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HomeMy WebLinkAboutNC0006254_Groundwater Monitoring Report March 2021_20210326PO Box 604 ▪ Fletcher, NC 28732 ▪ Cell: 828-508-4510 March 26, 2021 Mr. Brett Laverty NCDEQ Division of Water Resources Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778 RE: Groundwater Analytical Results – March 2021 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Mr. Laverty: On March 16, 2021, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site located at 1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7 and MW-8. The depth to groundwater in the monitoring wells ranged from 4.85 feet in MW-4 to 47.84 feet in MW-2. Refer to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well locations. All groundwater samples, with the exception of MW-2, were collected using a peristaltic pump connected to a Horiba U52-2 water quality meter with a flow through cell to collect groundwater parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP, and turbidity). Groundwater sample MW-2 was collected using a bailer once three well volumes were removed. Groundwater from the same bail as the sample was also poured into the flow cell to collect the approximate parameters. The groundwater samples were submitted on ice to Pace Analytical for the analysis of 8-RCRA Metals, pH, ammonia, TKN, sulfate, nitrogen, nitrite and nitrate. MW-2 was also analyzed for total dissolved solids (TDS) using EPA Method SM 2540C, and volatile organic compounds (VOCs) using EPA Method 6200B. The groundwater parameters for all samples are outlined in Table 2. The laboratory analysis of groundwater samples MW-1 detected levels of iron and manganese above the NCAC 2L groundwater standards. The laboratory analysis of MW-2 detected levels of arsenic, barium, iron, chromium, manganese and ammonia above the N CAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-3 detected levels of iron, manganese and ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-4 detected levels of iron and manganese above the NCAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-7 detected levels of iron above the NCAC 2L groundwater standards. Laboratory analysis of groundwater samples MW-6 and MW-8 did not detect any compounds exceeding the NCAC 2L groundwater standards. The analytical results are shown on attached Table 2 and the attached laboratory data sheets. Singleton Environmental, Inc. Singleton Environmental, Inc. During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the groundwater in monitoring well MW-4. During the March 2021 event a sheen was not observed; however, a VOC sample was collected from each monitoring well and analyzed using EPA Method 6200B. None of the concentrations were detected above the minimum laboratory detection levels. The compound levels detected in the groundwater analysis for the March 2021 sampling event were comparable to the November 2020 and July 2020 sampling events with the exception of the elevated iron in MW-7. Singleton Environmental, Inc. recommends sampling the monitoring wells again in July 2021. If you have any questions you can reach me at (828) 508-4510. Sincerely, Chris Singleton, P.G. Singleton Environmental, Inc. cc: Dave Hallock, Blue Ridge Tissue Corporation Attachments @A @A @A @A @A @A @A @A MW-2 MW-3 MW-4 MW-1 @A MW-5 MW-7 MW-6 MW-8 1 2 8 0 12601 3 2 0 1340 1360 1380 124014201240 1420 Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community Figure 60540673 1 May 2017 § 0 200 400Feet 1 inch = 200 feet Y a d k i n R i v e r R d Whisnant RdYad k i n R i v e r Yadkin R iver Roby Martin Rd#0 Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina Legend Property Boundary Yadkin River Flow Direction #Land Surface Elevation Contour (ft above mean sea level) Monitoring Well Location Abandoned Water Well#0@A Well ID Date Installed Total Depth (feet bls) Screened Interval (feet bls) Top of Casing Elevation (feet msl) Date Water Level Measured Depth to Water (feet BTOC) Groundwater Elevation (feet msl) MW-1 02/08/11 11 6-11 1253.71 11/09/20 11.77 1,241.94 MW-2 08/12/09 50 40-50 1323.03 11/09/20 47.84 1,275.19 MW-3 08/13/09 20 10-20 1299.02 11/09/20 18.25 1,280.77 MW-4 08/13/09 15 5-15 1247.23 11/09/20 4.85 1,242.38 MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A MW-6 08/06/14 29 19-29 1341.55 11/09/20 26.25 1,315.30 MW-7 08/06/14 24 14-24 1274.41 11/09/20 16.27 1,258.14 MW-8 08/06/14 20 10-20 1253.14 11/09/20 13.57 1,239.57 Notes: bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged AECOM Table 1 Monitoring Well Construction and Groundwater Elevations Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8 Sample Date 03/16/21 03/16/21 03/16/21 03/16/21 03/16/21 03/16/21 03/16/21 Temperature (°C)NS 15.2 N/A 15.60 14.60 14.83 13.91 15.00 pH (standard units)NS 6.87 N/A 6.37 6.07 5.28 5.91 5.91 Specific Conductivity (mS/cm)NS 0.266 N/A 0.571 0.25 0.029 0.086 0.098 Dissolved Oxygen (mg/L)NS 2.43 N/A 6.90 3.21 7.50 8.51 6.52 ORP (mV)NS 8.0 N/A 7.0 79.0 166.0 131.0 77.0 Turbidity (NTU)NS 4.6 N/A 0.4 8.4 9.3 4 1.5 Gallons Pumped NS 2.5 2.00 3.5 2 3.5 2 2 Cloudy/Odor No/No No/No Cloudy/Odor Cloudy/Odor No/No No/No No/No No/No Total Barium (ug/L)700 8.35 1730 256 68.5 98.9 54.5 13.2 Total Iron (ug/L)300 22800 69900 31900 9060 ND 2920 ND Total Manganese (ug/L)50 2380 710 3330 1590 16.7 23.5 ND Aresenic (ug/L)10 ND 16.4 ND ND ND ND ND Chromium (ug/L)10 ND 22.8 ND ND ND ND ND Lead (ug/L)15 ND 9.3 ND ND ND ND ND Sulfate N/A 2.9 1.3 19.2 2.3 ND 1.9 21.8 Amonia (mg/L)1.5 0.53 14.6 14.3 0.67 ND ND ND TKN (mg/L)N/A 0.75 14.6 11 0.97 ND ND ND Nitrogen NO2 plus NO3 (mg/L)N/A 0.045 0.089 0.22 ND ND 1.2 2.4 Nitrate (mg/L)10 0.045 ND 0.16 ND ND 1.2 2.4 Nitrite (mg/L)1 ND 0.16 0.06 ND ND ND ND pH (standard units)N/A 7.7 6.7 7.1 7.2 5.6 7.2 6.9 Total Disolved Solids (mg/L)N/A N/A 343 N/A N/A N/A N/A N/A EPA Method 6200B for VOCs N/A ND ND ND ND ND ND ND Notes: Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7 2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20 °C - degrees Celsius µS/cm - microsiemens per centimeter EPA - United States Environmental Protection Agency mg/L - milligrams per liter mV - millivolt NA - Not analyzed NS - No standard NTU - Nephelometric Turbidity Unit RCRA - Resource Conservation Recovery Act Bold samples indicate concentrations above the 2L Standard *MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample. 2L Standard Field Parameters Analytical Parameters Table 2 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina #=CL# March 25, 2021 LIMS USE: FR - CHRIS SINGLETON LIMS OBJECT ID: 92527951 92527951 Project: Pace Project No.: RE: Chris Singleton Singleton Environmental P.O. Box 2012 Enka, NC 28728 Blue Ridge Tissue Corp. Dear Chris Singleton: Enclosed are the analytical results for sample(s) received by the laboratory on March 16, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com Project Manager 1(828)254-7176 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 1 of 53 #=CP# CERTIFICATIONS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 2 of 53 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92527951001 MW-1 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92527951002 MW-2 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT SM 6200B 63 PASI-CPM1 SM 2540C-2011 1 PASI-ARED SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92527951003 MW-3 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92527951004 MW-4 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92527951005 MW-6 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92527951006 MW-7 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 3 of 53 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92527951007 MW-8 EPA 200.7 Rev 4.4 1994 6 PASI-ARDT SM 6200B 63 PASI-CSAS SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANAL EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 4 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-1 Lab ID:92527951001 Collected:03/16/21 10:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 03/21/21 22:39 7440-38-203/19/21 02:1410.0 1 Barium 83.5 ug/L 03/21/21 22:39 7440-39-303/19/21 02:145.0 1 Chromium ND ug/L 03/21/21 22:39 7440-47-303/19/21 02:145.0 1 Iron 22800 ug/L 03/21/21 22:39 7439-89-603/19/21 02:1450.0 1 Lead ND ug/L 03/21/21 22:39 7439-92-103/19/21 02:145.0 1 Manganese 2380 ug/L 03/21/21 22:39 7439-96-503/19/21 02:145.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/19/21 21:19 71-43-20.50 1 Bromobenzene ND ug/L 03/19/21 21:19 108-86-10.50 1 Bromochloromethane ND ug/L 03/19/21 21:19 74-97-50.50 1 Bromodichloromethane ND ug/L 03/19/21 21:19 75-27-40.50 1 Bromoform ND ug/L 03/19/21 21:19 75-25-20.50 1 Bromomethane ND ug/L 03/19/21 21:19 74-83-95.0 1 n-Butylbenzene ND ug/L 03/19/21 21:19 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/19/21 21:19 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/19/21 21:19 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/19/21 21:19 56-23-50.50 1 Chlorobenzene ND ug/L 03/19/21 21:19 108-90-70.50 1 Chloroethane ND ug/L 03/19/21 21:19 75-00-31.0 1 Chloroform ND ug/L 03/19/21 21:19 67-66-30.50 1 Chloromethane ND ug/L 03/19/21 21:19 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/19/21 21:19 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/19/21 21:19 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/19/21 21:19 96-12-81.0 1 Dibromochloromethane ND ug/L 03/19/21 21:19 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/19/21 21:19 106-93-40.50 1 Dibromomethane ND ug/L 03/19/21 21:19 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/19/21 21:19 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/19/21 21:19 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/19/21 21:19 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/19/21 21:19 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/19/21 21:19 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/19/21 21:19 