICATION NUMS OF MIN SIG DIFF % OF DIFFERENCE (IN ORIG. UNITS);' CONTROL FROM CONTROL 2 10.25% 4 0.0483 3 20.5% 4 0.0483 4 41% 4 0.0483 5 61.5% 4 0.0483 6 82% 4 0.0483 1 control 4 16.0 16.0 16.0 16.0 16.0 -0.0085 0.0343 0.0373 0.0267 0.0820 Title: Moore County File: Moore12004 Transform: ARC SINE (SQUARE ROOT(Y)) Shapiro - Wilk(s Test for Normality D = W = 0.1864 0.9505 Critical W = 0.8840 (a1ph = 0.01 , N = 24) W = 0.9160 (alpha = 0.05 , N = 24) I j Data PASS normality.test (alpha = 0.01). Continue analysis. I , Data FAIL to meet homogeneity of variance Additional transformations are useless. Hartley's Test for Homogeneity of Variance Bartlett's Test for Homogeneity of Variance Title: Moore County File: Moore12004 Transform: ,ARC SINE(SQUARE ROOT(Y)) These two tests can not be performed because at least one group has zero variance. assumption. . Title: File: Moore County Moore12004 Transform:: H ARC SINE (SQUARE ROOT (Y) ) Steel's Many -One Rank Test _ Hp: Control<Treatment GROUP IDENTIFICATION TRANSFORMED RANK MEAN SUM 1 Control 1.4120 2 10.25% 1.4120 3 18.001 : 10.00 4.00 4 20.5% 1.256 14.001 10.00 4.00 41% 1.2188 5 61.5% 1.1781 12.00 10.00 4.00 6 82 0 10.00 I ' 10.00 4.00 0.8357 10.00 10.00 4.00 * CRIT. SIG ;VALUE DF 0.05 Critical values are 1 tailed ( k = 5 ) 1 11)L Lauuratory nwdIvsls/L,ontarner!Preserrative Chain of Custody Page of Prepared by: P.O. Box 589 Lumberton,NC 28359 Project jtame: ,\ P 'v C ir)(,L'j. (9I0) 738 6190 Client Project #: FAX: (910) 671-8837 (q/L),f-I _rl �fF Re ort: FY- hone Collected by: (print): kx Collected by (signbture): Site/Facility ID#: P.O.#: Rush? ( Lab MUST Be Notified ) _ Same Day 200% Next Day. 100% __ Two Day.. 50% Sample ID Comp/Grab 'Matrix: SS- SoiVSolid Remarks: Relinquished by: (Signature) Relinquished by: ( ign ure) Relinquished by: (Signature) Matrix' Depth • , Date Results Needed: FAX? No Yes Date Time GW - Groundwater WW - WasteWater DW - Drinking Water OT - Other Time: ignature eceived by: Ignature) Received for lab by: (Signature) No. or Cntrs 414 EtiVIRONNIEN'T.AL SCICtiCE CORP. 12065 Lebanon Road Mt. Juliet'rN 37122 Phone (615) 758-5358 Phonc (300) 767-5359 FAX (615) 753-5359 CoCode: TBLLAAB Template/Prelogin Cooler #: Shipped Via: Remarks/Contaminant (lab use only) State of North Carolina Department of 'Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross, Jr., Secretary Alan W. Klimek, ;P.E., Director December 11, 2003 Dennis Brobst Moore County Public Utilities P O BOX 1927 Carthage, NC 28327 CDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL 'RESOURCES 0 2003 SUBJECT: Renewal Application Requirements forPermit NCi0037508 Moore County WPCF Dear Permittee: Your,NPDES permit for a municipally owned/operated WWTP expires on July 31, 2004. This advance notice is being sent to explain the new requirements for your permit renewal application. You are receiving this advance notice because your facility has a permitted flow at or above 1 MGD, or -your • • WWTP has a pretreatment program. If either of these criteria no 'longer apply to your facility, contact the NPDES Unit before submitting a renewal application. .Federal (40 CFR 122) and state (15A'NCAC 2H.0105(e)) regulations require that permit renewal applications•befiled at least 180 days prior to expiration of the current permit. Your renewal application is due to the Division no later than February 2, .2004. -Failure to apply for renewal by the appropriate deadline may result ina civil penalty assessment, or others enforcement activity at the discretion of the Director. The U.S. EPA revised and expanded the application requirements for municipal permits, effective August 1, 2001. EPA forms 1 and 2A are attached to this Notice, and must be used for your permit renewal application. The new application requirements mandate additional effluent testing: 1. Conduct three Priority Pollutant Analyses (PPAs) and submit results) with your renewal application. Collect samples for the PPAs in conjunction with sampling for your current quarterly toxicity test. The new PPA requirements differ from previous versions. Each PPA must include: > Analyses for all total recoverable metals listed in Part D of form 2A. ' This includes metals that are not normally monitored through your NPDES permit. > Analyses for total phenolic compounds and hardness. > Analyses for all of the volatile organic compounds listed in. Part D. > Analyses for all of the acid -extractable compounds listed in Part D. > Analyses for all base -neutral compounds' listed in Part D. 2. Conduct four toxicity tests for an organism other than Ceriodaphnia and submit results with your renewal application. The tests should be conducted quarterly, with samples collected on the same day as your current toxicity test. Call the Aquatic Toxicology Unit at (919) 733-2136 for guidance in conducting the additional tests. These additional analyses must accompany your permit renewal application, or any request for a major permit modification. The Division cannot draft your permit without' the additional data. Any data submitted cannot be over 41/2 years old, and must account for seasonal variation (samples cannot be collected during the same season each year if collected over multiple years). 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Visrr us ON THE irrERNET @ http://h2o.enr.state.nc.us/NPDES 919 733-5083, extension 511 (fax) 919 733-0719 charies.weaver@ ncmail.net Renewal Notice for Permit NC0037508 Moore County Page 2 If your permit already contains a requirement for an annual effluent pollutant scan, additional scans are not required [provided you have conducted at least 3 scans prior to submitting your application]. If any wastewater discharge will occur after the current permit expires, this NPDES permit must be renewed. Discharge of wastewater without a valid permit would violate Federal and North Carolina law. Unpermitted discharges of wastewater could result in assessment of civil penalties of up to $25,000 per day. If all wastewater discharge has ceased at your facility and you wish to rescind this permit, contact Vanessa Manuel of the Division's Compliance Enforcement Unit at (919) 733-5083, extension 532. You may also contact the Fayetteville Regional Office at (910) 486-1541 to begin the rescission process. • Use the checklist below t complete your renewal package. The checklist identifies the items you must submit with the permit renewal application. If you have any questions, please contact me. My telephone number, fax number and e-mail address are listed at the bottom of the previous page. Sincerely, 144 Charles H. Weaver, Jr. NPDES Unit cc: Central' Files' rFayett`eville REgional-Office, Water Quality Sectional NPDES File The following items are REQUIRED for all renewal'packages: ❑ A cover letter requesting renewal of the permit and documenting any changes at the facility since issuance of the last permit. Submit one signed original and two copies. ❑ The completed application form (copy attached), signed by the permittee or an Authorized Representative. Submit one signed original and two copies. ❑ If an Authorized Representative (such as a consulting engineer or environmental consultant) prepares the renewal package, written documentation must be ' provided showing the authority delegated to the Authorized Representative (see Part II.B.11.b of the existing NPDES permit). ❑ A narrative description of the sludge management plan for the facility. Describe how sludge (or other solids) generated during wastewater treatment are handled and disposed. If your facility has no such plan (or the permitted facility does not generate any solids), explain this in writing. Submit one signed original and two copies. This information can be included in the cover letter. Send the completed renewal package to: Mrs. Valery Stephens NC DENR / Water Quality / Point Source Branch 1617 Mail Service Center Raleigh, NC 27699-1617 .;State of North Carolina 'Department of Environment and Natural Resources Division of Water. Quality Michael F. Easley, Governor William G. Ross, Jr., Secretary Alan W. Klimek, P.E., Director: January 29, 2004 Mr. James Frye Moore County 1094 ADDOR ROAD ABERDEEN NC 28315 NCDENR ._� NORTH- CAROL!NA •DEPARTMENT OF Iy ENVIRONMENT;At,ID NATURAL RESOURCES [;BAN 3 0 2004 Subject: NPDES Permit Renewal Application Permit NC0037508 Moore County:WPCP Moore County Dear Mr. Frye: The NPDES Unit received your permit renewal application on January 20, 2004. Thank you for submitting this package. Your permit renewal application has been assigned to a staff member for review. If the reissuance of your permit is delayed, the existing requirements in your permit will remain in effect until the permit is renewed (or the Division takes other action). We'appreciate your patience and understanding while we work to resolve the backlog of projects. If you have any additional questions concerning renewal of the subject permit, please contact Charles Weaver at (919) 733- 5083, extension 511. Valery Stephens Point Source Unit cc: Fayetteville Regional Office, Water Quality Section NPDES-File Central Files 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 919 733-5083, extension 520 (fax) 919 733-0719 - VISIT US ON THE INTERNET ( http://h2o.enr,state.nc.us/NPDES Valery.Stephens@ricmail.net r - Department of Public Utilities Wastewater Treatment Plant 1094 A'ddor Road Aberdeen, NC 28315 aL' At co4ce January 2, 2004 Re: NPDES Permit Application NPDES Permit No. NC0037508 Moore County Water Pollution Control. Plant Mrs. Valery Stephens NCDENR/D WQ/NPDES 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Mrs. Stephens: Telephone: (910) 281-3146 Facsimile: (910) 281-2047 JAB 2 0 2004 t I1 1:,'Ott SOURCE GrIANCr:,3 Moore County's NPDES Permit expires July 4, 2004. In compliance with Federal (40 CFR 122) and State (15A NCAC 2H.0105(e)) regulations, we must submit a Permit Renewal a least 180 days prior to the expiration date. The following items are submitted: 1. Application Standard Form 2A-Municipal-Sections A, B, C, D, E,& F (in triplicate) 2. No renewal fee required as of January 1, 2004 The County of Moore requests that their existing Permit berenewed as is, without any modifications. If additional information is needed, please do not hesitate to call me at 910281-3146. Sincerely, /p James D. Frye, System Superintendent JDF/sab Enclosures: cc: Mr. Paul Rawls, Fayetteville Regional Office, DEM Mr. Steve Wyatt, County Manager Mr. Phillip Boles, Director of Public Utilities FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 PLICATION INFORMATIC:. PERMIT ACTION REQUESTED: renewal RIVER BASIN: AP, APPLICATION INFORMATION,FOR AWAPPUCANI An treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet. A.1. Facility Information. Facility Name Mailing Address 1094 Addor Road Aberdeen, NC 28315 Contact Person James D. Frye Title System Superintendent Telephone Number ( 910) 281-1146 Facility Address (not P.O. Box) ntro1 Plant A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Moore County Board of Commissionersi. Mailing Address PO Box 905 Carthage, NC 28327 Contact Person Michael Holden Title Telephone Number Chairman 1910-) 947-6403 Is the applicant the owner or operator (or both) of the treatment works? XX owner 0 operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. 0 facility If applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES NC0037508 PSD UIC OtherAir i 076511102 RCRA otherLand. App,. WQ8818018 A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of CollectionSystem Ownership Tn of Aberdeen 3400 separate ` town Pinehurst 9700 separate municipal until 3/04 Tn of Sou Pines 10900 separate ! town Tn of Pineb1»ff 1100 separate town Tn of Carthage 1870 Tourism/seasonal/resort 6000 (. PA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. separate separate town town Page 2 of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant • NCOf 1750 Form Approved 1/14i99 OMB Number 2040-0086 A.S. Indian Country. a. ' Is the treatment works located in Indian Country? Yes X No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? X Yes No A.6. Flow. Indicate the design flow rate of the treatment plant'(i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of 'This year" occurring no more than three months prior to this application submittal.' a. Design flow rate 6. 7 mgd Two Years A io Last Year This Year b. Annual average daily stow rate 4.475 4.338 1 ' 5.081 mgd c. Maximum daily flow rate 5.021 5.051 ' 6.259 mgd A.7. Collection System. Indicate the y type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. X Separate sanitary sewer approximate 17 miles % ' Combined stone and sanitarysewer A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? X Yes No If yes, list how many of each of the following types of discharge points the treatment works uses: i. Discharges of treated effluent 1 ii. Discharges of untreated or partially treated effluent iii. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) v. Other O () () 0 b. Does the treatment works discharge effluent to basins, g ponds, or other surface Impoundments that do not have outlets for discharge to waters of the U.S.? Yes X No If yes, provide the following for each surface impoundment: Location: Annual average daily volume discharged to surface impoundment(s) mgd Is discharge continuous or intermittent? c. Does the treatment works land -apply treated wastewater? Yes X No If yes, provide the following for each land application site: Location: Number of acres: Annual average daily volume applied to site: Mgd Is land application continuous or intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? Yes X No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 3 of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 Form Approved 1/14/99 OMB Number 2040-0086 If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). If transport is by a party other than the applicant, provide: Transporter name: Mailing Address: Contact person: Title: Telephone number. For each treatment works that receives this discharge, provide the following: Name: Mailing Address: Contact person: Title: Telephone number. If known, provide the NPDES permit number of the treatment works that receives this discharge. Provide the average daily flow rate from the treatment works into the receiving facility. mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not included in ! I i A.8.a through A.8.d above (e.g., underground percolation, well injection)? ! Yes X No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): Annual daily volume disposed of by this method: Is disposal through this method continuous or intermittent? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms -7550-8 & 7550-22., Page4of21 • FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 WASTEWATER DISCHARGES: Fonn Approved 1/14/99 OMB Number 2040-0086 If you answered "yes" to question A.8:a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "no" to question A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Duffel!. a. Outfall number 001 b. Location Aberdeen 28315 (Cityor town, if applicable) Moore (County) 35° 04' 04" (Latitude) c. Distance from shore (if applicable) d. Depth below surface (if applicable) e., Average daily flow rate f. Does this outfall have either an intermittent or a periodic discharge? If yes, provide the following information: Number of times per year discharge occurs: Average duration of each discharge: Average flow per discharge: Months in which discharge occurs: g. Is outfall equipped with a diffuser? Yes (Zip Code) North Carolina ft. ft. mgd o State �� 7q 28 10 (Longitude) X ' No (go to A.9.g.) ! I mgd A.10. Description of Receiving Waters. a. Name of receiving water Aberdeen Creek b. Name of watershed (if known) Yes X No United States Soil Conservation Service 14-digit watershed code (if known): c. Name of State Management/River Basin (if known): United States Geological Survey 8-digit hydrologic cataloging unit code Of known): d. Critical low flow of receiving stream (if applicable): . acute cfs _ chronic cfs e. Total hardness of receiving stream at critical low flow (if applicable): mg/l of CaCO3 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 5 of 21 Form Approved 1/14/99 OMB Number 2040.0086 FACILITY NAME AND PERMIT NUMB R: Moore County Water Pollution Control Plant ` NC0037508 A.11. Description of Treatment a. What levels of treatment are provided? Check all that apply. X Primary X Secondary Advanced Other. Describe: I b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 90 ' Design SS removal 90 Design P removal 10 Design N removal 75 % Other c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, chlorination please describe. ' If disinfection is by chlorination, is dechlorination used for this outfall? X / Yes No d. Does the treatment plant have post aeration? I Ye X No I. A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent parameters. Provide the Indicated effluent testing required by the permitting authority for each testing data for the following . outfall through which effluent Is discharged. Do not include information on combined sewer overflows in this section. All information reported be based collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes minimum, effluent testing data must be based on at least three samples and must be no more Outfall number: 001 must on data comply with QA/QC requirements of not addressed by 40 CFR Part 136. At a than four and one-half years apart. PARAMETER MAXIMUM DAILY VALUE AVERAGE DAILY VALUE Value Units Value . Units Number of Samples pH (Minimum) 6.32 s,u; 6.77 I s .u. 260 pH (Maximum) 7.85 s.u. 7.41 s'.tr. 260 Flow Rate 6,17 mgd 5.05 ' mgd 365 Temperature (venter) 22.4 ° C 15.9 i, °IC 365 Temperature (Summer) 26.0 a C 22.4 ° C 365 For pH please report a minimum and a maximum daily value _ , POLLUTANT MAXIMUM DAILY DISCHARGE' AVERAGE DAILY DISCHARGE !, 1: ANALYTICAL METHOD ML 1 MDL Conc. • Units Conc. Units Number of Samples CONVENTIONAL AND NONCONVENTIONAL COMPOUNDS. 1 BIOCHEMICAL OXYGEN BOD-5 14.1 mg/1 7.2 . mg/1 260 it SM5210B DEMAND (Report one) CBOD-5 FECALCOLIFORM 128 . #/100mL 13 • ;#/100mL - 260 SM9222D TOTAL SUSPENDED SOLIDS (TSS) 19 mg/1 13 mg/1 260 SM2540D END OF PART A. , REFER TO THE APPLICATION OVERVIEW TO DETERMINE WHICH OTHER PARTS OF FORM 2A.YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 6 of 21 FAC4LITY NAME AND PERMIT NUMBER: Moore County Water Pollution'Control Plant NC0037508 BASIC APPLICATION INFORMATION Form Approved 1/14/99 OMB Number 2040-0086 PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate > 0.1 mgd must answer questions B.1 through 8.6. All others go to Part C (Certification). B.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. 750,000 gpd includes the plant & towns Briefly explain any steps underway or planned to minimize inflow and infiltration. The plant & the towns are checking interceptor lineshoping to cut down on the influent. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area sunrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other stmctures through which treated wastewater is discharged from the treatment plant., Include outfalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground._ d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within 1/4 mile ofjthe property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. ! e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where that hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram'showing the processes of the treatment plant, including all bypass piping and all backup power sources or redundancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g, chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge pointsandapproximate daily flow rates between treatment units. Include a brief narrative description of the diagram. B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? _Yes . X No b If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). Name: Mailing Address: Telephone Number. Responsibilities of Contractor. 'B.5. Scheduled Improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment; effluent quality, or design (capacity of the treatment works. If the treatment works has several different implementation schedules•or is planning several improvements, submit separate response's to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. 001 b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. Yes X No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 7of21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 OMBorm ApprovedmberO4o-08 ' ; � OMB Number 2040.0086 c If the answer to B.5.b is "Yes; briefly describe, including new maximum daily inflow rate (if applicable). plan to purchase a new lime system as applicable. applicable. d. Provide dates imposed by any compliance For improvements planned independently Indicate dates as accurately as possible. • Implementation Stage — Begin construction - End construction- — Begin discharge — Attain operational level e. Have appropriate permits/dearances Describe briefly: schedule or any actual dates of completion for of local, State, or Federal agencies, indicate planned Schedule Actual Completion MM / DD / YYYY MM / DD / YYYY the implementation or obtained? actual , steps listed below, completion dates, as - - :_Yes X No _/_/ 2004 _// _/ / 2005 •_/ / _/ _/_/ _/ _/ _/ / / conceming other Federal/State requirements been B.6. EFFLUENT TESTING DATA Applicants that discharge required by the permitting this section. All information data must comply with addressed by 40 CFR Part and one-half years old. Outfall Number: 001 (GREATER THAN 0.1 MGD ONLY). to waters of the US must provide effluent testing data for the following authority for each outfall through which effluent is dischamed. Do parameters. Provide the indicated effluent testing not include information on combined sewer overflows in using 40 CFR Part 136 methods. In addition, this requirements for standard methods for analytes not three pollutant scans and must be no more than four reported must QA/QC requirements 136. At a minimum, be based on data collected through analysis conducted of 40 CFR Part 136 and other appropriate QA/QC effluent testing data must be based on at least POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ' ANALYTICAL METHOD ML / MDL Conc. Units Conc. -Units Number of Samples CONVENTIONAL AND NONCONVENTIONAL COMPOUNDS. AMMONIA (as N) < - 0. 50 mg/1 < 0.50 mg/1 26d SM4500F CHLORINE (TOTAL RESIDUAL, TRC) 304 ug/I 115 ug/1 I , 2601 SM4500G DISSOLVED OXYGEN 1 11.09 mg/1 9.35 -mg/1 365 TOTAL KJELDAHL NITROGEN (TKN) 2.10 mg/1 1.21 mg/l I , 141 351. 2 NITRATE PLUS NITRITE NITROGEN 16.0 mg/1 ' 13.1 mg/1 11 353.2 OIL and GREASE PHOSPHORUS (Total) 2.90 . mg/1 2. 34•- mgf 1 14 SM4500B&E TOTAL DISSOLVED SOLIDS (TDS) 1 . OTHER r I. i END OF -PART B. REFER TO THE APPLICATION OVERVIEW TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 8 of 21 FACILITY NAME AND PERMIT NUMB gg Moore County Water oLLutl Jon Control Plant NC0037508 OMB Number 2040-0086 BASIC APPLICATION INFORMATION 4 , . PART C. CERTIFICATION All applicants must complete the Certification Section. Refer to instructions to determine who is an officer forthe purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are `submitting. By signing this certification statement, applicants confirm that they have reviewed' Form 2A and have'completed all sections ' that apply to the facility for which this application is submitted. 1. , Indicate which parts of Form 2A you have completed and are submitting: X Basic Application Information packet Supplemental Application Information packet: Effluent Testing Data) , I Biomonitoring Data) Discharges and RCRA/CERCLA Wastes) Sewer Systems) I , ; . X Part D (Expanded X Part E (Toxicity Testing: X Part F (Industrial User Part G (Combined ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system.designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and ' complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fine and imprisonment for knowing violations. Name and official title Michael Holden - Chairman - Signature Telephone number . 910-947-6403 Date signed Q �,k0 8 `O 4 Upon request of the'permitting authority, you must submit any other information necessary to assess wastewater treatment practices at the treatment. works or identify appropriate permitting requirements. . SEND COMPLETED FORMS TO: EPA Fomi 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. i Page 9 of 21 Department of Public Utilities Wastewater Treatment Plant 1094 Addor Road Aberdeen, NC 28315 Waunty o/ P_Ao•oxe July 26, 2004 Re: Results for EPA Expanded Requirements for Permit Renewi al NPDES Permit No. NC0037508 Mrs. Valery Stephens NCDENR/DWQ/NPDES 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Mrs. Stephens: Telephone: (910) 281-3146 Facsimile: (910) 281-2047 COPY DENRFR JUL 2 2004 Please find included a copy of the Priority Pollutant Analysis and the Fat Head Minnow Toxicity test results for June 2004. This is the third set of test for plant renewal. This concludes the Priority Pollutant Analysis (PPAs) required for plant renewal. We are required to do one more Fathead Minnow Toxicity which will be done in September. I will send you those results as I receive them. If additional information is needed, please do not hesitate to call me at 910-281-3146. Sincerely, p, James D. Frye, System Superintendent JDF/sab Cc: Mr. Paul Rawls, Fayetteville Regional Office, DEM Mr. Charles Weaver, NPDES Unit Mr. Kevin Bowden, Aquatic Toxicology Unit Mr. Steve Wyatt, County Manager Mr. Phillip Boles, Director of Public Works • Attn: Client: Ms. Stephanie Brixcy lioorc County WWTP, 1094 Addor Road Aberdeen, NC 28315 Meriteih, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: Date Sample Rcvd: PY 7/20/04 6/25/04 Mleritech Work Order # Parameters 1,PA 624+Acrolcin+Acryl nitrile IPA 625 EPA 608 ▪ Antimony, total 1 fardncss, total aArsenic, total ▪ Beryllium, total • Cadmium, total • Calcium, total Chromium, total (olper,_totala� Lead, total Mercury. total Nickel, total . Selenium, total Silver, total 1h` laylium; tcital 0 011 ml,/l`-? %trig total . __ _,Ing/Itkft Cyanide, total < 0.005 mg/1 1'l cnol _total's P-.7. , 06250440 Result Sample: PPA 0624237 Analysis Date See attached 7/1/04 See attached 7/2/04 See attached 7/2/04 < 0.025 mg/1 6/29/04 115 mg eq CaCO3/1 6/28/04 < 0.010 mg/1 6/29/04 < 0.005 mg/1 6/29/04 < 0.002 mg/1 6/29/04 45.9 mg/1 6/28/04 < 0.005 mg/1 6/29/04 6/29/04 <0.010 mg/1 6/29/04 < 0.0002 mg/1 6/29/04 < 0.010 mg/1 6/29/04 < 0.010 mg/I 6/29/04 < 0.005 mg/1 6/29/04 6/29/04 6/29/04 7/2/04 7/9/04 Repotting Limit 0.025 mg/i 0.662 mg eq CaCO3/1 0.010 mg/1 0.005 mg/,I 0.002 mg/1 0.100 mg/1 0.005 , mg/1 0.002 .mg/] 0.010 mg/1 0.0002 mg/1 0.010 mg/1 0.010 mg/1 0.005 mg/1 0.020 mg/I 0.010 'mg/l 0.005 mg/I 0.010 mg/1 6/24/2004 Method EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 E1'A 200.7 1sPA 200.7 IVA 200.7 EPA 245.1 ".PA, 200.7 I?PA 200.7 EPA 200.7 l',PA 200.7 EPA 200.7 EPA 335.2. EPA 420.1 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, 642 Tamco Reidsville, iger tel (336) 342-4748 fax (336) Chain of Custody Record Inc. Road NC 27320 3427.1522 `-. . . " ..r., II , -AA Do, c, Oc., 4,1 N . 4.; I Client: Cf)C 0,..'1_,ST P;::,) NPDES# 11'4 CCy,1-) •,;25 ri ":.."") c.)::::,, .. .-,. ig./( Tel , : • '7.' •=3 / —' %- . Address: Attention: _AO 9 Li ,-1 0, (.1,.. r 12\ d. l'A .V.) a( 6,Q.,; 1 , (NA, ......-,,6.. -:,,, 1 s Fax 9 I I. - •-•-.32 i cy P.O. # (.0 ••;) C-s5 4 • 5,A. 4..;14'-e-',''''(,', g (j, ' Project # If Composite? Person Taking Sample (Signature): '''. Lab Use Only Sample - • Location/ID# Dale Date 1 Titne 1 Date 2 Time 2 C? G? # of Conts. Tests Required - Iced? Temp? pH OK? Chlorine OK? ,.:•)_"'::1-,•,•)---_":•-(4- 1-)t"-7:16-"0.'„I t-iiii - - - " " _ 1 0 E-_ rif- fi.: ,,-,?5 Li -r-I (...1 06 1 t ' i t.t .,\•I ' i il P nc i i AO -- 1 --C -7 - -'-L\O V !"1,f-c -7/1 , -4,-).-- = --- - --- ------------ -•.,ii _ . • i• i . • • , . ! 1, • ..: . ..„ . , , 1, -; : ' • ' . , -.. •., „ . - . _...._....... .. - ... - • . - . , . „...,.