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/19/21 21:19 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/19/21 21:19 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/19/21 21:19 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/19/21 21:19 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/19/21 21:19 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/19/21 21:19 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/19/21 21:19 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/19/21 21:19 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/19/21 21:19 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/19/21 21:19 108-20-30.50 1 Ethylbenzene ND ug/L 03/19/21 21:19 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 5 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-1 Lab ID:92527951001 Collected:03/16/21 10:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/19/21 21:19 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/19/21 21:19 98-82-80.50 1 Methylene Chloride ND ug/L 03/19/21 21:19 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/19/21 21:19 1634-04-40.50 1 Naphthalene ND ug/L 03/19/21 21:19 91-20-32.0 1 n-Propylbenzene ND ug/L 03/19/21 21:19 103-65-10.50 1 Styrene ND ug/L 03/19/21 21:19 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/19/21 21:19 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/19/21 21:19 79-34-50.50 1 Tetrachloroethene ND ug/L 03/19/21 21:19 127-18-40.50 1 Toluene ND ug/L 03/19/21 21:19 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/19/21 21:19 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/19/21 21:19 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/19/21 21:19 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/19/21 21:19 79-00-50.50 1 Trichloroethene ND ug/L 03/19/21 21:19 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/19/21 21:19 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/19/21 21:19 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/19/21 21:19 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/19/21 21:19 108-67-80.50 1 Vinyl chloride ND ug/L 03/19/21 21:19 75-01-41.0 1 m&p-Xylene ND ug/L 03/19/21 21:19 179601-23-11.0 1 o-Xylene ND ug/L 03/19/21 21:19 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)99 %03/19/21 21:19 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %03/19/21 21:19 460-00-470-130 1 Toluene-d8 (S)103 %03/19/21 21:19 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 7.7 Std. Units 03/21/21 15:35 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 2.9 mg/L 03/18/21 10:10 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.53 mg/L 03/18/21 13:08 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 0.75 mg/L 03/20/21 05:33 7727-37-903/19/21 18:000.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 6 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-1 Lab ID:92527951001 Collected:03/16/21 10:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.045 mg/L 03/17/21 00:310.040 1 Nitrogen, Nitrate 0.045 mg/L 03/17/21 00:31 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 03/17/21 00:31 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 7 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-2 Lab ID:92527951002 Collected:03/16/21 11:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic 16.4 ug/L 03/23/21 09:14 7440-38-203/21/21 12:5110.0 1 Barium 1730 ug/L 03/23/21 09:14 7440-39-3 M103/21/21 12:515.0 1 Chromium 22.8 ug/L 03/23/21 09:14 7440-47-303/21/21 12:515.0 1 Iron 69900 ug/L 03/23/21 09:14 7439-89-6 M103/21/21 12:5150.0 1 Lead 9.3 ug/L 03/23/21 09:14 7439-92-103/21/21 12:515.0 1 Manganese 710 ug/L 03/23/21 09:14 7439-96-5 M103/21/21 12:515.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/19/21 21:37 71-43-20.50 1 Bromobenzene ND ug/L 03/19/21 21:37 108-86-10.50 1 Bromochloromethane ND ug/L 03/19/21 21:37 74-97-50.50 1 Bromodichloromethane ND ug/L 03/19/21 21:37 75-27-40.50 1 Bromoform ND ug/L 03/19/21 21:37 75-25-20.50 1 Bromomethane ND ug/L 03/19/21 21:37 74-83-95.0 1 n-Butylbenzene ND ug/L 03/19/21 21:37 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/19/21 21:37 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/19/21 21:37 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/19/21 21:37 56-23-50.50 1 Chlorobenzene ND ug/L 03/19/21 21:37 108-90-70.50 1 Chloroethane ND ug/L 03/19/21 21:37 75-00-31.0 1 Chloroform ND ug/L 03/19/21 21:37 67-66-30.50 1 Chloromethane ND ug/L 03/19/21 21:37 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/19/21 21:37 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/19/21 21:37 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/19/21 21:37 96-12-81.0 1 Dibromochloromethane ND ug/L 03/19/21 21:37 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/19/21 21:37 106-93-40.50 1 Dibromomethane ND ug/L 03/19/21 21:37 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/19/21 21:37 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/19/21 21:37 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/19/21 21:37 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/19/21 21:37 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/19/21 21:37 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/19/21 21:37 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/19/21 21:37 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/19/21 21:37 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/19/21 21:37 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/19/21 21:37 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/19/21 21:37 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/19/21 21:37 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/19/21 21:37 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/19/21 21:37 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/19/21 21:37 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/19/21 21:37 108-20-30.50 1 Ethylbenzene ND ug/L 03/19/21 21:37 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 8 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-2 Lab ID:92527951002 Collected:03/16/21 11:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/19/21 21:37 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/19/21 21:37 98-82-80.50 1 Methylene Chloride ND ug/L 03/19/21 21:37 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/19/21 21:37 1634-04-40.50 1 Naphthalene ND ug/L 03/19/21 21:37 91-20-32.0 1 n-Propylbenzene ND ug/L 03/19/21 21:37 103-65-10.50 1 Styrene ND ug/L 03/19/21 21:37 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/19/21 21:37 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/19/21 21:37 79-34-50.50 1 Tetrachloroethene ND ug/L 03/19/21 21:37 127-18-40.50 1 Toluene ND ug/L 03/19/21 21:37 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/19/21 21:37 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/19/21 21:37 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/19/21 21:37 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/19/21 21:37 79-00-50.50 1 Trichloroethene ND ug/L 03/19/21 21:37 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/19/21 21:37 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/19/21 21:37 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/19/21 21:37 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/19/21 21:37 108-67-80.50 1 Vinyl chloride ND ug/L 03/19/21 21:37 75-01-41.0 1 m&p-Xylene ND ug/L 03/19/21 21:37 179601-23-11.0 1 o-Xylene ND ug/L 03/19/21 21:37 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %03/19/21 21:37 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %03/19/21 21:37 460-00-470-130 1 Toluene-d8 (S)101 %03/19/21 21:37 2037-26-570-130 1 Analytical Method: SM 2540C-2011 Pace Analytical Services - Asheville 2540C Total Dissolved Solids Total Dissolved Solids 343 mg/L 03/19/21 16:4825.0 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.7 Std. Units 03/21/21 15:54 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 1.3 mg/L 03/18/21 10:56 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 14.6 mg/L 03/18/21 15:26 7664-41-70.50 5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 9 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-2 Lab ID:92527951002 Collected:03/16/21 11:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 14.6 mg/L 03/20/21 05:36 7727-37-9 M103/19/21 18:000.50 1 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.089 mg/L 03/17/21 00:360.040 1 Nitrogen, Nitrate ND mg/L 03/17/21 00:36 14797-55-80.040 1 Nitrogen, Nitrite 0.16 mg/L 03/17/21 00:36 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 10 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-3 Lab ID:92527951003 Collected:03/16/21 11:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 03/23/21 09:04 7440-38-203/21/21 12:5110.0 1 Barium 256 ug/L 03/23/21 09:04 7440-39-303/21/21 12:515.0 1 Chromium ND ug/L 03/23/21 09:04 7440-47-303/21/21 12:515.0 1 Iron 31900 ug/L 03/23/21 09:04 7439-89-603/21/21 12:5150.0 1 Lead ND ug/L 03/23/21 09:04 7439-92-103/21/21 12:515.0 1 Manganese 3330 ug/L 03/23/21 09:04 7439-96-503/21/21 12:515.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/19/21 21:54 71-43-20.50 1 Bromobenzene ND ug/L 03/19/21 21:54 108-86-10.50 1 Bromochloromethane ND ug/L 03/19/21 21:54 74-97-50.50 1 Bromodichloromethane ND ug/L 03/19/21 21:54 75-27-40.50 1 Bromoform ND ug/L 03/19/21 21:54 75-25-20.50 1 Bromomethane ND ug/L 03/19/21 21:54 74-83-95.0 1 n-Butylbenzene ND ug/L 03/19/21 21:54 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/19/21 21:54 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/19/21 21:54 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/19/21 21:54 56-23-50.50 1 Chlorobenzene ND ug/L 03/19/21 21:54 108-90-70.50 1 Chloroethane ND ug/L 03/19/21 21:54 75-00-31.0 1 Chloroform ND ug/L 03/19/21 21:54 67-66-30.50 1 Chloromethane ND ug/L 03/19/21 21:54 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/19/21 21:54 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/19/21 21:54 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/19/21 21:54 96-12-81.0 1 Dibromochloromethane ND ug/L 03/19/21 21:54 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/19/21 21:54 106-93-40.50 1 Dibromomethane ND ug/L 03/19/21 21:54 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/19/21 21:54 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/19/21 21:54 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/19/21 21:54 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/19/21 21:54 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/19/21 21:54 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/19/21 21:54 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/19/21 21:54 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/19/21 21:54 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/19/21 21:54 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/19/21 21:54 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/19/21 21:54 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/19/21 21:54 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/19/21 21:54 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/19/21 21:54 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/19/21 21:54 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/19/21 21:54 108-20-30.50 1 Ethylbenzene ND ug/L 03/19/21 21:54 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 11 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-3 Lab ID:92527951003 Collected:03/16/21 11:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/19/21 21:54 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/19/21 21:54 98-82-80.50 1 Methylene Chloride ND ug/L 03/19/21 21:54 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/19/21 21:54 1634-04-40.50 1 Naphthalene ND ug/L 03/19/21 21:54 91-20-32.0 1 n-Propylbenzene ND ug/L 03/19/21 21:54 103-65-10.50 1 Styrene ND ug/L 03/19/21 21:54 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/19/21 21:54 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/19/21 21:54 79-34-50.50 1 Tetrachloroethene ND ug/L 03/19/21 21:54 127-18-40.50 1 Toluene ND ug/L 03/19/21 21:54 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/19/21 21:54 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/19/21 21:54 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/19/21 21:54 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/19/21 21:54 79-00-50.50 1 Trichloroethene ND ug/L 03/19/21 21:54 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/19/21 21:54 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/19/21 21:54 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/19/21 21:54 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/19/21 21:54 108-67-80.50 1 Vinyl chloride ND ug/L 03/19/21 21:54 75-01-41.0 1 m&p-Xylene ND ug/L 03/19/21 21:54 179601-23-11.0 1 o-Xylene ND ug/L 03/19/21 21:54 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %03/19/21 21:54 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %03/19/21 21:54 460-00-470-130 1 Toluene-d8 (S)102 %03/19/21 21:54 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 7.1 Std. Units 03/21/21 16:05 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 19.2 mg/L 03/18/21 11:12 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 14.3 mg/L 03/22/21 12:15 7664-41-70.30 3 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 11.0 mg/L 03/20/21 05:41 7727-37-9 M103/19/21 18:000.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 12 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-3 Lab ID:92527951003 Collected:03/16/21 11:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.22 mg/L 03/17/21 00:380.040 1 Nitrogen, Nitrate 0.16 mg/L 03/17/21 00:38 14797-55-80.040 1 Nitrogen, Nitrite 0.060 mg/L 03/17/21 00:38 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 13 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-4 Lab ID:92527951004 Collected:03/16/21 13:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 03/23/21 09:17 7440-38-203/21/21 12:5110.0 1 Barium 68.5 ug/L 03/23/21 09:17 7440-39-303/21/21 12:515.0 1 Chromium ND ug/L 03/23/21 09:17 7440-47-303/21/21 12:515.0 1 Iron 9060 ug/L 03/23/21 09:17 7439-89-603/21/21 12:5150.0 1 Lead ND ug/L 03/23/21 09:17 7439-92-103/21/21 12:515.0 1 Manganese 1590 ug/L 03/23/21 09:17 7439-96-503/21/21 12:515.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/19/21 22:12 71-43-20.50 1 Bromobenzene ND ug/L 03/19/21 22:12 108-86-10.50 1 Bromochloromethane ND ug/L 03/19/21 22:12 74-97-50.50 1 Bromodichloromethane ND ug/L 03/19/21 22:12 75-27-40.50 1 Bromoform ND ug/L 03/19/21 22:12 75-25-20.50 1 Bromomethane ND ug/L 03/19/21 22:12 74-83-95.0 1 n-Butylbenzene ND ug/L 03/19/21 22:12 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/19/21 22:12 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/19/21 22:12 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/19/21 22:12 56-23-50.50 1 Chlorobenzene ND ug/L 03/19/21 22:12 108-90-70.50 1 Chloroethane ND ug/L 03/19/21 22:12 75-00-31.0 1 Chloroform ND ug/L 03/19/21 22:12 67-66-30.50 1 Chloromethane ND ug/L 03/19/21 22:12 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/19/21 22:12 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/19/21 22:12 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/19/21 22:12 96-12-81.0 1 Dibromochloromethane ND ug/L 03/19/21 22:12 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/19/21 22:12 106-93-40.50 1 Dibromomethane ND ug/L 03/19/21 22:12 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/19/21 22:12 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/19/21 22:12 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/19/21 22:12 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/19/21 22:12 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/19/21 22:12 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/19/21 22:12 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/19/21 22:12 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/19/21 22:12 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/19/21 22:12 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/19/21 22:12 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/19/21 22:12 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/19/21 22:12 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/19/21 22:12 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/19/21 22:12 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/19/21 22:12 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/19/21 22:12 108-20-30.50 1 Ethylbenzene ND ug/L 03/19/21 22:12 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 14 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-4 Lab ID:92527951004 Collected:03/16/21 13:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/19/21 22:12 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/19/21 22:12 98-82-80.50 1 Methylene Chloride ND ug/L 03/19/21 22:12 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/19/21 22:12 1634-04-40.50 1 Naphthalene ND ug/L 03/19/21 22:12 91-20-32.0 1 n-Propylbenzene ND ug/L 03/19/21 22:12 103-65-10.50 1 Styrene ND ug/L 03/19/21 22:12 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/19/21 22:12 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/19/21 22:12 79-34-50.50 1 Tetrachloroethene ND ug/L 03/19/21 22:12 127-18-40.50 1 Toluene ND ug/L 03/19/21 22:12 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/19/21 22:12 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/19/21 22:12 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/19/21 22:12 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/19/21 22:12 79-00-50.50 1 Trichloroethene ND ug/L 03/19/21 22:12 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/19/21 22:12 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/19/21 22:12 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/19/21 22:12 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/19/21 22:12 108-67-80.50 1 Vinyl chloride ND ug/L 03/19/21 22:12 75-01-41.0 1 m&p-Xylene ND ug/L 03/19/21 22:12 179601-23-11.0 1 o-Xylene ND ug/L 03/19/21 22:12 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %03/19/21 22:12 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %03/19/21 22:12 460-00-470-130 1 Toluene-d8 (S)103 %03/19/21 22:12 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 7.2 Std. Units 03/21/21 16:59 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 2.3 mg/L 03/18/21 11:27 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.67 mg/L 03/18/21 13:21 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 03/20/21 05:46 7727-37-903/19/21 18:000.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 15 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-4 Lab ID:92527951004 Collected:03/16/21 13:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 03/17/21 00:450.040 1 Nitrogen, Nitrate ND mg/L 03/17/21 00:45 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 03/17/21 00:45 14797-65-0 M10.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 16 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-6 Lab ID:92527951005 Collected:03/16/21 12:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 03/23/21 09:20 7440-38-203/21/21 12:5110.0 1 Barium 98.9 ug/L 03/23/21 09:20 7440-39-303/21/21 12:515.0 1 Chromium ND ug/L 03/23/21 09:20 7440-47-303/21/21 12:515.0 1 Iron ND ug/L 03/23/21 09:20 7439-89-603/21/21 12:5150.0 1 Lead ND ug/L 03/23/21 09:20 7439-92-103/21/21 12:515.0 1 Manganese 16.7 ug/L 03/23/21 09:20 7439-96-503/21/21 12:515.