• ....... , - Method of Shipment: LI UPS Fed Ex Hand Delivery Other Comments: . . . ... \ i ....--- —7-- , -r i " 1--zi • ---, --„ ......,,.....„...... 6.01 41- c Lt,c;\ ' / Will these results be used for regulatory purposes? Ves EJ No i Relinquished by. , f . Vitt iLCA. /-Y.: A..Q,‘„,_,. _ Date: Time: • 0 (";)-50 L.( irz- (—Received by: Date / \ , • .1 r Time ),,,, 1 i 1 r r. -r-- .......,9 f ' , - Relinquished by Date • Time: .Fleceivect by: / Date Time: Relinquished by Date: Time Received at lab by: Dale Time: Client: Project: Client Sample ID: Sample Collection: MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc: Moore County WWTP 624 Trip Blank 06/24/04 Meritech ID#: 106250440TB Analysis:'07/01/04 Analyst: CAL EPA 624 VOLATILE ORGANICS. Parameter Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether "C111oroformY_,.-- Chloromethane Dibromochloromethane 12-Dibromoethane 1,1-Dichloroethane 1,2-Dichloroethane 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1, 1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1, 3-Dichloropropene Ethyl benzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Additional Compounds Acrolein < 50.0 ug/L Acrylonitrile . < 10.0 ug/L I hereby certify that I have reviewed and approve these data. Result < 1.00 ug/L < 1-.00 ug/L. < 1.00 ug/L < 5.00 ug/L < 1.00 ug/L < 1:00 ug/L < , 5.00 ug/L < 5.00 ug/L ., < 5.00 ug/L < 1.00 ug/L < .1.00 ug/L < 1.00 ug/L < 1.00 ug/L <.1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L <-1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L <. 1.00 ug/L <',1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 5.00 ug/L < 5.00 ug/L Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax Client: Project: Client Sample ID: Sample Collection: MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc: Moore County WWTP 624 0624237 PPAs 06/24/04 Meritech ID#: 06250440 Analysis: 07/0,'1 /04 Analyst: CAL EPA 624 VOLATILE ORGANICS Parameter Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Result < 1.00 ug/L < 1.00 ug/L < 1.00 ug/L < 5.00 ug/L < 1.00 ug/L < 1.00 ug/L < 5.00"ug/L < 5.00 ug/L. Chkoroform-�•; -� - 2 73-ug/L3 Chloromethane <'`5.00 ug/L Dibromochloromethane < 1.00 ug/L 1,2-Dibromoethane < 1.00 ug/L 1,1-Dichloroethane < 1.00 ug/L 1,2-Dichloroethane < 1.00 ug/L 1,4-Dichlorobenzene < 1.00 ug/L 1,2-Dichlorobenzene < 1.00 ug/L 1,3-Dichlorobenzene < 1.00 ug/L 1,1-Dichloroethene < 1.00 ug/L trans-1,2-Dichloroethene < 1.00 ug/L 1,2-Dichloropropane < 1.00 ug/L cis-1,3-Dichloropropene < 1.00 ug/L trans-1,3-Dichloropropene < 1.00 ug/L Ethyl benzene < 1.00 ug/L Methylene chloride < 1.00 ug/L 1,1,2,2-Tetrachloroethane < 1.00 ug/L Tetrachloroethene < 1.00 ug/L Toluene < 1.00 ug/L 1,1,1-Trichloroethane < 1.00 ug/L• 1,1,2-Trichloroethane < 1.00 ug/L Trichloroethene < 1.00 ug/L Trichlorofluoromethane < 5.00 ug/L Vinyl chloride < 5.00 ug/L Additional Compounds Acrolein < 50.0 ug/L Acrylonitrile . < 10.0 ug/L I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax Client: Project: Client Sample ID: Sample Collection: Parameter Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzyl butyl phthalate Bis(2-chloroethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethylhexyl)phthalate 4-Bromophenyl phenyl ether 2-Chloronaphthalene 4-Chlorophenyl phenyl ether Chrysene Dibenzo(a,h)anthracene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 3,3'-Dichlorobenzidine Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octyl phthalate 1,2-Diphenylhydrazine MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Moore County WWTP 625 0624237 PPAs 06/24/04 Meritech ID#: 06250440 Analysis: 07/02/04 Extraction: 06/,28/04 Analyst: CAL EPA 625 SEMIVOLATILE ORGANICS Result <10 ug/L <10 ug/L <10 ug/L <50 ug/L <10 ug/L < 10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <50 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L < 10 ug/L <10 ug/L Parameter Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnapthalene Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Phenanthrene Pyrene 1,2,4-Trichlorobenzene 4-Chloro-3-methylphenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 4,6-Dinitro-2-methylphenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol I hereby certify that I have reviewed and approve these data. Result <10 ug/L ;<10 ug/L <10 ug/L <10 ug/L <50 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L 10 ug/L <10 ug/L <10 ug/L <10 ug/L <10 ug/L <50 ug/L <50 ug/L <10 ug/L <50 ug/L <50 ug/L <10 ug/L <10 ug/L Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Faz, MERITECH, INC. ENVIRONMENTAL LABORATORIES A Division of Water Technology and Controls, Inc. Client: MCWWTP Project: PPA Client Sample ID: 0624237 PPAs Sample Collection: 06/24/04 EPA 608 - Organochlorine Pesticides Parameter Result Meritech ID: 062504.40 Extraction: 06/30/04 - Analysis: 07/02/04 Analyst: KB/MC Aldrin < 0.25 ug/L a-BHC < 0.25 ug/L , b-BHC < 0.25 ug/L d-BHC < 0.25 ug/L g-BHC < 0.25 ug/L 4,4'-DDD < 0.50 ug/L 4,4'-DDE < 0.50 ug/L 4,4'-DDT <0.50 ug/L Dieldrin ' - < 0.50 ug/L Endosulfan I < 0.25 ug/L Endosulfan II < 0.50 ug/L Endosulfan sulfate < 0.50 ug/L Endrin < 0.50 ug/L Endrin aldehyde < 0.50 ug/L Heptachlor < 0.25 ug/L Heptachlor epoxide < 0.25 ug/L Methoxychlor < 5.0 ug/L Toxaphene <50 ug/L Aroclor — 1016 < 0.50 ug/L Aroclor — 1221 < 1.0 ug/L Aroclor —1232 < 0.50 ug/L Aroclor — 1242 < 0.50 ug/L Aroclor — 1248 < 0.50 ug/L Aroclor — 1254 < 0.50 ug/L ; Aroclor — 1260 < 0.50 ug/L Chlordane <5.0 ug/L I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco `Road * Riedsville, NC 27320: (336) 342-4748 Ph * (336) 342-1522 Fax TestAmerica ANALYTICAL TESTING CORPORATION MERITECH, INC. FRANK PAZTOR 642 TAMCO RD. REIDSVILLE, NC Project: Project Name: Sampler: 2960- FUS'r :s (2s:IOMrOn .DRIVE • NASHVILLE. TENNESSHE 37204 800-763.0980 • 615-726.3104 FAX ANALYTICAL REPORT 2822 Lab Number: 04-A99950 Sample ID: 062540 Sample Type: Water 27320 Site ID: Date Time Date Time Collected: 6/24/04 Collected:- 7:41 Received: 6/29/04 Received: 14:19 Analyte Report Result Units Limit *PESTICIDES/PCB's/HERBICIDES* Aldrin Aroclor 1016. Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 a-BHC b-BHC d-BHC g-BHC, Lindane Chlordane 4,4'-DDD 4,4'-DDE 4,4'DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 0.25 0.50 1.00 0.50 0.50 0.50 0.50 0.50 0.25 0.25 0.25, 0.25 5.00 0.50 0.50 0.50 0.50 0.25 • 0.50' 0.50 0.50 0.50 0.25 0.25 5.00 50.0 5 1 1, 1 1 1 1 1 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 Dil Analysis Factor Date 7/ 1/04 7/ 2/04 7/ 2/04 7/ 2/04 7/ 2/04 7/ 2/04 7/ 7/ .7 / 7/ 7/ 7/ 7/ 7/ 7/ 7/ 7/ 2/04 2/04 1/04 1/04 1/04 1/04 1/04 1/04 1/04 1/04 1/04 7/ 1/04 7/ 1/04 7/ 1/04. 7/ 1/04 7/ 1/04 7/ 1/04 7/ 1/04 7/ 1/04 7/ 1/04 0:23 1:11 1:11 1:11 1:11 1:11 1:11 1:1 0:23 0:23 0:231 0:23 Analysis Time 0:23' 0:23 0:231 0:23 0:231 0:23 0:23I 0:231 0:23: 0:231' 1 0:23r 0:23' 0:23I 0:23 • Analyst Method Batch K. Burritt M. Cauthen M; Cauthen M�. Cauthen M. Cauthen M. Cauthen M. Cauthen M. Cauthen K! Burritt K. Burritt K: Burritt K. Burritt K. Burritt Burritt K: Burritt K Burritt K. Burritt K. Burritt K.� Burritt K. Burritt K.i Burritt K., Burritt K. Burritt K., Burritt K. Burritt K. Burritt 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608 608.2 608 4067 7680 7680 7680 7680 7680 7680 7680 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 4067 Sample report continued . . - ANALYTICAL REPORT Laboratory Number: 04-A99950• Sample ID .062540 Page 2 Sample Extraction Data Parameter - Wt/Vol Extracted Extract Vol Date Time Analyst Method OC Pest 500. ml 5. ml 6/30/04 K. Turner 608 PCB's 500. ml 5.00 ml 7/ 1/04 M. Ricke 608 .Surrogate it Recovery Target Range Pest Surr TCMX 81. 46. - 135. Pest Surr DCB 95. 30. - 117. Pest Surr DCB 64. 36. - 127. LABORATORY COMMENTS: ND = Not detected at the report limit. B = Analyte was detected in the method blank. J = Estimated Value below Report Limit. E = Estimated Value above the calibration limit of the instrument. # = Recovery outside Laboratory historical or method prescribed limits. End of Sample Report. TestAmerica ANALYTICAL TESTING CORPORATION 2960 FOSTBB Caeu:x'Om Dkivt; • (9499t LLe. TENVY.5SK6 37204 800-765-0980 • 615-726-3404 FAN PROJECT QUALITY CONTROL DATA Project Number: Project Name: Page: 1 Laboratory Receipt Date: 6/29/04 Matrix Spike Recovery Note: If'Blank is referenced as the sample spiked, insufficient volume was received for the defined analytical batch for MS/MSD analysis on an true sample matrix. Laboratory reagent water was used for QC,purposes., Analyte units Orig. Val. MS Val Spike Conc. Recovery Target Range Q.C. Batch Spike sample I ` **PEST/PCB/HERB PARAMETERS** Aldrin mg/1 <'0.00004 0-00086 0.00100. - 86 Aroclor 1016 mg/1 '< 0.00045 0.00881 0.0100 88 Aroclor 1260 mg/1 < 0.00049 0.00845 0.0100 84 g-BHC, Lindane mg/1 a 0.00003 0.00088 0.00100 88 4,4'DDT mg/1 c 0.00004 0.00098 0.00100 ' 98 Dieldrin mg/1 < 0.00004 0.00100 0.00100 100 Endrin mg/1 < 0.00003 0.00111 0.00100 111 Heptachlor mg/1 < 0.00003 0:.00089 0.00100. .89 Matrix Spike Duplicate 42. - 122. 4067 blank 50. - 114. 7680 blank 42. - 147. 7680 blank 1 32. - 127. :4067' blank. 25. - 160-' 4067 blank 136. - 146. 4067 blank 30..- 147. 4067 blank 34. - 111- 4067 blank Analyte units Orig. Val. Duplicate RPD Limit Q.C. Batch **PEST/PCB/HERB PARAMETERS** Aroclor 1016 mg/1 0.00881 - 0.00948 7.33 Aroclor 1260 mg/1 0.00845 0.009d7 7,08 Laboratory Control Data 7680 7680 Analyte - units Known Val. Analyzed Val t Recovery Target Range Q.C: Batch **PEST/PCB/HERB PARAMETERS** Aldrin mg/1 0.00100 0.00075 75 42'- 122 '4067 Aroclor .1016 mg/1 0.0100 0.00994' 99 50.- 114 7680 Aroclor 1260 mg/1 0.0100 0.00888 89 15 - 127 7680 a-BHC. mg/1 0.00100 0.00072 -72 37;-, 134 4067 b-BHC mg/1 0.00100 0.00082 82 17 -':147 4067 Project QC continued . . . Testi.merica ANALYTICAL TESTING CORPORATION 2960 FINITE CKeirrrain DRIVE • N. sH ILLE. TENNESSEE 37204 800-765-0980 • 615-726-3404 FAX . PROJECT QUALITY CONTROL DATA Project Number: Project Name: Page: 2 Laboratory Receipt Date: 6/29/04 Analyte Laboratory Control Data units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch d-BHC mg/1 0.00100 0.00048 48 19 - 140 4067 g-BHC, Lindane mg/1 - 0.00100 0.00076 76 32 - 127 4067 II Chlordane mg/1 0.0100 0.0103 103 45 - 119 4067 4,4'-DDD mg/1 0.00100 0.00091 91 31 - 141 4067 4,4'-DDE mg/1 0.00100 0.00089 89 30 -. 145 4067 4,4'DDT mg/1 0.00100 0.00084 84 . 25 - 160 4067 Dieldrin mg/1 0.00100 0.00087 '87 36 - 146 4067 Endosulfan i- mg/1 ,0.00100 0.00084 84 45 - 153 4067 Endosulfan II mg/1 0.00100 0.00089 89 10 - 202 4067 Endosulfan Sulfate mg/1 0.00100 0.00083 83 _ 26 - 144 4067 Endrin mg/1 0.00100 0.00095 95 30 - 147 4067 Endrin Aldehyde mg/1 6.00100 0.00088 88 40 - 144 4067 Heptachlor mg/1 0.00100 0.00079 79 34 - 111 4067 Heptachlor Epoxide mg/1 0.00100 0.00085 85 3 - 142 4067 Methoxychlor mg/1 0.00100 0.00100 100 53. - 152 4067 Toxaphene mg/1 0.0200 . 0.0263 132 11 41I'- 126 4067 Pest Surr TCMX % Rec - 84 46 - 135 7680 Pest Surr DCB % Rec 60 30,- 117 4067 Pest Surr DCB % Rec 35 36'- 127 7680 Analyte Analyte Duplicates units Orig. Val. Duplicate P.PD Limit Q.C. Blank Data Batch Sample Dup'd Blank Value Units - Q.C. Batch Date Analyzed Time Analyzed Project QC continued . . . TestAmerica ANALYTICAL TESTING CORPORATION 21160 Fnsm CHEICHTHA DRIt4: • N..JH¢LLLE, TEN96ssoE 37204 800-765-0980 • 615-726.3404 FAX PROJECT QUALITY CONTROL DATA Project Number: Project Name: Page: 3 Laboratory Receipt Date: 6/29/04 **PEST/PCB/HERB PARAMETERS** Aldrin Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 a-BHC b-BHC d-BBC a -BBC, Lindane Chlordane 4,4'-DDD 4,4'-DDE 4,4'DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene Pest Surr TCMX Pest Surr DCB Pest Surr DCB End of Report for Project 380531 < 0.00004 mg/1 4067 7/ 1/04 i 1:51 < 0.'00045 mg/1 7680 7/ 2/04 . 3:04 < 0.00070 mg/1 7680 7/ 2/04 3:04 < 0.00049 mg/1 7680 7/ 2/04 3:04 < 0.00022 mg/1 7680 7/ 2/04 3:04 < 0.00047 mg/1 7680 7/ 2/04 3:04 < 0.00036 mg/1 7680 7/ 2/04 3:04 < 0.00049 mg/1 7680 7/ 2/04 3:04 < 0.00004 mg/1 4067 7/ 1/04, 1:51 < 0.00004 mg/1 4067 7/ 1/04 151 < 0.00004 mg/1 4067 7/ 1/04 1:51 < 0.00003 mg/1 4067 7/ 1/04 I' 1:51 < 0.00074 mg/1 4067 7/ 1/04 1:51 < 0.00004 mg/1 4067 7/ 1/04 1:51 < 0.00004 mg/1 4067 7/ 1/04 1:51 < 0.00094 mg/1 4067 7/ 1/04 1:51 < 0.00004 mg/1 4067 7/ 1/04 1:51 < 0.00003 mg/1 4067 7/ 1/04 1:51 < 0.00004 mg/1 4067 7/ 1/04 1:51 < 0.00005 mg/1 4067 7/ 1/04 1:51 < 0.00003 mg/1 4067 7/ 1/04 '1:51! < 0.00005 mg/1 4067 7/ 1/04 1:51i < 0.00003 mg/1 4067 7/ 1/04 1:51) < 0.00004 mg/1 4067 7/ 1/04 ,1:51; < 0.00003 mg/1 4067 7/ 1/04 1:511 < 0.00059 mg/1 4067 7/ 1/04 1:51 78. % Rec 7680 7/ 2/04 3:04 65. t Rec 4067 7/ 1/04 1:51 61. % Rec 7680 7/ 2/04 3:04 Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:6/30/2004 Facility: Moore County WWTP NPDES # NC0037508 Laboratory: Meritech, Inc. ipe #: 001 County: Moore X /' i�t-� L- p. Signature of Operator in Responsible Charg�'� Signature of Laboratory Supervisor Comments MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time % Eff. Control Repl. Surviving # Original # Wt/original (Trig) Surviving # Original # Wt/original (mg) 10.25 20.5 Surviving # Original # Wt/original (mg) 41 Surviving # Original # Wt/original (mg) 61.5 Surviving # Original # Wt/original (mg) 82 Surviving # Original # Wt/original (mg) Water Quality Data ' Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (°C) Dilution H2O Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 6/22/2004 1 2 1:30 PM 3 4 10 •10 10 10 10 10 10 10 0.350 0.418 0.364 0.511 10 10 10 10 10 10 10 10 0.354 0.359 0.444 0.379 10 10 10 10 10 10 10 10 0.383 0.339 0.559 ' 0.329 10 10 10 10 10 10 10 10 0.428 0.421 0.416 0.416 10 10 10 10 10 10 10 10 0.304 0.390 0.430 0.441 10 10 10 10 10 .10 10 10 0.433 0.416 0.449 0.435 Day Avg Wt/Surv: Control % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) %° Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.411 100.0 0.411 100.0 0.384 100.0 0.403 100.0 0.420 100.0 0.391 100.0 0.433 0 1 2 3 4 5 6 8.17 / 8.12 8.15 / 8.10 8.32 / 8.23 8.30 / 8.20 8.35 / 8.30 8.22 1/ 8.28 8.29 / 8.31 7.42 / 7.33 7.46 / 7.30 7.38 / 6.95 7.36 / 6.92 7.41 / 7.05 7.63 1/ 7.09 7.65 / 7.10 25.0 / 24.8 25.0 / 24.7 25.0 / 24.9 25.0 / 24.8 25.0 / 24.9 25.0 I/ 24.9 25.0 / 24.8 1 2 4 5 6 8.17 / 7.93 8.17 / 7.80 7.98 / 7.93 7.90 / 7.80 7.66 / 7.70 7.90 i/ 7.99 7.88 / 7.93 7.86 / 7.04 7.90 / 7.10 7.50 / 6.74 7.40 / 7.35 8.31 / 7.21 7.89 I/ 7.20 7.91 / 7.20 25.0 / 24.8 25.0 / 24.7 25.0 / 24.9 25.0 / 24.8 25.0 / 24.8 25.0 !