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/19/21 22:30 71-43-20.50 1 Bromobenzene ND ug/L 03/19/21 22:30 108-86-10.50 1 Bromochloromethane ND ug/L 03/19/21 22:30 74-97-50.50 1 Bromodichloromethane ND ug/L 03/19/21 22:30 75-27-40.50 1 Bromoform ND ug/L 03/19/21 22:30 75-25-20.50 1 Bromomethane ND ug/L 03/19/21 22:30 74-83-95.0 1 n-Butylbenzene ND ug/L 03/19/21 22:30 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/19/21 22:30 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/19/21 22:30 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/19/21 22:30 56-23-50.50 1 Chlorobenzene ND ug/L 03/19/21 22:30 108-90-70.50 1 Chloroethane ND ug/L 03/19/21 22:30 75-00-31.0 1 Chloroform ND ug/L 03/19/21 22:30 67-66-30.50 1 Chloromethane ND ug/L 03/19/21 22:30 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/19/21 22:30 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/19/21 22:30 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/19/21 22:30 96-12-81.0 1 Dibromochloromethane ND ug/L 03/19/21 22:30 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/19/21 22:30 106-93-40.50 1 Dibromomethane ND ug/L 03/19/21 22:30 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/19/21 22:30 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/19/21 22:30 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/19/21 22:30 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/19/21 22:30 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/19/21 22:30 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/19/21 22:30 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/19/21 22:30 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/19/21 22:30 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/19/21 22:30 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/19/21 22:30 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/19/21 22:30 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/19/21 22:30 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/19/21 22:30 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/19/21 22:30 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/19/21 22:30 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/19/21 22:30 108-20-30.50 1 Ethylbenzene ND ug/L 03/19/21 22:30 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 17 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-6 Lab ID:92527951005 Collected:03/16/21 12:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/19/21 22:30 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/19/21 22:30 98-82-80.50 1 Methylene Chloride ND ug/L 03/19/21 22:30 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/19/21 22:30 1634-04-40.50 1 Naphthalene ND ug/L 03/19/21 22:30 91-20-32.0 1 n-Propylbenzene ND ug/L 03/19/21 22:30 103-65-10.50 1 Styrene ND ug/L 03/19/21 22:30 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/19/21 22:30 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/19/21 22:30 79-34-50.50 1 Tetrachloroethene ND ug/L 03/19/21 22:30 127-18-40.50 1 Toluene ND ug/L 03/19/21 22:30 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/19/21 22:30 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/19/21 22:30 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/19/21 22:30 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/19/21 22:30 79-00-50.50 1 Trichloroethene ND ug/L 03/19/21 22:30 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/19/21 22:30 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/19/21 22:30 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/19/21 22:30 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/19/21 22:30 108-67-80.50 1 Vinyl chloride ND ug/L 03/19/21 22:30 75-01-41.0 1 m&p-Xylene ND ug/L 03/19/21 22:30 179601-23-11.0 1 o-Xylene ND ug/L 03/19/21 22:30 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %03/19/21 22:30 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %03/19/21 22:30 460-00-470-130 1 Toluene-d8 (S)101 %03/19/21 22:30 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 5.6 Std. Units 03/21/21 16:39 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate ND mg/L 03/18/21 11:43 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 03/18/21 13:22 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 03/20/21 05:48 7727-37-903/19/21 18:000.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 18 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-6 Lab ID:92527951005 Collected:03/16/21 12:45 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 03/17/21 00:400.040 1 Nitrogen, Nitrate ND mg/L 03/17/21 00:40 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 03/17/21 00:40 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 19 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-7 Lab ID:92527951006 Collected:03/16/21 13:10 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 03/23/21 09:23 7440-38-203/21/21 12:5110.0 1 Barium 54.5 ug/L 03/23/21 09:23 7440-39-303/21/21 12:515.0 1 Chromium ND ug/L 03/23/21 09:23 7440-47-303/21/21 12:515.0 1 Iron 2920 ug/L 03/23/21 09:23 7439-89-603/21/21 12:5150.0 1 Lead ND ug/L 03/23/21 09:23 7439-92-103/21/21 12:515.0 1 Manganese 23.5 ug/L 03/23/21 09:23 7439-96-503/21/21 12:515.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/19/21 22:48 71-43-20.50 1 Bromobenzene ND ug/L 03/19/21 22:48 108-86-10.50 1 Bromochloromethane ND ug/L 03/19/21 22:48 74-97-50.50 1 Bromodichloromethane ND ug/L 03/19/21 22:48 75-27-40.50 1 Bromoform ND ug/L 03/19/21 22:48 75-25-20.50 1 Bromomethane ND ug/L 03/19/21 22:48 74-83-95.0 1 n-Butylbenzene ND ug/L 03/19/21 22:48 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/19/21 22:48 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/19/21 22:48 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/19/21 22:48 56-23-50.50 1 Chlorobenzene ND ug/L 03/19/21 22:48 108-90-70.50 1 Chloroethane ND ug/L 03/19/21 22:48 75-00-31.0 1 Chloroform ND ug/L 03/19/21 22:48 67-66-30.50 1 Chloromethane ND ug/L 03/19/21 22:48 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/19/21 22:48 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/19/21 22:48 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/19/21 22:48 96-12-81.0 1 Dibromochloromethane ND ug/L 03/19/21 22:48 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/19/21 22:48 106-93-40.50 1 Dibromomethane ND ug/L 03/19/21 22:48 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/19/21 22:48 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/19/21 22:48 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/19/21 22:48 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/19/21 22:48 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/19/21 22:48 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/19/21 22:48 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/19/21 22:48 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/19/21 22:48 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/19/21 22:48 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/19/21 22:48 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/19/21 22:48 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/19/21 22:48 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/19/21 22:48 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/19/21 22:48 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/19/21 22:48 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/19/21 22:48 108-20-30.50 1 Ethylbenzene ND ug/L 03/19/21 22:48 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 20 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-7 Lab ID:92527951006 Collected:03/16/21 13:10 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/19/21 22:48 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/19/21 22:48 98-82-80.50 1 Methylene Chloride ND ug/L 03/19/21 22:48 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/19/21 22:48 1634-04-40.50 1 Naphthalene ND ug/L 03/19/21 22:48 91-20-32.0 1 n-Propylbenzene ND ug/L 03/19/21 22:48 103-65-10.50 1 Styrene ND ug/L 03/19/21 22:48 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/19/21 22:48 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/19/21 22:48 79-34-50.50 1 Tetrachloroethene ND ug/L 03/19/21 22:48 127-18-40.50 1 Toluene ND ug/L 03/19/21 22:48 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/19/21 22:48 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/19/21 22:48 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/19/21 22:48 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/19/21 22:48 79-00-50.50 1 Trichloroethene ND ug/L 03/19/21 22:48 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/19/21 22:48 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/19/21 22:48 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/19/21 22:48 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/19/21 22:48 108-67-80.50 1 Vinyl chloride ND ug/L 03/19/21 22:48 75-01-41.0 1 m&p-Xylene ND ug/L 03/19/21 22:48 179601-23-11.0 1 o-Xylene ND ug/L 03/19/21 22:48 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %03/19/21 22:48 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %03/19/21 22:48 460-00-470-130 1 Toluene-d8 (S)100 %03/19/21 22:48 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 7.2 Std. Units 03/21/21 16:45 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 1.9 mg/L 03/18/21 12:29 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 03/18/21 13:24 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 03/20/21 05:49 7727-37-903/19/21 18:000.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 21 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-7 Lab ID:92527951006 Collected:03/16/21 13:10 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 1.2 mg/L 03/17/21 00:410.040 1 Nitrogen, Nitrate 1.2 mg/L 03/17/21 00:41 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 03/17/21 00:41 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 22 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-8 Lab ID:92527951007 Collected:03/16/21 12:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 03/23/21 09:27 7440-38-203/21/21 12:5110.0 1 Barium 13.2 ug/L 03/23/21 09:27 7440-39-303/21/21 12:515.0 1 Chromium ND ug/L 03/23/21 09:27 7440-47-303/21/21 12:515.0 1 Iron ND ug/L 03/23/21 09:27 7439-89-603/21/21 12:5150.0 1 Lead ND ug/L 03/23/21 09:27 7439-92-103/21/21 12:515.0 1 Manganese ND ug/L 03/23/21 09:27 7439-96-503/21/21 12:515.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 03/22/21 16:52 71-43-20.50 1 Bromobenzene ND ug/L 03/22/21 16:52 108-86-10.50 1 Bromochloromethane ND ug/L 03/22/21 16:52 74-97-50.50 1 Bromodichloromethane ND ug/L 03/22/21 16:52 75-27-40.50 1 Bromoform ND ug/L 03/22/21 16:52 75-25-20.50 1 Bromomethane ND ug/L 03/22/21 16:52 74-83-95.0 1 n-Butylbenzene ND ug/L 03/22/21 16:52 104-51-80.50 1 sec-Butylbenzene ND ug/L 03/22/21 16:52 135-98-80.50 1 tert-Butylbenzene ND ug/L 03/22/21 16:52 98-06-60.50 1 Carbon tetrachloride ND ug/L 03/22/21 16:52 56-23-50.50 1 Chlorobenzene ND ug/L 03/22/21 16:52 108-90-70.50 1 Chloroethane ND ug/L 03/22/21 16:52 75-00-31.0 1 Chloroform ND ug/L 03/22/21 16:52 67-66-30.50 1 Chloromethane ND ug/L 03/22/21 16:52 74-87-31.0 1 2-Chlorotoluene ND ug/L 03/22/21 16:52 95-49-80.50 1 4-Chlorotoluene ND ug/L 03/22/21 16:52 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 03/22/21 16:52 96-12-81.0 1 Dibromochloromethane ND ug/L 03/22/21 16:52 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 03/22/21 16:52 106-93-40.50 1 Dibromomethane ND ug/L 03/22/21 16:52 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 03/22/21 16:52 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 03/22/21 16:52 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 03/22/21 16:52 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 03/22/21 16:52 75-71-80.50 1 1,1-Dichloroethane ND ug/L 03/22/21 16:52 75-34-30.50 1 1,2-Dichloroethane ND ug/L 03/22/21 16:52 107-06-20.50 1 1,1-Dichloroethene ND ug/L 03/22/21 16:52 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 03/22/21 16:52 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 03/22/21 16:52 156-60-50.50 1 1,2-Dichloropropane ND ug/L 03/22/21 16:52 78-87-50.50 1 1,3-Dichloropropane ND ug/L 03/22/21 16:52 142-28-90.50 1 2,2-Dichloropropane ND ug/L 03/22/21 16:52 594-20-70.50 1 1,1-Dichloropropene ND ug/L 03/22/21 16:52 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 03/22/21 16:52 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 03/22/21 16:52 10061-02-60.50 1 Diisopropyl ether ND ug/L 03/22/21 16:52 108-20-30.50 1 Ethylbenzene ND ug/L 03/22/21 16:52 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 23 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-8 Lab ID:92527951007 Collected:03/16/21 12:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 03/22/21 16:52 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 03/22/21 16:52 98-82-80.50 1 Methylene Chloride ND ug/L 03/22/21 16:52 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 03/22/21 16:52 1634-04-40.50 1 Naphthalene ND ug/L 03/22/21 16:52 91-20-32.0 1 n-Propylbenzene ND ug/L 03/22/21 16:52 103-65-10.50 1 Styrene ND ug/L 03/22/21 16:52 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 03/22/21 16:52 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 03/22/21 16:52 79-34-50.50 1 Tetrachloroethene ND ug/L 03/22/21 16:52 127-18-40.50 1 Toluene ND ug/L 03/22/21 16:52 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 03/22/21 16:52 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 03/22/21 16:52 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 03/22/21 16:52 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 03/22/21 16:52 79-00-50.50 1 Trichloroethene ND ug/L 03/22/21 16:52 79-01-60.50 1 Trichlorofluoromethane ND ug/L 03/22/21 16:52 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 03/22/21 16:52 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 03/22/21 16:52 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 03/22/21 16:52 108-67-80.50 1 Vinyl chloride ND ug/L 03/22/21 16:52 75-01-41.0 1 m&p-Xylene ND ug/L 03/22/21 16:52 179601-23-11.0 1 o-Xylene ND ug/L 03/22/21 16:52 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)97 %03/22/21 16:52 17060-07-070-130 1 4-Bromofluorobenzene (S)94 %03/22/21 16:52 460-00-470-130 1 Toluene-d8 (S)100 %03/22/21 16:52 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.9 Std. Units 03/21/21 16:19 D6,H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 21.8 mg/L 03/18/21 12:45 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 03/18/21 13:25 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 03/20/21 05:50 7727-37-903/19/21 18:000.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 24 of 53 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Sample:MW-8 Lab ID:92527951007 Collected:03/16/21 12:15 Received:03/16/21 14:57 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 2.4 mg/L 03/17/21 00:390.040 1 Nitrogen, Nitrate 2.4 mg/L 03/17/21 00:39 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 03/17/21 00:39 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 25 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 607811 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 200.7 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3202062 Associated Lab Samples:92527951001 Matrix:Water Analyzed Arsenic ug/L ND 10.0 03/21/21 21:03 Barium ug/L ND 5.0 03/21/21 21:03 Chromium ug/L ND 5.0 03/21/21 21:03 Iron ug/L ND 50.0 03/21/21 21:03 Lead ug/L ND 5.0 03/21/21 21:03 Manganese ug/L ND 5.0 03/21/21 21:03 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3202063LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 536500 107 85-115 Barium ug/L 527500 105 85-115 Chromium ug/L 513500 103 85-115 Iron ug/L 50605000 101 85-115 Lead ug/L 520500 104 85-115 Manganese ug/L 516500 103 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 3202064MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92526487001 3202065 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 110 70-130107 3500ND553535 Barium ug/L 500 104 70-130101 35000.014 mg/L 535 519 Chromium ug/L 500 103 70-13099 4500ND514495 Iron ug/L 5000 100 70-130101 150000.42 mg/L 5440 5480 Lead ug/L 500 103 70-130100 2500ND515503 Manganese ug/L 500 102 70-13099 35000.056 mg/L 567 552 Parameter Units MS Result % Rec Limits Qual% RecConc. 3202066MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527398003 3202067 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 101 70-130114 13500ND503570 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 26 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3202066MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527398003 3202067 MSD Result MSD % Rec RPD MSDMS Spike Conc. Barium ug/L 500 90 70-130101 9500170618674 Chromium ug/L 500 87 70-13095 8500ND445483 Iron ug/L 5000 92 70-130101 105000ND47305220 Lead ug/L 500 84 70-13083 1500ND440437 Manganese ug/L 500 86 70-13096 10500ND432480 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 27 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608097 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 200.7 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3203539 Associated Lab Samples:92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Matrix:Water Analyzed Arsenic ug/L ND 10.0 03/23/21 08:57 Barium ug/L ND 5.0 03/23/21 08:57 Chromium ug/L ND 5.0 03/23/21 08:57 Iron ug/L ND 50.0 03/23/21 08:57 Lead ug/L ND 5.0 03/23/21 08:57 Manganese ug/L ND 5.0 03/23/21 08:57 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3203540LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 526500 105 85-115 Barium ug/L 512500 102 85-115 Chromium ug/L 483500 97 85-115 Iron ug/L 48305000 97 85-115 Lead ug/L 503500 101 85-115 Manganese ug/L 487500 97 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 3203541MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951002 3203542 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 104 70-130104 150016.4 535 538 Barium ug/L M1500-195 70-130-194 15001730757761 Chromium ug/L 500 91 70-13092 150022.8 478 482 Iron ug/L M15000-669 70-130-667 05000699003640036500 Lead ug/L 500 98 70-13098 05009.3 497 498 Manganese ug/L M150061870-130619 050071038003810 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 28 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 607693 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951004, 92527951005, 92527951006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3201474 Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951004, 92527951005, 92527951006 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/19/21 13:20 1,1,1-Trichloroethane ug/L ND 0.50 03/19/21 13:20 1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/19/21 13:20 1,1,2-Trichloroethane ug/L ND 0.50 03/19/21 13:20 1,1-Dichloroethane ug/L ND 0.50 03/19/21 13:20 1,1-Dichloroethene ug/L ND 0.50 03/19/21 13:20 1,1-Dichloropropene ug/L ND 0.50 03/19/21 13:20 1,2,3-Trichlorobenzene ug/L ND 2.0 03/19/21 13:20 1,2,3-Trichloropropane ug/L ND 0.50 03/19/21 13:20 1,2,4-Trichlorobenzene ug/L ND 2.0 03/19/21 13:20 1,2,4-Trimethylbenzene ug/L ND 0.50 03/19/21 13:20 1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/19/21 13:20 1,2-Dibromoethane (EDB)ug/L ND 0.50 03/19/21 13:20 1,2-Dichlorobenzene ug/L ND 0.50 03/19/21 13:20 1,2-Dichloroethane ug/L ND 0.50 03/19/21 13:20 1,2-Dichloropropane ug/L ND 0.50 03/19/21 13:20 1,3,5-Trimethylbenzene ug/L ND 0.50 03/19/21 13:20 1,3-Dichlorobenzene ug/L ND 0.50 03/19/21 13:20 1,3-Dichloropropane ug/L ND 0.50 03/19/21 13:20 1,4-Dichlorobenzene ug/L ND 0.50 03/19/21 13:20 2,2-Dichloropropane ug/L ND 0.50 03/19/21 13:20 2-Chlorotoluene ug/L ND 0.50 03/19/21 13:20 4-Chlorotoluene ug/L ND 0.50 03/19/21 13:20 Benzene ug/L ND 0.50 03/19/21 13:20 Bromobenzene ug/L ND 0.50 03/19/21 13:20 Bromochloromethane ug/L ND 0.50 03/19/21 13:20 Bromodichloromethane ug/L ND 0.50 03/19/21 13:20 Bromoform ug/L ND 0.50 03/19/21 13:20 Bromomethane ug/L ND 5.0 03/19/21 13:20 Carbon tetrachloride ug/L ND 0.50 03/19/21 13:20 Chlorobenzene ug/L ND 0.50 03/19/21 13:20 Chloroethane ug/L ND 1.0 03/19/21 13:20 Chloroform ug/L ND 0.50 03/19/21 13:20 Chloromethane ug/L ND 1.0 03/19/21 13:20 cis-1,2-Dichloroethene ug/L ND 0.50 03/19/21 13:20 cis-1,3-Dichloropropene ug/L ND 0.50 03/19/21 13:20 Dibromochloromethane ug/L ND 0.50 03/19/21 13:20 Dibromomethane ug/L ND 0.50 03/19/21 13:20 Dichlorodifluoromethane