/ 24.8 25.0 / 24.9 1 2 3 6/21/2004 6/22/2004 6/24/2004 24.00 23.83 23.95 134.00 142.00 146.00 47.00' 74.00 76.00 412 462 481 <0.1 <0.1 <0.1 0.2 1.5 1.0 42.00 59.00 217 Normal Hom. Var. NOEC LOEC ChV Method Survival 82 Growth GPI' Ifs': 82 >82 , >82 >82 Steers Stats Survival Conc. Critical 10.25 10 20.5 10 , >82 Steers Test Organisms t..:_ Cultured In -House Outside Supplier Hatch Date: 6/21/04 Hatch Time: 12:30-2:30 PM Overall Result ChV >82 Growth Calculated Critical Calculated 18 10 17 18 10 16 41 10 , 18 10 18 82 10 I 18 61.5 10 20 10 18 10 21 DWQ Form AT-5 (1/04) MERITECH Chronic Fathead Minnow Benchsheet. Transfer and Feeding Dates and Times Test Initiation Data: Start Date: •;):;) Start Time: 130 Initials/Signature: _ Date/Time Fed ci.r.::)./..-- Date/T.ime Born • Transfer Date Time Initials Day .1 '144) • Day 2 1,s, 4'4 -4:1/44 C-c(.. rg:?) Day 3. /int:A:DA— gc. Day 4 - Day 5- DaY 6 Test Termination Data: Initials/Signature: End Date: Date: End Time: )(.124).— # of Organisms per Chamber: IC. Test Vessel Size: r Test Solution Volume: Temp. of Stock: ;-)0')C., # of Reps: •Li Date Time 1 Day 0 f.;;? Day 1 Day 2 _D.a.y_3_ _ _ Day 4 Day 5 . Facility I i N PD ES # Dilution Water: .5..s\/...-f-t-110.(Vi.. Randomization: (YE§ NO Incubator #: Feeding Initials Time 2. Initials Time 3 Initials Lfcx.-)11-- SL— b :et prfL - 1 0 300 0,41 PrIA Day 6 I ' ‘.'l /1:14,:, SL. ttICK o'! , /S4 N r..7 • Chan-d1 7,nd..?h-yesi:.1a1 Deterrnins.-ii--ions Fa c 1 it y NPDES #K‹._CO5:),Lres.t Dates: S tartf, End Test Organism : Analyst Test Timel: Start Day COEIC • Ce,::,,--vtl,,,. 1 I 1 Z I .3 4 1 5 b [ / . I Reimarks - Temp. Initial I ,??.e," 7!.---';.:,,.:•2 I,..,I,r, ,:,3 "3'4 I :;.,-; .-.-: :9S X I ..;::-rs--7> ! . Final I :) '1. li'-: •,\ 4:: .- 1 .7) y ..4, .J7,4F-3 :?.%) PI -.),1,'"i I ',--i. '• U. 0. i n 1 z 1 al 1 t7.-ii, r'srcyce ;L. ?)(e) .1.3i,f, r-tq t -inal 1 3.-3:2 "71,:lic= IJ-c-L. le fi-7- •75 -c-i.---, PH 1 n i 1:1 a 1 1 L.`:1 /7?- c).1.,`:-; -.-S i!-, z•--- Pi. 'T51) 63...;" c,,- .‘l'?. ,111cz', F i nal I .:,.::. 0- r: f C. "?,,,q':'' C!.-7•2Z) • 75D 'iC,11.0 1 C.c.'.,,. 1 1 Alkalinity 1 -1-...J4-i ,...7,-;i'fli ----c.t --zsri1 1 I • . Hardne Ss . I !--c's k.3.7.;-s , 4:41 I , Conduct . Ini ti al'. 6.1 ‘`-",1 • :3.,-;;„ :.),-,-.4.7r- a:2cl ..,),0( 1 ,0.4...).., . 1 ;,77.-..: ! - Final I '.;.?;.--;.- ‘ :.-1.,--Q-?, Pi c-f 0 !:),42., Di'441 1.1',us,-5--_> ILA7:s 1 : Res. Chlorine I L.0,i Conc. R-11-1. I I I I 3 Temp. init±aJJ 2( lo 1.?1,‹ Final I q.S) I dV..)-- I Uay 4II o I / A's/ - 1:75," P.S 1,1f-N4:-.,s. 1 I , Remarks D .D. Initial I 1 , i-inalqi;;,-1rail'?-, 10 I pH initiaT,;;-4- Fcl- i na.I I • -7 .qpfg i I 7 &q. 1'45 . I 4-.3,:r 11.111 I 0,cici 7% G.& 17.V 1.71. 1 7.q.),--.) Ikr-Atil_ 11:inIc Hardness 1 1.1 .1 I 1 1 Conduct,.Iit1a1I3.7s- 12- 4g I I I Final I Li I Lit?: 11-.11-2TLI IV/,; I 1-1.St., I -C.z0 1,04-,;:' I ChiIt-t. 1 1 /..tD..k I if.),,; I Conc. I 1 1 2 I 3 Temp. in t I Final I I U.C. initial 1 . 1 Day 1 I 4 5 b 1 I 1 1 • 1 Remarks pH initial 18/p, 1 Final .1 1 1 1 1 . r6ne s s . I I 1 Mx: 1 '‘ I Con�uct.nit.ja11Lfl) Final Res.Chloririe 1 1 MERITECH, INC. FISH LARVAL SURVIVAL/GROWTH DATA SHEET CHRONIC FATHEAD MINNOW FACILITY: NPDES #: ;! DATE OF TEST: 5.:. € DATE WEIGHED: ORGANISM: PAGE' j ' OUTFALL;: INITIALS:' OF ' CONC REP. FOIL WT. (mg) FOIL WT. + ORG. (mg) WT. OF ORG. (mg) # ORG`. MEAN WT/ ORG. (mg) SURV % :� C.)e)1 c ,,} .11� .. �' i - I o ` - c. A 0)„ �a 1 1ti.:lt -1. tilt i 1' ,00 , 3s-14 Lob D } A i 6.�. , L L.,)� . ( • — - r.� C.s y ICJ , ' �, : [ t� c.'i B 11 �� a � . t € 1.0 ,C% , ; ci c C i Y Lei �'•.J ^).1.- f (`% ji%16 a. 11 �t MERITECH, FISH LARVAL SURVIVAL/GROWTH DATA SHE'ET CHRONIC FATHEAD MINNOW . , Reference Toxicant: )))c_tyr. DATE OF TEST: DATE WEIGHED: ORGANISM: A Ai f-410e1.1 PAGE •_:2- OF INITIALR; CONC REP. FOIL WT. (Mg) FOIL WT. + ORG. (mg) WT. OF ' ORG. (mg) # ORG. MEAN WT/ P'. (mg) SURV % A 1 -7 11-1&l. f c.,,./7/ •L.,' - 1-4:-/ 321> ,its e ) (a . - .''.4...11. fr_.) I. '''--- . 1 tr,`; 1 ,P (,...:.:... t>, . li,•\: /_..' . ) -C.PC:7 • -4'. 1 L' e 1 • -.' 7 I', k. 4.- ) . -/ tra 04. :0 4/,' / ix ( f—) " 1 i U.)• 1 CrD D .. ,,,,,,„ es `,,. i , ,.,•,.. ...,.. --7,1e, ., ..„,- ..7 ., -. ,. k2 . L,',,. A 17 -3 or, i",h4)(1- tq..if . .,...... .f.-.1 .3 b ..,-)DV t 0-o B a Ole, e 4i..) b i D. 6.20 • -,,,. !----°"---% ..--), '1 LI - . . 1 \...---.). ) .6(it...) L 0-,D R e . f / C,—/' 0 `... 1. r" () 05 • ,"7---.4'' 4 -2- . , ' , _ ".__'3 (.) — ( . • '' C--)C) D •idei A' . Lif7 0. • sti Lif I Li, . 1. L L.D ,, - A rl, 111.1,, 71 ,)-- g-. ,• t ,--- LC i t B 1 1. L.)-: .. J., ,..-4 , ( ,..,..,,,. Ol u pi /10..p ) 0.0 r (.7: r L1.41f-' (."-C) t L. f i''," [ ()' 1 I. I D i 13 •c-1( • t. ,...),-..., - t-r.:, it ., . i,f.-„s L t....);) MERITECH Mortality Data: Chronic Fathead Testi Start Date/Time i fie0.,-- End Date/Time ;- C2'd /f� Concentration _� :' �,: k Rep #1 Rep #2 Rep #3 Rep #4 Day 0 Day 1 Day 2 Day 3 Day 4 Day 5Day 6 Day 7 •c 0• 'C^ Concentration IC :3•C i Day 0 Day 1 Day 2 bay 3 Day 4 Day 5' Day 6 Day 7 c Rep :"1 Rep #2 Rep �j. G* ep �3 Rep #4 • Concentration Rep r1 Rep =2 Rep #3 Rep #4 Day 0 Day 1 Day 2 Day 3 Day 4, Day i - - 7 177.) .72) C_j 5 Day6 Day? ( .J MERITECH Mortality Data: Chronic Fathead Test Start Date/Time C:,;tir i End Date/Time'.> °4'..-_..; :' fi T,-- ConcentrationE- Rep #-1 Rep #2 Rep n3 •Rep r4 Day 0 Day 1 Day 2 Day 3 Day 4 Day 5. • f' ,1 tin -0 -0 73 C Cpncentration (s;[-j(. Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 , , Day 6 Day 7 1 C) 0 Rep #1 Rep #2 Rep #3 Rep #4 Cr' -) 1. Day 6 Day 7 1) C) D . ) Cam.• Concentration B / . Day 0 Day 1 Day 2 Day 3 Day 4 Rep #1 Rep #2 i `—) fj) '' I Day'5 Day 6 Reps 0 p L- / Day 7 Meritech, Inc. Bioas.sav Sample Chain of Custodj. 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 o�' Client Information Client: ('t1Cu`1� i43 . Contact: 5'11 hc•;,tg —tys i k erc� Address: iogiRcid.cc ' c. City: Rlo st; d Qc.; County: (1)0,cCQ.. State: NN1 Q Type of Facility Generating Effluent: Tel* ! C � i&evt: ula, �14C PO D# I��*- 1, •K1�C+l1 (_eaa NPDES #: Nc_,c(0 3 c4-5(.2 Phone: 91D 0S! - 3i Pipe Number: Zip: t.,V 3i5 was iltoc.-4 .r Sample Information Sampling Site: • fufN)Q'1t Sample Type: ✓ Grab Sampling Time: START Date: L at a4 END Date: 4 j a' j•a Sample Chilled (Covered with Ice): Yes ,✓ Collector's Name (Print): Collector's Signature: Composite Time: Time: 0 No of Containers o� �}U�1 PM PM Tni (Welty "Test Information Test Required: Chronic: V Test Organism: Ceriodaphnia Dubia: Y Acute: • TIC: okicity Test Concentration(s): List Any Special Requirements: Pimephales promelas: Mysidopsis balliiia: Ks ^(^' �� 1 li' 1�� 9 . Shipping Information 1 1 1 Relinquished By; ;D yl,L .t,I Date: (,10a/ 4 Time: lets(�PM Received By: /c (;. . /L' ;: ,,,-- Date: ‘ -z z- er. e•( Time: /D 61 AM PM Relinquished By: Date: Time: AM PM Received By: Date: Time:. AM PM Sample Temperature (C°): Method of Shipment: WTC(p/u) UPS Fed -Ex Circle One ' Other Sample Receiving (Laboratory Use Only) Received From: 1111n, sz- C Received By: , () C6-e Date: f_Q 0-/ Sample Temperature (C0): Q. 0,/ O. Sample Condition: Time': / d:c M pm / •Meritech, Inc. Bioassay Sample Chain of Custody 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 Client Information Client: InC.L.o 1 W Contact:-�^f�:r< . Br-1 Address: i 911 add or Rd City: .A b.er County: fy'i,^•cfk State: ri c. Type of Facility Generating Effluent: ?C; C_s.::t :cl,, 0.,io. c, 1,A9 PO'# Fcr►.i, NPDES # r4ic:0,39/5Cg Phone: °i. - 3 i q 14 Pipe Number: Zip: R i 1 Sample Information Sampling Site: F •} L I.A iT Sample Type: ✓ Grab Composite . # of Containers �2 Sampling Time: START Date: b aiz,:l Time: ?,r0 cmp pM END Date: t403/ 72. Time: n I7 �_ ; PM Sample Chilled (Covered with Ice): Yes — No , ' Collector's Name (Print): e+;,tt,,f . �r,;, cr r F1' Collector's Signature: 1, Toxicity Test Information Test Required: .Chronic: i✓ Acute: MC: i oxicity Test Concentration(s): List Any Special Requirements: Test Organism: Ceriodaphnia Dubia: �✓ Pimephales promelas: Mysidopsis Bahia: Shipping Information Relinquished By: ;,_,14:. A, Date: 0 Ce2736. Received B 1/ ' " ' Y /i% cr�L-��IC4.4^-Date: G •- G3 --a �/ Relinquished By: Date: Received By: Date: Sample Temperature (C°): Time: ;% iL-6 PM Time:/'././ (/ AM PM Timer ` AM PM Time: AM PM Method of Shipment: WTC(p/u) UPS Fed -Ex Circle One Other: Sample Receiving (Laboratory Use Only) Received From: I14(t, ite.b—OS Received By: 11/7 Date: Sample Temperature (C ): Sample tondr : Time: - 3M PM Meritech, Inc. .Bioassay Sample Chain of Custody', 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 Client Information Client: (Yltru,;;,c; e Contact: Address: tCP'4 Pt ccd..e('�cl. City: (A\•,Acc av—\ County: Der\ c)f k State: G C, 2c-136 C.<<iact 14. PO# f(\.;: NPDES #: :3° T.3bc2 Phone: ,9i0- 2Yi-31146. Pipe Number: NC Zip: , Type of Facility Generating Effluent: Sample Information Sampling Site: E-C c u Sample Type: ',- Grab Composite L✓•J�V i ;!��'L?.�i,# of Containers 3 : Dateatii osiTime: .;.. PM Date: i., 1 a5k`.) Time: 01, G PM Sample Chilled (Covered with Ice): Yes ✓ No Collector's Name (.Print): '" j t; ., c.-'' Sampling Time: START END Collector's Signature: l,,.v, Toxicity Test Information Test Required: Chronic: Acute: 'WC: u oxicity Test Concentration(s): List Any Special Requirements: Test Organism: Ceriodaphnia Dubia: ✓ Pimephales proinelas: Mysii dopsirrs//��balii a: 1 et\--hP..cd 1`Ll�0,:lv.ii a !/ r. Shipping Information Relinquished BY: Received By: Relinquished By:' Received By: Sample Temperature (C): Date: v(i,„ �( Ti:me:i 1125 , PM ate: � � y Time:%J•. : u b.pM Date: Time:, AM PM Date: Time: AM PM Method of Shipment: WTC(p/u) UPS Fed -Ex Circle One Other: Sample Receiving (Laboratory Use Only) Received From: Received By: ��,���:� Date: Cc�/c�c1 Sample Temperature (C°): /. 6/ / 6 Sample ondition: Tin1e:,�,>AM PM Title: Moore County Fish 6/22/04 File: Moore62204 Transform: NO TRANSFORMATION Shapiro - Wilk's Test for Normality D= W= 0.0677 0.9208 Critical W = 0.8840 (alpha = 0.01 , N = 24) W = 0.9160 (alpha = 0.05 , N = 24) Data PASS normality test (alpha = 0.01). Continue analysis. Title: Moore County Fish 6/22/04 File: Moore62204 Transform: NO TRANSFORMATION Bartlett's Test for Homogeneity of Variance Calculated B1 statistic = 18.7957 (p-value = 0.0021) Data FAIL B1 homogeneity test at 0.01 level. Try another transformation. Critical B = 15.0863 (alpha = 0.01, df = 5) = 11.0705 (alpha = 0.05, df = 5) Title: Moore County Fish 6/22/04 File: Moore62204 Transform: NO TRANSFORMATION Summary Statistics on Data TABLE 1 of 2 GRP IDENTIFICATION N MIN MAX ' MEAN 1 Control 4 0.3500 ' 0.51100.4108 2 10.25% 4 0.3540 0.4440! 0.3840 3 20.5% 4 0.3290 0.5590; 0.4025 4 41% 4 .0.4160 0.480 0.4203 5 61.5% 4 0.3040 0.4410 0.3913 6 82% 4 0.4160 0.4490' 0.4333 Title: Moore County Fish 6/22/04 File: Moore62204 Transform: NO TRANSFORMATION Summary Statistics -on Data TABLE 2 of 2 GRP IDENTIFICATION VARIANCE SD , SEM C.V. % 1 Control 0.0053' 0.0730 01 .0365 2 10.25% 0.0017 0.0414 0.0207 3 20.5% . , 0.0114 0.1069 0,0535 4 41% 0.0000 0.0057 '00028 5 61.5% 0.0039 0.0622 1 0.0311 6 82% 0.0002 0.0135 0.006.8- 17.7678 10.7898 26.5684 1.3513 15.8870 3.1217 Title: Moore County Fish 6/22/04 File: Moore62204 Transform: NO TRANSFORMATION Steel's Many -One Rank Test - Ho: Control<Treatment MEAN IN RANK GROUP IDENTIFICATION ORIGINAL UNITS SUM 1 Control 0.4108 2 10.25% 0.3840 17.00 3 20.5% 0.4025 16.00 4 41% 0.4203 2.0.00 5 61.5% 0.3913 18.00 6 82% 0.4333 , 21.00 CRIT. SIG VALUE DF 0.05 10.00 10.00 10.00 10.00 10.00 4.00 4.00 4.00 4.00 4.00 Critical values are 1 tailed ( k = 5 J' Department of Public Utilities Wastewater Treatment' Plant 1094 Addor Road Aberdeen, NC 28315 gilloaxe January 6, 2004 Re: EPA Expanded Requirements for Permit Renewal NPDES Permit No. NC0037508 Mrs. Valery Stephens NCDENR/D WQ/NPDES 1617 Mail Service Center Raleigh, NC 27699-1617 Telephone: (910) 281-3146 Facsimile: (910) 281-2047 Dear Mrs. Stephens: I received a letter in mid -December explaining that EPA had revised and expanded the application requirements for municipal permits. The new requirements mandate additional effluent testing: 1. Conduct 3 Priority Pollution Analysis (PPAs) 2. Conduct 4 toxicity tests for an organism other than Ceriodaphnia Our lab supervisor spoke with Charles Weaver (NPDES Unit) and Kevin Bowden (Aquatic Toxicology) explaining that the permit application was due and we had just found out about the additional tests. She was told to have a PPA and a Fat Head Minnow Toxicity test tun in January and 'then begin piggy backing with our regular quarterly testing starting in March. We will send the test results to you, Mr. Weaver and Mr. Bowden as we receive them. The tests for January have been scheduled for the week of the,18tn If additional information is needed, please do not hesitate to call me at 910-281-3146. Sincerely, l 'fames D. Frye, System Superintendent JDF/sab cc: Mr. Paul Rawls, Fayetteville Regional Office, DEM Mr. Steve Wyatt, County Manager Mr. Phillip Boles, Director of Public Utilities FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution. Control Plant NC0037508 Form Approved 1/14/99 OMB Number 2040-0086 SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Treatment Works. If the treatment works is required to have) a pretreatment program, or is otherwise required by the permitting following pollutants. Provide the indicated effluent testing information and any other information is has a design flow greater than or equal to 1.0 mgd or it has (or authority to provide the data, then provide effluent testing data for the required by the permitting authority for each outfall through which effluent discharged. Do not include information on combined sewer overflows collected through analyses conducted using 40 CFR Part 136 methods. In addition, these and other appropriate QA/QC requirements for standard methods for analytes not addressed below any data you may have on pollutants not specifically listed in this form. At a minimum, scans and must be no more than four and one-half years old. ' Outfall number: 001 (Complete once for each outfall discharging effluent in this section. All information reported must be based on data data must comply with' QA/QC requirements of 40 CFR Part 136 by 40 CFR Part 136. Indicate in the blank rows provided effluent testing data must be based on at least three pollutant i, , 1 to waters of the United S ates.