ug/L ND 0.50 03/19/21 13:20 Diisopropyl ether ug/L ND 0.50 03/19/21 13:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 29 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3201474 Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951004, 92527951005, 92527951006 Matrix:Water Analyzed Ethylbenzene ug/L ND 0.50 03/19/21 13:20 Hexachloro-1,3-butadiene ug/L ND 2.0 03/19/21 13:20 Isopropylbenzene (Cumene)ug/L ND 0.50 03/19/21 13:20 m&p-Xylene ug/L ND 1.0 03/19/21 13:20 Methyl-tert-butyl ether ug/L ND 0.50 03/19/21 13:20 Methylene Chloride ug/L ND 2.0 03/19/21 13:20 n-Butylbenzene ug/L ND 0.50 03/19/21 13:20 n-Propylbenzene ug/L ND 0.50 03/19/21 13:20 Naphthalene ug/L ND 2.0 03/19/21 13:20 o-Xylene ug/L ND 0.50 03/19/21 13:20 sec-Butylbenzene ug/L ND 0.50 03/19/21 13:20 Styrene ug/L ND 0.50 03/19/21 13:20 tert-Butylbenzene ug/L ND 0.50 03/19/21 13:20 Tetrachloroethene ug/L ND 0.50 03/19/21 13:20 Toluene ug/L ND 0.50 03/19/21 13:20 trans-1,2-Dichloroethene ug/L ND 0.50 03/19/21 13:20 trans-1,3-Dichloropropene ug/L ND 0.50 03/19/21 13:20 Trichloroethene ug/L ND 0.50 03/19/21 13:20 Trichlorofluoromethane ug/L ND 1.0 03/19/21 13:20 Vinyl chloride ug/L ND 1.0 03/19/21 13:20 1,2-Dichloroethane-d4 (S)%102 70-130 03/19/21 13:20 4-Bromofluorobenzene (S)%104 70-130 03/19/21 13:20 Toluene-d8 (S)%102 70-130 03/19/21 13:20 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3201475LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 54.250 108 60-140 1,1,1-Trichloroethane ug/L 50.050 100 60-140 1,1,2,2-Tetrachloroethane ug/L 53.750 107 60-140 1,1,2-Trichloroethane ug/L 53.450 107 60-140 1,1-Dichloroethane ug/L 48.550 97 60-140 1,1-Dichloroethene ug/L 51.050 102 60-140 1,1-Dichloropropene ug/L 51.650 103 60-140 1,2,3-Trichlorobenzene ug/L 53.050 106 60-140 1,2,3-Trichloropropane ug/L 53.450 107 60-140 1,2,4-Trichlorobenzene ug/L 52.450 105 60-140 1,2,4-Trimethylbenzene ug/L 50.650 101 60-140 1,2-Dibromo-3-chloropropane ug/L 51.650 103 60-140 1,2-Dibromoethane (EDB)ug/L 56.050 112 60-140 1,2-Dichlorobenzene ug/L 50.250 100 60-140 1,2-Dichloroethane ug/L 51.350 103 60-140 1,2-Dichloropropane ug/L 50.850 102 60-140 1,3,5-Trimethylbenzene ug/L 50.550 101 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 30 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3201475LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichlorobenzene ug/L 49.150 98 60-140 1,3-Dichloropropane ug/L 51.950 104 60-140 1,4-Dichlorobenzene ug/L 48.650 97 60-140 2,2-Dichloropropane ug/L 50.750 101 60-140 2-Chlorotoluene ug/L 49.350 99 60-140 4-Chlorotoluene ug/L 49.050 98 60-140 Benzene ug/L 49.850 100 60-140 Bromobenzene ug/L 48.550 97 60-140 Bromochloromethane ug/L 51.050 102 60-140 Bromodichloromethane ug/L 52.350 105 60-140 Bromoform ug/L 43.050 86 60-140 Bromomethane ug/L 40.150 80 60-140 Carbon tetrachloride ug/L 53.050 106 60-140 Chlorobenzene ug/L 50.750 101 60-140 Chloroethane ug/L 42.150 84 60-140 Chloroform ug/L 47.650 95 60-140 Chloromethane ug/L 36.250 72 60-140 cis-1,2-Dichloroethene ug/L 47.150 94 60-140 cis-1,3-Dichloropropene ug/L 54.250 108 60-140 Dibromochloromethane ug/L 54.350 109 60-140 Dibromomethane ug/L 53.450 107 60-140 Dichlorodifluoromethane ug/L 44.450 89 60-140 Diisopropyl ether ug/L 48.350 97 60-140 Ethylbenzene ug/L 50.450 101 60-140 Hexachloro-1,3-butadiene ug/L 50.350 101 60-140 Isopropylbenzene (Cumene)ug/L 52.350 105 60-140 m&p-Xylene ug/L 101100 101 60-140 Methyl-tert-butyl ether ug/L 50.150 100 60-140 Methylene Chloride ug/L 44.850 90 60-140 n-Butylbenzene ug/L 54.650 109 60-140 n-Propylbenzene ug/L 48.650 97 60-140 Naphthalene ug/L 50.550 101 60-140 o-Xylene ug/L 52.550 105 60-140 sec-Butylbenzene ug/L 49.750 99 60-140 Styrene ug/L 51.550 103 60-140 tert-Butylbenzene ug/L 41.050 82 60-140 Tetrachloroethene ug/L 50.750 101 60-140 Toluene ug/L 50.150 100 60-140 trans-1,2-Dichloroethene ug/L 48.850 98 60-140 trans-1,3-Dichloropropene ug/L 52.250 104 60-140 Trichloroethene ug/L 51.150 102 60-140 Trichlorofluoromethane ug/L 46.050 92 60-140 Vinyl chloride ug/L 41.550 83 60-140 1,2-Dichloroethane-d4 (S)%99 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 31 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3201476MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527515019 3201477 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 120 60-140109 1020ND24.0 21.7 1,1,1-Trichloroethane ug/L 20 126 60-140120 520ND25.2 23.9 1,1,2,2-Tetrachloroethane ug/L 20 117 60-140108 720ND23.3 21.7 1,1,2-Trichloroethane ug/L 20 122 60-140115 620ND24.5 22.9 1,1-Dichloroethane ug/L 20 122 60-140114 720ND24.4 22.8 1,1-Dichloroethene ug/L 20 132 60-140122 720ND26.3 24.4 1,1-Dichloropropene ug/L 20 127 60-140120 520ND25.3 24.0 1,2,3-Trichlorobenzene ug/L 20 100 60-140103 320ND20.0 20.6 1,2,3-Trichloropropane ug/L 20 121 60-140111 920ND24.2 22.2 1,2,4-Trichlorobenzene ug/L 20 103 60-140103 120ND20.6 20.5 1,2,4-Trimethylbenzene ug/L 20 107 60-140100 720ND21.3 20.0 1,2-Dibromo-3-chloropropane ug/L 20 114 60-140103 1120ND22.8 20.5 1,2-Dibromoethane (EDB)ug/L 20 120 60-140114 520ND23.9 22.8 1,2-Dichlorobenzene ug/L 20 102 60-14099 320ND20.4 19.8 1,2-Dichloroethane ug/L 20 128 60-140118 820ND25.5 23.7 1,2-Dichloropropane ug/L 20 118 60-140114 320ND23.5 22.8 1,3,5-Trimethylbenzene ug/L 20 107 60-140100 720ND21.5 20.0 1,3-Dichlorobenzene ug/L 20 107 60-14098 920ND21.4 19.6 1,3-Dichloropropane ug/L 20 116 60-140110 520ND23.2 22.0 1,4-Dichlorobenzene ug/L 20 101 60-14097 520ND20.3 19.4 2,2-Dichloropropane ug/L 20 128 60-140120 620ND25.6 24.1 2-Chlorotoluene ug/L 20 107 60-140100 720ND21.4 20.0 4-Chlorotoluene ug/L 20 102 60-14096 720ND20.5 19.2 Benzene ug/L 20 120 60-140113 620ND24.1 22.6 Bromobenzene ug/L 20 104 60-14097 720ND20.8 19.4 Bromochloromethane ug/L 20 126 60-140121 420ND25.2 24.3 Bromodichloromethane ug/L 20 117 60-140113 320ND23.5 22.7 Bromoform ug/L 20 101 60-14096 520ND20.2 19.1 Bromomethane ug/L 20 97 60-14094 320ND19.3 18.9 Carbon tetrachloride ug/L 20 129 60-140127 220ND25.9 25.4 Chlorobenzene ug/L 20 114 60-140106 820ND22.9 21.1 Chloroethane ug/L 20 124 60-140106 1520ND24.8 21.3 Chloroform ug/L 20 125 60-140117 720ND25.0 23.4 Chloromethane ug/L 20 88 60-14088 120ND17.5 17.6 cis-1,2-Dichloroethene ug/L 20 118 60-140114 420ND23.7 22.7 cis-1,3-Dichloropropene ug/L 20 122 60-140116 520ND24.5 23.2 Dibromochloromethane ug/L 20 119 60-140113 520ND23.8 22.5 Dibromomethane ug/L 20 120 60-140119 120ND24.1 23.8 Dichlorodifluoromethane ug/L 20 114 60-140107 620ND22.8 21.4 Diisopropyl ether ug/L 20 118 60-140109 820ND23.6 21.7 Ethylbenzene ug/L 20 111 60-140106 420ND22.1 21.3 Hexachloro-1,3-butadiene ug/L 20 109 60-140113 320ND21.8 22.5 Isopropylbenzene (Cumene)ug/L 20 114 60-140110 420ND22.8 21.9 m&p-Xylene ug/L 40 110 60-140106 440ND44.1 42.5 Methyl-tert-butyl ether ug/L 20 116 60-140108 720ND23.3 21.7 Methylene Chloride ug/L 20 116 60-140107 820ND23.2 21.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 32 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3201476MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527515019 3201477 MSD Result MSD % Rec RPD MSDMS Spike Conc. n-Butylbenzene ug/L 20 109 60-140109 120ND21.7 21.8 n-Propylbenzene ug/L 20 103 60-14098 520ND20.7 19.7 Naphthalene ug/L 20 98 60-14097 120ND19.6 19.5 o-Xylene ug/L 20 115 60-140108 720ND23.1 21.5 sec-Butylbenzene ug/L 20 108 60-140105 320ND21.5 20.9 Styrene ug/L 20 110 60-140104 620ND22.0 20.7 tert-Butylbenzene ug/L 20 89 60-14085 520ND17.8 17.0 Tetrachloroethene ug/L 20 110 60-140109 120ND22.0 21.7 Toluene ug/L 20 115 60-140111 420ND23.1 22.2 trans-1,2-Dichloroethene ug/L 20 125 60-140115 820ND24.9 23.0 trans-1,3-Dichloropropene ug/L 20 120 60-140111 720ND23.9 22.3 Trichloroethene ug/L 20 123 60-140115 720ND24.6 22.9 Trichlorofluoromethane ug/L 20 121 60-140115 420ND24.1 23.1 Vinyl chloride ug/L 20 106 60-140101 520ND21.1 20.2 1,2-Dichloroethane-d4 (S)%103 70-130104 4-Bromofluorobenzene (S)%100 70-130101 Toluene-d8 (S)%99 70-13099 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 33 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608218 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92527951007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3204139 Associated Lab Samples:92527951007 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/22/21 13:34 1,1,1-Trichloroethane ug/L ND 0.50 03/22/21 13:34 1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/22/21 13:34 1,1,2-Trichloroethane ug/L ND 0.50 03/22/21 13:34 1,1-Dichloroethane ug/L ND 0.50 03/22/21 13:34 1,1-Dichloroethene ug/L ND 0.50 03/22/21 13:34 1,1-Dichloropropene ug/L ND 0.50 03/22/21 13:34 1,2,3-Trichlorobenzene ug/L ND 2.0 03/22/21 13:34 1,2,3-Trichloropropane ug/L ND 0.50 03/22/21 13:34 1,2,4-Trichlorobenzene ug/L ND 2.0 03/22/21 13:34 1,2,4-Trimethylbenzene ug/L ND 0.50 03/22/21 13:34 1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/22/21 13:34 1,2-Dibromoethane (EDB)ug/L ND 0.50 03/22/21 13:34 1,2-Dichlorobenzene ug/L ND 0.50 03/22/21 13:34 1,2-Dichloroethane ug/L ND 0.50 03/22/21 13:34 1,2-Dichloropropane ug/L ND 0.50 03/22/21 13:34 1,3,5-Trimethylbenzene ug/L ND 0.50 03/22/21 13:34 1,3-Dichlorobenzene ug/L ND 0.50 03/22/21 13:34 1,3-Dichloropropane ug/L ND 0.50 03/22/21 13:34 1,4-Dichlorobenzene ug/L ND 0.50 03/22/21 13:34 2,2-Dichloropropane ug/L ND 0.50 03/22/21 13:34 2-Chlorotoluene ug/L ND 0.50 03/22/21 13:34 4-Chlorotoluene ug/L ND 0.50 03/22/21 13:34 Benzene ug/L ND 0.50 03/22/21 13:34 Bromobenzene ug/L ND 0.50 03/22/21 13:34 Bromochloromethane ug/L ND 0.50 03/22/21 13:34 Bromodichloromethane ug/L ND 0.50 03/22/21 13:34 Bromoform ug/L ND 0.50 03/22/21 13:34 Bromomethane ug/L ND 5.0 03/22/21 13:34 Carbon tetrachloride ug/L ND 0.50 03/22/21 13:34 Chlorobenzene ug/L ND 0.50 03/22/21 13:34 Chloroethane ug/L ND 1.0 03/22/21 13:34 Chloroform ug/L ND 0.50 03/22/21 13:34 Chloromethane ug/L ND 1.0 03/22/21 13:34 cis-1,2-Dichloroethene ug/L ND 0.50 03/22/21 13:34 cis-1,3-Dichloropropene ug/L ND 0.50 03/22/21 13:34 Dibromochloromethane ug/L ND 0.50 03/22/21 13:34 Dibromomethane ug/L ND 0.50 03/22/21 13:34 Dichlorodifluoromethane ug/L ND 0.50 03/22/21 13:34 Diisopropyl ether ug/L ND 0.50 03/22/21 13:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 34 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3204139 Associated Lab Samples:92527951007 Matrix:Water Analyzed Ethylbenzene ug/L ND 0.50 03/22/21 13:34 Hexachloro-1,3-butadiene ug/L ND 2.0 03/22/21 13:34 Isopropylbenzene (Cumene)ug/L ND 0.50 03/22/21 13:34 m&p-Xylene ug/L ND 1.0 03/22/21 13:34 Methyl-tert-butyl ether ug/L ND 0.50 03/22/21 13:34 Methylene Chloride ug/L ND 2.0 03/22/21 13:34 n-Butylbenzene ug/L ND 0.50 03/22/21 13:34 n-Propylbenzene ug/L ND 0.50 03/22/21 13:34 Naphthalene ug/L ND 2.0 03/22/21 13:34 o-Xylene ug/L ND 0.50 03/22/21 13:34 sec-Butylbenzene ug/L ND 0.50 03/22/21 13:34 Styrene ug/L ND 0.50 03/22/21 13:34 tert-Butylbenzene ug/L ND 0.50 03/22/21 13:34 Tetrachloroethene ug/L ND 0.50 03/22/21 13:34 Toluene ug/L ND 0.50 03/22/21 13:34 trans-1,2-Dichloroethene ug/L ND 0.50 03/22/21 13:34 trans-1,3-Dichloropropene ug/L ND 0.50 03/22/21 13:34 Trichloroethene ug/L ND 0.50 03/22/21 13:34 Trichlorofluoromethane ug/L ND 1.0 03/22/21 13:34 Vinyl chloride ug/L ND 1.0 03/22/21 13:34 1,2-Dichloroethane-d4 (S)%101 70-130 03/22/21 13:34 4-Bromofluorobenzene (S)%95 70-130 03/22/21 13:34 Toluene-d8 (S)%101 70-130 03/22/21 13:34 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3204140LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 47.450 95 60-140 1,1,1-Trichloroethane ug/L 44.750 89 60-140 1,1,2,2-Tetrachloroethane ug/L 45.150 90 60-140 1,1,2-Trichloroethane ug/L 46.450 93 60-140 1,1-Dichloroethane ug/L 43.550 87 60-140 1,1-Dichloroethene ug/L 46.350 93 60-140 1,1-Dichloropropene ug/L 45.350 91 60-140 1,2,3-Trichlorobenzene ug/L 49.450 99 60-140 1,2,3-Trichloropropane ug/L 46.450 93 60-140 1,2,4-Trichlorobenzene ug/L 50.450 101 60-140 1,2,4-Trimethylbenzene ug/L 46.350 93 60-140 1,2-Dibromo-3-chloropropane ug/L 48.350 97 60-140 1,2-Dibromoethane (EDB)ug/L 46.650 93 60-140 1,2-Dichlorobenzene ug/L 48.850 98 60-140 1,2-Dichloroethane ug/L 40.850 82 60-140 1,2-Dichloropropane ug/L 43.150 86 60-140 1,3,5-Trimethylbenzene ug/L 45.350 91 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 35 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3204140LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichlorobenzene ug/L 49.550 99 60-140 1,3-Dichloropropane ug/L 45.050 90 60-140 1,4-Dichlorobenzene ug/L 49.850 100 60-140 2,2-Dichloropropane ug/L 47.950 96 60-140 2-Chlorotoluene ug/L 45.850 92 60-140 4-Chlorotoluene ug/L 45.550 91 60-140 Benzene ug/L 45.250 90 60-140 Bromobenzene ug/L 46.350 93 60-140 Bromochloromethane ug/L 47.950 96 60-140 Bromodichloromethane ug/L 43.050 86 60-140 Bromoform ug/L 46.950 94 60-140 Bromomethane ug/L 47.450 95 60-140 Carbon tetrachloride ug/L 48.950 98 60-140 Chlorobenzene ug/L 48.350 97 60-140 Chloroethane ug/L 43.950 88 60-140 Chloroform ug/L 44.750 89 60-140 Chloromethane ug/L 39.250 78 60-140 cis-1,2-Dichloroethene ug/L 43.150 86 60-140 cis-1,3-Dichloropropene ug/L 46.250 92 60-140 Dibromochloromethane ug/L 48.350 97 60-140 Dibromomethane ug/L 48.650 97 60-140 Dichlorodifluoromethane ug/L 49.550 99 60-140 Diisopropyl ether ug/L 40.250 80 60-140 Ethylbenzene ug/L 47.250 94 60-140 Hexachloro-1,3-butadiene ug/L 48.150 96 60-140 Isopropylbenzene (Cumene)ug/L 48.650 97 60-140 m&p-Xylene ug/L 94.7100 95 60-140 Methyl-tert-butyl ether ug/L 43.850 88 60-140 Methylene Chloride ug/L 43.650 87 60-140 n-Butylbenzene ug/L 47.750 95 60-140 n-Propylbenzene ug/L 45.550 91 60-140 Naphthalene ug/L 49.550 99 60-140 o-Xylene ug/L 47.550 95 60-140 sec-Butylbenzene ug/L 47.050 94 60-140 Styrene ug/L 48.150 96 60-140 tert-Butylbenzene ug/L 39.150 78 60-140 Tetrachloroethene ug/L 48.550 97 60-140 Toluene ug/L 46.950 94 60-140 trans-1,2-Dichloroethene ug/L 44.650 89 60-140 trans-1,3-Dichloropropene ug/L 46.150 92 60-140 Trichloroethene ug/L 49.150 98 60-140 Trichlorofluoromethane ug/L 48.950 98 60-140 Vinyl chloride ug/L 43.950 88 60-140 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%97 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 36 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3204141MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92528108002 3204142 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 2000 98 60-14099 12000ND19601980 1,1,1-Trichloroethane ug/L 2000 92 60-14095 32000ND18401890 1,1,2,2-Tetrachloroethane ug/L 2000 92 60-14093 12000ND18401860 1,1,2-Trichloroethane ug/L 2000 95 60-14099 52000ND18901990 1,1-Dichloroethane ug/L 2000 89 60-14090 12000ND17801800 1,1-Dichloroethene ug/L 2000 96 60-140100 42000ND19202000 1,1-Dichloropropene ug/L 2000 93 60-14095 22000ND18601890 1,2,3-Trichlorobenzene ug/L 2000 89 60-14097 92000ND17801940 1,2,3-Trichloropropane ug/L 2000 95 60-14097 22000ND19101940 1,2,4-Trichlorobenzene ug/L 2000 95 60-14099 42000ND18901980 1,2,4-Trimethylbenzene ug/L 2000 95 60-14096 1200031122102240 1,2-Dibromo-3-chloropropane ug/L 2000 93 60-14096 42000ND18601930 1,2-Dibromoethane (EDB)ug/L 2000 93 60-14099 5200070.6 1940 2040 1,2-Dichlorobenzene ug/L 2000 97 60-14097 02000ND19401940 1,2-Dichloroethane ug/L 2000 81 60-14087 5200062922502370 1,2-Dichloropropane ug/L 2000 93 60-14094 22000ND18501890 1,3,5-Trimethylbenzene ug/L 2000 95 60-14096 1200013520302050 1,3-Dichlorobenzene ug/L 2000 100 60-140100 02000ND20002000 1,3-Dichloropropane ug/L 2000 93 60-14094 12000ND18601890 1,4-Dichlorobenzene ug/L 2000 100 60-140100 02000ND19901990 2,2-Dichloropropane ug/L 2000 88 60-14088 12000ND17501770 2-Chlorotoluene ug/L 2000 94 60-14094 02000ND18801880 4-Chlorotoluene ug/L 2000 93 60-14092 12000ND18601840 Benzene ug/L M120009560-140169 12200093301120012700 Bromobenzene ug/L 2000 96 60-14096 02000ND19101920 Bromochloromethane ug/L 2000 95 60-14099 42000ND19001980 Bromodichloromethane ug/L 2000 88 60-14092 42000ND17701840 Bromoform ug/L 2000 93 60-14095 22000ND18701900 Bromomethane ug/L 2000 87 60-140108 212000ND17502160 Carbon tetrachloride ug/L 2000 104 60-140108 42000ND20802170 Chlorobenzene ug/L 2000 101 60-140102 12000ND20302050 Chloroethane ug/L 2000 121 60-140121 02000ND24202410 Chloroform ug/L 2000 90 60-14091 22000ND17901820 Chloromethane ug/L 2000 77 60-14080 42000ND15401590 cis-1,2-Dichloroethene ug/L 2000 86 60-14087 22000ND17101750 cis-1,3-Dichloropropene ug/L 2000 94 60-14096 32000ND18701930 Dibromochloromethane ug/L 2000 96 60-14099 32000ND19301980 Dibromomethane ug/L 2000 101 60-140105 32000ND20202090 Dichlorodifluoromethane ug/L 2000 97 60-140102 42000ND19502030 Diisopropyl ether ug/L 2000 75 60-14090 92000169032003500 Ethylbenzene ug/L 2000 99 60-140102 3200024922302290 Hexachloro-1,3-butadiene ug/L 2000 96 60-140102 62000ND19302050 Isopropylbenzene (Cumene)ug/L 2000 102 60-140103 02000ND20502060 m&p-Xylene ug/L 4000 101 60-140105 34000119052205390 Methyl-tert-butyl ether ug/L 2000 83 60-14092 7200080624602640 Methylene Chloride ug/L 2000 84 60-14089 52000ND16801780 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 37 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3204141MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92528108002 3204142 MSD Result MSD % Rec RPD MSDMS Spike Conc. n-Butylbenzene ug/L 2000 97 60-14098 02000ND19501950 n-Propylbenzene ug/L 2000 96 60-14095 12000ND19201900 Naphthalene ug/L 2000 84 60-14094 102000ND18302030 o-Xylene ug/L 2000 99 60-140104 4200073227102810 sec-Butylbenzene ug/L 2000 100 60-140100 02000ND19901990 Styrene ug/L 2000 98 60-14099 12000ND19601980 tert-Butylbenzene ug/L 2000 84 60-14084 02000ND16801690 Tetrachloroethene ug/L 2000 103 60-140107 32000ND20702130 Toluene ug/L M120009860-140160 1220007830979011000 trans-1,2-Dichloroethene ug/L 2000 89 60-14094 52000ND17901880 trans-1,3-Dichloropropene ug/L 2000 91 60-14095 42000ND18301900 Trichloroethene ug/L 2000 107 60-140111 42000ND21302220 Trichlorofluoromethane ug/L 2000 122 60-140123 12000ND24402460 Vinyl chloride ug/L 2000 89 60-14091 22000ND17701810 1,2-Dichloroethane-d4 (S)%93 70-13095 4-Bromofluorobenzene (S)%96 70-13096 Toluene-d8 (S)%97 70-13099 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 38 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608062 SM 2540C-2011 SM 2540C-2011 2540C Total Dissolved Solids Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3203297 Associated Lab Samples:92527951002 Matrix:Water Analyzed Total Dissolved Solids mg/L ND 25.0 03/19/21 16:48 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3203298LABORATORY CONTROL SAMPLE: LCSSpike Total Dissolved Solids mg/L 260250 104 90-110 Parameter Units Dup Result QualifiersRPDResult 92527951002 3203299SAMPLE DUPLICATE: Total Dissolved Solids mg/L 355 3343 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 39 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608092 SM 4500-H+B-2011 SM 4500-H+B-2011 4500H+B pH Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Parameter Units Dup Result QualifiersRPDResult 92526593001 3203528SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 7.4 D6,H327.5 Parameter Units Dup Result QualifiersRPDResult 92527951007 3203529SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 6.4 D6,H366.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 40 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 607145 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 300.0 IC Anions Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3198588 Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Matrix:Water Analyzed Sulfate mg/L ND 1.0 03/18/21 09:24 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3198589LABORATORY CONTROL SAMPLE: LCSSpike Sulfate mg/L 51.550 103 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3198590MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951001 3198591 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 108 90-110110 2502.9 57.0 57.9 Parameter Units MS Result % Rec Limits Qual% RecConc. 