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE Conc. Units Mass .Units Conc. Units Mass Units Number of . Samples ANALYTICAL METHOD MU MDL METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY ARSENIC < 0. 0051mg/1 < 0. 00 5mg/= 10; ' EPA200.8 BERYLLIUM I. CADMIUM < 0.002mg/1 < 0.002mg/. 10 EPA200.8 CHROMIUM < 0.005mg/1 <_0.005mg/� 10 EPA200.8. COPPER 0.042mg/1 0.029mg/: 29 EPA200.8l. LEAD 0 0.006mg/1 < 0.003mg/- 1Q EPA200.8 MERCURY 0, 0004mg/1 < 0.00J2mg/1 � I 10 ' - EPA245.1 NICKEL 0 0.007mg/1 < 0.005mg/1 •�' 10, EPA200.8 SELENIUM .0.00=mg/1 < 0.005mg/1 1 10; EPA200.8 SILVER 0 0.006mg/1 < 0.002mg/1 29i EPA200.8 THALLIUM ZINC 0 0.07Lmg/1 0.051mg/1 29' EPA200.8 CYANIDE B BDL mg/1 BDL mg/1 5' 335.3 TOTAL PHENOLIC COMPOUNDS 1 i HARDNESS (AS CaCO3) Use this space (or a separate sheet) to provide information on other metals requested by the pe mit writer. Aluminum 1.28 m /l , � 3.812mg/1 10L EPA200.8 Iron 1.402mg/ 3.76Cmg/1 101 EPA200.8 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 10 of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 • Outfall number: 001 ' (Complete once for each outfall discharging effluent to waters of the United States.) neu V nrenuen..� " AVERAGE DAILY DISCHARGE:: METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. Use this space (or a separate sheet) to provide information on other metals requested by the permit writer Mol bdenum Chloride. 39...mg/1 NO3+NO2-N 9.22 mg/1 4200.8 Page l0a of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 Form Approved 1/14i99 OMB Number 2040-0086 Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the Uriited States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE 1 ANALYTICAL METHOD MU MDL Conc. Units Mass Units Conc. Units Mass Units Number of , Samples VOLATILE ORGANIC COMPOUNDS. ACROLEIN i ACRYLONITRILE i. BENZENE BROMOFORM 1 CARBON TETRACHLORIDE l, CLOROBENZENE CHLORODIBROMO-METHANE ', 1 CHLOROETHANE I,! 2-CHLORO-ETHYLVINYL ETHER CHLOROFORM Ii I DICHLOROBROMO-METHANE 1,1-DICHLOROETHANE I 1,2-DICHLOROETHANE I I. TRANS-1,2-DICHLORO-ETHYLENE 1,1-DICHLOROETHYLENE 1,2-DICHLOROPROPANE 1,3-DICHLORO-PROPYLENE ETHYLBENZENE - i' METHYL BROMIDE METHYL CHLORIDE METHYLENE CHLORIDE . 1,1,2,2-TETRACHLORO-ETHANE 1 TETRACHLORO-ETHYLENE 1 , TOLUENE 1. " EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 11 of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 Form Approved 1/14/99 OMB Number 2040-0086 Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT • MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE \ ANALYTICAL METHOD MU MDL Conc. Units Mass Units Conc. Units Mass Units Number 1 of ; Samples 1,1,1-TRICHLOROETHANE I' 1,1,2-TRICHLOROETHANE TRICHLORETHYLENE I. VINYL CHLORIDE1. i. Use this space (or a separate sheet) to provide information on other volatile o genic compounds requested by the permit writer. I , ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL . 2-CHLOROPHENOL , 2,4-DICHLOROPHENOL 'I 2,4-DIMETHYLPHENOL 4.6-OINITRO-O-CRESOL 2,4-DINITROPHENOL i 2-NITROPHENOL 4-NITROPHENOL PENTACHLOROPHENOL I PHENOL 2,4,6-TRICHLOROPHENOL Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer: I, BASE -NEUTRAL COMPOUNDS. ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE BENZIDINE BENZO(A)ANTHRACENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 12 of 21 BENZO(A)PYRENE FACILITY NAME AND PERMIT NUMBER Moore County Water Pollution Control Plant NCO037508 Form Approved 1/1449 OMB Number 2(340-0086 Outfall number: nut (Complete once for each outfell discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE Conc. Units Mass Units Conc. Units Mass Units Number of Samples ANALYTICAL METHOD MU MDL 3,4 BENZO-FLUORANTHENE . . BENZO(GHI)PERYLENE r, 1 BENZO(K)FLUORANTHENE BIS (2-CHLOROETHOXY) METHANE I' BIS (2-CHLOROETHYL)-ETHER 1 BIS (2-CHLOROISO-PROPYL) ETHER I BIS (2-ETHYLHEXYL)'PHTIiALATE 4-BROMOPHENYL PHENYL ETHER BUTYL BENZYL PHTHALATE 2-CHLORONAPHTHALENE 4-CHLORPHENYL PHENYL ETHER CHRYSENE DI-N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE. DIBENZO(A,H) ANTHRACENE 1,2-DICHLOROBENZENE I • 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 3,3•DICHLOROBENZIDINE DIETHYL PHTHALATE DIMETHYL PHTHALATE 2,4-DINITROTOLUENE 2,6-DINITR0TOLUENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 13 of 21 • 1,2-DIPHENYLHYDRAZINE FACILITY NAME AND PERMIT NUMBER Moore County Water Pollution Control Plant NC0037508 Form Approved 1/14i99 . OMB Number 2040-0086 Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE , Conc. Units Mass Units Conc. Units 'Mass Units' Number 1 of 1 Samples .ANALYTICAL METHOD MU MDL FLUORANTHENE i FLUORENE HEXACHLOROBENZENE •• HEXACHLOROBUTADIENE - HEXACHLOROCYCLO- PENTADIENE „ . HEXACHLOROETHANE i INDEN0(1,2,3-CD)PYRENE ISOPHORONE NAPHTHALENE NITROBENZENE N-NITROSODI-N-PROPYLAMINE I N-NITROSODI- METHYLAMINE I • N-N ITRO S O D I-P H E N Y LA M I N E i PHENANTHRENE PYRENE 1,2,4-TRICHLOROBENZENE I Use this space (or a separate sheet) to provide information on other base -neutral .compounds requested by the permit writer. Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides) requested by the permit writer. END OF PART D. REFER TO THE APPLICATION OVERVIEW TO DETERMINE WHICH 2A YOU MUST COMPLETE , OTHER PARTS OF FORM EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 14 of 21 • • FACILITY NAME AND RMIT NILMft More County water Pollution Control Plant NC0037508. Form Approved 1/14/99 OMB Number 2040-0086 SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the pastI1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years' prior;to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronictoxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this' section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. I • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on ttie'cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. I . ' • If you have already submitted any of the information requested in Part E, you need not submit it again: Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using attemate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions) on which other sections of the form to complete. li E.1. Required Tests. Indicate the number of whole effluent Xchronic acute toxicity tests conducted in the past four and one-half years. , following chart for each whole effluent toxicity test conducted in the last four and one-half nears. Allow one E.2. Individual Test Data. Complete the column per test (where each species constitutes a test). Copy this page if Test number: more than Test -three tests are being reported. number. Test number: a. Test information. Result, Attached Test species & test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab (samples used. 24-Hour composite 1 Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each) 1 Before disinfection After disinfection N 1 After dechlorination 1 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 15 of 21 • FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NCCC37508 j Form Approved 1/14/99 OMB Number 204o-o086 Results Attached Test number:. ' Test number: number: .Test e. Describe the point in the treatment process at which the sample was collected. Sample was collected: f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both. Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If labora ory water, specify type; if receiving water, specify source. Laboratory water Receiving water l i. Type of dilution water. It salt water, specify "natural° or type of artificial sea salts or brine used. Fresh water Salt water - j. Give the percentage effluent used for all concentrations in the test series. I , i k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. r Acute: Percent survival in 100% . effluent " % ; % / %. • LC50 95% C.I. % ' % Control percent survival % 1 ' Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 16 of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 ! i Form Approved 1/14,99 OMB Number 204o-0086 'Chronic: NOEC - % % ° IC25 % Control percent survival % Other (describe) • m. Quality Control/Quality Assurance. - 1 Is reference toxicant data available? Was reference toxicant test within acceptable bounds? i' 1' What date was reference toxicant test run (MM/DD/YYYY)? Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatrnent works involved in a Toxicity Reduction Evaluation? I. _Yes X No If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information: If you have submitted of toxicity, within the past four and one-half years, provide the dates the information results. Date submitted: (MM/DD/YYYY) biomonitoring test information, was submitted to the permitting I I or information regarding the cause authority and a summary of the Summary of results: (see instructions) I , i END OF PART E. REFER TO THE APPLICATION OVERVIEW TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE.. • ;; EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 17 of 21 Effluent Toxicity Report Form - Chronic Pass/kai1 an Facility: MOORE CO WWTP Acute,LC50 Date: 12/11/03 NPDES#: NC0037508 Laboratory Perfor ing Test: MERITECH LABS, INC. X Signature �� tof Operator in�zMeffponsible Charge, *. Signature of Laboralto jf supervisor Pipe#: County: ROBESON Comments: ..* PASSED: -8.85% Reduction * Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 Environmental Sciences Branch Div. oflWater Quality N.C. DENR 1621 Maiil Service Center Raleigh,iNorth Carolina 27699-1621 10 11 12 # Young Produced Adult (L)ive (D)ead 22 Effluent %: 41% TREATMENT 2 ORGANISMS 1 22 2 17 3 20 4 24 5 25 6 25 25 18 12 26 24 # Young Produced 28 23 22 23 28 24,19 19 24 24 22 27 Adult (L) ive (D) ead L L •L L L L L L L- L L L pH Control Treatment 2 D.O. Control Treatment 2 1st sample lst sample 2nd sample 8.00 7.98 7.86 8.06 s t a r ' t lst sample e n d 7.86 7.08 7.77 7.09 8.01• 7.89 7.84 8.00 r t 1st sample e n d 7.74 7.15 7.90 7.12 8.05 8.04 8.02 8.04 s t, e a n r d t 2nd sample 7.77 7.08 7.83 7.03 LC50/Acute Toxicity Test (Mortality expressed as %, combinin Chronic Test Results ,'Calculated t = -1.285 Tabular t = 2.508 % Reduction = -8.85 % Mortality 8.33 Control 10.00 Treatment 2 Avg.Reprod. 21.67 Control 23.58 Treatment 2. Control CV I9.416% % control orgs producing 3rd brood 91:7% PASS FAIL Check One Complete This For Either Test Test Start Date: 112/03/03 Collection (Start) Date Sample 1: 12/01/03 Sample-2: 12/04/03 Sample Type/Duration Grab Comp. Duration Sample 1 Sample 2 Sample replicates) % % % % % % .% % % % X,' 24 hrs 24.1 hrs D I L U T 2nd lst P/F S S A A M M P P Hardness(mg/1) Spec. Cond.(µmhos). i Chlorine(mg/1) temp. at receipt(°C) 44 167 457 465 <0.1 <0.1 0.1 2.5 Concentration, Mortality LC50 = % 95% Confidence Limits % -- % Method of Determination Moving Average Probit Spearman Karber - 'Other ,start;/end Note: Please Complete This Section Also start/end Control High Cnnr pH Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) D.O. Effluent Toxicity Report Forzn - Chronic Pass/Fail 'and Ac LC50 Facility: MOCRE CO WWTP NPDES#: #: Laboratory Perforwing Test: MERITECH LABS, INC. S1.paLure Signature bf Operatcr i `P sponsible Charge A /'�/ or Laboratory Supervisor NC0037508 Pioett: i Date: 09/18/03 County: ROBESON Comments: t PASSED: -11.07% Reduction * :fork Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 Environmental Sciences Branch Div. oif Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 6 7 8 9 10 11 12 t Young "Produced • 19 20 17 27 24 23 17 19 18 21 16 23 Adult (L) ive (D) ead L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 n Young Produced 22 25 23 16. 15 22 23 28 25 25 23 24 Adult (L)ive (D)ead pH lst.sample Control Treatment 2 : D.O. Control Treatment 2 8.04 8.02 7.81 7.98 s t a r t 1st sample e n d 7.58 7.06 7.33 7.05 1st sample 8.03 8.01 7.75 7.89 s t a r t ,1st sample e n d 7.80 7.05 7.77 7.02 2nd sample 8.05 8.02 7.92 7.89 a r t 2nd sample e n d 7.66 7.11 7.58 7.04 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Chronic Test Results 'Calculated t. -1.563 Tabular t = 2.508 % Reduction = -11.07 % Mortality Avg.Reprod. 0.00 Control 20.33 Control 0.00 Treatment 2 22.58 Treatment 2 (Control CV 16.423% % control orgs producing 3rd- brood 91.7% . • r. I. PASS FAIL Check One Complete, This For Either Test Test Start Date: 09/10/03 Collection (Start); Date Sample 1: 09/08/03 Sample 2: 09/11/03 Sample Type/Duration Sample 1 Sample 2 Grab Comp', Duration 23.2 hrs 24.1 hrs D I L U T 2nd 1st P/F S A M S A M P Hai dness (mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at',receipt(°C) • % % Concentration Mortality start/end LC50 =• % 95%Confidence Limits .. o -- o Method of Determination Moving Average Probit Spearman Karber - Other 44 168 350 385 <0.1 •<0.1 0.2 0.2 • Note: Please Complete This Section Also Control start/end pH Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) High Conc. D.O. .Effluent Toxicity Report Form -. Chronic Pass/Fail and Acute ,. LC50 Date: 06/12/03 X S•gna"ture of Signature of Facility: AMERIC_1N WATER SERVICE-MOORE NPDES7: NC0037508 Laboratory Performing Test: MERITECH, INC. Operator in R/esponsible Charge - Latoratory Supervisor Work Order: MAIL 'ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 Pipe#: 001 County: MOORE Comments: PASSED: -2.89% Reduction * Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Wit Sexvice Center Raleigh',, North Carolina 27699-1621 9 10 11 12 n Young Produced 24 20 20 13 17 22 20 15 19 24 19 29 Adult (L)ive (D)ead L L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 25 21 22 20 18 23 16 19. 