3198592MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527960016 3198593 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 108 90-110109 1500.56J 54.4 55.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 41 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 607272 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 350.1 Ammonia Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951001, 92527951002, 92527951004, 92527951005, 92527951006, 92527951007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3199159 Associated Lab Samples:92527951001, 92527951002, 92527951004, 92527951005, 92527951006, 92527951007 Matrix:Water Analyzed Nitrogen, Ammonia mg/L ND 0.10 03/18/21 13:05 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3199160LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Ammonia mg/L 5.05 99 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3199161MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951001 3199162 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 94 90-11094 050.53 5.2 5.2 Parameter Units MS Result % Rec Limits Qual% RecConc. 3199163MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951002 3199164 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 98 90-11098 0514.6 19.5 19.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 42 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608126 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 350.1 Ammonia Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3203622 Associated Lab Samples:92527951003 Matrix:Water Analyzed Nitrogen, Ammonia mg/L ND 0.10 03/22/21 11:59 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3203623LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Ammonia mg/L 5.05 100 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3203624MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92528368001 3203625 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 99 90-11099 05ND5.0 5.0 Parameter Units MS Result % Rec Limits Qual% RecConc. 3203626MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92528368002 3203627 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 100 90-110100 05ND5.0 5.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 43 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608001 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 351.2 TKN Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3202841 Associated Lab Samples:92527951001 Matrix:Water Analyzed Nitrogen, Kjeldahl, Total mg/L ND 0.50 03/20/21 04:57 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3202842LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Kjeldahl, Total mg/L 10.610 106 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3202843MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527477001 3202844 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L 10 101 90-110104 2100.89 11.0 11.2 Parameter Units MS Result % Rec Limits Qual% RecConc. 3202845MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527556001 3202846 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11014490-110144 01030.3 44.7 44.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 44 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 608003 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 351.2 TKN Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3202864 Associated Lab Samples:92527951002, 92527951003, 92527951004, 92527951005, 92527951006, 92527951007 Matrix:Water Analyzed Nitrogen, Kjeldahl, Total mg/L ND 0.50 03/20/21 05:38 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3202865LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Kjeldahl, Total mg/L 9.110 91 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3202866MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951002 3202867 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11011190-110125 51014.6 25.7 27.1 Parameter Units MS Result % Rec Limits Qual% RecConc. 3202868MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951003 3202869 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11015590-110154 11011.0 26.5 26.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 45 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 607037 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrate + Nitrite, Unpres. Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951005, 92527951006, 92527951007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3198299 Associated Lab Samples:92527951001, 92527951002, 92527951003, 92527951005, 92527951006, 92527951007 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 03/17/21 00:09 Nitrogen, Nitrite mg/L ND 0.040 03/17/21 00:09 Nitrogen, NO2 plus NO3 mg/L ND 0.040 03/17/21 00:09 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3198300LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.51.5 103 90-110 Nitrogen, Nitrite mg/L 1.01 101 90-110 Nitrogen, NO2 plus NO3 mg/L 2.52.5 102 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3198301MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527712001 3198302 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 98 90-11098 01.5ND 1.5 1.5 Nitrogen, Nitrite mg/L 1 94 90-11094 010.25 1.2 1.2 Nitrogen, NO2 plus NO3 mg/L 2.5 100 90-11099 02.50.18 2.7 2.7 Parameter Units MS Result % Rec Limits Qual% RecConc. 3198303MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92528001006 3198304 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 99 90-11099 01.50.020J 1.5 1.5 Nitrogen, Nitrite mg/L 1 99 90-11098 011.9 1.9 Nitrogen, NO2 plus NO3 mg/L 2.5 99 90-11099 02.5 3.4 3.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 46 of 53 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 607038 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrate + Nitrite, Unpres. Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92527951004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3198305 Associated Lab Samples:92527951004 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 03/17/21 00:43 Nitrogen, Nitrite mg/L ND 0.040 03/17/21 00:43 Nitrogen, NO2 plus NO3 mg/L ND 0.040 03/17/21 00:43 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3198306LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.51.5 102 90-110 Nitrogen, Nitrite mg/L 0.981 98 90-110 Nitrogen, NO2 plus NO3 mg/L 2.52.5 101 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3198307MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92527951004 3198308 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 93 90-11093 01.5ND 1.4 1.4 Nitrogen, Nitrite mg/L M118990-11090 01ND0.91 0.91 Nitrogen, NO2 plus NO3 mg/L 2.5 91 90-11091 02.5ND 2.3 2.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 47 of 53 #=QL# QUALIFIERS Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS The precision between the sample and sample duplicate exceeded laboratory control limits.D6 Sample was received or analysis requested beyond the recognized method holding time.H3 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 48 of 53 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92527951001 607811 607845MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951002 608097 608106MW-2 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951003 608097 608106MW-3 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951004 608097 608106MW-4 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951005 608097 608106MW-6 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951006 608097 608106MW-7 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951007 608097 608106MW-8 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92527951001 607693MW-1 SM 6200B 92527951002 607693MW-2 SM 6200B 92527951003 607693MW-3 SM 6200B 92527951004 607693MW-4 SM 6200B 92527951005 607693MW-6 SM 6200B 92527951006 607693MW-7 SM 6200B 92527951007 608218MW-8 SM 6200B 92527951002 608062MW-2 SM 2540C-2011 92527951001 608092MW-1 SM 4500-H+B-2011 92527951002 608092MW-2 SM 4500-H+B-2011 92527951003 608092MW-3 SM 4500-H+B-2011 92527951004 608092MW-4 SM 4500-H+B-2011 92527951005 608092MW-6 SM 4500-H+B-2011 92527951006 608092MW-7 SM 4500-H+B-2011 92527951007 608092MW-8 SM 4500-H+B-2011 92527951001 607145MW-1 EPA 300.0 Rev 2.1 1993 92527951002 607145MW-2 EPA 300.0 Rev 2.1 1993 92527951003 607145MW-3 EPA 300.0 Rev 2.1 1993 92527951004 607145MW-4 EPA 300.0 Rev 2.1 1993 92527951005 607145MW-6 EPA 300.0 Rev 2.1 1993 92527951006 607145MW-7 EPA 300.0 Rev 2.1 1993 92527951007 607145MW-8 EPA 300.0 Rev 2.1 1993 92527951001 607272MW-1 EPA 350.1 Rev 2.0 1993 92527951002 607272MW-2 EPA 350.1 Rev 2.0 1993 92527951003 608126MW-3 EPA 350.1 Rev 2.0 1993 92527951004 607272MW-4 EPA 350.1 Rev 2.0 1993 92527951005 607272MW-6 EPA 350.1 Rev 2.0 1993 92527951006 607272MW-7 EPA 350.1 Rev 2.0 1993 92527951007 607272MW-8 EPA 350.1 Rev 2.0 1993 92527951001 608001 608220MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92527951002 608003 608221MW-2 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92527951003 608003 608221MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92527951004 608003 608221MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92527951005 608003 608221MW-6 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92527951006 608003 608221MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92527951007 608003 608221MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 49 of 53 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92527951 Blue Ridge Tissue Corp. Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92527951001 607037MW-1 EPA 353.2 Rev 2.0 1993 92527951002 607037MW-2 EPA 353.2 Rev 2.0 1993 92527951003 607037MW-3 EPA 353.2 Rev 2.0 1993 92527951004 607038MW-4 EPA 353.2 Rev 2.0 1993 92527951005 607037MW-6 EPA 353.2 Rev 2.0 1993 92527951006 607037MW-7 EPA 353.2 Rev 2.0 1993 92527951007 607037MW-8 EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 03/25/2021 08:35 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 50 of 53 Page 51 of 53 Page 52 of 53 Page 53 of 53