16 21 25 23 Adult (L) ive (D) ead pH 1st sample Control Treatment 2 D.O. Control Treatment 2 8.00 8.00 7.85 7.77 s t a r t 1st 1st sample 2nd sample 7.99 8.00 7.80 7.75 s e t n a d r t sample 1st 7.57 7.05 7.55 7.04 8.02 8.00 7.94 7..95 e t e n a n d r d t sample 2nd sample 7.80 7.03 7.84 7.05 7.67 7.09 7.61 7.04 LC50/Acute Toxicity (Mortality expressed Test as %, combining replicates Chronic Test Results Calculated t = -0.383 Tabular t = 2.508 % Reduction = -2.89 %i Mo'rtality Avg.Reprod. . 0.00 Control 20.17 Control ;, . 0 . 00 Treatment 2 20.75 ' Treatment 2 Control CV 21.232% % control orgs producing 3rd ..brood j 83.3% I ' PASS FAIL Check One CompletelThis For Either Test Test Start Dater 06/04/03 Collection•(Star:t) Date Sample 1: 06/02403, Sample 2:06/05/03 Sample Type/Duration 2nd 1st P/F Grab Comp.' Duration D I S S Sample 1 iX '24 hrs L A A U M M Sample 2 ' iX , 24 hrs T P P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine (mg/1) Sample temp. at receipt(°C) 42 160 354 415 <0.1 <0.1 1.5 1.7 % % % % % % % % % % % % % % % % % % % % Concentration Mortality LC50 = 95% Confidence Limits % -- % Method of Determination Moving Average _ Probit Spearman Karber Other -- start end Note: Please Complete This Section Also start/end Control pH Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) High Conc. D.O. 1,1 kk Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/13/03 Facility! AMERICAN WATER SERVICE-MOORE NPDESt: Laboratory Performing Test: MERITECH, INC. X r insponsible Charge Signature of Laboratory Supervisor, NC0037508 Pipe..=: 001 County: MOORE Comment s,: * PASSED: -15.14% Reduction * Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 Environmental Sciences Branch Div. of;Water Quality N.C. DEN?. 1621 Mail Service Center Raleigh Borth Carolina 27699-1621 5 6 7 8 9 '10 11 12 # Young Produced 18 16 18 20 17 18 18 17 21 19 19, 17 Adult (L) ive (D) ead Effluent %: 41% ' TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 21 20' 20 22 23 25 19 19 21 22 19, 20 Adult (L)ive (D)ead •L Chronic Test Results ,'Calculated t = -4.128 Tabular t = 2.508 % Reduction = -15.14 % Mortality Avg.Reprod. '„0M0 Control. 18.17 Control 0:00 Treatment 2 20.92 Treatment 2 Control CV p.725% % control orgs 'producing 3rd brood ' 100% PASS FAI Xjl Check One 1st sample 1st pH 'Control Treatment 2 D.O. Control Treatment 2 7.98 7.94 7.88 7.95 s t a r t 1st sample e n d 7.81 7.08 7.77 7.06 sample 2nd sample 7.99 7.95 7.86 7.95 s t a r t 1st e n, d sample 7.74 7.12 7.60 6.84 7.99 7.94 7.97 7.98 s t a r t 2nd e n d sample. 7.71 7.08 7.56 6.95 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete'This For Either Test Test Start Date:1 03/05/03 Collection (Star;t) Date Sample 1:,03/03/I03,, Sample 2: 03/06/03 Sample Type/Duration Sample 1 Sample 2 Grab Comp., Duration X 23.3 hrs Ix 22.5 hrs D I L U T 1st S A M P 2nd P/F S A M P Hardness(mg/1) Spec. Ccnd . (µmhos ) Ch]Jorine(mg/1) Sample temp. atIreceipt(°C) 46 174 380 457 <0.1 <0.1 0.5 0.5 % % % • o % % % % % % % % % % a % % % % % Concentrati do Mortality star:/end LC50 95% Confidence Limits % -- Method of Determination Moving Average _ Probit _ Spearman Karber _ Other Note: Please Complete This Section Also start/end Control j High • Organism Tested: Ceriodaphnia dubia Duration.(hrs): D.O. Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) • Effluent Toxicity Report Form - L Chronic, Pass/Fail and Acute;LC50 Date: 12/11/02 Facility: AMERICAN WATER SERVICE-MOORE -NPDES#: Laboratory Performing Test: MERITECH, INC. X ature o •perator ignature of Laborat onsible Charge upervisor NC0037508 Pipe#: 001 County: MOORE Comments: * PASSED: -6.78% Reduction * Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh; North Carolina 27699-1621 8 9 10 11 12 # Young Produced 28 30 30 29 • 2 9\ ,24 28 30 33 16 32 30 Adult (L)ive (D)ead Effluent %: 41% • TREATMENT 2 ORGANISMS 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 30 33 36 30 27 26 26 30 3.1 29 32 32 Adult (L) ive (D) ead Chronic Test Results Calculated t = Tabular t = % Reduction = -6.78 %, Mortality Avg.Reprod. 0E.00 Control 28.25 Control . O'L00 Treatment 2 30.17 Treatment 2 Control CV 15Y767% % control orgs producing 3rd brood 91.7% PASS FAI Check One pH Control Treatment,2 D.O. Control Treatment 2 1st sample 8.05 8.04 7.83 7.89 s t e a •n r d t 1st sample 7.65 7.10 7.72 7.02 1st sample 2nd sample 8.03 8.11 7.84 7.86 s t a r t 1st 8.06 8.04 7..86 7.98 s e t' e n a n d r d sample 2nd sample 7.62 7.04 7.58 7.03 7.63 7.02 7.71 7.06 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete;This For Either Test Test Start Date: 12/04/02 Collection (Start) Date Sample 1: 12/0202, Sample 2: 12/05/02 Sample Type/Duration Sample 1 Sample 2 Grab Comp'. Duration , 24 hrs IX 24 hrs D I L U T 2nd 1st P/F S A P S A P Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at;receipt(°C) 46 176 403 452 <0.1 <0.1 1.2 0.4 % % % % % % % A% % % % % % % % % % % % %. Concentration Mortality start end LC50 = '95% Confidence Limits % -- Method of Determination Moving Average - Probit Spearman Karber - Other Note: Please Complete This Section Also start/end Control High r,,nn pH Organism Tested: Ceriodaphnia dubia. Duration(hrs): D.O. Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/19/02 Facility: AMERICAN WATER SERVICE-MOORE NPDES#: NC0037508 Pipe#: 001 County: MOORE Laboratory Per ormin X is Test: MERITECH,.INC. ignature ot Operator-t Responsible Signature ot Laboratory pervisor Charge Comments: *.PASSED: 0.00% Reduction * MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS Environmental Sciences Branch Div. of water Quality N.C. DENR 1621 Mail Service Center Raleigh,'North Carolina 27699-1621 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 17 24 30 25 30 25 25 21 21 30 30 23 Adult (L)ive (D)ead L. Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 21 3 22 31 27 28 33 29 18 36 21 Adult (L)ive (D)ead L .. L L _32 Chronic Test Results Calculated t = Tabular t = % Reduction = � % Mortality Avg.Reprod. 0.00 ' • Control 25.08 Control 1' 8.33 Treatment 2 25.08 Treatment 2 Control CV 17.038% % control orgs producing 3rd brood 91.7% PASS FAI Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 8.12 8.13 7.89 7.98 s t a r t 1st sample e n d 7.55 7.07 7.57 7.04 1st sample 2nd sample 8.16 8.18 7.91 8.01 t a r t 1st 8.17 8.11 7.96 7.96 s e t e n a n d r d t sample 2nd sample 7.47 7.06 7.61 7.05 7.43 7.06 7.50 6.96 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either Test Test Start Date: 09/11/02 Collection (Start) Date Sample 1: 09/09/02 Sample 2: 09/12/09 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 X, 24 hrs L A A U M M Sample 2 , X: 22.6 hrs T P P Hardness (mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 46 180 442 454 <0.1 <0.1 1.7 0.1 % % % % % % % % % % % % % % % % % % Concentration Mortality start/end LC50 = 95% Confidence Limits % -- Method of Determination Moving Average Probit Spearman'Karber _ Other Note: Please Complete This Section Also start/end Control High Cnnn pH Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) D.O. Effluent Toxicity Report Form - Chronic Pass Fail and Acute LC50 Date: 06/13/02 Facility: AMERICAN WATER SERVICE-MOORE NPDES#: NC4037508 Pipe#: 001 County: MOORE Laboratory Performing Test: MERITECH, INC. X Signature of Operator in Responsible Charge /1141 Signature of La -oratory Supervisor Comments: * PASSED: -18.63% Reduction * Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail,Service Center Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2. 3 4 5 6 7 8 9 10 11 12 . # Young Produced 24 22 19 23 24 22 26 20 20 15 25 23 Adult (L)ive (D)ead Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young'Produced 24 29 24. 25 26 22 23 22 29 28 31 29 Adult (L)ive (D)ead 'Chronic Test Results Calculated t = -3.261 Tabular t = 2.508 % Reduction = -18.63 %� Mortality Avg.Reprod. 0.00 Control 21.92 Control jr 0:.00 Treatment 2 26.00 Treatment 2 Control CV 13,.820% % control orgs producing 3rd brood . 91.7% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample 2nd sample 8.11 8.07 7.93 8.06 8.05 8.06 7.84 7.89 8 .01 8.04 7.82 7.94 s s s t e t e t a n a n a r d r d r t •t t 1st sample 1st sample 2nd sample 7.68, 7.07 7.57 7.02 7.62 7.04 7.62 6.94 e n d 7.50 7.05 7.45 7.05 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates Complete This For Either Test Test Start Date: 06/05/02 Collection (Start)'Date Sample 1: 06/03/02 Sample 2: 06/06/02 Sample Type/Duration 2nd 1st P/F Grab Comp. Duration D I S S Sample 1 i X' 24.5 hrs L . A A U M M Sample 2 IX 24 hrs T P P Hardness(mg/1) Spec. Cond. (jimhos) Ch1orine(mg/1) Sample temp. atIreceipt(°C) 42 175 420 461 <0.1 <0.1 0.1 2.4 % % % % % % % % % % % % % % % % . % %' % % •Concentration 1, Mortality start LCSO = % 95% Confidence Limits % -- Method of Determination Moving Average Probit Spearman Karber Other Note: Please Complete This Section Also end start/end Control IpH; Organism Tested: Ceriodaphnia dubia Duration(hrs): High Conc. D.O. Copied from DWQ form AT-1 (3/87),rev. 11/95 (DUBIA ver. 4.41) EfilUent Toxicity Report Form - Chronic Pass/Fail and Acute'LC50 Date: 03/14/02 Facility:ERICAN WATER'SERVICE-MOORE NPDES#: NC0037508 Pipe#: 001 County: MOORE Laboratory Performing' Test: MERITECH, INC'. X . Signature o Operator in esponsible Charge Signature of Laborato pervisor Comments: *;PASSED: -23.08% Reduction * Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail1Service Center Raleigh, North Carolina 27699-1621 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 24 20 21 14 22 19 23 21 22 20 20 21 Adult (L)ive (D)ead L Effluent %: 41% . TREATMENT 2 ORGANISMS 3 4 7 8 9 10 11 12 # Young Produced 20 25 24 25 25 27 26 27 27 27 25 26 Adult (L) ive (D) ead L Chronic Test Results Calculated t = Tabular t = % Reduction = -23.08 Mortality Avg.Reprod. 0.00 j Control 20.58 Control 0.00 Treatment 2 . i 25.'33 Treatment !Control CV 12.160% % control orgs producing 3rd brood 91.7% PASS FAIL f Check Onel pH Control Treatment 2 D.O. Control Treatment 2 1st sample 7.66 7.70 7.55 7.73 s t a r t 1st sample e n d 7.60 7.62 7.60 7.57 1st sample 2nd sample 7.66 7.68 7.53 7.42 s t a r 1st 7.63 7.65 7.37 7.52 s e t n a d r t sample 2nd sample 7.58 7.03 7.73 7.17 e n d 7.62 7.24 7.62 7.22 LC50/Acute Toxicity Test' (Mortality expressed as % combining replicates Complete This For Either Test Test Start Date: 03/06/02 Collection (Start) Date Sample 1: 03/04/02 Sample 2: 03/07/02 Sample Type/Duration Sample 1 Sample 2 Grab Comp. Duration 24 hrs X, 24 hrs D I L U T 1st S A M M Hardness(mg/1) Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 4 4 1 ..... =- -....._... 17614E3 i . <0. <C._ 2.i % % % % % ., % % % % % % % % % % % % % % % Concentration Mortality start/end LC50 = 95% Confidence Limits Method of Determination Moving Average Probit _ Spearman Karber _ Other I Note: Pease Complete =hi_ Section : _sc Control tart/End pH Organism Tested: Ceriodaphnia dubia Duration(hrs): copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) High Conc. D.G. Effluent Toxicity Report Form - Chronic Date: 12/13/01 Facility: AMERICAN WATER SERVICE-MOORE NPDES#: NC0037508 Pipe#: 001'County: MOORE Laboratory Performing Test: MERITECH, INC. X Signature of Operator Responsible Charge Signature of Laboratupervisor Comments: * PASSED: -8.28% Reduction * Work Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL.ORGANISMS 1 2 3 4 Environmental Sciences Branch Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh; North Carolina 27699-1621 9 10 11 12 # Young Produced 22 30 27 28 22 23 22 27 25 30 29 29 Adult (L)ive (D)ead L L L LLLL L L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9' 10 11 12 pH Young Produced 28 29 28 32 23 21 29 28 30 29 33 30 Adult (L)ive (D)ead L L L Control Treatment 2 D.O. Control Treatment 2 LLLLLLL lst sample 1st sample 2nd sample 8.06 8.11 7.81 7.93 8.09 8.12 7.80 7.93 8.10 8.11 8.02 7.95 s s s t e t e t e a n a n a r d r d r d t t t lst sample lst sample 2nd sample 7.67 7.22 7.58 7.06 7.75 7.30 7.58 7.07 7.78 7.27 7.66 7.32 LC50/Acute Toxicity Test Chronic Test Results Calculated t'= -1.612 Tabular t = 2.508 % Reduction = -8.28 % Mortality Avg.Reprod. I 01.00 (Control 26.17 Control ' 0'.00 Treatment 2 28.33 Treatment 2 Control CV ;12.285% % control orgs producing 3rd " brood 100% PASS FAIL Check One Complete This For Either Test Test Start Date 12/05/01 Collection (Start) Date Sample 1: 12/03401 Sample 2: 12/06/01 Sample Type/Duration Sample 1 Sample 2 Grab Comp. Duration SIX ! 24 hrs X 24 hrs 2nd lst P/F D I S S L A A U M M T P P Hardness(mg/1) 'Spec. Cond.(µmhos) Chlorine(mg/1) Sample temp. at ;receipt(°C) 46 197 435 520 <0.1 <0.1 1.0 0.1 (Mortality expressed as % combining replicates . % % % % % J % % % % % % % % % % % % % % % Concentration'' Note: Please Complete This Section Also Mortality start•/end . start/end LC50 = 95% Confidence Limits o Method of Determination Moving Average Probit Spearman Karber Other Control Organism Tested: Ceriodaphnia dubia Duration(hrs): High Conc. D.O. Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Date: 09/19/01 Facility: AMERICAN "LATER SERVICE-MOORE NPDES#: NC0037508 Pipe#: 001 County: MOORE Laboratory Performing Test: MERITECH, INC. x Signature of Opera iEfor in Responsible Charge ,--- Signature of Labox'a ¢''`y Supervisor Comments: * PASSED: -19.17% Reduction * [Mork Order: MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Environmental Sciences Branch Div. of Water Quality N.C. pENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10.11 12 # Young Produced 18 22 22 23. 21 22 17 10 25 20 22. 18 Adult (L)ive (D)ead •L Effluent %: 41% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced 24 24 23 22 22 25 22 23 24 24 28 25 Adult (L)ive (D)ead . Chronic Test Results 'Calculated t = Tabular t = % Reduction = -19.17 ,% Mortality Avg.Reprod. 0.00 Control 20.00 Control 0.00 Treatment 2 23.83 Treatment 2 Control CV 19.540% % control orgs producing 3rd brood 100% PASS FAIL Check One pH Control Treatment 2 D.O. Control Treatment 2 1st sample 1st sample '2nd sample 8.15 8.17 7.98 8.07 s a r t. 1st sample e n 7.97 7.30 7.98 7.50 8.13 8.19 8.03 8.07 s t a r t ,lst 8.10 8.15 8.04 8.17 e t e n a n d r d t sample 2nd sample 7.85 7.45 7.58 7.26 7.72 7.51 7.62 7.30 LC50/Acute Toxicity Test (Mortality expressed as %, combining. replicates) Complete This For Either Test Test Start Date: 09/12/01 Collection (Start) Date Sample 1: 09/10/01 Sample 2: 09/13/01 Sample Type/Duration Sample 1 Sample 2 Grab Comp. Duration X' 24 hrs 24.1 hrs 2nd 1st P/F D I S S L A A U M M T P P Hardriess(mg/1) Spec. ,Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt(°C) 46 175 462 485 <0.1 <0.1 1.7 0.3 % Concentration Mortality LC50 95% Confidence Limits -- Method of Determination Moving Average Probit Spearman Karber _ Other start/end Note: Please Complete This Section Also start/end Control High 1 D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs): Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) r. MER1TECHI INC. ENVIRONMENTAL LABORATORIES A Division .Of Water Technology and Controls, Inc. Client: Moore County WWTP ' Date Sampled 109/25/03 1094 Addor Rd Digested II 99/25/03 Aberdeen, NC 28315 Analysis 110/03/03 Attention Stephanie Brixey Analyst: PI I NPDES # NC0037508 EPA 1631 Low Level Mercury Analysis Meritech ID # Sample ID Result Reporting Limit MBLK1003B Method Blank <0.5 ng/L 0.5,ng/I M09250309 Field Blank < 1.0 ng/L 1 1.0 ng/1 i M09250310 Plant Effluent 16.3 ng/L (.1.0'ng/1 I hereby certify that 1 have reviewed and approve these data. Laboratory Representative 642 Tamco Road • P.O. Box 27 • Reidsville, NO7320 (336) 342-4748 • (336) 342-1522 Fax Client: Moore County WWTP 1094 Addor Rd Aberdeen, NC 28315 Attention Stephanie Brixey NPDES # .NC0037508 MERITECK • ENVIRONMENTAL LABORATORIES A Division of Water Technology and Controls', Inc. I Date Sampled :'12/Q8/03 Digested. 12/08/03 Analysis 1,2/11/03. Analyst: ; ' EH EPA 1631 Low Level Mercury Analysis 1 ' , Meritech ID # ' Sample ID • Result • ' Reporting Limit MBLK1211B MethOd.Blank ' <,0.5 ng/L O. !ng/1 M12080301 Field Blank ' < 1.0ng/L !I'M ng/l .- • M12080302 Effluent 11.8 ng/L .1.0 6g/I ; .. I hereby certify that I have reviewed and approve these data. aboratory Repre'sentative !. 1 642 Tamco Road • P.O. Box 27 • Reidsville, NC27320. (336) 342-4748 • (336) 342-1522 Fax FAC1 JTY NAME AND PERMIT NUMBER: Moore County Water Pollution Control Plant NC0037508 Fomi Approved 1/14/99 OMB Number 2040-0086 SUPPLEMENTAL APPLICATION INFORMATION PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which, receive RCRA,'CERCLA, or other remedial wastes must. complete Part F. GENERAL INFORMATION: F.1. Pretreatment Program. • Does the treatment works have, or is it subject to, an approved pretreatment, program? XYes No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (ClUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. I , a. Number of non -categorical SIUs. b. Numberof'CIUs. 1 1 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. I; F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Intek I Mailing Address: 105.Taylor Street Aberdeen, NC 28315 F.4. Industrial Processes. Describe all of the industrial processes that affect or contribute to the SIU's discharge. F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. - , Principal product(s): woven polyester fabric polyester yarn -dyes Raw material(s): F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 159,407 gpd ( X continuous or intermittent) • b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. I gpd - (continuous or intermittent) 1 F.7. Pretreatment Standards. Indicate whether the SIU. is subject to the following: • a. Local limits X Yes No b. Categorical pretreatment standards _Yes X No If subject to categorical pretreatment standards, which category and subcategory? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 18 of 21 FACILITY NAME AND PERMIT NUMBER: Moore County Water Pollution' Control Plant NC003750 Form Approved 1/14/89 OMB Number 2040.0086 F.8. Problems at the Treatment Works Attributed to Waste Discharged by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years?. - Yes X'No If yes, describe each episode. RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years _No,(go to F.12.) received RCRA haliardous or mass, specify units). Units waste by truck; rail, or dedicated pipe? _Yes F.10. Waste Transport. Method by which RCRA waste is received (check all that apply): Truck Rail Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume EPA Hazardous Waste Number Amount . , i CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remedlation Waste. 'Does the treatment works currently (orhas it peen notified Yes (complete F.13 through F.15.) . ' that it will) receive waste'from and future site. other remedial waste remedial activities? - 1 . originates (or is expected to originate in 'I _No , Provide a list of sites and the requested information (F.13 - F.15.) for each current F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or ' ' the next five years). • F.14. Pollutants. List the hazardous constituents that are received (or are, expected to be received). Include • (Attach additional sheets if necessary). data on 'volume and concentration, if known. F.15: Waste Treatment. a. Is this waste treated (or will it be treated) prior to entering the treatment works? No •• 1 _Yes If yes, describe the treatment (provide information about the removal efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? Continuous If intermittent, describe - discharge schedule. _Intermittent - • • END OF PART F: REFER TO THE APPLICATION OVERVIEW TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE 1 '' ' EPA Form 3510-2A (Rev. 1-99). Replaces EPA forriis 7550-6 & 7550-22. Page 19 of 21 0310812004 15: 39 9102812047 1 MOORE COMITP PAGE 02/03 FACILITY NAME AND PERMIT pNUMBER: moot C iur Lf 1 DtJJa Uu)ttcA CDf1kio1 Nay} NC po394og SUPPLEMENTAL APPLICATION INFORMATION Farm Approved 1/14199 • OMB Number 2040.0086 .PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant Industrial users or which receive RCRA, CERCIA, or other remedial wastes must complete Part F. GENERAL INFORMATION: F.1. Pretreatment Program. Does the treatment works have, or is it subject to, an approved pretreatment program? Yes No F.2. Number of Significant Industrial Users (Sills) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of Industrial users that discharge to the treatment works. a. -Number of non -categorical SIUs. b, Number of CIUs. SIGNIFICANT INDUSTRIAL. USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Mailing Address: �c c0\1C1C CI. abak dew N 3IS F.4. Industrial Processes. Describe all of the Industrial processes that affect or contribute to the SIU's discharge. F.6. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materiels discharge. Principal product(s); C. DL),N 'C CAS Raw materlal(s): F.6. Flow Rate. hat affect or contribute to the SIU's 53}.LL\ Coated.. u,,1 rh c\i c�s►.�zinc, oc load cbicizr a. Process wastewater flow rate, Indicate the average daily volume of process wastewater discharged Into the collection system in gallons per day (gpd) and whether the discharge Is continuous or intermittent 1 % t . 500 gpd ( X continuous or Intermittent) b. Non -process wastewater flow rate, Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or Intermittent, gpd (____continuous or intermittent) _ F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits X Yes No b. Categorical pretreatment standards ,,-,Yes No If subject to categorical pretreatment standards, which category and subcategory? `l0 CAR '413 e.lac.koQtaki n0 EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 & 7550-22. Page 16 of 21 034181200,4 15:39- 9102812047 MOORE COWWTP PAGE 03/03 FACILITY NAME AND PERMIT NUMBER: f''rkzort r�n UJa.NQC �01WAill n eAtt (bl` 1 leant. r4 C OD3'1504 I' Form Approved 1/14199 OMANumber 2040-0086 F.B. Problems at the Treatment Works Attributed to Waste Discharged by the SIU. Has.the SIU caused upsets, interference) at the treatment works In the past three years? or contributed to any problems (e.g., _Yes, )( No IF yes, describe each episode. . I. RCRA HAZARDOUS• WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous Yes' _No (go to F.12.) F.10. Waste Transport. Method by which RCRA waste is received (check all that apply): _ -Truck Rail 'Dedicated Plpe waste by truck, rail, or dedicated pipe? ; - i F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass: specify units): EPA Ha73r,ctpMs Waste Number Amount Units i CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12, Remadlatton. Waste. Does the treatment works currently (or has it been notified that ti well) receive waste • Yes (complete F.13 through F.15.) No Provide a list of sites and the requested Information (F.13 - F.15.) fat each current and future site. F.13. Waste Origin, Describe ttie site and type of facility at which the CERCLAIRCRAIor other.remediel waste the next five years). from remedial activities? 1 originates (or is expected to originate in F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include (Attach additional sheets If necessary). data on volume and concentration, if known. F.15, Waste Treatment . a. Is this waste treated (or will It be treated) prior to entering the treatment works? Yes No If yes, describe the treatment (provide Information about the namoval efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? _Continuous Intermittent If intermittent; describe discharge schedule. •" I • r END OF PART F. REFER TO THE APPLICATION OVERVIEW TO DETERMINE WHICH' 2A YOU MUST COMPLETE OTHER PARTS OF FORM - H 1 EPA Form 3510-2A (Rev, 1-99). Replaces EPA forms 7550-8 & 7550-22. Page 19 of 21 Pretreatment Annual Report (PAR) Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe Enter BDL values as < (value) Total # of samples => Maximum (mg/1) _> or Maximum (lb/d) => or 6-month-using BDL Average (mg/1) => : -- `or Average Loading (Ib/d)_> - % violations,(chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> Total # of samples => Maximum (mg/1) _> or Maximum (lb/d) => or 6 month using BDL Average (mg/I) => or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> 'Total # of samples => Maximum (mg/1) => or Maximum (lb/d) _> or 6 month using BDL Average (mg/1) => or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) => Control Authority, Town Name => Moore County WWTP Name => Moore County WPCP NPDES # => NC0037508 lst 6 months, dates => 01-01-02 06-30-02 2nd 6 months, dates => 07-01-02 12-31-02 Industry Name Intek Corporation 1UP # A004 Pipe # 001 Flow, mgd BOD TSS Ammonia 1st 6 months 2nd 6 months lst 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 176 171 10 10 10 10 1 0 0.324 0.346 - 226 213 320 180 12.6 N / A 0.138 0.170 118 89 185 . 131 12.6 -- -N/A 0 0 0 - 0 0 0 N/A N/A 0 0 0 0 0 0 N/A .N/A Arsenic Cadmium Chromium COD 1st 6 months 2nd 6 months, 1st 6 months 2nd 6 months 1st 6 months . 2nd 6 months 1st 6 months 2nd 6 months. 1 1 1 1 1 1 10 - 10 < 0.005 < 0.005 < 0.001 < 0.001 <0.002 < 0.002 1648 1192 - < 0.005 < 0.005 < 0.001 < 0.001 < 0.002 < 0.002 1018 869 N/A N/A N/A N/A - N/A N/A 0 0 N/A N/A N/A N/A N/A N/A 0 0 Copper Cyanide Lead Mercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months I - 1 0 0 1 1 1 1 < 0.002 0.005 N / A N / A _ < 0.005 < 0.005 < 0.00020 < 0.00020 < 0.002 0.005 N / A N / A < 0.005 < 0.005 < 0.00020 < 0.00020 0 0 N/A N/A N/A N/A N/A N/A 0 0 N/A N/A N/A N/A N/A N/A * POTW must enter at least one of these four rows, Please indicate how averages were calculated Avg period could be month, Qtr, or 6-month & if BDL , 1 /2BDL, or zero values used. BDL => Below Detection Limit IUP => Industrial User Permit SNC => Significant Non -Compliance TRC => Technical Review Criteria mg/1=> milligrams per liter lb/d => pounds per day mgd => million gallons per day WWTP => wastewater treatment plant Chapter: PAR Guidance File name: PAR_IDSF.xIsakr iSiohebstime/ Q 1c 1il flttr 9, section B, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe - Page Pretreatment Annual Report (PAR) Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe Enter BDL values as < (value) Total # of samples => * Maximum (mg/I) _> - * - or Maximum (1b!d) _> - * or 6 month using BDL Average (mg/1) _> - * or Average Loading (lb/d) => % violations, (chronic SNC is>= 66%) _> % T'RC violations, (SNC is >= 33 %) _> Total # of samples => * Maximum (mg/I) => * or Maximum (lb/d) => * or 6 month using BDL Average (mg/1) => * or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) => % TRC violations, (SNC is >= 33 %) _> Total # of samples => * Maximum (mg/1) _> * or Maximum (1b/d) _> * or 6 month using BDL Average (mg/1) _> * or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> Industry Name Intek Corporation IUP # A004 Pipe # 001 NO2 + NO3 Total Phos Barium Beryllium lst 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1 0 1 0 1 1 1 1 <0.50 N/A 1.40 N/A 0.012 _0.012_ <0.001._ <0.001_.- <-0.50— " --N/-A ------- 1.40 -- = N-/'A -0.012 -- 0012 - <0.001 <0.001 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A TTO 1st 6 months 2nd. 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1 1 <0.10 <0.10 < 0.10 <0.10 N/A N/A N/A N/A , 1st 6 months 2nd 6 months lst 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months * POTW must enter at least one of these four rows, Please indicate how averages were calculated Avg period could be month, Qtr, or 6-month & if BDL , 1/2BDL, or zero values used. BDL => Below Detection Limit IUP => Industrial User Permit SNC => Significant Non -Compliance TRC => Technical Review Criteria mg/I => milligrams per liter lb/d => pounds per day mgd => million gallons per day WWTP => wastewater treatment plant Chapter: PAR Guidance File name: PAR_IDSF.xIs I vi iohe eA'iigilq 1cli6ikr 9, section B, pages 12, 13, 14 Blank IDSF Fonn, Copy and use in your PAR Number each set for each IUP pipe - Page of Pretreatment Annual Report (PAR) Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe Enter BDL values as < (value) Total # of samples => * Maximum (mg/1) _> * or Maximum (lb/d) => * or 6 month using BDL Average (mg/1) => -- *_ _ _---or-Auerage.Loading (lb/d)--> - % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %),=> Total # of samples => * Maximum (mg/1) _> * or Maximum (lb/d) _> * or 6 month using BDL Average (mg/1) _> * or Average Loading (lb/d) _> % violations,'(chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> * Total # of samples => or 6 month using BDL Average (mg/1) => or Maximum (lb/d) => or Average (mg/1) _> - or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) => TRC violations, (SNC is >= 33 %)'=> Industry Name Intek'Corporation IUP # A004 Pipe # .001 Nickel Selenium Silver Zinc 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months. 2nd 6 months 1st 6 months 2nd 6 months 1 1 1 1 1 1 1 l < 0.005 < 0.005 < 0.005 < 0.005 < 0.002 < 0.002 0.096 0.074 <0.005 < 0.005 < 0.005 < 0.005 < 0.002 - - < 0.002 0.096 -- 0.074 N/A - N/A N/A N/A N/A N/A N/A N/A N/A . N/A N/A 'N/A N/A N/A N/A N/A • pH Oil & Grease Aluminum• Antimony 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6-months 1st 6 months 2nd 6 months 10 10 22 17 2 1 1 1 7.59 7.80. 52' 66 0.12 0.20 0.25 0.37 N/A N/A 25.5 20.2 0.11 0.20 0.25 0.37 0 0 0 0 - `N/A. N/A N/A -N / A 0 0 - 0 0 N/A N/A N/A N/A Fluoride Chloride Molybdenum TKN 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1 1 1 1 1 0 1 0 0.85 0.87 4.6 4.1 < 0.002 N/A 18 N/A 0.85 0.87 4.6 4.1 <0.002 N/A 18 . N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A. N/A N/A N/A 4* POTW must enter at least one of these four rows, Please indicate how averages were calculated Avg period could be month, Qtr, or 6:month & if BDL , 1/2BDL, or zero values used. BDL => Below Detection Limit IUP => Industrial User Permit SNC => Significant Non -Compliance TRC => Technical Review Criteria mg/1=> milligrams per liter lb/d => pounds per day mgd => million gallons per day - WWTP => wastewater treatment plant Chapter: PAR Guidance File name:PAR_IDSF.xlsaLamgieheiskeAC1 lKh&itthr 9, section B, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe - Page of Pretreatment Annual Report (PAR) Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe Enter BDL values as < (value) Total # of samples => * Maximum (mg/I) => * or Maximum (lb/d) _> -*. — or'6 month using BDL Average (mg/1) _> * _ __ ._==or_Average-Loading (lb/d) _> % violations,(chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 -%) _> * Total # of samples =>. Maximum (mg/I) _> .. or Maximum (lb%d) _> or 6 month using BDL Average (mg/1) _> or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> Total # of samples => Maximum (mg/1) => or Maximum (Ib/d) _> or 6 month using BDL Average (mg/1) _> or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) => % TRC violations, (SNC is >= 33 %) _> ' Control Authority, Town Name => Moore County WWTP Name => Moore County WPCP NPDES # => NC0037508 1st 6 months, dates => 01-01-02 to 06-30-02 2nd 6 months, dates => 07-01-02 to 12-31-02 Industry Name Erico Incorporated IUP # A005 Pipe # 01. Flow, mgd BOD . TSS Ammonia . 1st 6 months. 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months . 2nd 6 months- 178 173 6 0 ** 6 0 ** 5 0 0.030 0.028 12 N/A 2 N/A 2.17 N/A 0.0158 0.0144 5.8 N/A - <2 N/A 1.25 - -N/A 0 0 0 0 0 0 N/A N/A 0 0- 0 . 0 0 0 • N/A N/A Arsenic Cadmium Chromium - COD 1st 6 months ' 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1 0 11 10 " 6 1 6 0 ** <0.00,5 = N/A <0.002 <0.002 0.009 - 0.021 21• .; N/A <0.005 • N/A <0.002.. <0.002 0.002 0.021 14 N/A N/A • N/A 0. . 0, 0. 0 0 . 0 N/A N/A . 0 - 0 0 0 0 0- Copper Cyanide Lead . . Mercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 11 10 2 1 5' 1 1 0 0.600 0.295 < 0.005 < 0.005 < 0.005 < 0.003 < 0.00020 N, / A 0.099 0.150 < 0.005 . . < 0.005 < 0.005 < 0.003 • < 0.00020 N / A 0 0 0 0 0 0 N./A N/A 0 0 0 0 0 0 N/A N/A * POTW must enter at least one of these four rows, Please indicate how averages were calculated Avg period could be month, Qtr, or 6-month & if BDL , 1/2BDL, or zero values used. ** See Narrative BDL => Below Detect on Limit IUP => Industrial Use Permit ' SNC => Significant Non -Compliance TRC => Technical Review Criteria mg/1 mill => !grams per liter Ib/d => pounds per day mgd,=> million gallons per day WWTP => wastewater treatment plant Chapter: PAR Guidance File name: PAR IDSF.xlstRitnisiehathatimeA1i i , lchllptIor 9, section B, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe - Page of Pretreatment Annual Report (PAR) Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe Enter BDL values as < (value) Total # of samples => * Maximum (mg/1) _> " _ _ = or Maximum (lb/d) => -=or 6-1honth=using -BDL-"Average-(mg/1) _> * or Average Loading (lb/d) => % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> Total # of samples => Maximum (mg/1) _> * or Maximum (Ib/d).=>_ * or 6 month using BDL Average (mg/1) _> * or Average Loading (lb/d) _> % violations, (chronic SNC is >= 66%) =>" • % TRC violations, (SNC is >= 33: %). => Total # of samples _> * _ Maximum (mg/I) _> * or Maximum (Ib/d) _> * or 6 month using BDL Average (mg/1) _> * or Average Loading (lb/d) _> % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is.>= 33 %) _> Industry Name Erico Incorporated IUP # A005 Pipe # : 01 Fe Molybdenum TKN NO2 + NO3 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months lst 6 months 2nd 6 months 1st 6 months 2nd 6 months 1 0 1 0 5 0 •1 0 0.051 N / A 0.074 N / A __ . _ _ _4.70__ __ _ _ N./ A -- _ - -- 0.7-1----- - ---N -/-A- -- - - 0:05-1 N/A 0.074 N/A 2.52 N/A 0.71 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A . N/A , N/A - N/A Total Phos TTO lst 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1 0 1 0 0.21 N/A .. <0.10 N/A 0.21 N / A < 0.10 Certifies for - TTO as not N/A N/A N/A being •,- . N / A. " N / A N / A present 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months * POTW must enter at least one of these four rows, Please indicate how averages were calculated Avg period could be month, Qtr, or 6-month & if BDL , 1/2BDL; or zero values used. BDL => Below Detection Limit IUP => Industrial User Permit SNC => Significant Non -Compliance TRC => Technical Review Criteria ing/1=> milligrams per liter lb/d => pounds per day mgd => million gallons per day WWTP => wastewater treatment plant 4 Chapter: PAR Guidance File name: PAR _!DSF.xlsl'lbmnisiehadritimerC'i ; lch>IPttzr 9, section B, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe - Page of Pretreatment Annual Report (PAR) Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe Enter BDL values as < (value) Total # of samples => Maximum (mg/I) => or Maximum (lb/d) => or 6 month using BDL Average (mg/I) _> -- or Average -Loading (Ib/d) => % violations, (chronic SNC is >= 66%) _> % TRC violations, (SNC is >= 33 %) _> Total # of samples => Maximum (mg/1) _> * or Maximum (1b/d) _> * or 6 month using BDL Average (mg/1) _> * or Average Loading (lb/d) _> % violations, (chronic SNC is >= 66%) _> % TRC-violations, (SNC is >= 33 %) _> * * Total # of samples => Maximum (mg/1) _> or Maximum, (lb/d) _> or 6 month using BDL Average (mg/1) => or Average Loading (Ib/d) _> % violations, (chronic SNC is >= 66%) => % TRC violations, (SNC is >= 33 %) _> Industry Name Erico Incorporated IUP # A005 Pipe # 01 Nickel Selenium Silver Zinc 1st 6 months 2nd 6 months 1st 6 months 2nd 6. months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 11 10 1 0 6 1 6 1 0.100 0.273 < 0.005 N / A < 0.005 < 0.005 < 0.025 < 0.025 0.007 0.094 < 0.005 -N / A < 0.005 < 0.005- < 0.025 - < 0.025- 0 0 N/A N/A 0 0 0 0 0 0 N/A N/A 0 0 0 0 pH Oil & Grease- Chloride Aluminum 1st 6 months 2nd 6 months 1st 6 months - 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 12 10 1 1 5 1 2 1 9.83 9.69 1.8 21.0 26 139 0.75 0.29 N/A N/A 1.8 21.0 12 139 0.43 0.29 0 0 0 0 N/A N/A N/A N/A 0 0 0 0 N/A N/A N/A N/A Fluoride Barium Beryllium Antimony 1 st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months _ 2nd 6 months 1 0 1 0 1 0 1 0 0.84 N/A <0.625 N/A <0.001 N/A 0.005 N/A 0.84. N/A <0.625 N/A <0.001 N/A 0.005 N/A N/A N/A - N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A * POTW must enter at least one of these four rows, Please indicate how averages were calculated Avg period could be month, Qtr, or 6-month & if BDL , 1/2BDL, or zero values used. BDL => Below Detection Limit IUP => Industrial User Permit SNC => Significant Non -Compliance TRC => Technical Review Criteria mg/1=> milligrams per liter lb/d => pounds per day mgd => million gallons per day WWTP => wastewater treatment plant • • Chapter: PAR Guidance File name: PAR_IDSF.xls(Ron iohmlati¢.eiCi grist, IGIMPtkr 9, section B, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe - Page of MOORE COUNTY WATEPLUTION CONTROL PLANT S. R. 1100, 4 MILES S.E. OF PINEBLUFF, NO. CAR. 28373 4 G ? �4',`°' P � P o GOAOo� O 1.0-13.4 m g.d. SE\/AGE :UENT ,ISr'oSAL I t • 1.0-13.4 m.g.d. 0 -13.4 1 mq.d.. Return Activated 0-6.7mr.d. B.O.P. Make -Up 0 -1.4 m.q.d. ---PRIMARY SLUDGE _ .LWASTE ACTIVATED - -SLUDGE---- THICKENER • -&N A-E-R 0•B I C DIGESTER SLUDGE I 1.0 -13.4 * rn.g.dl • t �� ' .., GPO ? ‹' e p?� GPO Return Activated 0-6.7m.a.d, J SLUDGE DRYING BEDS Drainage to Raw Sewage Influent 1.0 -13.4 , m.g.d. EFFLUENT Discharge 001 6,7 MGD ° Land Application ° Llrrifill Subtitled "1)" ;�:; PROCESS FLOW SCHEMATIC •1. r (,1• `� '„ r• t:inicblu(fis --.- • .7 • _ y / / / /\ 7..1 �J C• =J •. • •` Lam. �.•� 1094 Addor Road : Aberdeen. NC 28315 T. \: Secondary highway. hard SurtaCe -.-. - InlcrsUte Route ' U.S. Route ( Stale Route February 20, 19 Legend OX — Facility — Outfall NPDES:N00017508 MOORE COUNTY WATER POLLUTION CONTROL PLANT JAMES DELMO FRYE. System Superintendent (910) 281-3146 Fax: (910) 281-2047 RCAD CI —a SSI FICAT7ON .1. oy Imp•a<d write Unimp(wed road_ P1NEBLUFF, N. C. N 3500 —W 7922.5/7.5 1 tiAB •:.( I: (,,ICVLS..0 IVIC.: DMA 7111 ix ir-6/511ES Y147 State of Nottli Carolina Department of Environment and Natural Resources Division of Water Quality , PERMIT NAME/OWNERSIP CHANGE FORM Any changes made to this form vvill result in the application being returned. (THIS FORMAIAY BE PHOTOCOPIED FOR USE AS AN bRIINA4,) For more information, visit our web site at: h2o.ennstate.ric.Us'indpu/ L gEOTJIRED ITEMS 1. Submit one original of the completed and appropriately executed permit Name/Ownership Change Form. For a change of ownership, the certification must be signed by both the current permit holder and the new applicant. For a name change only, •the certification must be signed by the applicant. 2._ Provide legal document.ton-of the transfer -of ownership (auch.-as"a Contract, deed, artiele of incorporation, et.) for ownership changes. A copy of the Association Bylaws and Declarations should be submitted for a change of Qv/unship to a Homeowner's Association. 3. Submit a properly executed Operation ancl Maintenance Agreement for all Single!FaMily- Spray/Drip Irrigation permits requesting a change of ownership. II. CURRENT PE I' Iv INFORMATION 1. Permit number: NC 0037508- • 2. Permit holder's name: 3. ofEdan nume and title Denn is BrObs t- 11 (Person legally respoble for permit) 1 _ . Di-rectarMoore-. CountY • -- Moore Waterand:7:Sew:er:AUthoritS, 4. Mailing address: 5227 Highway 15-501, P. (title) 0 Box 19127 City : Carthage Telephone number; (910 ) 947-6315 M. INMW OWNER/NAME INFORMATION State: NC . 28327 Facsimile rturaber: (910 ) 94 7 - 9, 92 • 1. This request for a permit change is a result of: a. Changein ownership of property/company b. Name change only X c Otheplea.wexplain)Mi5Oreirlqater. and Sewer" Authority was dissolved , ebruary Z000'," and, all assets were transferred to the County of Moore. FORM: PNOCF 06/00 Page 1 of 2 1,4 • 2, New owner's name (name to be used in permit): County of -Moore W. David McNi1;1,Jr. SCILiS 3. New owner's or signing official'a name and title: 4. Mailkg address: (Person legally responsible for pemait) County Manager (title) Moore,County Public Utilities, IP.' O. Box 1927 Car Carthage State: Telephone number: ( 9 1° ) •9 4 7 6 3 15 IV. CERrITFICATION NC Zip: r 2 8 3 2 7 • Facsimile number: 9 1'0 ) 9 4 7 -.1 9 9 2 1, Current Permittee's Certification: Dennis B r ob S t , attest that this application for_name/Ownership change has been reviewed and. is accurate and complete to the best of ray knowledge. I understand that if all required parts of this application are not completed and that if all required supporting information and attachmentts aranot included, this application package Will be returned as incomplete. I understand I will continue to be responsible for compliance with the Date: current pemnt until a new permi Signature: / - 2. A.pplicants Certification: is Jr W . David McN e i 1 1,,attest ter this application for name/ownershiP change has been reviewed and is accurate and complete to the best of my knowledge. I understand that if all required parts of this application are not, completed and that if all required supporting information and. attachmentare' not included, this application mfas.uc Signatire: o pieta. L/f4/14/ Pate: package wi1 be r 1. THE COMPLETED APPLICATION PACICAGE;INCLUDING ALL SUPPORTING INFORMATION, AND MATERIALS, SHOULD BE SENT TO THE FOLLOWING ODRESS: NORTH CAROLLNA DEPARTMENT OF ENVIROMNIENT AND NATURAL RESOURCES - DIVISION OF WATER QUALITY NON -DISCHARGE PERMITTING UNIT l• EtV‘ii.5. Postal Service: 1617 MAIL SERVICE CENTER • 512 NORTH SALISBURY, STREET, SUITE 1219 RALEIGH, NORTH CAROLINA 27699..161.7 • ' • RALEIGH, NORTH CAROLINA. 27604 TELEPHONE NUMBER: (919) 733-5083 I! i; FORM: PNOCF 06/00 Page 2 of 2 -1 ` � ` -FEB� � ^�= o ^WZ r ADDENDUM 1 NPDES PERMIT # NC0037508 REQUEST FOR RENEWAL January 2,2004 Sludge Management Plan: The Sludge Management Plan for the Moore County Water Pollution Control Plant consists of two items. 1. Disposal of Sludge in a Subtitle D Landfill. 2. Land Application Permit (Permit #WQ0018018) which has never'been used. If you have any questions concerning our Sludge Management Plan do not hesitate to call James D. Frye at 910-281-3146.